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0086 BAXTER ROAD - Health
. �, =� _ - z�; . '86�Baxter`�Road` - ��Hyannis :_ <, — --- .� :_ - -- - - , - .310 109` -- A i �, � ��, n '� � i J BENNETT ENVIRONMENTAL ASSOCIATES, INC. LICENSED SITE PROFESSIONALS,ENVIRONMENTAL SCIENTISTS,GEOLOGISTS,ENGINEERS 1573 Main Street,P.O.Box 1743 (508)896-1706 Brewster,MA 02631 fax(508)896-5109 LETTER OF TRANSMITTAL TO: DATE: JOB NUMBER: Ms Ruby Pierce and James Donohue 6/4/15 BEAI5-10764 27 Cedar Street Cambridge,MA 02140 REGARDING: 86 Baxter Road (Map 310,Parcel 109) Hyannis,MA SHIPPING METHOD: Regular Mail ❑X Pick Up ❑ Priority Mail ❑ Hand Deliver ❑ Express Mail ❑ Other ❑ Certified Mail ❑ Green Card/RR ❑ COPIES DATE DESCRIPTION 1 5/26/15 LETTER OF FINDINGS—LIMITED REMOVAL ACTION w/Supporting Documentation i For review and comment: ❑ For approval: ❑ As requested: ❑ For your use: ❑ REMARKS: cc:Cosmo Gallinaro,LSP—Common Sense Environmental(Insurers Consultant) Tom McKean,Director—Barnstable Public Health Division Timothy Lavelle,Hazardous Materials Specialist—Barnstable Public Health Division Thomas K.Lynch—Barnstable Town Administrator John Cosmo,Fire Prevention Officer—Barnstable Fire Department David Bennett,LSP—Bennett Environmental Associates FROM: John D.Tadema-Wielandt,Senior Environmental Scientist Project Manager/]r If enclosures are not as noted,kindly notify us at once BENNETTENVIRONMENTALAsSOCIATES, IkIC0 . LICENSED SITE PROFESSIONALS © ENVIRONMENTAL SCIENTISTS © GEOLOGISTS © ENGINEERS 1573 Main Street-P.O. Box 1743, Brewster, MA 02631 O 508-896-1706 B Fax 508-896-5109 www.benneft-ea.com BEA15-10764 May 26, 2015 Ms. Ruby Pierce and James Donohue 27 Cedar Street Cambridge,MA 02140 RE: LETTER OF FINDINGS—LIMITED REMOVAL ACTION 86 Baxter Road (Map 310, Parcel 109) Hyannis,MA Dear Ms. Pierce and.Mr. Donohue, Pursuant to our agreement dated April 3, 2015, BENNETT ENVIRONMENTAL ASSOCIATES, INC. (BEA) has prepared the following narrative as documenting environmental assessment and remedial response performance for the excavation and proper disposal of 13.08 tons of contaminated soils as associated with a minor release of fuel oil from an abandoned underground storage tank(UST)at the subject property. The following narrative and supporting documentation describe the conditions at the property and the measures taken in response to absolve significant impacts,consistent with the regulatory requirements set forth in the MA Contingency Plan(MCP), under 310 CMR 40.0318. BACKGROUND On April 1, 2014, BEA personnel were at the subject property as a Third Party Inspector (TPI)subcontracted by Tank Removal Services,LLC(TRS).to conduct soil certification at the time of UST removal as is the policy of the Barnstable Fire Department and as recently promulgated in the new UST regulations under 310 CMR 80.00.Upon arrival at the property,the 275-gallon,single- wall, steel UST had been uncovered, cut open and the contents removed. TRS personnel reported that 55-gallons of fuel oil had been removed from the tank by All & Inclusive Environmental via vac-truck and transported off-site under a Uniform Hazardous Waste Manifest. Hyannis Fire Department personnel(Lieutenant John Cosmo)were also on-site to witness the UST removal. The tank was subsequently removed from the ground and placed on the ground adjacent to the tank grave for inspection. Subsequent to removing the tank,wetness and stained soils were observed on the bottom of the tank at the southern end. Soil samples were then collected within the tank grave from the sidewall and bottom of hole areas for field screening with a photoionization detector(PID), The soil samples were screened by"jar headspace"method,as consistent with the MA DEP policy WSC-94- 400. PID readings from the soil samples collected from the tank grave reported organic'vapor readings from 2.5 ppmv in the northern sidewall sample(SW-N: 1-T)to 99 ppmv in the bottom of hole sample from the southern end of the tank grave(BOH-S: @T)indicating significant impact to soils in the area of the former tank. The operator was then instructed to dig to 5'bgs in the southern EMERGENCY SPILL RESPONSE & WASTE SITE CLEANUP © SITE ASSESSMENT A PERMITTING ® SEPTIC DESIGN&INSPECTION WATER SUPPLY DEVELOPMENT,OPERATION&MAINTENANCE © WASTEWATER TREATMENT,OPERATION&MAINTENANCE MAY 26,2015 PIERCE-DONOHUE:86 BAXTER RD.-HYANNISBEAI5-10764 PAGE 2 OF 6 LIMITED REMOVAL ACTION-LETTER OF FINDINGS end of the tank grave where another soil sample(BOH-E @ 5')was collected. The sample was then screened in the field with a PID,with a result of 62 ppmv,confirming significantly impacted soils. In an attempt to determine the vertical extent of significant soil impact, a hand boring was performed in the southern end of the tank grave with a 3-inch stainless-steel bucket auger. Two-foot composite soil samples were performed from 5-7'(15.5 ppmv)and 7-9'(6.8 ppm),where refusal was encountered,due to a rock.'Based on the decreasing PID readings,the vertical extent of impact had apparently been defined as within 7-9' of grade within an estimated 6' x 6' area. The HB-1: 5-7 sample and the HB-1: 7-9'sample were then submitted to Alpha Analytical laboratory for extractable petroleum hydrocarbon (EPH) with polycyclic aromatic hydrocarbon (PAH) analysis and volatile petroleum hydrocarbons(VPH)with target BTEX analytes. A composite sample from the tank grave was also submitted for EPH analysis for the purpose of disposal characterization. The area of impact was then covered against rainfall infiltration. Analytical results for the soil samples submitted were received on April 10, 2015. The results reported concentrations of Fractional EPH/PAHs and VPH/BTEX below the applicable RCS- 1 Standards in the HB-1: 5-7 sample. Concentrations of EPH/PAH and VPH/BTEX were reported as non-detect in the HB-1: 7-9' sample,indicating a depth of significant impact at approximately 7' bgs. The Contaminated Stockpile sample did report concentrations of fractional C9 to C18 Aliphatics above the RCS-1 Standards. A summary of the analytical results is provided below in Table 1. MAY 26,2015 PIERCE-DONOHUE:86 BAXTER RD.-HYANNISBEAI5-10764 PAGE 3 OF 6 LIMITED REMOVAL ACTION-LETTER OF FINDINGS Table 1: Sample Results Compared to Reportable Concentrations RCS-1 Criteria Residence -86 Baxter Road-Hyannis,MA CONTAM. CLIENT SAMPLE ID STOCKPILE COMP. HB-1:5-7' BB-I:7-9' SAMPLING DATE 01-APR-15 01-APR-15 01-APR-15 LAB SAMPLE ID L1506663-01 L1506663-02 L1506663-03 RCS-1-14 Units Volatile Petroleum Hydrocarbons Benzene 2 mg/kg NA ND(<0.279) ND.(<0.141) C5-C8 Aliphatics mg/kg NA ND(<6.98) ND(<3.52) C5-C8 Aliphatics,Adjusted 100 mg/kg NA ND(<6.98) ND(<3.52) C9-Cl0 Aromatics 100 mg/kg NA 7.09 ND(<3.52) C9-C12 Aliphatics mg/kg NA 12.9 ND(<3.52) C9-C12 Aliphatics,Adjusted 1000 mg/kg NA ND(<6.98) ND(<3.52) Ethylbenzene 40 mg/kg NA ND(<0.279) . 1, (<0.141) Methyl tert butyl ether 0.1 mg/kg NA �0.14: ND(<0.07) Naphthalene 4 mg/kg NA ND(<0.559) ND(<0.281) o-Xylene 100 mg/kg NA ND(<0.279) ND(<O.141) p/m-Xylene 100 mg/kg NA ND(<0.279) ND(<0.141) Toluene 30 m NA ND <0.279 ND <O.141 Extractable Petroleum H}1drocarbons, _ 2-Methylnaphthalene 0.7.. mg/kg ND(<1.82) �^ ND(<0.658) ND(<0.336) Acenaphthene 4 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) Acenaphthylene 1 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) Anthracene 1000 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) Benzo(a)anthracene 7 mg/kg ND(<I.82) ND(<0.658) ND(<0.336) Benzo(a)pyrene 2 mg/kg. ND(<1.82) ND(<0.658) ND(<0.336). Benzo(b)fluoranthene 7 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) Benzo(ghi)perylene 1000 mg/kg ND(<1.82) ND(<0.658) ND.(<0.336) Benzo(k)fluoranthene 70 mg/kg ND.(<1.82) ND(<0.658) ND(<0.336) CI I-C22 Aromatics mg/kg 893 434 ND(<6.73) C11-C22 Aromatics,Adjusted 1000 mg/kg 893 434 ND(<6.73) C19-C36 Aliphatics 3000 mg/kg 664 325 ND(<6.73) C9-C18 Aliphatics 1000 mg/kg 1690 980 ND(<6.73) - - .. .. Chrysene 70 mg/kg ND(<1.82) _ ND(<0.658) ND(<0.336) Dibenzo(a,h)anthracene 0.7 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) Fluoranthene 100.0 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) Fluorene 1000 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) Indeno(1,2,3-cd)Pyrene 7 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) Naphthalene 4 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) Phenanthrene 10 mg/kg ND(<1.82) ND(<0.658) ND(<0.336) P rene 1000 m ND <1.82 ND <0.658 ND <0.336 Green shading indicates concentrations above the applicable RCS-1 Standards Gray shadin indicates where results were ND,but reporting concentrations were above the RCS-1 Standards. ENVIRONMENTAL ASSESSMENT/REMEDIAL RESPONSE BEA personnel returned to the Site on April 8,2015 to perform environmental assessment in MAY 26,2015 PIERCE-DONOHUE:86 BAXTER RD.-HYANNIS/BEAI5-10764 PAGE 4 OF 6 LIMITED REMOVAL ACTION-LETTER OF FINDINGS the area of the tank grave,in order to qualify the extent and magnitude of significant environmental impact. BEA personnel performed four hand borings outside the dwelling in the area of the former tank and two in the basement of the subject dwelling. Hand boring HB-2 was performed in the center of the tank grave to confirm the vertical extent of impact. Hand borings HB-3,HB-4 and HB- 5 were advanced south, north and west of the former tank, respectively, to determine the lateral extent of significant impact. Hand borings HB-6 and HB-7 were performed in the basement of the subject dwelling to determine if any impacted soils were present beneath the footprint of the house. Two-foot composite soil samples were collected with a 3" stainless steel bucket auger and screened in the field with a photoionization detector(PID)by j ar headspace method,consistent with the MA.DEP policy WSC-94-400. Results of the field screening reported concentrations of organic vapors ranging from 38.6 ppm in the HB-2: 3-5' sample to non-detect. Based on field screening results the extent of impact had been confirmed as within T of grade within an estimated 6'x T area, centered on the former tank location. The HB-2:9-10'sample was then sent to Alpha Analytical,for extractable petroleum hydrocarbon(EPH)with polycyclic aromatic hydrocarbon(PAH)analysis,to confirm the vertical extent of soil impact. The HB-6: 0-5'composite sample was also submitted for total petroleum hydrocarbon(TPH) analysis to confirm the lateral extent of petroleum impact. BEA personnel inspected the basement of the dwelling and did not observe a petroleum odor nor could they identify petroleum impacted soils on the basement floor. Photoionization readings in the living space and basement were recorded as Non-Detect(ND <0.2 ppmv). Results of the soil analyses,received on April 16,2015,reported concentrations of fractional EPH and target PAHs as non-detect in the HB-2: 9-10'sample. Similarly the HB-6: 0-5' composite - sample reported concentrations of TPH as non-detect. These results confirmed the lateral and vertical extent of significant impact in an approximate 6' x Tx T (D) area of significant impact. BEA returned to the subj ect property on May 6,2015,to direct petroleum contaminated soil removal as performed by Brundage Site Work of Wellfleet,M.A. BEA employed field screening by "jar headspace"method and Dexsil PetroFlag testing to direct the removal of approximately 9 cubic yards(13.08 tons)of contaminated soil from an approximate 10'x Tx 8'(D)area of impact. Based on the field screening of discrete end-point sidewall and bottom-of-hole samples, four discreet sidewall samples and a discrete bottom-of-hole sample were submitted for MA Certified analysis of EPH/PAHs and VPHBTEX concentrations. Laboratory analysis reported all EPH/PAH and VPHBTEX concentrations as Non-Detect (ND) in all samples submitted, wherein the reporting limits were less than the strictest applicable RCS-1 Reportable Concentrations and strictest S-1/GW- 1 —Method 1 —Risk Characterization standards. Contaminated soils totaling 13.08 tons were transported to Aggregate Industries in South Dennis,MA as a licensed asphalt batch facility for disposal/recycling. The final Bill of Lading with tare loads is included as an enclosure to this Letter of Findings to document appropriate remedial waste management. MAY 26,2015 PIERCE-DONOHUE:86 BAXTER RD.-HYANNISBEAI5-10764 PAGE 5 OF 6 LIMITED REMOVAL ACTION-LETTER OF FINDINGS RISK CHARACTERIZATION Results of the laboratory analysis, received May 14, 2015, reported all EPH/PAH and VPHBTEX concentrations in end-point soil samples collected from the extent of excavation as ND wherein the reporting limits were less than the strictest applicable RCS-1 Reportable Concentrations. The RCS-1 Reportable Concentrations are analogous to the strictest S-1 (GW-1), Method 1 Risk Characterization standards relied on in review of risk characterization. As such,all significant fuel oil impacts have been removed and there is no significant risk associated with residual petroleum hydrocarbon concentrations along the release area based on the analyses performed and reported results. CONCLUSIONS Significant fuel oil impact to soils was generated as result of an apparent minor release to the environment from an abandoned UST. Excavation operations resulted in the removal of some 9 cubic yards(13.08 tons)of fuel oil contaminated soils from the qualified area of release. End-point soil samples collected from the extent of soil removal reported all residual EPH/VPH and target analyte concentrations as ND wherein the reporting limits were less than the strictest applicable RCS-1 Reportable Concentrations. As such,based on the contaminated soil removal performed and MA Certified laboratory analytical results for end-point samples submitted,it is apparent that there is no significant risk to human health or to the environment, associated with the subject release given the testing performed. This data qualifies the efficacy of the LRA Completion,as consistent with the provisions of 310 CMR 40.0318,to support project closure and document regulatory compliance, wherein no Release Notification or Remedial Response liabilities remain under the provisions of 310 CMR 40.0000 as based upon the available data and regulations in effect at the time of this reporting. The findings of this investigation, as represented herein, document regulatory compliance with governing regulations and set forth the rationale and technical justification for project closure specific to the area of release. While these records are archived in your folder at our offices,you are required under the provisions of 310 CMR 40.0318(7)to maintain a copy of this Limited Removal Action Completion Statement for a minimum period of five(5)years. If you have any questions or need additional information,please contact me directly at your earliest convenience. Sincerely, B TT ENVIRQNMENT AL ASSOCIATES, INC. Jo)pr1 D. Tadema-Wielandt, Senior Environmental Scientist Project Manager MAY 26,2015 PIERCE-DONOHUE:86 BAXTER RD.-HYANNISBEAI5-10764 PAGE 6 OF 6 LIMITED REMOVAL ACTION-LETTER OF FINDINGS Encl. - Site Plan entitled "Limited Removal Action Completion..." prepared by BENNETT ENVIRONMENTAL ASSOCIATES, INC., dated 5/6/2015 -Bill of Lading (BWSC-112)to transport soil to facility -Aggregate Industries Soil Recycling Submittal -Al Soil Recycling Certificate -Bill of Lading(BWSC-112, A, B, log sheet) completion of shipment to recycling facility - Weight Slip - Laboratory Analytical Reports -Alpha Analytical -Lab#L1506663 (4/10/15) -Alpha Analytical-Lab #L1507116 (4/16/15) -Alpha Analytical—Lab #L1509831 (5/14/15) Cc. Cosmo Gallinaro, LSP—Common Sense Environmental (Insurers Consultant) Tom McKean, Director—Barnstable Public Health Division Timothy Lavelle, Hazardous Materials Specialist—Barnstable Public Health Division Thomas K. Lynch—Barnstable Town Administrator John Cosmo, Fire Prevention Officer—Barnstable Fire Department David Bennett, LSP—Bennett Environmental Associates I Massachusetts Department of Environmental Protection BWSC112 Bureau of Waste Site Cleanup i Release Tracking Number BILL OF LADING (pursuant to 310 CMR 40.0030) ❑Ll I A. LOCATION OF SITE OR DISPOSAL SITE WHERE REMEDIATION WASTE WAS GENERATED: 1. Release Name/Location Aid: Residential Property 2. Street Address: 86 Baxter Road 3. Cityrrown: Hyannis Zip Code: 02601-0000 ❑ 5. Check her if a Tier Classification Submittal has been provided to DEP for this disposal site: ❑ a. Tier 1A ❑ b. Tier 1 B ❑ b. Tier 1 C ❑ d. Tier II 6. If applicable provide the Permit Number: B. THIS FORM IS BEING USED TO:(check one: B1-64): ❑✓ 1. Submit a Bill of Lading(BOL)to transport Remediation Waste to Temporary Storage or a Receiving Facility. Response Actions associated with this BOL(check all that apply): ❑ a. Immediate Response Action(IRA) ❑ e.Comprehensive Response Actions ❑ b. Release Abatement Measure(RAM) f.. Limited Removal Action(LRA): (must be retained pursuant to 310 CMR ® c. Downgradient Property Status(DPS) 40.0034(6);can't be submitted via eDEP ❑ d. Utility Release Abatement Measure(URAM) ® g.Other ❑ 2. Submit an Attestation of Completion of Shipment to Temporary Storage(Sections C, F and J are not required): ❑ 3. Submit an Attestation of Completion of Shipment to a Receiving Facility(Sections C, F and J are not required): ❑ 4. Certify that Remediation Waste Was Not Shipped,and the Bill of Lading is Void. (Sections C, D, E, and F are not required) 5. Date Bill of Lading submitted to the Department: b.eDEP Transaction ID: (mm/dd/yyyy) 6. Period of Generation Associated with this Bill of Lading 04/20/2015 to 05/20/2015 (mm/dd/yyyy) (mm/dd/yyyy) (All sections of this transmittal form must be filled out unless otherwise noted) 4 The Bill of Lading is not considered complete until the Attestation of Completion of Shipment is received by the Department. C. DESCRIPTION OF WASTE AND WASTE SOUCE: 1. Contaminated Media/Debris(check all that apply): ❑✓ a. Soil ❑ b. Groundwater ❑ c. Surface Water ® d. Sediment ❑ e. Vegetation or Organic Debris f. Demolition/Construction Waste ❑ g. Inorganic Absorbent Materials ❑ h. Other. 2. Uncontainerized Waste(check all that apply): ❑ a. Inorganic Absorbent Materials ❑ b.Other: Revised:03/10/2010 V SAQI, Page 1 of 5 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC112 Release Tracking Number BILL OF LADING LLI (pursuant to 310 CMR 40.0030) ❑_ C. DESCRIPTION OF WASTE AND WASTE SOURCE (cont.): 3. Containerized Waste(check all that apply): ❑ a.Tank Bottoms/Sludges ❑ b.Containers ❑ c. Drums ❑ d. Engineered Impoundments ❑ e.Other: 4. Estimated Quantity: 50.00 ❑Tons FV Cu.Yds. ❑Gallons 5. Contaminant Source(check one): ❑ a.Transportation Accident ❑✓ b. Underground Storage Tank ❑ c. Brownfields Redevelopment ❑ d.Other: 6. Type of Contaminant(check all that apply): ❑ a. Gasoline ❑ b. Diesel Fuel ❑✓ c.#2 Fuel Oil ❑ d.#4 Fuel Oil ❑ e.#6 Fuel Oil ❑ f. Jet Fuel ❑ g.Waste Oil ❑ h. Kerosene ❑ i.Chlorinated Solvents ❑ j. Urban Fill ❑ k.Other: 7. Constituents of Concern(check all that apply): ® a.As ® b. Cd ❑ c.Cr ❑d. Pb ❑ e. Hg ❑✓ f. EPH/TPH ❑✓ g.VPH ❑ h. PCBs ❑ i.VOCs ❑j. SVOCs ❑ k. Other: 8. If applicable,check the box for the Reportable Concentration Category of the site: ❑✓ a. RCS-1 ❑ b. RCS-2 ❑✓ c. RCGW-1 ❑d. RCGW-2 9. Remediation Waste Characterization Documentation(check at least one): ❑✓ a.Site History Information Q b.Sampling Analytical Methods and Procedures ❑✓ c. Laboratory Data ❑✓ d. Field Screening Data ❑ e. Characterization Documentation previously submitted to the Department i. Date submitted: I ii.Type of Documentation:_ (mm/dd/yyyy) D.TRANSPORTER OR COMMON CARRIER INFORMATION: 1. Transporter/Common Carrier Name: Brundage Site Work 2. Contact First Name: Corey 3. Last Name: Brundage 4. Street: 1100 Old Chequessett Neck Road 5.Title: President 6. Cityrrown: Wellfleet 7. State: MA 8. Zip Code: 02667-0000 9.Telephone: (774)836-0012 10. Ext: 11. Fax: Revised:03/10/2010 Page 2 of 5 Massachusetts Department of Environmental Protection BWSC112 Bureau of Waste Site Cleanup Release Tracking Number LLI BILL OF LADING (pursuant to 310 CMR 40.0030) E.RECEIVING FACILITYITEMPORARY STORAGE LOCATION: 1. Operator/Facility Name Aggregate Industries 2. Contact First Name:William 3. Last Name: Reinhardt 4. Street: 230 Great Western Road 15.Title: GM of Environmental Safety 6. Citylrown:I South Dennis 7. State: MA 8. Zip Code: 02660-0000 9.Telephone: (781) 341-5500 10. Ext:E1 11. Fax: (781) 341-2440 12. Type of Facility:(Check one) a. Temporary Storage i. Period of Temporary Storage: to l mm/dd/ y mm/dd/yy y ii. Reason for Temporary Storage: Q✓ b. Asphalt Batch/Hot Mix ® c. Landfill/Disposal d. Landfill/Structural Fill e. Landfill/Daily Cover a f. Asphalt Batch/Cold Mix ❑ g. Thermal Processing h. Incinerator ❑ i. Other: 13. Division of Hazardous Waste/Class A Permit Number: S-01-027 14. Division of Solid Waste Permit Number: 15. EPA Identification Number: MAD985286384 F.LSP SIGNATURE AND STAMP: I attest under the pains and penalties of perjury that I have personally examined and am familiar with this submittal form, including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of(i)the standard of care in 309 CMR 4.02(1), (ii)the applicable provisions of 309 CMR 4.02(2)and(3),and 309 CMR 4.03(2), and(iii)the provisions of 309 CMR 4.03(3),to the best of my knowledge,information and belief,the assessment action(s)undertaken to characterize the Remediation Waste which is(are)the subject of this submittal for acceptance at the facility identified in this submittal comply with applicable provisions of 310 CMR 40.0000, and such facility is permitted to accept Remediation Waste having the characteristics described in this submittal. I am aware that significant penalties may result,including,but not limited to, possible fines and imprisonment, if I submit information which I know to be false, inaccurate or materially incomplete. I 1. LSP#: 14303 2. First Name: David 3. Last Name: Bennett (508) 896-1706 4.Telephone: 5. Ext. �c4 6. FAX: (508)89 -51 �� -AVIO `~ :d- :r. v C. B111`41,1E 7.Signature: }r Sao. s03 y` F; rSTE�r55U .' 8. Date: 9. LSP Stamp: ' ° rE PROF m/d /yyyy) ' '� Q %� Revised:03/10/2010 Page 3 of 5 Apr 2715 02:36p Cambridge Teachers FCU 617-492-0131 p.2 its►' G. PERSON SUHMIMNG BILL OF LADING: f. Ctink ar Coat¢w.f., —1 6.cnar3e In cortact r.;j.,m Caarm or e1?re'St ?n U C vlane porw . 2 PJa'rufafprgarora;m RcSidCr141s1 Pro�ray _.--'_ _.._ .__ _-- Lea.!r;. ,.UF erce Donohue owtrn _. ... _. Camb(fd a _..__. ...... _._ 7. city,Tawn:L_ •`A-- `.-- --�b. s:a•�: j� I q zv� [Defaa.oDOD _ t0 o 1:.Tct-_phwx:,(617)492.4712 y-I f rc _._. • ......__._..._.._. .._.... _ ._...___ � i f. Fax H.RMATtONSHIP TO SrM OF PERSON SUBUf1-RNG BILL OF LADING: oI j? twe t3 emrgA rP at•Y :� Rp u'PR,. Q a Ovne' v b.C+ae`a!w �f C GeretatOr J C T a�Sprrf- © e Other RP of PRP S,eze,.�� 2. Fs ub y,Stcuredterder a Ahn.ipalty+rrh Exe•ntl Stet Is(85 de`rxA by la G.L c21E.sTt 3. Agenryo:Pub;cUadyo. aRghtofVJay(andcGued4f1G.Le.21E,a*) 04. Pe(wnUrdr:aWagResparseicrio% SpocAyRetatonshlp I. REQUIRED ATTACHIAEMS AND SUBMITTALS: at, I:het):1»Ie Ir6M Re5p09a8f.Cti,�!r;5)on vf!iett DIA oPn•;rt rst153!.1,J8^!.are 1' Y')b.fb"to ef;orS?�;s;• parrndfs)andbraNpa.aka��cdC%DEPwEPA.1!thobeci:cicoc6 t�ans _�as+�tex- dr5!)rg'x ePal'caN6 pravr'ocr�thwe3f. 1.. (�►ad Mm If��nm�glapbtc i•.Smrat:rr pror•acd o*i 1nis f:nrrs inco-rw.e A P-oxly amr= Sssec ^r�rs b rr- BYto:.tOCD�yyY_.rr�.Ls �-p 3, Ctr+C%herR toc8r.9j!9a'tt•A LSP�i91af:mnG nr'rg[frI r7titt±ria':3�t6,Bala A•+7 cla+lry-r�';,�-•e5 P,7i�ICa J. CERTIFI Ti H41,A U BtLL FUIOlNGa'csl ardor thn pa zs ar.i pcsu;es o pc.ue.U*ri aedarr :' tltt»fofa^rs1•: nlsined _eutmitl3lna.jSn•er erod67. ttratiift asad o�m i ' y 67xfi0a^;M.y y tp••hryo/Ctaaoe�irviamsis rrmedutcly ras w=be farow..a'r.'•s3 CRirfirrtiYran the rraleri3l IA(Ofm s!Gn colte'ftm in this subrri!lal is,IO the beY otcl a+raefedpe an peDer,tr.Ie, 1ha!I am(cuv aMoarro.to taafa7hs a to-«rho t m behaV al the er-Y bgsay ra=ponslr tx fM1i=bm tthe pa w�a ere'y an>Rase betteP Pds r:rart.�at n madP am a ruaae tna:t�erp t+m aigrt•!Ita If(>ef^ati es•HHY^rr�D:rw I Tcted to Poasibte Gres and Irrpns-encnl.for x lffu!'y sutti:nq hlse,,ra:c rratc,or mCnntp e r�Sar7w or 7 U Pro 3 law. pony Owner F y Rub Pierce — c. Donohue Wane al p?sCn or entity reoo' S. oil- Sexaj H) nrr'>d lYri: tte Se,l.031TWDt0 Pape a o.•5 Massachusetts Department of Environmental Protection BWSC112 Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 CMR 40.0030) Release Tracking Number F] �R J. CERTIFICATION OF PERSON SUBMITTING BILL OF LADING(cont.): ED 6.Check here if the address of the person providing certification is different from address recorded in Section H. 7. Street: 8. City/Town: 9. State: 10. Zip Code: 11.Telephone: 1 12. Ext 13. Fax: YOU ARE SUBJECT TO AN ANNUAL COMPLIANCE ASSURANCE FEE OF UP TO$10,000 PER BILLABLE YEAR FOR THIS DISPOSAL SITE.YOU MUST LEGIBLY COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE.IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Date Stamp(MassDEP USE ONLY): r Revised:-03/10/2010 Page 5 of 5 SOIL RECYCLING SUBMITTAL Revised 3/12/99 AGGREGATE INDUSTRIES Environmental Services .- 11 P11 Turnpike Street;Stoughton; MA 02072 TeL (781) 341=5500 _ Fax:(781)341-2440 Site Information: NAME Residential Property CONTACT Ruby Pierce STREET 86 Baxter Road PHONE CITY/TOWN Hyannis STATE/ZIP MA 02601 Generator Information: NAME Ruby Pierce CONTACT STREET 27 Cedar Street PHONE (617)492-4712 CITY/TOWN Cambridge STATE/ZIP MA 02140 Consultant Information: NAME Bennett Environmental Associates, Inc. CONTACT John Tadema-Wielandt STREET 1573 Main St./P.O. Box 1743 PHONE 508-896-1706 CITY/TOWN Brewster STATE/ZIP MA 02631 Estimated Soil Quantity: TONS 75 CUBIC YARDS 50 Soil Contaminants (gasoline,diesel fuel,motor oil,etc.) Virgin#2 fuel oil Analyses Performed (check all that apply) �✓ TPH ED As pH Reactivity(S,CN) PCBs Flash Cr Pb TCLP(metals)if required VOCs Cd Hg based on total levels other All the above tests Laboratory analytical Screening Data were performed lei data attached 1®I Attached Instrument Used and Constituents Found 99 ppmv on Mini-Rae 3000 Photoionization detector. Environmental Services.Revised 3/12/99. page 1 of 3 Apr 2715 02:36p Cambridge Teachers FCU 617-492-0131 p,1 Description/Source of Release: UST Corrosion on UST DATEOFRELEASE Historic OTHER,DESCRIBE Soil Description PHYSICAL DESCRIPTION(SAND,.GRAVEL.SILT,ETCJ Sand CLA551FICATION METHOD USCS' Check if the following materials are present(check all that apply) CLAY 0 CONSTRUCTION DEBRIS OTHER DELETERIOUS MATERIALS(PLEASE UST) COAL VEGITATIVE MATTER ASH Soil Characterization Methodology Sampling Method GRAB COMPOSITE 8 LASED .G.HE SAMPLES ACE SCREENED,VISUALLY CONTAMINATED) CONSTITUTESOFCONCERN Petroleum,No.2 Fuel oil Site History ElCHECK 1F EXTRA SHEETS ATTACHED CURRENT USE Residence PAST USE Resedgrice I,the generator,having used due diligence determined that there is no reason to suspect or believe thatthe petroleum contaminated soil has been impacted by any releases of oil or hazardous materials other than that of the known source or I have identified the additional oil and hazardous materials that are suspected or known to be present in the soil,in addition to those associated with the known release, including any anthropogenic contaminants. 1 I,the generator,realize that due diligence shall consisit of a search of information and.records reasonably available to the generator of the contaminated soil and sufficient to make the determination.Such records and information may include, but are not limmited to,those of the generator,location of generation(i.e.facility if not the generator),the Department's Bureau of Waste Site Cleanup and the municipality(i.e.Board of Health,Fire Department)within which the site is located. All samples for VC)C analysi ere collected according to DEP policy#99 445. SIGNATURE OF GENERAiO DATE oF GENERATOR-PRINTED NAME Ruby Pierce •�1 AGGREGATE Environmental Services.Revised 3112M. page 2 of 3 ■,ow+�xa A site diagram is required indicating any major structures or roads,excavation areas and stockpile locations. All sampling locations must be noted. 0 CHECK IF DIAGRAM ATTACHED Site Diagram NAME OF INDIVIDUAL PREPARING DIAGRAM: AGGREGATE Environmental Services(BTES/900)12/3/97.Revised 3/12/99. page.3 of 3 movaues AGGREGATE Aggregate Industries Phone 781-344-1100 INDUSTRIES Northeast Region Fax 781-341-5523 1101 Turnpike Street www.aggregate-us.com Stoughton,Massachusetts 02072 RECEIVED May 29,2015 John Tadema- Wielandt Bennett Env PO Box 1743 Brewster, Ma 02631 Re: Soil, Residence Baxter Rd Hyannis, Ma Release Tracking#LRA Recyclable soil from the above referenced project was last received at our facility May 6 ,2014. A total of 13.08 tons has been received from the project. I have since been advised that shipment is complete.I have attached a copy of the BOL,along with e-dep forms 112A_& 112B to close the BOL. Thank you for recycling with Aggregate Industries. Regards, William R. Reinhardt Iv anagei Delivering Value A member of the Holcim Group Massachusetts Department of Environmental Protection BWSC112 Bureau of Waste Site Cleanup Release Tracking Number BILL OF LADING (pursuant to 310 CMR 40.0030) ❑_ � A LLI I . A. LOCATION OF SITE OR DISPOSAL SITE WHERE REMEDIATION WASTE WAS GENERATED: 1. Release Name/Location Aid: Residential Property 2. Street Address: 86 Baxter Road 3. City/Town: JHyannis Zip Code: 02601-0000 ❑ 5. Check her if a Tier Classification Submittal has been provided to DEP for this disposal site: ❑ a. Tier 1A ❑ b. Tier 1 B ❑ b. Tier 1 C ❑ d. Tier II 6. If applicable provide the Permit Number: B. THIS FORM IS BEING USED TO:(check one: B1-64): ❑ 1. Submit a Bill of Lading(BOL)to transport Remediation Waste to Temporary Storage or a Receiving Facility. Response Actions associated with this BOL(check all that apply): ❑ a. Immediate Response Action(IRA) ❑ e.Comprehensive Response Actions ❑ b. Release Abatement Measure(RAM) ❑ f.. Limited Removal Action(LRA): (must be retained pursuant to 310 CMR ❑ c. Downgradient Property Status(DPS) 40.0034 6 ;can't be submitted via eDEP ❑ d. Utility Release Abatement Measure(URAM) ❑ g.Other ❑ 2. Submit an Attestation of Completion of Shipment to Temporary Storage(Sections C, F and J are not required): ✓❑ 3. Submit an Attestation of Completion of Shipment to a Receiving Facility(Sections C, F and J are not required): ❑ 4. Certify that Remediation Waste Was Not Shipped,and the Bill of Lading is Void. (Sections C, D, E,and F are not required) 5. Date Bill of Lading submitted to the Department: b.eDEP Transaction ID: (mm/dd/yyyy) 6. Period of Generation Associated with this Bill of Lading 04/20/2015 to 05/20/2015 (mm/dd/yyyy) (mm/dd/yyyy) (All sections of this transmittal form must be filled out unless otherwise noted) The Bill of Lading is not considered complete until the Attestation of Completion of Shipment is received by the Department. C. DESCRIPTION OF WASTE AND WASTE SOURCE: 1. Contaminated Media/Debris(check all that apply): ® ❑ c. Surface Water ❑ d. Sediment ® e. Vegetation or Organic Debris a. Soil ❑ b.Groundwater ® f. Demolition/Construction Waste ❑ g. Inorganic Absorbent Materials ❑ h. Other: 2. Uncontainerized Waste(check all that apply): ❑ a. Inorganic Absorbent Materials ❑ b.Other] Revised:03/10/2010 Page 1 of 5 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC112 Release Tracking Number LL11BILL OF LADING (pursuant to310CMR40.0030) ❑_ LR C. DESCRIPTION OF WASTE AND WASTE SOURCE (cont.): 3. Containerized Waste(check all that apply): ❑ a.Tank Bottoms/Sludges ❑ b.Containers ® c. Drums ❑ d. Engineered Impoundments ❑ e.Other] 1. 4. Estimated Quantity: ❑Tons ❑ Cu.Yds. []Gallons 5. Contaminant Source(check one): ® a.Transportation Accident ❑ b. Underground Storage Tank ® c. Brownfields Redevelopment ❑ d.Other: 6. Type of Contaminant(check all that apply): ❑ a. Gasoline ❑ b. Diesel Fuel ❑ c.#2 Fuel Oil ❑ d.#4 Fuel Oil ❑ e.#6 Fuel Oil ❑ f. Jet Fuel ❑ g.Waste Oil ❑ h. Kerosene ❑ i.Chlorinated Solvents ❑ j. Urban Fill ❑ k.Other: 7. Constituents of Concern(check all that apply): ® a.As ® b.Cd ❑ c.Cr ❑d. Pb ❑ e. Hg ❑ f. EPH/TPH ❑ g.VPH ❑ h. PCBs ❑ i.VOCs ❑j. SVOCs ❑ k.Other: 8. If applicable,check the box for the Reportable Concentration Category of the site: ❑ a. RCS-1 ❑ b. RCS-2 ❑ c. RCGW-1 ❑d. RCGW-2 ' 9. Remediation Waste Characterization Documentation(check at least one): ❑ a. Site History Information 0 b.Sampling Analytical Methods and Procedures ❑ c. Laboratory Data ❑ d. Field Screening Data ❑ e.Characterization Documentation previously submitted to the Department i. Date submitted: ii.Type of Documentation: (mm/dd/yyyy) D.TRANSPORTER OR COMMON CARRIER INFORMATION: 1. Transporter/Common Carrier Name: Brundage Site Work 2. Contact First Name: Icorey 3. Last Name: Brundage 4. Street: 1100 Old Chequessett Neck Road 5.Title: lPresident 6. City/Town: lWelifleet 7. State: MA 8. Zip Code: 02667-0000 9.Telephone: (774)836-0012 10. Ext: 11. Fax: Revised:03/10/2010 Page 2 of 5 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC112 Release Tracking Number BILL OF LADING (Pursuant to310 CMR40.0030) E.RECEIVING FACILITYITEMPORARY STORAGE LOCATION: ti 1. Operator/Facility Name Aggregate Industries 2. Contact First Name:William 3. Last Name: Reinhardt a. Street: 230 Great Western Road 5.Title: GM of Environmental Safety 6. Cityrrown:I South Dennis 7. State: MA 8. Zip Code: 02660-0000 9.Telephone: (781) 341-5500 10. Ext: 11. Fax: (781) 341-2440 12. Type of Facility: (Check one) a. Temporary Storage i. Period of Temporary Storage:�� to (mm/dd/yyyy) (mm/dd/yyy ) ii. Reason for Temporary Storage: ❑✓ b. Asphalt Batch/Hot Mix F-1 c. Landfill/Disposal d. Landfill/Structural Fill ❑ e. Landfill/Daily Cover F✓ f. Asphalt Batch/Cold Mix ® g. Thermal Processing ❑ h. Incinerator ® i. Other. 13. Division of Hazardous Waste/Class A Permit Number: S-01-027 14. Division of Solid Waste Permit Number: 15. EPA Identification Number: IMAD985286384 F.LSP SIGNATURE AND STAMP: I attest under the pains and penalties of perjury that I have personally examined and am familiar with this submittal form, including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of(i)the standard of care in 309 CMR 4.02(1), (ii)the applicable provisions of 309 CMR 4.02(2)and(3),and 309 CMR 4.03(2), and(iii)the provisions of 309 CMR 4.03(3),to the best of my knowledge,information and belief,the assessment action(s)undertaken to characterize the Remediation Waste which is(are)the subject of this submittal for acceptance at the facility identified in this submittal comply with applicable provisions of 310 CMR 40.0000, and such facility is permitted to accept Remediation Waste having the characteristics described in this submittal. I am aware that significant penalties may result,including,but not limited to, possible fines and imprisonment, if I submit information which I know to be false, inaccurate or materially incomplete. 1. LSP#: 2. First Name: 3. Last Name: 4.Telephone: 5. Ext. 6. FAX: 7. Signature: 8. Date: 9. LSP Stamp: (mm/dd/yyyy) Revised:03/10/2010 Page 3 of 5 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC112 Release Tracking Number BILL OF LADING(pursuant to310CMR40.0030) ILI I G. PERSON SUBMITTING BILL OF LADING: 1. Check all that apply: ® a.change in contact name ❑ b.Change of address ❑ c.change in person undertaking response actions 2. Name of Organization: Residential Property 3. Contact First Name:I Ruby 4. Last Name: Pierce 5. street:27 Cedar Street 16.Title: Property Owner 7. City/Town: Cambridge 18. State: MA 9. Zip Code: 22140-0000 10.Telephone: (617)492-4712 11. Ext 12. Fax: H. RELATIONSHIP TO SITE OF PERSON SUBMITTING BILL OF LADING: ® Check here to change relationship ❑✓ 1. RP or PRP: ✓❑ a. Owner ❑ b.Operator ❑ c.Generator ❑ d.Transporter ❑ e. Other RP or PRP Specify: ® 2. Fiduciary, Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E, s.2): ❑ 3. Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.50)) ❑ 4. Any Other person Undertaking Response Actions: Specify Relationship I. REQUIRED ATTACHMENTS AND SUBMITTALS: ❑ 1. Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order(s), permit(s)and/or approvals issued by DEP or EPA. If the box is checked,you must attach a statement identifying the applicable provisions thereof. ❑ 2. Check here if any non-updatable information provided on this form is incorrect,e.g. property address. Send corrections to BWSC.eDEP@state.ma.us ✓❑ 3. Check here to certify that the LSP Opinion containing the material facts,data,and other information is attached. J. CERTIFICATION OF PERSON SUBMITTING BILL OF LADING : 1.I, ,attest under the pains and penalties or perjury(i)that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that, based on my inquiry of those individuals immediately.responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true, accurate and complete,and(iii) that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. 1/the person or entity on whose behalf this submittal is made am/is aware that there are significant penalties, including, but not limited to, possible fines and imprisonment,for willfully submitting false, inaccurate,or incomplete information. 2. By: 3. Title: 4. For 5. Date: (Name of person or entity recorded in Section H) (mm/dd/yyyy) Revised:03/10/2010 Page 4 of 5 i Massachusetts Department of Environmental Protection BWSC112 Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 CMR 40.0030) Release Tracking Number FTUE] J. CERTIFICATION OF PERSON SUBMITTING BILL OF LADING(cont.): 0 6.Check here if the address of the person providing certification is different from address recorded in Section H. 7. Street: 8. City/Town: 9. State: 10. Zip Code: 11.Telephone: 12. Ext 13. Fax: YOU ARE SUBJECT TO AN ANNUAL COMPLIANCE ASSURANCE FEE OF UP TO$10,000 PER BILLABLE YEAR FOR THIS DISPOSAL SITE.YOU MUST LEGIBLY COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE.IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Date Stamp(MassDEP USE ONLY): i Revised:03/10/2010 Page 5 of 5 LlMassachusetts Department of Environmental Protection BWSC112A Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 CMR 40.0030) Release Tracking Number. r77771 SUMMARY OF SHIPMENT SHEET 1 OF A A. SUMMARY OF SHIPMENT(To be filled out by the receiving facility upon receipt of Remediation Waste): 1. Date of Shipment: 2. Date of Receipt: 3. Number of Loads Shipped: 4. Daily Volume Shipped: (mm/dd/yyyy) (mm/dd/yyyy) ❑yds3 PItons gals 5.Totals Recorded on this Summary of Shipment Sheet: B• ❑ Check here if additional BWSC112A BOL Summary Sheets are needed. Revised:03/10/2010 Page 1 of 1 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC112B Release Tracking Number BILL OF LADING(Pursuant to310CMR40.0030) ILI SUMMARY SHEET SIGNATURE PAGE � r A. ACKNOWLEDGE T IPT EMEDIATION WASTE AT RECEIVING FACILITY OR TEMPORARY STORAGE: 1.I, attest under the pains and penalties or perjury(i)that I have personally examined and am familiar with the information contained in this submittal, including any and all documents accompanying this transmittal form,(ii)that, based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true,accurate and complete,and(iii) that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. I/the person or entity on whose behalf this submittal is made am/is aware that there are significant penalties, including,but not limited to, possible fines and imprisonment,for willfully submitting false,inaccurate,or incomplete information. 2 By: William R. Reinhardt 3. Title: Mngr. Env.Srvcs. 4. For: lAggregate Ind. 5. Date: S ' Z 5 ` 1 5 (mm/dd/yyyy) 6. Date of Final Shipment associated with this Bill of Lading: 5-G - 1 (mm/dd/yyyy) B. ACKNOWLEDGEMENT OF SHIPMENT AND RECEIPT OF REMEDIATION WASTE BY PERSON CONDUCTING RESPONSE ACTIONS ASSOCIATED WITH THIS BILL OF LADING: 1.I, John T a d e ma—W i e 1 a n d t , attest under the pains and penalties or perjury(i)that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true,accurate and complete,and(iii) that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. I/the person or entity on w o e behal h' submittal is made am/is aware that there are significant penalties, including,but not limited to, possible fi d' ri At.-for willfully submitting false inaccurate or incompI roj ect .Manager 2. By: Ly. _ information 3. Title: 'E-n-V!-r7u n a s s o c 4. For Ruby Pierce Pro e ty Owner 5. Date:1 6/4/2015 (Name of person or entity recorded in Section G (mm/dd/yyyy) ❑ 6.Check here if the address of the person providing certification is different from address recorded in BWSC112 Section H. 7. Street: 8. City/Town: 9. State: 10. Zip Code: 11.Telephone: 12. Ext: 13. Ema' ❑ 14. Check here if attaching optional supporting documentation such as copies of Load Information Summary Sheets Revised:03/10/2010 Page 1 of 1 o I Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup I BILL OF LADING Transport Log Sheet I Release Tracking Number Page OF 1. LOAD INFORMATION: Si1t�fT ns o e esenttve: iReceiiing Fac T rary o�Repre ntative: Load 1: a Date of Shipment: Time of Shipment: >rI i +D` dAm Date of Receipt: !Time of Receipt: 5r (i t PM I -2�/5 EX PM Truck/Tractor Registration: Trailer Registration(if any): I�jj h_ /_ / ff 60M NON I Load S¢e(cu.yds. ons�. / s Load 2: Signature of Transporter Representative: i Receiving Facility/Temporary Storage Representative: I Date of Shipment:P Time of Shipment: I i Datejof Receipt: Time of Receipt: ❑ AM ❑ PM i ❑ AM ❑ PM I I Truck/Tractor Registration: Trailer Registration(if any): I I Load Size(cu.yds./tons): Load 3: Signature of Transporter Representative: I Receiving Facillty/Temporary Storage Representative: i I I i Date of Shipment: Time of Shipment: I i ❑ AM ❑ PM I Date o'f Receipt Time of Receipt: [—] AM ❑ PM Truck/Tractor Registration: Trailer Registration(if any): I Load!Size(cu.yds.Rons): ' I i Load 4: Signature of Transporter Representative: I Receiving Facility/Temporary Storage Representative: I i Date of Shipment: Time of Shipment: AM PM i Date of Receipt Time of Receipt: AM PM Truck/Tractor Registration: Trailer Registration(if any): I f I Load Size(cu.ydsJtons): Load 5: Signature of Transporter Representative: i Receiving Facilitylremporary Storage Representative: I I Date of Shipment: Time of Shipment: I Date of Receipt: Time of Receipt: AM PM O AM PM Truck/Tractor Registration: Trailer Registration(if any): I I Load Size(cu.yds./tons): I i Load 6: Signature of Transporter Representative: I Receiving Facility/Temporary Storage Representative: I I i Date of Shipment: Time of Shipment: i Date of Receipt Time of Receipt: E] AM PM I E] AM E] PM Truck/Tractor Registration: Trailer Registration(if any): I i Load Size(cu.yds./tons): I J. LOG SHEET VOLUME INFORMATION: Total Volume Recorded This Page(cu.yds./tons) ` Total Carried Forward(cu.yds./tons): Total Carried Forward and This Page(cu.yds./tons): 1/13/11 SCALE TICKET INQUIRY BEGIN DATE 5/6/2015 LOCATION D701 END DATE 5/6/2015 SELL/BUY/TRANS ALL SHIP/RECEIVE ALL Ticket Loc Date Time Customer Order Product Carrier Vehicle Qt 115,086,776 D701 5/6/2015 1:15:41AM BENNETT EN CONTAMINA CUSTOMER BRUNDAGE 3.08 Tickets 1 13.08 05/06/2015 3:05:44PM AGGREGATE INDUSTRIES NE REGION, INC. Serial No:04101515:26 IHA Y T I CAL i ANALYTICAL REPORT Lab Number: L1506663 Client: Bennett Environmental Associates 1573 Main Street Brewster, MA 02631 ATTN: David Bennett Phone: (508)896-1706 Project Name: PIERCE-DONAHUE Project Number: BEA15-10764 Report Date: 04/10/15 The original project report/data package is held by Alpha Analytical.This report/data package is paginated and should be reproduced only in its entirety.Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003).NJ NELAP(MA935),RI(LA000065),ME(MA00086),. PA.(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(1-2217),USDA(Permit #P-330-1.1-00240). Eight Walkup Drive,Westborough, MA 01581-1019 508-898-9220 (Fax) 508-898-9193 800-624-9220-www.alphalab.com Page 1 of 36 Serial_No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 I I Alpha Sample Collection Sample ID Client ID Matrix Location Date/Time Receive Date I L1506663-01 CONTAM. STOCKPILE COMP. SOIL 86 BAXTER RD. HYANNIS, MA 04/01/15 11:00 04/03/15 L1506663-02 HB-1: 5-7'- SOIL 86 BAXTER RD. HYANNIS, MA 04/01/15 11:15 04/03/15 L1506663-03 HB-1: 7-9' SOIL 86 BAXTER RD. HYANNIS, MA 04/01/15 11:30 04/03/15 I i I I i i i i I Page 2 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10.764 Report Dater 04/10/15 MADEP MCP Response Action Analytical Report Certification This form provides certifications for all samples performed by MCP methods. Please refer to the Sample Results and Container Information sections of this report for specification of MCP methods used for each analysis. The following questions pertain only to MCP Analytical Methods. An affirmative response to questions A through F is required for"Presumptive Certainty"status A Were all samples received in a condition consistent with those described on the Chain-of- YES Custody, properly preserved (including temperature) in the field or laboratory, and. prepared/analyzed within method holding times? B Were the analytical method(s) and all associated QC requirements specified in the selected YES CAM protocol(s)followed? C Were all required corrective actions and analytical response actions specified in the selected YES` CAM protocol(s) implemented for all identified performance standard non-conformances? D Does the laboratory report comply with all the reporting requirements specified in CAM VII A, YES "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data?" E a. VPH, EPH,.and APH Methods only: Was each method conducted without significant YES modifications ? Refer to the individual methods for a list of significant modifications). E b. APH and TO-15 Methods only:Was the complete analyte list reported for each method? N/A F Were all applicable CAM protocol QC and performance standard non-conformances identified YES and evaluated in a laboratory narrative(including all "No" responses to Questions A through E)? A response to questions G, H and I is required for"Presumptive Certainty"status G Were the reporting limits at or below all CAM reporting limits specified in the selected CAM NO protocol(s)? H Were all QC performance standards specified in the CAM protocol(s) achieved? NO I Were results reported for the complete analyte list specified in the selected CAM protocol(s)? YES For any questions answered "No", please refer to the case narrative section on the following page(s). Please note that sample matrix information is located in the Sample Results section of this report. tia Page 3 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC,for all NELAC accredited parameters.The data presented in this report is organized by parameter(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter.If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific% recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications.Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will be disposed after 3 business days from the date the project is completed. Please contact Client Services at 800-624-9220 with any questions. Page 4 of 36 �`� Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 Case Narrative(continued) MCP Related Narratives VPH fAttbd i 4 9 In reference to question G: �}p~�•l'a1 oc� fcJ�l l� L1506663-02 has elevated detection limits due to the dilution required by the elevated concentrations of non1 _ target compounds in the sample. One or more of the target analytes did not achieve the requested CAM Jp reporting limits. �1 In reference to question H: The surrogate recovery for L1506663-02 is outside the acceptance criteria for 2,5-dibromotoluene-fid (148%); however, the sample was not re-analyzed due to coelution with obvious interferences.A copy of the chromatogram is included as an attachment to this report. The results are not considered to be biased. EPH In reference to question G: L1506663-01 and -02: One or more of the target analytes did not achieve the requested CAM reporting limits. t, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: "`'U" ' Michelle M. Morris Title: Technical Director/Representative Date: 04/10/15 Page 5 of 36 —\"'°� Serial No:04101515:26 I ORGANICS Page 6 of 36 Serial No:04101515:26 PETROLEUM HYDROCARBONS Page 7 of 36 I Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS Lab ID: L1506663-01 D Date Collected: 04/01/15 11:00 Client ID: CONTAM. STOCKPILE COMP. Date Received: 04/03/15 Sample Location: 86 BAXTER RD. HYANNIS, MA - Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 98,EPH-04-1.1 Extraction Date: 04/08/15 01:46 Analytical Date: 04/10/15 00:04 Cleanup Method1: EPH-04-1 Analyst: SR Cleanup Date1: 04/09/15 Percent Solids: 90% Quality Control Information - Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbons-Westborough Lab - -- - - —'--� -- — — --_ - - -- - - - a C9-C18 Aliphatics 1690 mg/kg 36.5 — 5 C19-C36 Aliphatics 664 mg/kg 36.5 — 5 ._...._......- ---.._..... ....._._..—-- -— ------ — —...------------- --- ----- ----— --......_._.___...__.._.__.._.... —----------......--- ----._.._.__.... C11-C22 Aromatics 893 mg/kg 36.5 — 5 ----- ------._.._... -- ---------------._—..—.------------_—___—................ __._._—...----...------- C11-C22 Aromatics,Adjusted 893 mg/kg 36.5 — 5 ------.............._.._.—.._.....- ....-----...----._...._..--.._..---._.._......._....--- - - -........_..... ----._.___._..-- — _....._....__....._.._._..- --._.....--- —.._..........__..._.._..._..._...._. Naphthalene ND mg/kg 1.82 — 5 2-Methyinaphthalene ND mg/kg 1.82 — 5 --------...--.........................------......-----..... _.._. Acenaphthylene ND mg/kg 1.82 — 5 Acenaphthene -------------_-- -- ND-------------mg/kg 1.82 — — -- — 5 .._-......._._............_...._._....-....__._.............--...._.._....--.....__..._............................_......-...----.—....................__........_._._...__._.._.__.... - ...--...-----—— ....__._..__...._....................----..._...._.................._........................... Fluorene ND mg/kg 1.82 — 5 Phenanthrene ND mg/kg 1.82 — 5 ._._.......__...............__._.._._........._..—.-_.....----...._.....----......------........_.._.._._..- --------..._—.._..---..... .._...._.__..__...._.__._.._..._..------ -—_....._.__...--._..... --.... _ —_........_...... Anthracene ND mg/kg 1.82 — 5 _..._..--------------- ------------ -- ---------------- ----------- -------------- - --- ------------. Fluoranthene ND mg/kg 1.82 — 5 ...............................................-------._...._... -....._—..__...__._...----------------------——..-----._....— Pyrene ND mg/kg 1.82 — 5 Benzo(a)anthracene ND mg/kg 1.82 — 5 Chrysene ND mg/kg 1.82 — 5 —......... —..._._..__—_... Benzo(b)fluoranthene ND mg/kg 1.82 — 5 Benzo(k)fluoranthene _--- --- ND —�------- mg/kg �-_�-- 1.82 -----------5------ Benzo(a)pyrene ND mg/kg 1.82 — 5 ---............. — ..— — Indeno(1,2,3-cd)Pyrene ND mg/kg 1.82 — 5 ......... -....._...._.. .._......_..---.._........_ ......... -----.—._.-...........- --------- —._...._.........._._......_.._.._.... __-- — —.._...._..__.....__......_...- ..._.._._..---...._.._._.._...,...._..----..._........_...----..__....._._._._. Dibenzo(a,h)a nth racene ND mg/kg 1.82 — 5 —-------...— -—- ----- --- ------- --- ----------------------.._.._,.._.-----._._...------ --—........._. Benzo(ghi)perylene ND mg/kg 1.82 — 5 �L� FiA Page 8 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS Lab ID: L1506663-01 D Date Collected: 04/01/15 11:00 Client ID: CONTAM. STOCKPILE COMP. Date Received: 04/03/15 Sample Location: 86 BAXTER RD. HYANNIS, MA Field Prep: Not Specified Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbons=Westborough Lab Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 88 40-140 o-Terphenyl 54 40-140 2-Fluorobiphenyl 102 40-140 2-Bromonaphthalene 91 40-140 �L�L rFirl Page 9 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS Lab ID: L1506663-02 D Date Collected: 04/01/15 11:15 Client ID: HB-1: 5-7' Date Received: 04/03/15 Sample Location: 86 BAXTER-RD:HYANNIS, MA Field Prep: - Not Specified - Matrix: Soil Analytical Method: 100,VPH-04-1.1 Analytical Date: 04/08/15 00:01 Analyst: BS Percent Solids: 97% 'Quality Control Information, Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Were samples received in methanol? Covering the Soil Methanol ratio: 1:1 +/-25% Parameter Result Qualifier Units RL MDL Dilution Factor Volatlle.Petroleum Hydrocarbons-Westborough Lab C5-C8 Aliphatics ND mg/kg 6.98 — 2 C9-C12 Aliphatics 12.9 mg/kg 6.98 — 2 C9-C10 Aromatics 7.09 mg/kg 6.98 — 2 C5-C8 Aliphatics,Adjusted ND mg/kg 6.98 — 2 C9-C12 Aliphatics,Adjusted ND mg/kg 6.98 — 2 -- —._...---_— ._.__...... ..................... --- ---..__.... —_.._,_. ._.._._._.__...-- Benzene ND mg/kg 0.279 — 2 Toluene ND mg/kg 0.279 — 2 Ethylbenzene ND mg/kg 0.279 — 2 ._..._..._............ p/m-Xylene ND mg/kg 0.279 2 o-Xylene ND mg/kg 0.279 — 2 Methyl tert butyl ether ND mg/kg 0.140 — 2 __....-..... _. Naphthalene ND mg/kg 0.559 — 2 Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 111 70-130 2,5-Dibromotoluene-FID 148 Q 70-130 !1L HA Page 10 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 • Report Date: 04/10/15 SAMPLE RESULTS . Lab ID: L1506663-02 D Date Collected: 04/01/15 11:15 Client ID: HB-1: 5-7 Date Received: 04/03/15 Sample Location: 86 BAXTER RD. HYANNIS, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 98,EPH-04-1.1 Extraction Date: 04/08/15 01:46 Analytical Date: 04/09/15 20:54 Cleanup Method1: EPH-04-1 Analyst: SR Cleanup Date1: 04/09/15 Percent Solids: 97% Quality Control Information Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbons-Westborough.Lab iL C9-C18 Aliphatics 980 mg/kg 13.2 — 2 C19-C36 Aliphatics 325 mg/kg 13.2 — 2 C11-C22 Aromatics 434 mg/kg 13.2 — 2 ------------------- — ----.._ --- —------....... ------------------- ------------- ------_----- C11-C22 Aromatics,Adjusted 434 mg/kg_ --13.2— --__--_--- 2 — Naphthalene ND mg/kg 0.658 — 2 2-Methylnaphthalene ND mg/kg 0.658 — 2 Acenaphthylene ----- -------------Np-----�-----------mg/kg 0.658-------_----- 2 ----- Acenaphthene ND mg/kg 0.658 — 2 --..._...._.._._......,.—.._.............—--- -....-...........--- ...- -..__.._._.._._..._......__.._..._...__....._.........._.__.........- -.._..__....... ._........... --......._._._..__.,.--._..._._._.....----..._..--- -..._...------ ....._.. Fluorene ND mg/kg 0.658 — 2 Phenanthrene ND mg/kg 0.658 — 2 Anthracene ND mg/kg 0.658 — 2 Fluoranthene ND mg/kg 0.658 — 2 Pyrene ND mg/kg 0.658 — 2 ——_..._....... ........__.......-----._._...—._..-- —._.._.__......-----------...------,----------........._._.._.._._._._.. --------- -- ......---....--....— --.._._...._.... Benzo(a)anthracene ND mg/kg 0.658 — 2 Chrysene ND mg/kg 0.658 — 2 Benzo(b)fluoranthene ND mg/kg 0.658 — 2 Benzo(k)fluoranthene ND mg/kg 0.658 — 2 Benzo(a)pyrene ND mg/kg 0.658 — 2 --- ---- -------.._......_—.._....__....._._.__._....--- --....__..._..........._..__.._... --- ..... __.._..-----..._...--- ------._....--------.._....._.._...._._----- Indeno(1,2,3-cd)Pyrene ND mg/kg 0.658 — 2 _ -- - - ----—...._._._....._...._........---—..__...._.__._..... - —.... - ---.._._._..--- —._.... — --- ...__..... 9.9_ .—._..._....__..._..---....---- ._._.._...__....-- ----------...__.._ Dibenzo a,h anthracene ND mg/kg 0.658 — 2 Benzo(ghi)perylene ND mg/kg 0.658 — 2 Page 11 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS. Lab ID: L1506663-02 D Date Collected: 04/01/15 11:15 Client ID: HB-1: 5-T . . Date Received: t 04/03/15 Sample-Location: 86 BAXTER RD. HYANNIS, MA -`- "Field,Prep:� - _ Not-Specified Parameter Result Qualifier Units RL MDL Dilution Factor Extr tie Petroleum Hydrocarbons-Westborough k,.' .- - _:•l-'Ra.��' h: ^auil'd:23rt�if+.•,al• ..Sr rsr �'. 'nt- t, - _ ,s Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 70 40-140 o-Terphenyl 59 40-140 2-Fluorobiphenyl 102 40A40 2-Bromonaphthalene 80 40-140 Page 12 of 36 ' Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS Lab ID: L1506663-03 Date Collected: 04/01/15 11:30 Client ID: HB-1: 7-9' Date Received: 04/03/15 Sample Location: 86 BAXTER RD. HYANNIS, MA Field Prep: Not Specified Matrix: Soil Analytical Method: 100,VPH-04-1.1 Analytical Date: 04/08/15 13:49 Analyst: BS Percent Solids: 97% . Quality Control Information Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Were samples received in methanol? Covering the Soil Methanol ratio: 1.3:1 Parameter Result Qualifier Units RL MDL Dilution Factor Volatile Petroleum:Hydrocarbons-WestboroughLab C5-C8 Aliphatics ND mg/kg 3.52 - 1 --.-..-_P---.._.....---.---......__..._....-----.-.---__..._......_.__._.__....._------._.__—.._......_-_--------.._._.__.__.._....___............._.-__._._.....---.9__.g_.__....__..._.___..._._.._.._._......---.--.--...__..—_...__._......__..._.-_...__.._......_ C9-C12 Aliphatics; ND m /k 3.52 - 1 —.................-..._...__...----.._.—...---—-...---....---._..._._............._.... -..._.._.._.............._._._........-----...._.._,_......- - ....__._._..._..-- .....__.._..__.._... -._.._..... C9-C10 Aromatics ND mg/kg 3.52 • - 1 ............_...__._..__.._....__..._._............_....._._._..._..._._..._...._....._.._....-----..__...----— — — 05-C8 Aliphatics,Adjusted ND mg/kg 3.52 - 1 .._._..__....__..._..._................. _.__..._......._... ---...__..--._...- .,... C9-C12 Aliphatics,Adjusted ND mg/kg 3.52 - 1 --- -- -- - -- --- ----------------- _._.._.._..__..---------- - -...-----...-- ---- -.....----- ---..... - -----._.._..........-- -------------- Benzene ND mg/kg 0.141 - 1 -- ------- ----- -------- - -------- - -..--- --- ------ ---- - ----.................. -- ----------- Toluene ND mg/kg 0.141 - 1 Ethylbenzene ND mg/kg 0.141 - 1 .-...--------- ----- -- ----....--- -----...__......-- - - - --- -....----....__...._.._...-------.._._.._..--- p/m-Xylene ND mg/kg 0.141 - 1 o-Xylene ND mg/kg 0.141 - 1 -------._..._-...__._......_... -..__.......__..__._._...-------..__....- --....--- ---- - .._.. ------- ------------------ -- - Methyl tert butyl ether ND mg/kg. 0.070 - 1 ----...---- --._._..........._........-........-----------...---..__... ---...................._._.............__._...-..._._..__..._.............--....._...- .......__........__..__._._._._._._.....-_._..__._.......------------_-- ....__._...---- Naphthalene ND mg/kg 0.281 - 1 Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 109 70-130 2,5-Dibromotoluene-FID 114 70-130 1 i Page 13 of 36 i Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS Lab ID: L1506663-03 Date Collected: 04/01/15 11:30 Client ID: HB-1: 7-9' Date Received: 04/03/15 Sample•Location: 86 BAXTER RD-HYANNIS, MA _ Field Prep: "- Not Specified i Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 98,EPH-04-1.1 Extraction Date: 04/08/15 01:46 Analytical Date: 04/09/15 15:14 Cleanup Method1: . EPH-04-1 Analyst: SR Cleanup Date1: 04/09/15 Percent Solids: 97% Quality Control Information Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbons-Westborough Lab. :. C9-Cl8 Aliphatics ND mg/kg 6.73 - 1 C19-C36 Aliphatics ND mg/kg 6.73 - 1 C11-C22 Aromatics ND mg/kg 6.73 - 1 C11-C22 Aromatics,Adjusted ND mg/kg 6.73 - 1 Naphthalene ND mg/kg 0.336 - 1 ---- ------ .._.__.-..............._..---... -- -------------- -------—---------.._..--- __ --- -__ _ _- 2-Methylnaphthalene ' ND mg/kg 0.336 - 1 -._... --_-...-._.—_.__..........,_... --��-... -------------------------------------------- - Acenaphthylene ND mg/kg 0.336 - 1 ...-............._..._._.....__._._..__........._._....._..._........_---............_.. -...-- _-- - -- ----._... .....---..... _._._._._.,....------... .._.._.,- -._...._......._._._..........__._....._...._.._._..._..._. Acenaphthene ND mg/kg 0.336 - 1 --...._._....._................__._._.._........_......_.._..__....__...._.,.._ ..__.__..__..._.._._.._...._........ -.._..-----.........__.._...._..._ ......- ._...__._._....._ _..._.._.._._......_....._._... ----..................................._.........---......................... _.._.._... Fluorene ND mg/kg 0.336 -- 1 ...._,................................_....._..._..........................-........--....................-----.._._..._....._...._......--- _.._._._..---...__._...__... - ......_.._...__._.... -._.........._...._-__._......_........_....-.....----._..._----.._._....--_..._.._.__.._.._._.._...... Phenanthrene ND mg/kg 0.336 - 1 -......._._......_._.__._........_._.._.._.._._-..__... _.._..-- -..-----._._._.._._._._....----.._.....-- -------... -- -------..._ - -- ..-.-.-.....-................_._..._......................,.......................----..._._...... Anthracene ND mg/kg 0.336 - 1 -------..._..._................__._._._....._....._..._._._._..__,_....-- ---._._....--..._.._._........_...._...-- --.._._..._._._..--..._._........ -...- -...—_......_...._._..._._..._._._...__.._._.._...__-....-..._._.. . - Fluoranthene ND mg/kg 0.336 - 1 -----......._....---- ---.._.__....._.._.........-_-- --- --------- --- -.._.._..-_...--- _._.,- ---------- - _...- -..............-....... ---- - Pyrene ND mg/kg 0.336 - 1 -- ------_.....__------.._.._._-...__............-- .-_.-..-----.- - ------- -- ----- - .._.. _--- .......--..-_......._.............._.._ _......_..._.._-.__....._.__._. Benzo(a)anthracene ND mg/kg 0.336 - 1 Chrysene ND mg/kg 0.336 - 1 Benzo(b)fluoranthene ND mg/kg 0.336 - 1 iBenzo(k)fluoranthene ND mg/kg 0.336 - 1 Benzo(a)pyrene ND mg/kg 0.336 - 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.336 - 1 I Dibenzo(a,h)anthracene ND mg/kg 0.336 - 1 Be nzo(ghi)perylene ND mg/kg 0.336 - 1 i I Page 14 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS Lab ID: L1506663-03 Date Collected: 04/01/15 11:30 Client ID: HB-1: 74 Date Received: 04/03/15 Sample Location: 86 BAXTER RD. HYANNIS, MA Field Prep: Not Specified . Parameter Result Qualifier Units RL MDL Dilution Factor EzfitractaL7le Petro leum Hydrocarbons Westborough Lal � Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 68 40-140 o-Terphenyl 69 40-140 2-Fluorobiphenyl 81 40-140 2-Bromonaphthalene 73 40-140 ; s Page 15 of 36 I Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 Method Blank Analysis Batch Quality Control Analytical Method: 98,EPH-04-1.1 Extraction Method: EPA 3546 Analytical Date: 04/09/15 08:45 Extraction Date: 04/08/15 01:46 Analyst: SR Cleanup Method: EPH-04-1 Cleanup Date: 04/09/15 Parameter Result Qualifier units RL MDL Extractable Petroleum Hydrocarbons Westborough Lab for-sample(s): -01=03*'Batch:` WQ774197=1 C9-C18 Aliphatics ND mg/kg 6.51 -- _.....------- ---._...._._...__....-_..._._......_.....------------------.._._..-- ..._...- ---------- --._._.....__.._..._....__...-----.._......._...- - -._......._.._....... C19-C36 Aliphatics ND mg/kg 6.51 - C11-C22 Aromatics ND mg/kg 6.51 -- C11-C22 Aromatics,Adjusted ND mg/kg 6.51 - Naphthalene ND mg/kg 0.326 - 2-Methylnaphthalene ND mg/kg 0.326 - - Acenaphthylene ND mg/kg 0.326 - Acenaphthene ND mg/kg 0.326 -- Fluorene ND mg/kg 0.326 -- ----- --.._._.. ---------...----------- - -------- ---..__....------- - ..._.._....----......._.. --- Phenanthrene ND mg/kg 0.326 -- Anthracene ND mg/kg 0.326 -- Fluoranthene ND mg/kg 0.326 -- Pyrene - -------�------- ND ----- mgikg----0.326 ..------_--------- -- ----- -..-,_ --- —----.-...-- --- --_._...----------------- Benzo(a)anthracene ND mg/kg 0.326 - Chrysene ND mg/kg 0.326 - Benzo(b)fluoranthene ND mg/kg 0.326 -- - _--- _......._..----... _..__..__....... -...__......__................--._...--.._..------..-.._._...._..-- - -- --......._..._...__....__.._....._......_..._..._......_._-...... Benzo(k)fluoranthene ND mg/kg 0.326 -...._.,..----............_................-- ---...---._..._._..__....__._.._..._._..._...._....-- ._.-- -------._.-......_._...-..... --.._........-- - - Benzo(a)pyrene ND mg/kg 0.326 .._.......- ----._...------ -..---......_. -- -.......--...--._.._._.._.._._... Indeno(1,2,3-cd)Pyrene ND mg/kg 0.326 - Dibenzo(a,h)anthracene ND mg/kg 0.326 - Benzo(ghi)perylene ND mg/kg 0.326 -- Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 61 40-140 o-Terphenyl 92 40-140 2-Fluorobiphenyl 101 40-140 2-Bromonaphthalene 93 40-140 Page 16 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 Method Blank Analysis Batch Quality Control Analytical Method: 100,VPH-04-1.1 Analytical Date: 04/07/15 10:33 Analyst: BS Parameter Result Qualifier Units RL MDL Volatile Petroleum Hydrocarbons-'Westborough,Lab for sample(s): 02. ' Batch: WG774295-3 C5-C8 Aliphatics ND mg/kg 2.67 -- C9-C12 Aliphatics ND mg/kg 2.67 - C9-C10 Aromatics ND mg/kg 2.67 - ._.._...._.._..._._....----- - ... -------...__....- ----- - 05-C8 Aliphatics,Adjusted ND mg/kg 2.67 - C9-C12 Aliphatics,Adjusted ND mg/kg 2.67 -- -------._...._..._..- ---._......---...._..._._..__----- .._.._-_.....----- ----------...----._...__..._._...._.._...------- - --...... _....--- Benzene ND mg/kg 0.107 - Toluene --------�--------- ND --- mg/kg 0.107�----------------- Ethylbenzene ND mg/kg 0.107 - --- ----- ---...-- -------------._...._..._.._._..--- —- ---- .... _-- -- ---- p/m-Xylene ND mg/kg 0.107 -- o-Xylene ------.----- --Np--------- mg/kg 0.107 --------_----------- Methyl tert butyl ether— ND mg/kg 0.053 - Naphthalene ND mg/kg 0.213 - Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 88 70-130 2,5-Dibromotoluene-FID 92 70-130 - E Page 17 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 Method Blank Analysis Batch Quality Control Analytical Method: 100,VPH-04-1.1 Analytical Date: 04/08/15 10:12 Analyst: BS Parameter Result Qualifier units RL MDL Volatile Petroleum Hydrocarbons-Westborough Lab for sample(s): 03 Batch: WG774664-3- 05-C8 Aliphatics ND mg/kg 2.67 - C9-C12 Aliphatics ND mg/kg 2.67 -- C9-C10 Aromatics ND mg/kg 2.67 -- ........._._.....--..............._......-_.-1._.............---._.._....,.- -- - -- - ---..._..__...__...--... -..._..------ -.._..._--..-.-....—._......__...__-_._...--.....-- ..... --......_.. --..... C5-C8 Aliphatics,Adjusted ND mg/kg 2.67 - C9-C12 Aliphatics,Adjusted ND mg/kg 2.67 - Benzene ND mg/kg 0.107 -- Toluene ND mg/kg 0.107 -- Ethylbenzene ---- — ND _.— -- mg/kg 0.107 -----._..-----.___— p/m-Xylene ND mg/kg 0.107 - o-Xylene ND mg/kg 0.107 - Methyl tert butyl ether ND mg/kg 0.053 - �- Naphthalene ND mg/kg 0.213 -- Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 84 70-130 2,5-Dibromotoluene-FID 90 70-130 Page 18 of 36 Serial No:04101515:26 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits Extractable Petroleum-Hydrocarbons-Westborough Lab Associated sample(s): 01-03 Batch: WG774197-2 WG7,74197-3 C9-C18 Aliphatics _ _ __ _- r�88�� - 74 --__ - 40-140- - 17 _ __ 25 - C19-C36 Aliphatics_ _ �109"� �98� _ 40-140 11 25 C11-C22 Aromatics F-124-7 r-116-__J - '___40-140 F-7 _-- _ _-25 Naphthalene __ J_ 88"'� _ r -82--::] 40-140 ` 7 25 - 2'Methylnaphthalene _ 100 _ - -�"91�� - _ _40-140 - - 25 _ - - _Acenaphthylene „-_-- - - 97`-� rw86��. 40-140 ^_ 12 -- - -�_ 25 ---T-� Acenaphthene '-102i_^___ -90�__ ! _ 40-140 _ _F13� 25 Fluorene `_-�112'—'�.1 _r _100!� i 40-140 -_ 11 - 25 _Phenanthrene1_17� 108'��^^ - 40140 F �B�� _- 25 Anthracene _- � —130"!, —_ {'-120—� ` ` - -__40-140_ _- F-8� V- 25 - Fluoranthene 120 _- - J - 113T,___ _ 40-140- -- -r-fi� _ _ 25 Pyrene �'121�"-"� r 114-"�l 40-140 �6�, 25 Benzo(a)anthracene 114 f__108__-J ^' 40-140 �5 25 Chrysene _- ir--1237 _F-117 40-140 r^`5---1 - 25 Benzo(b)fluoranthene _ _^ [_124= T -�r-'-"-118�, s _ 40-140 - -_F_5"_J _- l _ ,25 _Benzo(k)fluoranthene_ F7.11677 r�11 7 _ 40-140 F-5 - ^25 -_ J Benzo(a)PYrene_- F-7117 _7 - _[' 712��y 40-140 _ r—'4— 1 _ 25 - Indeno(1,2,3-cd)Pyrene - _ 94'-� _ _ �""'90"��-- 40-140 - _r'�4� - 25 Dibenzo(a,h)anthracene _ 116� f_112 40-140 ^F-4'� 25 '- _Benzo(ghi)perylene r-115�� 111—� T 40-140 F 25 Nonane(C9) T -547-7 Y r^44�"� - _ 30-140 r__20'^i_ _ _ 25^-_- Page 19 of 36 �;.� Serial No:04101515:26 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits Extractable Petroleum-Hydrocarbons-Westborough Lab Associated sample(s):` 01-03 Batch: W6774197-2 WG774197-3 Decane(C10) -- 6 _ �3'� - - - 40-140 19 - 25 Dodecane(C12) ------� 76� 63'r�.___-__-----__---40-140 _25_._. -Tetradecane(C14)T 7777 84 _ 40-140_ 20 - - -- 25' - _-- - — Hexadecane(C16) 93 80` 40-140 15 25 Octadecane(C18) - 98 88 40-140 i1 25 Nonadecane(C19) 100 r"�'91� 40-140 25 Eicosane(C20) 40-140 9 25 Docosane(C22) r�101'�� �93i 40-140 25 Tetracosane(C24) L -.0 - - ----- 92 — 40-140 - _.-1...___�►�.1. ___..-. _ 25-.-...-.__.-._.. -- Hexacosane(C26) - - 101, - ^- - =92 - 40-140 25 Octacosane(C28) 98 �- 89 40-140 10 25 - Triacontane(C30) 162 92 40-140 10 25 -� .......... _-_ ...-- Hexatriacontane(C36) �•"92� -- 84 40-140 -^ '�9 -�- 25 LCS LCSD Acceptance Surrogate %Recovery Qual %Recovery Qual Criteria Chloro-Octadecane 65 60 40-140 o-Terphenyl 89 81 40-140 2-Fluorobiphenyl 96 99 40-140 2-Bromonaphthalene 90 91 40-140 %Naphthalene Breakthrough 0 0 %2-M ethyl naphtha lene Breakthrough 0 0 Page 20 of 36 Serial No:04101515:26 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits Volatile-Petroleum Hydrocarbons-Westborough Lab Associated,sample s-): 02 Batch: WG774295-1 WG774295-2 C5-C8 Aliphatics 102 r —106'�� _- — 70-130 - ��4�^ -A 25 — C9-C12ABphatics r-10= r-112 70-130 6 25 -C9-C10Aromatics �'""95 _�'97 "'�'_- _ 70-130 - -��-_ - 25 _Benzene iF""99 �"-'.102' -� -_70-130-- -__ -3-77-1 25 t_ Toluene .__-� __---- ---- - �100� - -_r.�_1021� _ 70-130 2�- 25- --- -- -- - - -Ethylbenzene-- �-101"'���_'-- _- tr -`104= -__ 70-130_---F_,3-1---_f_.^.- 25 p/m-Xylene - r -101 r_._-103'7 70-130 f'-'�2� 25 -— o_Xylene �102�— r�103� - _70-130 _--��� - --__ 25-_- -- Methyl tert butyl ether -=02 -_-_ _1027 71 - 70-130 25- Naphthalene ---- F— 7= 98� 70-130 --1----� - w- 25 _- -_---_ -1_2,4Tri methyl benzene _ -96= 97 70-130 -� � --^_ 25 Pentane _ 96 F-99-_-7 _ 70-130 _=3�_---^_ 25 2-Methylpentane 107. 111 70-130 4 25 2,2,4Trimethylpentane -- 10`- 7 �_r�1_10� 70-130 _r^4T� _25 n-Nonane 106 111 30-130 5 25 n-Decane rl106:� 112' 70-130 r-67 25 - n-Butylcyclohexane -� V—�_`- ;106:-77 110 ^-__ 70-130 -_r'-4 -, _ 25 Page 21 of 36 Serial No:041'01515:26 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits -Gol'�`atile Petroleum Hy,0 ocarbons 1Nestborou h Labe Associatetl sarn ,le s 02-1 Batch:. WG.774295-1" WG77.4295-2: :,; LCS LCSD Acceptance Surrogate %Recovery Qual %Recovery Qual Criteria 2,5-Dibromotoluene-PID 94 93 70-130 - 25-Dibromotoluene-FID 97 98 70-130 i Page 22 of 36 � ��� Serial No:04101515:26 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits �olatile Petroleum Hydrocarbons-Westborough.Lab Associate&sample(s): 03 Batch: WG774664-1 WG774664-2 C5-C8 Aliphatics - '-_- ^-- 167 - - -- r-87� - - - 70.130 - 21 - -, _- 25 C9-C12 Aliphatics - _ r"711277 __---.F-95��.-- 70-130 _- 17-1 ----__25 C9-C10 Aromatics -_-�'- 100� - - 84 �-� 70-130 17 - _ 25 - --_ - Benzene 99—' 83 70-130 17 25 Toluene -- -- -_- _— -_ 100--l- - _ F-84� i - - 70-130 - _ 78 - - _- 25 -Ethylbenzene - -- - -- — -F-7102�'� ��- -- --- �85' --- ,_ 70-130 �- - - 18� - -- --25- - -- -- --- p/m-Xylene __- '104"�'�_ — r-86��- - 70-130 -_��-�19�� 25 o_Xylene — -- - =106 —F_88�-- -- - --- 70-130_ 19� 25 ------ - Methyl tert butyl ether -_ --- 103�-_ ''-88—� �y 70-130 - 15 i_ _25___ -y Naphthalene - - -- =101'� 96 �! - T-70-130 - J _--- 25 1,2,4_Tri methyl benzene 84� _ 70-130 - - 17 T--_ ^ --25 Pentane -- ['�"'100'-'""1 —80'^'-r -_ 70-130 22 - 25 2-Methylpentane �91�7 70-130 _ r121^� 25_ _2,2,4 Trimethylpentane C�111_77 ` r-91---_-] A 70-13020—'J _25 -- n-Nonane 11- J- ��93 '"" - - 30-130 18 - 25 n-Decane �-113'""� 95�3 70-130 17 25- tt__ - n-Butylcyclohexane -_ - 1—� _ - F_ '�94�� 70-130 - 16 _ 25 Page 23 of 36 Serial No:041101515:26 Lab Control Sample Analysis Batch Quality Control Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 LCS LCSD %Recovery RPD . Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits olatile Petcol�eum"�Hy,;drocar' bons�Westborough b-Associated sample(s)': 03 Batch:' WG7,7466:4;1 WG7746642 = LCS LCSD Acceptance Surrogate %Recovery Qual %Recovery Qual Criteria - 2,5-Dibromotoluene-PID 98 100 70-130 25-Dibromotoluene-FID 102 105 70-130 r Page 24 of 36 � ��� Serial No:04101515:26 INORGANICS MISCELLANEOUS f Page 25 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS Lab ID: L1506663-01 Date Collected: 04/01/15 11:00 Client ID: CONTAM.STOCKPILE COMP. Date Received: 04/03/15 Sample Location: 86 BAXTER RD.HYANNIS,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst General Chemistry W.estboroug Lab Solids,Total 89.8 % 0.100 NA 1 - 04/08/15 00:11 30,2540G RT i Page 26 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS Lab ID: L1506663-02 Date Collected: 04/01/15 11:15 Client ID: HB-1:5a' T Date Received: 04/03/15 Sample Location: 86 BAXTER RD.HYANNIS,MA Field Prep:, Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor. Prepared Analyzed Method Analyst General Chemistry-',Westborough Lab Solids,Total 96.9 % 0.100 NA 1 - 04/08/15 00:11 30,2540G RT 1 a j -Page 27'of 36 i Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 SAMPLE RESULTS Lab ID: L1506663-03 Date Collected: 04/01/15 11:30 Client ID: _ HB-1:7-9' ---- Date Received: 04/03/15 Sample Location: 86 BAXTER RD.HYANNIS,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst General Chemistry Westborough Lab Solids,Total 97.4 % 0.100 NA 1 - 04/08/15 00:11 30,2540G RT, I I Page 28 of 36 Serial No:04101515:26 Lab Duplicate Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 Parameter Native Sample Duplicate Sample Units RPD Qual RPD Limits General,;,Chemistry-;Westboro,ugh.Lab..Associated::'sample(s) 0'.1'03` .QC.Batch ID; WG7741.74-1� QG`Sampl'ec•,L1.506660-02„ Client,ID DUP"Sample .Solids,Total 89.3 - 90.3 % 20 Page 29 of 36 __ �� Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 Sample Receipt and Container Information. Were project specific reporting limits specified? YES Reagent H2O Preserved Vials Frozen on: NA Cooler Information Custody Seal Cooler A Absent Container Information Temp Container ID Container Type Cooler pH deg C Pres Seal Analysis(*) L1506663-01A Glass 120mi/4oz unpreserved A N/A 3.2 Y Absent TS(7),EPH-DELUX-10(14) L1506663-02A Vial McOH preserved A N/A 3.2 Y Absent VPH-DELUX-10(28) L1506663-02B Glass 120ml14oz unpreserved A N/A 3.2 Y Absent TS(7),EPH-DELUX-10(14) L1506663-03A Val McOH preserved A N/A 3.2 Y Absent VPH-DELUX-10(28) L1506663-03B Glass 120ml/4oz unpreserved A N/A 3.2 Y Absent TS(7),EPH-DELUX-10(14) Container Comments L1506663-01 A L1506663-02B L1506663-03B i *Values in parentheses indicate holding time in days Pa 9 e 30 of 36 � , .. Serial No:O41O1515:26 Project Name: PIERCE-DONAHUE Lab Number: L15O6663 Project Number: BEA15-10764 Report Date: 04/10/15 GLOSSARY Acronyms EDL Estimated Detection Limit:This value represents the level to which target analyte concentrations are reported as estimated values,when those target analyte concentrations are quantified below the reporting limit(RL).The EDL includes any adjustments from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction(SPME). EPA Environmental Protection Agency. LCS Laboratory Control Sample:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. LCSD Laboratory Control Sample Duplicate:Refer to LCS. LFB Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. MDL Method Detection Limit:This value represents the level to which target analyte concentrations are reporied as estimated values, when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any adjustments from dilutions,concentrations or moisture content,where applicable. MS Matrix Spike Sample:A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. MSD Matrix Spike Sample Duplicate:Refer to MS. NA Not Applicable. NC Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameters reporting unit. NI Not Ignitable. RL Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration.The RL includes any adjustments from dilutions,concentrations or moisture content,where applicable. RPD Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference(RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. SRM Standard Reference Material:A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. Footnotes 1 -The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. Terms Total:With respect to Organic analyses,a'Total'result is defined as the summation of results for individual isomers or Aroclors.If a'Total' result is requested,the results of its individual components will also be reported.This is applicable to'Total'results for methods 8260,8081 and 8082. / Analytical Method:Both the document from which the method originates and the analytical reference method.(Example:EPA 8260B is shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A Spectra identified as"Aldol Condensation Product". B The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(1 Ox)the concentration found in the blank.For MCP-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(IOx) the concentration found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(IOx)the concentration found in the blank AND the analyte was detected above one-half the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For NJ- Air-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit.For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable concentrations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone). C . Co-elution:The target analyte co-elutes with a known lab standard(i.e.surrogate,internal standards,etc.)for co-extracted analyses. D Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations of the analyte. E -Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. Report Format: Data Usability Report TN Page 31 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 Data Qualifiers G The concentration may be biased high due to matrix interferences(i.e,co-elution)with non-target compound(s).The result should be considered estimated. H The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. I The lower value for the two columns has been reported due to obvious interference. M Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for this analyte. NJ Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(TICS),where the identification is based on a mass spectral library search. P The RPD between the results for the two columns exceeds the method-specified criteria. Q The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than 5x the RL.(Metals only.) R Analytical results are from sample re-analysis. RE Analytical results are from sample re-extraction. S Analytical results are from modified screening analysis. J Estimated value.This represents an estimated concentration for Tentatively Identified Compounds(TICS). ND -Not detected at the reporting limit(RL)for the sample. Report Format: Data Usability Report /�L�L FiA Page 32 of 36 Serial No:04101515:26 Project Name: PIERCE-DONAHUE Lab Number: L1506663 Project Number: BEA15-10764 Report Date: 04/10/15 REFERENCES 30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA- WPCF. 18th Edition. 1992. 98 Method for the Determination of Extractable Petroleum Hydrocarbons (EPH), MassDEP, May 2004, Revision 1.1 with QC Requirements &Performance Standards for the Analysis of EPH under the Massachusetts Contingency Plan,WSC-CAM-IVB, July 2010. 100 Method for the Determination of Volatile Petroleum Hydrocarbons (VPH), MassDEP, May 2004, Revision 1.1 with QC Requirements & Performance Standards for the Analysis of VPH under the Massachusetts Contingency Plan,WSC-CAM-IVA, July 2010. LIMITATION OF LIABILITIES Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential.or.special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. Page 33 of 36 Serial No:04101515:26 Certification Information Last revised December 16,2014 The following analytes are not included in our NELAP Scope of Accreditation: Westborough Facility EPA 524.2: Acetone, 2-Butanone(Methyl ethyl ketone (MEK)), Tert-butyl alcohol, 2-Hexanone, Tetrahydrofuran, 1,3,5-Trichlorobenzene,4-Methyl-2-pentanone(MIBK), Carbon disulfide, Diethyl ether. EPA 8260C: 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene, lodomethane (methyl iodide), Methyl methacrylate, Azobenzene. EPA 8270D: 1-Methyinaphthalene, Dimethylnaphthalene,1,4-Diphenylhydrazine. EPA 625: 4-Chloroaniline,4-Methylphenol. SM4500: Soil: Total Phosphorus, TKN, NO2, NO3. EPA 9071: Total Petroleum Hydrocarbons, Oil&Grease. Mansfield Facility EPA 8270D: Biphenyl. EPA 254OD: TSS EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility: Drinking Water EPA 200.8: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.1: Mercury; EPA 300.0: Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500E-C, SM4500CN-CE, EPA 180.1, SM213013,SM4500C1-D, SM232013, SM2540C, SM450OH-B EPA 332: Perchlorate. Microbiology: SM9215B; SM9223-PIA, SM9223B-Colilert-QT, Enterolert-QT. Non-Potable Water EPA 200.8: AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se;Ag,TI,Zn; EPA 200.7: AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn; EPA 245.1, SM4500H,B, EPA 120.1, SM251013, SM2540C, SM234013, SM23206, SM4500CL-E,SM4500E-BC, SM426C, SM4500NH3-BH, EPA 350.1: Ammonia-N, LACHAT 10-107-06-1-B:Ammonia-N, SM4500NO3-F, EPA 353.2: Nitrate-N,SM4500NH3-BC-NES, EPA 351.1, SM4500P-E,SM4500P-B, E, SM52201), EPA 410.4, SM52106,SM5310C, SM4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM25401). EPA 624:Volatile Halocarbons &Aromatics, EPA 608: Chlordane,Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs EPA 625: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil. Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9222D-MF. For a complete listing of analytes and methods, please contact your Alpha Project Manager. Page 34 of 36 �:. u r R' : " a3 1,� s s �dD a.r.Q m -n 'v m Po D,' D' ,^."'--`-''`'- �a4' , �? 3_?u: �' r, � S w x o a N #� �. io Ul :y%`>^+? .-;lty 3:^•':.:'.5. v% '?s: :.c�'ct 'm..=. m o 0 0. k:P El b S E. :r' rC: i4i i,., <D 4 —F CO N t 7 m y a. XL w s� a .`" ' s �•ct:_: s'' "E" rf 3 �• a C. m oo' bo . cr' ,3 ,.r;y y (DUl �i O _N..bj';,•?i:':' n.3'_?'t'f't,. .� .N' '1 .. Z i :.•'.'�'*1£''"iztf y' b'� .3� :k \�,..tj ff� !2 QJ: N 7 /� x c.`f 2 ='�: a^:i:' .ti Y' y*� r l�. O CO' 00 0 CD Vror [Tl. •"�gfS `.?t C%`4: i.! `' 4Y$ i � _Z Cn (1. 0DD m O m +• CJ ;'.�:ay.... s73'ni�:.. .. �p ¢• m C .�.L s.. • .:� �. 7 v 2..C7 ': o D p.. :•• N ' co o m , n I e (D' CJ1 3 6, a n O p rn 3 D�� w �. w Ga w N n - . . co y : _ 0 y wo S� C CCD w CD o �m � m Z CD CD o m o 3 CD w.0 U) + .. w q �' r ■ .A. = m 5 D n CD CD : �t r z Vr zt 'v CD 3 4' .0 � N . N ' — o co m j p. S:. 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T �: o' ■ o.. e N 3— F:�•apH�� T.'. :vv.Z Serial No:04101515:26 Quantitation Report (QT Reviewed) Data Path : I: \PVPH\150407ali\ Data File P150407A20.D Signal (s) FID2B.ch Acq On 8 Apr 2015 12 : 01 am Operator PVPH:BS -Sample' 11506663-02D, 41;16, 12 . 1, .05 Misc wg774295, icall0810 ALS Vial 20 Sample Multiplier: 1 Integration File: autointl.e Quant Time: Apr 08 08 : 16: 45 2015 Quant Method I: \PVPH\150407ali\vph-ali.m Quant Title VPH ALIPHATIC QLast Update Mon Mar 23 07 : 55:52 2015 Response via Initial Calibration Integrator: ChemStation Volume Inj . Signal Phase Signal Info Sub List Default - All compounds listed Response— Signal:P150407A20.D\FID2B.ch 450000 e o 400000 0 N 350000 300000 250000 m _ r 200000 150000 i 100000 50000 N 9 0 ime 0.00 2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 vph-ali.m Wed Apr 08 09: 09: 43 2015 Page: 2 Page 36 of 36 Sample Results Comparison with MCP/GW-1 Criteria. CLIENT SAMPLE ID CONTAM.STOCKPILE COMP. HB-1:5-7' HB-1:7-9' SAMPLING DATE 01-APR-15 01-APR-15 01-APR-15 LAB SAMPLE ID L1506663-01 L1506663-02 L1506663-03 CAS Number Sl/GI-14 Units Qual Qual Qual General Chemistry-Westborough Lab Solids,Total % 89.8 96.9 97.4 Volatile Petroleum'Hydrocarbons-W.estborou hLab Benzene 7143-2 2 In 0.279 U 0.141 U C5-C8 Ali hatics --CB-ALPHA-UJ In 6.98 U 3.52 U CS-C8 Ali hatics,Adjusted 5-C8-ALPHAI 100 In 6.98 U 3.52 U C9-C10 Aromatics -CIO-ALPHA 1 00 In 7.09 3.52 U C9-C12 Ali hatics -C12-ALPHA-UJ In 12.9 3.52 U C9-C12 Ali hatics,Adjusted 9-Cl2-ALPHA 1000 mgft 6.98 U 3.52 U Ethylbenzene 100-414 40 m 0.279 U 0.141 U Methyl tert butyl ether 1634-04-4 0.1 m '0.14 U 0.07 U Naphthalene 91-20-3 4 m 0.559 U 0.281 U o-Xylene 9547-6 400 mgIkg 0.279 U 0.141 U /m-Xylene 179601-23-1 400 mgfkg 0.279 U 0.141 U Toluene 108-88-3 1 30 mgIkg 0.279 U 0.141 U ctable Petroleum Hydrocarbons!Westborough Lab 2-Methylna hthalene 91-57-6 0.7 m7 1.82 d U 0.658 U 0.336 U Acena hthene 83-32-9 4 m 1.82 U 0.658 U 0.336 U Acena hthylene 208-96-8 1 mgIkg 1.82 j U 0.658 U 0.336 U Anthracene 120-12-7 1000 mgIkg 1.82 U 0.658 U 0.336 U Benzo a anthracene 56-55-3 7 mglkg 1.82 U 0.658 U 0.336 U Benzo a yrene 50-32-8 2 m 1.82 U 0.658 U 0.336 U Benzo b fluoranthene 205-99-2 7 m 1.82 U 0.658 U 0.336 U Benzo( hi)perylene 191-24-2 1000 P.!gIkgg 1.82 U 0.658 U 0.336 U Ic Benzo fluoranthene 207-08-9 70 1.82 U 0.658 U 0.336 U C11-C22 Aromatics -C22-ALPHA-UJ 893 434 6.73 U CII-C22 Aromatics,Adjusted 1-C22-ALP 1000 893 434 6.73 U C19-C36 Ali hatics -C36-ALPHA 3000 664 325 6.73 U C9-C18 Ali hatics -C18-ALPHA 1000 r 1690 ( 980 6.73 U Chrysene 218-01-9 70 m 1.82 U 0.658 U 0.336 U Dibenzo a,h anthracene 53-70-3 0.7 m j 1.82 U 0.658 U 0.336 U Fluorantheue 20644-0 1000 m 1.82 U 0.658 U 0.336 U Fluoreue 86-73-7 1000 mgft 1.82 U 0.658 U 0.336 U Indeno 1,2,3-cd Pyrene 193-39-5 7 In 1.82 U 0.658 U 0.336 U Naphthalene 91-20-3 4 mgtkg 1.82 U 0.658 U 0.336 U Phenanthrene 85-01-8 10 mgIkg 1.82 U 0.658 U 0.336 U Pyrene 129-00-0 1000 mgIkg 1.82 U 0.658 U 0.336 U Alpha Analytical Labs provides this custom reporting format as a convenience to our clients. As such,we cannot be held liable for errors or omissions associated with the regulatory standards listed above and/or the sample results highlighted by comparison with the standards Effective as of June 20,2014). Only compounds detected with reporting limits that exceed the corresponding regulatory standard in at least one sample are included on the summary sheets. Refer to the laboratory report in Adobe Acrobat .PDF format to check results or read any associated project narrative that may be present.In all cases,the signed, hardco y Alpha Analytical Labs laboratory report is the official document for reporting laboratory results. Sample Results Comparison with Reportable Concentrations RCS-1 Criteria. CLIENT SAMPLE ID CONTAM.STOCKPILE COMP. HB-1:5-7' HB-1:7-9' SAMPLING DATE 01-APR-15 01-APR-15 01-APR-15 LAB SAMPLE ID L1506663-01 L1506663-02 L1506663-03 CAS Number RCS-1-14 Units Qual Qual Qual General Chemistry-Westborough Lab Solids,Total^ -- % 89.8 96.9 97.4 Volatile Petroleum Hydrocarbons=Westborough Lab Benzene 71-43-2 2 mgtkg 0.279 U 0.141 U C5-C8 Ati hatics C8-ALPHA-UJ m 6.98 U 3.52 U C5-C8 Ali hatics,Adjusted 5-C8-ALPH6 100 m 6.98 U 3.52 U C9-Cl0 Aromatics -CIO-ALPHA 100 mgtkg 7.09 3.52 U C9-C12 Ali hatics -C12-ALPHA-UJ m 12.9 3.52 U C9-C12 Ali hatics,Adjusted 9-C12-ALP 1000 m 6.98 U 3.52 U Ethylbenzene 100-414 40 m 0.279 U 0.141 U Methyl tert butyl ether 1634-04-4 0.1 m o.14 i U 0.07 U Naphthalene 91-20-3 4 m 0.559 U 0.281 U o-Xylene 95-47-6 100 m 0.279 U 0.141 U !m-Xylene 179601-23-1 100 mgtkg 0.279 U 0.141 U Toluene 108-88-3 30 m 0.279 U 0.141 U Extractable Petroleum Hydrocarbons;Westborough Lab 2-Methylna hthalene I 91-57-6 0.7 Img/kgg - -1.82 � U 0.658 U 0.336 U Acena hthene 83-32-9 4 1.82 U 0.658 U 0.336 U Acena hthylene 208 96 8 1 1.82 U 0.658 U 0.336 U Anthracene 120-12 7 1000 1.82 U 0.658 U 0.336 U Benzo a anthracene 56-55-3 7 1.82 U 0.658 U 0.336 U Benzo a yrene 50-32-8 2 1.82 U 0.658 U 0.336 U Benzo b fluoranthene 205-99-2 7 1.82 U 0.658 U 0.336 U Benzo ghi erylene 191-24-2 1000 1.82 U 0.658 U 0.336 U Benzo fluoranthene 207-08-9 70 1.82 U 0.658 U 0.336 U C11-C22 Aromatics -C22-ALPHA-UJ 893 434 6.73 U CII-C22 Aromatics,Adjusted 1-C22-ALP 1000 893 434 6.73 U C19-C36 Ali hatics -C36-ALPHA 3000 664 325 6.73 U C9-C18Ali hatics -C18-ALPHA 1000 m 1 ___1690 1 980 6.73 U Chrysene 218-01-9 70 m 1.82 U 0.658 U 0.336 U Dibenzo a,h anthracene 53-70-3 0.7 mgft 1.82 U 0.658 U 0.336 U Fluoranthene 20644-0 1000 mglkg 1.82 U 0.658 U 0.336 U Fluorene 86-73-7 1000 m 1.82 U 0.658 U 0.336 U Indeno 1,2,3-cd Pyrene 193-39-5 7 m 1.82 U 0.658 U 0.336 U Naphthalene 91-20-3 4 mgtkg 1.82 U 0.658 U 0.336 U Phenanthrene 85-01-8 10 mgfkg 1.82 U 0.658 U 0.336 U Pyrene 129-00-0 1000 m 1.82 U 0.658 U 0.336 U Alpha Analytical Labs rovides this custom reporting format as a convenience to our clients. As such,we cannot be held liable for errors or omissions associated with the regulatory standards listed above and/or the sample results highlighted by comparison with the standards Effective as of A 6125,2014). Only compounds detected with reporting limits that exceed the corresponding regulatory standard in at least one sample are included on the summary sheets. Refer to the laboratory report in Adobe Acrobat .PDF format to check results or read any associated project narrative that may be resent.In all cases,the signed, hardco y AI may Analytical Labs laboratory report is the official document for reporting laboratory results. Serial No:04161515:43 HA ANALYTICAL ANALYTICAL REPORT Lab Number: L1507116 Client: Bennett Environmental Associates 1573 Main Street Brewster, MA 02631 ATTN: David Bennett Phone: (508) 896-1706 Project Name: PIERCE-DONAHUE Project Number: BEA15-10764 Report Date: 04/16/15 The original project report/data package is held by Alpha Analytical.This report/data package is paginated and should be reproduced only in its entirety.Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086), PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(1-2217),USDA(Permit #P-330-11-00240). Eight Walkup Drive,Westborough, MA 01581-1019 508-898-9220 (Fax) 508-898-9193 800-624-9220-www.alphalab.com Page 1 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 Alpha Sample Collection Sample ID Client ID Matrix Location Date/Time Receive Date L1507116-01 HB-1:9-10' SOIL 86 BAXTER RD.,HYANNIS 04/08/15 11:00 04/09/15 L1507116-02 HB-6: 0-5' COMP SOIL 86 BAXTER RD.,HYANNIS 04/08/15 15:00 04/09/15 Page 2 of 31 � �� Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 MADEP MCP Response Action Analytical Report Certification This form provides certifications for all samples performed by MCP methods. Please refer to the Sample Results and Container Information sections of this report for specification of MCP methods used for each analysis.The following questions pertain only to MCP Analytical Methods. An affirmative response to questions A through F is required for"Presumptive Certainty" status A Were all samples received in a condition consistent with those described on the Chain-of- YES Custody, properly preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding times? B Were the analytical method(s) and all associated QC requirements specified in the selected YES CAM protocol(s) followed? C Were all required corrective actions and analytical response actions specified in the selected YES CAM protocol(s) implemented for all identified performance standard non-conformances? D Does the laboratory report comply with all the reporting requirements specified in CAM VII A, YES "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data?" E a. VPH, EPH, and APH Methods only: Was each method conducted without significant YES modifications ? Refer to the individual methods for a list of significant modifications). E b. APH and TO-15 Methods only:Was the complete analyte list reported for each method? N/A F Were all applicable CAM protocol QC and performance standard non-conformances identified YES/ and evaluated in a laboratory narrative (including all"No"responses to Questions A through E)? A response to questions G, H and I is required for"Presumptive Certainty"status G Were the reporting limits at or below all CAM reporting limits specified in the selected CAM YES protocol(s)? H Were all QC performance standards specified in the CAM protocol(s) achieved? YES I Were results reported for the complete analyte list specified in the selected CAM protocol(s)? YES For any questions answered "No", please refer to the case narrative section on the following page(s). Please note that sample matrix information is located in the Sample Results section of this report. At;� Page 3 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15' Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC,for all NELAC accredited parameters.The data presented in this report is organized by parameter(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter.If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific% recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications.Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will be disposed after 3 business days from the date the project is completed. Please contact Client Services at 800-624-9220 with any questions. Page 4 of 31 .'.� Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 Case Narrative(continued) MCP Related Narratives Report Submission All MCP required questions were answered with affirmative responses; therefore, there are no relevant protocol-specific QC and/or performance standard non-conformances to report. i I,the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained , in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. �,1�Authorized Signature: Cristin Walker Title: Technical Director/Representative Date: 04/16/15 Page 5 of 31 ` Serial No:04161515:43 ORGANICS { Page 6 of 31 Serial No:04161515:43 PETROLEUM HYDROCARBONS Page 7 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 SAMPLE RESULTS Lab ID: L1507116-02 Date Collected: 04/08/15 15:00 Client ID: HB-6: 0-5' COMP Date Received: 04/09/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Extraction Method:EPA 3546 Analytical Method: 1,8015C(M) Extraction Date: 04/13/15 22:33 Analytical Date: 04/14/15 23:29 Analyst: AR Percent Solids: 97% Parameter Result Qualifier Units RL MDL Dilution Factor Petroleum Hydrocarbon-Quantitati66-Westborough L-ab _ TPH ND ug/kg 34100 — 1 Acceptance Surrogate %Recovery Qualifier Criteria o-Terphenyl 81 40-140 i I Page 8 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 Method Blank Analysis Batch Quality Control Analytical Method: 1,8015C(M) Extraction Method: EPA 3546 Analytical Date: 04/14/15 16:51 Extraction Date: 04/13/15 22:33 Analyst: AR Parameter Result Qualifier Units RL MDL Petroleum Hydrocarbon Quantitation-Westborough Lab for sample(s)' 02 :Batch: 'WG775610=1 TPH ND ug/kg 31900 — Acceptance Surrogate %Recovery Qualifier Criteria o-Terphenyl 79 40-140 Page 9 of 31 Serial No:04161515:43 Lab Control Sample Analysis Batch Quality Control Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 LCS LCSD %Recovery RPD ' Parameter %Recovery Qual %Recovery Qual Limits. RPD Qual Limits Petroleum Hydrocarbon;Quantitation WestboroughsL b Associated sample(s):: 02 B h: WG775610 TPH - t84'" 40-140 40 LCS LCSD Acceptance Surrogate %Recovery Qual %Recovery Qual Criteria o-Terphenyl 93 40-140 Page 10 of 31 Serial No:04161515:43 Lab Duplicate Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 RPD Parameter Native Sample Duplicate Sample Units RPD Qual Limits Petroleum Hydrocarbon:Quantitation.--Westborough?Lab Associated,sample(s): 02 QC Batch ID: `WG77561;0=3"`,QC"Sample: 1,1.5070W02''Clienf ID DUP , Sample _ TPH 80000 299000 ug/kg 1.16, Q 40 Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria o-Terphenyl 88 86 40-140 Page 11 of 31 _ . � •ti''•�• Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 SAMPLE RESULTS Lab ID: L1507116-01 Date Collected: 04/08/15 11:00 Client ID: HB-1:9-10' Date Received: 04/09/15 'Sample Location: 86 BAXTER RD.,HYANNIS Field Prep:- Not Specified Matrix: Soil Analytical Method: 100,VPH-04-1.1 Analytical Date: 04/13/15 21:45 Analyst: BS Percent Solids: 97% bualityCo�trollnforina one Condition of sample received:`+ Satisfactory Sample Temperature upon receipt: Received on Ice Were samples received in methanol? Covering the Soil Methanol ratio: 1:1 +/-25% Parameter Result Qualifier Units RL MDL Dilution Factor Volatile Petroleum Hydrocarbons=,We is borough Lab J C5-C8 Aliphatics ND mg/kg 2.84 — 1 C9-C12 Aliphatics ND mg/kg 2.84 — 1 C9-C10 Aromatics ND mg/kg mglkg 2.84 — 1 -----...__..._...._...---- -- ---............... C5-C8 Aliphatics,Adjusted ND mg/kg 2.84 — 1 C9-C12 Aliphatics,Adjusted ND mg/kg 2.84 — 1 — Benzene ND mg/kg 0.114 — 1 Toluene ND mg/kg 0.114 — 1 Ethylbenzene ---.------ -----..-- ND ---- mg/kg --..-- 0.114--- — -----1 -..--- p/m-Xylene ND mg/kg 0.114 — 1 o-Xylene ND mg/kg 0.114 — 1 Methyl tert butyl ether ND mg/kg 0.057 — 1 Naphthalene ND mg/kg 0.228 — 1 Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID gg 70-130 2,5-Dibromotoluene-FID 101 70-130 - 11L HA Page 12 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764• Report Date: 04/16/15 SAMPLE RESULTS Lab ID: L1507116-01 Date Collected: 04/08/15 11:00 Client ID: HB-1:9-10' Date Received: 04/09/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 98,EPH-04-1.1 Extraction Date: 04/14/15 13:27 Analytical Date: 04/16/15 11:30 ' Cleanup Method1: EPH-04-1 Analyst: SR Cleanup Datel: 04/15/15 Percent Solids: 97% Quality Controflnformation- Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbons=.Westborough L•ab C9-C18 Aliphatics ND mg/kg 6.67 - 1 -------------.......--.._....-_._..._.._... - C19-C36 Aliphatics ND mg/kg 6.67 - 1 _ -- --------..__.._._...._...--.---------..................._._._.__...---.._._._....__.._..._..._..- ---........_............_.. _....._,._._..._... ._..........._.-..__.._._........._........._...-...._.._----.._-...-- -----... C11-C22 Aromatics ND mg/kg 6.67 - 1 ---................ ------ _ _ --. C11-C22 Aromatics,Adjusted ND mg/kg 6.67 - 1 --------- -----------------.......__`..-.-------------- ----- _ __ ---�...- ---- ---- Naphthalene ND mg/kg 0.334 - 1 2-Methylnaphthalene ND mg/kg 0.334 - 1 Acenaphthylene — ND mg/kg 0.334 1 Acenaphthene ND mg/kg 0.334 - 1 -------- - ---......-- --......... -- - -------_.....---..—.,------ -- ----...--- ---- - -- ----._._...._..-------- ---—-- .._._. Fluorene ND mg/kg 0.334 - 1 -......_......._._...---- _ ._...--------- --.. Phenanthrene ND mg/kg 0.334 - 1 --- -- ---..._....------....__......- ..._.._._...- -..__..._.. ...._.._..._.__...._........--...............,.._........... ..- ........._..._...._...__.,... ------..._ -- -----..__..._....--...---...._._._._.....---- ..._......._._..._...__..._... Anthracene ND mg/kg 0.334 - 1 ---- -------.._....._......------ ---------- .-_...-----.._..-----..........._...........-------- ---...._.._._... - --------..__._._.._._.__.._...------------ ._...- - Fluoranthene ND mg/kg 0.334 - 1 Pyrene ND mg/kg 0.334 - 1 Benzo(a)anthracene ND mg/kg 0.334 - 1 Chrysene ND mg/kg 0.334 - 1 Benzo(b)fluoranthene ND mg/kg 0.334 - 1 -------- ......--....... Benzo(k)fluoranthene ND mg/kg 0.334 - 1 ---------...--..-...._._._....---- ._... ...-_.._.__.._._._......_..._........._.....__..._._._.__... --.....-- - - ._..._._..----.._._..._._.... --._.._._.......----..._....._..__..._..___.....-_..._....__.....__..._._...-_._._....----....._..............--- Benzo(a)pyrene ND mg/kg 0.334 - 1 ._.._.__........._._........_........_._..._....__._.._.._._........._.._._......_.._.__._..._._..------ --- - _---._..__...._,.._......_..-.....-------..- --... ---- Indeno(1,2,3-cd)Pyrene ND mg/kg 0.334 - 1 -- -- ------------ - --- ----------- .----------.._.__...__._._....---------- -- - --_ -.._....._._.....—.__----------- Dibenzo(a,h)a nth racene ND mg/kg 0.334 - 1 Benzo(ghi)perylene ND mg/kg 0.334 - 1 t AN Page 13 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 SAMPLE RESULTS Lab ID: L1507116-01 Date Collected: 04/08/15 11:00 Client ID: HB-1:9-10' Date Received: 04/09/15 Sample Location: 86 BAXTER-RD.;HYANNIS - Field Prep: Not*Specified Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum.Hydrocarbons Westborough Lab' Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 71 40-140 o-Terphenyl S1 40-140 2-Fluorobiphenyl 81 40-140 2-Bromonaphthalene 73 40-140 17 Page 14 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 Method Blank Analysis Batch Quality Control Analytical Method: 1A0,VPH-04-1.1 Analytical Date: 04/13/15 11:32 Analyst: BS Parameter Result Qualifier Units• RL MDL Volatile Petroleum Hydrocarbons-Westborough Lab for sample(s): 01 Batch: W.G775491=3 -: C5-C8 Aliphatics ND mg/kg 2.67 - C9-C12 Aliphatics ND mg/kg 2.67 - ----- -----.—.. ------ --------- -------- -------------—--------- C9-C10 Aromatics ND mg/kg 2.67 - 05-C8 Aliphatics,Adjusted ND mg/kg 2.67 - C9-C12 Aliphatics,Adjusted ND mg/kg 2.67 - Benzene ND mg/kg 0.107 - Toluene ND mg/kg 0.107 - Ethylbenzene ND mg/kg 0.107 - p/m-Xylene ND mg/kg 0.107 -- o-Xylene ND mg/kg 0.107 - Methyl tent butyl ether.------------ —_-ND --------- mg/kg 0.053 ---- - ---------..--- . Naphthalene ND mg/kg 0.213 - Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 93 70-130 2,5-Dibromotoluene-FID 96 70-130 , { Page 15 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 Method Blank Analysis Batch Quality Control Analytical Method: 98,EPH-04-1.1 Extraction Method: EPA 3546 Analytical Date: 04/15/15 19:19 Extraction Date: 04/14/15 13:27 Analyst: SR Cleanup Method: EPH-04-1 Cleanup Date: 04/15/15 Parameter Result Qualifier units RL MDL Extractable Petroleum Hydrocarbons-Westborough Lab for sample(s): 01 Batch" WG775798-1 ' C9-C18 Aliphatics ND mg/kg 6.57 - C19-C36 Aliphatics -------._.— ND_...---------- mg/kg 6.57 --------_------------- C11-C22 Aromatics ND mg/kg 6.57 - C11-C22 Aromatics,Adjusted ND mg/kg 6.57 -- Naphthalene ND mg/kg 0.329 - 2-Methylnaphthalene ND mg/kg 0.329 - Acenaphthylene ND mg/kg 0.329 - Acenaphthene ND mg/kg 0.329 - Fluorene ND mg/kg 0.329 - ..._._.......--...... —__ —..._._.__._._.....-...—._ . Phenanthrene ND mg/kg 0.329 - ------ .._..__...---..__..__._...._.._..._..._......._..__.. Anthracene ND mg/kg 0.329 - Fluoranthene ND mg/kg 0.329 - Pyrene ND mg/kg 0.329 -- Benzo(a)anthracene ND mg/kg 0.329 -- --...- -- - -- ----.._.._............._.--. --..._..--- --.._.. - -- ---------- ------- Chrysene ND mg/kg 0.329 -- _........_.._-....__I.._.._.._..._._._-._...._...----- ---._._._..._........_—..-....------...-------- _.._._._._._.. _._-._._._._................- - ._..._.__.._...._..._.._........_................._.. Benzo(b)fluoranthene ND mg/kg 0.329 - Benzo(k)fluoranthene ND mg/kg 0.329 — - Benzo(a)pyrene ND mg/kg 0.329 - Indeno(1,2,3-cd)Pyrene ---------------ND----------- mg/kg 0.329 --------_.............. - ------------- ._... _... - .._..... -.._...- ..__....._._........--- Dibenzo(a,h)anthracene ND mg/kg 0.329 - - -....__... -------._..._- - .•_..- ---..—. _ - ---- --- .._._...._.....-----------—------_........._.......__.._..- ...._.._.,._.._..- -..._...._......... -- Benzo(ghi)perylene ND mg/kg 0.329 - Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 47 40-140 o-Terphenyl 70 40-140 2-Fluorobiphenyl 77 40-140 2-Bromonaphthalene 71 40-140 Page 16 of 31 Serial No:04161515:43 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits Volatile Petroleum Hydrocarb ciat6am ons,,Westborough;Lab�Assoii aple(s):I 01 Batch:. ,WG77549iA WG775491'-2 <.. C5-C8 Aliphatics --- --__ r91� J -84i�-- --- 70-130- 25- C9-C12 Aliphatics 70.130 f"-'5 '' _ 25 C9-C10 Aromatics _ - -_ 85 " �`81,- _- 70-130 -�4'�--�---' 25- ---_-^- Benzene ^89"- F_- 82—__J 70-130 25 Toluene r--88. f 82 70-130 _ - -- - 25 Ethylbenzene - ["'.-88-r-7_ ---r "l82- _-_-T 70-130- -_�_ 7�� y --- --_25_ y--- p/m-Xylene "87�7-1 �'81 1 - 70-130 - �_, 6 7_7_ 25 -o_Xylene --- -[--789�� - 83 � --- 70-130 —����- ------25 Methyl tert butyl ether 1007-7 �l91—� - 70-130 10w� 25 -Naphthalene - -` _ —96=i f� 89�� 70-130� _ —7-7-1 -i --- 25 ---- - 1,2,4-Trimethylbenzene - �;85 - -"81-1 - 70^130 - �r-4'-7 -- _-- 25-"-- - - Pentane r"'"�86� r_83J 70-130 4 - 25 2-Methylpentane r95"T1 -89' , 70-130 'r—7__'_J 25 2,2,4 Trimethylpentane ���84"�'� 70-130 � 25 90i n_Nonane 92 - i -^—87 �5"-� �� - 30 130_i _�-- -- - --25 ---- n-Decane 92 90 70-130 3 25 n-Butylcyclohexane F:-793?- 1 87'--] 70-130 '6�] 25 Page 17 of 31 :A""` HA. Serial No:04161515:43 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 LCS L CSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits Volatile Petroleum Hydrocarbons-Westborough Lab Associated_sample(S): 01 Batch: WG775491-1 WG775491-2 LCS LCSD Acceptance Surrogate %Recovery Qual %Recovery Qual Criteria 2,5-Dibromotoluene-PID 97 95 70-130 2,5-Dibromotoluene-FID 101 98 70-130 Page 18 of 31 Serial No:04161515:43 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 L CS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits Extractable Petroleum Hydrocarbons-Westborough Lab Associated sample(s): 01 Batch: WG775798-2 WG775798-3 C9-C18Aliphatics ` ^7�---' - r-68—� --_ 40-140 r_-6"71- _ -_ 25 C19-C36 Aliphatics �8 '-- �BO� 40-140 25 — ^ _C11-C22 Aromatics r _ 40-140 _----- 25 _ --— Naphthalene 51---I U 40.140 2 __J 25 2-Methyl naphthalene, --- -- Y =62-1 - 73 l _ - - 40-140- 16 _- - 25 Acenaphthylene657 � ` - _— 40-140_ 11 - _ —� 25 -,- Acenaphthene _ 67—"1 -72____1_ 40-140 25 Fluorene 77 _ 40-140 25 Phenanthrene _— 78 78T� 40-140 �� p0�"'''"�- 25 90l -Anthracene ---... -^__---- —-- �— � - ------- -�r90�'""� - -- - -- 40.140 L� 25 - - -- -- Fluoranthene _ __ 807-7 80- 1---_� 40-140 -- �0�_ -_ 25- --- Pyrene F 40-140 �r0'T� 25 _Benzo(a)anthracene 73 _ 74'T-]- 40-140 -_ 1 -- 25 Chrysene -64� 67 .. 40-140 F-571 25 - Benzo(b)fluoranthene _ - _ --- 85 ,- f 6-5 _ _! — 40-140 s _ �0 - — 25 - - Benzo(k)fluoranthene F-78-- -`--_ r"�79�� _ �! _ 40-140 1,�� - 25 Benzo(a)pyrene r__7.1 r -72= - 40-140 -��1 25 -Indeno(1,2,3-cd)Pyrene -F'62-7 62' -_ -- _40-140 - �0�---_ - 25 _ _-- Dibenzo(a,h)anthracene �52'—� �'58 40-140 25 Benzo(ghi)perylene rl74-") _- —74��- 40-140 �0-�_ 25 - --Nonane(C9) �-"44 47�� -: --- 30.140--� .F-7 -_ 25 Page 19 of 31 Serial No:04161515:43 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits Extractable Petroleum;Hydrocarbons-Westborough Lab Associated:sample(s): 01 Bat`ch: WG775798-2 W6775798-3 Decane(C10) ,52 55 40-140 6 25 Dodecane(C12) _.-.__.—....--------- 6 --_-- 64, --_ ---- 40-140 0 .Z ---- -- -25------ Tetradecane(C14) _- 7071 - - --J"7-69 '� 40.140 " 11 v 25 Hexadecane(C16) 73, , 73 40-140 0. 25 Octadecane(C18) 75 75 40-140 0 25 Nonadecane(C19) '7T, - 71 „ 40-140 �. 25 Eicosane(C20) 7= 40-1400., 25 -- Docosane(C22) -`------- 76. - _ 77 40-140 1"-"� 25 Tetracosane(C24) ;"�76 77 40-140 1 25 Hexacosane(C26) �76�'�"7 77 40-140 - - 25 Octacosane(C28) 74.. 75 40-140 1 ., - 25 Triacontane(C30) �7�7 "'�� 78 40-140 - 1 25 -Hexatriacontane(C36) — -_— - �`�-71 —^ �76 -- M40-140 '- 25 LCS LCSD Acceptance Surrogate %Recovery Qual %Recovery Qual Criteria Chloro-Octadecane 54 52 40-140 o-Terphenyl 71 70 40-140 _ 2-Fluorobiphenyl 65 76 40-140 2-Bromonaphthalene 67 70 40-140 %Naphthalene Breakthrough 0 0 %2-Methyl naphthalene Breakthrough 0 0 Page 20 of 31 L�L\HA i Serial_No:04161515:43 INORGANICS MISCELLANEOUS Page 21 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 SAMPLE RESULTS Lab ID: L1507116-01 Date Collected: 04/08/15 11:00 Client ID: HB-1:9-10' Date Received: 04/09/15 Sample Location: 86 BAXTER RD.,HYANNIS _ Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst Solids,Total 97.0 % 0.100 NA 1 04/10/15 21:57 30,2540G RT I i i Page 22 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 SAMPLE RESULTS Lab ID: L1507116-02 Date Collected: 04/08/15 15:00 Client ID: HB-6:0-5'COMP Date Received: 04/09/15 Sample Location: 86 BAXTER RD•,HYANNIS _Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst 6erieral Chemistry�,_1LVestborougfi;Lab Solids,Total 97.4 % 0.100 NA 1 - 04/10/15 02:05 30,2540G RT • T Page 23 of 31 Serial No:04161515:43 Lab Duplicate Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 Parameter Native Sample Duplicate Sample Units RPD Qual RPD Limits GenT eralGhre'rnistry Westb.orough;Cab QssocatedsamPle,(s):;,02 QC Batch'IDc .1NG774:$70 1 Qc Sam ae:�aL1506435-02 Client•:ID �DUP Sam •�.— �ral/1i�iM�IYiP .` a�.: Solids,Total 89.8 89.3 % yi ;. , 20 r , LG neraf Chemistry-,Westb"orough;Lab;"Associatedlsarnple s . a01 r QC:Batch LD:, WG,775123-1 QC,Sarn_le N-0-6L7116=OM1> Solids,Total 97.0 97.2 % 20 { i I Page 24 of 31 �ti� Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 Sample Receipt and Container Information Were project specific reporting limits specified? YES Reagent H2O Preserved Vials Frozen on: NA Cooler Information Custody Seal Cooler A Absent B Absent Container Information Temp Container ID Container Type Cooler pH deg C Pres Seal Analysis(*) L1507116-01A Vial McOH preserved A N/A 4.1 Y Absent .VPH-DELUX-10(28) L1507116-01B Glass 120ml/4oz unpreserved B N/A 2.8 Y Absent TS(7),EPH-DELUX-10(14) L1507116-02A Glass 120mil4oz unpreserved A N/A 4.1 . Y Absent TS(7),TPH-DRO-D(14) L *Values in parentheses indicate holding time in days Page 25 of 31 Serial No:O4161515:43 Project Name: PIERCE-DONAHUE Lab Number: L15O7116 Project Number: BEA15-10764 Report Date: 04/16/15 GLOSSARY Acronyms EDL Estimated Detection Limit:This value represents the level to which target analyte concentrations are reported as estimated values,when those target analyte concentrations aie quantified below the reporting limit(RL).The EDL includes any adjustments from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction(SPME). EPA Environmental Protection Agency. LCS Laboratory Control Sample:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. LCSD Laboratory Control Sample Duplicate:Refer to LCS. LFB Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. MDL Method Detection Limit:This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any adjustments from dilutions,concentrations or moisture content,where applicable. MS Matrix Spike Sample:A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. MSD Matrix Spike Sample Duplicate:Refer to MS. NA Not Applicable. NC Not Calculated: Tenn is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. NI Not Ignitable. RL Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration.The RL includes any adjustments from dilutions,concentrations or moisture content,where applicable. RPD Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference(RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. SRM Standard Reference Material:A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. Footnotes I The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. Terms Total:With respect to Organic analyses,a'Total'result is defined as the summation of results for individual isomers or Aroclors.If a'Total' result is requested,the results of its individual components will also be reported.This is applicable to'Total'results for methods 8260,8081 and 8082. Analytical Method:Both the document from which the method originates and the analytical reference method.(Example:EPA 8260B is shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A Spectra identified as"Aldo]Condensation Product". B The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(I Ox)the concentration found in the blank.For MCP-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(10x) the concentration found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(1 Ox)the concentration found in the blank AND the analyte was detected above one-half the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For NJ- Air-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable concentrations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone). C Co-elution:The target analyte co-elutes with a known lab standard(i.e.surrogate,internal standards,etc.)for co-extracted analyses. D Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations of the analyte. E Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. Report Format: Data Usability Report Page 26 of 31 Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 Data Qualifiers G The concentration may be biased high due to matrix interferences(i.e,co-elution)with non-target compound(s).The result should be considered estimated. H The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. I The lower value for the two columns has been reported due to obvious interference. M Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for this analyte. NJ Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(TICS),where the identification is based on a mass spectral library search. P The RPD between the results for the two columns exceeds the method-specified criteria. Q The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than Sx the RL.(Metals only.) R Analytical results are from sample re-analysis. RE Analytical results are from sample re-extraction. S Analytical results are from modified screening analysis. J Estimated value.This represents an estimated concentration for Tentatively Identified Compounds(TICs). ND -Not detected at the reporting limit(RL)for the sample. Report Format. Data Usability Report A'A'HA, Page 27 of 31 I Serial No:04161515:43 Project Name: PIERCE-DONAHUE Lab Number: L1507116 Project Number: BEA15-10764 Report Date: 04/16/15 REFERENCES 1 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IV, 2007. 30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA- WPCF. 18th Edition. 1992. 98 Method for the Determination of Extractable Petroleum Hydrocarbons (EPH), MassDEP, May 2004, Revision 1.1 with QC Requirements & Performance Standards for the Analysis of EPH under the Massachusetts Contingency Plan,WSC-CAM-IVB, July 2010. 100 Method for the Determination of Volatile Petroleum Hydrocarbons (VPH), MassDEP, May 2004, Revision 1.1 with QC Requirements& Performance Standards for the Analysis of VPH under the Massachusetts Contingency Plan, WSC-CAM-IVA, July 2010. LIMITATION OF LIABILITIES Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. Page 28 of 31 Serial No:04161515:43 Certification Information Last revised December 16,2014 The following analytes are not included in our NELAP Scope of Accreditation: Westborough Facility EPA 524.2: Acetone, 2-Butanone (Methyl ethyl ketone(MEK)), Tert-butyl alcohol, 2-Hexanone, Tetrahydrofuran, 1,3,5-Trichlorobenzene,4-Methyl-2-pentanone (MIBK), Carbon disulfide, Diethyl ether. EPA 8260C: 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene, lodomethane (methyl iodide), Methyl methacrylate, Azobenzene. EPA 8270D: 1-Methyl naphthalene, Dimethylnaphthalene,1,4-Diphenylhydrazine. EPA 625: 4-Chloroaniline,4-Methylphenol. SM4500: Soil: Total Phosphorus, TKN, NO2, NO3. EPA 9071: Total Petroleum Hydrocarbons, Oil &Grease. Mansfield Facility EPA 8270D: Biphenyl. EPA 254OD: TSS EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility: Drinking Water EPA 200.8: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.1: Mercury; EPA 300.0: Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500E-C, SM4500CN-CE, EPA 180.1, SM21306,SM4500C1-D, SM232013, SM2540C,SM450OH-B EPA 332: Perchlorate. Microbiology: SM921513; SM9223-PIA,SM9223B-Colilert-QT, Enterolert-QT. Non-Potable Water EPA 200.8:AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn; EPA 200.7:AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn; EPA 245.1, SM45001-1,6, EPA 120.1, SM251013, SM2540C,SM234013,SM232013, SM4500CL-E, SM4500E-BC, SM426C, SM4500NH3-BH, EPA 350.1:Ammonia-N, LACHAT 10-107-06-1-13: Ammonia-N, SM4500NO3-F, EPA 353.2: Nitrate-N,SM4500NH3-BC-NES, EPA 351.1,SM4500P-E, SM4500P-B, E, SM52201), EPA 410.4, SM521013, SM5310C, SM4500CL-D, EPA 1664,SM14 510AC, EPA 420.1,SM4500-CN-CE, SM25401). EPA 624:Volatile Halocarbons &Aromatics, EPA 608: Chlordane, Toxaphene,Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs EPA 625: SVOC (Acid/Base/Neutral Extractables), EPA 60014-81-045: PCB-Oil. Microbiology: SM9223B-Colilert-QT; Enterolert-QT,SM9222D-MF. ! For a complete listing of analytes and methods, please contact your Alpha Project Manager. Page 29 of 31 Serial No:04161515:43 Da di te�ReC iri;l�b' •, CHAlN �OF CUSTODY - PAGE 1 OF 1 HA+:� ••• - 1 ; r; --p.rt Informa'tion Data Deliverables Billing Information P dA 1. El FAX ® EMAIL ® Same as Client info PO#:10764 Westborough,MA Mansfield,MA Project Name:Pierce-Donahue TEL:60MOB-9220 TEL SOM22.9300 ® ADEX ❑ Add'I Deliverables FAX:508-898-9193 FAX 608.822.328E Project Location:86 Baxter Rd, Hyannlss Regulatory Requirements/Report Limits State/Fad Pro&am MA MCP Criteria RCS-1 Client:Bennett Environmental Assoclates Project*BEA15-10764 • • '-• • • Address:P,O.Box 1743/1573 Main Street Project Mana er:Davld Bennett/JTW ® Yes ❑ No Are MCP Analytical Methods Required? ❑ Yes ® No Is Matrix Spike MS Required on this SOG? If es see note in Comments Brewster MA 02631 ALPHA Quote#: ❑ Yes ® No Are CT RCP Reasonable Confidence Protocols Rea ulred? Phone:(5028)896-1706 ANALYSIS • SAMPLE HANDLING Fax:(508)896-5109 ®Standard ❑Rush(ONLY IF PRE-APPROVED) Filtration Email:dbennetta@bennett-ea.com 0 Done N Not Needed ❑These samples have been Previously analyzed by Alpha Due Date: /,`/,tTlme: ❑ Lab to do Other Project Specific Requirements/Comments/Detection Limits: 7 Preservation • (If MS is required, indicate in Sample Specific Comments which samples and what tests MS to be ❑ Lab to de performed. (Note: All CAM methods for inorganic analyses require MS every 20 soil samples) below) specify al _ o x ALPHA:i ab'IQ Sample ID Collection Sample Sampler's 4 J(Las$.O.nly)' :;; Date Time Mattix Initials samp)espedne 'Ll Comments HB-1:9-10' 418/15 11:00 soil Jos ® ❑ ❑ ❑ ❑ ❑ ' HB-6:0-5'Comp 4/8/15 3::00 Soil JDB ❑ ❑ ❑ r:..... pia•: ..., ������� oi,� ��'� El 1010 ❑ ❑ ❑ • 0.1;' El ❑ 0 ❑ 0 ❑ El ❑ ❑ 0 ❑ ❑ 0 EEO] ❑ ❑ T; PLEASE ANSWER QUESTIONS ABOVEi Container Type v A Preservativ F A - - _ _ _ _ _ %PleaegtPriiiboleary!;leglbly�;; : e :;ah?l(b6mple(91y,Samples>can:; IS YOUR PROJECT Relinquished By: D te/Ti a Received By: bete/Tlme -tifrr2arouiyd tlmeylogk!wpl;nal sfiitt uhGltany<enibigulties'ere:. MA MCP or CT R C P 5 ° �- '�ra��00)ved:':�llsertip)es ri + ✓s�ubM111ed eresuliJtipt tti; No:ot-o)m (j'�r9 •d Qlphia roaM 'sPaymerit'7e(ms,'::,-; ORMeJAN 2ofe) *' Page 30 of 31 ... n:- -" s t ... :Oz 'M:r:-y a^p ❑ m m v M fD X 3 m Q . 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'� ❑ .❑ ❑ T rn:.: N - . fn O m� ro.c a 39 °m r r z. a c1' .. m a m V 5 0 'o' fir- C. m r� q�^.: m'O m.o m o z o' m n''o_' • o. Y�' W CD m�—:•fitcr.n� •, m z :. a K, c�• 3I.p 3.rx '�a"��:m.:o`m.Gs�fi� ('1`�"F' 'r .. �. � • fate . Sample Results Comparison with MCP/GW-1 Criteria. CLIENT SAMPLE ID HB-1:9-10' 1113-6:0-5'COMP SAMPLING DATE 08-APR-15 08-APR-15 LAB SAMPLE ID L150 I M-M L1507116-02 CAS Number SI/G1-14 Units Qual Qual General Chemistry-Westborough Lab Solids,Total — % 97 97.4 Petroleum Hydrocarbon Quantitatiou-Westborou b Lab TPH — 1000 m 34.1 U Vo stile Petroleum Hydrocarbons-Westborou b Lab Benzene i 71-43-2 1 2 m 0.114 U C5-C8 Ali hatics -CB-ALPHA-UJ m 2.84 U C5-C8 Ali hatics,Adjusted 5-C8-ALPHA 100 m 2.84 U C9-C10 Aromatics -CIO-ALPHA-1 100 mgAkg 2.84 U C9-C12 Ali hatics -C12-ALPHA-UJ m 2.84 U C9-C12 Ali hatics,Adjusted 9-C12-ALP 1000 m 2.84 U Ethylbenzene 100-414 40 m 0.114 U Methyl tert butyl ether 1634-04-4 0.1 m 0.057 U Naphthalene 91-20-3 4 m 0.228 U o-Xylene 95-47-6 400 m 0.114 U /m-Xylene 179601-23-1 400 m 0.114 U Toluene 108-88-3 30 m 0.114 U Extractable Petroleum Hydrocarbons-Westborou h Lab 2-Methylna hthalene 91-57-6 0.7 m 0.334 U Acena hthene 83-32-9 4 m 0.334 U Acena hthylene 208-96-8 1 m 0.334 U Anthracene 120-12-7 1000 m 0.334 U Benzo a anthracene 56-55-3 7 m 0.334 U Benzo a yrene 50-32-8 2 m 0.334 U Benzo fluoranthene 205-99-2 7 m 0.334 U Benzo( hi)perylene 191-24-2 1000 m 0.334 U Benzo fluoranthene 207-08-9 70 m 0.334 U C11-C22 Aromatics -C22-ALPHA-UJ m 6.67 U CII-C22 Aromatics,Adjusted 1-C22-ALP 1000 m 6.67 U C19-C36 Ali hatics -06-ALPHA 3000 m 6.67 U C9-C18 Ali hatics -C18-ALPHA 1000 m 6.67 U Chrysene 218-01-9 70 In 0.334 U Dibenzo a,h authracene 53-70-3 0.7 m 0.334 U Fluoranthene 206-44-0 1000 In 0.334 U Fluorene 86-73-7 1000 mgIkg 0.334 U Indeno 1,2,3-cd Pyrene 193-39-5 7 m 0.334 U —Naphthalene 91-20-3 4 m 0.334 U Phenauthrene 85-01-8 10 m 0.334 U Pyrene 129-00-0 1000 mgft 0.334 U Alpha Analytical Labs provides this custom reporting format as a convenience to our clients. As such,we cannot be held liable for errors or omissions associated with the regulatory standards listed above and/or the sample results highlighted by comparison with the standards Effective as of June 20,2014). Only compounds detected with reporting limits that exceed the corresponding regulatory standard in at least one sample are included on the summary sheets. Refer to the laboratory report in Adobe Acrobat .PDF format to check results or read any associated project narrative that may be present.In all cases,the signed, hardco y Alpha Analytical Labs laboratory report is the official document for reporting laboratory results. Serial No:05141514:51 s Y HA ANA LYTI CA L - ANALYTICAL REPORT Lab Number: L1509831 Client: Bennett Environmental Associates 1573 Main Street Brewster, MA 02631 ATTN: David Bennett Phone: (508) 896-1706 Project Name: PIERCE-DONAHUE Project Number: BEA15-10764 Report Date: 05/14/15 The original project report/data package is held by Alpha Analytical.This report/data package is paginated and should be reproduced only in its entirety.Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Certifications&Approvals: MA(M-MA086),NY (11148),CT(PH-0574),NH(2003),NJ NELAP(MA935),RI(LA000065),ME(MA00086), PA(68-03671),VA(460195),MD(348),IL(200077),NC(666),TX(T104704476),DOD(1-2217),USDA(Permit #P-330-11-00240)., Eight Walkup Drive,Westborough, MA 01581-1019 508-898-9220 (Fax) 508-898-9193 800-624-9220-www.alphalab.com Page'1 of 41 Serial No:05141514: 1 Project Name: PIERCE-DONAHUE Lab Number: L150983 Project Number: BEA15-10764 Report Date: 05/14/15 Alpha Sample Collection Sample ID Client ID Matrix Location Date/Time Receive Date L1509831-01 SW-N:1-8' SOIL 86 BAXTER RD.,HYANNIS 05/06/15 10:00 05/07/15 L1509831-02 SW-S:6-8' SOIL 86 BAXTER RD.,HYANNIS 05/06/15 10:00 05/07/15 L1509831-03 SW-E:2-8' SOIL 86 BAXTER RD.,HYANNIS 05/06/15 10:00 05/07/15 L1509831-04 SW-W:1-8' SOIL 86 BAXTER RD.,HYANNIS 05/06/15 10:00 05/07/15 L1509831-05 BOH@8' SOIL 86 BAXTER RD.,HYANNIS 05/06/15 10:00 05/07/15 Page 2 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 MADEP MCP Response Action Analytical Report Certification This form provides certifications for all samples performed by MCP methods. Please refer to the Sample Results and Container Information sections of this report for specification of MCP methods used for each analysis.The following questions pertain only to MCP Analytical Methods. An affirmative response to questions A through F is required for"Presumptive Certainty"status A Were all samples received in a condition consistent with those described on the Chain-of- YES Custody, properly preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding times? B Were the analytical method(s) and all associated QC requirements specified in the selected YES CAM protocol(s)followed? C Were all required corrective actions and analytical response actions specified in the selected YES CAM protocol(s) implemented for all identified performance standard non-conformances? D Does the laboratory report comply with all the reporting requirements specified in CAM VII A, YES "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data?" E a. VPH, EPH, and APH Methods only: Was each method conducted without significant YES modifications ? Refer to the individual methods for a list of significant modifications). E b. APH and TO-15 Methods only:Was the complete analyte list reported for each method? N/A F Were all applicable CAM protocol QC and performance standard non-conformances identified YES and evaluated in a laboratory narrative (including all"No"responses to Questions A through E)? A response to questions G, H and I is required for"Presumptive Certainty"status G Were the reporting limits at or below all CAM reporting limits specified in the selected CAM YES protocol(s)? H Were all QC performance standards specified in the CAM protocol(s) achieved? YES I Were results reported for the complete analyte list specified in the selected CAM protocol(s)? YES For any questions answered "No", please refer to the case narrative section on the following page(s). Please note that sample matrix information is located in the Sample Results section of this report. Page 3 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC,for all NELAC accredited parameters.The data presented in this report is organized by parameter(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e.Surrogate Spike Recovery)is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter.If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported,the Laboratory ID of the re-analysis or re-extraction is designated with an"R"or"RE",respectively.When multiple Batch Quality Control elements are reported(e.g.more than one LCS),the associated samples for each element are noted in the grey shaded header line of each data table.Any Laboratory Batch,Sample Specific% recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report.All specific QC information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications.Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted.Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H(CAM)or 4(RCP)when"NO"is checked,the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table.The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold,Alpha's policy is to hold samples(with the exception of Air canisters)free of charge for 21 calendar days from the date the project is completed.After 21 calendar days,we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples.Air canisters will be disposed after 3 business days from the date the project is completed. Please contact Client Services at 800-624-9220 with any questions. I Page 4 of 41 °� Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 Case Narrative(continued) MCP Related Narratives Report Submission All MCP required questions were answered with affirmative responses; therefore,there are no relevant protocol-specific QC and/or performance standard non-conformances to report. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge'and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: J"�,th' Michelle M, Morris Title: Technical Director/Representative Date: 05/14/15 Pa9 e 5 of 41 Serial No:05141514:51 ORGANICS Page 6 of 41 Serial No:05141514:51 PETROLEUM HYDROCARBONS I Page 7 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-01 Date Collected: 05/06/15 10:00 Client ID: SW-N:1-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Analytical Method: 100,VPH-04-1.1 Analytical Date: 05/12/15 01:23 Analyst: BS Percent Solids: 97% 5uality Control Information .1 Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Were samples received in methanol? Covering the Soil Methanol ratio: 1:1 +/-25% Parameter Result Qualifier Units RL MDL Dilution Factor Volatile-Petroleum,Hydrocarbons-Westborough"Lab C5-C8 Aliphatics ND mg/kg 2.81 - 1 C9-C12 Aliphatics ND mg/kg 2.81 - 1 - -----_..._ --- -...._._......_._.._........_..__....-...._--- - - -.......--__... ---- .._.._. _._..._..._.._.. _._..._....------- ----... ...-----...._........ _...._.._.._..._.._.,__....._----- C9-C10 Aromatics ND mg/kg 2.81 - 1 C5-C8 Aliphatics,Adjusted ND mg/kg 2.81 - 1 C9-C12 Aliphatics,Adjusted ND mg/kg 2.81 - 1 Benzene ND mg/kg 0.112 - 1 Toluene ND mg/kg mg/kg 0.112 - 1 __... ........... - - -----..---....... -----...-- —---.... ------------ -- - ----- ------ ...----- - Ethylbenzene ND mg/kg 0.112 - 1 p/m-Xylene ND mg/kg 0.112 - 1 o-Xylene ND mg/kg 0.112 - 1 ----._...---.._..._..-----...._.._......_.._...__.._._..--...._- ._._..__.....------- - --- -- -.._........ --.._.._........._..------- ----._... ----- _ .._.. _ _._..._...._._..- Methyl tert butyl ether ND mg/kg 0.056 - 1 --------._-_..__..-_----...._..-_..___._—._.__.-._-------------�------------------------------ -- --- -...__...----..._---- Naphthalene ND mg/kg 0.225 - 1 Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 127 70-130 2,5-Dibromotoluene-FID 122 70-130 �. Page 8 of 41 Serial No-.05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-01 Date Collected: 05/06/15 10:00 Client ID: SW-N:1-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 98,EPH-04-1.1 Extraction Date: 05/10/15 04:30 Analytical Date: 05/13/15 03:21 Cleanup Method1: EPH-04-1 Analyst: SR Cleanup Date1: 05/11/15 Percent Solids: 97% Quality Control Information - Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbons-Westborough Lab C9-C18 Aliphatics ND mg/kg 6.77 - 1 C19-C36 Aliphatics ND mg/kg 6.77 - 1 C11-C22 Aromatics ND mg/kg 6.77 - 1 ............ ---- ---- .._._..._....._._........._......-.........._.--..._.... - ...._.._.__...._._..---- - ...- ---.._.... --..__.,_.__,....- ...._..-- ..__..........__.._._,.- --._...._..............- .._...._ C11-C22 Aromatics,Adjusted ND mg/kg 6.77 - 1 Naphthalene ND mg/kg 0.338 - 1 _...__..__—_._._._..----------- ------- —.—..-.--- 2-Methylnaphthalene ND mg/kg 0.338 - 1 Acenaphthylene ND mg/kg 0.338 - 1 Acenaphthene ND mg/kg 0.338 - 1 .._._......_..------------.._.._.......---.......------ --...........----._.... —......._...................---------... -.._._... -- ._........._..-----..._..._.__._...__...---.._.__.._......... --- Fluorene ND mg/kg 0.338 - 1 Phenanthrene ND mg/kg 0.338 - 1 Anthracene ND m /k _ 0.338 1 ._........ — __._........__—._......._._-..._..........__...-- _-----------..............._ -....... Fluoranthene ND mg/kg 0.338 - 1 Pyrene ND mg/kg 0.338 - 1 . -.._._...._.-.._._._... ----.._._._._......_....._..- -.._.._..._...----.—..._._... ---- ._...-----............---....---.._.__....----..... ----- Benzo(a)anthracene ND mg/kg 0.338 - 1 Chrysene ND mg/kg 0.338 - 1 -----...------------------ --- ------- ------ - --- -- --._._...-------------_ ------ Benzo(b)fluoranthene ND mg/kg 0.338 - 1 -----._.._...---..._.._._..__......._......._...._......__.........__.._._._.__.....__..__......_....__.._.__.....__...._. - _-- ---._......_..... .._-..._..__........_....._.. -._._.........._._._.__..._._._........_.........._.............................. --._.......--- Benzo(k)fluoranthene ND mg/kg 0.338 - 1 Benzo(a)pyrene ND mg/kg 0.338 - 1 --------- .._..__.._._...._..._...............-_....__.__,_._._.._.___._._..........--.._._..._...__......_.._._..- --....----- ----- ---- _.._.... -----._... ----...------...-_.._...----- -- Indeno(1,2,3-cd)Pyrene ND mg/kg 0.338 - 1 - ----.._... -- -............._.__...--._..._...... -------...-----... -._...------..._....__.._.._.........__.....__._-..__.._.._._—....._ .._._......._..... -_.-..._.............. -- Dibenzo(a,h)anthracene ND mg/kg 0.338 - 1 Benzo(ghi)perylene ND mg/kg 0.338 - 1 Page 9 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-01 Date Collected: 05/06/15 10:00 Client ID: SW-N:1-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field-Prep:" 'Nof Specified" " Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbons Westborough Lab- Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 78 40-140 o-Terphenyl 78 40-140 2-Fluorobiphenyl 79 40-140 2-Bromonaphthalene 80 40-140 i Page 10 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-02 Date Collected: 05/06/15 10:00 Client ID: SW-S:6-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Analytical Method: 100,VPH-04-1.1 Analytical Date: 05/12/15 02:04 Analyst: BS Percent Solids: 97% Quality Control Information Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Were samples received in methanol? Covering the Soil Methanol ratio: 1:1 +/-25% Parameter Result Qualifier Units RL MDL Dilution Factor Volatile Petroleum Hydrocarbon bo s Westborough Lab C5-C8 Aliphatics ND mg/kg 2.85 - 1 _..........---._._..._._.-.._..............--- .....--- __ -.__....------- ----------- ----...... C9-C12 Aliphatics ND mg/kg 2.85 - 1 C9-Cl0 Aromatics ND mg/kg 2.85 - 1 C5-C8 Aliphatics,Adjusted ND mg/kg 2.85 - 1 C9-C12 Aliphatics,Adjusted ND mg/kg 2.85 - 1 ---- -------------- —----------._..----- --- ---._...__... ----- -..�------------ -_ ---.. Benzene ND mg/kg 0.114 - 1 Toluene ND mg/kg 0.114 - 1 ----------------_._.._.................._.._... _...- - - -.._._..---._...__ ---.._......._._..__._..- ---- ------ Ethylbenzene ND mg/kg 0.114 - 1 ---------------- -- --....----—- -- ------- p/m-Xylene ND mg/kg 0.114 - 1 o-Xylene ND mg/kg 0.114 - 1 -------------- -..-------------- - ---------------_ -------- --- _-.._._.__.... _._--.- -- Methyl tert butyl ether ND mg/kg 0.057 - 1 Naphthalene .ND mg/kg 0.228 1 Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 107 70-130 2,5-Dibromotoluene-FID 102 70-130 Page 11 of 41 Serial— No:05141514:51 I Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-02 Date Collected: 05/06/15 10:00 Client ID: SW-S:6-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 98,EPH-04-1.1 Extraction Date: 05/10/15 04:30 Analytical Date: 05/13/15 03:53 Cleanup Method1: EPH-04-1 Analyst: SR Cleanup Date1: 05/11/15 Percent Solids: 97% _ Quality;Control Information F Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbo1ns Westborough Lab•, _ _ _. _ _y '__� C9-C18 Aliphatics ND mg/kg 6.76 - 1 C19-C36 Aliphatics ND mg/kg 6.76 - 1 ..._._.._.__... - ---....._._..._._..._-...__.__........------------- ----------------._....--- ---------------------- -----.... C11-C22 Aromatics ND mg/kg 6.76 - 1 ......._....._..--- -- ...._._..._... _ __ --- ..__._.....------------....- ------ ------ -....-----.._..----- ----_.--...-_ -...__.-.- C11-C22 Aromatics,Adjusted ND mg/kg 6.76 - 1 -------------- ----..----........................ - Naphthalene ND mg/kg 0.338 - 1 ----- -..-_.-.------...----..__._._..------- ------_------------ ----.._._.._..----- - --..__._._......_.....................----..................._._._..._..._......--.._..--....._ 2-Methylnaphthalene ND mg/kg 0.338 - 1 _.. -----.-.....-----------——----------------------.._... ------------ --- Acenaphthylene ND mg/kg 0.338 - 1 Acenaphthene ND mg/kg 0.338 - 1 Fluorene ND mg/kg 0.338 - 1 Phenanthrene ND mg/kg 0.338 - 1 ------------- -------...-- ---- ----------_._... -- ---------._..._.. --.. Anthracene ND mg/kg 0.338 - 1 -------..._..._................._..._.._..-..-_....._... ...-__.._._._.._..------ ----- — -__------- --- ----- --.,.-- - ---------- ------- - -- - - Fluoranthene ND mg/kg 0.338 - 1 _.-..........._.._..-- -- -... --..__...- ...._.--- - --- ---...-- - .._......_..----..._...._...- ------ _....-._..._......_........ - Pyrene ND mg/kg 0.338 - 1 _...---------------.....-- _-....._._._.._..._._...._...._.._.-_-------- __...... --.._._..._...............- -._..........._.._..__... -...._....._._..._......_ _.._.-_.._..... - --._...... _ Benzo(a)anthracene ND mg/kg 0.338 - 1 ------- ---------- - ----......__..----.....---------- ._..... ----- ---- - -----.._.......---- - ...._.........._.... __._............ .._.__._._........__.-_.__. Chrysene ND mg/kg 0.338 - 1 ---- ---...---..-.. ----..---- --------- -- --- ------- -----....__.._._..- --._._....__... ....._..........._..._...._..-- Benzo(b)fluoranthene ND mg/kg 0.338 - 1 Benzo(k)fluoranthene ND mg/kg mg/kg 0.338 - 1 Benzo(a)pyrene ND mg/kg 0.338 - 1 ..........----._._._... -- ----------------- ----------- ------------- ..._-... -- -- ..... -- - Indeno(1,2,3-cd)Pyrene ND mg/kg 0.338 - 1 -......_.............--.--......_.__..._...._... --------..... -.... -.....__..._._......... Dibenzo(a,h)anthracene ND mg/kg 0.338 - 1 .........................................._.._...._._.........................................---------------............................_....--------------.__.._..---..-............. ._.._...._...-- ----._._...-- ------ -----...---- --...- ......_.._._..- Benzo(ghi)perylene ND mg/kg 0.338 - 1 i Page 12 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-02 Date Collected: 05/06/15 10:00 Client ID: SW-S:6-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hyd`rocarbons:=Westborough Labs r r ` Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 67 40-140 o-Terphenyl 82 40-140 2-Fluorobiphenyl 78 40-140 2-Bromonaphthalene 80 40-140 Page 13 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-03 Date Collected: 05/06/15 10:00 Client ID: SW-E:2-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD;HYANNIS Field Prep: Not Specified Matrix: Soil Analytical Method: 100,VPH-04-1.1 Analytical Date: 05/12/15 02:44 Analyst: BS Percent Solids: 96% ' .� Qiial'Ity�Co ®Il6forirreatiori Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Were samples received in methanol? Covering the Soil Methanol ratio: 1:1 +/-25% __J Parameter Result Qualifier Units RL MDL Dilution Factor Volatile Petroleum Hydrocarbons Westborough-Lab C5-C8 Aliphatics ND mg/kg 2.86 - 1 C9-C12 Aliphatics ND mg/kg 2.86 - 1 C9-C10 Aromatics ND mg/kg 2.86 - 1 . . ...._..._...---......._.......................- _ _ _ - - -- -.._.__...._..__..... _-.....__.._..._......_...-_-._....__._.._...---- -----.... -._..._......_•_....._..._..................... ._...._._......-....... C5-C8 Aliphatics,Adjusted ND mg/kg 2.86 - 1 C9-C12 Aliphatics,Adjusted ND mg/kg 2.86 - 1 Benzene ND mg/kg 0.115 - 1 --------...------------ ----- -- -------- ----- -----..- ----.-...--.-------------- ------ Toluene ND mg/kg 0.115 - 1 Ethylbenzene ND mg/kg 0.115 - 1 -------_ _._.._...._.._...-............- ----------------- ----- - - ------ --------.._....._......__...-- p/m-Xylene ND mg/kg 0.115 - 1 o-Xylene ND mg/kg 0.115 - 1 Methyl tert butyl ether ND mg/kg 0.057 - 1 Naphthalene ND mg/kg 0.229 - 1 Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 117 70-130 2,5-Dibromotoluene-FID 112 70-130 Page 14 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-03 Date Collected: 05/06/15 10:00 Client ID: SW-E:2-8' Date Received: 05/07/15 Sample Location: 86 BAXTER kD.,HYANNIS Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 98,EPH-04-1.1 Extraction Date: 05/10/15 04:30 Analytical Date: 05/13/15 04:25 Cleanup Method1: EPH-04-1 Analyst: SR Cleanup Date1: 05/11/15 Percent Solids: 96% Quality Control Information Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbons-Westborough Lab C9-Cl8 Aliphatics ND mg/kg 6.83 — C19-C36 Aliphatics ND mg/kg 6.83 - 1 C11-C22 Aromatics ND mg/kg 6.83 .. - 1 --------- ----- - -_......__...._...- --. -----._.....------ .....-._..... -- C11-C22 Aromatics,Adjusted ND mg/kg 6.83 - 1 Naphthalene ND mg/kg 0.341 - 1 2-Methylnaphthalene -_----- _ -- ND_-..-_ -..---mg/kg-------0.341 ------- 1 --- Acenaphthylene ND _mg/kg...._._.__....__0_341._.....-- ------ ------ ---- --.._..----.._.__....,_..... ..........._.....__..__.-...................... .:------......__.._...__......_._...--------,.-_._..... -- Acenaphthene ND mg/kg 0.341 - 1 ---------._.._..-------- ----------_.-_.._.--,-. -- ------.......------------ --- --- Fluorene ND mg/kg 0.341 - 1 Phenanthrene ND mg/kg 0.341 - 1 Anthracene ND mg/kg 0.341 - 1 Fluoranthene ND mg/kg 0.341 - 1 Pyrene ND mg/kg 0.341 - 1 Benzo(a)anthracene ND mg/kg 0.341 _......_._......_...-._..- 1 - ----.._..-- -.-._.._......-...................__..............---..._._......._.._...__._...._...---..__...__._..- -...__._._....__..._.._...---..._...__......._... Chry sene ND mg/kg 0.341 - 1 Ben . ............... -..............._..._._..--.......-_...-......__.._..._......--__....._._.._... .,._........... .__..-....._.._..-----.._...-- -- ---- Benzo(k)fluoranthene ND mg/kg 0.341 - 1 ----------- ----- ------..- --------------.._...----- --- ---. ...._---------- ---------------- Benzo(a)pyrene ND mg/kg 0.341 - 1 ---------- - - -...__...._....._....._..- .__..... -_....---- ----- - Indeno(1,2,3-cd)Pyrene ND mg/kg 0.341 - 1 Dibenzo(a,h)a nth racene ND mg/kg 0.341 - 1 Benzo(ghi)perylene ND _._._._.._mg/kg --......_-0.341._...------------..__.....__.._.._..�._.:_.. - .. --------............. ---- --- ----------------_. .. Page 15 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-03 Date Collected: 05/06/15 10:00 Client ID: SW-E:2-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.;HYANNIS y Field Prep: Not Specified Parameter Result Qualifier Units RL MDL Dilution Factor Extra file Petroleum;Hydrocarbons;,Westborough Lab ' r t.,' r�� '�is y.. •c i , �,� a_. u- ter .. - Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 52 40-140 o-Terphenyl 68 40-140 2-Fluorobiphenyl 72 40-140 2-Bromonaphthalene 73 40-140 Page 16 of 41 , Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-04 Date Collected: 05/06/15 10:00 Client ID: SW-W:1-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Analytical Method: 100,VPH-04-1.1 Analytical Date: 05/12/15 03:25 Analyst: BS Percent Solids: 96% Quality Control Information Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Were samples received in methanol? Covering the Soil Methanol ratio: 1:1 +/-25% Parameter Result Qualifier Units RL MDL Dilution Factor volatile Petroleum Hydrocarbons-West borough Lab `. r C5-C8 Aliphatics ND mg/kg 2.69 - 1 ..—_—._._....__....__........_..... --- C9-C12 Aliphatics -_ ND----------- --mg/kg --2.669------------ 1 .--- C9-C10 Aromatics ND mg/kg 2.69 1 C5-C8 Aliphatics,Adjusted ND mg/kg 2.69 - 1 -------------._.._..__....._....- - - -....-......._._...._.................---..-_....._.._...__...._..._.,....--_-...........__....... _.._.__...__.._....._....__._..._...__._.._-..._._..._._...----..._,.._.._._.. _.__......._...---- ---- C9-C12 Aliphatics,Adjusted ^ -- ND ------ - mg/kg -- 2.69 -- Benzene------- ---- - ----------ND---------— mg/kg 0.107 - ------ 1------ Toluene ND mg/kg ---- -....--- .._...._............_._.. Ethyibenzene ND mg/kg 0.107 - 1 p/m-Xylene ND mg/kg 0.107 - 1 o-Xylene ND mg/kg 0.107 - 1 --..__...._._.._..._....._.-.-.._ _ ....-_............--... .----......_.-_.....__._...._.._..................._---------------.....----... -.._._...----................—.........-- -- Methyl tert butyl ether ND mg/kg --0_054 -^ 1 Naphthalene ND mg/kg 0.215 - 1 - Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID. 112 70-130 2,5-Dibromotoluene-FID 106 70-130 { Page 17 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-04 Date Collected: 05/06/15 10:00 Client ID: SW-W:1-8' Date Received: 05/07/15 Sample Location: 86 BAXTER-RD.'HYAN NIS Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 98,EPH-04-1.1 Extraction Date: 05/10/15 04:30 Analytical Date: 05/13/15 04:58 Cleanup Method1: EPH-04-1 Analyst: SR Cleanup Date1: 05/11/15 Percent Solids: 96% - Quality Control Information Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method AL Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum Hydrocarbons Westborough Lab ,_: C9-C18 Aliphatics ND mg/kg 6.79 - 1 C19-C36 Aliphatics ND mg/kg 6.79 - 1 .........._..........----- ..._..._..._............_.........._...._._.._.._..._._..----- ...—..-. _-----._.._.._.__..._....---._.......__._...__._.._...._.....— - ----.._..__......._......__._....------------_....._...._......__...._..---- C11-C22 Aromatics ND mg/kg 6.79 - 1 C11-C22 Aromatics,Adjusted ND mg/kg 6.79 - 1 _............ ------_ --- _ _ --,...,..._._.......__..__.._.._.._._...-._._..---------- ---- ...------ --.._...---- - .._..-_-_-.... ------ _..._....__.............._....... Naphthalene ND mg/kg 0.339 - 1 2-Methylnaphthalene ND mg/kg 0.339 - 1 Acenaphthylene ND mg/kg 0.339 - 1 Acenaphthene ND mg/kg 0.339 - 1 Fluorene ND mg/kg 0.339 - 1 -........_...._.._......---- Phenanthrene ND mg/kg 0.339 - 1 Anthracene ND mg/kg 0.339 - 1 ---------- _...........--.......--- ..._..__.....-- -..._..- ...._.....__._..-- Fluoranthene ND mg/kg 0.339 - 1 Pyrene -- ND-----...__..._...---.__....... - - -m-g-/kg-.... ._._....---0.33...9 ..._...._ .__.._.... .._..._._........._..._....._.._.-..._.._....................._........._1.. ..._...._._..._...... Benzo(a)anthracene ND mg/kg 0.339 - 1 Chrysene ND mg/kg 0.339 - 1 Benzo(b)fluoranthene ND mg/kg 0.339 - 1 Benzo(k)fluoranthene ND mg/-kg-----.... -0.3-39 ------- ......_._............... - ----- --.._.----- .__._.._._._-.._.._.__..._......_...... -.._.__.1.. _........._............ Benzo(a)pyrene ND mg/kg 0.339 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.339 - 1 ........_.._....................---..........._......-..... __.._... -..._... -..._.._._..._.._._..-..-..--....__.._..._..........__.....__...- --..__._... ---..._.-------- ---....__.......... ---._.......__._.._... Dibenzo(a,h)anthracene ND mg/kg 0.339 - 1 Benzo(ghi)perylene ND mg/kg 0.339 - 1 hA. Page 18 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: ' L1509831-04 Date Collected: 05/06/15 10:00 Client ID: SW-W:1-8, Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroff yHm drocarbons.-Westborough Lab Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 45 40-140 o-Terphenyl 80 40-140 2-Fluorobiphenyl 76 40-140 i 2-Bromonaphthalene 78 40-140 I Page 19 of 41 Serial No:05141514:51 Project Name: ' PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-05 Date Collected: 05/06/15 10:00 Client ID: BOH@8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS '" —Field Prep: Not Specified Matrix: Soil Analytical Method: 100,VPH-04-1.1 Analytical Date: 05/12/15 04:06 Analyst: BS 1 Percent Solids: 97% -. - Quality Control Infolrmation f:. tro .. Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Were samples received in methanol? Covering the Soil Methanol ratio: 1:1 +/-25% Parameter Result Qualifier Units RL MDL Dilution Factort V6latil-'T a Petroleum Hydrocarbons-Westborough Lab C5-C8 Aliphatics ND mg/kg 2.60 - 1 C9-C12 Aliphatics ND mg/kg 2.60 - 1 C9-Cl0 Aromatics ND mg/kg 2.60 - 1 C5-C8 Aliphatics,Adjusted ND mg/kg 2.60 - 1 C9-C12 Aliphatics,Adjusted ND mg/kg 2.60 - 1 Benzene ND ---- ---- - - -mg/k-g---...--0-.1-0-4 --....__.._._.._._._._.-_ _....._..-- ---- - --.._.—._..--_..... --................. Toluene ND mg/kg 0.104 - 1 --._..._.----...- -.._._...- ------- ------ ---- - ----- --- ---- --- ---...------._.-..-.-.------ - Ethylbenzene ND mg/kg 0.104 - 1 p/m-Xylene ND mg/kg 0.104 - 1 o-Xylene ND mg/kg 0.104 - 1 __....................._.._. Methyl tert butyl ether ND mg/kg 0.052 - 1 - ------ - -- ... --...------- --................. .- Naphthalene ND mg/kg 0.208 - 1 Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 119 70-130 2,5-Dibromotoluene-FID 114 70-130 Page 20 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-05 Date Collected: 05/06/15 10:00 Client ID: BOH@8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix:, Soil Extraction Method: EPA 3546 Analytical Method: 98,EPH-04-1.1 Extraction Date: 05/10/15 04:30 Analytical Date: 05/13/15 05:30 Cleanup Method1: EPH-04-1 Analyst: SR Cleanup Date1: 05/11/15 Percent Solids: 97% Quality Control Information ' Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result .Qualifier Units RL MDL Dilution Factor Extractable Petroleum.Hydrocarbons-Westborough.Lab C9-C18 Aliphatics ND mg/kg 6.78 - 1 C19-C36 Aliphatics ND mg/kg 6.78 - 1 .--._---........_......__._.._........-------— - - ............... --------------._.._...__._..._..--- .._._...__.... - ------ .....-- -.._.._.... - ----...---.._.....,.- C11-C22 Aromatics ND mg/kg 6.78 - 1 -------- — - ---...--------------.._._-....._..........- -_.,._ ----------------— -----_ ---..._....._..-------._.-......_. C11-C22 Aromatics,Adjusted ND mg/kg 6.78 - 1 Naphthalene ND mg/kg 0.339 - 1 2-Methylnaphthalene ND mg/kg 0.339 - 1 - —-------------------------------.....---- ------ —--- --------- .......... ...... __ Acenaphthylene ND mg/kg 0.339 - 1 _......._-......._.._._............_.........._._....-----.._-._........----_.__._....--...--. .._..... —._._......_.._...-- -- -.....--------._.._......_._...._....... -- --- - Acenaphthene ND mg/kg 0.339 - 1 ---------- ------ ---- ---------- ------ -.._....__—..--- —-.._... ---...--......-........------ --- ----- ._.—_.... Fluorene ND mg/kg 0.339 Phenanthrene ND mg/kg 0.339 - 1 Anthracene ND mg/kg 0.339 - 1 Fluoranthene ND mg/kg 0.339 - 1 --._..............-.....--..... ---- ..._...--- ..__..__._._... ..._,.._.__...........- ---....__.-...........--._..._...__...- --......__....--.._._....__..........- --- ...._........---- .....-----......------ ----._.....- -- ----- Pyrene ND mg/kg 0.339 - 1 Benzo(a)anthracene ND mg/kg 0.339 - 1 Chrysene ND mg/kg Benzo(b)fluoranthene ND mg/kg 0.339 - 1 ...................-._._..-.._.......-_-------------- - ----_ ----- ------ --- ---------------._._.._..__. Benzo(k)fluoranthene ND mg/kg 0.339 - 1 -- ----. ------.._...._.._.-.__..........---...- ....--..._.._.........-_.._..--- ....._-._._._........__,_.._...._..._._.. _—_...__.._..__..._._._.._....- -..............................._.....- Benzo(a)pyrene ND mg/kg 0.339 - 1 ---........... .._ Indeno(1,2,3-cd)Pyrene ND mg/kg 0.339 - 1 --...__(j._.--..-------------- _____—._.._.-._.._.---------- ---- ---- -------...__....---- ----..--------- Dibenzo a,h anthracene ND mg/kg 0.339 - 1 Benzo(ghi)perylene ND mg/kg__._...___0.339— -_ ---- - -- 1- _— HA Page 21 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-05 Date Collected: 05/06/15 10:00 Client ID: BOH@8' Date Received: 05/07/15 Sample Location: 86_13AXTER RD.,HYANNIS Field Prep: Not Specified Parameter Result Qualifier Units RL MDL Dilution Factor Extractable Petroleum;.Hydro�carbons tW sese borough Lab Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 79 40-140 o-Terphenyl 83 40-140 2-Fluorobiphenyl 79 40-140 2-Bromonaphthalene 81 40-140 i Page 22 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 . Project Number: BEA15-10764 Report Date: 05/14/15 Method Blank Analysis Batch Quality Control Analytical Method: 98,EPH-04-1.1 Extraction Method: EPA 3546, Analytical Date: 05/13/15 01:45 Extraction Date: 05/10/15 04:30 Analyst: SR Cleanup Method: EPH-04-1 Cleanup Date: 05/11/15 Parameter Result Qualifier Units RL MDL Extractable Petroleum Hydrocarbons-Westborough Lab for sample(s): 01-65 Batch. WG783669-1.. C9-C18 Aliphatics ND mg/kg 6:31 - C19-C36 Aliphatics ND mg/kg 6.31 - C11-C22 Aromatics ND mg/kg 6.31 - C11-C22 Aromatics,Adjusted ND mg/kg 6.31 - ----._._..-...._.........._......_..._..--- ..-._- .._._._._.............---..._..---- _ ......_._._._.....__..... _ --..__...-- ---- ._._.._.....- -- --• - Naphthalene ND mg/kg 0.315 - 2-Methyinaphthalene ND mg/kg 0.315 - Acenaphthylene ND mg/kg 0.315 Acenaphthene ND mg/kg 0.315 - Fluorene .-_----------------ND _-----.—.. mg/kg-----0.315- _ Phenanthrene ND mg/kg 0.315 -- Anthracene ND mg/kg 0.315 - - ...__........_...------------._._.._._..-- Fluoranthene ND mg/kg 0.315 - Pyrene ----------- ----ND---------------mg/kg -------0.315--- -- . Benzo(a)anthracene ND mg/kg 0.315 -- Chrysene ND mg/kg 0.315 - _..-- ..._._..... ....-.._......-...._...--.._.._..----- - ----._.-._ Benzo(b)fluoranthene ND mg/kg 0.315 - Benzo(k)fluoranthene ND mg/kg 0.315 - Benzo(a)pyrene ND mg/kg 0.315 --._......._,..--..._-._..._...- - - -.._......_......-- -- _.....- - .......---......... ------ _...-—-...------- -- Indeno(1,2,3-cd)Pyrene ND mg/kg 0.315 - --------------.._......_...-........_....-- ._...__..._.._......_._-._......._._._..-----------._...------------ -- ------ -_ - Dibenzo(a,h)anthracene ND mg/kg 0.315 - ---- - -----------..._..-- --.._..._---- -....--- ------------------------------- -- - Benzo(ghi)perylene ND mg/kg 0.315 - Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 84 40-140 c-Terphenyl 80 40-140 2-Fluorobiphenyl 82 40-140 2-Bromonaphthalene 83 40-140 Page 23 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831' Project Number: BEA15-10764 Report Date: 05/14/15 Method Blank Analysis Batch Quality Control Analytical Method: 100,VPH-04-1.1 Analytical Date: 05/11/15 11:09 Analyst: BS Parameter Result Qualifier units RL MDL olatile Petroleum Hydrocarbons 1Westborough Lab for:san ple(s): 01-95 Batch: WG78417913 C5-C8 Aliphatics ND mg/kg 2.67 -- ......_.......__._....._ - ---------.... --- —-........ -- ----._._..._..---..._.__._...--------------........_._..----._..__......._.... C9-C12 Aliphatics ND mg/kg 2.67 - C9-C10 Aromatics ND mg/kg 2.67 - _.._-..._..._.._......_...--- -..... ----------- ------ ---- --... - ._..._.._.__......-._....----.._.—_ _ —.-._.-._.._..-_.... _._...- ....._........_..._ C5-C8 Aliphatics,Adjusted ND mg/kg 2.67 - C9-C12 Aliphatics,Adjusted ND mg/kg 2.67 Benzene ND mg/kg 0.107 - Toluene ----------------- ND ----------...._._mg/kg 0.107 -�----- --_--------- Ethylbenzene ND mg/kg 0.107 - p/m-Xylene ND mg/kg 0.107 -- o-Xylene ND mg/kg 0.107 - Methyl tert butyl ether ND mg/kg 0.053 - ---- ..-- ---- -------- --.—_—......__._.-....------------ ---------- ....--------- Naphthalene ND mg/kg 0.213 - Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 97 70-130 2,5-Dibromotoluene-FID 94 70-130 F o.� Page 24 of 41 Serial No:05141514:51 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits Extractable Petroleum Hydrocarbons-Westborough Lab Associated sample(s): 01-05 Batch: WG783609-2 WG783609-3 i—__ C9-C 18 Aliphatics - --_ -- 71--7 - -- - r_627__� - -_ 40-140 14 25 C19-C36 Aliphatics 87 82 40-140 6 25 C 11-C22 Aromatics�- - _ -- - - -r"'91^� _ 103 - _ 40-140 —_ 12 - 25.____ ----- - - Naphthalene r"-78 _ 80 — 40-140 _ — _E_�3�— 25 2-Methylnaphthalene -- - 86 r___89__ -7 40-140 �3� 25 Acenaphthylene - _ 84 r'�86—�_ 40-140 �2� 25 - - Acenaphthene -- r-87 90-7 - 40-140 - �3�` --_ 25 - Fluorene f—89 v _93_ -- - 40-140 �4� - 25 Phenanthrene 90___J F_ 40-140 5 -- 25 - Anthracene _ r 702� �'107 40140 � 75��� 25 Fluoranthene - - --- - - - — I - 92� -- - - --�'-'99'-`�-- 40-140 25------- - - -Pyrene - _- �-94� r�102� 40-140 F_8__'1 - 25 - __- Benzo(a)anthracene 92 101 40-140 9 25 Chrysene 97'Tf 106 40-140 9� 25 _- Benzo(b)fluoranthene _ 95�-1 r-104—, 40-140 25- - Benzo(k)fluoranthene 92 —.101 ^� 40-1409 25 Benzo(a)pyrene r'991 108' 40-140 9--� - 25 Indeno(1,2,3-cd)Pyrene 78 86^----� 40-140 10 25 Dibenzo(a,h)anihracene F'�-92-� =01--- 40-140 . 25 _-- Benzo(ghi)perylene --[-—'93= r-102—, 40-140 25 - _ -- Nonane(C9) 59�� r 47 30-140 r--23--7 25 Page 25 of 41 Ak HA I - Serial No:05141514:51 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits Extractable Petroleum Hydrocarbons-Westborough Lab Associated sample(s):01=05 Batch:WG783609-2WWG783609-3 Decane(C10) - - �`68 58 40-140 F 16 1 25 Dodecane(C12) 77 ��69'T"� 40-140 11 25 Tetradecane(C14) - - �"82 �� 1.- w73"`� 40-140 12 25 - Hexadecane(C16) 84 �'75r�-1 40-140 11 - __-- 25-- --_- - Octadecane(C18) 88 �80�� 40-140 7710 1 25 - Nonadecane(C19) 81^^- 40-140 25 -Eicosane(C20) ---.--- - --- - 1 88i------- �82-� -- -- - --- 40-140 -- - - -25 - -------- Docosane(C22) �`88 �82' ! 40-140 F-7^? 25 Tetracosane(C24) 87 40-140 6�� 25 Hexacosane(C26) - 87 F^82��- - --- -40-140 - F 6'"; 25 ---- - -- Octacosane(C28) F`86 � -80 40-140 7 25 Triacontane(C30) 85 80 40-140 r"�6. 25 Hexatriacontane(C36) 78 72 40-140 �8�, 25 LCS LCSD Acceptance Surrogate %Recovery Qual %Recovery Qual Criteria Chloro-Octadecane 82 67 40-140 o-Terphenyl 92 124 40-140 2-Fluorobiphenyl 89 90 40-140 2-Bromonaphthalene 91 92 40-140 %Naphthalene Breakthrough 0 0 %2-Methyl naphthalene Breakthrough 0 0 Page 26 of 41 Serial No:05141514:51 Lab Control Sample Analysis Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits LVolatileisetroleumlHydrocarbons-Westborough; Assoc iated�sample(s): 01-05 Batch: WG784179-1! WG784179-2 C5-C8 Aliphatics �^ 90 97 70-130 7 25 C9-C12 Aliphatics - 9477, 77100�� 70-130 — 25 C9-C10 Aromatics 89- 1 95 70-130 7 25 Benzene - _-_F �= ��102--7 --- 70-130 F 25_ T Toluene 94 �-'101 � 70-130 �� 25 - - - - - - - -- -- --- --_- .- - - - Ethylbenzene 95 - 102 70-130 25 p/m-Xylene W — r-96--7 -^ -- , - ---_70-130 25 o.Xylene - -- ---— -- �T95'-'� --- -f-102"� -- - _- 70-130 r -• - --6__�___�-1._ .- .--- 25 ----- --- ---- - - Methyl tert butyl ether 103"� 70_130 4 _ 25 99�'� - Naphthalene -- -- - r�92`: _ -- ---r-95 __- _. - . _70-130 --- 25. --- --- 1,2,4-Trimethylbenzene —- ��'t39�� _ —95 -- - 70-130 [--6'- - - 25 Pentane ` - - 867"-� 92'-� 70-130 [T6�1 25 2-Methylpentane-- _-_ - 92 - -��99"-� -�_-- - -70-130 -r_7�_ -25 2,2,4-Trimethylpentane fir^--101�� 70-130 r�"�7� �- 25 r n-Nonane ,94 k _ 1 101 -- _. - - 30 130 L8_^1 -25 �'e'9_7771.n-Decane 4"7, r 100'T�--------- 70-130 _6 � - ---- 25 ------- - n-Butylcyclohexane --_J�96�.t 104 70-130 8" 7 25_ Page 27 of 41 ti� Serial No:051'41514:51 Lab Control Sample Analyses Project Name: PIERCE-DONAHUE Batch Quality Control Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 LCS LCSD %Recovery RPD Parameter %Recovery Qual %Recovery Qual Limits RPD Qual Limits �Uolatlle Petroleum'Hydrocacborls=lNestborough;Laa Associated] ample(s): ,01-05 Batch WG784179 1, WG78.4179-2 r �• ar. c.7"S '3'..A-r-•4oll.leY.. -'-; 6Cr`4t7�::sw'fi.r12. .rr_---mac__ 'a'S� LCS LCSD Acceptance Surrogate %Recovery Qual %Recovery Qual Criteria 2,5-Dibromotoluene-PID 97 102 70-130 25-Dibromotoluene-FID 95 99 70-130 f Page 28 of 41 i Serial No:05141514:51 INORGANICS MISCELLANEOUS '. Page 29 of 41 Serial_No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-01 Date Collected: 05/06/15 10:00 Client ID: SW-N_1-8' Date Received: 05/07/15' Sample Location: 86 BAXTER RD.,HYANNIS . Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst General,Chemistry .WestboroughsLab'"� __ .-_ Solids,Total 97.0 % 0.100 NA 1 - 05/07/15 22:38 30,2540G RT I ' Page 30 of 41 iSeri al_No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-02 Date Collected: 05/06/15 10:00 Client ID: SW-S:6-8' Date Received: 05/07/15 Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units' RL MDL Factor Prepared Analyzed Method Analyst General Chemistry Westborough Lab ` Solids,Total 96.5 % 0.100 NA 1 - 05/07/15 22:38 30,2540G RT r I f Page 31 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 i SAMPLE RESULTS I Lab ID: 1-1509831-03 Date Collected: 05/06/15 10:00 i Client ID:- SW-E:2-8�-- ---- Date Received:- 05/07/15_._ Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst General`Chernistry, lNestborq Lab Solids,Total 96.3 % 0.100 NA 1 - 05/07/15 22:38 30,2540G RT Page 32 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15110764, Report Date: 05/14/15 SAMPLE RESULTS Lab ID: L1509831-04 Date Collected: 05/06/15 10:00 Client ID: SW-W:1-8' Date Received: 05/07/15 Sample Location: 86 sAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst General_Chemistry=:Westborough:Lab = Solids,Total 96.1 % 0.100 NA 1 - 05/07/15 22:38 30,2540G RT I • i - F;A Page 33 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE ' Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 . ! SAMPLE RESULTS Lab ID: L1509831-05 Date Collected: 05/06/15 10:00 Client ID: ` soH@8' - Date Received: - 05/07/15"' - Sample Location: 86 BAXTER RD.,HYANNIS Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RL MDL Factor Prepared Analyzed Method Analyst General ChemigLr.y—estborough,Lab, �` Solids,Total 97.2 % 0.100 NA 1 - 05/07/15 22:38 30,2540G RT Page 34 of 41 i ' I Serial—No:05141514:51 i i Lab Duplicate Analysis { Project Name: PIERCE-DONAHUE Batch Quality Control f Lab Number: L1509831 Project Number: BEA15-10764 j Report Date: 05/14/15 f Parameter Native Sample Duplicate Sample Units RPD Qual RPD Limits 'GeneraI', hemi9t ,WestboroughsLab AssociatedsarnpIi 05. QGrBatch ID: 1NG7$3029 1 _• QC,.SamPle:. 1`509653-01 Zlient ID .DU.P Sample � . :J Solids,Total 90.6 89.8 % -: 1 - 20 I I 1 r 1 II 1 I I d � f 1 i j i 4 i Page 35 of 41 } Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 Sample Receipt and Container Information Were project specific reporting limits specified? YES Reagent H2O Preserved Vials Frozen on: NA Cooler Information Custody-Sea[ Cooler A Absent i Container Information . Temp Container ID Container Type Cooler pH deg C Pres Seal Analysis(*) L1509831-01A Vial McOH preserved A N/A 3.0 Y Absent VPH-DELUX-10(28) L1509831-01 B Glass 120m1/4oz unpreserved A N/A 3.0 Y Absent TS(7),EPH-DELUX-10(14) L1509831-02A Vial McOH preserved A N/A 3.0 Y Absent VPH-DELUX-10(28) L1509831-02B Glass 120mi/4oz unpreserved A N/A 3.0 Y Absent TS(7),EPH-DELUX-10(14) L1509831-03A Vial McOH preserved A N/A 3.0 Y Absent VPH-DELUX-10(28) L1509831-03B Glass 120ml/4oz unpreserved A N/A 3.0 Y Absent TS(7),EPH-DELUX-1 0(14) L1509831-04A Vial McOH preserved A N/A 3.0 Y Absent VPH-DELUX-10(28) L1509831-04B Glass 120m1/4oz unpreserved A N/A 3.0 Y Absent TS(.7.),EPH-DELUX-10(14) L1509831-05A Vial McOH preserved A N/A 3.0 Y Absent VPH-DELUX-10(28) L1509831-05B Glass 120ml/4oz unpreserved A N/A 3.0 Y Absent TS(7),EPH-DELUX-10(14) *Values in parentheses indicate holding time in days Page 36 of 41 Serial_No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L15O9831 Project Number: BEA15-10764 Report Date: 05/14/15 GLOSSARY Acronyms EDL Estimated Detection Limit:This value represents the level to which target analyte concentrations are reported as estimated values,when those target analyte concentrations are quantified below the reporting limit(RL).The EDL includes any adjustments from dilutions,concentrations or moisture content,where applicable.The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction(SPME). EPA Environmental Protection Agency. LCS Laboratory Control Sample:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. LCSD Laboratory Control Sample Duplicate:Refer to LCS. LFB Laboratory Fortified Blank:A sample matrix,free from the analytes of interest,spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. MDL Method Detection Limit:This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit(RL).The MDL includes any adjustments from dilutions,concentrations or moisture content,where applicable. MS Matrix Spike Sample:A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. MSD Matrix Spike Sample Duplicate:Refer to MS. NA Not Applicable. NC Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. NI Not Ignitable. NP Non-Plastic:Term is utilized for the analysis of Atterberg Limits in soil. RL Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration.The RL includes any adjustments from dilutions,concentrations or moisture content,where applicable. RPD Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference(RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. SRM Standard Reference Material:A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. Footnotes 1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. Terms Total:With respect to Organic analyses,a'Total'result is defined as the summation of results for individual isomers or Aroclors.If a'Total' result is requested,the results of its individual components will also be reported.This is applicable to'Total'results for methods 8260,8081 and 8082. Analytical Method:Both the document from which the method originates and the analytical reference method.(Example:EPA 8260B is shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A Spectra identified as"Aldo]Condensation Product". B The analyte was detected above the reporting limit in the associated method blank.Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(IOx)the concentration found in the blank.For MCP-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(10x) the concentration found in the blank.For DOD-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times(1 Ox)the concentration found in the blank AND the analyte was detected above one-half the reporting limit(or above the reporting limit for common lab contaminants)in the associated method blank.For NJ- Air-related projects,flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit.For NJ-related projects(excluding Air),flag only applies to associated field samples that have detectable concentrations of the analyte,which was detected above the reporting limit in the associated method blank or above five times the reporting limit for common lab contaminants(Phthalates,Acetone,Methylene Chloride,2-Butanone). C Co-elution:The target analyte co-elutes with a known lab standard(i.e.surrogate,internal standards,etc.)for co-extracted analyses. D Concentration of analyte was quantified from diluted analysis.Flag only applies to field samples that have detectable concentrations of the analyte. Report Format: Data Usability Report HA Page 37 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 Data Qualifiers E Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. G The concentration may be biased high due to matrix interferences(i.e,co-elution)with non-target compound(s).The result should be considered estimated. H The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. I The lower value for the two columns has been reported due to obvious interference. M Reporting Limit(RL)exceeds the MCP CAM Reporting Limit for this analyte. NJ Presumptive evidence of compound.This represents an estimated concentration for Tentatively Identified Compounds(TICS),where the identification is based on a mass spectral library search. P The RPD between the results for the two columns exceeds the method-specified criteria. Q The quality control sample exceeds the associated acceptance criteria.For DOD-related projects,LCS and/or Continuing Calibration Standard exceedences are also'qualified on all associated sample results. Note:This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than 5x the RL.(Metals only.) R Analytical results are from sample re-analysis. RE Analytical results are from sample re-extraction. S Analytical results are from modified screening analysis. J Estimated value.This represents an estimated concentration for Tentatively Identified Compounds(TICS). ND -Not detected at the reporting limit(RL)for the sample. Report Format: Data Usability Report Page 38 of 41 Serial No:05141514:51 Project Name: PIERCE-DONAHUE Lab Number: L1509831 Project Number: BEA15-10764 Report Date: 05/14/15 REFERENCES 30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA- WPCF. 18th Edition. 1992. 98 Method for the Determination of Extractable Petroleum Hydrocarbons (EPH), MassDEP, May 2004, Revision 1.1 with QC Requirements & Performance Standards for the Analysis of EPH under the Massachusetts Contingency Plan,WSC-CAM-IVB, July 2010. 100 Method for the Determination of Volatile Petroleum Hydrocarbons (VPH), MassDEP, May 2004, Revision 1.1 with QC Requirements & Performance Standards for the Analysis of VPH under the Massachusetts Contingency Plan,WSC-CAM-IVA, July 2010. LIMITATION OF LIABILITIES Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. Page 39 of 41 Serial No:05141514:51 Certification Information Last revised December 16,2014 The following analytes are not included in our NELAP Scope of Accreditation: Westborough Facility EPA 524.2: Acetone, 2-Butanone (Methyl ethyl ketone(MEK)), Tert-butyl alcohol, 2-Hexanone, Tetra hyd rofuran, 1,3,5-Trichlorobenzene,4-Methyl-2-pentanone (MIBK), Carbon disulfide, Diethyl ether. EPA 8260C: 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene, lodomethane (methyl iodide), Methyl methacrylate, Azobenzene. EPA 8270D: 1-Methyl naphthalene, Dimethylnaphthalene,1,4-Diphenylhydrazine. EPA 625:` 4-Chloroaniline, 4-Methylphenol. SM4500: Soil: Total Phosphorus, TKN, NO2, NO3. EPA 9071: Total Petroleum Hydrocarbons, Oil &Grease. Mansfield Facility EPA 8270D: Biphenyl EPA 2540D: TSS EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Tri methyl benzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. The following analytes are included in our Massachusetts DEP Scope of Accreditation,Westborough Facility: Drinking Water EPA 200.8: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,TI; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.1: Mercury; EPA 300.0: Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500E-C, SM4500CN-CE, EPA 180.1,SM213013,SM4500CI-D, SM23206, SM2540C, SM4500H-B EPA 332: Perchlorate. Microbiology: SM921513; SM9223-PIA, SM9223B-Colilert-QT, Enterolert-QT. Non-Potable Water EPA 200.8: AI,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,TI,Zn; EPA 200.7: AI,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,TI,V,Zn; EPA 245.1, SM4500H,B, EPA 120.1, SM251013, SM2540C, SM234013,SM232013, SM4500CL-E, SM4500E-BC, SM426C, SM4500NH3-BH, EPA 350.1:Ammonia-N, LACHAT 10-107-06-1-B:Ammonia-N, SM4500NO3-F, EPA 353.2: Nitrate-*N, SM4500NH3-BC-NES, EPA 351.1,SM4500P-E, SM4500P-B, E, SM52201), EPA 410.4, SM521013,SM5310C, SM4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE,SM25401). EPA 624: Volatile Halocarbons &Aromatics, EPA 608: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs EPA 625: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil. Microbiology: SM9223B-Colilert-QT;Enterolert-QT, SM9222D-MF. For a complete listing of analytes and methods, please contact your Alpha Project Manager. Page 40 of 41. i.. '•' m -.. w 3 a. — CD ie / D �:.::- .5; �+' gyp. d 7 fn va"3:. O � m - m co 0 o f a o N w CO CD V? �i:i>: ;..'.. rye . 'a �'.. .O CO 0 m m o m .9. m m N oo m - ma ..N co .. m m C m fn Co N N > > o p ♦/ O Q c N Z DNS C (~d _ o D 3 (n CD z N m p ny ZFm m �: a. CD CO v m N V N .6 .J o � m3 O m 0 O. 0 p .® .y. v v `o v , j5C m 2 m n T co co (D co'. m o 0 o w� -� w w O Cl) 7 m Q: o Z . C) .. N Q. • O:. ID railm,. 3 o m.ci co . D .o O . 0 O.N # m : w •• :..�. .v. m o 0 0 0 0, Q rn Q m m m m m m CnQ p X 3 3 3 3 3 CD'N ro m o N 3 m U O CL p ro= Z : z a o o 0 0 o m 3 co �m < m m - - 2 V N .•. 7 ... x O 7 m � O O.. N ;Cl y 7 m N D . N 7 C- C- L C- C- :.: CA 2 3 co .« O W m g O m N 6 CD m v; N n .n ❑ ❑ ❑ ® ® ® D Di] ® 0 0 EPH with target PAHs z r *�� v CD . t l r' a; m mo m X' • ,0.1❑ ❑ ❑ ON' ® VPH withtarget BTEX x *" ch :fl:': m N o 4. � ❑ D ❑ ❑ D ❑ ❑ ;w:; `^ 000 r ❑ ❑ ❑ ❑ ❑:❑ z z z ':.' o O o ❑ ❑ ❑ ❑ Dp ❑ r D m . a ❑ D ❑ D ❑ ❑:❑ ❑ .. 0 CL � D . 6 ❑ DD:❑ ❑ ❑ D RL m � r S4: ❑ ❑ ❑ ❑ ❑ ❑ � ® r, J- CD EF a • CD o c, O o m m 2 ❑ ❑ ❑ ❑ ❑ w ~ C W m D~ m m •.O`•,r D me ro - z CD ❑ ❑ D ❑ ❑: o J a. . oCD Na 0 O � C m Xt me m ; �';a:: "'o'Ya.m�:..:•._ •m F to on ari .. U. _ o O m ... a J a.®o.::-t" w. o n o o- z • A. '"3i: m � :.'t�..-.`...t!4m�O tbT�',n1�„ .N N N • Ill '•'y�.J' r Sample Results Comparison with MCP/GW-1 Criteria. CLIENT SAMPLEED SW-N:1-8' SW-S:6-8' SW-E:2-8' SW-W:1-8' BOH 8' SAMPLINGDATE 06-MAY-15 06-MAY-15 06-MAY-15 06-MAY-15 06-MAY-IS LAB SAMYLE ID L1509831-01 L1509831-02 L1509831-03 L1509831-04 L1509831-05 CAS Number SI/G1-14 Units Qual Qual Qual Qual Qual General Chemistry-Westborough Lab Solids,Total t % 97 96.5 96.3 96.1 97.2 Volatile Petroleum Hydrocarbom-Westborough Lab Benzene 7143-2 1 2 m 0.112 U 0.114 U 0.115 U 0.107 lu 0.104 U CS-C8 Aliphatics C8-ALPHA-UJ m 2.81 U 2.85 U 2.86 U 2.69 2.6 U C5-C8 AIi hatics,Adjusted 5-C8-ALPHA 100 m 2.81 U 2.85 U 2.86 U 2.69 2.6 U C9-CIO Aromatics -C10-ALPHA 100 m 2.81 U 2.85 U 2.86 U 2.69 U 2.6 U C9-C12 Ali hatics -C12-ALPHA-UJ m 2.81 U 2.85 U 2.86 U 2.69 U 2.6 U C9-C12 Ali hatics,Adjusted -C12-ALP 1000 m 2.81 U 2.85 U 2.86 U 2.69 U 2.6 U Ethylbenzene 100414 40 m 0.112 U 0.114 U 0.115 U 0.107 U 0.104 U Methyl tert butyl ether 1634-044 0.1 m 0.056 U 0.057 U 0.057 U 0.054 U 0.052 U Naphthalene 91-20-3 4 m 0.225 U 0.228 U 0.229 U 0.215 U 0.208 U o-Xylene 95.47-6 400 m 0.112 U 0.114 U 0.115 U 0.107 U 0.104 U p/m-Xylene 179601-23-1 400 m 0.112 U 0.114 U 0.115 U 0.107 U 0.104 U Toluene 108-88-3 30 m 0.112 U 0.114 U 0.115 U 0.107 U 0.104 U Extractable Petroleum Hydrocarbons;-Westborough Lab 2-Methylna hthalene 91-57-6 0.7 m 0338 U 0338 U 0341 U 0339 U 0339 U Acena hthene 83-32-9170 m 0338 U 0338 U 0341 U 0.339 U 0339 U Acena hthylene 208-96-8m 0338 U 0.338 U 0341 U 0339 U 0339 U Anthracene 120-12-7 m 0.338 U 0338 U 0341 U 0339 U 0339 U Beozo a anthracene 56-55.3m 0338 U 0338 U 0341 U 0339 U 0339 U Benno a cane 50-32-8m 0338 U 0338 U 0341 U 0339 U 0339 U Benzo b fluoranthene 205-99-2m 0338 U 0338 U 0.341 U 0339 U 0339 U Benno hi a lene 191-24-2 m 0338 U 0338 U 0.341 U 0339 U 0339 U Benno k fluoranthene 207-08-9mwkR 0338 U 0338 U 0341 U 0339 U 0339 U C11-C22 Aromatics -C22-ALPHA-UJ m 6.77 U 6.76 U 6.83 U 6.79 U 6.78 U CII-C22 Aromatics,Adjusted I-C27,ALPEU 1000 mgIkg 6.77 U 6.76 U 6.83 U 6.79 U 6.78 U C19-C36 Ali hatics -C36-ALPHA 3000 mgIkg 6.77 U 6.76 U 6.83 U 6.79 U 6.78 U C9-C18 Ali hatics -CIS-ALPHA 1000 mgtkg 6.77 U 6.76 U 6.83 U 6.79 U 6.78 U Chrysene 218-01-9 70 mgft 0338 U 0.338 U 0.341 U 0339 U 0339 U Dibenzo a,h anthracene 53-70.3 0.7 m 0338 U 0338 U 0341 U 0339 U 0339 U Fluoranthene 20644-0 1000 mglkg 0.338 U 0338 U 0341 U 0339 U 0339 U Fluorene 86-73-7 1000 mgft 0338 U 0338 U 0.341 U 0339 U 0339 U Indeno 1,2,3-cd rene -193-39-5 7 mWkg 0338 U 0.338 U 0341 U 0339 U 0339 U Naphthalene 91-20-3 4 mgft 0338 U 0338 U 0341 Ti 0339 U 0339 U Phenanthrene 85-01-8 10 m 0338 U 0338 U 0341 U 0.339 U 0.339 U Pyrene 129-00.0 1000 mglkg 0338 U 0338 U 0341 U 0339 U 0339 U Alpha Analytical Labs provides this custom reporting format as a convenience to our clients. As such,we cannot be held liable for errors or omissions associated with the regulatory standards listed above and/or the sample results highlighted by corn arison with the standards Effective as of June 20,2014). Only compounds detected with reporting th limits at exceed the corresponding ulato standard in at least one sample are included on the summary sheets. Refer to the laboratory report in Adobe Acrobat .POF format to check results or read any associated project narrative that may be present.In all cases the signed hardcopy Alpha Analytical Labs laboratoryreport is the official document for reportinp laboratory results. Route 132 BARNSTABLE REFERENCE MA Route 25 Route 28 - PLAN TITLED "SUBDIVISION PLAN OF LAND IN BARNSTABLE", PREPARED BY JOSEPH SELWYN, CIVIL ENGINEER, DATED 7/23/49 - TOWN OF BARNSTABLE ASSESSOR'S MAP 3 10 PARCEL 109 ots NOTE: THIS SITE PLAN WAS NOT PREPARED FROM ANY INSTRUMENT SURVEY AND v UNDER NO CIRCUMSTANCES SHOULD THE DISTANCES, BEARING AND/OR OTHER __ a FEATURES SHOWN BE USED TO ESTABLISH PROPERTY LINES. � m LOCUS EXISTING 275-gal �a�ut5r FUEL OIL AST KEY MAP LEGEND EXTENT OF SOIL REMOVAL 10' x 7' x 8'(D) HB HAND BORING FEED AND RETURN LINES FORMER 275-gal UST Off' my -4 HB-5 "HB-I /HB-2 / HB-G H B-3/ H B-7 SEE DETAIL 0 6U��h�go Q SHED Q BASEMENT/EXTERIOR DETAIL SCALE 1"=5' / LOCUS / �x 8G BARTER ROAD 40 �x Project: RUBY PIERCE and JAMES DONOHUE 27 CEDAR STREET- CAMBRIDGE,MA 02140 Title: LIMITED REMOVAL ACTION COMPLETION 86 BAXTER ROAD-HYANNIS,MA 02601 BENNETT ENVIRONMENTAL SITE PLAN BEA ASSOCIATES, INC. LICENSED SITE PROFESSIONALS, ENVIRONMENTAL SCIENTISTS, 0 20 40 GO GEOLOGISTS, ENGINEERS 1573 MAIN STREET,P.O. BOX 1743,BREWSTER,MA 02631 PHONE:(508)896-1706 www.bennett-ea.com FAX:(508)896-5109 SCALE 1 "=20' DATE SCALE BY CHECK JOB NUMBER 05/06/15 As Noted SRF JTW BEA15-10764