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0143 OLD YARMOUTH ROAD - Health
143 OId Yarmouth Road Hyannis 4en n A 344 WSW* 02 _ 4 I y F t i I� �I „I zz� Date: 10/2Y 113 TOWN OF BARNSTABLE TOXIC AND HAZARDOUS MATERIALS -111 FORM NAME OF BUSINESS: 4<4,<AS eokk BUSINESS LOCATION: lLt-6 ©lob k< k4,, Y EE k.nvt,s INVENTORY MAILING ADDRESS: 5o 6!,r a-(- w��1, 0;L6`/-6, TOTAL AMOUNT: TELEPHONE NUMBER: Sao 6- 4 oo- 7602 e 111 D a o s CONTACT PERSON: _ Ka ,� Ay c yv EMERGENCY CONTACT TELEPHONE NUMBER: MSDS ON SITE? TYPE OF BUSINESS: $m�`�' �'�a��/ d✓�a�ti�canaKc�� 5�ora�ft- �1e5 - �oa��gal INFORMATION / RECOMMENDATIONS: '� ( D�a-�e_ �18�51o�.n�c�a1 Fire District: U,V?5 11 re 1<eZ 10 QWC s 0; hWU,(- 4 I 3,0064-1, 000 -'- ) 5 -�' -f'o �Ya,ts�e15•ht o a 4.51'G Mct "9'S Co( ��cz � 2Y 3) r1bor io-I v,- 19•►,9 2 a Y� ,��arL�' r2.o64f• L i'oma--4-avvk,cc-vtova-.t i&;�iKI-�- ,�� a Svice, a. cmrfikivw�5 a ct. I b f an� c � L)�-S oge.,' �°ode.w}s Flo long�� aSte T aZn p-olr Won: `�ast shipment o�haz4a'c)ous �nraste:� V • Name of Hauler: ��'-1"<avtg0o<�- Destination-�*,5f kee,O recoas ori-f e!:,s,io,,Ktf,.es� Waste Product: Licensed? Yes No `F cQaeg oQ� spr�sQ-� NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous material use, storage and disposal of 111 gallons or more a month requires a license from the Public Health Division. LIST OF TOXIC AND HAZARDOUS MATERIALS The Board of Health and the Public Health Division have determined that the following products exhibit toxic or hazardous characteristics and must be registered regardless of volume. Observed / Maximum Observed / Maximum y Antifreeze (for gasoline or coolant systems) Miscellaneous Corrosive E(NEW ❑ USED Cesspool cleaners Automatic transmission fluid Disinfectants Engine and radiator flushes Road salts (Halite) Hydraulic fluid (including brake fluid) Refrigerants SZ Mfotor Oils Pesticides l�J NEW USED,f o �" ;.-I All*w (insecticides, herbicides, rodenticides) +,vg �e'M Photochemicals (Fixers) Gasoline, Jet fuel,Aviation gas Diesel Fuel, kerosene, #2 heating oil ❑ NEW ❑ USED Miscellaneous petroleum products: grease, Photochemicals (Developer) lubricants, gear oil ❑ NEW ❑ USED Degreasers for engines and metal Printing ink Degreasers for driveways&garages Wood preservatives (creosote) Caulk/Grout Swimming pool chlorine 3 Battery acid (electrolyte)/Batteries Lye or caustic soda Rustproofers Miscellaneous Combustible Car wash detergents Leather dyes Car waxes and polishes Fertilizers Asphalt& roofing tar PCB's Paints, varnishes, stains, dyes Other chlorinated hydrocarbons, fl Lacquer thinners(I KC-. 2. M15K) (including carbon tetrachloride) ❑ NEW ❑ USED Any other products with "poison" labels (including chloroform, formaldehyde, Paint&varnish removers, deglossers hydrochloric acid, other acids) Miscellaneous. Flammables Other products not listed which you feel Floor&furniture strippers may be toxic or hazardous (please list): Metal polishes Q< ' 8& 64 5 iy, aou-ss XimoviyLa Laundry soil &stain removers (including bleach) bk S Spot removers&cleaning fluids n (dry cleaners) vk4' o,C,L je lg bey �5�c�d� Other cleaning solvents 1 Bug and tar removers �t I 6L Moves to 4 44 e, Windshield wash 1`1�001CIL,—TIC b4 6 W A WHITE COPY-HEALTH DEPARTMENT/CANARY COPY-BUSINESS Applicant's lSignature ff Staff's niti I VAG`/ I V1,L I VI�l2yt1'�� - y Ha and us Materials Inventory Sheet Checklist 9 .6 Date Physical Street Address-Check database to ensure it exists Working Phone Number Actual Amounts -( ie. gas being used to fuel machines, thinner to clean brushes all count as hazardous materials-no blanks) Storage Information - location of storage, how long is storage for? If none, note that. Disposal Information =where and who? If none, note that. --Applicant Signature -understand what is listed and noted taff Initial -any questions, know who to ask Vehicle Washing/Rinsing? -give a vehicle washing policy and •t. explain it I- Attach the Business Certificate with your sign off and comments **The inventory form should explain what the business consists of and the procedures they are doing. Notes need to be left to explain what you discussed with them. L YOU WISH TO OPEN A BUSINESS? 0 For Your information: Business certificates (cost$40.00 for 4 years). A business certificate ONLY REGISTERS YOUR NAME in town (which you must do by M.G.L.-it does not give you permission to operate.) Business Certificates are available at the Town Clerlc s Office, 1"FL., 367 Main Street, Hyannis, MA 02601 (Town Hall) DATE: 09 2' /7011 Fill in please: APPLICANT'S YOUR NAME/S: `l1/ Ta n/'pk1r1SoA/ C- AL Uf 5 BUSINESS YOUR HOME ADDRESS: L c $ - itrlq 12Z .6Lf .3 TELEPHONE # Home Telephone Number M$ L1 Z '9 - 23 Z 1, NAME OF CORPORATION: V C . NAME OF NEW BUSINESS '1- Q(J tc) TYPE OF BUSINESS AL ES IS THIS A HOME OCCUPATION? YES NO ADDRESS OF BUSINESS 1, f-t l{ . AWi�5-/dkAP/PARCEL NUMBER (Assessing) i When'starting a new business there are several things you must do in order to be in compliance th the rrukles and regulations of the Town of Barnstable. This form is intended to assist you in obtaining the information you may need. You MUST GO TO 200 Main.St. - (corner of Yarmouth Rd. & Main Street) to make sure you have the appropriate permits and licenses required to legally operate your business in this town. 1: BUILDING COMMISSIONER'S OFFIC This individual has beoninforme o any permit requirements that pertain to this type of business. tho'ized Signature COMMENTS: 420 N ni ia 2. BOARD OF HEALTH This individual h en in ed of the permit re uiremants that pertain to this type of busine Authorized gnature* COMMENTS: :MUSt'vianyvM AIM �FAZARDOUS MATFRIai S REGULATIONS 3. CONSUMER AFFAIRS (LICENSING AUTHORITY) This individual has been informed of the licensing requirements that pertain to this type of business. Authorized Signature' . COMMENTS: r . Date:Oq/211�/21011 �- 6 TOWN OF BARNSTABLE TOXIC AND HAZARDOUS MATERIALS ON-SITE INVENTORY NAME OF BUSINESS: T AL/to BUSINESS LOCATION: N3 UL A yMKMQVIA 01) , N IRAIAI S - A4d v+ INVENTORY MAILING ADDRESS: FLEs-r Ueygio PAt-1-1 , MARSTOWS,v /LL S - 44l9 TOTAL AMOUNT: TELEPHONE NUMBER: 5og - 3 60 - loz o CONTACT PERSON: k1AA10CR.50i1 AL VC5 EMERGENCY CONTACT TELEPHONE NUMBER: Sog-3 6o- !D Zo MSDS ON SITE? TYPE OF BUSINESS: C L A S5 it A pro SALES INFORMATION/RECOMMENDATIONS: Fire District: Waste Transportation: Last shipment of hazardous waste: Name of Hauler: Destination: Waste Product: Licensed? Yes No NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous material use, storage and disposal of 111 gallons or more a month requires a license from the Public Health Division. LIST OF TOXIC AND HAZARDOUS MATERIALS The board of health and the Public Health Division have determined that the following products exhibit toxic or hazardous characteristics and must be registered regardless of volume. Observed / Maximum Observed / Maximum Antifreeze (for gasoline or coolant systems) Miscellaneous Corrosive ❑ NEW ❑ USED Cesspool cleaners Automatic transmission fluid Disinfectants Engine and radiator flushes Road salts (Halite) Hydraulic fluid (including brake fluid) Refrigerants Motor Oils Pesticides ❑ NEW ❑ USED (insecticides, herbicides, rodenticides) Gasoline, Jet fuel,Aviation gas Photochemicals (Fixers) Diesel Fuel, kerosene,#2 heating oil ❑ NEW ❑ USED Miscellaneous petroleum products: grease, Photochemicals (Developer) lubricants, gear oil ❑ NEW ❑ USED Degreasers for engines and metal Printing ink Degreasers for driveways&garages Wood preservatives (creosote) Caulk/Grout Swimming pool chlorine Battery acid (electrolyte)/Batteries Lye or caustic soda Rustproofers Miscellaneous Combustible Car wash detergents Leather dyes S d n Car waxes and polishes Fertilizers Asphalt& roofing tar PCB's Paints, varnishes, stains, dyes Other chlorinated hydrocarbons, Lacquer thinners (including carbon tetrachloride) ❑ NEW ❑ USED Any other products with "poison" labels -- - - - _ (including chloroform, formaldehyde, Paint&varnish removers, deglossers hydrochloric acid, other acids) Miscellaneous. Flammables Other products not listed which you feel Floor&furniture strippers may be toxic or hazardous`(please list): Metal polishes Laundry soil &stain removers /l �• 3 (including bleach) Spot removers&cleaning fluids (dry cleaners) Other cleaning solvents Bug and tar removers Windshield wash WHITE COPY-HEALTH DEPARTMENT/CANARY COPY-BUSINESS Applicant's Signature Staff's Initials YOU WISH TO.OPEN A BUSINESS? For Your Information: Business certificates(cost$30.00 for 4 years). A business certificate ONLY REGISTERS YOUR NAME in town(which you must do by M.G.L.-it does not give you permission to operate.) Business Certificates are available at the Town Clerk's Office, 1' FL.,367 Main Street, Hyannis, MA 02601 (Town.Hall) DATE: - O 6 Fill in please: 1 APPLICANT'S YOUR NAME: C1 Go g Q 0 NG ROD 6 +� BUSINESS YOUR HOME ADDRESS: 'a 7 G9 6-E6,16 L PATTO N P H `Wvlvl� TELEPHONE # Home Telephone Number 7T=g-'2,G Q IS NAME,OF NEW BUSINESS \1/'Q6.PG G( Ob A L 6 c- 7 Yot QF BI.ISINI=SS U C ti C.�� IS THIS A HOME OCOUPA- ON'0 YES ,�Nfl 1-lave yd'u b°eei n given approval frwr the .building da--Isioh'�. YES NO . ADOFI;ESS OF BUSCNESS ( LI 3 ,n L; - D C? 1 MAP/PARCEL N.UMBI;R r- .�. When starting a new business there are several things you must do in order to be in compliance with the rules and regulations of the Town of Barnstable. This form is intended to assist you in obtaining the information you may need. You MUST. GO TO 200 Main St. - (corner of Yarmouth Rd.&Main Street) to make sure you have the appropriate permits and licenses required to legally operate your business in this town. 1. BUILDING COM ER'S OFFICE This individ al s n in a any perrAit requirements that pertain to this type of business. Aut onzed nature** I- , pMMENT f S CC . 2. BOARD OF HEALTH. This individual has bbp_qp4nform d of th ermit requirements that pertain to this type of business. Authorize Signature COMMENTS: 3. CONSUMER-AFFAIRS(LICENSING AUTHORITY) This individual has been informed of the licensing requirements that pertain to this type of business. Authorized Signature* COMMENTS: .- .,w .� �'--`-�-.+..�:•-•.rr-y,(;C,...•�.TcM'�`�r+-..+-.m-r•_.:..-��.�,...frtrr�(4Y!`�,,Sri,•rU.•..�-''�, .s�k''''"Y'�^..�ik-.:f=���,� .'-s''°'�9.,r�.- ,....�i[•,-„-�^�r^;�r-..Re... - ,;}. i 4 TOWN OF BARNSTABLE Date: ........a................�.................... ®'New Application * LICENSE APPLICATION r BMWSenaLE, # El 9 MASS. g 200 Main Street 1639• ,a ❑ Transfer Hyannis;MA 02601 �``'`""' .• � •-�"'�.� Other 508-862-4674 ~�-� NO BUSINESS MAY OPERATE WITHOUT A VALID LICENSE ON THE PRENnsES s r Name of appljcanVcorporation:, A.u_ _v� ,_-NCW0. (A. t) U�1._ti Al RN 6 If 6. Home phone#: ��__���...1.._�_6 Address of applicant/corporatibn:�I .G-!J 6= ..- -..-:..�-�- ©- + Ni ..- Business phone#: - -- ......... ................ _._........._............................_......__.._..............._---........--......... _...-- D/B/Ao .... Business phonA.#: ----------_._..._....__.___._._.__...._._.__._....._.__.._____..__. Business location: 1 __..Q-L 1) N) A/2M_[7 Q°C.._H....__A�.z.-.--_.-.-'-.-'---. - - - -._..._.._._._._...-- ------ ------------...- - -._...- ._._....- -------... --- Business mailing address: _._..._ _ Local business address: Local mailing address: ---.....---------------------- LICENSE TYPE: .. Q...... .. ..! .. .. .5...........G...G.�.......��... .................................. Annual ®° Seasonal HOURS OF OPERATION: (1.10 __....._...._......................_S..A .._..... FID#:.. _ Name of manager: .- fhl .C ... _.........._.:....._.._._.._.._...... e • maa.l Local mailing address: ,7..._C .to.. ...r'�..! ... -......(P�1'�.'' ' "........4......p"#"4 ..:�.! .,;.�....4�............M..�..........0_ 2...6.j.I.......... Manager's Permanent mailing address_ 5 A M( C. .._... Manager's home phone#: 5__Dfr S3�I_-q_3S I- Business phone#: _7._� W- 9 3G -0-5.. 14 u; ......_._ E. Name of property owe: C y 6-ity�Q n 50 ASSESSOR'S MAP/PARCEL# MAP n4 ............ PARCEL 3 a List any flammable substance or hazardous waste used in business(specify): rwl C 71 Applic ant s„ti,mustr "contact the Building Commissioner's office, (508) 862-4038, h.: _._ the Bo Health office, (508) 862-4644, and the appropriate Fire District office'. to=�schedule inspections. r. ; Signature of applicant,_' � (7 _I Xown use c7? REAL ESTATE TAXES PAID IN FULL PAYMENT AGREEMENT IN EFFECT ON IS THIS USE PERMITTED WITHIN THIS ZONING DISTRICT? YES ❑ NO ❑ INSPECTORS APPROVAL " Capacity set by Building Division................................._.............................................. Building/Zoning..............._.._........._..................._............-................._........ Date ........._...................................._................_._......... Board of Health..............................................._..................................................._......_._.... Date _................._.................._..._............................_... Wire ....................................................._......._......... Date ..... ...........-............. Plumbing .-.......-..............._........_......._......._............_................__._......Date ..._._........._......._....._.................._............. Gas Date .... ............................................... Fire District .. .v......_......._......._....__....................................._... Date --._._......_.....--....._.................................. Comments:....................................................... ................................................................:t......................_........_...._...._..._....................................................................._..............._.................... White-Licensing Authority Canary-Health Division Gold--Building Commissioner Pink-Fire Department Dater /2q/6& TOWN OF BARNSTABLE TOXIC AND HAZARDOUS MATERIALS ON-SITE INVENTOR a D NAME OF BUSINESS: BUSINESS LOCATION: old 7INVENTORY MAILING ADDRESS: '� j1 TOTAL AMOUNT: TELEPHONE NUMBER: CONTACT PERSON: . l t�T/2 n ikli 1-in EMERGENCY CONTACT TELEPHONE NUMBER: MSDS ON SITE? _ u TYPE OF BUSINESS: ' INFORMATION/RECOMMENDATIONS: Fire D'strict: Waste Transportation: Last shipment of hazardous waste: Name of Haulers Destination: Waste Product: Licensed? Yes No NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous materials use, storage and disposal of 111 gallons or more a month requires a license from the Public Health Division. LIST OF TOXIC AND HAZARDOUS MATERIALS The Board of Health and the Public Health Division have determined that the following products exhibit toxic or hazardous characteristics and must be registered regardless of volume. Observed/Maximum Observed/Maximum _ Antifreeze (for gasoline or coolant systems) _ Misc. Corrosive NEW USED Cesspool cleaners Automatic transmission fluid Disinfectants Engine and radiator flushes Road Salts (Halite) Hydraulic fluid (including brake fluid) Refrigerants Motor Oils Pesticides NEW USED (insecticides, herbicides, rodenticides) Gasoline, Jet fuel, Aviation gas Photochemicals (Fixers) Diesel Fuel, kerosene, #2 heating oil NEW USED Misc. petroleum products: grease, Photochemicals (Developer) lubricants, gear oil NEW USED Degreasers for engines and metal Printing ink Degreasers for driveways &garages Wood preservatives (creosote) Caulk/Grout Swimming pool chlorine Battery acid (electrolyte)/Batteries Lye or caustic soda Rustproofers Misc. Combustible Car wash detergents Leather dyes Car waxes and polishes Fertilizers Asphalt & roofing tar PCB's Paints, varnishes, stains, dyes Other chlorinated hydrocarbons, Lacquer thinners (inc. carbon tetrachloride) NEW USED Any other products with "poison" labels Paint &varnish removers, deglossers (including chloroform, formaldehyde, Misc. Flammables hydrochloric acid, other acids) Floor&furniture strippers Other products not listed which you feel I Metal polishes may be toxic or hazardous (please list): Laundry soil & stain removers x U1W tuv(4 a (including bleach) ' �A d.:4 . Spot removers & cleaning fluids (dry cleaners) Other cleaning solvents Bug and tar removers Windshield wash WHITE COPY-HEALTH DEPARTMENT/CANARY COPY-BUSINESS �I YOU WISH TO.OPEN A BUSINESS? For Your Information: Business certificates(cost$30.00 for 4 years). A business certificate ONLY REGISTERS YOUR NAME in town(which you must do by M.G.L.-it does not give you.permission to operate.) Business Certificates are available at the Town Clerk's Office, I FL,367 Main Street, Hyannis, MA 02601 (Town Hall) DATE: Fill in please: APPLICANT'S YOUR NAME: A BUSINESS YOUR HOME ADDRESS: fGC�IaTAy D 4VAWKS -AAA 69 TELEPHONE # Home Telephone Number NAME. AOF NEW BUSINESS TYPE OF BUSINESS is THIS DOME.0.CCUPATIIONO YES �.Nt:9 7:7 ._ 777 Have you been given.approval from the building division. YES N0 MAP/PARCEL NUMBER yy� 6� SOD ADDRESS OF BUSINESS When starting a new business there are several.things you must do in order to be in compliance with the rules and regulations of the Town of Barnstable. This form is intended to assist you in obtaining the information you may need. You MUST GO TO 200 Main St. - (corner of Yarmouth Rd.&Main Street) to make sure you have the appropriate permits and licenses required to legally operate your business in this town. 1. BUILDING COMMISSIONE FFICE This individual ha be rmed oftny permit requirements that pertain to this type of business. uthorized Signatur COMMENTS: 2. BOARD OF HEALTH This individual has bee f of rmit requirements that pertain to this type of business. A horized Signature** COMME TS: Ocoag•r�, Frr- �a &-2— /pix-4- Oki S i�P �%SCE . -k) --lf4S'd=�P� L' n n ddba 3. CONSUMER AFFAIRS (LICENSING AUTHORITY) This individual has been informed of the licensing requirements that pertain to this type of business. Authorized Signature* COMMENTS: Dater /if /U TOWN OF BARNSTABLE TOXIC AND HAZARDOUS MATERIALS ON-SITE INVENTORY" , N� NAME OF BUSINESS: /-�UfiO � � �3 C��O YA�MOIr� R,D 4%/a'Ni5 -A" )NEVJLOCA ►X BUSINESS LOCATION: __SQA Q W M On ;&n4461- 44A INVENTO�IRY MAILING ADDRESS:Qn 6nl- TOTAL AMOUNT: TELEPHONE NUMBER:� '- 0� CONTACT PERSON:�/4�► Z 14►AA✓i/ EMERGENCY CONTACT TELEPHONE NUMBER: S4 MSDS ON SITE? TYPE OF BUSINESS: US 6?S E)Ig A,_1 F IS INFORMATION/RECOMMENDATIONS: Fire District: Waste Transportation: Last shipment of hazardous,waste: Name of Hauler: Destination: Waste Product: Licensed? Yes No NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous materials use, storage and disposal of 111 gallons or more a month requires a license from the Public Health Division. LIST OF TOXIC AND HAZARDOUS MATERIALS The Board of Health and the Public Health Division have determined that the following products exhibit toxic or hazardous characteristics and must be registered regardless of volume. Observed/Maximum Observed/Maximum Antifreeze (for gasoline or coolant systems) Misc. Corrosive NEW USED Cesspool cleaners Automatic transmission fluid Disinfectants Engine and radiator flushes Road Salts (Halite) Hydraulic fluid (including brake fluid) Refrigerants Motor Oils Pesticides NEW USED (insecticides, herbicides, rodenticides) Gasoline, Jet fuel, Aviation gas Photochemicals (Fixers) Diesel Fuel, kerosene, #2 heating oil NEW USED Misc. petroleum products: grease, Photochemicals (Developer) lubricants, gear oil NEW USED Degreasers for engines and metal Printing ink Degreasers for driveways &garages Wood preservatives (creosote) Caulk/Grout Swimming pool chlorine Battery acid (electrolyte)/Batteries Lye or caustic soda Rustproofers I Misc. Combustible Car wash detergents Leather dyes Car waxes and polishes Fertilizers Asphalt & roofing tar PCB's Paints, varnishes, stains, dyes Other chlorinated hydrocarbons, Lacquer thinners (inc. carbon tetrachloride) NEW USED Any other products with "poison" labels Paint &varnish removers, deglossers (including chloroform, formaldehyde, Misc. Flammables hydrochloric acid, other acids) Floor &furniture strippers Other products not listed which you feel Metal polishes may be toxic or hazardous (please list): Laundry soil & stain removers 0 -411 ems 4okc ,s /O CAX &,IAsk (including bleach) Spot removers & cleaning fluids y � I (dry cleaners) Other cleaning solvents Bug and tar removers Windshield wash WHITE COPY-HEALTH DEPARTMENT/CANARY COPY-BUSINESS LOCATION SEWAGE PERMIT NO. VILLAGE INSTA LLER'S NAME & ADDRESS Covooyer BUILDER OR OWNER DATE PERMIT ISSUED 7 'c-- 7 DATE COMPLIANCE ISSUED ? _ � '= 749 � ��,�� ` , i `� � � .. X � _� � � ' r J . �� � R._.-� a_ 0-0No. ...... - �y- FizB.....�...:�............ ` THE COMMONWEALTH OF MASSACHUSETTS BOARD O HEA T _ -------OF.......... Applira#ion for Dispngal Works Toustrurtinn Vamit Application is hereby made for a Permit to Construct (L<or Repair ( ) an Individual Sewage Disposal System at: GGQ �/?,�lDYM P'0, ..................................................... ........... __ ............. ...... ...--------- - Locat•n Address f� or Lot No. ---.._.._1 � ---------- 1�.rfo 6.24?C KS 21 iu !''.b 3'1,� 4 ca a 3 -------------- .--•- ---------- Owner / Address (ra 61+W fir' --------- Installer ('t t' f D��e..........................rJ ,t>t .�/t Address of TypeDwellindingNo. of Bedrooms_._.._.._ Size Lot..G';>� G'...--Sq. feet U g— ...._.....Expansion Attic ( ) Garbage Grinder (—}-- P4 Other—Type of Building _fir-4 k:6-C........ No. of persons..........?-............ Showers ( /) — Cafeteria ( --�- Q' Other fixtures o s ce i- u .�"°..-..--- ------��a>C---------- . ...• r W Design Flow..........1,?-.6.........................gallons per person per day. Total daily flow____........._......_....................___gallons. WSeptic Tank—Liquid capacity// ..gallons Length................ Width-_-____-___.-_-. Diameter__--____-____- Depth................ Disposal Trench—No..................... Width.................... Total Length.................... Total leaching area.....................sq. ft. Seepage Pit No.— __-- Diameter .... ........... Depth below inlet...:-`....... Total leaching area' T sq. ft. Z Other Distribution box (j) Dosing tank ( ) Percolation Test Results Performed by______________________ �� Date_;'s o a 7� . -------•---•---------------------•-•••.... . .-................................. 'y `` Test Pit No. 1......�._.__minutes per inch Depth of Test Pit----54.._..._... Depth to ground water________________________ Test Pit No. 2................minutes per inch Depth of Test Pit..................... Depth to ground water........................ RS •-------------------------••-•••--------•-••-•. -----------------------•--•--••-----•-•--........---•--......-----...---...•............._.---••-.-------- 0 Description of Soil.......................... Q1 .t ............. ----------------...------•--------------•-------------•--------............---- x V ....-•-•-•••••••---•••••-•--••--•--•-•------••------•------•-•---••---------•------•.................••-----••-••-••--•--------•----•-••----.....--•------••-•--••-•--•-----•---•----.....-••----•-- W ----•-••--••-----•-------------•-•••--•-•--•-•-•--•-•--•----------------•-•-•._....-••-•-......--"----•------•-----------------•----•-•-----.................. = ......... UNature of Repairs or Alterations—Answer when applicable....................................................•___.__._......................._........... ----------------------------•-----•----------------------•----------- ...------••----•----•......•------•----------------......------------------•---------•-------------------------------•---- Agreement: r, The undersigned agrees to install the aforedescribed Individual Sewage Disposal System in accordance with the provisions of iI'I'M 5 of the State Sanitary Code— The undersigned further agrees not to place the system in operation until a Certificate of Compliance has been issued by the board of health. Sign --- Date y Application Approved By. = ---------------------- --- d- Date Application Disapproved for 1he following reasons--------------------------•-•-------------•---------------------------------------------------•••--•-------_-.... ------------------------•-••----•---------------------------.•.......------•----------------------...---•--------------------------------------•--------------------------------....--.---•------•----. Date Permit No. - Issued-- ................................................ Date _" C-77;� No----------------_------- t ' FEB.............................. THE COMMONWEALTH OF MASSACHUSETTS A RD EE m Appliraation for Ui4pniial Works Cnondrurtioaa raml x xt `Application is hereby made for a Permit to Const or Repair. ( ) an Individual Sewage Disposal ;.... system at ' r Loca ion-Address or Jt No ......................................' c car ..... Address ........................ Installer " Address Type of Building `'" Size Lot__.O__4-a .....Sq. feet U Dwelling—No. of Bedrooms_____________ '^^-- .............Expansion Attic ( ) Garage Grinder p, Other—Type of Building a�L0:� _..____ No, of persons. __ __.______._ Showers (I ) —Cafeteria Other fixtures t � t�+ r------ �---� -- 4�/C-- - -._... P - 11 a W Design Flow___.. .� 'a_____....._ __gallons per person per day. Total daily flow.................. ___gallons f!®"?.. Gd Se ptic Tank—Liquid capacit gallons Length________________ Width__. . Diameter-__-__ ___ Depth.__................ W Disposal Trench No Width... Total Length.................... Total leaching area_ q. ft. s Seepage Pit No`.... ......... Diameter_____ck_____________ Depth,below inlet._ ...... Total leaching area:................... q.._._s ft. z Other Distribution box Dosing tank aPercolation Test Result+s� Performed by_.......................................... *" ...........:._. Date...................... Test Pit No. 1_.:;_, ".___._minutes per inch Depth of Test Pit _ _____________ Depth to ground water........................ Test Pit No. 2.;::.,._.__._:.minutesper inch •yDepth of'Test Pit ._:___.: Depth to3`ground water :___________________ • x • Description of Soil---------------------• .... - -----._._ ...------ - --- ------ '--------- -------- •• --------------- - , U ------------------------------------------------ -----------------•------ W ............. ---------- ----------------------- ---- ------ ----: U Nature of Repairs or Alterations' Answer when applicable :__________________ _ .................... Agreement The undersigned agrees to install the aforedescribed Individual Sewage,Disposal System in accordance with the provisions of TIT Li 5 of the State Sanitary Code—The undersigned further agrees not to place the system in. operation until a Certificate of Compliance has.bee' issued by thoard of health:' �. Sig ed {. - ....................... ..: ., ' Application Approved BY . . ................. -- -- --•nate............... Application Disapproved for'Me following reasons-----------------------••-------•--•--------•--- --•--. --•-----------................................ ................................ -- ---• . . •. __ . C t�7— Date Permit No......... - Issue _ .Z Y� ..,w Date b THE COMMONWEALTH OF MASSACHUSETTS 130ARD OF EALTH } Ol=:::. ................... Zr .ittr a#r>of TomptiFaitrp A THIS IS TO-CERTIFY, That the Idd viduat Sewage`Disposal System constructed ( ) or Repaired 1 1 °( 1• 3+ by = 4_4 }� }g S. ' ° j Ff "�• V ! r i!J".............................� V-� pInsta e „ w atk --- -- . --------rb.....--•---. -- ------. ---= i has been installed in accordance'with theprovisions of bf�l'ie State Sanitary CT� des "ln the application for Disposal Works Construction Permit �'o _. dated ,1 _____ THE ISSUANCE OF THIS CERTIFICATE:SHA NOT BE CONSTRUE AS A GUARANTEE THAT THE SYSTEM WILL FUNCTION SkISF C7"ORY „ x Z ---- ` Inspector k -. 2, L I DATE__...__.... .. .............................. '___ . � THE COMMQNWEALTOF MASSACHUSETTS ^ A HEALTH; �. . . `3 A Nof��lt� y r $K•, FEE --- C us Permission $hereby granted........ .` - to Const;uc orat No r ndiv Se r DI al S s I � ) � Y f.. str , �.• as shown on the'application for Disposal Works>Constr ction Per 1 '` ed__=. - j -- - - - - ---- -- :Board of Health — tom€ i; DATE_ bum , � ; ' � • T: � .ram t ��^h �t . FORM 1255 HOSES & WARREN. INC.. PUBLISHERS - - -` - .• yy y COMMONWEALTH OF MASSACHUSETTS EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS m + DEPARTMENT OF ENVIRONMENTAL PROTECTION 20 RIVERSIDE DRIVE, LAKEVILLE, MA 02347 508-946-2700 JANE SWIFT RECEIVED BOB DURAND Governor Secretary JUL 11 2001 LAUREN A.LISS TOWN OF BARNSTABLE Commissioner HEALTH DEPT. URGENT LEGAL MATTER:PROMPT ACTION NECESSARY COP_ CERTIFIED MAIL:RETURN RECEIPT REOUESTED July 2,2001 Pentti's Automotive RE: BARNSTABLE(HYANNIS)-BWSC 143 Old Yarmouth Road Pentti's Automotive Hyannis,MA 02601 143 Old Yarmouth Road RTN#4-16335 NOTICE OF RESPONSIBILITY M.G.L. c. 21E,310 CMR 40.0000 ATTENTION: Reijo Alton ; On May 21, 2001 at 8:47 AM the Department of".,Environmental Protection (the "Department") received oral notification of a release and/or threat of release of oil and/or hazardous material at the above referenced property which requires one or more response actions. A leaking 55-gallon drum of solvent was observed in a storage trailer on-the above-referenced property. The drum poses a Threat of Release per 310 CMR 40.0312"Threats of Release Which Require Notification Within Two Hours." The'Massachusetts Oil and Hazardous Material Release Prevention and Response Act, M.G.L. c.21E, and the Massachusetts Contingency Plan (the "iviCP"), 3 i 0 CiviR 40.0000, require the performance of response actions to prevent harm to health, safety, public welfare and the environment which may result from this release and/or threat of release and govern the conduct of such actions. The purpose of this notice is to inform you of your legal responsibilities under State law for assessing and/or remediating the release at this property. For purposes of this Notice of Responsibility, the terms and phrases used herein shall have the meaning ascribed to such terms and phrases by the MCP unless the content clearly indicates otherwise. The Department has reason to believe that the release and/or threat of release which has been reported is or may be a disposal site as defined by the M.C.P. The Department also has reason to believe that you (as used in this letter, "you" refers to Pentti's Automotive) are a Potentially Responsible Party (a "PRP") with liability under M.G.L. c.21E §5, for response action costs. This liability is "strict", meaning that it is not based on fault, but solely on your status as owner, operator, generator, transporter, disposer or other person specified in M.G.L. c.21E §5. This liability is also "joint and several", meaning that you may be liable for all response action costs incurred at a disposal site regardless of the existence of any other liable parties. This information is available in alternate format by calling our ADA Coordinator at(617)574-6872. DEP on the World Wide Web: http:/twww.magnetstate.ma.us/dep i„�M1 Printed on Recycled Paper v 2 The Department encourages parties with liabilities under M.G.L. c.21E to take prompt and appropriate actions in response to releases and threats of release of oil and/or hazardous materials.By taking prompt action, you may significantly lower your assessment and cleanup costs and/or avoid liability for costs incurred by the Department in taking such actions. You may also avoid the imposition of,the amount of or reduce certain permit and/or annual compliance assurance fees payable under 310 CMR 4.00. Please refer to M.G.L. c.21E for a complete description of potential liability. For your convenience, a summary of liability under M.G.L.c.21E is attached to this notice. You should be aware that you may have claims against third parties for damages, including claims for contribution or reimbursement for the costs of cleanup. Such claims do not exist indefinitely but are governed by laws which establish the time allowed for bringing litigation. The Department encourages you to take any action necessary to protect any such claims you may have against third parties. At the time of oral notification to the Department, the following response actions were approved as an Immediate Response Action(IRA): • Removal of Tanks/Drums/Containers. • All Remediation Waste must be properly stored/handled and disposed of within 120 days from the date of generation per 310 CMR 40.0030. ACTIONS REQUIRED Additional submittals are necessary with regard to this notification including,but not limited to,the filing of a written IRA Plan, IRA Completion Statement and/or an RAO statement. The MCP requires that a fee of$750.00 be submitted to the Department when an RAO statement is filed greater than 120 days frhm the date of initial notification. Specific approval is required from the Department for the implementation of all IRAs, and Release Abatement Measures (RAMS) pursuant to 310 CMR 40.0420 and 310 CMR 40.0443, respectively. Assessment activities, the construction of a fence and/or the posting of signs are actions that are exempt from this approval requirement. In addition to oral notification,310 CMR 40.0333 requires that a completed Release Notification Form (BWSC-103, attached) be submitted to the Department within sixty (60) calendar days of May 21, 2001. You must employ or engage a Licensed Site Professional (LSP) to manage, supervise or actually perform the necessary response actions at this site. You may obtain a list of the names and addresses of these licensed professionals from the Board of Registration of Hazardous Waste Site Cleanup Professionals at(617)556-1145. Unless otherwise provided by the Department, potentially responsible parties ("PRP's") have one year from the initial date of notification to the Department of a release or threat of a release,pursuant to 310 CMR 40.0300, or from the date the Department issues a Notice of Responsibility,whichever occurs earlier, to file with the Department one of the following submittals: (1) a completed Tier Classification Submittal; (2) a Response Action Outcome Statement or, if applicable, (3) a Downgradient Property Status. The deadline for either of the first two submittals for this disposal site is May 21,2002. If required by the MCP, a completed Tier I Permit Application must also accompany a Tier Classification Submittal. This site shall not be deemed to have had all the necessary and required response actions taken unless and until all substantial hazards presented by the release and/or threat of release have been eliminated and a level of No Significant Risk exists or has been achieved in compliance with M.G.L. c.21E and the MCP. s `. 3 J1 If you have any questions relative to this Notice, please contact Andrew L. Jones at the letterhead address or at (508) 946-2785. All future communications regarding this release must reference the following Release Tracking Number: 4-16335. Very truly yours, jau- Richard F.Packard,Chief Emergency Response/Release Notification Section P/ALJ/cb CERTIFIED MAIL NO. 7099 3220 0002 0275 7463 RETURN RECEIPT REQUESTED Attachments: Release Notification Form;BWSC-103 and Instructions Summary of Liability under M.G.L.c.21E Department's guide to hiring a Licensed Site Professional. cc: Board of Health PO Box 534 Hyannis,MA 02601 Board of.Selectmen 367 Main Street Hyannis,MA 02601 Fire Dept 95 High School Road Ext. Hyannis,MA 02601 COMMONWEALTH OF MASSACHUSETTS L w F EXECUTIVE OFFICE OF ENVIRONMENTAL FFATRS + d DEPARTMENT OF ENVIRONMENTAL PRO 20 RIVERSIDE DRIVE LAKEVILLE MA 02347 508-946- � c v� ,o1M S�ev RECEIVE® JANE SWIFT BOB DURAND Governor Secretary J U L 0 2 2002 ' LAUREN A.LISS TOWN OF BARNSTABLE Commissioner HEALTH DEPT, June 24, 2002 Reijo Alton RE: HYANNIS--BWSC Penttis Automotive RTN: 4-16335 143 Old Yarmouth Road Penttis Automotive Hyannis, Massachusetts 02601 143 Old Yarmouth Road NON-SE-02-3T-030 NOTICE OF NONCOMPLIANCE THIS IS AN IMPORTANT NOTICE. FAILURE TO TAKE ADEQUATE ACTION IN RESPONSE TO THIS NOTICE COULD RESULT IN SERIOUS LEGAL CONSEQUENCES. Dear Mr. Alton: The Massachusetts Department of Environmental Protection, Bureau of Waste: Site Cleanup (the "Department"), is tasked with ensuring the permanent cleanup of oil and hazardous material releases pursuant to Massachusetts General Law Chapter 21 E ("Chapter 21 E"). The law is implemented through regulations known as the Massachusetts Contingency Plan, 310 CMR 40.0000 et seq. (the "MCP"). Through the MCP, the Department is currently regulating a release of oil that has occurred at 143 Old Yarmouth Road, Hyannis, Massachusetts. The Department was first notified of the release on May 21, 2001. The Department's records indicate that you (as used in this Notice, "you" collectively refers to Penttis Automotive) are a Potentially Responsible Party("PRP") for this release. This Notice is provided to inform you that you are not in compliance with the MCP. The Department has no record of your completing the response actions required by the MCP to address this release. Attachment A of this Notice is. a Noncompliance Summary sheet that outlines the provisions of the MCP that you have not complied with. Contained within the Noncompliance Summary are the necessary action(s) you must complete to return to compliance. Additionally, there is a prescribed deadline for your completion of the action(s). This information is available in alternate format by calling our ADA Coordinator at(617)574-6872. DEP on the World Wide Web: http://www.state.ma.gov/dep Z0 Printed on Recycled Paper ' 4rofl1TT r Page 2 The Department may assess a Civil Administrative Penalty potentially in excess of $7,000 if you continue to be in noncompliance with the violation(s) cited herein. Notwithstanding this Notice of Noncompliance ("NON"), the Department reserves the right to exercise the full extent of its legal authority in order to obtain full compliance with all applicable requirements, including, but not limited to, criminal prosecution, civil action in court-imposed civil penalties, or administrative penalties assessed by the Department. Finally, Attachment 2 of this Notice is a fact sheet containing supplemental information regarding this NON. If you have any questions regarding this matter, or if you would like to discuss compliance with this Notice, please contact John Handrahan, at the letterhead address or by telephone at (508) 946-2883. All future communications regarding this matter must reference Release Tracking Number 4-16335. Very truly yours, on tan E. Hobill,Regional Engineer of Waste Site Cleanup H/JH/rr Attachment 1: Noncompliance Summary Sheet Attachment 2: Supplemental Information Regarding This Notice of Noncompliance CERTIFIED MAIL # 7001 0320 0001 4831 3382 RETURN RECEIPT REQUESTED cc: Board of Selectmen Town Hall 367 Main Street Hyannis, MA 02601 Board of Health P.O. Box 534 Hyannis, MA 02601 DEP-SERO Attn: Regional Enforcement Office (2 Copies) Attn: Data Entry A ATTACHMENT I NOTICE OF NONCOMPLIANCE NONCOMPLIANCE SUMMARY ENTITUPOTENTIALLY RESPONSIBLE PARTY IN NONCOMPLIANCE Penttis Automotive 143 Old Yarmouth Road Hyannis, Massachusetts 02601 LOCATION WHERE NONCOMPLIANCE OCCURRED OR WAS OBSERVED: Penttis Automotive 143 Old Yarmouth Road Hyannis DATE(S)WHEN NONCOMPLIANCE OCCURRED OR WAS OBSERVED: May 21, 2002 DESCRIPTION OF ACTIVITY OR CONDITION RESULTING IN NONCOMPLIANCE: 1. You have not submitted a 'Response Action Outcome (RAO) Statement, Tier Classification Submittal or Downgradient Property Status Submittal to the Department. One of the above referenced documents is required to be submitted to the Department within one (1) year of notification that a release of oil and/or hazardous material has occurred, as is required by 310 CMR 40.0501(3). DESCRIPTION OF REQUIREMENT NOT COMPLIED WITH 1. Pursuant to 310 CMR 40.0501(3), except where a site has filed a Response Action Outcome (RAO) or a Downgradient.Property Status Submittal, all sites for which the Department receives notification of a release or threat of release of oil and/or hazardous material pursuant to 310 CMR 40.0300 on or after October 1, 1993, shall be classified as either a Tier I or Tier II disposal site in accordance with 310 CMR 40.0500. A Tier Classification submittal and, if applicable, a Tier I Permit application, shall be submitted to the Department within one year of the earliest date computed in accordance with 310 CMR 40.0404(3). DESCRIPTION AND DEADLINES OF ACTIONS TO BE TAKEN To avoid imposition of a Civil Administrative Penalty in the amount of$7,000 for violations of the MCP, you must complete the following action(s) within thirty (30) days of your receipt of this NON: y: 1. Submit to the Department either a Response Action Outcome Statement, Downgfadient Property Status Statement, or a Tier Classification with, if necessary, a completed Tier I Initial Permit Application. All items must be prepared in full accordance with the MCP. Notwithstanding this NON, the Department reserves the right to exercise the full extent of its legal authority to obtain full compliance with all applicable requirements, including but not limited to, criminal prosecution, civil action including court-imposed civil penalties, and Civil Administrative Penalties issued by the Department. ATTACHMENT 2: SUPPLEMENTAL INFORMATION REGARDING THIS NOTICE OF NONCOMPLIANCE This attachment further explains why this Notice of Noncompliance (NON) has been issued to you. Why was I issued this NON? The Department's records indicate that you have not submitted one or more of the documents listed in the attached NON. This NON was issued to inform you of this fact and offer you an opportunity to come back into compliance by submitting the missing information to the Department by the deadlines specified in the NON. You are listed in the Department's records as the person who is responsible for cleaning up the release cited in the attached NON. For example, at the time you or another party notified the Department that the release occurred, you either informed the Department that you accepted responsibility for the cleanup or you were sent a "Notice of Responsibility" (NOR) by the Department informing you that we found you responsible for the release. In either case, the Department has reason to believe that you are an owner, operator, generator, transporter, disposer, or person who otherwise caused the release or threat of release of oil and/or hazardous materials cited in the attached NON. . This means that, under Section 5 of M.G.L. Chapter 21E, you are a Potentially Responsible Party (PRP) and liable for response action costs associated with the release. As a PRP, you are required to conduct and complete certain response actions outlined in the MCP to clean up the release of oil and/or hazardous materials expeditiously. What happens if I fail to comply with or respond to the NON? You have thirty (30) days from the date you receive the NON to comply. If you fail to comply, you will be assessed a penalty by the Department. Your total penalty exposure can be considerable. For example, penalties can be assessed for each day you remain in noncompliance. Note that the Department is allowed by law to back calculate daily penalties to begin on the date you received the NON. You can be penalized thousands of dollars should you fail to comply with or respond to the NON by the 30-day deadline. Please refer to the Civil Administrative Penalty Statute, Chapter 21A, Section 16 and 310 CMR 5.00, the Civil Administrative Penalty Regulations, for complete details on the Administrative Penalty rules. When the cleanup contractor finished the work in the field, I thought my dealings with the Department were finished. What more do I have to do? This is a common question asked when a NON is received. PRPs often think their dealings with the Department are over when, for example, the fieldwork is completed by a cleanup contractor. Examples of this type of fieldwork include cleaning up a spill from a saddle tank leak on a roadway, or removing contaminated soil from a tank grave during a tank replacement or oil- contaminated debris from a storage tank after a fire. The fieldwork may be complete, but you still must submit some paperwork to the Department to prove that the cleanup was undertaken in compliance with the MCP. The MCP includes deadlines by which you must complete response actions and submit information about those response actions to the Department. We track the progress of cleanups by checking to see if you are sending information about your cleanup progress to the Department on time. For example, if we do not receive a Response Action Outcome Statement(RAO)before the 1-year anniversary date of the release, we must assume that the environmental cleanup.has not been completed. For work to continue after the 1-year anniversary date of the release, the MCP requires that you submit a Tier I or.Tier II_Classification to the Department. If the Department does not receive either an RAO or Tier Classification by the 1-year anniversary date, we must assume that you are not implementing any cleanup at all. Without your cooperation in obtaining the cleanup information, the Department does not know whether serious environmental problems are being addressed. If work is not being performed, the Department must take action to ensure it happens. On the other hand, you may have finished the cleanup but neglected to forward the cleanup documentation required by the MCP. What do I have to do to comply with the NON? First all response actions not directly managed b the Department staff must be overseen and p Y g Y P . directed by a "Licensed Site Professional" or LSP. LSPs are licensed by the Commonwealth, and their stamp and signature are required (together with yours) on all but one form you must submit to the Department. If you don't already have the forms and information required for you to comply with this NON, contact the consultant and/or cleanup contractor who worked on your cleanup. If you have not undertaken any cleanup work, contact an LSP immediately. A list of LSPs may be obtained by calling (617) 556-1091 or viewing the list on the Internet at http://www.state.ma.us/Isp. The documents you must submit to the Department require LSP stamp and signature. For example, when a cleanup is completely finished, the MCP requires that you submit a document called a"Response Action Outcome" (RAO) to the Department in which you attest that you have completed the cleanup in accordance with the MCP. If you do not submit an RAO to the Department, the case remains open in the Department's files even if the fieldwork is completely finished. If you received this NON and you think the fieldwork is completely finished, call your cleanup contractor and LSP to find out how to have an RAO prepared and submitted to the Department. If more environmental studies or cleanup are needed (for example, following the initial cleanup of a highway spill or soil contamination found.during a tank replacement), you must submit forms describing your plans to continue the work in a timely manner. Again, these forms must contain an LSP's stamp and signature, and be co-signed by you. Depending on the circumstances, the possible submittals are an Immediate Response Action (IRA) Plan, IRA Status Report, IRA Completion Statement, and/or a Tier Classification Submittal and Tier I Permit Application. You should also be aware that the Department does not become involved in or help mediate billing disputes with insurance companies, cleanup contractors, or LSPs. A common response to a NON is that an insurance company is slow on paying cleanup bills or will not cover various p Y pY g p cleanup costs. We also hear that cleanup firms and LSPs will not send in RAOs and other forms because their clients have not paid their bills. These matters must be resolved privately by you. You ultimately must comply with the attached NON or be subject to significant penalties from the Department. FiNSNESS ENVIRONMENTAL October 24, 2002 Barnstable Board of Health 367 Main Street Hyannis, MA 02601 Re: Response Action Outcome Statement Pentti's Aµtomotive 143vQl� i i .= �`"11y nis,Massachusetts RTN 4-16335 Dear Sir or Madam: Finsness Environmental has recently completed an environmental investigation on the referenced property in accordance with applicable regulations of the Massachusetts Contingency Plan(310 CMR 40.0000). In summary, one drum was observed at the subject property, which posed a potential release threat. The issue was identified to the MADEP on May 21, 2001. The drum has been removed and upon inspection, no threat of a release remains in this area of the site. Therefore, based upon the data presented above, it is our opinion that no release has occurred and a Class A-1 RAO is applicable for the Site. This type of RAO indicates that a permanent solution has been achieved and no deed restrictions are required in the specified area of the Site. A copy of the completed report can be reviewed and/or copied at the Massachusetts Department of Environmental Protection's (MADEP) Southeast Regional Office in Lakeville, Massachusetts. This letter was submitted to satisfy public notification requirements of the MADEP. Sincerely, FINSNESS ENVIRONMENTAL 3 � Nat aniel L. Finsness Licensed Site Professional(MA45156) cc: MADEP=Southeast Regional Office 140 Longhill Avenue • Tel.: (508)679-2002 Somerset,Massachusetts • Fax: (508)679-2205 02726 • E-Mail: fmsnessnameganet.net I, 66 ARTICLE XIX. DISTRIBUTION OF COMMERCIAL ADVERTISING Section 1. The distribution of commercial advertising on handbills, cards, signs or in any other form, by placing the same on or in vehicles which are parked on the public ways, in public places, or other areas open to the public, is prohibited. Section 2. Any person violating the provisions of this ordinance shall be punished by a fine not to exceed fifty ($50.00) dollars. Adopted June 25, 1963. Approved July 22, 1963. Amended May 18, 1976. Approved September 13, 1976. .\ tion of Section 2. ARTICL E XX. ' UNREGISTERED MOTOR VEHICLE OR TRAILER REGULATION Ro person shall have more than one (1) unregistered motor vehicle or trailer or any part or portion thereof, ungaraged on premises owned, occupied or controlled by him at anytime. This ordinance shall not apply to any vehicles used for agricultural purposes nor shall it apply to premises duly licensed under the provisions of Chapter 140 of the General Laws. Any person failing to remove such vehicle or vehicles, or any part or portion thereof, within seven (7) days, after notice by the Police Department of the town, shall be subject to a fine of not more than three hundred ($300.00) dollars. Each day during any portion of which violation is permitted to exist, shall constitute a separate offense. Adopted March 8, 1967. Approved April 27, 1967. Amended October 23, 1969. Approved December 17, 1969. Amended: July 17, 2003 by unanimous vote of the Town Council ` Penni's Automotive Rei jd,laltonen Phonc(508)809-0539 143 Old Yarmouth Rd. Hyannis,MA 02601 rei.jo@penttis.com w: Date: 6 /2 3/®y TOWN OF BARNSTABLE TOXIC AND HAZARDOUS MATERIALS ON-SITE INVENTORY NAME OF BUSINESS: &L, ' V_e_ BUSINESS LOCATION: 193 0" -- • � INVENTORY MAILING ADDRESS: `� TOTAL AMOUNT: TELEPHONE NUMBER: wog — go ct — 0 5-,39 • o�S CONTACT PERSON:_ RE150 A141-1-OAl Al EMERGENCY CONTACT TELEPHONE NUMBER: MSDS ON SITE? TYPE OF BUSINESS: V-e ' cam- mA4A'o aA,4,4-e�44t C-e— LAe s INFORMATION/RECOMMENDATIONS: �� �" "rusl� ud!�K _ Fire District: Piwc�o sal Borg-ear �"b Mecx�4'h (�-�(�• Laih�t �e.�4M/�'��F gG�s ea��%ze�t Waste Transportation: Last shipment of a�zardous waste: Name of Hauler: - rtul Destination: " s s Waste Product: 6c6*1• e-s' Licensed? Yes No A NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous materials use, storage and disposal of 111 gallons or more a month requires a license from thePublic Health Division. LIST OF TOXIC AND HAZARDOUS MATERIALS t5+.�-LZ - o y �' r5 The Board of Health and the Public Health Division have determined that the following roducts exhibit qA2 or hazardous characteristics and must be registered regardless of volume. s J�'`"�'K • es Observed/Maximum Observed/Maxim u Znd Antifreeze (for gasoline or coolant systems) Misc. Corrosive NEW USED Cesspool clean rsg 2 3 c y• F -$ Automatic transmission fluid Disinfectants Il-9 Engine and radiator flushes Road Salts (Halite) Hydraulic fluid (including brake fluid) Refrigerants �� � Coo? Oils Pesticides aW Cwi_s. NEW USED (insecticides, herbicides, rodenticides) Gasoline, Jet fuel, Aviation gas Photochemicals (Fixers) Diesel Fuel, kerosene, #2 heating oil NEW USED Misc. petroleum products: grease, Photochemicals (Developer) lubricants, gear oil NEW USED Degreasers for engines and metal Printing ink Degreasers for driveways &garages Wood preservatives (creosote) Caulk/Grout Swimming pool chlorine Battery acid (electrolyte)/Batteries Lye or caustic soda Rustproofers Misc. Combustible Car wash detergents Leather dyes Car waxes and polishes Fertilizers ,Asphalt & roofing tar PCB's Paints, varnishes, stains, dyes Other chlorinated hydrocarbons, Lacquer thinners (inc. carbon tetrachloride) NEW USED Any other products with "poison" labels Paint &varnish removers, deglossers (including chloroform, formaldehyde, Misc. Flammables hydrochloric acid, other acids) Floor &furniture strippers Other products not listed which you feel \ 4`Metal polishes may be toxic or hazardous (please list): Laundry soil & stain removers (including bleach) Spot removers &cleaning fluids (dry cleaners) Other cleaning solvents Bug and tar removers Windshield wash WHITE COPY-HEALTH DEPARTMENT/CANARY COPY-BUSINESS ' z3 z 0-arq 47Y No C)`-� Town of Barnstable-Health Department Page 1 t HAZARDOUS MATERIALS INVENTORY SITE VISITS DBA: Penti's Auto Body Fax: Corp Name: Mailing Address Location: 143 Old Yarmouth Road,Hyannis Street: 143 Old Yarmouth Road mappar: 1 City: Hyannis Contact: Wendy Salmi C;SV A cv INc—w State: Ma Telephone: 775-3271 �� Zip: 02601' Emergency: Person Interviewed: Business Contact Letter Date: Category: VehicleMaintenance Inventory Site Visit Date: Type: ,„ .I,AQ, Follow Up/Inspection Date: public water ❑ indoor floor drains ❑ outdoor surface drains ❑d license required ❑ private water ❑d indoor holding tank mdc ❑ outdoor holding tank mdc ❑ currently licensed ❑ town sewage ❑ indoor catch basin/drywell ❑ outdoor catch basin/drywell expir ❑� on-site sewage ❑ indoor on-site syste ❑ outdoor onsite system date: ......................... ......................... FLOOR DRAIN IS SEALED. NO EMPLOYEES/ALL PARTNERS. compliance: MANIFESTS ON SITE IN FILE CABINET. PAINTS&WASTE THINNER IN Satisfactory PAINT ROOM(NON FLAMMABLE ROOM). NO SPRAY BOOTH. FLOOR DRAINS PLUGGED. MUST HAVE SPRAY BOOTH AND HAVE MSDS SHEETS ON SITE. SHALL START RECYCLING OF OIL FILTERS. ALSO SMALL QUANTITIES OF RUBBING COMPOUND AND REDUCER. t/p �z i DZM - REMARKS: ��� o��[/C 12/30/97 Manifest unit on-site. Paints on metal raeks in storage room. �. Paint gun cleaner uses 5 gal.lacquer thinner. Unifirst takes rags and - uniforms. No lid on rag car. Hydraulec lift 2-20 gal.Dumpster is overflowing. Bring in Manifest. ORDERS: 1.Dispose of or bring inside ' 2-20 gal,1-5 fal,and 1-5 gal drum of unknown material.2.Dispose of unused tires,empty dumpster. 3. Dispose of a bring inside all can parts on ground. 4. Thirty days to fix unknown waste �ats situation. 5/13/02 REMARKS: Speedi Dry Oil abs.pads.RajWs kept in covered metal container.Large jobs (Painting)done at Brito's w/spray booth. Stainless steel removes steel monthly. ORDERS: Label drums&flame rest.Cabinet. Don't mix products in containers. Remove tires stored outside must be removed G after 10 tires. Batterys reycled with Interstate. Needs Manifest& ✓dam/ ¢ MSD 6/22/04 Has not purchased a -- license for last year. Needs to be updated. 0 %C i i a� a,i �� Page 2 Town of Barnstable-Health Department HAZARDOUS MATERIALS INVENTORY Chemicals: ❑ Zero Toxic Waste Materials d❑ gty's>25 Ibs dry or 50 gals liquid but less than 111 gals ❑ gty's 111 gals or more descnptign„_ , N, , gty:, , it of measure,,, motor oil 55 Gallons ..._..._..._.._.--_._................._...........___.___.._.__.__..__....... __....._.___.......__..._.._..._.....__._....._.....__.......___........_____._._.....__._......._......................... __-_.... acquer thinners_ 55Gallons paint,varnishes,stains,dyes -� 20Gallons Waste Transporter: 'Clean Harbors Fire District: Last HW Shipment Date: Waste Hauler Licensed: No bowl__ .10 1 :1 Hazardous Materials On-Site Inventory/Inspection For ALL Shops and Businesses in the Town of Barnstable DBA: Location: ate: e,. -- Z_ z--a 1 CA 3 Physical Features to Inspect: Hazardous waste generation sites (production/manufacturing areas): Waste storage areas: Satellite accumulation points throughout: HazMat stored outdoors — CHECK OUTSIDE: Shipping and receiving areas: Run down of shop activities: Housekeeping practices: C HazMat On-Site Inventory/Inspection: Records to Review for SQGs and CESQGs Location: Site visit date: (n -`L�— D • Hazardous Waste Manifests: • Employee training documentation (if required): • Hazardous substance spill control and contingency plan: • MSDS on site? • HazMat Inventory records (if applicable): • HazMat Waste Shipping documentation: • Spill records (if applicable): Town of Barnstable Regulatory Services �FTHE Tp�� Thomas F. Geiler, Director * Public Health Division anxxsrna�, 9� 1639.MASS. �0� Thomas McKean,Director .elf p''��a 200 Main Street, Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 May 17, 2005 TO: Samantha Westgate Bennet& O'Reilly, Inc. PO Box 1667 Brewster, MA 02631 RE: RESPONSE TO YOUR REQUEST FOR SITE INFORMATION IN IN COMPLIANCE WITH MGL 21E The Health Department files were searched for information regarding the property at 143 Old Yarmouth Road, Hyannis listed as Map 344 - Parcel 078.001 and adjacent properties listed in the application form received from you on May 4, 2005. The following items, if checked, apply to the property or adjacent properties: UNDERGROUND FUEL TANK INFORMATION There are no records on file concerning underground fuel and chemical storage tanks at this property or any of the other adjacent properties. X The attached underground fuel and chemical storage information concerns the tank(s) located at: 344-081 —Removed- see attached report 344-078.001 - Removed—see attached report RELEASE/SPILL INFORMATION No hazardous material releases were reported to the Health Division regarding the subject property or any of the adjacent properties. —X The attached release information concerns the properties located at: 143 Old Yarmouth Road 380 Yarmouth Road Q:/health/wpfiles/1430ldYarmouthRoad-HY SEPTIC SYSTEM/SEWER INFORMATION There is no as-built card record on file regarding the existing onsite sewage disposal system. The property is connected to Town Sewer. The attached onsite sewage disposal system information is enclosed. 143 Old Yarmouth Road—344-078.001 WATER SUPPLY INFORMATION _X The Health Department has no record of a private water supply well location onsite, if there is a well onsite at this property. It is suggested you contact the appropriate Water Department to determine whether the building is connected to Town water. The Health Department records indicate there are private water supply wells at the following location: Please forward me a copy of the 2 1 E report after your completion of the report. My mailing address is: Barnstable Health Division 200 Main Street Hyannis, MA 02601 Sincerely, i Thomas A. McKean Director of Public Health Q:/health/wpfiles/1430ldYarmouthRoad-HY <THE To, The Town of Barnstable Health Department raux►ac J 367 Main Street, Hyannis, MA 02601 �+r0� Office 508-790-6265 Thomas A. McKean FAX 508-775-3344 Director of Public Health 21E# : APPLICATION FOR 21E INFORMATION SEARCH FEE $-34-.00 DATE: NAME OF PERSONy� REQUESTING INFORMATION: ENGINEERING' FIRM:��X,p�� ADDRESS : \S-f 3 rQ si(1 S�[�pk I Po x kULo-7 TELEPHONE # : ADDRESS OF SITE LOCATION: aA, '-Aaf ul\c� S %oOk ' o � ASSESSORS MAP NO. : t` w PARCEL NO. : C>7116COt o rn PRESENT BUSINESS NAME: GROUNDWATER DIRECTION FLOW: - SPECIFIC SITES YOU WISH TO RECEIVE RELEASE INFORMIATION: ASSESSORS--MAP-NO'. : 3Lkck PARCEL NO. : ASSESSORS MAP NO. : 3LAL 3 PARCEL NO. : Cgs ASSESSORS MAP NO. : PARCEL NO. : ASSESSORS MAP. NO. : PARCEL NO. : C-3L\ct oy 5-noz 6 Date: 6 /z 3/o ll TOWN OF BARNSTABLE TOXIC AND HAZARDOUS MATERIALS ON-SITE INVENTORY NAME OF BUSINESS: eat S • BUSINESS LOCATION: 193 01cl �_Agdd2ISTA&h �'o�• , /�ic�,z+us INVENTORY MAILING ADDRESS: '� TOTAL AMOUNT: TELEPHONE NUMBER: SD 9 v 9®Ct - D��9 L c~.;-iS CONTACT PERSON:_REIJ-® 4AJ-1-OAlet/ EMERGENCY CONTACT TELEPHONE NUMBER: MSDS ON SITE? TYPE OF BUSINESS: -- b,cnl . k "all,C-.R— tAes rT c�.cc a sS INFORMATION/RECOMMENDATIONS: �� � �' - &dd Fire District: s U A 3 ct n.ru s + ,le ems®.5" 6oald -6 14 eaRAAh (.�-� �• L�Yr�t (=�fqM/+'!�}�L`S c r�- Waste Transportation: 4Qom- Last shipment of hazardous,waste: Name of Hauler:—V__A1A - ha A Destination: eocc_h"e4 Q �Iavv�s 5•�� Waste Product: baV*,P,u*e_s- Licensed? Yes No MIA NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous materials use, storage and disposal of 111 gallons or more a month requires a license from the Public Health Division. LIST OF TOXIC AND HAZARDOUS MATERIALS The Board of Health and the Public Health Division have determined that the following products exhibit toxic or hazardous characteristics and must be registered regardless of volume. Observed/Maximum Observed/Maximum Antifreeze (for gasoline or coolant systems) _ Misc. Corrosive NEW USED Cesspool cleaners Automatic transmission fluid Disinfectants Engine and radiator flushes Road Salts (Halite) Hydraulic fluid (including brake fluid) Refrigerants Motor Oils Pesticides ✓ NEW USED '(insecticides, herbicides, rodenticides) Gasoline, Jet fuel, Aviation gas Photochemicals (Fixers) Diesel Fuel, kerosene, #2 heating oil NEW USED f Misc. petroleum products: grease, Photochemicals (Developer) lubricants, gear oil NEW USED Degreasers for engines and metal Printing ink Degreasers for driveways &garages Wood preservatives (creosote) Caulk/Grout Swimming pool chlorine Battery acid (electrolyte)/Batteries Lye or caustic soda Rustproofers Misc. Combustible Car wash detergents Leather dyes Car waxes and polishes Fertilizers Asphalt & roofing tar PCB's Paints, varnishes, stains, dyes Other chlorinated hydrocarbons, Lacquer thinners (inc. carbon tetrachloride) NEW USED Any other products with "poison" labels Paint &varnish removers, deglossers (including chloroform, formaldehyde, Misc. Flammables hydrochloric acid, other aids) Floor &furniture strippers Other products not listed which you feel Metal polishes may be toxic or hazardous (please list): Laundry soil & stain removers (including bleach) Spot removers & cleaning fluids (dry cleaners) Other cleaning solvents Bug and tar removers Windshield wash WHITE COPY-HEALTH DEPARTMENT/CANARY COPY-BUSINESS TOWN OF BARNSTABLE COMPLIANCE: CLASS., 1. Marine,Gas Stations, Repair . Printers BOARD OF HEALTH 0 satisfactory 3.Auto Body Shops unsatisfactory- 4.Manufacturers COMPANY «LA (see"Orders") 5.Retail Stores 6.Fuel Suppliers ADDRESS /12;, (� PQ -Class: 7. Miscellaneous QUANTITIES AND STORAGE (IN= indoors;OUT=outdoors) MAJOR MATERIALS Case lots Drums Above Tanks Underg-round Tanks IN OUT IN OUT IN JOUT #&gallons Age ITest Fuels: Gasoline,Jet Fuel (A) Diesel, Kerosene, #2 (B) Heavy Oils: �J waste motor oil (C) new motor oil(C) transmission/hydraulic Synthetic Organics: degreasers C GI Miscellaneous: - n. , CC �S wpo -� 2 2PL rSp-S DISPOSALIRECLAMATION REMARKS: 1. Sanitary Sewage 2.Water Supply � �i UJ b own Sewer '.Public _ coVr�Q On-site OPrivate 7-6:� S OA(� 14 _ .f_ gr� 3. Indoor Floor Drains YES N0�4_ O Holding tank:MDC ' O Catch basin/Dry well O On-site system \ 4. Outdoor Surface drains:YES NO x QRDERS O Holding tank:MDC 44621UL. I O Catch basin/Dry well O On-site system 5.Waste Transporter 1b 71 PAS, Name of Hauler Destination Waste Product Licensed? 1. 2. � ,� �" %her►-�.,-� � � a..� Person (s) Interviewed Inspector Date 508-775-3271 "Ib Pentti's Auto 143 Old Yarmouth Road Hyannis,MA 02601 Auto Body Used Car Towing Sales • • F TOWN OF BARNSTABLE COMPLIANCE: CLASS: 1.Marine,Gas Stations,Repair satisfactory 2.Printers BOARD OF HEALTH O 3.Auto Body Shops �. unsatisfactory- 4. an COMPANY / (see"Orders") 5.Retail Stores 6.Fuel Suppliers ADDRESS O lass: 7.Miscellaneous QUANTITIES AND STORAGE (IN=indoors; OUT_outdoors) MAJOR MATE LALS Case lots Drums Above Tanks Underground IN OUTI IN OUT IN OUT #&gallons Age Test Fuels: Gasoline,Jet Fuel (A) Diesel, Kerosene, #2 (B) H waste motor oil. new motor oil (C) tra missio ydraulic Synthetic Organics: degreasers uv1l%6Z � Miscellaneous: , a I 6 6 Ili � -'� Il�� E RLD 0 c re)11 z— -x DISPOSAL/R.E(:LAMATION REMARKS: r 1. Sanitary Sewage 2. ater Supply Town Sewer ublic S CP On-site Private 3. door Floor Drains YES N0 ` /jam n Iolding tank: MDC ®0 Catch basin/Dry well -" 0 On-site system ��ok, l 4. Outdoor Surface drains:YES NO ORDE S: 0 Holding tank:MDC 6 Se98 WO O Catch basin/Dry well O On-site system ° 5. Waste Transporter Name of Hauler Destination Waste Product Licensed? • A1 S NO 2. Gn/I Pers n (s) Interviewed Ins ect 7 Date -- a TOXIC AND HAZARDOUS MATERIALS REGISTRATION FORM NAME OF BUSINESS: R is Mail To: BUSINESS LOCATION: l g3Ct8. WjCMn LAh-d rin� 5 Board of Health MAILING ADDRESS: Town of Barnstable P.O. Box 534 TELEPHONE NUMBER: _!50&-77f� �7 I Hyannis, MA 02601 CONTACT PERSON: l EMERGENCY CONTACT TELEPHONE NUMBER: 6,.6_0_a7271 - 770q Does your firm store any of the toxic or hazardous materials listed below, either for sale or for your own use, in quantities totalling, at any time, more than 50 gallons liquid volume or 25 pounds dry weight? YES >— NO This form must be returned to the Board of Health regardless of a yes or no answer. Use the enclosed envelope for your convenience. If you answered YES above, please indicate if the materials are stored at a site other than your mailing address: ADDRESS: TELEPHONE: LIST OF TOXIC AND HAZARDOUS MATERIALS The Board of Health has determined that the following products exhibit toxic or hazardous character- istics and must be registered regardless of volume. Please estimate the quantity beside the product that you store: Quantity/Case Quantity/Case Antifreeze (for gasoline or coolant systems) Drain cleaners ctcA Automatic transmission fluid Toilet cleaners Engine and radiator flushes Cesspool cleaners Hydraulic fluid (including brake fluid) Disinfectants :{ Motor oils/waste oils Road Salt (Halite) 0 Gasoline, Jet fuel Refrigerants Diesel fuel, kerosene, #2 heating oil Pesticides (insecticides, herbicides, Other petroleum products: grease, lubricants rodenticides) Degreasers for engines and metal Photochemicals (fixers and developers) Degreasers for driveways & garages Printing ink Battery acid (electrolyte) Wood preservatives (creosote) Rustproofers Swimming pool chlorine Car wash detergents Lye or caustic soda Car waxes and polishes Jewelry cleaners Asphalt & roofing tar Leather dyes Paints, varnishes, stains, dyes Fertilizers (if stored outdoors) Paint & lacquer thinners PCB's Paint & varnish removers, deglossers Other chlorinated hydrocarbons, Paint brush cleaners (inc. carbon tetrachloride) Floor & furniture strippers Any other products with "Poison" labels Metal polishes (including chloroform, formaldehyde, Laundry soil & stain removers hydrochloric acid, other acids) (including bleach) Other products not listed which you feel may Spot removers & cleaning fluids be toxic or hazardous (please list): (dry cleaners) Other cleaning solvents Bug and tar removers Household cleansers, oven cleaners i White Copy-Health Department/ Canary Copy-Business �'s 508-775-3271 Pentti's Auto 143 Old Yarmouth Road Hyannis, MA 02601 Auto Body Used Car Towing Sales TOWN OF BARNSTABLE COMPLIANCE: CLASS: 1.Marine,Gas Stations,Repair 0 satisfactory 2.Printers BOARD OF HEALTH 3.Auto Body Shops unsatisfactory- 4.Manufacturers COMPANY f4tV,+r 1 (see"Orders") 5.Retail Stores 6.Fuel Suppliers ADDRESS /q) ® 1d )���` 6 Class: 7.Miscellaneous QUANTITIES AND STORAGE (IN=indoors;OUT=outdoors) MAJOR MATERIALS Case lots Drums Above Tanks Underg-round IN OUT IN OUT IN OUT #&gallons Age Test Fuels: Gasoline,Jet Fuel(A) Diesel, Kerosene, #2(B) Heavy Oils: i-Sr X waste motor oil (C) jai , new motor oil(C) transmission/hydraulic Synthetic Organics: degreasers Miscellaneous: V 1 dal fie.,tz i✓v1,ll::n,ua�H . �{ •�( (/ �r l�s i i � G 1. DISPOSAIJRECLAMATION REMARKS: 1. Sanitary Sewage 2.Water Supply '60 A-7 S b1't • 11 M-S i�4 0 Town Sewer OPublic a,ivy,43 vq�Y 3!kOn-site OPrivate a 3. Indoor Floor Drains YES NO 0 Holding tank: MDC �' '� ��"_ 0 Catch basin/Dry well .1�,, V t� GCA.... . �Y�'�+"�rG r ®c 1 0 On-site system 4.a I J �t���ra/6!� � ,�r4` l,iin �� 4. Outdoor Surface drains:YES NO ORDERS: 0 Holding tank:MDC ( ir'ALL# il or'b, -,:,I;Y Z-Z4, ci I /-zs q 0,ef /-S =:i 0 Catch basin/Dry well O On-site system U Uw�to. it...c�•�evl e V�3 t�v vim. r-reS 5.Waste Transporter OVi OVI ✓dVttid� J � ) ft 7� VUL'�z°d.G'Li.a Glib Name of Hauler Destination Waste Product Licensed?, YES No .._� 1. mot,,,er►-�� U cam.d - k1, 2. Z�3©_ Person (s) Interviewed Insp ctor Date TOWN OF BARNSTABLE COMPLIANCE: CLASS: 1.Marine,Gas Station Repair BOARD OF HEALTH satisfactory 2•Punters g.-3.Auto Body Shops unsatisfactory- 4.Manufacturers 9 COMPANYd�' 0� 5.Retail Stores - (see"Orders") y� ,g 6.Fuel Suppliers ADDRESS 7.Miscellaneous it ,& AUANTITIES AND STORAGE (IN=indoors;OUT=outdoors) MAJOR MATER SDrums Underground Tanks IN OUT IN OUT IN OUT #&gallons I e I Test Fuels: Gasoline,Jet Fuel(A) Diesel, Kerosene, #2 (B) Heavy Oils: waste motor oil(C) new motor oil (C) Synthetic Organics: degreasers ._rj � Miscellaneous: DISPOSAL/RECI AMATION REMARKS: 1. Sanitary Sewage 2.Water Supply 4yi4,14 Town Sewer AVPublic �;. 'On-site O Private 3. Indoor Floor Drains YES N0 ^ A O Holding tank:MDC � z .e O Catch basin/Dry well O On-site system 4. Outdoor Surface drains:YES NO OMERS O Holding tank:MDC O Catch basin/Dry well O On-site system 5.Waste Transporter Name of Hauler Destination Waste Product 2. AvX_ Person (s) Interviewed Inspector Date �A. Peritti's Automotive 143 Old Yarmouth Rd. j r Hyannis, MA 02601 Reijo -- Phone:508-775-3271 i Fax:508-77 8-0994 i Www.penttis.com F - TOWN OF BARNSTABLE COMPLIANCE: CLASS: 1.Marine,Gas Stations,Repair 1 BOARD OF HEALTH O satisfactory 2.3.Printers 3.Auto Body Shops unsatisfactory- 4.Manufacturers COMPANY (see"Orders") 5.Retail Stores 6.Fuel Suppliers ADDRESS � g� j 7.Miscellaneous QUANTITIES AND STORAGE (IN=indoors;OUT=outdoors) MAJOR MATESUnderground ank t IN OUT IN OUT IN OUT #&gallons Age Test Igo V :7 woo _ e Heavy Oils: ,r waste motor oil (C) � new motor oil(C) /04 .transmission/h draulic Y ` Synthetic Organics: degreasers Mi ell eo sue: O�`�/` '`z_� � P DISPOSALIRECI AMATION REMARKS' 1. Sanitary Sewage 2. ater Supply <1 zrj,-�4, xt�"4" O Town Sewer fPublic �n-site OPrivate 3. Indoor Floor Drains YES N0_V_ O Holding tank:MDC O Catch basin/Dry well O On-site system 4. Outdoor Surface drains:YES NO ORDERS: O Holding tank:MDC I "7 O Catch basin/Dry well - O On-site system 5. Waste Transporter ' Z Name of Hauler Destination Waste Product 4 2 Person(s) Interviewed Inspector Date �'glva A��o�;; � p. t � - CO d . r I I NUMBER 40 THE COMMONWEALTH OF MASSACHUSETTS FEE $62.00 TOWN OF BARNSTABLE AGENT'S OR SELLER'S LICENSE - CLASS II TO BUY AND SELL SECOND-HAND MOTOR VEHICLES In accordance with the provisions.of Chapter.i40 of the General Laws with amendments thereto --------------------------------- ------------- -` Re jo Altonen DBA PE1V7T1'S AUTO,& TOWING-- ---- -- - -- -- ---- -------------- is hereby licensed to buy and sell second-hand motor vehicles ---------------------------- ----------------------- 143 Old Yarmouth Road.. Hyannis . ------ ---------- ------------ on premises described as follows: ------ ------------------------ ------------ 40 X 60 garage area. 12 X 12 office& 150 X 100 front parking area. RESTRICTIONS: ------------------------------MAXIMUM OF25_V,EIIGF,S.TO_BE,plP4Y1D,--- ----------------------------------------- -------------------------------------------------------------------- December 31, 1999 Signed .............C:.: . ................... ................................................................... .THIS LICENSE EXPIRES JANUARY 1, 2001 THIS LICENSE MUST BE POSTED IN A CONSPICUOUS PLACE UPON THE PREMISES. • LOCATION, 1SE AGE PERMIT NO. Qom' ecp VI'LLAGE INSTA LLER'SG NAME i ADDRESS zv-4 6- BUILDER OR OWNER DATE PERMIT ISSUED Q ` DATE COMPLIANCE ISSUED r— --, i �_ .� �� � � � � ''a s ��, �1 ' � v o , r� �" i�j �� � �� __.1 LIMITED REMOVAL ACTION COMPLETION SUPPORTING DOCUMENTATION Formerly Penti's Automotive 143 Old Yarmouth Road Hyannis, MA B005-4316 SEPTEMBER 149 2005 JuENNETT AO'REIL]L�, Inc. Engineering, Environmental & Surveying Services 1573 Main Street Sanitary 21E/Site Remediation Property Line PO Box 1667Brewster,MA 02631 Site Development Hydrogeologic Survey Subdivision Waste Water Treatment Water Quality Monitoring Land Court �e 508-896-6630 Water Supply Licensed Site Professional Trial Court Witness 508-896-4687 Fax BENNETT A 0'KEILL Inc. Engineering, Environmental & Surveying Services 1 1573 Main Street Sanitary 21E/Site Remediation Property Line r_ PO Box 1667 Site Development Hydrogeologic Survey Subdivision Brewster,MA 02631 Waste Water Treatment Water Quality Monitoring Land Court 508-896-6630 Water Supply Licensed Site Professional Trial Court Witness 508-896-468 7 Fax B005-4316 September 14, 2005 Mr. James Walker 726 Falmouth Road Hyannis,MA 02601 RE: LIMITED REMOVAL ACTION COMPLETION STATEMENT Formerly Penti's Automotive 143 Old Yarmouth Road,Hyannis,MA Dear Mr. Walker, BENNETT& O'REILLY,INC. has prepared the following narrative and attached Supporting Documentation as the Limited Removal Action Completion Statement(LRAC)for remedial response activities conducted at the above referenced property in accordance with 310 CMR 40.0318. .The Limited Removal Action(LRA)was conducted to mitigate potential human exposure and environmental hazards related to a historic release of hydraulic fluid from a subsurface reservoir which serviced the nearby lift system located within the on-site commercial building. Such release was discovered through physical testing conducted as part of an ASTM Phase II Environmental Site Assessment for 'the impending sale of the subject property. At that time,impacted soils were encountered in a hand boring (HB-12)conducted in near proximity to the reservoir and subsequent laboratory analytical substantiated a 120-day Reportable Condition. On July 6,2005,BENNETT& O'REILLY,INC. inspected soil removal operations conducted within the subject building in.the area of the former subsurface lift. Field screening of soil samples collected at each of the sidewalls(SW)and at the bottom of hole(BOH)as well as visual observations indicated the need to extend the area of excavation to the south to include the area of impact encountered at HB-12. On July 8, 2005) BEN ET T & O'REILLY I`NC,. returned to the Site to provide technical assistance to the excavation contractor and document Limited Removal Action operations in extending the excavation to the south beneath the adjacent partition wall resulting in a 10'x 12'x 8-9'(D)area of soil removal. Laboratory analysis of confirmatory soil samples collected at the extent of excavation along the sidewall and bottom of hole areas reported total petroleum hydrocarbons(TPH)and fractional extractable petroleum hydrocarbons(EPH)below the applicable and most stringent RCS-1 Reportable Concentration standards, as well as the most stringent S-1/GW-1 Method 1 - Risk Characterization standards, as representing a condition of"No Significant Risk"without any further Notification and/or Remedial Response liability,in accordance with the provisions of the Massachusetts Contingency Plan (MCP)pursuant to 310 CMR 40.0318.A total of some 33.35 tons of contaminated soil were generated as a result of the LRA and on September 6,2005 were transported under an approved Bill of Lading to Aggregate Industries in South Dennis,MA,as a licensed asphalt batching facility.As such,this report documents regulatory compliance and establishes the technical rationale and justification for project closure as a Limited Removal Action specific to the provisions of 310 CMR 40.0318. 1 SEPTEMBER 14,2005 WALKERB005-4316 PAGE 2 OF 6 LIMITED REMOVAL ACTION COMPLETION The work conducted by BENNETT & O'REILLY, INC., represented herein, has proceeded under my supervision in a manner consistent with the MCP Response Action Performance Standards, pursuant to 310 CMR 40.0191 and the QA/QC policies of BENNETT& O'REILLY, INC. The facts and statements herein are, to the best of our knowledge, a true and accurate representation of the site activities,remedial response actions,and environmental conditions associated with the proj ect. As such, this document serves as the technical justification and rationale for the Limited Removal Action Completion. ENVIRONMENTAL CONDITIONS [Refer to Appendix A] The property at 143 Old Yarmouth Road(herein referred to as the"subject property")is located along the east side of Old Yarmouth Road,less than one-half mile north of the intersection of Yarmouth Road and Route 28 in the Barnstable village of Hyannis,MA. The property is identified on Barnstable Assessor's Map 344 as Parcel 78-01 and contains a total of some 0.23 acres of commercially developed land. The parcel contains a 1,600SF single-story steel warehouse-style building constructed on a concrete slab as an automotive repair shop in 1978. The building contains a front office area,bathroom services,and a rear storage room across the south of the building and a large garage area across the north of the building. The building was reportedly used most recently for auto body repair and painting. A paved parking area is provided along Old Yarmouth Road and a paved driveway provides access to the rear of the building from Bodick Road. The remainder of the property is vacant of development. The immediately surrounding area is characterized as highly developed with various egregious-use industrial and commercial properties to the north, south and east, including automotive repair, manufacturing, production and distribution outfits. Commercial and residential properties are located to the west of the subject property. In review of regional groundwater contours, groundwater flow was interpreted to be in a southeasterly direction toward Mill Creek. Site-specific groundwater contours,however, illustrated a south-southwesterly groundwater flow direction toward the Barnstable Water Department pumping station located approximately one-quarter mile from the subj ect property. Groundwater was encountered at approximately 8-9'below grade surface(bgs)across the property.According to the MA DEP BWSC GIS mapping, the subject property is located within the Zone II of several public water supply wells located approxllr ate ly one-q'a art er male so',.th and 1s-cons.der ed a CulTent Drinking�xlater Solace Area (CDWSA). The property is not within the Zone A of any surface water supply. The subject property is within the designated Sole Source Aquifer located to the east of the Cape Cod Canal. As such,the RCGW-1 Reportable Concentrations are applicable for groundwater quality,as are the GW-1,GW-2 and GW-3 groundwater criteria under Method 1 - Risk Characterization in consideration of routes for potential exposures relative to ingestion, inhalation and significant environmental impact and direct contact. Based on the CDWSA designation and the proximity of residential properties, the RCS-1 Reportable Concentrations are applicable for soils. Site conditions relative to frequency/intensity of use and accessibility of soils indicate that the S-1,S-2 and S-3 (GW-1,GW-2 and GW-3)soil categories are applicable in consideration of Method 1 - Risk Characterization. This criterion is used to determine notification and/or remedial response liabilities pursuant to 310 CMR 40.0000. BACKGROUND [Refer to Appendix B] A single hydraulic lift and associated reservoir were identified within the subject garage bay upon site inspection being conducted in accordance with ASTM 1527 standards on behalf of the property SEPTEMBER 14,2005 WALKERBO05-4316 PAGE 3 OF 6 LMTED REMOVAL ACTION COMPLETION owner for the impending sale of the property. According to the property owner, the lift "stopped working" at some point. The subsurface storage of hydraulic oil associated with the lift in conjunction with the loss of oil pressure was noted as a Recognized Environmental Condition for which the physical testing of soils was conducted. On May 13,2005,hand borings HB-11 and HB-12 were conducted as angled borings within the subject building in locations adjacent to the hydraulic lift and its reservoir, respectively. In each location,two foot composite soil samples were collected from grade to 6' below grade surface (bgs). Each soil sample was placed in a sealed 250-milliliter jar with an aluminum septum. The jars were then agitated to develop organic vapors and field screened with a photoionization detector (PID) by "jar headspace" method for total organic volatiles (TOV), as consistent with the MA DEP "Interim Soils Policy..." WSC 94-400. Each TOV concentration was reported as 0.2ppm. Based on visual and olfactory observations of apparent OHM impact in the HB-12:4-6'soil sample,however,PetroFlag'TPH analyses were conducted on each of the HB-11:4-6' and HB-12:4-6' soil samples. The HB-11:4-6' sample reported a TPH concentration of 35mg/Kg, significantly less than the applicable RCS-1 Reportable Concentration of 200mg/Kg. The HB-12:4-6' sample, however, reported a TPH concentration which exceeded 2,000mg/Kg. As such, the HB-12:4-6' soil sample was forwarded to Groundwater Analytical of Buzzards Bay, MA for confirmatory TPH analyses and "fingerprint" identification. Laboratory analytical received May 31, 2005, reported a TPH concentration of 5,400mg/Kg identified as within the range for lubricating or hydraulic oil for the BB-12:4-6'soil sample,as exceeding the applicable RCS-1 Reportable Concentration of 200mg/Kg. In the Phase II ESA report dated May 31, 2005, BENNETT & O'REILLY, INC. advised the property owner of the findings of the physical testing stating that the noted impact represented a 120-day Reportable Condition with Release Notification and Remedial Response liability for the subject property, in accordance with 310 CMR 40.0000. A written proposal was subsequently provided to the property owner wherein BENNETT & O'REILLY, INC. would provide technical oversight for the remedial response actions required at the subject Site. LIMITED REMOVAL ACTION COMPLETION [Refer to Appendices C and D] On June 22, 2005, BENNETT& O'REILLY, INC. received a message from the prospective. buyer, Mr. Karl Anderson, stating that CEJ Excavating had removed the subsurface lift and appurtenances,as well as surrounding soils,and they had been stockpiled on the concrete flooring within the subject building. On July 6,2005,BENNETT&O'REILLY,INC.responded to the Site to inspect the environmental conditions within the area of excavation. Upon arrival, an area of excavation approximately Tx 8.5'x 8.5'(D)was observed. It was noted at that time that the area of BB-12 was still intact and had not been included in the preliminary soil removal operations. As such, sidewall soil samples were collected from the north (SW-N), east (SW-E), west (SW-W) sidewalls and from the bottom of hole (BOH-N). Field screening of these endpoint samples reported low-level TOV concentrations<_6.2ppm. In order to further qualify hydraulic oil impact,PetroFLAG TPH analyses were conducted on"worst case"soil sample SW-N:3-8'as well as BOH-N:8.5-9.0'. Such screening reported TPH concentrations of 173 mg/Kg and 35 mg/Kg,respectively. As such, SW-E:3-8', SW-W:3-8'and BOH:8.5-9'were preserved for confirmatory TPH analysis,while"worst case"SW-N:3-8'was preserved for EPH with all PAHs, in accordance with the Implementation of the MADEP VPH/EPH Approach [Policy#WSC-02-411]. A contaminated stockpile soil sample was also collected at this time for MA Disposal Characterization. SEPTEMBER 14,2005 WALKER/13005-4316 PAGE 4 OF 6 LIMITED REMOVAL ACTION CONIPLET10N On July 8,2005,BENNETT&O'REILLY,INC.personnel returned to the subject property to provide technical support to CEJ Excavating in the removal of additional soils along the south sidewall of the excavation where HB-12 was conducted. Such excavation continued until field screening, indicated closure objectives could be met. At such time, endpoint samples were collected from along the.south sidewall(SW-S(3):3-8.5)as well as from within the bottom of hole in the south section of the excavation(BOH-S(3):8.5-9'). It is noted that upon completion of soil removal operations,the area of excavation covered an area 10' (W)x 12' (L), including some T which extended beneath the adjacent partition wall. The area of excavation was subsequently secured with caution tape pending confirmatory laboratory analytical. Laboratory analytical received on July 27,2005 and July 28,2005 reported each of the sidewall and bottom of hole exposure points from the extent of the excavation as below reportable limits(BRL) for TPH and fractional EPH and PAH concentrations,wherein the reporting limits are substantially less than the applicable RCS-1 Reportable Concentrations as well as the most stringent S-1/GW-1 Method 1 -Risk Characterization standards. It was further noted that MA Disposal Characterization conducted on a contaminated stockpile sample reported all PCBs and metals below the reported limits(BRL)of the analyses where the reporting limits are less than the most stringent RCS-1 Reportable Concentrations and the S-1/GW-1 Method 1 - Risk Characterization standards. As such, it was determined that the significant impact had been removed from the Site with background conditions met and the potential human and environmental exposures successfully mitigated. A summary of the laboratory analysis for the confirmatory soil samples is presented in Table I and Table II. TABLE SUMMARY OF TPH LABORATORY ANALYSIS METHOD 1-RISK CHARACTERIZATION:SOIL LOCATION TPH RESULTS RCS, S-1 SOIL S-2 SOIL S-3 SOIL [mg/Kg=ppm] x STTANDARD STANDARD STANDARD STANDARD [µkg—PPmI [[tg/g—PPmI [µkg-PPm] 310 CMR 310 CMR 310 CMR �r 40.975(6)(a) 40.975(6)(b) 40.975(6(c) r GW-1/GW-2/GW-3 GW-1/GW-2/GW-3 GW-1/GW-2,'GW-3 SW-S(3):3-8' BRL(<60) ag 20Q�w' e 200/800/800 200/2,000/2,000 200/5,000/5,000 SW-W:3-8' BRL(<62) 200/800/800 200/2,000/2,000 200/5,000/5,000 SW-E:3-8 BRL(<62) 0 200/800/800 200/2,000/2,000 200/5,000/5,000 BOH-N: BRI (<62) � ?00 m 200/800/800 200/2,000/2,000 200/5,000/5,000 (8.5-9.0) a 4 BOH-S(3) �� (8.5-9.0') BRL(<61) 2Q0 200/800/800 200/2,000/2,000 200/5,000/5„000 ,. .. TPH=Total Petroleum Hydrocarbon BRL=Below Reportable Limit Shaded area designates appropriate soil category SEPTEMBER 14,2005 WALKERB005-4316 PAGE 5 OF 6 LIMITED REMOVAL ACTION COMPLETION TABLE II SUMMARY OF EPH LABORATORY ANALYSIS METHOD 1-RISK CHARACTERIZATION:SOIL LOCATION EPH w/PAH sRCS�1 S-1 SOIL S-2 SOIL S-3 SOIL [mg/Kg=ppm] 5� x �.�STANDARD STANDARD STANDARD STANDARD 1(µg/g ppml 111g/g=ppml 111g/g=ppm) Iµg/g=ppml s 310 CMR 310 CMR 310 CMR 40.975(6)(a) 40.975(6)(b) 40.975(6)(c) GW-1/GW-2/GW-3 GW-1/GW-2/GW-3 GW-1/GW-2/GW-3 SW-N:3-8 C9 to C18 BRL(<33) �p00 1,000/1,000/1,000 2,500/2,500/2,500 5,00015,00015,000 C19 to C36 BRL(<33) 2 SO,Q �?- -2,500/2,500/2,500 5,00015,00015,000 5,000/5,000/5,000 C11 to C22 BRL(<33) 200 � 200/800/800 200/2,000/2,000 200/5,000/5,000 All PAHs BRL(<0.56) r A110 7 All>0.7 All>0.7 All>0.7 EPH=Extractable Petroleum Hydrocarbon BRL=Below Reportable Limit Shaded area designates appropriate soil category RISK CHARACTERIZATION [Refer to Appendix D] Soil As previously represented,the RCS-1 Reportable Concentration soil category was considered in review of LRA performance standards,in accordance with the provisions of 310 CMR 40.0318.These criteria are the same as the. S-1/GW-1 Method 1 - Risk Characterization thresholds. Laboratory analytical reported TPH and fractional EPH and target PAH concentrations in each discrete sidewall (SW)and bottom of hole(BOH)areas as BRL and therefore substantially below the RCS-1 Reportable Concentrations as well as the most stringent S-1/GW-1 Method-1 Risk Characterization Standards for consideration of all human exposures related to potential ingestion, inhalation and dermal contact. As such, a condition of"No Significant Risk" has been achieved for all foreseeable activities and uses in support of project closure. Groundwater Giouiidvdattci tiT'ipa%t was considered as part off-this prvjcCt. i ue Bvn saiiipiw%Gnoctvu eL o.J- 9.0'bgs were reported as below the reportable limit(BRL)of the TPH analyses conducted. Again,these limits are substantially less than the applicable RCS-1 Reportable Concentrations and the strictest Method 1 -Risk Characterization standards as a measure ofpotential leaching to groundwater. All other TPH and fractional EPH and target PAH's concentrations were also reported as BRL as representing background conditions. In addition,it is noted that on-site monitoring wells were sampled as part of the original Phase II ESA[5/31/05]wherein concentrations were reported as less than the reporting limits of the VOCs and TPH or EPH analyses conducted. As such,no potential for groundwater impact was considered and no groundwater analysis was conducted nor deemed necessary in support of the Limited Removal Action Completion without any activity or use limitations for the protection of public health safety and the environment. CONCLUSIONS The Limited Removal Action completed at 143 Old Yarmouth Road included the excavation and recycling via asphalt batching of some 33.35 tons of contaminated soil as removed from a 10'x 123 x 8.5- SEPTEMBER 14,2005 WALKER/130054316 PAGE 6 OF 6 - LIMITED REMOVAL ACTION COMPLETION 9.0' area of soil removal within the subject building in the area of the former subsurface hydraulic lift. Laboratory analysis was used to qualify the removal of such contamination and the effectiveness of remedial response activities in the area of the release. This information was applied to RCS-1 Reportable Concentrations and the most stringent S-1/GW-1 Method 1 -Risk Characterization wherein background conditions have been met and a condition of"No Significant Risk" has been established. As such, background conditions have been achieved and a Limited Removal Action Completion Statement is applicable for the closure of the area of excavation, as noted on the Site Plan, with no restriction to activities or use of the site,as technical justification to support project closure within the 120-Day notification period. The findings of this investigation, as represented herein, set forth the rationale and technical justifications for project closure,as established by the Limited Removal Action Completion Statement. The LRA report is based upon the available data and regulations in effect at the time of this reporting. Should you have any questions or need additional information, please contact our office at your convenience. Respectfully yours, BE ILLY,INC. Da ' �hjnrett, P Kara M.Risk,ES Director of ental Services Senior Project Manager cc: Mr. John Klimm-Barnstable Town Administrator Mr. Thomas McKean-Barnstable Board of Health Lt. Chase -Hyannis Fire Department LIMITED REMOVAL ACTION COMPLETION SUPPORTING DOCUMENTATION Former Penti's Automotive 143 Old Yarmouth Road Hyannis, MA B005-4316 SEPTEMBER 14, 2005 Prepared BL. BENNETT& O'REILLY, INC. 1573 Main Street-P.O. Box 1667 Brewster, MA 02631 David C. Bennett, LSP. Prepared For: Mr. James Walker 726 Falmouth Road Hyannis, MA APPENDIX A: Reference Plans - Figure 1: Site Locus Plan [USGS Topographic Quad., Hyannis, MA. 1998] (excerpt) - Figure 2: Ground-Water Resources of Cape Cod, MA [LeBlanc et al, 1986] (excerpt) -Figure 3: MA DEP BWSC Site Scoring Map [2005] -Site Plan entitled,"Limited Removal Action..."prepared by BENNETT&OREILLY,INC., dated July 22, 2005. APPENDIX B: Field Reports - Field Response Log APPENDIX C: Environmental Records -BWSC-012A,B, C: Bill of Lading [Aggregate Industries] APPENDIX D: Laboratory Analysis -Remedial Response - Soil (7/20/05, 7/25/05, 7/26/05) [Groundwater Analytical, Inc.] APPENDIX E: Quality Assurance/Quality Control Plan APPENDIX A .143 Old Yarmouth Road-- Hyannis,MA 104031",70017-09 - 41040'31",7001515 40 ' ��,��G t � �` .`• �r,541� °" � ,k rya c�.�` �.Y s:� ' na,*€'. t # ll f '. • ti�r r �.. �" ' � ��. *sus ?� '�,,. F, z a� Ze x, „ems Q 41 , r ♦d 45 LOCUS - at t; ' r, " rare . ���� r +�� Yell �'' '� �,� • �,+, ,� ��* � i .y •� • r i .. o- ,-VOW 1- J ��, i� t y � it a r� •'F �!- ' 2*,x � a4 '� �.r ��� �r:a '� a '� �`1� } �, i_ ,.* - • AN 1039'18",7001709"NAD83 41039'18" 70015'15" MN TN t i2 t MILE 160 1000 0 1000 2000 3000 4000 FEET Printed from TOPO!©1998 Wildflower Pmductions www.to o.com FIGURE 1: The subject property at 143 Old Yarmouth Road in Hyannis,MA is located along the east side of Old Yarmouth Road,less than one-half mile north of the intersection of Yarmouth Road and Route 28 in the Barnstable village of Hyannis,MA. Of -� yew+°+a•:._ai._ �$,a.'�' Y �. � $' "\ # �F ���+ '-�« �. we 24 a LOCUS # 18 , ,�,� d`a. " z =. '^,. �` �,. �, �' ag,. ?i6. "' sue,.. �Y �• a - VV ,,.,4� � * '*'�.. �^�{ s • �, � +tom� �i `�+'.�* y a « n FIGURE 2: In review of regional groundwater contours,groundwater flow was interpreted to be in a southeasterly direction toward Mill Creek. Site-specific groundwater contours, however, illustrated a southerly groundwater flow direction toward the Barnstable pumping station located approximately one-quarter mile from the subject property. 943 Old Yarmouth Road .Hyannis, MA SIN,, NN w t ) � � `. LOCUS N'''"", ` ,"., s MRO �-� flag eamAad+x7lh ArdMig-P FIGURE 3: According to the MA DEP BWSC GIS mapping,the subject property is located within the Zone II several public water supply wells located approximately one-quarter mile south and is considered a Current Drinking Water Source Area(CDWSA). APPENDIX B PAGE 1 OF 5 WALKER-BO05-4316 FIELD RESPONSE LOG Walker B005-4316 Responsible Party: Mr. James Walker 143 Old Yarmouth Road Hyannis, MA 02601 Property Location: 143 Old Yarmouth Road Hyannis, MA 02601 Background Conditions: • The subj ect property is located along the east side of Old Yarmouth Road,less than one-half mile north of the intersection of Yarmouth Road and Route 28 in the Barnstable village of Hyannis, MA. • The property is identified on Barnstable Assessor's Map 344 as Parcel 78-01 and contains a total of some 0.23 acres of commercially developed land. The parcel contains a 1,600SF single-story steel warehouse-style building constructed on a concrete slab in 1978. The property was former used as an automotive repair shop in 1978. The building was reportedly used most recently for auto body repair and painting. The remainder of the property is vacant of development. I Environmental Conditions: • According to the MA DEP BWSC GIS mapping,the subject property is located within the Zone II several public water supply wells located approximately one-quarter mile south and is considered a Current Drinking Water Source Area(CDWSA). • The subject property is within the designated Sole Source Aquifer located to the east of the Cape Cod Canal. As such, the RCGW-1 Reportable Concentrations are applicable for groundwater quality,as are the GW-1,GW-2 and GW-3 groundwater criteria under Method 1 - Risk Characterization . The RCS-1 Reportable Concentrations are applicable for soils. ISite conditions relative to frequency/intensity of use and accessibility of soils indicate that i the S-1,S-2 and S-3(GW-1,GW-2 and GW-3)soil categories are applicable in consideration of Method 1 - Risk Characterization. PAGE 2 OF 5 WALKER-BO05-4316 • Groundwater was encountered at approximately 8-9' below grade surface (bgs) across the property. Remedial Response: Date Time 5/13/05 BENNETT&O'REILLY,INC.arrive on-site to conduct environmental assessment activities in association with Suspect Conditions identified in the Phase II Environmental Site Assessment. Conduct hand boring HB-12 as an angled boring within the subject building adjacent to the hydraulic lift reservoir. Collect two foot composite soil sample from grade Y p p to 6'below grade surface(bgs). Place each soil sample in a sealed 250-milliliter Jjar with an aluminum septum. Agitate jars to develop organic vapors and field screen with a photoionization detector(PID)by"jar headspace"method for total organic volatiles(TOV). TOV concentration reported as 0.2ppm. PetroFlag TPH analyses exceeded 2,000mg/Kg. Forward soil sample to laboratory for confirmatory TPH analyses. 5/31/05 Receive laboratory analytical reporting a TPH concentration of 5,400mg/Kg identified as within the range for lubricating or hydraulic oil, as exceeding the applicable RCS-1 Reportable Concentration of 200mg/Kg. BENNETT & O'REILLY, INC. advised the property owner's representative of the findings of the physical testing stating that the noted impact represented a 120-day Reportable Condition with Release Notification and Remedial Response liability for the subject property, in accordance with 310 CMR 40.0000. 7/6/05 9:30 am BENNETT & O'REILLY, INC. personnel (Kara Risk, ES/PM; Samantha Westgate, ET) arrive on-site. The southwest bay door adjacent to the area of soil removal is noted as up and blocked by the former awning. The hydraulic lift and reservoir have been removed as has soils from a T (W) x 8.5' (L) x 8.5' deep area. The area of HB-12 noted as significantly impacted with hydraulic oil remains intact. Carefully collect sidewall and bottom of hole samples via a hand auger. Place soils into 250 mL glass jars sealed with aluminum septa, agitate and screen using a PID [Photovac 2020] photoionization detector as follows: LOCATION DEPTH PID PAGE 3 OF 5 WALKER-BO05-4316 SW-N 0-3' 2.7 3-8' 6.2 SW-S 0-3' 3.1 3-8' 3.7 SW-E 0-3' 3.7 3-8' 4.6 SW-W 0-3' 2.5 3-8' 5.5 BOH 8.5-9' 3.3 (damp soils) Note darkened soils at approximately 5'below grade. Collect a soil sample specifically from that area darkened soils. Place into a 250 mL glass jar sealed with an aluminum septum, agitate and screen using a PID [Photovac 2020] photoionization detector as follows: LOCATION DEPTH PID Darkened Soils 5' 2.8 Collect contaminated stockpile soil sample for MA Disposal Characterization. 11:00 am Gauging on-site monitoring wells in review of site-specific groundwater flow direction [Refer to the Monitor Well Sampling Log]. Perform Dexsil PetroFlag analysis of selected soil samples. Screen as follows: LOCATION DEPTH DEXSIL SW-N 3-8' 173 mg/Kg BOH-N 8.5-9' 35 mg/Kg Additional soil removal is needed in the area of HB-12. 12:30 m p BENNETT& UREILLY, INC.personnel secure the Site and depart. 1:15 pm Return to BENNETT & UREILLY, INC. office. Kara Risk speaks with Lynette Walker regarding the assessment conducted to date and the need to further extend the area of excavation to the south(HB-12). Ms.Walker is also informed that measures should be taken to secure the building and area of excavation such as the placement of plywood in the bay doorway. i PAGE 4 OF 5 WALKER-BO05-4316 BENNETT & O'REILLY, INC. personnel arrive at the office. Kara Risk speaks to the excavator, Christian Jolly of CEJ Excavating, regarding extension of the excavation to the south. Concerns are expressed regarding the excavation approaching the interior wall. Chris Jolly states that he will assume responsibility relative to protecting the adjacent wall and/or shoring needs. Prepare soil samples for confirmatory laboratory analysis. 7/8/05 9:00 am BENNETT&O'REILLY,INC.personnel(Kara Risk,ES/PM)arrive on-site and are met by the excavator, Chris Jolly. Instruct the excavator to remove the additional concrete to the south of the excavation and adjacent to the southern partition wall in the area of HB-12. Collect soil samples. Screen with the PID as follows: LOCATION DEPTH PID SW-S(1) 3-8' 4.7 BOH-S 8-9' 5.3 i Perform Dexsil PetroFlag analysis on the soil samples. Screen as follows: LOCATION DEXSIL(m /g_o SW-S(1):3-8' 367 BOH-S:8-9' >2,000 Extend the sidewall south area. Recollect soil samples. Screen as follows: LOCATION PID DEXSIL SW-S(2) 5.1 1091 mg/Kg BOH BDL Extend the sidewall south area fully beneath the partition wall. Recollect soil samples. I j LOCATION PID DEXSIL SW-S(3) 3.2 0.0 mg/Kg Secure the Site with caution tape. instruct the contractor that BENNT ETT & O'REILLY, INC.will contact him when the laboratory results are in and will prepare a Bill of Lading for the transport of soils off-site. Advise the contractor to segregate the concrete and metal from the stockpile: I - i PAGE 5 OF 5 WALKER-BOOS-4316 Prepare samples for confirmatory laboratory analysis. BENNETT& UREILLY, INC. personnel depart the site. Submitted by: BENNETT & UREILLY, INC. Kara M. Ris , ES H Project Manager Samantha Westgate Environmental Technician This Field Response Log is a compilation offield observations, interviews with individuals familiar with the project and a review of public record. As such, it is intended to he an accurate and complete record of pertinent information. However, based on the reliance on thirdparty and hearsay information included, no guarantee or warranties of the accuracy and completeness of that information is expressed or implied. i i i I APPENDIX C ro x i September 9, 2005 AGGREGATE David Bennett INDUSTRIES Bennett & O'Reilly, Inc. 1573 Main Street P.O. Box 1667 Brewster, MA 02631 Re: Soil, James Walker 143 Old Yarmouth Road Hyannis, MA Release Tracking#: LRA Recyclable soil from the above referenced address was received at our facility on September 6,.2005. Attached are the shipper's log of soil receipts, which total 33.35 tons, along with the Bill of Lading and other receipt documentation. We will issue a"Certificate of Recycling"upon request after processing. Thank you for recycling soil at our So. Dennis facility. Yours truly, William R. Reinhardt Manager, Soil Division AGGREGATE INDUSTRIES- Northeast Region, Inc. 1101 Turnpike Street Stoughton,Massachusetts 02072 Telephone 781-344-1100 Facsimile 781-341-5523 SOIL RECYCLING SUBMITTAL Revised 3/12/99 AGGREGATE INDUSTRIES nv'f- ac> r L _g_ - k4r tz ��1101`Turnp�ke Street, Stoughton AMA 02072 ��Tel (781)341, 5500 `� � Fax (781)341 2440� �r"�� _, 4..1....x, sm..,.<s s.... ..... .. ._s.r_w'z_,.:.. Site Information: NAME James Walker CONTACT STREET 143 Old Yarmouth Road PHONE 508-775-0100 CITY/TOWN Hyannis STATE/ZIP MA/02601 Generator Information: NAME James Walker CONTACT STREET 726 Falmouth Road PHONE 508-775-0100 CITY/TOWN Hyannis STATE/ZIP MA/02601 Consultant Information: NAME BENNETT&O'REILLY, INC. CONTACT Kara Risk STREET 1573 Main Street P.O. Box 1667 PHONE 508-896-6630 CITY/TOWN Brewster STATE/ZIP NIA. 02631 Estimated Soil Quantity: TONS 53 CUBICYARDS 35 Soil Contaminants (gasoline,diesel fuel,motor oil,etc.) Hydraulic oil i Analyses Performed (check all that apply) ❑ TPH ❑ As ❑ pH ❑ Reactivity(S,CN) ❑ PCBs ❑ Flash ❑ Cr ❑ Pb TCLP(metals)if required ❑ vocs ❑ Cd ❑ Hg ❑based on total levels ❑ other j I All the above tests Laboratory analytical Screening Data were performed I I data attached I,J Attached j . Instrument Used and Constituents Found PetroFLAG TPH analysis=>2000mg/Kg Environmental Services.Revised 3/12/99. page 1 of 3 i I Description / Source of Release: UST DATE OF RELEASE Unknown OTHER,DESCRIBE AST Soil Description PHYSICAL DESCRIPTION(SAND,GRAVEL,SILT,ETC.) SAND,fine to medium CLASSIFICATION METHOD Unified Soil Classification Method Check if the following materials are present(check all that apply) P ❑CLAY B CONSTRUCTION DEBRIS ❑ OTHER DELETERIOUS MATERIALS(PLEASE LIST) i COAL ❑ VEGITATIVE MATTER I ASH Soil Characterization Methodology Sampling Method GRAB a) COMPOSITE BIAED SAMPLES ❑ (E GS HEA SPACE SCREENED,VISUALLY CONTAMINATED) CONSTITUTES OF CONCERN Hydraulic oil I Site History CHECK IF EXTRA SHEETS ATTACHED CURRENT USE Boat storage PAST USE Automotive repair I,the generator,having used due diligence determined that there is no reason to suspect or believe that the petroleum contaminated soil has been impacted by any releases of oil or hazardous materials other than that of the known source or I have identified the additional oil and hazardous materials that are suspected or known to be present in the soil,in addition to those associated with the known release,including any anthropogenic contaminants. I,the generator,realize that due diligence shall consisit of a search of information and records reasonably available to the generator of the contaminated soil and sufficient to make the determination.Such records and information may include, but are not limmited to,those of the generator, location of generation(i.e.facility if not the generator),the Department's Bureau of Waste Site Cleanup and the municipality(i.e.Board of Health,Fire Department)within which the site is located. All samples for VOC analysis were collected according to DEP policy#99-415. I _ i FNATURE OF GENERATOR '7 r "" � DATE ] 4 GENERATOR-PRINTED NAME James Walker AGGREGATE Environmental Services.Revised 3/12/99. page 2 of 3 ' INDUSTRIES i �y A site diagram is required indicating any major structures or roads,excavation areas and stockpile locations. All sampling locations must be.noted. ElCHECK IF DIAGRAM ATTACHED Site Diagram NAME OF INDIVIDUAL PREPARING DIAGRAM: • Y-Y AGGREGATE Environmental Services(BTES/900)12/3/97.Revised 3/12/99. page 3 of 3 INUUSfl 0 'i Massachusetts Department of Environmental Protection BWSC-012A Bureau of Waste Site Cleanup Release Tracking Number* BILL OF LADING (pursuant to 310 CMR 40.0030) _ LRA A. LOCATION OF SITE OR DISPOSAL SITE WHERE REMEDIATION WASTE WAS GENERATED: Release Name(optional): Walker Street: 143 Old Yarmouth Road Location Aid: Map 344 Parcel 78-01 Cityfrown: Hyannis ZIPCode: 02601 Date/Period of Generation: 6/2 2/0 5 to: 7/8/0 5 Additional Release Tracking Numbers Associated with this Bill of Lading: .Note: If this Bill of Lading is the result of a Limited Removal Action(LRA) taken prior to Notification, a Release Tracking Numberis not needed. B. PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF LADING: Name of Organization: Name of Contact: James Walker Title: Property Owner Street: 726 Falmouth Road City/Town: Hyannis State: MA ZIP Code: 02601 Telephone: (508) 775-0100 Ext.: C. RELATION5HIP TO RELEASE of PER50N coNDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF LADING: ❑✓ RP or PRP Specify: ✓� Owner Operator ❑ Generator ❑ Transporter Other RP or PRP: Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E,s.2) Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21E,s.5())) Other Person: If an owner and/or operator is not conducting the response action associated with the Bill of Lading,provide on an attachment the name, contact person,address and telephone number,including any area code and extension,for each,if known. D. TRANSPORTER OR COMMON CARRIER INFORMATION: Transporter/Common Carrier Name: CEJ Excavating Contact Person: Christian Jolly Title: Owner/Operator Street: P.O. Box 631 Dennis MA ZIPCode: 02638 City/Town: State: Telephone: (774) 353-6524 Ext.: E. RECEIVING FACILITY/TEMPORARY STORAGE LOCATION: Operator/FacilityName: Aggregate Industries Contact Person: Bill Reinhardt Title: Soils Manager Street: 230 Great Western Road City/Town: South Dennis State: MA ZIP Code: 02660 Telephone: 7 81-3 41-5 5 0 0 Ext.: Type of Facility: ✓� Asphalt Batch/Cold Mix ❑ Landfill/Disposal Incinerator Temporary Storage (check one) Asphalt Batch/Hot Mix Landfill/Daily Cover Other: ❑ Thermal Processing Landfill/Structural Fill EPA Identification#: MAD 985286384 Division of Hazardous Waste/Class A Permit#: S-01-0 2 7 Division of Solid Waste Management Permit#: Actual/Anticipated Period of Temporary Storage(specify dates if applicable): to: Reason for Temporary Storage: Revised 10/3/94 Page 1 of 3 Massachusetts Department of Environmental Protection BWSC-012A Bureau of Waste Site Cleanup { Release Tracking Number' BILL OF LADING (pursuant to 310 CMR 40.0030) - LRA E. RECEIVING FACILITY/TEMPORARY STORAGE LOCATION(continued): Temporary Storage Address: Street: City/Town: State: ZIP Code: F. DESCRIPTION OF REMEDIATION WASTE: (check all that apply) Contaminated Media(check all that apply): Soil O Groundwater O Surface Water O Other:_ Contaminated Debris(check all that apply): O Vegetation or Organic Debris Demolition/Construction Waste OInorganic Absorbant Materials O Other: ElNon-hazardous Uncontainerized Waste(check all that apply): O Non-aqueous Phase Liquid O Other: Non-hazardous Containerized Waste(check all that apply): O Tank Bottoms/Sludges O Containers O Drums OEngineered Impoundments O Other: Type of Contamination(check all that apply): . El Gasoline ❑ Diesel Fuel 11 #2 Oil ❑ #4 Oil #6 Oil ❑ Waste Oil ❑ Kerosene R Jet fuel ❑ Other:_ 1-11rr9raill ;c ni I Estimated Volume of Materials: Cubic Yards: 35 Tons: 5:1. Other: Contaminant Source(check one/specify): ❑ Transportation Accident ❑ Underground Storage Tank © Other: _ Fuel line Response Action Associated with Bill of Lading(check one): El Immediate Response Action ❑ Release Abatement Measure ❑ Utility-Related Abatement Measure W1 Limited Removal Action Comprehensive Response Action El Other Remediation Waste Charcterization Support Documentation attached: Ei� Site History Information R Sampling and Analytical Methods and Procedures W Laboratory Data R Field Screening Data If supporting documentation is not appended,provide an attachment stating thedate and in connection with what document such information was previously submitted to DEP. G. LICENSED SITE PROFESSIONAL(LSP)OPINION: Name of Organization: BENNETT & 0'REILLY. INC. LSP Name: David C. Bennett Title: Director of Env. Services Telephone: . (508) 896-6630 Ext.: I attest under the pains and penalties of perjury that I have personally examired and am familiar with this submittal,including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of (1)the standard of care in 309 CMR 4.02(1), (ii)the applicable provisions of 309 CMR 4.02(2)and(3),and (iii)the provisions of 309 CMR 4.03(5), to the best of my knowledge,information and belief,the assessment actions undartaken to characterize the Remediation Waste which is(are)the subject of this submittal for acceptance at the facility identified in this subnittal comply with the appli isions of 310 CMR 40.0000,and such facility is permitted to t Remed' do Waste having the characteristics described in this su ` hat significant penalties may result, including,but not limit d to ne d imprisonment,if I submit in4rmation which I to or materially incomplete. DWO LSP Signature: Seal: BENNETT No.4-403 Date: License Number: 4303 �SIT l i, Revised 10/3/94 Page 2 of 3 Massachusetts Department of Environmental Protection BWSC-012A Bureau of Waste Site Cleanup Release Tracking Number* BILL OF LADING (pursuant to 310 CMR 40.0030) ❑ _ LRA H. CERTIFICATION OF PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING: I certify under penalties of law that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this certification,and that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained herein is,to the best of my knowledge and belief,true,accurate and complete. I am aware that there are significant .penalties,including,bu t limited to,possible fines and imprisonment,for willfully submitting false,inaccurate,oTiv plate information. Signature: Date: 0/ / Q� Name of Person(prin James Walker I Revised 10/3/94 Page 3 of 3 Massachusetts Department of Environmental Protection BWSC-012B Bureau of Waste Site Cleanup BILL OF LADING (pursuant to 310 CIVIR 40.0030) Release Tracking Number SUMMARYSHEET OF I. LOAD INFORMATION: Signatiure of Transporter Representative: Receiving acili empora torage Representative: Load 1: �i���.�r7'lZ. 1J � , Date of Shipmer�y lTiime of Shipment: `C:3, [�AM ❑ PM Date of�Zeq6i p t Time of Receipt: C/ ❑ Truck/Tractor Registration: Trailer Registration(if any): I � / / � AM M k Q ' 73/�6 r Load Size(cu.yds./tons): Load 2: Signatiure of Transporter Representative: I Re ' ing Facility/Temporary Storage Representative: Date of§hipment- Time of Shipment: , AM Date of Receipt: Time of Receipt: l / (" ri ` r�. '/,f ❑ I ❑ AM 14 PM Truck/Tractor Registration: Trailer Registration(if any): , Load Size(cu.yds./tons): Load 3: Signatiure of Transporter Representative: Receiving Facility/TemporaryStorage Representative: I Date of Shipment: Time of Shipment: , AM � Date of Receipt M I p Time of Receipt: TrucklTractor Registration: Trailer Registration(if any): CCC"" l ul 0 3 �� [� AM PM I Load Size(cu.yds./tons): . to Load 4: Signatiure of Transporter Representative: I I Receiving Facility/Temporary Storage Representative: i Date of Shipment: Time of Shipment: ❑ AM ❑ PM Date of Receipt Time of Receipt: AM PM I ❑ ❑ , Truck/Tractor Registration: Trailer Registration(if any): I i I Load Size(cu.yds./tons): I !Load 5: Signatiure of Transporter Representative: Receiving Faciiityffemporary Storage Representative-.- Date of Shipment: Time of Shipment: I Date of Receipt: Time of Receipt: ❑ AM ❑ PM i [] AM ❑ PM Truck/Tractor Registration: Trailer Registration(if any): I i Load Size(cu.yds./tons): , Load 6: Signatiure of Transporter Representative: I Receiving Facility/Temporary Storage Representative: I Date of Shipment: . Time of Shipment: i Date of Receipt Time of Receipt: ❑ AM ❑ PM , ❑ AM PM Truck/Tractor Registration: Trailer Registration(if any): I i Load Size(cu.yds./tons): J. LOG SHEET VOLUME INFORMATION: Total Volume Recorded This Page(cu.yds.Aons) Total Carried Forward(cu.yds./tons): Total Carried Forward and This Page(cu.yds./tons): Revised 10/3/94 Page 1 of 1 r Massachusetts Department of Environmental Protection BWSC-012C Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 31/0 CMR 40.0030) Release Tracking Number SUMMARY SHEET l OF K. SUMMARY OF SHIPMENTS: Daily Volume Shipped Date of Shipment: Date of Receipt: Number of Loads Shipped: (cu.yds. on: Summary Sheet Total Shipped: 7 3 Bill of Lading Total Shipped (only if different): Revised 1013/94 Page 1 of 2 Massachusetts Department of Environmental Protection BWSC-012C Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 CMR 40.0030 Release Tracking Number SUMMARY SHEET ' ONLY COMPLETE ONE COPY OF THIS PAGE AND ATTACH TO THE FINAL COPY OF THE SUMMARY SHEET. L. ACKNOWLEDGMENT OF RECEIPT OF REMEDIATION WASTE AT RECEIVING FACILITY OR TEMPORARY STORAGE: Receiving Facility/Temporary Storage Representative(print): William R. Reinhardt Title: Manager �r Signature: Date: '/ M. ACKNOWLEDGMENT OF SHIPMENT AND RECEIPT OF REMEDIAI N WASTE BY PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL LADING: I certify.under penalties of law that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this certification,and that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in herein is,to the best of my knowledge and belief,true,accurate and complete, I am aware that there are significant penalties,including,but not limited to,possible fines and imprisonment,for willfully submitting false,inaccurate,or incomplete information. i q Signature: Date: 1 1-4 ' Name of Person(print): Kara Risk, Senior Environmental Scientist BEN= & O TEILLY, INC. for J Mes Walker Revised 10/3/94 Page 2 of 2 APPENDIX D 'I RECEIVED JUL 2 7 2005 GROU�®OWATER Groundwater Analytical,Inc. ®� P.O.Box 1200 ANA L TI ® 228 Buz Main Street (� Buzzards Bay, MA 02532 Telephone(508)759-4441 July 20, 2005 FAX(508)759-4475 www.groundwateranalytical.com Mr. David Bennett Bennett & O'Reilly, Inc. P.O. Box 1667 Brewster, MA 02631 LABORATORY REPORT Project: Walker/113005-4316 Lab I D: 85330 Received: 07-06-05 Dear Dave: Enclosed are the analytical results for the above referenced project. The project was processed for Standard turnaround. This letter authorizes the release of the analytical results, and should be considered a part of this report. This report contains a sample receipt report detailing the samples received, a project narrative indicating project changes and non-conformances, a quality control report, and a statement of our state certifications. The analytical results contained in this report meet all applicable NELAC standards, except as may be specifically noted, or described in the project narrative. This report may only be used or reproduced in its entirety. attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Should you have any questions concerning this report, please do not hesitate to contact me. Sincerely, Jonathan R. Sanford President J RS/s and Enclosures GROUNDWATER ANALYTICAL Sample Receipt Report Project: Walker/13005-4316 Delivery: GWA Courier Temperature: 3.2'C Client: Bennett&O'Reilly, Inc. Airbill: n/a Chain of Custody: Present Lab ID: 85330 Lab Receipt: 07-06-05 Custody Seal(s): n/a 85330-1 SW-N:3-8' Soil 7/6/05 10:30 MA DEP EPH with PAHs Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644557 250 mL Glass Proline BX16975 None n/a n/a 06-24-05 aLabIfD Sit ietd f '=4MatnS mpledvmMethod� r r t° Notes era w ,. 'Q0 85330-2 SW-W3-8' Soil 7/6/05 10:45 TPH by GC ASTM D3328-00 Mod Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644562 250 mL Glass Proline BX16975 None n/a n/a 06-24-05 Lab:ID " YF�eld ID Matr�xk Sam led "Method3 "' x 7 85330-3 SW-E:3-8' Soil 7/6/05 10:30 TPH by GC ASTM D3328-00 Mod Con ID Container Vendor QC Lot Presery QC Lot Prep ` Ship C644564 250 mL Glass Proline BX16975 None n/a n/a 06-24-05 LabID �' � �F�eld IDS c �': ��• Matnz' Sam led, �� �MetFiodm�a � '� ,, �§�`'�� v�y,� � , '� ;Not� �� �"3��' �=� 85330-4 BOH(N):8.5-9.0' Soil 7/6/05 11:00 TPH by GC ASTM D3328-00 Mod Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644565 250 mL Glass Proline BX16975 None n/a n/a 06-24-05 ri �v-'cr"��.a �'r r Va x" r4-.d$ "�"2 9 �F�eld30 s � Matnz Sampled Method � 7. sNotes ,.. s 85330-5 Contaminated Stockpile Soil 7/6/05 11:00 EPA 60106/7471A 5 RCRA Metals EPA 8082 PCBs TPH by GC ASTM D3328-00 Mod EPA 9045C Corrosivity EPA 1010 Mod Ignitability EPA SW-846,Chp.7 Reactivity Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644566 250 mL Glass Proline BX16975 None n/a n/a 06-24-05 C609360 250 mL Glass n/a n/a None n/a n/a n/a 85330-6 Contaminated Stockpile Soil 7/6/05 11:00 EPA 8260E TCL Volatile Organics Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C589413 40 mL VOA Vial Proline BX15002 Methanol R-4255S 12-06-04 n/a C562533 40 mL VOA Vial Proline BX15491 NaHSO4 R-4159A 03-11-05 n/a C562585 40 mL VOA Vial Proline BX15491 NaHSO4 R-4159A 03-11-05 n/a C562519 40 mL VOA Vial Proline BX15491 NaHSO4 R-4159A 03-11-05 n/a Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Data Certification Project: Walker/BO115-4316 Lab ID: 85330 Client: Bennett&O'Reilly,Inc. Received: 07-06-05 16:50 �qk1A DEP Com endturilo�f Arial teal Methods` � ���``' ) Project Location: n/a MA DEP RTN: . n/a This Form provides certifications for the following data set: EPA 8260R:. 85330-06 EPA 8082:. 85330-05 MA DEP EPH: 85330-01 EPA 60106: 85330-05 EPA 7470A/IA: 85330-05 Sample Matrices: Groundwater ( ) Soil/Sediment (X) Drinking water ( ) Other ( ) r MCF�SW 846 # .. 8260B (X) 8151A ( ) 8330 ( ) 601013 (X) 7470A/1A (X) Metliods,Used; _ „ i 8270C ( ) 8081A ( ) VPH ( ) 6020 ( ) 9012A� ( ) As spec f ed i MA`oEP 8082 (X) 8021 B ( ) EPH (X) 7000 S' ( ) Other ( ) u, u a ug a CompendiumofAnatyhcal .ti List ReleaseTrackmgNumber,(RTW � _.e � � ;a„ „ r 3 r SW 846 Method-90t 2A(EgwGalent[o 9010 raM�®i-@Phy"stologically Available Cyanide(PAt7 Methpd � <6(oheckali thatapply)}� 3S SW 86 Methods 7000 Senes< List individual'method and analyteµ9 ,N i� �,.u ; �+yin few"_.,ass.,, sr..re<u ..v.c AN An affirmative response to questions A, B,C and D is required for"Presumptive Certainty"status. A. Were all samples received by the laboratory in a condition consistent with that described on the Chain-of-Custody documentation for the data set? Yes B. Were all QA/QC procedures required for the specified analytical method(s) included in this report followed, including the requirement to note and discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Yes C. Does the analytical data included in this report meet all the requirements for"Presumptive Certainty,"as described in Section 2.0 of the MA DEP document CAM VII A,Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data? Yes D. VPH and EPH methods only: Was the VPH or EPH method run without significant modifications,as specified in Section 11.3? Yes A response to questions E and F below is required for"Presumptive Certainty"status. E. Were all QC performance standards and recommendations for the specified methods achieved? No F. Were results for all analyte-Fist compounds/elements for the specified / method(s)reported? - No All No answers are addressed in the attached Project Narrative. I,the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is,to the best of my knowledge and belief,accurate and complete. Signature: /�� / Position: President Printed Name: d' gonathan R.Anford Date: 07-20-05 Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Massachusetts DEP EPH Method Extractable Petroleum Hydrocarbons by GC/FID Field ID: SW-N:3-8' Matrix: Soil . Project: Walker/BO054316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85330-01 QC Batch ID: EP-2094-M Sampled: 07-06-05 10:30 Instrument ID: GC-9 Agilent 6890 Received: 07-06-05 16:50 Sample Weight: 16 g Extracted: 07-13-05 08:00 Final Volume: 1 mL Analyzed(AL): 07-18-05 20:48 %Solids: 85 . Analyzed(AR): 07-18-05 21:33 Aliphatic Dilution Factor: 1 Analyst: MM Aromatic Dilution Factor: 1 EPH Rnges� �_ _�_, ;; " " Concentration Umts eartAng umt . n-C9 to n-C18 Aliphatic H drocarbons t BRL mg/Kg 33 n-CI9 to n-C36 Aliphatic Hydrocarbons t BRL mg/Kg 33 n-Cl 1 to n-C22 Aromatic Hydrocarbons'° BRL mg/Kg 33 Unadjusted n-C11 to n-C22 Aromatic Hydrocarbons t BRL mg/Kg 33 CAS Number,j Anal e�r� � � -'_ yt_ C nc tration� Notee, '�Un)ts xepong umrt 91-20-3 Naphthalene BRL mg/Kg 0.56 91-57-6 2-Methyl naphthalene BRL mg/Kg 0.56 85-01-8 Phenanthrene BRL mg/Kg 0.56 83-32-9 Acenaphthene BRL mg/Kg 0.56 208-96-8 Acenaphthylene BRL mg/Kg 0.56 86-73-7 Fluorene BRL mg/Kg 0.56 120-12-7 Anthracene BRL mg/Kg 0.56 206-44-0 Fluoranthene BRL mg/Kg 0.56 129-00-0 Pyrene BRL mg/Kg 0.56 56-55-3 Benzo[a]anthracene BRL mg/Kg 0.56 218-01-9 Chrysene BRL mg/Kg 0.56 205-99-2 Benzo[b]fluoranthene BRL mg/Kg 0.56 207-08-9 Benzo[k]fluoranthene BRL mg/Kg 0.56 50-32-8 Benzo[a]pyrene BRL mg/Kg 0.56 193-39-5 1 Indeno[1,2,3-c,d]pyrene BRL mg/Kg 0.56 53-70-3 Di benzo[a,h]anthracene BRL mg/Kg 0.56 191-24-2 Benzo[g,h,i]perylene BRL mg/Kg 0.56 QC Surrogate Compoun`d � �e Spike] MeasuredReeovery QC Lrmits � Fractionation: 2-Fluorobiphenyl 3.0� 2.5 84 % 40-140% 2-Bromonaphthalene 3.0 2.7 91 % 40-140% Extraction: Chloro-octadecane 3.0 1.6 53 % 40-140% ortho-Terphenyl 3.0 2.2 73 % 40-140 *.. ..:�°.:;a' .mr A/QCCCrf1ICattOnt ,':-sa. w Fiz- '�' 1. Were all QA/QC procedures required by the method followed? Yes 2. Were all performance/acceptance standards for the required QA/QC procedures achieved? Yes 3. Were any significant modifications made to the method,as specified in Section 11.3.1.1? No Method non-conformances indicated above are detailed below on this data report,or in the accompanying project narrative and project quality control report. Release of this data is authorized by the accompanying signed project cover letter. The accompanying cover letter,project narrative and quality control report are considered part of this data report. Method Reference: Method for the Determination of Extractable Petroleum Hydrocarbons,MA DEP(Revision 1.1,2004). Sample extraction performed by microwave accelerated solvent extraction technique. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. t Hydrocarbon range data excludes concentrations of any surrogate(s)and/or internal standards eluting in that range. 0 n-C11 to n-C22 Aromatic Hydrocarbons range data excludes the method target analyte concentrations. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8082 Polychlorinated Biphenyls (PCBs) by GC/ECD Field ID: Contaminated Stockpile Matrix: Soil Project: Walker/BO05-4316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85330-05 QC Batch ID: PB-2196-P Sampled: 07-06-05 11:00 Instrument ID: GC-6 HP 5890 Received: 07-06-05 16:50 Sample Weight: 15 g Extracted: 07-14-05 09:00 Final Volume: 1 mL Cleaned Up: 07-18-05 10:00 Percent Solids: 99 Analyzed: 07-19-05 03:35 Dilution Factor: 1 Analyst: CRL `CAS Number Anatyte t� t .wConcenfratmn ,` {� Notes Units r Report��gum�t ; v 1 2 6 74-1 1-2 Aroclor 1016 BRL ug/Kg 80 11104-28-2 Aroclor 1221 BRL ug/Kg 80 1 1 1 41-1 6-5 Aroclor 1232 BRL ug/Kg 80 53469-21-9 Aroclor 1242 BRL ug/Kg 80 12672-29-6 Aroclor 1248 BRL ug/Kg 80 11097-69-1 Aroclor 1254 BRL ug/Kg 80 11096-82-5 Aroclor 1260 BRL ug/Kg 80 37324-23-5 Aroclor 1262 t BRL ug/Kg 80 11100-14-4 Aroclor 1268 BRL ug/Kg 80 QC SurrogateCompou ndjSpked Measured 5 Recioweryi � QC LLmtts First Tetrachloro-m-xylene 13 6 48 % 30-150 Column Decachlorobiphenyl 13 7 53 % 30-150% Second Tetrachloro-m-xylene 13 6 47 % 30-150 Column Decachlorobiphenyl 13 8 61 % 30-150% Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Sample extraction performed by EPA Method 3545. Cleanup performed by EPA Method 3660B and EPA Method 3665A. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. t Non-target analyte. Result is based on a single mid-range calibration standard. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Trace Metals - Field ID: Contaminated Stockpile Matrix: Soil Project: Walker/BOOS-4316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85330-05 Percent Solids: 99 Sampled: 07-06-05 11:00 Received: 07-06-05 16:50 Analysis Method QC Batch ID Prep Method Prepared Sample Weight Instrument ID Analyst EPA 601013' MB-0652-S EPA 3050B 07-09-05 11:25 0.5 g ICP-1 PE 3000 EB EPA 7471A' MP-1814-S EPA 7471A 07-08-05 09:00 0.6 g CVAA-1 PE FIMS EB CAS Number, Ana�lyte � C nceifrafionN°teskUnits sRportmt�mltQF� Aitalyzecl Method 7440-38-2 Arsenic,Total BRL mg/Kg 0.98 1 07-11-05 15:29 EPA 60106' 7440-43-9 Cadmium,Total BRL mg/Kg 0.49 1 07-11-05 15:29 EPA 60106' 744047-3 Chromium,Total BRL mg/Kg 9.8 1 07-11-05 15:29 EPA 60108' 7439-92-1 Lead,Total BRL mg/Kg 9.8 1 07-11-05 15:29 EPA 60106' 7439-97-6 Mercury,Total BRL mg/Kg 0.034 1 07-08-05 14:21 EPA 7471A' Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. DF Dilution Factor. - Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 SROUNDWATER ANALYTICAL Inorganic Chemistry Field ID: Contaminated Stockpile Matrix: Soil Project: Walker/BO05-4316 Received: . 07-06-0516:50 Client: Bennett&O'Reilly,Inc. Lab ID: 85330-05 Sampled: 07-06-05 11:00 %solids: 99 Container: 250 mL Glass Preservation: Cool Analyte. � � Resu[trxUnits RL� DF We�ghf AnalyiedQC BatVI ch Method ,st A aly t Corrosivity(as pH) 5.5 pH NA 1 20 g 07-07-0511:00 PH-0617-S EPA 9045C 2 Jew Ignitabil ity(as Flashpoint) >165 °F 70 1 100g 07-07-0511:00 FP-0317-S EPA 1010Mod 3 JBW Reactive Cyanide BRL mg/Kg 50 1 10g 07-07-0513:00 RC-0551-S SW-846 Chp.7.3 1 JBW Reactive Sulfide BRL mg/Kg 100 1 log 1 07-07-0513:00 RS-0551-S SW-846Chp.7.3 n/a JBW Method Reference: Methods for Chemical Analysis of Water and Wastes,US EPA,EPA-600/4-790-020(Revised 1983),and Methods for the Determination of Inorganic Substances in Environmental Samples,US EPA,EPA/600/R-93/100(1993),and Standard Methods for the Examination of Water and Wastewater,APHA,Twentieth Edition 11998),and Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. RL Reporting Limit. DF Dilution Factor. 1 Instrument ID: Milton Roy Spectronic 401 2 Instrument ID: Accumet AR50 3 Instrument ID: Boekel 152800 Flash Point Tester Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM Method`D3328-00 (Modified) Hydrocarbon Fingerprint by GC/FID Field ID: SW-E:3-8' Matrix: Soil Project: Walker/BO05-4316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85330-03 QC Batch ID: HF-2276-M Sampled: 07-06-05 10:30 Instrument ID: GC-12 Agilent 6890 Received: 07-06-05 16:50 Sample Weight: 16 g Extracted: 07-20-05 09:00 Final Volume: 1 mL Analyzed: 07-22-05 07:04 Dilution Factor: 1 Analyst: MB %Solids: 94 No petroleum product was identified for this sample. m• "s3 � RS =-:rm "'s"�,"w."aCOI1Cent1'dtl0n a"3%=mS a a' NOfeSrc� '.URItS a Anal te' v Re ortm L�m�t Total Petroleum Hydrocarbons BRL mg/Kg 61 QG<Surrrogate ,ompound g,4, Spiked Measured " '�Recove y, QC Limits= ortho-Terphenyl 2.7 2.1 76 % 60-140% Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM METHOD D3328-00 (Modified) ,Hydrocarbon Fingerprinting by GC/FID Lab ID: 85330-03 Hydrocarbons Laboratory 1.0 0.8 0.6 0.a 0.2 0.0 0 5 10 15 20 25 30 35 Retention Time (Minutes) GROUNDWATER ANALYTICAL ASTM Method D3328-00 (Modified).: Hydrocarbon Fingerprint by GC/FID Field ID: Contaminated Stockpile Matrix: Soil Project: Walker/B005-4316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85330-05 QC Batch ID: HF-2276-M Sampled: 07-06-05 11:00 Instrument ID: GC-12 Agilent 6890 Received: 07-06-05 16:50 Sample Weight: 15 g Extracted: 07-20-05 09:00 Final Volume: 1 mL Analyzed: 07-21-05 12:56 Dilution Factor: 5 Analyst: MB %Solids: 99 �zKr' s& zs 1i"'-va�"' y'€ "xa* ' ;rQUdlltatlVC�d nttftcatlon ¢ AE This sample has GC/FID characteristics that are similar to: 1. Petroleum products in the Lubricating Oil (n-C14 to n-C36) range. ytAnalg ew, t s : �. ' x E °Concetitratton � � ' , s r F�, Porting�fw„ m„az=%. Total Petroleum Hydrocarbons 9,300 mg/Kg 300 �Vwc- d d 60-140% Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. d Surrogate recovery not measurable due to required sample dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM METHOD D3328-00 (Modified) Hydrocarbon Fingerprinting by GC/FID Lab ID: 85330-05 Hydrocarbons Laboratory 1.0 0.8 0.6 0.4 0.2 0.0 0 5 10 15 20 25 30 35 Retention Time (Minutes) GROUNDWATER ANALYTICAL EPA Method 826013 TCL Volatile Organics by GUMS Field ID: Contaminated Stockpile Matrix: Soil Project: Walker/BO05-4316 Container: 40 mL VOA Vial Client: Bennett&O'Reilly,Inc. Preservation: NaHSO4/Cool Laboratory ID: 85330-06 QC Batch ID: VM1-1604-S Sampled: 07-06-05 11:00 Instrument ID: MS-1 HP 5890 Received: 07-06-05 16:50 Sample Weight: 4.8 g Analyzed: 07-11-05 14:07 %Solids: 99 Analyst: LMG Dilution Factor: 1 74-87-3 Chloromethane BRL ug/Kg 11 75-01-4 Vinyl Chloride BRL ug/Kg 11 74-83-9 Bromomethane BRL ug/Kg 11 75-00-3 Chloroethane BRL ug/Kg ii 1 75-35-4 1,1-Dichloroethene BRL ug/Kg 5, 67-64-1 Acetone BRL ug/Kg 210 75-15-0 Carbon Disulfide BRL ug/Kg 53 75-09-2 Methylene Chloride BRL ug/Kg 53 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 5 1634-04-4 Methyl tert-butyl Ether(MTBE) BRL ug/Kg 5 75-34-3 1,1-Dichloroethane BRL ug/Kg 5 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 5 78-93-3 2-Butanone(MEK) BRL ug/Kg 53 67-66-3 Chloroform BRL ug/Kg 5 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 5 56-23-5 Carbon Tetrachloride BRL ug/Kg 5 71-43-2 Benzene BRL ug/Kg 5 107-06-2 1,2-Dichloroethane BRL ug/Kg 5 79-01-6 Trichloroethene BRL ug/Kg 5 78-87-5 1,2-Dichloropropane BRL ug/Kg 5 75-27-4 Bromodichloromethane BRL ug/Kg 5 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 5 108-10-1 4-Methyl-2-Pentanone(MIBK) BRL ug/Kg 53 108-88-3 Toluene BRL ug/Kg 5 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 5 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 5 127-18-4 Tetrachloroethene BRL ug/Kg 5 591-78-6 2-Hexanone BRL ug/Kg 53 124-48-1 Dibromochloromethane BRL ug/Kg 5 108-90-7 Chlorobenzene BRL ug/Kg 5 100-41-4 Ethylbenzene BRL ug/Kg 5 1 08-3 8-3/1 0 64 2-3 meta-Xylene and para-Xylene - 10 ug/Kg 5 95-47-6 ortho-Xylene 7 ug/Kg 5 100-42-5 Styrene 6 ug/Kg 5 75-25-2 Bromoform BRL ug/Kg 5 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 5 u.• QC Surrogate Compound ys,s Spiked MeasuredRecouer , � QC Ltmtts t Dibromofluoromethane 50 54 107 % 70-130%° 1,2-Dichloroethane-d4 50 52 103 % 70-130 Toluene-de 50 52 105 % 70-130 4-Bromofluorobenzene 50 170 338 % m 70-130 Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Sample preparation performed by EPA Method 5035A. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. m Surrogate recovery outside recommended limits due to sample matrix interference. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL = EPA Method 06013 TCL Volatile Organics by GC/MS Field ID: Contaminated Stockpile Matrix: Soil Project: Walker/6005-4316 Container: 40 mL VOA Vial Client: Bennett&O'Reilly,Inc. Preservation: NaHSO4/Cool Laboratory ID: 85330-06RA1 QC Batch ID: VM1-1607-S Sampled: 07-06-05 11:00 Instrument ID: MS-1 HP 5890 Received: 07-06-05 16:50 Sample Weight: 4 g Analyzed: 07-14-05 12:32 %Solids: 99 Analyst: LMG Dilution Factor: 1 ti a ; aCAS tJumberAnalyte oncentrabon F= Notes -Units �:, ReportingLrmrt 74-87-3 Chloromethane BRL ug/Kg 13 75-01-4 Vinyl Chloride BRL ug/Kg 13 74-83-9 Bromomethane BRL ug/Kg 13 75-00-3 Chloroethane BRL ug/Kg 13 75-35-4 1,1-Dichloroethene BRL ug/Kg 6 67-64-1 Acetone BRL ug/Kg 260 75-15-0 Carbon Disulfide BRL ug/Kg 64 75-09-2 Methylene Chloride BRL ug/Kg 64 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 6 1634-04-4 Methyl tert-butyl Ether(MTBE) BRL ug/Kg 6 75-34-3 1,1-Dichloroethane BRL ug/Kg 6 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 6 78-93-3 2-Butanone(MEK) BRL ug/Kg 64 67-66-3 Chloroform BRL ug/Kg 6 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 6 56-23-5 Carbon Tetrachloride BRL ug/Kg 6 7143-2 Benzene BRL ug/Kg 6 107-06-2 1,2-Dichloroethane BRL ug/Kg 6 79-01-6 —Trichloroethene BRL ug/Kg 6 78-87-5 1,2-Dichloropropane BRL ug/Kg 6 75-27-4 Bromodichloromethane BRL ug/Kg 6 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 6 108-10-1 4-Methyl-2-Pentanone(MIRK) BRL ug/Kg 64 108-88-3 Toluene BRL ug/Kg 6 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 6 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 6 127-18-4 Tetrachloroethene BRL ug/Kg 6 591-78-6 2-Hexanone BRL ug/Kg 64 124-48-1 Dibromochloromethane BRL ug/Kg 6 108-90-7 Chlorobenzene BRL ug/Kg 6 100-41-4 Ethylbenzene BRL ug/Kg 6 108-38-3/10GA2-3 meta-Xylene and para-Xylene 19 ug/Kg 6 95-47-6 ortho-Xylene 11 ug/Kg 6 100-42-5 Styrene 11 ug/Kg 6 75-25-2 Bromoform BRL ug/Kg 6 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 6 , QC�Surrogate�CompounrlT� er�.;��,� � Spifced Measured ��� kRecovery �,� �'� "m°"r���� C L"tmtts� Di_bromofluoromethane 50 47 93 % 70-130% I 1,2-Dichloroethane-d4 50 1 47 1 93 % 70-130 Toluene-da 50 44 87 % 70-130% 4-Bromofluorobenzene 50 230 468 % m 70-130% Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Sample preparation performed by EPA Method 5035A. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. m Surrogate recovery outside recommended limits due to sample matrix interference. _ Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Project Narrative Project: Walker/BO05-4316 Lab ID: 85330 Client: Bennett%&O'Reilly, Inc. p Received: 07-06-05 16:50 : $FH'ya��r'e 'S 3.�, s r,� � 4 Documentation sand Glient Comrrun�catiQn The following documentation discrepancies,and client changes or amendments were noted for this project: 1 . Sample 85330-05 was also analyzed for TPH by ASTM D3328-00 Modified,per Kara Risk,07-08-05. 2 . Samples 85330-2 through-4 for analysis by ASTM D3328-00-Mod.were extracted and then held for potential analysis, per Kara Risk,07-08-05. FF r ,�..� 'S z ��B MethodModifcations, No��n��C�o�n�formancesand Obs�er�u4ations �F & � �,� , � �- �`,�� The sample(s) in this project were analyzed by the references analytical method(s), and no method modifications, non-conformances or analytical issues were noted,except as indicated below: 1 . EPA 601013 Note:Samples 85330-05. Samples were analyzed for selected target analytes,as requested by client. 2 . EPA 8260B Non-conformance: Sample 85330-06.Sample had a surrogate recovery outside recommended limits due to matrix interference. Sample reanalysis confirms matrix interference. 3 . EPA 8260B Note:Samples 85330-06. Sample was analyzed for only selected target analytes,as requested by client. Groundwater Analytical, Inc., P.O. Box 1200,228 Main Street, Buzzards Bay, MA 02532 —GROUNDWATER- �®®//p�®��N�__228 Main Street,P.O.Box 1200 /T U d I E wizards-Bay,MA-02532-- -- ANALYTICAL Telephonedwater nalyti al.com 508)759-4475 AND WORK ORDER N2 107249 www.groundwaterana lytical.cam Project Name: Firm: TURNAROUND ANALYSIS REQUEST STANDARD(10 Business Days) Volatilas SemirolaQles Pes ,rb CBs Metals Peemeum mnrboo Hat. General Chemist ether Project Number: Address: thadah he Val. IFH WI Waste ❑ PRIORITY(5 Business Days) _ S ❑ RUSH(RAN- a (Rush requires Rush Authorization Number) p 000 .n 3 ❑ ❑ d a Sampler Name: City/State _/Zip: ❑Please Email to: o 1 � Qxp tl , (`ilf� �Z � L�tPlease FAX to:( 1�9(e-gloli•� m ' o ` o Ri s ❑ Pr ect Mana is Telephone- BILLING A - a o 1 0 0 0 o y �, E Lab)89t0- u-0-6o ° ° ❑ 70 Purchase Order No.:RCS-43110 m e otl ? _ INSTRUCTIONS:Use ❑ Third Party Billing: m o 0 2 z a a o z separate line for each container(except replicates). =A a _ ❑ GWAQuote: a ;o d a d d E s - ❑ s o e Sampling Matrix e o 0 0 0 0 0 0 0 0 6 ❑ I. 0 0 ° 6 a ❑ Type Containers) Preservation R s A a a ❑ € SAMPLE - _ - _ LABORATORY W o a d m � ❑ o o ° o IDENTIFICATION 3 - `moo' - a e _ NUMBER �" m a a A o ; m s s g A x p ❑ & ❑ w w - - w > a to (Lab Use Only) - e _ n a r o n d o e E E E E S E r$ti n r n! d ¢ .; u — — A E ❑ ❑ o o 0 ❑❑ ❑ ❑ ❑ ❑ ❑ ❑ In ❑ ❑ 0000 ❑ ❑ ❑ ❑ a , ❑ ❑ G ❑ ❑ ❑ ❑ ❑ ❑ ❑ C G C ijj e 7 7, M - LLL FFF ELL 1 2 F .. .. q REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program Project Specific OC NOTE:All samples submitted subject to Standard Terms and Conditions on reverse hereof. MA DEP MCP Data Enhancement Affirmation State Standard Deliverables Many regulatory programs and EPA methods require project Relinquished by Sampler: Date Time Received by: Receipt Temperature: specific QC.Project specific QC includes Sample Duplicates, �/�y YES ONO MCP Data Certification is required. ❑CT IfdMCP GW-1B-1 ❑PWS Form Matrix Spikes,and/or Matrix Spike Duplicates.Laboratory QC is 6 Z; ❑�❑aeo-pp,ara not project specific unless prearranged.Project specific OC za•c aemmmeraed ❑ME ❑MCP GW-2/S-2 ❑MWRA li wished Recei OYES D9N0 MCP Drinking Water Sample Required. MA El STARS ❑ samples are charged on a per sample basis.Each MS,MSD q Date Time Container Count: and Sample Duplicate requires an additional sample aliquot. / [,� 9 (Require collection Of contingent duplicate sample. ❑NH ❑Drinking Water R n(�J / Trip blanks are also required.IIVOA sample collected) ❑NY ❑Wastewater Project Specific OC Required Selection of OC Sample Relinquis Dat Time Received by boratory: Shipping/Airbill Signature: ❑RI ❑Waste Disposal ❑Sample Duplicate ❑Please use sample: '7' `� Number: - too ❑VT ❑Dredge Material ❑Matrix Spike r.� Cu Method of Shipment:tgGWA Courier❑Express Mail❑Federal Express stody Seal ❑_ ❑ ❑Matrix Spike Duplicate ❑UPS❑Hand❑ Number: I - r 1 ,:I ---------------- ------.. -----I l --_.6�[ p®UNiddy/�,w, j 228 Main Street,P.O.Box 1200 1 - - ----BuzxardsBay, P.MAo25a2---------- - - ----CHAIN-OF-C—USTODY-RECORD----__..__.._�._ 1 t ANALYTICAL Telephone(508)759-4441-FAX(508)759-4475 AND WORK ORDER N 2( 108596 www.groundwateranalytical.com Project Name: T4� TURNAROUNDWa1U_ IANALYSIS REQUEST �STANDARD(10 Business Days) Valatiles Semhoutlla PenRIeNtIPtBs Meuh xaz. sexral Cftmft" Other edble Yal Eat Il Yel."H Wade Project Number: Address: ❑ PRIORITY(5 Business Days) - u ❑ RUSH(RAN- ) a _ (Rush requires Rush Authorization Number) o c V ' o e Sampler Name: City/State/Zip Please Email to:. o Please FAX to:�Y)fC KCU04 i9'�+ 3 m N 6 A ❑ o $ Pro ect Manager: Telephone: /�w y BILLING o 0 0 0 0 3 106 �iPurchase Order No.: D05-431(a 003 0 0 e = /❑_Third Party Billing: w o _ = f o g . o INSTRUCTIONS:Use separate line for each container(except replicates). ❑ GWA Quote: F d -- 1�e 0 o o - o Sampling Matrix T Contains s o 0 0 o a o o a o o� ❑ a o - o 6 o YPe r( ) Preservation _ a 0 A s t d - LABORATORY o - 9 e o A m ❑ 0 SAMPLE _ - x = 6 e S q } s m o 3 A 8 IDENTIFICATION 3` w - < e o a e _ - NUMBER o g F - ❑ € (Lab Use Only) s r d S o 0 0 - E E F n.�.. 0 0 o n ^ m ¢¢ m r c o `✓ a C S Q H 3 0 o S o _ ❑❑❑ ❑ G ❑ ❑ ❑ ❑ ❑ ❑ G 0000 ❑ ❑ ❑ ❑ ❑ ❑ O ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ;.. ... s,�q fx- i, :'„'r t r.,- .�� -,.v�� a CS 1.'C `@ CA:ad". fi, F,�.. r`'.irn `:?•� .t '� r' - y . - - --` I - - - - --- i ' IN 14 < 4- (s r REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program Project Specific DC NOTE:All samples submitted subject to Standard Terms and Conditions on reverse hereof. MA DEP MCP Data Enhancement Affirmation State Standard Deliverables Many regulatory programs and EPA methods require project Filtillnquished by Sampler: Date Time Received by: Receipt Temperature: iii��� specific QC.Project specific QC includes Sample Duplicates, ' }YES XNO MCP Data Certification is required. ❑CT f�[MCP GW-1/S-1 ❑PWS Form Matrix Spikes,and/or Matrix Spike Duplicates.Laboratory QC is f ❑ ❑t` e° 5 3 OYES NO MCP Drinking Water Sample Required. ❑O M"E /❑MCP GW-2/S-2 ❑MWRA not project specific unless prearranged.Project specific OC 2 a onv a tle° I�l}vIA ❑NY STARS ❑ samples are charged on a per sample basis.Each MS,MSD Relinquished by: Date Time Received by: ,Q.S,�' Container Count: (Require collection Of Contingent duplicate sample. ( and Sample Duplicate requires an additional sample aliquot r- I Trip blanks are also required.If VOA sample collected) ❑NH ❑Drinking Water 7 13 D5 Signature: ❑NY ❑Wastewater Project Specific OC Required Selection of OC Sample Relinquished by: Date Time Received by Laborato : Shipping/Airbill g ❑RI ❑Waste Disposal ❑Sample Duplicate ❑Please use sample: Nu tmber. 7(3 oS 1'?t21 ❑VT ❑Dredge Material ❑Matrix Spike Method of Shipmen: GWA Courier❑Express Mail❑Federal Ex a Custody Seal ❑— ❑ ❑Matrix Spike Duplicate Number: ❑UPS❑Hand❑ I i i 4 ' I f� 1 i GROUNDWATER A NALYTICAL -_ar Quality Assurance/Quality Control - r=t ''r Groundwater Analytical conducts an active Quality Assurance program to ensure the production of high quality, valid data. This program closely follows the guidance provided by Interim Guidelines and Specifications for Preparing Quality Assurance Project Plans, US EPA QAMS-005/80 (1980), and Test Methods for Evaluating Solid Waste, US EPA, SW-846, Update III (1996). Quality Control protocols include written Standard Operating Procedures (SOPs) developed for each analytical method. SOPS are derived from US EPA methodologies and other established references.. Standards are prepared from commercially obtained reference materials of certified purity, and documented for traceability. Quality Assessment protocols for most organic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. All samples, standards, blanks, laboratory control samples, matrix spikes and sample duplicates are spiked with internal standards and surrogate compounds. All instrument sequences begin with an initial calibration verification standard and a blank; and excepting GUMS sequences, all sequences close with a continuing calibration standard. GUMS systems are tuned to appropriate ion abundance criteria daily, or for each 12 hour operating period, whichever is more frequent. Quality Assessment protocols for most inorganic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. Standard curves are derived from one reagent blank and four concentration levels. Curve validity is verified by standard recoveries within plus or minus ten percent of the curve. ,r'. '.t ci`_ Xs ✓b, ' "kt= "N'. �;.' `��rx �'�' °,��.���s.. � Af �v x B �efll]Itl®nSa} u a r � ati "� ..�'I' s,?s,,,'S. Batches are used as the basic unit for Quality Assessment. A Batch is defined as twenty or fewer samples of the same matrix which are prepared together for the same analysis, using the same lots of reagents and the same techniques or manipulations, all within the same continuum of time, up to but not exceeding 24 hours. Laboratory Control Samples are used to assess the accuracy of the analytical method. A Laboratory Control Sample consists of reagent water or sodium sulfate spiked with a group of target analytes representative of the method analytes. Accuracy is defined as the degree of agreement of the measured value with the true or expected value. Percent Recoveries for the Laboratory Control Samples are calculated to assess accuracy. Method Blanks are used to assess the level of contamination present in the analytical system. Method Blanks consist of reagent water or an aliquot of sodium sulfate. Method Blanks are taken through all the appropriate steps of an analytical method. Sample data reported is not corrected for blank contamination. Surrogate Compounds are used to assess the effectiveness of an analytical method in dealing with each sample matrix. Surrogate Compounds are organic compounds which are similar to the target analytes of interest in chemical behavior, but which are not normally found in environmental samples. Percent Recoveries are calculated for each Surrogate Compound. I Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL -- - Quality Control Report Laboratory Control Sample Category: ASTM D3328-00 Mod Hydrocarbon Fingerprint Instrument ID: GC-12 Agilent 6890 QC Batch ID: HF-2276-M Extracted: 07-20-05 09:00 Matrix: Soil Analyzed: 07-20-05 21:16 Units: mg/Kg Analyst: MB Measured� Recovery � QC L_mtts Fuel Oil No.2 130 100 77 % 60-140% C Surrogate Com ound w. s �' Sptked Measuredg ,. OC Ye l� QLlmlts s mom` ortho-Terphenyl 2.7 2.1 79 % 1 60-140% Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02,: American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL . _ Qualitys=Cont"rol Report Method Blank Category: ASTM D3328-00 Mod Hydrocarbon Fingerprint Instrument ID: GC-12 Agilent 6890 QC Batch ID: HF-2276-M Extracted: 07-20-05 09:00 Matrix: Soil Analyzed: 07-20-05 20:28 Analyst: MB tr'� NOtC5�5 a L1nitS -' _R¢poitin Ltm�� Concenatio(il Total Petroleum Hydrocarbons BRL mg/Kg 30 4 , ;- � 5�`Iked MeasUrCd QC �RCCOYe r , QC Llm tS ..x Surrogate Compound :: P� F ortho-Terphenyl 2.7 1.9 73 % 60-140% Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. --Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL_ Quality Control Report - Laboratory ColntrolSamples LCS LCSD Category: EPA Method 8260B TCL Instrument ID: MS-1 HP 5890 Instrument ID: MS-1 HP 5890 QC Batch ID: VM1-1607-SL Analyzed: 07-14-05 07:06 Analyzed: 07-14-05 07:41 Matrix: Soil Analyst: LMG Analyst: LMG Units: ug/Kg CAS Number Analyte J. iLCSDupltcate ) x QCltmtts� Measur ed: c �S iked' MeasureiisReco've `fRPD S ike ? RPD p Re ove x _ .p .74-87-3 Chloromethane 50 52 104 % 50 51 102 %• 2 % 70-130% 25% 75-014 Vinyl Chloride 50 52 105 % 50 51 102 % 2 % 70-130% 25% 74-83-9 Bromomethane 50 48 96 % 50 47 95 % 2 % 70-130% 25% 75-00-3 Chloroethane 50 49 98 % 50 47 93 % 4 % 70-130% 25% 75-354 1,1-Dichloroethene 50 53 107 % 50 49 97 % 8 % - 70-130% 25% 67-64-1 Acetone 100 88 88 % 100 86 86 % 2 % 70-130% 25% 75-15-0 Carbon Disulfide 100 92 92 % 100 85 85 % 8 % 70-130% 25 75-09-2 Methylene Chloride 50 47 94 % 50 46 91 % 2 % 70-130% 25% 156-60-5 trans-1,2-Dichloroethene 50 47 94 % 50 46 93 % 2 % 70 130% 25% 1634-04-4 Methyl tert-butyl Ether(MTBE) 50 44 89 % 50 45 90 % 2 % 70-130% 25% 75-34-3 1,1-Dichloroethane 50 45 90 % 50 45 90 % 0 % 70-130% 25% 156-59-2 cis-1,2-Dichloroethene 50 48 95 % 50 47 94 % 2 % 70-130% 25% 78-93-3 2-Butanone(MEK) 100 86 86 % 100 1 83 83 % 4 % 70-130% 25% 67-66-3 Chloroform 50 43 85 % 50 42 84 % 2 % 70-130% 25% 71-55-6 1,1,1-Trichloroethane 50 41 83 % 50 40 80 % 2 % 70-130% 25% 56-23-5 Carbon Tetrachloride 50 39 78 % 50 38 77 % 3 % 70-130% 25% 71-43-2 Benzene 50 48 95 % 50 47 95 % 2 % 70-130% 25% 107-06-2 1,2-Dichloroethane 50 39 78 % 50 40 80 % 3 % 70-130% 25% 79-01-6 Trichloroethene 50 47 94 % 50 46 93 % 2 % 70-130% 25% 78-87-5 1,2-Dichloropropane 50 46 92 % 50 47 95 % 2 % 70-130% 25% 75-274 Bromodichloromethane 50 43 1 86 % 50 43 86 % 0 % 70-130% 25% 10061-01-5 cis-1,3-Dichloropropene 50 46 92 % 50 46 93 % 0 % 70-130% 25% 108-10-1 4-Methyl-2-Pentanone(MIBK) 100 79 79 % 100 90 90 % 13 % 70-130% 25% 108-88-3 Toluene 50 47 94 % 50 47 93 % 0 % 70-130% 25% 10061-02-6 trans-1,3-Dichloropropene 50 42 84 % 50 44 88 % 5 % 70-130% 25% 79-00-5 1,1,2-Trichloroethane 50 53 107 % 50 55 110 % 4 % 70-130% 25 127-184 Tetrachloroethene 50 56 112 % 50 1 53 106 % 6% 70-130% 25 591-78-6 2-Hexanone 100 98 98 % 100 100 100 % 2 % 70-130% 25% 124-48-1 Dibromochloromethane 50 50 100 % 50 48 97% 4 % 70-130% 25% 108-90-7 Chlorobenzene 50 57 113 % 50 55 110 % 4 % 70-130% 25% 100-41-4 Ethylbenzene 50 56 ill % 50 53 106 % 6 % 70-130% 25% 108-38-3/10642-3 meta-Xylene and para-Xylene 100 110 114 % 100 110 111 % 0 % 70-130% 25% 95-47-6 ortho-Xylene 50 55 111 % 50 57 113 % 4 % 70-130% 25% 100-42-5 Styrene 50 58 116 % 50 58 115 % 0 % 70-130% 25% 75-25-2 Bromoform 50 50 100 % 50 51 101 % 2 % 70-130% 25 79-34-5 1,1,2,2-Tetrachloroethane 50 46 91 % 50 48 1 97 % 4 % 70-130% 25 ;�QC Surrggate Compound•. .. Spiked Me ured_ Recovery rSpike Measured RecovQry QC�Ltinttsx Dibromofluoromethane 50 46 92 % 50 44 88 % 70-130 1,2-Dichloroethane-d4 50 43 86 % 50 48 96 % 70-130% Toluene-de 50 54 107 % 50 53 106 % 70-130% 4-Bromofluorobenzene 50 53 107 % 50 54 107 % 70-130% Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Sample preparation performed by EPA Method 5030B. Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. - Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL QualiWControl`Report T _ Method Blank - Category: EPA Method 8260E TCL Instrument ID: MS-1 HP 5890 QC Batch ID: VM1-1607-SR Analyzed: 07-14-05 08:16 Matrix: Soil Analyst: LMG GAtS Number a Anal e �� Coricentrafion F � NotesUnits �n�h�L�m�t s P 74-87-3 Chloromethane BRL ug/Kg 10 75-014 Vinyl Chloride BRL ug/Kg 10 74-83-9 Bromomethane BRL ug/Kg 10 75-00-3 Chloroethane BRL ug/Kg 10 75-35-4 1,1-Dichloroethene BRL ug/Kg 5 67-64-1 Acetone BRL ug/Kg 200 75-15-0 Carbon Disulfide BRL ug/Kg 50 75-09-2 Methylene Chloride BRL ug/Kg s0 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 5 1634-04-4 Methyl tert-butyl Ether(MTBE) BRL ug/Kg 5 75-34-3 1,1-Dichloroethane BRL ug/Kg 5 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 5 78-93-3 2-Butanone(MEK) BRL ug/Kg 50 67-66-3 Chloroform BRL ug/Kg 5 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 5 56-23-5 Carbon Tetrachloride BRL ug/Kg 5 71-43-2 Benzene BRL ug/Kg 5 107-06-2 1,2-Dichloroethane BRL ug/Kg 5 79-01-6 Trichloroethene BRL ug/Kg 5 78-87-5 1,2-Dichloropropane BRL ug/Kg 5 75-274 Bromodichloromethane BRL ug/Kg 5 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 5 108-10-1 4-Methyl-2-Pentanone(MIBK) BRL ug/Kg 50 108-88-3 - Toluene ---- - - BRL ug/Kg 5 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 5 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 5 127-18A Tetrachloroethene BRL ug/Kg 5 591-78-6 2-Hexanone BRL ug/Kg 50 12448-1 Dibromochloromethane BRL ug/Kg 5 108-90-7 Chlorobenzene BRL ug/Kg 5 100-41-4 Ethylbenzene BRL ug/Kg 5 1 0 8-3 8-3/1 064 2-3 meta-Xylene and para-Xylene. BRL ug/Kg 5 95-47-6 ortho-Xylene BRL ug/Kg 5 100-42-5 Styrene BRL ug/Kg 5 75-25-2 Bromoform BRL ug/Kg 5 79-34-5 1,1,2,2-Tetrach loroethane BRL ug/Kg 5 QC Surrogate t�ompound s Spiked Me"asu fed �E Recoueiy b �� 90-9 mlts �. :, .. t >d. Dibromofluoromethane 50� 45 90 % 70-130 1,2-Dichloroethane-d4 50 45 90 % 70-130% Toluene-d8 50 53 107 % 70-130% 4-Bromofluorobenzene 50 61 121 % 70-130 Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Sample preparation performed by EPA Method 5035A. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL - _ - QualityContro6rQort _ Laboratory Control Samples- - LCS. LCSD Category: MA DEP EPH Method Instrument ID: GC-9 Agilent 6890 Instrument ID: GC-9 Agilent 6890 QC Batch ID: EP-2094-M Extracted: 07-13-05 08:00 Extracted: 07-13-05 08:00 Matrix: Soil Analyzed(AL): 07-14-05 01:09 Analyzed(AL): 07-14-05 02:38 Units: mg/Kg Analyzed(AR): 07-14-05 01:54 Analyzed(AR): 07-14-05 03:22 Analyst: MM Analyst: MM [CAS,�N,�umber Anal a , -LCS 3 � LCSDuphcate QCLrmtts�� Spiked Meas�rea Recovery Spiked MS�d Recovery RPD Sp�[ce RPD 111-84-2 n-Nonane(C9) _ 3.3 1.9 59 % 3.3 1.8 55 % 8 % 30-140°�0 25% 124-18-5 n-Decane(C,0) 3.3 2.2 68 % 3.3 2.1 63 % 7 % 40-140% 25% 112-40-3 n-Dodecane(C72) 3.3 2.3 69 % 3.3 2.1 64 % 7 % 40-140% 25% 629-59-4 n-Tetradecane(C14) 3.3 2.5 75 % 3.3 2.3 69 % 7 % 40-140% 25% 544-76-3 n-Hexadecane(Cl 6) 3.3 2.7 83 % 3.3 ..6 78 % 6 % 40-140% 25% 593-45-3 n-Octadecane(C18) 3.3 3.0 91 % 3.3 3.0 90 % 1 % 40-1,40% 25% n/a n-C9 to n-C18 Group 20 15 74 % 20 14 1 70 % 6 % 40-140% 25% 629-92-5 n-Nonadecane(C19) 3.3 2.9 89 % 3.3 2.9 88 % 1 % 40-140% 25% 112-95-8 n-Eicosane(C20) 3.3 2.8 84 % 3.3 2.7 82 % 3 % 40-140% 25% 629-97-0 n-Docosane(C22) 3.3 2.6 80 % 3.3 2.6 78 % 3 % .40-140%• 25% 646-31-1 n-Tetracosane(C24)- 3.3 2.5 76 % 3.3 2.5 74 % 2 % 40-140% 25% 630-01-3 n-Hexacosane(C26) 3.3 1 2.5 75 % 3.3 2.4 74 % 2 % 40-140% 25% 630-024 n-Octacosane(C28) 3.3 2.3 70 % 3.3 2.3 70 % 1 % 40-140% 25% 638-68-6 n-Triacontane(C30) 3.3 2.2 68 % 3.3 2.2 67 % 0 % 40-140% 25% 630-06-8 n-Hexatriacontane(C36) 3.3 1.8 55 % 3.3 1.8 55 % 0 % 40-140% 25% n/a n-C19 to n-C36 Group 26 20 75 % 26 19 74 % 1 % 40-140% 25% 91-20-3 Naphthalene 3.3 2.3 70 % 3.3 2.1 64 % 8 % 40-140% 25% 91-57-6 2-Methyl naphthalene 3.3 2.5 74 % 3.3 1 2.3 1 69 % 8 % 40-140% 25% 208-96-8 Acenaphthylene 3.3 2.6 80 % 3.3 2.4 73 % 8 % 40-140% 25% 83-32-9 Acenaphthene 3.3 2.4 73 % 3.3 2.2 67 % 9 % 40-.140% 25%. 86-73-7 Fluorene 3.3 2.5 76 % 3.3 2.3 70 % 9 % 40-140% 25%° 85-01-8 Phenanthrene 3.3 1 2.9 89 % 3.3 2.8 84 % 6 % 40-140% 25`/6 120-12-7 Anthracene 3.3 3.0 91 % 3.3 2.9 87 % 5 % 40-140% 25%. 206-44-0 Fluoranthene 3.3 2.8 86 % 3.3 2.7 82 % 4 % 40-140% 25% 129-00-0 Pyrene 3.3 2.7 83 % 3.3 2.6 79 % 4 % 40-140% 25% 56-55-3 Benzo[a]anthracene 3.3 2.6 79 % 3.3 2.5 1 75 % 5 % 40-140% 25% 218-01-9 Chrysene 3.3 2.6 78 % 3.3 2.4 72 % 8 % 40-140% 25% 205-99-2 Benzo[b]fluoranthene 3.3 2.5 76 % 3.3 2.3 70 % 9 % 40-140% 25% 207-118-9 Benzo[k]fluoranthene 3.3 2.3 70 % 3.3 2.2 68 % 4 % 40-140% 25 50-32-8 Benzo[a]pyrene 3.3 2.3 71 % 3.3 2.2 66 % 7 % 40-140% 25% 193-39-5 Indeno[1,2,3-c,d]pyrene 3.3 2.3 71 % 3.3 2.2 66 % 7 % 40-140% 25% 53-70-3 Dibenzo[a,h]anth race ne 3.3 2.5 76 % 3.3 2.4 71 % 7 % 40-140% 25% 191-24-2 Benzo[g,h,i]perylene 3.3 2.3 71 % 3.3 2.2 66 % 7 % 40-140% 25% n/a PAH Group 56 43 77 % 56 41 72 % 7 % 40-140% 25% QC Surro afe Com ound � �S ikeddlMeasaiea r�R11'ecoue .S tked ueas°yea �Recove ay QC Ltmtts� . �$ .r. P _. r. P �a. .<e� rrys, ., 9 , �0.. .� . �1et ..., .. �. Fractionation: 2-Fluorobiphenyl 2.7 2.3 85 % 2.7 2.3 85�% 40-140% 2-Bromonaphthalene 2.7 2.3 85 % 2.7 2.3 85 % 40-140 Extraction: Chloro-octadecane 2.7 1.5 56 % 2.7 1.4 52 % 40-140 ortho-Terphenyl 2.7 2.3 85 % 2.7 2.1 78 % 40-140 1 sue" _ ° Fracttonatton B eakthr gAval.uation a .± Lt_mtts 91-20-3 Naphthalenes LCS 0 % LCSD 0 % 5% 91-57-6 2-Methyl naphthalene LCS 0 % LCSD 0 % 5% Method Reference: Method for the Determination of Extractable Petroleum Hydrocarbons,MA DEP(Revision 1.1,2004). Method modified by use of microwave accelerated solvent extraction technique. Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. The LCS and LCSD are prepared from separate source standards than those used for calibration. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality-Control Report _ _ - -- Method Blank Category: MA DEP EPH Instrument ID: GC-9 Agilent 6890 QC Batch ID: EP-2094-M Extracted: 07-13-05 08:00 Matrix: Soil Analyzed(AL): 07-13-05 23:41 Analyzed(AR): 07-14-05 00:25 Analyst: MM t , EPH Ranges ; Concersiiaton�, Note-` Units Re rt�gumt ^� n-C9 to n-C18 Aliphatic Hydrocarbons t BRL mg/Kg 30 n-C19 to n-C36 Aliphatic Hydrocarbons t BRL mg/Kg 30 n-C11 to n-C22 Aromatic Hydrocarbons t° BRL mg/Kg 30 Unadjusted n-C11 to n-C22 Aromatic Hydrocarbons t BRL mg/Kg 30 E% CAS Number Analyte 3 _ th � A14.6 CntrdtlOf� e,r 4 n O eS..E .n .. :UmtS 4 Reportmg Lama 91-20-3 Naphthalene BRL mg/Kg 0.50 91-57-6 2-Methyl naphthalene BRL mg/Kg 0.50 85-01-8 Phenanthrene BRL mg/Kg 0.50 83-32-9 Acenaphthene BRL mg/Kg 0.50 208-96-8 Acenaphthylene BRL mg/Kg 0.50 86-73-7 Fluorene BRL mg/Kg 0.50 120-12-7 Anthracene BRL mg/Kg 0.50 206-44-0 Fluoranthene BRL mg/Kg 0.50 129-00-0 Pyrene BRL mg/Kg 0.50 56-55-3 Benzo[a]anthracene BRL mg/Kg 0.50 218-01-9 Chrysene BRL mg/Kg 0.50 205-99-2 Benzo[b]fluoranthene BRL mg/Kg 0.50 207-08-9 Benzo[k]fluoranthene BRL mg/Kg 0.50 50-32-8 Benzo[a]pyrene BRL mg/Kg 0.50 193-39-5 Indeno[1,2,3-c,d]pyrene BRL mg/Kg 0.50 53-70-3 Dibenzo[a,h]anthracene BRL mg/Kg 0.50 191-24-2 1 Benzo[g,h,i]perylene BRL mg/Kg 0.50 -QC Surrogate Compound: � _ �, Sprkecl Mea§ured�� Recovery d ,� � Q rmrts�'µ ` Fractionation: 2-Fluorobiphenyl 2.7 2.3 87 % 40-140% 2-Bromonaphthalene 2.7 2.4 89 % 40-140% Extraction: Chloro-octadecane 2.7 1.8 66 % 40-140% ortho-Terphenyl 2.7 2.2 81 % 40-140% Method Reference: Method for the Determination of Extractable Petroleum Hydrocarbons,MA DEP(Revision 1.1,2004). Sample extraction performed by microwave accelerated solvent extraction technique. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. t Hydrocarbon range data excludes concentrations of any surrogate(s)and/or internal standards eluting in that range. 0 n-C11 to n-C22 Aromatic Hydrocarbons range data excludes the method target analyte concentrations. -Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL = Q ualit Control Re ort w - Yy P Laborator Control-Satnples LCS LCSD Category: EPA 8082 Instrument ID: GC-6 HP 5890 Instrument ID: GC-6 HP 5890 QC Batch ID: PB-2196-P Extracted: 07-14-05 09:00 Extracted: 07-14-05 09:00 Matrix: Soil Cleaned Up: 07-14-05.16:00 Cleaned Up: 07-14-05 16:00 Units: ug/Kg Analyzed: 07-15-05 22:53 Analyzed: 07-16-05 00:38 Analyst: CRL Analyst: CRL D �Cate "s a 1CAS Number }Analyte sp ked Measured Recoverysp3kea Measured 1 Recovery ,RPDg QC L�m�ts ybts[rCol �e2nd°Cb4 �tst�Gol 2ndgcolp .� �r„;,W 1ri Coly�2sd Col &t"9st Co1,;,, tend Cols+. st Cols„�2nd ColSpRie"` £� RpD 12674-11-2 Aroclor1016 330 290 290 1 88% 1 87% 330 270 280 81% 84% 9% 4% 40-140% Y30%H 11096-82-5 Aroclor1260 .ts330 340 350 102% 105% 330 360 370 108% 111% 6% 5% 40-140% 30% p 3 -`�. -3 �S''r£z�, ,�, ." _'s t �. QC SSrrogate�C�ompound � Sur`,rogate Recovery r Q CLmnts�n. Tetrachloro-m-xylene �13 11 10 82% 77% 13 9.4 8.9 70% 67% 30-150% Decachlorobiphenyl 13 13 14 98% 108% 13 1 14 15 104% 113% 30-150% Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Sample extraction performed by EPA Method 3545. Cleanup performed by EPA Method 3660E and EPA Method 3665A. Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL _ - - Quality.Control Report - - . - Method 1131 kW`-T _ Category: EPA Method 8082 Instrument ID: GC-6 HP 5890 QC Batch ID: PB-2196-P Extracted: 07-14-05 09:00 Matrix: Soil Cleaned Up: 07-14-05 16:00. Analyzed: 07-15-05 22:18 Analyst: CRL IA Number Analyte' Conceritratton N'ot s; "`, .,Units a Porti��� met 1 2 674-1 1-2 Aroclor 1016 BRIL 7 ug/Kg 80 1 1 1 04-28-2 Aroclor 1221 BRL ug/Kg 80 1 1 1 41-1 6-5 Aroclor 1232 BRL ug/Kg 80 53469-21-9 Aroclor 1242 BRL ug/Kg 80 12672-29-6 Aroclor 1248 BRL ug/Kg 80 11097-69-1 Aroclor 1254 BRL ug/Kg 80 11096-82-5 Aroclor 1260 BRL ug/Kg 80 37324-23-5 Aroclor 1262' BRL ug/Kg 80 1 1 1 00-1 4-4 Aroclor 1268 BRL ug/Kg 80 µQC Surrogate Compound ,.,„ r Sptked Measured ° Recoueryt & nQ_CLtmtts' A �. First Tetrachloro-m-xylene 13 10 78 30-150% Column Decachlorobiphenyl 13 13 100 % 30-150 Second Tetrachloro-m-xylene 13 9.9 74 % 30-150 Column Decachlorobiphenyl 13 15 109 % 30-150% Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Sample extraction performed by EPA Method 3545. Cleanup performed by EPA Method 3660E and EPA Method 3665A. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. t Non-target analyte. Result is based on a single mid-range calibration standard. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL r Quality.Control Report Laboratory Control Samples Category: Metals Matrix: Soil Units: mg/Kg Sample Type Method QC Batch ID Prep Method Prepared Analyzed Instrument ID Anal s LCS EPA 6010B MB-0652-SL EPA 3050B 07-09-05 11:25 07-11-05 15:02 ICP-1 PE 3000 EB LCS EPA 7471A MP-1814-SL EPA 7471A 07-08-05 09:00 07-08-05 14:14 CVAA-1 PE FIMS EB LCSD EPA 6010E MB-0652-SL EPA 3050E 07-09-05 11:25 07-11-05 15:05 ICP-1 PE 3000 EB LCSD EPA 7471A MP-1814-SL EPA 7471A 07-08-05 09:00 07-08-05 14:17 CVAA-1 PE FIMS EB �J 'f CAS_Number Analyte „ rs LCS F LCS Du hcate C L1m1ts Method o fi r r a Q x S eked Measured `rRecoue :s 1S eked Measured. Recove RPD `RP a q P v N i'� p ,5�5 „ 4 ps•f Y lU �, p.ld` ^g �3 7440-38-2 Arsenic 110 110 98% 110 110. 100% 1% 80-120% 30% EPA 60108 7440-43-9 Cadmium 110 110 102% 110 110 100% 1% 82-118% 30% EPA 6010E 744047-3 1 Chromium t 150 160 106% 150 160 105% 0% 79-121 % 30% EPA 6010E 7439-92-1 Lead 160 160 101% 160 160 102% 0% 80-120% 30% EPA 60106 7439-97-6 Mercury 8.4 6.7 80% 8.4 7.1 85% 3% 51-149% 1 30% EPA 7471A Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Method Blank Category: Metals Matrix: Soil Analysis Method QC Batch ID Prep Method Prepared Sample Volume Instrument ID Analyst EPA 6010E MB-0652-SB EPA 3050B 07-09-05 11:25 0.5 g ICP-1 PE 3000 EB EPA 7471A MP-1814-SB EPA 7471A 07-08-05 09:00 0.6 g CVAA-1 PE FIMS EB CAS Number Analyte � Concentration Notes€ 'Umts Reponingtlmlt+ EDFz Anal zetl Method : 7440-38-2 Arsenic BRL mg/Kg 1.0 1 07-11-05 14:58 EPA 6010E 4 7440-43-9 Cadmium BRL mg/Kg 0.50 1 07-11-05 14:58 EPA 6010E 7440-47-3 Chromium BRL mg/Kg 10 1 07-11-05 14:58 EPA 6010E 7439-92-1 Lead BRL mg/Kg 10 1 07-11-05 14:58 EPA 6010B 7439-97-6 Mercury BRL mg/Kg 0.033 1 07-08-05 14:14 EPA 7471A Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. DF Dilution Factor. - Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 . GROUNDWATER ANALYTICAL _ - Quality_C_ontrol Report _ Laboratory Control Samples = LCS LCSD Category: EPA Method 8260B TCL Instrument ID: MS-1 HP 5890 Instrument ID: MS-1 HP 5890 QC Batch ID: VM1-1604-SL Analyzed: 07-11-05 08:44 Analyzed: 07-11-05 09:19 Matrix: Soil Analyst: LMG Analyst: LMG Units: ug/Kg i CAS Numbers a Analyte � LCS a° .tLCSDuphcate sQC,L mtts $ Measured � Spi ked, Reco ery� Spiked Measured Recovery RPDike 3RPD_` s ,. ems 74-87-3 Chloromethane 50 55 109 % 50" 49 98 % 12 % 70-130% 25% 75-014 Vinyl Chloride 50 49 99 % 50 44 88 % 11 % 70-130.% 25 74-83-9 Bromometharie 50 Si 102 % 50 47 94 % 8 % 70-130% 25 75-00-3 Chloroethane 50 51 103 % 50 43 86 % 17 % 70-130% 25 75-35-4 1,1-Dichloroethene 50 42 84 % 50 42 83 % 0 % 70-130% 25 67-64-1 Acetone 100 82 82 % 100 77 77 % 6 % 70-130% 25 75-15-0 Carbon Disulfide 100 73 73 % 100 76 76 % 4 % 70-130% 25 75-09-2 Methylene Chloride 50 52 105 % 50 51 103 % 2 % 70-130% 25 156-60-5 trans-1,2-Dichloroethene 50 43 86 % 50 42 83 % 2 % 70-130% 25% 1634-04-4 Methyl tert-butyl Ether(MTBE) 50 47 93 % 50 46 92 % 2 % 70-130% 25 75-34-3 1,1-Dichloroethane 50 43 86 % 50 42 84 % 2 % 70-130% 25% 156-59-2 cis-1,2-Dichloroethene 50 46 92 % 50 44 89 % 4 % 70-130% 25% 78-93-3 2-Butanone(MEK) 100 88 88 % 100 1 91 91 % 3 % 70-130% 25% 67-66-3 Chloroform 50 41 82 % 50 40 80 % 2 % 70-130% 25% 71-55-6 1,1,1-Trichloroethane 50 36 72 % 50 39 77 % 8 % 70-130% 25% 56-23-5 Carbon Tetrachloride 50 37 73 % 50 36 72 % 3 % 70-130% 25 7143-2 Benzene 50 45 90 % 50 44 89 % 2 % 70-130% 25 107-06-2 1,2-Dichloroethane 50 40 81 % 50 40 80 % 0 % 70-130% 25% 79-01-6 Trichloroethene 50 41 83 % 50 40 80 % 2 % 70-130% 25 78-87-5 1,2-Dichloropropane 50 45 91 % 50 1 45 90 % 0 % 70-130% 25 75-27-4 Bromodichloromethane 50 43 86 % 50 43 85 % 0 % 70-130% 25% 10061-01-5 cis-1,3-Dichloropropene 50 46 92 % 50 45 91 % 2 % 70-130% 25 108-10-1 4-Methyl-2-Pentanone(MIBK) 100 87 1 87 % 100 85 85 % 2 % 70-130% 25 108-88-3 Toluene 50 44 88 % 50 44 88 % 0 % 70-130% 25 10061-02-6 trans-1,3-Dichloropropene 50 39 77 % 50 38 77 % 3 % 70-130% 25% 79-00-5 1,1,2-Trichloroethane 50 48 96 % 50 48 96 % 0 % 70-130% 25% 127-18-4 Tetrachloroethene 50 41 83 % 50 39 78 % 5 % 70-130% 25% 591-78-6 2-Hexanone 100 92 92 % 100 90 90 % 2 % 70-130% 25 12448-1 Dibromochloromethane 50 45 89 % 50 43 86 % 5 % 70-130% 25 108-90-7 Chlorobenzene 50 47 95 % 50 47 94 % 0 % 70.-130% 25% 100-414 Ethylbenzene 50 44 88 % 50 43 86 % 2 % 70-130% 25 108-38-3n0e-42-3 meta-Xylene and para-Xylene 100 93 93 % 100 91 91 % 2 % 70-130% 25% 95-47-6 ortho-Xylene 50 46 92 % 50 47 95 % 2 % 70-130% 25 100-42-5 Styrene 50 47 95 % 50 49 97 % 4 % 70-130% 25% 75-25-2 Bromoform 50 45 91 % 50 46 92 % 2 % 70-130% 25 79-34-5 1,1,2,2-Tetrachloroethane 50 44 89 % 50 47 94 % 7 % 70-130% 25% SutrOgate OmpounlSpiked MeasuredRecouery Spiked Measuretl�Recovery $�QC Ltmtts . ; _., DibromofIuoromethane 50 49 98 % 50 48 97 % 70-130 112-Dichloroethane-d4 50 56 112 % 50 51 101 % 70-130% Toluene-de 50 58 115 % 50 59 118 % 70-130% 4-Bromofluorobenzene 50 55 110 % 50 59 119 % 70-130 Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Sample preparation performed by EPA Method 5030B. Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Method Blank -- Category: EPA Method 8260B TCL Instrument ID: MS-1 HP 5890 QC Batch ID: VM1-1604-SB Analyzed: 07-11-05 09:54 Matrix: Soil Analyst: LMG CASN:umber 3>Analytex, Concentatlon Notes `Umtsx ' Reaortmgt�m�t -` 74-87-3 Chloromethane BRL ug/Kg 10 75-014 Vinyl Chloride BRL ug/Kg 10 74-83-9 Bromomethane BRL ug/Kg 10 75-00-3 Chloroethane BRL ug/Kg 10 75-35-4 1,1-Dichloroethene BRL ug/Kg 5 67-64-1 Acetone BRL ug/Kg 200 75-15-0 Carbon Disulfide BRL ug/Kg 50 75-09-2 Methylene Chloride BRL ug/Kg 50 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 5 1634-04-4 Methyl tert-butyl Ether(MTBE) BRL ug/Kg 5 75-34-3 1,1-Dichloroethane BRL ug/Kg 5 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 5 78-93-3 2-Butanone(MEK) BRL ug/Kg 50 67-66-3 Chloroform BRL ug/Kg 5 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 5 56-23-5 Carbon Tetrachloride BRL ug/Kg 5 71-43-2 Benzene BRL ug/Kg 5 107-06-2 1,2-Dichloroethane _ BRL ug/Kg 5 79-01-6 Trichloroethene BRL ug/Kg 5 78-87-5 1,2-Dichloropropane BRL ug/Kg 5 75-27-4 Bromodichloromethane BRL ug/Kg 5 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 5 108-10-1 4-Methyl-2-Pentanone(MIBK) BRL ug/Kg 50 108-88-3 Toluene BRL ug/Kg 5 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 5 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 5 127-18-4 Tetrachloroethene BRL ug/Kg 5 591-78-6 2-Hexanone BRL ug/Kg 50 124-48-1 Dibromochloromethane BRL ug/Kg 5 108-90-7 Chlorobenzene BRL ug/Kg 5 100-414 Ethylbenzene BRL ug/Kg 5 1 08-3 8-3/1 06 4 2-3 meta-Xylene and pars-Xylene BRL ug/Kg 5 95-47-6 ortho-Xylene BRL ug/Kg 5 100-42-5 Styrene BRL ug/Kg 5 75-25 2 Bromoform BRL ug/Kg 5 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 5 QG SurrogateCompound Sptked 'MeMCI" Recduery "gSz QC Limits k Dibromofluoromethane 50 50 99 % 70-130% 1,2-Dichloroethane-d4 50 47 95 % 70-130% Toluene-d8 .50 59 118 % 70-130% 4-Bromofluorobenzene 50 62 125 % 70-130% Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update III(1996). Sample preparation performed by EPA Method 5035A. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER --- -ANALY_TICAL -- - - _ xem--.:.ems,=��>__ .. . - ...._ - .._. -' — — _•. _—��_£—�,,._..�"* .�..... _ � —_ ---. `- - Certifications and Approvals - Groundwater Analytical maintains environmental laboratory certification in a variety of states. Copies of our current certificates may be obtained from our website: http://www.groundwateranalytical.com/quaIifications.htm rkC � xr a,gw CONNECTICUT;Qe rtment of Health Ser iees,�PH 0586" � � � � ;�h 5fr Categories: Potable Water,Wastewater,Solid Waste and Soil http://www.dph.state.ct.us/BRS/Environmental Lab/OutStateLabList.htm z t -'''a ' ` t =� F,°»..s `xi'�," `k' $k<� tiM zk 'y" %a3�,'rz:^9 .�i�r. ,kk FLORIDA, Departmenit,of Health', Bureau"of Laboratories,¢E87643 , XN `,, "'.'' `,..-"� Categories:SDWA,CWA, RCRA/CERCLA http://www.floridadep.orgliabs/qa/dohforms.htm Categories: Drinking Water and Wastewater http://www.state.me.us/dhs/eng/water/Compliance.htm 7 „_ �e tsu" ' `�t`"i�s �'u $,`a.¢"�. i^a MASSACHUSETTS, Department of Enurronmental Protection, M MA. D' �. , .N. . _ . ._ mr a Categories: Potable Water and Non-Potable Water http://www.state.ma.us/dep/bspt/wes/fiIes/certlabs.pdf fNEW HAMPSWIRE, Department�of�Env�ronmenta{Serv,�ces;�202703 �� ����, ,�;� �,,,�� ,� � �,� �;g` Categories: Drinking Water and Wastewater http://www.des.state.nh.us/asp/NHELAP/labsview.asp c x�xxrea y +° x�t .DeartentoHealth11754NEWYORK m } 0 ,.w.Ff :: " � �.. ,�" '?, - ..a+x„ S. .."<,.a'✓' 673tM5 .f. >., -.� _,.s.,.r",'. r.s.�.� ah.wxtw - .w., .sn .' e^- a �.u,ex:.:, �. Categories: Potable Water, Non-Potable Water and Solid Waste http://www.wadsworth.org/labceWelap/comm.html �, 2" ' ,,PENNSYLVANIA De artmernt of EnvironmentalxProtectiorr 68 6fi5 r ' .,3::''::...'s",':U �.2. Environmental Laboratory Registration (Non-drinking water and Non-wastewater) http://www.dep.state.pa.us/Labs/Registered/ c x�.s at .�'��ea yiv�,.�.,s� RHOD.E ISLAND, Departmen#of#Health;�54 �� x �` `k'i5, #` z e ,.' "°�." _ `'' :.. P rz—, Categories:Surface Water,Air,Wastewater, Potable Water;Sewage http://www.healthri.org/labs/labsCT—MA.htm :U S Department of Agriculture,Soil.Permit, S 53921" � �- ' ���� ; Foreign soil import permit F �, '^`�{�✓, ".m.�&" k&ew"S vut roes.a .z ti: cciz-:* tea, _ w..sk`tf uE� ..kc°C"\*gyp4..... IV IuERNT,Department ouironrnental onservati�pp.on Water Supply Dision � ,� � � I Category: Drinking Water http://www.vermontdrinkingwater.orglwsops/labtable.PDF Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 RECEIVE® JUL 2 7 2005 GROU DWATE Groundwater Analytical,Inc. P.O.Box 1 �4NALY TIlCAL Buzzards Main Street 200 Buzzards Bay,MA 02532 Telephone(508)759-4441 July 26, 2005 FAX(508)759-4475 www.groundwateranalytical.com Mr. David Bennett Bennett & O'Reilly, Inc. P.O. Box 1667 Brewster, MA 02631 LABORATORY REPORT AMENDMENT Project: Walker/BO05-4316 Lab I D: 85330 Received: 07-06-05 Dear Dave: Enclosed are the amended analytical results for the above referenced project. This letter authorizes the release of the analytical results, and should be considered a part of this report. This report contains a sample receipt_ report detailing the samples received, a project narrative indicating project changes and non-conformances, a quality control report, and a statement of our state certifications. The analytical results contained in this report meet all applicable NELAC standards, except as may be specifically noted, or described in the project narrative. This report may only be used or reproduced in its entirety. I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Should you have any questions concerning this report, please do not hesitate to contact me. Sincerely, Eric H.Je en Operatio s Man er EHJ/kal Enclosures GROUNDWATER ANALYTICAL Sample Receipt Report Project: Walker/BO05-4316 Delivery: GWA Courier Temperature: 3.2'C Client: Bennett&O'Reilly, Inc. Airbill: n/a Chain of Custody: Present Lab ID: 85330 Lab Receipt: 07-06-05 Custody Seal(s): n/a Lab'ID FieldlD"- t x Fw 85330-1 SW-N:3-8' Soil 7/6/05 10:30 MA DEP EPH with PAHs Con ID Container Vendor QC Lot Presery QC Lot I Prep Ship C644557 250mLGlass Proline BX16975 None n/a J n/a 1 06-24-05 " Lab;ID � > FieIdID � Matnx Sa 1eda� v�4Method ""� "Owl x 85330-2 SW-W:3-8' Soil 7/6/05 10:45 TPH by CC ASTM D3328-00 Mod Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644562 250mLClass Proline BX16975 None n/a n/a 06-24-05 fey.Lab°liB ,�' Feld lD, _ S�amP 85330-3 SW-E:3-8' Soil 7/6/05 10:30 TPH by CC ASTM D3328-00 Mod Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644564 250 mL Class Proline BX16975 None n/a n/a 06-24-05 85330-4 BOH(N):8.5-9.0' Soil 7/6/05 11:00 TPH by CC ASTM D3328-00 Mod Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644565 250 mL Glass Proline BX16975 None n/a n/a 06-24-05 Lab IDS Field ID '+ Matn k Sam led "tilettiod Notes " Y 85330-5 Contaminated Stockpile Soil 7/6/05 11:00 EPA 6010B/7471A 5 RCRA Metals EPA 8082 PCBs TPH by CC ASTM D3328-00 Mod EPA 9045C Corrosivity EPA 1010 Mod Ignitability EPA SW-846,Chp.7 Reactivity Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644566 250 mL Glass Proline BX16975 None n/a n/a 06-24-05 C609360 250 mL Glass n/a n/a None n/a n/a n/a "�. .1 ,yak" T.a ,:.» . Lab"I!t7 r yi Freld tD �� Marix ; SampledMethod � nx a � „ x ¢. r. 1_a .,, z,�� ,.Notesw 85330-6 Contaminated Stockpile Soil 7/6/05 11:00 EPA 8260E TCL Volatile Organics Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C589413 40 mL VOA Vial Proline BX15002 Methanol R4255S 12-06-04 n/a C562533 40 mL VOA Vial Proline BX15491 NaHSO4 R4159A 03-11-65 n/a C562585 40 mL VOA Vial Proline BX15491 NaHSO4 R-4159A 03-11-05 n/a C562519 40 mL VOA Vial Proline BX154911 NaHSO4 I R-4159A 03-11-05 n/a Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Data Certification Project: Walker/8005-4316 Lab ID: 85330 Client: Bennett&O'Reilly,Inc. Received: 07-06-05 16:50 s�a +�x'F § y MA DEP Compendium of=Analyttcal;Method x Project Location: n/a MA DEP RTN: n/a This Form-provides certifications for the following data set: EPA 8260B: 85330-06 EPA 8082: 85330-05 MA DEP EPH: 85330-01 EPA 60106: 85330-05 EPA 7470A/IA: 85330-05 Sample Matrices: Groundwater ( ) Soil/Sediment (X) Drinking Water ( ) Other ( ) MPSW846 � %p 8260B (X) 8151A ( ) 8330 ( ) 6010E (X) 7470A/1A (X) �r m0th"o0 Used r 8270C ( ) 8081A ( ) VPH ( ) 6020 ( ) 9012A2 ( ) w' nsspec f ed n Mn oEP 8082 (X) 8021 B ( ) EPH (X) 7000 S3 ( ) Other ( ) aComendwmofAnalytical ,1nt�R�ease�rl�ackingJumbr(RTNjfRWn�� v,�� �t�... � .� w , 2;SWfi846 Method 9012A(Equivalent[0 90�1�4)or�MA DEP Fhys}ofog}cally Available Cyanide(FACT Method '� (check allathat appl"y, 3S'`�Sw 846Method'7000Ser}es-GsE ind!utdual An affirmative response to questions A, B,C and D is required for"Presumptive Certainty"status. A. Were all samples received by the laboratory in a condition consistent with that described on the Chain-of-Custody documentation for the data set? Yes B. Were all QA/QC procedures required for the specified analytical method(s) included in this report followed, including the requirement to note and discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Yes C. Does the analytical data included in this report meet all the requirements for"Presumptive Certainty,"as described in Section 2.0 of the MA DEP document CAM VII A,Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data? Yes D. VPH and EPH methods only: Was the VPH or EPH method run without significant modifications,as specified in Section 11.3? Yes A response to questions E and F below is required for"Presumptive Certainty"status. E. Were all QC performance standards and recommendations for the specified methods achieved? No F.. Were results for all analyte-list compounds/elements for the specified method(s)reported? No All No answers are addressed in the attached Project Narrative. I,!the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is,to the best of my knowledge and belief,accurate and complete. Signature: Position: Operations Manager Printed Name: Eric H.je sen Date: 07-26-05 Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM Method D3328-00 (Modified) Hydrocarbon Fingerprint by GC/FID Field ID: SW-W:3-8' Matrix: Soil Project: Walker/BO05-4316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85330-02 QC Batch ID: HF-2276-M Sampled: 07-06-05 10:45 Instrument ID: GC-9 HP 6890 Received: 07-06-05 16:50 Sample Weight: 16 g Extracted: 07-20-05 09:00 Final Volume: 1 mL Analyzed: 07-26-05 02:31 Dilution Factor: 1 Analyst: MB %Solids: 94 No petroleum product was identified for this sample. Total Petroleum Hydrocarbons BRL mg/Kg 61 '.s,'QC Surrogate Compound � � 3 �� Spiked Measured�s�; Recovery},�,f,; t : �QC Limits: ortho-Terphenyl 2.7 1.9 71 % 60-140% Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM METHOD D3328-90 (Modified) Hydrocarbon Fingerprinting by GC/FID Lab ID: 85330-02 Hydrocarbons Laboratory 1.0 0.s 0.6 0.4 1 0.2 0.0 0 5 10 15 20 25 30 35 Retention Time (Minutes) GROUNDWATER ANALYTICAL ASTM Method D3328-00 (Modified) Hydrocarbon Fingerprint by GC/FID Field ID: SW-E:3-8' Matrix: Soil Project: Walker/BO05-4316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85330-03 QC Batch ID: HF-2276-M Sampled: 07-06-05 10:30 Instrument ID: GC-12 Agi lent 6890 Received: 07-06-05 16:50 Sample Weight: 16 g Extracted: 07-20-05 09:00 Final Volume: 1 mL Analyzed: 07-22-05 07:04_ Dilution Factor: 1 Analyst: MB %Solids: 94 fi s F 1, m ud6tdty elden �ftcat�o " ` a < ff No petroleum product was identified for this sample. , � � - Z A _, w 'y., ,_ Limit Total Petroleum Hydrocarbons BRL mg/Kg 61 C Surro ate C;om oufld' � 7 � Sprke] �Measured Rerovery�,..,r.�_ r. � _ �� QC<L�mrts_ -'�- P y n. m � 60-140% ... . ortho-Ter hen I 2.7 2.1 76 /o Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM METHOD D3328-00 (Modified) Hydrocarbon Fingerprinting by GC/FID Lab ID: 85330-03 Hydrocarbons Laboratory 1.0 0.a 0.6 0.a 0.2 0.0 0 5 10 15 20 25 30 35 Retention Time (Minutes) GROUNDWATER ANALYTICAL ASTM Method D3328-00 (Modified) Hydrocarbon Fingerprint by GC/FID Field ID: BOH(N):8.5-9.0' Matrix: Soil Project: Walker/BO05-4316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85330-04 QC Batch ID: HF-2276-M Sampled: 07-06-05 11:00 Instrument ID: GC-9 HP 6890 Received: 07-06-05 16:50 Sample Weight: 16 g Extracted: 07-20-05 09:00 Final Volume: 1 mL Analyzed: 07-26-05 04:05 Dilution Factor: 1 Analyst: MB %Solids: 86 1 f ' UalldtlVe IdentlflCdthOfii �+ • z No petroleum product was identified for this sample. r/�rldE � .� .-:,h" v, ��wC{OnentGatlOfls NQte53�z� JET,�nitS '$�',.q Reportin8, rf.. Total Petroleum Hydrocarbons BRL mg/Kg 66 M �, ?��-�ra�v� QCSurrogateCompoundM S Iked Measured ; ortho-Terphenyl 1 2.9 1 2.1 73 % 60-140% Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM METHOD D3328-90 (Modified) Hydrocarbon Fingerprinting by GC/FID Lab ID: 85330-04 Hydrocarbons Laboratory 1.0 0.s 0.s 0.a 0.2 0.0 0 5 10 15 20 25 30 35 Retention Time (Minutes) f GROUNDWATER ANALYTICAL Project Narrative Project: Walker/BO054316 Lab ID: 85330 Client: Bennett&O'Reilly, Inc. Received: 07-06-05 16:50 The following documentation discrepancies,and client changes or amendments were noted for this project: 1 . Sample 85330-05 was also analyzed for TPH by ASTM D3328-00 Modified, per Kara Risk,07-08-05. 2 . Samples 85330-02 through-04 for analysis by ASTM D3328-00-Mod.were taken off hold and analyzed,per Kara Risk. ,,� � r `B Method Modifica tions;No Conformances and,Observations The sample(s) in this project were analyzed by the references analytical method(s),and no method modifications, non-conformances or analytical issues were noted,except as indicated below: 1 . EPA 601013 Note: Samples 85330-05.Samples were analyzed for selected target analytes,as requested by client. 2 . EPA 8260B Non-conformance: Sample 85330-06. Sample had a surrogate recovery outside recommended limits due to matrix interference. Sample reanalysis confirms matrix interference. 3 . EPA 8260B Note:Samples 85330-06.Sample was analyzed for only selected target analytes,as requested by client. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 228 Main Street,P.0.Box 1200 _ __GROUNDWATER------- ----- ---- ----------- ._._.. _....Buzzards-ER -o2sa2---- --- —C�IAfN=OF�USTD!DY RECORD--_.-._. __._...---.._..-_ �4NALYTICAL Telephone(508)759-4441•FAX(508)7594475 www.groundwateranalytical.com AND WORK ORDER N� 107249 Project Name: Firm: `LVS TURNAROUND ANALYSIS REQUEST J STANDARD(10 Business Days) Volatiles semivolatil42ME Wont Project Number: Address: Netals r ayjapan�� Q ❑ PRIORITY(5 Business Days)OM5- L��J��O �S�aJ �(1 S� I ❑ RUSH(RAN- t G N�Sam ler Name: (lQc7 (Rush requires Rush Authorization Number) 'uF City/State/Zi000 oo/ ❑Please Email to: " Y wi I Please FAX to: 9)9l0-9(.Bl P o _ g Pr ect Mana f: Telephone: BILLING ° - - d ° a ff 1 $ o ? L��J g9lo- (oto3 ) ° o 0 0 0 ❑ ❑ z d N rff . U Purchase Order No.:F,Of1 -c{';Il INSTRUCTIONS:Use separate line for each container(except replicates). ❑ Third Party Billing: m - ¢ a e s o s o s ❑ G WA Quote: a z- " p o Sampling a m N s�" i o a 2 a Matrix Type Containers) Preservation R o 0 o a o o 0 0 0 0' o ❑ o ° �a E SAMPLEw " o g n 9 g a y e d ❑ m o IDENTIFICATION 3 3 - 3 _ s ,� a o o - - _ LABOR Ry NUMBER q� - b 9 s ❑ o e ° p g (Lab Use Only) IE o ¢¢�n n a w l R v A O e � 2 � E b ❑ ❑ n O c4 ❑oo ❑ ❑ c o0 ooca❑o 0 ono a0000 ❑ off � � � � _ 0 - ❑ ❑ ❑ ❑ u ❑ o r I t REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OB x. �{ - ' JECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program State Standard Project Specific QC NOTE:All samples submitted subject to Standard Terms and Conditions on reverse hereof. MA DEP MCP Data Enhancement Affirmation Deliverables Many regulatory programs and EPA methods require project Relinquished by Sampler: Date Time Received AYES ONO ❑CT kMCP GW-1/S-1 ❑PWS Form specific OC.Project specific QC includes Sample Duplicates, M Receipt Temperature: 0 MCP Data Certification Is required. Matrix Spikes,and/or Matrix Spike Duplicates.Laboratory QC is l AYES ®NO MCP Drinking Water Sa b Z rO 9 ❑ME ❑MCP GW-2/S.2 ❑MWRA not project specific unless prearranged.Project specific QC / Ell.°Remp—ux, .3 mple Required. samples are charged on a per sample basis.Each MS,MSD quished 2-6'o RBCO"Aen°�" MA ❑NY STARS ❑ R It Date Time Receiv Container Count: (Require collection Of contingent duplicate sample. ❑NH p Drinking Water and Sample Duplicate requires an additional sample aliquot. [,� 9 Trip blanks are also required.It VOA sample collected) ❑NY ❑Wastewater b� Signature: Protect Specific OC Required Selection of OC Sample Relinquis Dat Time Received by abo story: Shipping/Airbill t�1 ❑RI ❑Waste Disposal El Sample Duplicate z-!�0 1�r 4 AA oy\. ` ❑VT ❑Dredge Material ❑Matrix Spike Please use sample: f11 Number: ❑— ❑ ❑Matrix Spike Duplicate Method of Shipment:bt GWA Courier❑Express Mail❑Federal Express Custody Seal ❑UPS O Hand❑ Number: n uh. l 228 Main Street,RO.Box 1200 t GROUNDWATER Buzzards_Bay MA02532 -------- ------ - _. —CHAIN-OF-CUSTODY-RECORD---------- --- ------------ ----'' Telephone(508)759-4441.FAX(508)7594475 i ANALYTICAL www.groundwateranalytical.com AND WORK ORDER NP 108596 Project Name: Fi n V�/ I'1 � /1 TURNAROUND ANALYSIS REQUEST lJ STANDARD(10 Business Days) volaxles semlrolatll MBE vea.nm xaz. Project Number. Address: IEmamaee of Est.TPx Vol Wasta GtmeralClremitlry Other `� r o ❑ PRIORITY(5 Business Days) - lJ1 to 1 OD G( I ❑ RUSH(RAN s (Rush requires Rush Authorization Number) ❑ ❑❑❑ y3 ❑ ❑ 2` Sampler lName: City/State/Zip: Please Email to: .. a Ajoi— Please FAX to�75_pgrp•T[49 3` m J A Project Manager: Telephone: BILLING `" 0 - w o = / _ tea d a DQS-�F31(v 4 Purchase Order No.: W o � 0 0 ❑ Third Party Billing: INSTRUCTIONS:Use separate line for each container(except replicates). a _ V s ❑ a o e o c s e = ❑ GWAQuote: Sampling Matrix Type Contalner(s) Preservation R ° o 0 0 0 0 0 0 0 0 6 0 5 0 o S $ ° e ❑ SAMPLE LABORATORY m - a - e e o u o z o ❑ 0 9 IDENTIFICATION NUMBER a -_ - o`' m e ° F x ❑ p Q g �. c m (Lab Use o - 3 - _� e e e $ S E E S' a - E e m o a _ '� ❑ _ ❑ m _ ° ❑ - - ❑ n ❑ ❑ o ❑ ❑ ❑ ❑ 0 c ❑ o 7 « E In z REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program Project Specific QC NOTE:All samples submitted subject to Standard Terms and Conditions on reverse hereof. MA DEP MCP Data Enhancement Affirmation State Standard Deliverables Marry regulatory programs and EPA methods require project Rplyiquished by Sampler: Date Time Received specific QC.Project specific QC includes Sample Duplicates, by: Receipt Temperature: ESXNO MCP Data Certification is required. ❑cT MCP GW-1/S-1 ❑PWS Form Matrix Spikes,and/or Matrix Spike Duplicates.laboratory QC is f OYES (L�� o�❑Relrigerxt d s3 NO MCP Drinking Water Sampie Required. �❑M"E ❑MCP GW-2/S-2 ❑MWRA not project specific unless prearranged.Project specific__ ✓^ zsc ate,xroce psnA ❑NY STARS p samples are charged on a per sample basis.Each MS,MSD Relinquished by: Date Time Received by: Container Count: (Require coIlBCtion Of Contingent duplicate sample. ( and Sample Duplicate requires an additional sample aliquot. �d-SU Trip blanks are also raquhed.If VOAsample collected) ❑NH ❑Drinking Water 7 13-v Signature: ❑NY ❑Wastewater Project S equired Selection of OC Sample by: Date Time Received b Laborato Shi gSpecific OCR Relinquished P Y PPing/Airbill ❑RI ❑Waste Disposal p Sample Duplicate ❑Please use sampler Number: ❑VT ❑Dredge Material ❑Matrix Spike WIU& ❑— ❑ ❑Matrix Spike Duplicate Method of Shipmen: GWA Courier❑Express Mail❑Federal Ex es Custody Seal ❑UPS❑Hand p Number: V I I. GROUNDWATER ANALYTICAL Quality Assurance/Quality Control a rProgdm OYeraVleW 'a, t 7 �; n:• , Groundwater Analytical conducts an active Quality Assurance program to ensure the production of high quality, valid data. This program closely follows the guidance provided by Interim Guidelines and Specifications for Preparing Quality Assurance Project Plans, US EPA QAMS-005/80 (1980), and Test Methods for Evaluating Solid Waste, US EPA, SW-846, Update III (1996). Quality Control protocols include written Standard Operating Procedures (SOPS) developed for each analytical method. SOPs are derived from US EPA methodologies and other established references. Standards are prepared from commercially obtained reference materials of certified purity, and documented for traceability. Quality Assessment protocols for most organic analyses include a minimum of one laboratory control sample one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. All samples, standards, blanks, laboratory control samples, matrix spikes and sample duplicates are spiked with internal standards and surrogate compounds. All instrument sequences begin with an initial calibration verification standard and a blank; and excepting GC/MS sequences, all sequences close with a continuing calibration standard. GC/MS systems are tuned to appropriate ion abundance criteria daily, or for each 12 hour operating period, whichever is more frequent. Quality Assessment protocols for most inorganic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. Standard curves are derived from one reagent blank and four concentration levels. Curve validity is verified by standard recoveries within plus or minus ten percent of the curve. ,, x t + * B �eflnitlOnS " r b r 5�° ",*.»"' mf :3'aav� ^S§. 'x. Batches are used as the basic unit for Quality Assessment. A Batch is defined as twenty or fewer samples of the same matrix which are prepared together for the same analysis, using the same lots of reagents and the same techniques or manipulations, all within the same continuum of time, up to but not exceeding 24 hours. Laboratory Control Samples are used to assess the accuracy of the analytical method. A Laboratory Control Sample consists of reagent water or sodium sulfate spiked with a group of target analytes representative of the method analytes. Accuracy is defined as the degree of agreement of the measured value with the true or expected value. Percent Recoveries for the Laboratory Control Samples are calculated to assess accuracy. Method Blanks are used to assess the level of contamination present in the analytical system. Method Blanks consist of reagent water or an aliquot of sodium sulfate. Method Blanks are taken through all the appropriate steps of an analytical method. Sample data reported is not corrected for blank contamination. Surrogate Compounds are used to assess the effectiveness of an analytical method in dealing with each sample matrix. Surrogate Compounds are organic compounds which are similar to the target analytes of interest in chemical behavior, but which are not normally found in environmental samples. Percent Recoveries are calculated for each Surrogate Compound. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Laboratory Control Sample Category: ASTM D3328-00 Mod Hydrocarbon Fingerprint Instrument ID: GC-12 Agilent 6890 QC Batch ID: HF-2276-M Extracted: 07-20-05 09:00 Matrix: Soil Analyzed: 07-20-05 21:16 Units: mg/Kg Analyst: MB a t �Analytc_,, �p"�� � �, ,� �mm Pked� Measured�� Recovery- QC L�mtts � , Fuel Oil No.2 130, 100 77 % 60-140% �QC�Sur ogate Gompoun�d �.F,,q _ � a � � �Spiked Measur, Recavery� -'_`QC Etrtt�ts - ortho-Terphenyl 2.7 2.1 79 % 60-140% Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. r r Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Method Blank Category: ASTM D3328-00 Mod Hydrocarbon Fingerprint Instrument ID: GC-12 Agi lent 6890 QC Batch ID: HF-2276-M Extracted: 07-20-05 09:00 Matrix: Soil Analyzed: 07-20-05 20:28 Analyst: MB COnCentl%dtlOn '- NOteS; r,}` UmtS e '�Repoitngtrmit, Total Petroleum Hydrocarbons BRL mg/Kg 30 ` C Surro ate Com ound` nS "Me ed Skeil ` asur " Recove ` � CKllmlts „ " ortho-Terphenyl 2.7 1 1.9 73 % 60-t140% Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Certifications and Approvals Groundwater Analytical maintains environmental laboratory certification in a variety of states. Copies of our current certificates may be obtained from our website: http://www.groundwateranalytical.com/qualifications.htm Department of Health Services PH 0586R � xx' Categories: Potable Water,Wastewater,Solid Waste and Soil http://www.dph.state.ct.us/B RS/Envi ron mental_Lab/O utStateLabLi st.htm Iry FL®RI,DA,yDepa ent�f Healt ,P. areauofrLaoorres; E87643 ,, Categories:SDWA, CWA, RCRA/CERCLA http://www.floridadep.org/labs/qa/dohforms.htm r 'n a. a ' rr� "'t�� G;�,x"r%, .�" ��'Nr � - ,. 'i 'Yraar,;a•«. MAINE, ®apartment of Human Seraurces, M 1p03 Categories: Drinking Water and Wastewater http://www.state.me.us/dhs/englwater/Compliance.htm MASSAGFI3USETTSepartmentnui onrtental;Protection M-M NMI � � u Categories: Potable Water and Non-Potable Water http://www.state.ma.us/dep/bspt/wes/fiIes/Certiabs.pdf �'NEW�HAMPSHIRE;Department of Env�rron�ental'Seru�c`�s, 2©2�7�0�� �,,�"_� _ ,m Categories: Drinking Water and Wastewater http://www.des.state.nh.us/asp/NHELAP/Iabsview.asp mefNEW 0RK ea� h ' 11754 „ ... Categories: Potable Water, Non-Potable Water and Solid Waste http://www.wadsworth.org/labcealelap/comm.html "'^ �a t z�+ PENNSYLVANIA, Departrrient of Environmental Protection, 68 6615 `�� � � 2A&"a.a. :a Environmental Laboratory Registration(Non-drinking water and Non-wastewater) http://www.dep.state.pa.us/Labs/Registered/ ',4 a - `,sfr w.r�,.44t gene RHODE ISLAND, De artj pf'of p Categories:Surface Water,Air,Wastewater, Potable Water,Sewage http://www.healthri.org/labs/labsCT-MA.htm CIO °�' n' n°^�''k'r"�i'a� F } ' FU,SFepa�tment of�Agr�culture,Soil�Perm�t�s553921 � a � c:,ni'c r Za4lt ^'n Foreign soil import permit `VERMONT, Department0o�f�Environmenfal Conservation,Water Supply Division ' �, - Category: Drinking Water http://www.Vermontdrinkingwater.org/wsops/labtable.PDF Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 RECEIVED JU 2 8 2005 Groundwater Analytical, Inc. GROUNDWATER P.O.Box 1200 228 ANALYTICAL Buz Main Street Buzzards Bay,MA 02532 Telephone(508)759-4441 July 25, 2005 FAX(508)759-4475 www.groundwateranalytical.com Mr. David Bennett Bennett & O'Reilly, Inc. P.O. Box 1667 Brewster, MA 02631 LABORATORY REPORT Project: Walker/13005-4316 Lab ID: 85416 n Received: 07-08-05 Dear Dave: Enclosed are the analytical results for the above referenced project. The project was processed for Standard turnaround. This letter authorizes the release of the analytical results, and should be considered a part of this report. This report contains a sample receipt report detailing the samples received, a project narrative indicating project changes and non-conformances, a quality control report, and a statement of our state certitications. The analytical results contained in this report meet all applicable NELAC standards, except as may be specitically noted, or described in the project narrative. This report may only be used or reproduced in its entirety. I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the intormation, the material contained in this report.is, to the best of my knowledge and beliet, accurate and complete. Should you have any questions concerning this report, please do not hesitate to contact me. Sincerely, P Eric H sen Oprati ns M ana r EHJ/sm Enclosures GROUNDWATER ANALYTICAL Sample Receipt Report Project: Walker/BO05-4316 Delivery: GWA Courier Temperature: 3.0'C Client: Bennett&O'Reilly, Inc. Airbill: n/a Chain of Custody: Present Lab ID: 85416 Lab Receipt: 07-08-05 Custody Seal(s): n/a Lab ID �F�eld ID,�� t, Matnx- SamPled` Method ' s � iNotesr' p � . ws % J 85416-1 SW-S:3-8(3) Soil 7/7/05 10:30 TPH by GC ASTM D3328-00 Mod Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644560 250 mL Glass Proline BX16975 None n/a n/a 06-24-05 r1,Fie Id11Dz -, m s x r 85416-2 BOH(S):8-9'(3) Soil 7/7/05 10:30 TPH by GC ASTM D3328-00 Mod Con ID Container Vendor QC Lot Presery QC Lot Prep Ship C644558 250 mL Glass Proline BX16975 None n/a n/a 06.24-05 Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM Method D3328-00 (Modified) Hydrocarbon Fingerprint by GC/FID Field ID: SW-S:3-8(3) Matrix: Soil Project: Walker/13005-4316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85416-01 QC Batch ID: HF-2279-M Sampled: 07-07-05 10:30 Instrument ID: GC-12 Agilent 6890 Received: 07-08-05 17:55 Sample Weight: 15 g Extracted: 07-22-05 08:00 Final Volume: 1 mL Analyzed: 07-23-05 22:55 Dilution Factor: 1 Analyst: MB %Solids: 99 No petroleum product was identified for this sample. A�alyte� � " � IConcentra€onw wr ' �, Units RePorfw0�mi€ Total Petroleum Hydrocarbons BRL mg/Kg 60 "�QC Ate,-,mpound rSpikei, iMea§�ured„�;p :Rec'oyerj%� � �,�e hp, �y QC limits �x� , ortho-Terphenyl 2.7 2.2 81 % 60-140% a. Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM METHOD D3328-00 (Modified) Hydrocarbon Fingerprinting by GC/FID Lab ID: 85416-01 Hydrocarbons Laboratory 1.0 0.$ 0.6 0.4 0.2 0.0 0 5 10 15 20 25 30 35 Retention Time (Minutes) GROUNDWATER ANALYTICAL ASTM Method D3328-00 (Modified) Hydrocarbon Fingerprint by GC/FID Field ID: BOHN:8-9'(3) Matrix: Soil Project: Walker/BO05-4316 Container: 250 mL Glass Client: Bennett&O'Reilly,Inc. Preservation: Cool Laboratory ID: 85416-02 QC Batch ID: HF-2279-M Sampled: 07-07-05 10:30 Instrument ID: GC-12 Agilent 6890 Received: 07-08-05 17:55 Sample Weight: 15 g Extracted: 07-22-05 08:00 Final Volume: 1 mL Analyzed: 07-23-05 23:40 Dilution Factor: 1 Analyst: MB %Solids: 97 .. ¢, QualitatrveIdentiftcatron No petroleum product was identified for this sample. PoAnalyCe � � � ................... . t oncentratton Notes �f"mts RePorttngt�mt Total Petroleum Hydrocarbons BRL mg/Kg 61 QCSurrogate Com ound,d S tked r,,,ed��; Recovery, G Ltmrtsk` .,o a,�,. P �. g�.. P rr..„ ;, . ..ti ortho-Terphenyl 2.7 2.2 81 60-140% Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Results are reported on a dry weight basis. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. t Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ASTM METHOD D3328-00 (Modified) Hydrocarbon Fingerprinting by GC/FID Lab ID: 85416-02 Hydrocarbons Laboratory 1.0 0.a 0.6 0.a 0.2 0.0 0 5 10 15 20 25 30 35 Retention Time (Minutes) GROUNDWATER ANALYTICAL Project Narrative Project: Walker/8005-4316 Lab ID: 85416 Client: Bennett&O'Reilly, Inc. Received: 07-08-05 17:55 F c & �� ; A Docurnentat�on and�ClientCommur�ication, xeF , c . .tu ,.� ,e " The following documentation discrepancies,and client changes or amendments were noted for this project: 1 . No documentation discrepancies,changes,or amendments were noted. _ B Method Modrfrcations; NonCfoncendOs ma ervafionsl N, X�P The sample(s) in this project were analyzed by the references analytical method(s),and no method modifications, non-conformances or analytical issues were noted,except as indicated below: 1 . No method modifications, non-conformances or analytical issues were noted. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 /� x 228 Main Street,P.O.Box 1200 -GRC1U1V WA/CN— Bunards BaY,MA f12532- — - -GH'AIN-OF-6USTODY RECORD - --- ...........----------- ANALYTICAL Telephone(508)759-4441•FAX(508)759-4475 AND WORK ORDER N G 108595 www.groundwateranalytical.com Project Name: Firm: TURNAROUND ANALYSIS REQUEST C/ F valalilea Semholatlles P IerDNCBs Metals Peb.1— Har. General Chem) �(STANDARD(10 Business Days) y titradante Ell x al Waste chemistry inner Project Number: Aditss: l ❑ PRIORITY(5 Business Days) 4J�1/� �� t►11l11/1/J�JIIWO- ❑ RUSH(RAN- ) g `N `A o 51 � (Rush requires Rush Authorization Number) x 0 0000 e Sa ler Neale: C' I State Zip: J ( �- ❑Please Email N ' n 1 Please FAX to:: m Q o r-o' ct Manager- Telephone: BILLING _ N n a _ x 3 ❑ Y > e /� ? ❑ ❑ ❑ ❑ ❑ ❑ ❑ d c o N Qi O t t0.7�so urchase Order No.: 3(� o o ia ❑ Third Party Billing: m -_ o s _° o INSTRUCTIONS:Use separate line for each container(except replicates). ❑ GWAquote: _' = 0 8 o z e z o p g Matrix Type Containers a $ e o e ° d a $ ° o T e Sam IIn o ❑ o ❑ ❑ o o a a o 6 ° e o o a s ra g _ Yp ( ) Preservation R _ s = „ a SAMPLE a - _ _ LABORATORY W o = _ e o ❑ o z o IDENTIFICATION W - q - m = NUMBER „�" a a _ - ? a m 4 _ z o ❑ ° € F w 3 s (Lab Use Only) m _ pe s = ° o O c 3 o o E E E o o E w rw "'3r o S a m o ti m a' = r- LS Y" i a"i `�' S e a e o ,,�,°• 9 O❑❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑❑❑❑ ❑ ❑ ❑ ❑ ❑ O ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ Q3b SIJ�- :3 3 - F 4' . -': •_ - _ 17 7. -77 tw .. .. REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program Project Specific QC NOTE:All samples submitted subject to Standard Terms and Cc erse hereof. MA DEP MCP Data Enhancement Affirmation State Standard Deliverables Many regulatory programs and EPA methods require project I'quished by Sampler: Date Time eived by: ? eceipt Temperature: �/ specific QC.Project specific QC includes Sample Duplicates, 03 J96ES ONO MCP Data Certification IS required. ❑CT MCP GW-1/S-1 ❑PWS Form Matrix Spikes,and/or Matrix Spike Duplicates.Laboratory QC is ;� z c ❑ME /❑\MCP GW-2/S-2 ❑MWRA not project specific unless prearranged.Project specific QC OYES iTO MCP Drinking Water Sample Required. samples are charged on a per sample basis.Each MS,MSD Reli ished Date Time R v d by: 0 Container Count: (Require Collection of contin ent du lioate earfl I®. A ❑NY STARS ❑ and Sample Duplicate requires an additional sample aliquot. �, g p p ❑NH ❑Drinking Water rip T blanke�0, fired If VOAsample collected) p NY ❑Wastewater Project Specific OC Required Selection of OC Sample Frell ished D e Time R v Iabo ry: Shipping Ai bill Trip Signatu ❑RI ❑Waste Disposal ❑Sample Duplicate 0 Please use sample: Number: �zQ 5•' ❑VT ❑Dredge Material ❑Matrix Spike Meth of Shipment: WA Courier❑L;pvilss Mail❑Federal pr ss Custody Seal ❑_ ❑ ❑Matrix Spike Duplicate UPS❑Hand❑ Number: GROUNDWATER ANALYTICAL Quality Assurance/Quality Control t f *" r xnv''i^w, ,a- +•# cx x .a.*';."�'a0M, Pf06rdrTl�OVerV1eW t rQ' �ew 3�� ��r, .,.',xr: ,°Ftr x -y- :7• ?y4''1ko 1`x_. ,aY: r...�."#,':e'a�.C�:�', x _"w. ,zz" s,^`_"_ a &.3>t?ss`a ` ."g "'''a. `. s +} Groundwater Analytical conducts an active Quality Assurance program to ensure the production of high quality, valid data. This program closely follows the guidance provided by Interim Guidelines and Specifications for Preparing Quality Assurance Project Plans, US EPA QAMS-005/80 (1980), and Test Methods for Evaluating Solid Waste, US EPA, SW-846, Update III (1996). Quality Control protocols include written Standard Operating Procedures (SOPS) developed for each analytical method. SOPs are derived from US EPA methodologies and other established references. Standards are prepared from commercially obtained reference materials of certified purity, and documented for traceability. Quality Assessment protocols for most organic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. All samples, standards, blanks, laboratory control samples, matrix spikes and sample duplicates are spiked with internal standards and surrogate compounds. All instrument sequences begin with an initial calibration verification standard and a blank; and excepting GC/MS sequences, all sequences close with a continuing calibration standard. GC/MS systems are tuned to appropriate ion abundance criteria daily, or for each 1.2 hour operating period, whichever is more frequent. Quality Assessment protocols for most inorganic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. Standard curves are derived from one reagent blank and four concentration levels. Curve validity is verified by standard recoveries within plus or minus ten percent of the curve. cam:s t'na�. " Q r °;k ` " ",��, vrk4r�� .�fi"M�•'�= a �,{. wDefinitions ar : �re ��` 1wa { rcrc s` '' w't ..6_ h G .- ,. �,'NA.},.pus. _ _.:`"" Batches are used as the basic unit for Quality Assessment. A Batch is defined as twenty or fewer samples of the same matrix which are prepared together for the same analysis, using the same lots of reagents and the same techniques or manipulations, all within the same continuum of time, up to but not exceeding 24 hours. Laboratory Control Samples are used to assess the accuracy of the analytical method. A Laboratory Control Sample consists of reagent water or sodium sulfate spiked with a group of target analytes representative of the method analytes. Accuracy is defined as the degree of agreement of the measured value with the true or expected value. Percent Recoveries for the Laboratory Control Samples are calculated to assess accuracy. Method Blanks are used to assess the level of contamination present in the analytical system. Method Blanks consist of reagent water or an aliquot of sodium sulfate. Method Blanks are taken through all the appropriate steps of an analytical method. Sample data reported is not corrected for blank contamination. Surrogate Compounds are used to assess the effectiveness of an analytical method in dealing with each sample matrix. Surrogate Compounds are organic compounds which are similar to the target analytes of interest in chemical behavior, but which are not normally found in environmental samples. Percent Recoveries are calculated for each Surrogate Compound. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Laboratory Control Sample Category: ASTM D3328-00 Mod Hydrocarbon Fingerprint Instrument ID: GC-12 Agilent 6890 QC Batch ID: HF-2279-M Extracted: 07-22-05 08:00 Matrix: Soil Analyzed: 07-23-05 13:40 Units: mg/Kg Analyst: MB £Anatyte ' auSpiked *„ 'Mea'sured Recovery `QC Lmtts_" Fuel Oil No.2 130 1 110 85 % 60-140 QCzSurrogafe Compound}�� ,�,,,;�� � ���,,t Piked _,� �Measuredk�" � °[eco��err� ��QC Limtfs��, ortho-Terphenyl 2.7 2.3 88 % 60-140 Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Method Blank Category: ASTM D3328-00 Mod Hydrocarbon Fingerprint Instrument ID: GC-12 Agilent 6890 QC Batch ID: HF-2279-M Extracted: 07-22-05 08:00 Matrix: Soil Analyzed: 07-23-05 12:53 Analyst: MB .'.r�: ";,"e`. ,. ,�.a``«....� Concentrattons r< 4Nofes";`,tit` :� "Utltts purting+Etamif4 Total Petroleum Hydrocarbons BRL mg/Kg 30 , QC Surrogate op,mpound2"c0 ��. Spiked Measured � Recouer�y QCLtmits -,w ortho-Terphenyl 2.7 2.0 74 % 60'-140 % . Method Reference: Comparison of Waterborne Petroleum Oils by Gas Chromatography,Annual Book of ASTM Standards,Volume 11.02, American Society for Testing and Materials(2000). Method modified to quantify total petroleum hydrocarbons in the range n-C 9 through n-C 36. Results are quantified on the basis of a series of aromatic and aliphatic hydrocarbons,using 5-alpha-androstane as an internal standard. Sample extraction performed by microwave accelerated solvent technique. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample size and dilution. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Certifications and Approvals Groundwater Analytical maintains environmental laboratory certification in a variety of states. Y rY �' Copies of our current certificates may be obtained from our website: http://www.groundwateranalytical.com/qualifications.htm _ a :":' 2.w�r , .� �(s r: v s r„^i d «C A 5 2 CONyN,ECTICUPk'T, Depa, rtment of Health Ser:Vices RH 0586" �, � � r �„ Categories: Potable Water,Wastewater,Solid Waste and Soil http://www.dph.state.ct.us/BRS/Environmental Lab/OutStateLabList.htm FLORIDA, Departmentof Health, Boreauof Laboratories,FE87643� h Categories:SDWA,CWA, RCRA/CERCLA http://www.fIoridadep.org/labs/ga/doh forms.htm k l"r spa q; �» MAINS, Department of�Human Services, MA103 _ r M�� � Categories: Drinking Water and Wastewater http://www.state.me.us/dhs/eng/water/Compliance.htm MASSACHUSETTS, De'a`rtmentfof�Environrnental Protection, M MA 103, � ��� " Categories: Potable Water and Non-Potable Water http://www.state.ma.us/dep/bspt/wes/fi Ies/certI abs.pdf 7 s as as t v r a �c x 'INN EW& �HAMPSHIRE, Department ofEnvironmentalServices 202703 , a �� � � , 7 �7 `X 5TL�1 i F �a, Categories: Drinking Water and Wastewater http://www.des.state.nh.us/asp/NHELAP/Iabsview.asp =NEW PORK, Departme.nt of Health, �11754�, �r ~a v__"`'raa-ai+a:. ,:r. ,�s ` � b r .mr' 8 r gz ��,-.,. s... .__ �. �« ,� -rrnbF c w*`.r't+o.rt. re' i'Pn va.,e-. ^'.,�.,. 'o,- vvF,..., a....,..i +b.;:a, ;: +-tSlAa�.,se.Me n:. .t' _ W Categories: Potable Water, Non-Potable Water and Solid Waste http://www.wadsworth.org/labcert/elap/comm.html � '.' .�,'aa, tsr 4"' 's-ad�r r.vr�*.rnrn�rr'{�''���a a°�a'r�� k' �'.�Adxa a.ampau3','� h«r � P&'��^'� e � °�' r� � arj .�r„ro:�:✓: �,>PENNSYLVAN'IA De artment of Environmental Protection68 665�� � .,.»�-'c° r�.xX�".&� $+�?. ep�.'d++3`ra si,�r.�,Y4 l �:�:+. ,..,,+.;,:, ..+, ,� ,.. mi.t% ix'=* ,��4C w F�:��'.x._�'+.'" �`•'�s .._�i.�?" �z ^�7 ems..� r.���� Environmental Laboratory Registration(Non-drinking water and Non-wastewater) http://www.dep.state.pa.us/Labs/Registered/ i bt r rvg_y x?F,✓..r r� "� S'�rt � 'wri Px n,�.^�� ''� ad ' 3^'�d 1 -_8 ns b.,. �. Categories:Surface Water,Air,Wastewater, Potable Water,Sewage http://www.healthri.org/labs/iabsCT—MA.htm ,.: r"1a2n. t r x�rM : a =U S sDe artmentiof A nculture Sod Permit.� S 53921 Foreign soil import permit r ,'2w. -x �„hr 2".cYY"F+F.4�"d VERMONT, Department3of Environmenta[Conservgtion,4iNater Supply Divisipnl*wt Category: Drinking Water http://www.vermontdrinkingwater.org/wsops/labtable.PDF Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 APPENDIX E BENNETT A 09 REILLY, Inc. Engineering, Environmental & Surveying Services 1573 Main Street Sanitary 21E/Site Remediation Property Line PO Box 1667 Site Development Hydrogeologic Survey Subdivision Brewster,MA 02631 Waste Water Treatment Water Quality Monitoring Land Court 508-896-6630 Water Supply Licensed Site Professional Trial Court Witness 508-896-4687 Fax QUALITY ASSURANCE & QUALITY CONTROL PROGRAM Quality Assurance & Quality Control Program For Soil and Groundwater Sampling INTRODUCTION The Quality Assurance & Quality Control AQA/QC) Program outlines the purpose, policies, organization and operations to support sampling work conducted by BENNETT&O'REILLY,INC.., The procedures and protocal represented herein are consistent with the MA DEP "Standard References for Monitor Wells" [WSC-310-91], and the recommendations of a MA certified laboratory. Implementation of this program will help to ensure the validity of data used to provide professional engineering and environmental opinions to clients. The following definitions are used in the QA/QC Program: Quality Assurance refers to the concepts used in defining a system for verifying and maintaining a desired level of quality in a product or process. Quality Control is a specific,step-by-step description of how the Quality Assurance Program will be carried out. This QA/QC Program guides field sampling activities. Project specific QA/QC Programs are adopted when warranted. Modifications to the QA/QC Program may be made only after specific approval by the QA/QC Officer(Project Manager). 1 The specific objectives of the QA/QC Program are to: 1. specify the level of quality of each field procedure used in collecting samples; 2. identify deficiencies in field procedures which might affect the quality of data; and 3. require sufficient documentation to verify the credibility of the sampling methods employed. PROGRAM ORGANIZATION AND RESPONSIBILITY The Project Manager of BENNETT & O'REILLY, INC., is responsible for the quality of work -produced. The Project Manger directs the QA/QC Program to document the control of field efforts and resulting data. In this capacity,the Project Manager is expected to do the following: 1. prepare detailed QC Plans; 2. obtain analytical and sampling procedures reference materials; 3. ensure that all field test and measurement equipment is maintained and calibrated properly; 4. monitor quality assurance activities to ensure conformance with authorized policies, procedures, and sound practices,and recommend improvements as necessary, 5. ensure that all field sampling is conducted in accordance with guidelines contained herein, 6. oversee all field sampling efforts to detect conditions which might directly or indirectly jeopardize the utility of resulting analytical data, such as improper calibration of equipment or cross-contamination through improper storage of samples; 7. ensure that sample handling procedures are adequate for the sample types received; 8. inspect the quality of purchased sampling materials. 2 SAMPLE MANAGEMENT, COLLECTION,AND PREPARATION Introduction Sample management and stringent documentation are essential for successful quality assurance. The procedures in this section are designed to ensure collection of samples which truly represent the matrix being sampled by eliminating trace levels of contaminants from external sources. Sample Management The management of samples,up to the point of delivery to the laboratory for analysis, is under the supervision of the Project Manager,who shall ensure that samples are collected,labeled,preserved, stored, and transported according to the prescribed methods. If significant deviations from the sampling protocol occur,resulting in a suspected compromise of the sample integrity, all samples collected during the sampling effort prior to correction of the procedure will be discarded and fresh samples collected. Sample Collection Groundwater Monitoring wells will be sampled in accordance with the following sampling procedures: 1. Identify the well and record the well number on the groundwater sampling record an an Monitoring Well Sampling Log(attached). 2. Open the well cap and measure total organic volatile (TOV) concentrations at the wellhead with the use of a portable photoionization detector. Record levels detected. 3. Measure groundwater level to the nearest 0.01 foot from the top of the well casing using a water level indicator. Record water level on a Monitoring Well Sampling Log (attached). Water level indicators will be decontaminated between wells. 4. The volume of standing water in the well casing will be calculated and recorded on the Monitoring Well Sampling Log. At least three well volumes will be purged either by pump or disposable bailer. Newly installed monitoring wells will be developed by purging at least ten volumes. Purging of wells will be complete when either dissolved oxygen,pH, conductivity or temperature has stabilized relative to previous sampling rounds. Once the purging is complete,wells will be screened for each of the above parameters and recorded on the Sampling Log . 5. Samples will be collected using either a disposable bailers or pump. Samples will be transferred into appropriately sterilized/preserved containers, taking care to minimize agitation of the sample [Refer to attached "Recommended Sample Containers..." Groundwater Analytical]. 3 6. Sample containers will be properly labeled with tags provided by the laboratory. Samples will be logged in on a chain-of-custody form. 7. Samples taken for precipitate metal analysis will be acidified to a pH of less than 2.0 in the field. When sampling water for volatile compounds, care must be exercised to prevent loss of compound through evaporation, and to control susceptibility to outside contamination. Precautionary measures include: 1. avoiding engine exhaust,gasoline containers,degreasing solvents,solvent-laden rags and non-compatible decontamination agents; 2. sampling bottles will only be opened at the time of sampling and quickly closed after collecting the sample,preventing aeration of the sample with the atmosphere or any other gas; 3. slowly filling bottles to capacity with sample and securing cap without entraining air bubbles; 4. inverting the bottle while tapping lightly to check for air bubbles; 5. adding additional sample to eliminate air bubbles if present,repeating steps 3 and 4; 6. placing samples on ice(approximately VQ immediately after collection in a dark, dry location; 7. segregating samples with a secondary barrier such as zip-lock bags, etc.; and 8. analyzing sample as soon as possible within the specific holding times after collection. Pump tubing will be decontaminated as follows: l. Pump non-phosphate detergent solution through system for two minutes. 2. Pump clean hot tap water through system for two minutes or until clear,whichever is longer. 3. Pump analyte-free water through system for two minutes. 4. Seal tubing ends;wrap and label with date of cleaning. 4 Soils When collecting and screening soil samples, the procedures to be used are: 1. Prior to sampling surficial locations,surface vegetation,rocks,leaves,and debris will be cleared from the sample point to allow collection of a clean soil sample. If surficial soil samples are to be collected,a hand trowel or shovel and spatula will be used. The sampling equipment will be decontaminated as outlined below. 2. Boring samples will be collected via drilling rig-operated split spoon procedures. Soil samples collected from excavations or test pits will be collected directly with an auger (if necessary) from grade to approximately four feet below grade. Samples collected at deeper depths will be obtained directly from the bucket of the backhoe. A stainless steel spatula will be used to remove soil from the backhoe bucket for placement in the appropriate sample containers. 3. Soil samples collected for TOV screening will be placed in glass soil jars with aluminum foil placed under the screw cap. Samples will be allowed to warm to ambient temperature before screening or will be screened in a heated vehicle after warming. The jar will be shaken for fifteen seconds prior to warming and after warming to ensure proper headspace development. Total organic vapors will be measured via a portable photoionization detector (PID) and their concentration recorded either on a Geological Borehole Log or field log. 4. Soil samples will.be stored and shipped in appropriate sealed containers. 5. Sample containers will be marked to indicate sampling date, time, location, and depth. Samples will be logged in on chain-of-custody, forms(copy attached). 6. The stratigraphy of each soil boring and test pit excavation,and the construction of each monitoring well will be recorded by the on-site geologist on the appropriate Geologic Borehole Log or test pit field log(copies attached). When sampling soils for volatile compounds, care must be exercised to prevent loss of compound and to control susceptibility to outside contamination. Precautionary measures include: 1. avoiding engine exhaust,gasoline containers,degreasing solvents,solvent-laden rags and non-compatible decontamination agents; 2. opening sampling bottles only at the time of sampling and quickly closing after collecting the sample; 3. placing samples on ice(approximately 4° Q immediately after collection in a dark, dry location; 5 4. segregating samples with a secondary barrier such as zip-lock bags, etc.; and 5. analyzing sample as soon as possible within the specific holding times after collection. Soil sampling equipment (shovel, auger, etc.) will be decontaminated between each sampling location with a potable water rinse, alconox soap wash, and a final potable water rinse. Drilling and excavating apparatus (augers, rods, casing, core barrels, backhoe bucket, and other equipment coming in contact with the borehole or excavation)will be decontaminated between each boring and excavation via steam cleaning. If necessary,an alconox soap wash followed by a steam cleaning will be included. Sample Preservation To prevent or retard the degradation/modification of chemicals in samples during transit and storage, the samples will be refrigerated at or below 4° C in appropriately preserved containers. Samples will be delivered to the laboratory by courier or by overnight delivery service. DATA MANAGEMENT Logging of Samples The accountability of a sample begins when the sample is taken from its natural environment. Sample handling (chain-of-custody) records must be completed at the time of sampling. The following chain-of-custody procedure must be implemented by the Field Team Leader to assure sample integrity. 1. The samples are under custody of the Field Team Leader if: a.they are in his (or her)possession; b.they are in view after being in possession: c. they are locked up or sealed securely to prevent tampering; or, d. they are in a designated secure area. 2. The"original"of the sample handling form must accompany the samples at all times after collection. A copy of the sample handling form is kept by the Field Team Leader. 3. When samples are transferred in possession, the individuals relinquishing and receiving will sign, date, and note the time on the form. 6 The Sampling Handling Record will contain information to distinguish each sample from any other sample. This information will include: 1. the project for which sampling is being conducted; 2. the matrix being samples (air, groundwater, soil, etc.); 3. the sampling date and time; 4. field sample identification number and chain-of-custody identification number; 5. the number and type of containers and the type of preservative used(if any); and, 6. signature of the person performing the sampling. Each sample will be assigned a unique identification number,which will be marked on the sample container. The sample handling record will be forwarded to the laboratory with the samples. As a precaution against this record being lost or altered,the sampling personnelwill retain a copy of the sampling handling record documenting all information up until the first change of sample custody. This record will be filed by the Project Manager. Sample Identification Numbers Reporting of date to the data management system will require the assignment of a unique identification number to each sample collected(including quality control samples). A record will be maintained by the Project Manager to associate the field sample with the various identification numbers used to analyze the field sample. Specific sample identification procedures are developed for each field sampling effort by the Project Manager. FORM SAMPLES BENNETT & O'REILLY, Inc. MONITOR WELL SAMPLING LOG 1573 Main street,P.O. Box 1667 Brewster, MA 02631 Engineering and Environmental Services (508)896-6630 FAX(508)896-4687 CLIENT DATE(S) TIME: TIDE: LOCATION JOB NUMBER SAMPLER MEASURING POINT GROUND SURFACE OR T.O.C: T.O.C. Elev.of Total Standing Water Depth to Static Volume HNU Dissolved Well reference Depth Purged Water Table Conductivity Temperature Water Volume 9ed PI-101 pH Oxygen Comments: Number point of Well (feet) Height Elevation (gallons) (gallons) (ppni) (mg/L) (F) (feet) (feet) (feet) (feet) NOTES: 1573 Main Street,P.O.Box 1667 BENNETT & OREILLY, Inc. Brewster,MA 02631 Engineering and Environmental Services (508) 896-6630 MONITOR WELL SAMPLING LOG CLIENT DATE(S) LOCATION JOB # MEASURING POINT SAMPLER GROUNDSURFACE OR T.O.C. Well Elev. of Total Depth to Standing Water Static Volume . HNU Comments Number reference.- - Depth of Water Water Table. Volume Purged PI-101 point Well (Feet) Height Elevation (gallons); (gallons). (ppm): (feet) (feet) (feet) (feet) NOTES: 1573 Main Street,P.O. Box 1667 BENNETT & OREILLY, Inc. Brewster, MA 02631 Engineering and Environmental Services . (508) 896-6630 MONFFOR WELL SAMPLING LOG RESPIRATION ANALYSIS CLIENT DATE(S) LOCATION JOB# SAMPLER Well Total Approx. Standing Length of HNU Methane Oxygen Carbon Comments: Number Depth of Depth to Water screen PI-101 (%CH,) (%OZ) Dioxide Well Water Height above (ppm) (%CO,) (feet) (feet) (feet) SWL NOTES: BENNETT & O'REILLY, Inc. Sheet or 1573 Main Street 508-896-663.0 _ PO Box 1667 508-896-4687 Fax Brewster,MA 02631 Job Number: Date: Time: Test Hole Number: Job Name: Witness: Casing I. D.: Ground Elevation: Reference Elevation(TOC): Falling Head ❑ Rising Head ❑ Aquifer Saturation Thickness(If Confined): Depth of Boring(A): Well Screen Length(L): Length of Test Section(L): Depth.of Groundwater Table(H): Depth of Top of Test.Section.(B).: Type of Material in:Test.Zone Notes: TIME ELAPSED WATER ACTIVE 2r (sec.) TIME(sec.) h/Ho DEPTH(x) HEAD(h) H >B n STATIC A n� --i 2R l— h=H-X(falling head) or h=X-H (rising head) Ho=H-Xo(falling head) or Ho=Xo-H (rising head) Xo=X at t=0 A,B, H&L are defined above. JOD Nam : Location: Weather: Start Date: Witness: Pump & low Rate Location: TOC: Location: TOC: Location:. TOC ., NOTES: Time Time Depth to Water Static Water Lv. Draw Down Depth to Water Static Water Lv. Draw Dawn Depth to Water Static Wate(Lv. Draw Down pH/COnd.fTemp. (sec). 0 1 2 3 4 5 6 7 8 _ — 9 15 30 (sec.) 45 (min) 1 2 3 4 5 — 6 _ 7 8 9 10 20 30 40 — 50 60 70 80 90 100 190 280 370 460 550 640 4730 820 910 1000 BENNETT & O'REILLY, Inc. Sheet of 1573 Main Street 508-896-6630 PO Box 1667 508-896-4687 Fax Brewster,MA 02631 Sieve Analysis Data and Computation Sheet Job Number: Date: Job Name: Sample Number: Sample Collected By: Sample Tested By: Notes SIEVE WEIGHT PERCENT CUMULATIVE' PROJECT OPENING SIEVE RETAINED RETAINED PERCENT MANUAL MILLI- MESH IN GRAMS (Cumulative) FINER SPECIFICATION METERS (Cumulative) PASSED MESH SIEVE TOTAL Sample Weight Wet: Sample Weight Dry: Percent Moisture: Sample Weight Passed Through Sieves: BENNETT & O'"ILLY, Inc. Sheet of 1573 Main Street 508-896-6630 PO Box 1667 508-896-4687 Fax Brewster,MA 02631 Job Number: Date: Job Name: SAND GRAVEL SILT SAND Test Hole Number: E] Witness: Drilling Contractor: PEAT CLAY Sampling Method: GEOLOGIC BOREHOLE LOG Type qtnnfinrcl Pe 3etMtionWell Lithology/Sediment Blows per °fo of ithology Depth °f Depth Specification.&Remarks Description Sample 6"Drive Recovery . PID Response 5 (ppm) 10 15 20 25 swL: 30 35 40 45 50 BENNETT&UREILLY,Inc. Project Name: Sheet 1573 Main St.,P.O.Box 1667 Project Location: Boring No. Brewster,MA.02631 Project Number: Location Surface Elev. Groundwater Readings Casing Sampler Core Start Date Date Reading Type Finish Date 1 Size I.D. Driller 2 Hammer Wt. Inspector 3 Hamer Fall Sample Sampling Inches TOV SPT Well Depth type-No. Depth(ft) Pen Rec Blow Count 6" Reading N-Value Soil Description Installation 5-ft 10-ft 15-ft 20-ft Sand Cohesive Soils Granular Soils Sample Type NOTES: Gravel < 2 =very soft < 4 =very loose SS-split spoon Sand/Gravel 2-4 .=soft 5-10 =loose ST-shelby tube Silt/Sand 4-8 = medium stiff 11-30 =medium AF-aguer flights Top/Sub Soil 8-15 =stiff 30-50 dense RC-rock core Clay 15-30 =very stiff > 50 = very dens MA-Microliners Fill > 30 =Hard HA-Hand Auger BENNETT & O'REILLY Inc. REPORT NUMBER: 508-896-6630 1573 Main Street 508-896-4687 Fax PO Box 1667 Brewster,MA 02631 INSPECTORS DAILY RECORD OF WORK PROGRESS . Job Number: . Date: Job Name: Feature: Contractor: Type of Work: Weather Conditions: Temperature: Contractor's Work Force(Indicate classification,including Subcontractor personnel) Equipment in or idled(identify which) . Materials or equipment delivered,quantity or pay items placed Non-conforming materials or work,field problems,inspections of previously reported deficiencies Summary of construction activities 228 Main Street,P.O.Box CHAIN-OF-CUSTODY RECORD p 120o N_ 049825 GROUNDWATER Buzzards Bay,MA 02532 Telephone(508)759=4441 AND WORK ORDER ANALYTICAL FAX(508)759-4475 'roject Name: Firm: TURNAROUND ANALYSIS REQUEST Volaliles semlvalaOlas PesUHerblPCas Malale Pabal-am draserbsn Hat. General Chemistry Other ❑ STANDARD(10 Business Days) dredab e o d.TPH lv.I.TPH Waste 'roject Number: Address: ❑ PRIORITY(5 Business Days) e ❑ RUSH(RAN- ) F F3 (Rush requires Rush Authorization Number) ° ° ❑ ° "3 ° ° ,ampler Name: City/State/Zip: git Please FAX ❑ YES ❑ NO a it FAX Number: 3 t2 W e it 3roject Manager: Telephone: BILLING 0 a IQ 10 0 0 0 0 a Purchase Order No.: GWA Reference No.: e ❑ ' yg a � km1 9 �iq5 fill NSTRUCTIONS:Use separate line for each container(except replicates). ❑ ❑ ❑ ❑ ❑ ❑ ❑ ° ❑ ❑ a ❑ o _ r, ❑ Matrix Type Contalner(s) Preservation Flnerad „ ., e € s o ,ampling o o z ❑ 3 a 5 LABORATORY W o n 9 a ; s E o o SAMPLE o -aNUMBER ey m >1 d ° ° € IDENTIFICATION y o: c " a a y _ m (Lab Use Only) 2 g o e a a £ 0 0 0 w > a3 = E E o ES s e a o s m a m a 3 ❑❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ O ❑ ❑ ❑o ❑ 1' ❑ ❑ ❑ ❑ ❑ ❑ 0 0 o o 0 REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program Project Specific CC NOTE:All.samples submitted subject to Standard Terms and Conditions on reverse hereof. ❑Safe Drinking Water Act Many regulatory programs and EPA methods require project Relinquished by Sampler: Date Time Received by: Receipt Temperature: ❑MA DEP Form specific OC.Project specific OC Includes Sample Duplicates, ❑NPOES/Clean Water Act Matrix Spikes,and/or Matrix Spike Duplicates.Laboratory OC is Specify State: not project specific unless prearranged.Project specific OC pP 9 In/Alrbill ❑ Time RCRA/Haz.Waste Char. samples are charged on a per sample basis.For water samples, Relinquished by: Date me Received by: Shi ❑MA MCP(310 CMR 40) each MS,MSD and Sample Duplicate requires an additional Number: Reportable Concentrations sample aliquot. ❑RCGW-1 ❑RCS-1 Protect Specific❑C Required Selection of OC Sample Relinquished by: Date I Time Received by Laboratory: Custody Seall ❑RCGW 2 0 RCS-2 ❑Sample Duplicate O Selected by laboratory Cooler Serial Number: ❑MA Dredge Disposal ❑Matrix Spike ❑Please use sample: ❑NH❑RI❑CT❑ME Method of Shipment: ❑GWA Courier❑Express Mail ❑Federal Express Specify Category: 0 Matrix Spike Duplicate 0UPS 0 Hand ❑ �YIlIOT$'C$,G�BOR�TORl$S,!� - AM CERT.No-,Af-MA 063 449 R7Z 130 SAND16eff, .EGA 02563 50,6( 6460) 1-600-139-6460 LAB USE ONLY: FAX(-'W)6M-6446 WATER ANALYSIS REQUISITION: DATE: DATE RECEIVED: SAMPLE NO.: TIME: NO. COPIES: NEXT DAY SERVICE BY 5:00 PM ( $20.00 Surcharge ) PICK UP: MAIL: NAME: WATER LOCATION: PHONE: FAX: MAILING ADDRESS: SAMPLED BY: PAYMENT/AMT. RECEIVED: WELL SPECS.: BILL TO/AMT.: - - — Lab use only. ANALYSIS REQUESTED; WATER SAMPLE TYPE: FHA-HUDNA HETERO-TROPHIC PLATE COUNT COPPER NEW WELL COLIFORM BACTERIA LEAD EXISTING WELL PH ARSENIC TOWN WATER CONDUCTANCE SILICA _ IRRIGATION NITRATE-N ZINC FILTER/CONDITIONER NITRITE-N TDS MISCELLANEOUS SODIUM TANNINS NEW MAIN IRON SULFIDE TITLE 5 MANGANESE SILVER POOL SPA CHLORINE POTASSIUM RCRA 8 CALCIUM IOC's COLIFORM BACTERIA MAGNESIUM SEC. CONT. PSEUDOMONAS HARDNESS FLUORIDE HETEROTROPHIC PLATE COUNT ALKALINITY OTHER ANALYSIS REQUESTED: SULFATE FECAL COLIFORM CHLORIDE METHOD: DEP SAMPLES COLOR VOLATILE ORGANICS PWS/#: TURBIDITY METHOD: SAMPLE SITE: FREE CO2 METALS Cie. Sink) AMMONIA-N METHOD: SAMPLE LOCATION: ODOR (ie. KitchetJWell) INSTRUCTIONS: BACTERIA-Obtain sterile sample bottle. Remove strainer/aerator from faucet. Turn on cold water. Allow it to run (5)five minutes. Fill container. Do not touch the inside of the bottle or the cap with anything. POTABLE WATER SAMPLE- Follow instructions for bacteria. Sample size approximately 500 mis. LEAD- Cali lab for instructions. VOLATILE ORGANICS/METALS- Call lab for instructions. CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. Client: 449 Route 130 Address: Proj. No. Project Name: Sandwich, MA 02563 (508)888-6460/ 1-800-339-6460 Sampler: FAX (508)888-6446 Phone#: Signature: Fax#: Field No. Date Time.. Comp Grab Station Location Container Pres. Sample type Analysis Requested Relinquished: Date/Time Received: Reliquished: Date[Time Received: Relinquished: Date/Time Received: Relinquished: Date/rime Received: TECHNICAL REFERENCE RECOMMENDED 1PRESERVATION, ii HOLDING Volatile Organics by Gas Chromatography/Mass Spectrometry (GC/MS) Parameter Method Matrix Minimum Recommended Containers(s)2 Required Holding Qty,' Preservation Time' Cool to 4°C' Volatile EPA Aqueous 40mL 3 x 40mL VOA Vials12 HCl to pH<24 14 Days Organics 8260B Remove Chlorine' 1 x 40mL VOA Vial with Methanol Cool to 4°C' Volatile EPA and 3 x 40mL VOA Vials with Methanol and Soil 40mL 14 Days Organics 8260B Sodium Bisulfate and 1 unpreserved Sodium Bisulfate container for percent moisture Cool to 4°C' Wastewater 12 HCl to pH<24 Volatile EPA 624 Aqueous 40mL 3 x 40mL VOA Vials Remove 14 Days Organics Chlorine' Drinking Cool to 4°C' Water EPA Aqueous 40mL 3 x 40mL VOA Vials" HCl to pH<24 14 Days Volatile 524.2 Remove Organics Chlorine' Volatile Organics by Gas Chromatography(GC) Parameter Method Matrix Minimum Recommended Containers(s)2 Required Holding Qty,l Preservation Time' Cool to 4°C' Volatile EPA 12 HCl to pH<24 Organics 8021B Aqueous 40mL 3 x 40mL VOA Vials Remove 14 Days Chlorine' GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS,PRESERVATION, and HOLDING TIMES Volatile EPA 1 x 40mL VOA Vial with Methanol Cool to 4°C' . Organics 8021B Soil 40mL and 1 unpreserved container for Methanol 14 Days percent moisture Wastewater Cool to 4°C' Volatile EPA 601 Aqueous 40mL 3 x 40mL VOA Vials12 Remove 14 Days Organics Chlorine' Cool to 4°C' Wastewater 12 HCl to pH<24 Volatile EPA 602 Aqueous 40mL 3 x 40mL VOA Vials Remove 14 Days Organics Chlorine' Semivolatile Organics by Gas Chromatography/Mass Spectrometry (GC/MS) Parameter Method Matrix Minimum Recommended Containers(s)' Required Holding j Qty,l Preservation Time' Sem Cool to 4°C'ivolatile EPA 2 x 1L Amber Glass Bottle 9 Aqueous 1 L w/teflon liner" Remove 7 Days Organics 8270C Chlorine I Semivolatile EPA Soil 30g Glass Jar w/teflon liner17 Cool to 4°C' 14 Days10 Organics 8270C Wastewater Cool to 4°C3 Semivolatile EPA 625 Aqueous 1L 2 x 1L Amber Glass Bottle Remove 7 Days' w/teflon liner Organics Chlorine' GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS,PRESERVATION, and HOLDING Pesticides, PCBs and Herbicides by Gas Chromatography (GC) Parameter Method Matrix Minimum Recommended Required Holding Qty' Containers(s)2 Preservation Time' Organochlorine EPA 2 x 1L Amber Glass? o t 400 Pesticides 8081A Aqueous 1L Bottle w/teflon liner RemoveChlorine7 7 Days' Organochlorine EPA Soil 30g Glass Jar w/teflon Cool to 4°C' 14 Days1' Pesticides 8081A liner 17 2 x 1L Amber Glass ° 3 PCBs EPA 8082 Aqueous 11 Bottle w/teflon liner" Remove tChlorine' 7 Days' PCBs EPA 8082 Soil 30g Glass Jar w/teflon liner Cool to 4°C' 14 Days10 PCBs in Oil EPA 8082 Organic 5g 1 x 40mL VOA Vial None 14 Days10 Modified Liquid Cool to 4°C3 EDB and DBCP EPA 8011 Aqueous 40mL 3 x 40mL VOA HC1 to pH<21 14 Days Vials Remove Chlorine' EDB in Soil EPA 8011 Soil 30g 1 x 60mL Glass Jar Cool to 4°C3 14 Days Modified w/septum cap Chlorinated EPA 2 x 1L Amber Glass? Cool to 4°C3 9 Herbicides 8151A Aqueous 1L Bottle w/teflon liner Remove Chlorine' 7 Days Chlorinated EPA Soil 30g Glass Jar w/teflon Cool to 4°C3 14 Days10 Herbicides 8151A liner 17 GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS,PRESERVATION, and HOLDING TIMES Organophosphorus EPA 2 x 1L Amber Glass o t 400 Pesticides 8141A Aqueous 1L Bottle w/teflon liner Remove Chlorine' 7 Days' Organophosphorus EPA Soil 30g Glass Jar wheflon Cool to 4°C' 14 Days10 Pesticides 8141A liner 17 Wastewater 2 x 1L Amber Glass Cool to 4°C'Check Organochlorine EPA 608 Aqueous 1L Bottle w/teflon liner" pH;Adjust 5_96; 7 Days' Pesticides Remove Chlorine' 2 x 1L Amber Glass Cool to 4°C' Wastewater PCBs EPA 608 Aqueous 1L Bottle w/teflon liner" Remove Chlorine' 7 Days9 Wastewater 2 x 1L Amber Glass Cool to 4°C' 9 Chlorinated EPA 615 Aqueous 1L Bottle w/teflon liner" Remove Chlorine' 7 Days Herbicides Drinking Water EDB EPA 504 3 x 40mL VOA Cool to 4°C'Add 14 Days and DBCP ,1 Aqueous 40mL Y Vials" Sodium Thiosulfate26 2 x 1L Amber Glass HCl to pH<2a Drinking Water EPA 508.1 Aqueous 1L Bottle w/teflon liner" Cool to 4°C' 14 Dayszz Chlorinated Pesticides Remove Chlorine24 2 x 1L Amber Glass Cool to 4°C' Drinking Water EPA 515.1 Aqueous 1L Bottle w/teflon liner" ' 14 Da ys23 Herbicides Remove Chlorine Drinking Water 2 x 1L Amber Glass HCl to pH<21 Semivolatile Organics EPA 525.2 Aqueous 1L Bottle w/teflon liner" Cool to 4°C' 14 Days22 Remove Chlorine24 GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS, PRESERVATION, 1d HOLDING Monochloroacetic Drinking Water Acid Buffer at pH 3 Carbamate Pesticides EPA 531.1 Aqueous 60mL 2 x 60mL Glass Vial Cool to 4°C' 28 Days Remove Chlorine' 2 x 500mL Amber Cool to 4°C3 Drinking Water EPA 548.1 Aqueous 250mL Glass Bottle w/teflon Add Sodium 14 Days21 Endothall liner" Thiosulfate26 Cool to 4°C3 Drinking Water Diquat EPA 549.2 Aqueous 1L 2 x 1L Black Plastic Add Sodium 7 Days" and Paraquat Bottle Thiosulfate16 ` Add NH4C1 Drinking Water 3 x 40mL Amber Cool to 4°C3 28 Haloacetic Acids EPA 552.2 Aqueous 40mL . VOA Vials12 Add Sodium 14 Days (HAAs) Thiosulfate16 Petroleum Hydrocarbons by Gas Chromatography(GC) Parameter Method Matrix Minimum Recommended Required Holding Qty.l Containers(s)' Preservation Time' Hydrocarbon 2 x 1L Amber Glass Fingerprint ASTM Aqueous 1L Bottle w/teflon liner" Cool to 4°C3 H2SO4 7 Day? D3328-90 to pH<2 GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS, PRESERVATION, and 1 Hydrocarbon Fingerprint ASTM Glass Jar w/teflon D3328-90 Soil 30g liner" Cool to 4°C3 14 Days10 2 x 1L Amber Glass Cool to 4°C3 H2SO4 TPH by(GC/FID) Modified EPA 8100 Aqueous 1L Bottle w/teflon liner? to pH< 7 Days' TPH by(GC/FID) EPA 8100 Soil 30g Glass Jar w/teflon Cool to 4°C3 14 Days10 Modified liner 17 EPA 8100 2 x 1L Amber Glass? Cool to 4°C3 HZSO4 g API DRO Modified Aqueous 1L Bottle w/teflon liner to pH<213 7 Days API DRO EPA 8100 Soil 30g Glass Jar w/teflon Cool to 4°C3 14 Days10 Modified liner 17 API GRO EPA 8015 Aqueous 40mL 3 x 40mL�VOA Cool to 4°C34 14 Days Modified Vials HCl to pH<2 1 x 40mL VOA Vial EPA 8015 with Methanol and 1 Cool to 4°C3 API GRO Modified Soil 40mL unpreserved Methanol 14 Days container for percent moisture 2 x 1L Amber Glass CT ETPH CT ETPH Aqueous 1L Bottle w/teflon liner" Cool to 4°C3 7 Days' CT ETPH CT ETPH Soil 30g Glass Jar w/teflon Cool to 4°C3 14 Days10 liner GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS,PRESERVATION, and HOLDING TIME'S 2 x 1L Amber Glass Cool to 4°C'H SO ME DRO ME 4.1.25 Aqueous 1L Bottle w/teflon liner, to pH<2"z 4 7 Days' ME DRO ME 4.1.25 Soil 30g Glass Jar w/teflon Cool to 4°C' 14 Days10 liner ME GRO ME 4.2.17 Aqueous 40mL 3 x 40mL�VOA Cool to 4°C'4 14 Days Vials HCl to pH<2 1 x 40mL VOA Vial with Methanol and 1 Cool to 4°C' ME GRO ME 4.2.17 Soil 40mL unpreserved Methanol 14 Days container for percent moisture MA DEP VPH MA DEP Aqueous 40mL. 3 x 40mL�VOA Cool to 4°C'4 14 Days VPH 1998 Vials HCl to pH<2 1 x 40mL VOA Vial MA DEP with Methanol and 1 Cool to 4°C' MA DEP VPH VPH 1998 Soil 40ML unpreserved Methanol 28 Days container for percent moisture MA DEP 2 x 1L Amber Glass Cool to 4°C'H2SO4 ,o MA DEP EPH EPH 1998 Aqueous 1L Bottle w/teflon liner to pH<2" 14 Days MA DEP EPH MA DEP Soil 30g Glass Jar w/teflon Cool to 4°C3 7 Days' EPH 1998 liner GROUNDWATER ANALYTICAL RECOMMENDED 1PRESERVATION, 1 1 Hazardous Waste Characterization Analyses Parameter Method Matrix' Minimum Recommended Required Holding Qty' Containers(s)' Preservation Time' TCLP/SPLP Volatile EPA x 125mL Glass Vial b o s �9 Organics 1311/1312 Solid18 150g w/teflon septum cap Cool to 4 C 14 Days EPA 8260B EPA TCLP/SPLP Metals, 1311/ 1312 Semivolatiles, EPA 18 300g Glass Jar w/teflon Cool to 4 o ' 28 Days19 Pesticides and 6010B/7470A Solid liner" C 14 Days19 Herbicides EPA 8270C EPA 8081A EPA 8151A Ignitability EPA 1010 Solid 50g Glass or Plastic Jar None None Modified Corrosivity(as pH) EPA 9045C Solid 50g Glass or Plastic Jar Cool to 4°C' None Reactivity SW-846 Solid 50g Glass or Plastic Jar Cool to 4°C' None Free Liquids EPA 9095 Solid 100g Glass or Plastic Jar None None GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS PRESERVATION, and HOLDING TIMES Metals by ICP, GFAA and CVAA Parameter Method Matrix Minimum Recommended Required Holding Qty.' Containers(s)2 Preservation Time' Total Metals(except EPA 6010B Aqueous. 100mL Plastic Bottle HNO,to pH<2 180 Days Mercury) Dissolved Metals Filter First"HNO to (except Mercury) EPA 6010B Aqueous 100mL Plastic Bottle pH<2 s 180 Days Total Metals(except EPA 6010B Soil 15g Glass or Plastic Cool to 4°C3 180 Days Mercury) Bottle Total Mercury EPA 7470A Aqueous 100mL Plastic Bottle HNO,to pH<2 28 Days Dissolved Mercury EPA 7470A Aqueous 100mL Plastic Bottle Filter pH<2 to 28 Days Total Mercury EPA 7471A Soil 15g Glass or Plastic Cool to 4°C3 28 Days Bottle Wastewater and Drinking Water Total EPA 200.7 Aqueous 100mL Plastic Bottle HNO,to pH<2 180 Days Metals(except Mercury) D GROUNDWATER ANALYTICAL RECOMMENDED 1PRESERVATION, 1 1 Wastewater Dissolved Filter First"HNO3 to Metals(except EPA 200.7 Aqueous 100mL Plastic Bottle pH<2 180 Days Mercury) Wastewater and Drinking Water Total EPA 245.1 Aqueous 100mL Plastic Bottle HNO3 to pH<2 28 Days Mercury Wastewater Dissolved EPA 245.1 Aqueous 100mL Plastic Bottle Filter First"p <HNO3 to 28 Days Mercury Colorimetric Methods for Metals Speciation Parameter Method Matrix Minimum Recommended Required Holding Qty.l Containers(s)' Preservation Time' Chronu' SM 3500- Hexavalen Cr D EPA Aqueous 100ML Plastic Bottle Cool to 4°C3 24 Hours 7196A Chromium, EPA Glass or Plastic Hexavalent 7196A Soil 15g Bottle Cool to 4°C3 30 Days Iron,Ferrous SM 3500- Analyze Fe D Aqueous 100ML Plastic Bottle None Immediately GROUNDWATER ANALYTICAL RECOMMENDED 1PRESERVATION, i 1 Inorganic Analyses Parameter Method Matrix Minimum Recommended Required Holding Qty.' Containers(s)Z Preservation Time8 Acidity SM 2310 B Aqueous 100mL Plastic or Glass Cool to 4°C3 14 Days Bottle Alkalinity SM 2320 B Aqueous 100mL Plastic or Glass Cool to 4°C3 14 Days EPA 310.2 Bottle BOD SM 5210 B Aqueous 1L Plastic or Glass Cool to 4°C 48 Hours Bottle CBOD SM 5210 B Aqueous 1L Plastic or Glass Cool to 4°C3 48 Hours Bottle EPA 325.2 Plastic or Glass Chloride EPA 300.0 Aqueous 50mL Bottle None 28 Days EPA 9251 Chlorine,Total SM 4500- Plastic or Glass None Analyze Residual Cl G Aqueous 200mL Bottle Immediately Chemical Oxygen SM 5220 D Aqueous 50mL Plastic or Glass H2SO4 to pH3 2 28 Days Bottle Cool to 4 C Demand(COD) SM 2120 B Plastic or Glass Color Aqueous SOmL Bottle Cool to 4°C3 48 Hours GROUNDWATER ANALYTICAL RECOMMENDED SAMPLEand 1 Cyanide,Amenable to Plastic or Glass Remove Sulfide14 Chlorination EPA 335.1 Aqueous 500mL Bottle NaOH to pH>12 14 Days Cool to 4°C3 EPA 335.3 EPA 335.4 Plastic or Glass Remove Sulfide"Cyanide,Total EPA Aqueous 500mL Bottle NaOH to pH 3 9012Al2 14 Days Cool to 4 C SM 4500-F Fluoride C EPA Aqueous 300mL Plastic Bottle Only None 28 Days 300.0 MBAS(Surfactants) SM 5540 C Aqueous 250mL Plastic or Glass Cool to 4°C3 48 Hours Bottle SM 4500- Plastic or Glass H2SO4 to pH<2 Nitrogen,Ammonia NH3 G Aqueous 4 OOmL Bottle Cool to 4°C3 28 Days SM 4500- Plastic or Glass Nitrogen,Nitrate NO3 F Aqueous 100ML Bottle Cool to 4°C3 48 Hours EPA 300.0 Nitrogen,Nitrate SM 4500- Plastic or Glass (Chlorinated Drinking NO3 F Aqueous 100mL Bottle Cool to 4°C3 14 Days Water) EPA 300.0 SM 4500- Plastic or Glass Nitrogen,Nitrite NO3 F Aqueous 100ML Bottle Cool to 4°C3 48 Hours EPA 300.0 Nitrogen,Nitrate plus SM 4500- Plastic or Glass H2SO4 to pH<2 Nitrate Aqueous 100ML ° 3 28 Days NO3 F Bottle Cool to 4 C GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS,PRESERVATION, and HOLDING Nitrogen,Total Plastic or Glass H2SO4 to pH s 2 28 Days Kjeldahl(TKN) EPA 351.2 Aqueous SOOmL Bottle Cool to 400 Odor SM 2150 B Aqueous 200mL Glass Bottle Only Cool to 4°C3 24 Hours Oil and Grease, SM 5520 B 1 x 11,Amber Glass? H2SO4 to pH<213 Gravimetric EPA 1664 Aqueous 11, Bottle w/teflon liner Cool to 4°C3 28 Days EPA 9070 Organic Carbon,Total SM 5310 B Plastic or Glass H2SO4 to pH s 2 28 Days (TOC) EPA 9060 Aqueous 25mL Bottle Cool to 4 C Oxygen,Dissolved M 4500-0 Aqueous 300mL Glass Bottle Only None Analyze G Immediately SM 4500- Plastic or Glass Analyze pH H+B EPA Aqueous 25mL Bottle None Immediately 9040B Petroleum SM 5520 1 x 1L Amber Glass? H2SO4 to pH<213 Hydrocarbons,Total CF Aqueous 1L Bottle w/teflon liner Cool to 4°C3 28 Days (TPH-IR) EPA 420.2 1 x 1L Amber Glass? H2SO4 to pH<2 °C3 28 Days Phenolics,Total EPA 9066 Aqueous 500mL Bottle w/teflon liner Cool to 4 SM 4500-P Filter(0.45 µm) Phosphate,Ortho F Aqueous SOmL Glass Bottle Only Cool to 4°C3 48 Hours SM 4500-P Plastic or Glass H2SO4 to pH<2 2g Days F Aqueous 50mL Bottle Cool to 4 C 3 Phosphorus,Total GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS,PRESERVATION, and HOLDING Phosphorus,Total SM 4500-P Plastic or Glass H2SO4 to pH<2 (Low-level 0.005 E Aqueous 50mL Bottle Cool to 4°C' 28 Days mg/L) Solids,Settleable(SS) SM 2540 F Aqueous 1L Plastic or Glass Cool to 4°C' 48 Hours Bottle Solids,Total(TS) SM 2540 B Aqueous 100ML Plastic or Glass Cool to 4°C' 7 Days Bottle Solids,Total SM 2540 C Aqueous 100ML Plastic or Glass Cool to 4°C' 7 Days Dissolved(TDS) Bottle Solids,Total SM 2540 D Aqueous 100mL Plastic or Glass Cool to 4°C 7 Days Suspended(TSS) Bottle Solids,Total Volatile SM 2540 E Aqueous 100ML Plastic or Glass Cool to 4°C' 7 Days (TVs) Bottle Solids,Volatile SM 2540 E Aqueous 100ML Plastic or Glass Cool to 4°C' 7 Days Suspended(VSS) Bottle EPA 2540 Plastic or Glass Solids,Volatile E Aqueous 100mL Bottle Cool to 4°C' 7 Days Dissolved(VDS) SM 2510B Plastic or Glass Specific Conductance EPA Aqueous 100mL Bottle Cool to 4°C' 28 Days 9050A SM 4500- Sulfate SO4 F EPA Aqueous 50mL Plastic or Glass Cool to 4°C' 28 Days 300.0 EPA Bottle I9056 f GROUNDWATER ANALYTICAL RECOMMENDED 1PRESERVATION, 1 1 SM 4500- Plastic or Glass NaOH to pH>9 Sulfide S2 D Aqueous 500mL Bottle 2mL Zinc Acetate 7 Days Cool to 4°C' Turbidity SM 2130 D Aqueous 100mL Plastic or Glass Cool to 4°C' 48 Hours Bottle Microbiological Analyses Parameter Method Matrix Minimum Recommended Required Holding Qty.' Containers(s)' Preservation Time' Wastewater Total SM 9222 B Cool to 4°C' Coliform(Membrane Aqueous 100ML Sterilized Bottle Remove Chlorine 6 Hours Filtration) Wastewater Fecal SM 9222 D Cool to 4°C' Coliform(Membrane Aqueous 100mL Sterilized Bottle Remove Chlorine' 6 Hours Filtration) Drinking Water Total SM 9222 B Cool to 4°C' Coliform(Membrane Aqueous 100mL Sterilized Bottle Remove Chlorine' 30 Hours Filtration) Drinking Water Total SM 9223 B Aqueous 100mL Sterilized Bottle Cool to 4°C' 30 Hours Remove Chlorine Coliform(Colilert) Drinking Water Fecal SM 9222 D Aqueous 100mL Sterilized Bottle Cool to 4°C' 30 Hours Coliform(Membrane q Remove Chlorine' Filtration) GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS, Drinking Water E. SM 9222 Aqueous 100111L Sterilized Bottle Cool to 4°C3 7 30 Hours Coli SM 9223 Remove Chlorine Heterotrophic Plate Cool to 4°C' Count(Standard Plate SM 9215 Aqueous 100mL Sterilized Bottle Remove.Chlorine' 30 Hours Count) Sampling Notes 1. The minimum quantity specified is the minimum amount of sample material necessary to perform the analysis.This quantity allows for no margin of error. For some analyses,Groundwater Analytical recommends specific types and numbers of containers(e.g.,an Aqueous Volatile Organic sample requires 3 x 40mL Glass Vials w/teflon septum caps).In such cases,the recommended container(s)allow for an adequate margin of error. For other analyses,Groundwater Analytical only recommends a general type of container(e.g.,a Solid Semivolatile Organic sample requires a Glass Jar w/teflon liner).In such cases,it is strongly recommended that twice the minimum quantity of sample material be collected in the recommended type of container. For solid samples,in addition to the minimum quantities required for individual analyses,each sample also requires 20g of sample material for a percent solids(or percent moisture)determination.Example:A soil sample collected for TPH-IR(30g),8 RCRA Metals(2.6g)and PCBs(30g)requires a minimum of 62.6g of material for the desired analyses,and 20g of material for percent solids(or percent moisture),for a total required minimum of 82.6g of material.It is then recommended that this minimum be doubled,and at least 165.2g of sample material be collected in a Glass Jar w/teflon liner. For solid samples,all minimum quantities are calculated net of all foreign objects,such as sticks,leaves and rocks. 2. Only sample containers pre-cleaned according to US EPA protocols are recommended.Appropriate pre- cleaned and pre-preserved containers are available from Groundwater Analytical.Pre-cleaned sample containers should not be pre-rinsed with sample prior to sample collection.Pre-rinsing may cause elevated results. 3. Samples should be immediately cooled,stored and shipped refrigerated.4°C(34T)is the recommended temperature for most analyses.Refrigeration retards biological degradation,reduces the volatility of compounds,retards the hydrolysis of non-aqueous compounds,reduces absorption effects and prevents continuing chemical reactions. 4. Adjust to pH<2 with Hydrochloric Acid(HC1).Acidification retards biological action,reduces absorption effects and prevents the formation of precipitates and/or complexes. Sulfuric Acid(HZSO4)or Sodium Bisulfate(NaHSOJ may be substituted for HCl in EPA Methods 8021B, 8011,and 8260B. GROUNDWATER ANALYTICAL 1 1 1CONTAINERS, PRESERVATION, i HOLDING 5. Adjust to a pH range of 4.0 to 5.0 with Hydrochloric Acid(HCI),Sulfuric Acid(H2SO4)or Sodium Hydroxide(NaOH). 6. If sample will not be received by laboratory within 24 hours of collection,then adjust to specified pH range with Sulfuric Acid(HZSO4)or Sodium Hydroxide(NaOH).The pH adjustment may be omitted if it is performed upon receipt at the laboratory within 24 hours,and may be omitted if the sample is extracted within 48 hours of collection. 7. If free chlorine is present in the sample,then Sodium Thiosulfate(Na2S203)should be added.Free chlorine can react with organic compounds to form chlorination by-products.Free chlorine is likely to be found in chlorinated municipal drinking waters and treated wastewaters. Sodium Thiosulfate,a reducing agent,is added to remove the free chlorine.For most levels of free chlorine,add 4 drops of 10%Sodium Thiosulfate to samples in 40mL vials,and add 5mL of 10%Sodium Thiosulfate to samples in 1L bottles. 8. The listed Holding Time is the maximum time a sample may be held between collection and initiation of analysis or extraction. 9. Samples must be extracted within 7 days of collection.Extracts must then be analyzed within 40 days of extraction. 10. Samples must be extracted within 14 days of collection.Extracts must then be analyzed within 40 days of extraction. 11. Samples for dissolved metals must be filtered prior to preservation with Nitric Acid(HNO3).Filtration must be done with a 0.45 micron membrane filter.Field filtration and preservation is preferred. However,if field filtration is not possible,samples should be cooled at 4°C and shipped to the laboratory for filtration and preservation.Filtration must be done as soon as practical after collection.Groundwater Analytical recommends that filtration be done within 24 hours of collection.If samples are not going to be field filtered,do not preserve samples with Nitric Acid(HNO3). 12. Aqueous samples samples for Volatile Organic Analyses(VOA)must be collected without any headspace or air bubbles.Volatile organics dissolved in water tend to volatilize readily and will fill any air bubble available in the vial.Particularly with low level samples,this results in a loss of material upon opening the vial.VOA vials must be filled slowly until the liquid forms a meniscus on the rim of the vial.The cap should then be gently placed on the vial,taking care not to disturb the crown of liquid,and firmly rotated tight.The vial should then be examined to verify the absence of all air bubbles. 13. Adjust to pH<2 with Sulfuric Acid(H2SO4).Alternatively,Hydrochloric Acid(HCI)may be used. 14. Maximum holding time is 24 hours when Sulfide is present. Samples may be tested with lead acetate paper before the pH adjustment in order to determine if Sulfide is present.If Sulfide is present,it can be removed by the addition of Cadmium Nitrate powder until a negative spot test is obtained.The sample is then filtered,and NaOH is added to adjust the pH>12. GROUNDWATER ANALYTICAL RECOMMENDED SAMPLE CONTAINERS,PRESERVATION, andHOLDING 15. Adjust to pH<2 with Nitric Acid(HNO,)or Sulfuric Acid(H2SO4).Acidification retards biological action, reduces absorption effects and prevents the formation of precipitates and/or complexes. 16. Samples should be collected with a minimum of aeration.The sample bottle should be filled completely, excluding all headspace,and capped. 17. Extractable organic samples are susceptible to Phthalate ester contamination.Phthalate ester contamination is generally caused by sample contact with a plastic material,particularly flexible plastics.Use care to avoid sample contact with any plastic,other than Teflon. 18. Specified quantities of sample material are for only single phase solid samples(i.e.no free liquids).Liquid phase or multiple phase samples require different quantities of sample material.Contact laboratory for advice prior to collecting liquid phase or multiple phase samples for TCLP analyses. 19. Samples for TCLP Volatile Organics analysis must be leached within 14 days of collection.The leachate must then be analyzed within 14 days of leaching. Samples for TCLP Metals analysis must be leached within 28 days of collection,if Mercury is being analyzed.The leachate must then be analyzed within 28 days of leaching.If Mercury is not being analyzed, then samples for TCLP Metals must be leached within 180 days of collection,and the leachate analyzed within 180 days of leaching. Samples for TCLP Semivolatile Organics,TCLP Pesticides,and TCLP Herbicides analyses must be leached within 14 days of collection.The leachate must then be extracted within 7 days of leaching.The extract must then be analyzed within 40 days of extraction. 20. Samples must be analyzed within 7 days of collection.However,if Heptachlor is not being determined, sample holding time to analysis may be extended to 14 days. 21. Samples must be extracted within 7 days of collection.Extracts must then be analyzed within 14 days of extraction. 22. Samples must be extracted within 14 days of collection.Extracts must then be analyzed within 30 days of extraction. 23. Samples must be extracted within 14 days of collection.Extracts must then be analyzed within 28 days of extraction. 24. Add 40-50mg of Sodium Sulfite to each liter of sample to reduce free chlorine that may be present.Free chlorine can react with organic compounds to form chlorination by-products.Free chlorine is likely to be found in chlorinated municipal drinking waters and treated wastewaters.Alternatively,use 40-50mg of Sodium Arsenite.Do not use Sodium Thiosulfate,as it may produce a residue of elemental sulfur which may interfere with the determination of some analytes. 25. Samples must be extracted within 7 days of collection.Extracts must then be analyzed within 30 days of extraction. GROUNDWATER ANALYTICAL RECOMMENDED PRESERVATION, and HOLDING 26. Add Sodium Thiosulfate to reduce free chlorine that may be present.Free chlorine can react with organic compounds to form chlorination by-products.Free chlorine is likely to be found in chlorinated municipal drinking waters.Use approximately 80mg of Sodium Thiosulfate per liter of sample. 27. Samples must be extracted within 7 days of collection.Extracts must then be analyzed within 21 days of extraction. 28. Samples must be extracted within 14 days of collection.Extracts must then be analyzed within 7 days of extraction GROUNDWATER ANALYTICAL COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL. PROTECTION STANDARD REFERENCES FOR MONITORING`WELLS SECTION 1.2 TABLE OF CONTENTS Section 1.2 Page i January 1991 •SECTION 1.2 TABLE OF CONTENTS 1.0 Introduction 1.1 Foreword 1.2 Table of Contents 1.3 Definitions 2.0 First Steps 2.1 Reconnaissance Surveys 2.2 Work and Cost Plans (Reserved) 2.3 Health and safety Plans 3.0 Subsurface Investigations 3.1 Exploratory Test Pits 3.2 Drilling Techniques 3.3 Borings in Contaminated Areas 3.4 In-Situ Sampling of Soil 3.5 soil Classification 3.6 In-situ sampling of Rock 3.7 Rock Classification 3.8 Laboratory Tests for soil 3.9 Plugging Boreholes 4.0 Piezometers, observation wells and Monitoring Wells 4.1 Monitoring Well Network Design 4.2 selection of well Construction Materials 4.3 Well Installation Procedures 4.4 As-built Notes and Records 4.5 Well Development 4.6 Decommissioning of Monitoring wells 5.0 Interpretation of Ground Water and Aquifer Characteristics 5.1 Water Level Measurements 5.2 In-situ Hydraulic conductivity Tests 5.3 Pumping Tests 5.4 Packer Tests 5.5 surveying and Datum Planes 6.0 sampling of Monitoring wells 6.1 , Quality Assurance/Quality control 6.2 Sampling Techniques 6.3 Sample Handling 6.4 Chain of Custody 6.5 Decontamination of Sampling Equipment section 1.2 Page ii January 1991 section 1.2 Table of Contents (continued) 7.0 Computer Models (Reserved) 8.0 Geophysical Techniques (Reserved) i Barnstable GROUNDWATER WELL GAUGING MA DATE:04tM5 Mffi:11:00 AM TIDE:N/A a WELL T.O.C. D.T.W. S.W.L. FLOW VECTOR W MW 1 30.06 8.52 21.54 S 160 W MW-2 29.23 6.05 21.18 (1960) MW-3 29.17 1 8.21 20.96 MW-4 29.OG 8.13 20.93h LOCUS DATE:07/06/05 TIlM:10:30 AM TIDE:N/A o O O N WELL T.O.C. D.T.W. S.W.L. FLOW VECTOR Ln O MW-1 30.06 9.22 20.84 S 40 E KEY MW-2 29.23 8.72 20.51 (176°) A MW-3 29.17 18.89 2028. LEGEND MW-4 29.06 8.80 20.26 �a�° � �TB Test Baring o� *HB Hand Boring p MW Monitor Well 0 0 Utility Pole ® Catch Basin &� � tioGs o� Aso Payed T13-1/MW-IA Parkiin,3 }j .Sty. Area O h/- n Q 0 > Bay Door \ 'IV � �0� _ AREA OF LIMITED ��s��o� Mio2, �`k�ad `' REMOVAL ACTION + �c, Bay Door t O'x 12' 8'-9'(D) �O� (COM�S E Ar OM, r RcIAL�/Norm O Approximate Location of �� + At) /1t �QO yO / � Hydraulic Lift / �..JJ HB-4 L A ° Approximate Location of } 0 OVERVIEW �y P�°��ao Stone \\` ��\ / NB 1 0 Reservoir Scale 1"=w F� te.� CO? ypy ' \ GpQ rprl` \\ ° HB-12 ° * / TB-2/MW--2A ;,9F Approximate Location of Floor Dram_.0 Stone *HB-6 SjO Bay Door T,P Cb% Approximate Location of Abandoned Holding Tank Paved -10 Driveway Stone Approximate Location of Former UST ATB-81MW-4 TB-3/MW-3Q DETAIL Project James Walker Scale 1^=10' c/o Lynette Walker,726 Falmouth Road,Hyannis,MA 02601 Title: LIMITED REMOVAL ACTION COMPLETION 143 Old Yarmouth Road,Barnstable(Hyannis),MA BENNETT & 01REILLY, INC. ENGINEERING,ENVIRONMENTAL,&SURVEYING SERVICES 1573 MAIN STREET,P.O.BOX 1667 BREWSTER,MA 02361 PHONE:(508)89&6630 FAX(%8)89646V DATE SCALE BY CHECK I JOB NUMBER DRAWWG:C\...\WnvironmentaNWalket'43 16E5A.d" 07/22/05 As Noted KMR/e DCB B005-4316 , ------------- _ -,GENERAL.CONSTRUCTION NOTES INLET D A B s EIASIN TO BE LOCATED OUTSIDE OF BUILDING y�• 4 '3-6'/ 3•-0 2`6*- rwHE E•POSSIBLE, COVER TO HAVE A CENTER HOLE. -. ,� 4'VENT TO ROOF ` _ 4-0• �A TiOHT`COVER MUST 8E USED IF BASIN F "R r �,' 3 6a3'6� 0. IS LOCATED INSIDE OF BUILDING. `` • 4' 0•/ 3 6 3 0! t� 4••da4.O• 3•-07 2.6. .OPENING SHALL BE NOT LESS THAN24•DIA. EXTRA HEAVY ,7— 'C.I INLET FROM >< THE CATCH BASIN SHALL BE SO LOCATED WASH,STAND _ ,_ LONG BENDC.I 6' 4 0/ 3' 0' 4 0 C T. TEE 4`•O a4'-O 4-0• 3 6 - AND CONSTRUCTED THAT SURFACE WATER SHALL OR —+ •N 4'•fi•/ 4•O� 3.6* - BE EXCLUDED. FLOOR DRAIN v-WATER LINE Z" —' .. - - 4' fia4'• 3'•6' 3'0* . INLET PIPE SMALL BE AT LEAST FOUR - / _.-_ _ OUTLET TO S 0� .3''6,`` 3`'0� INCHES ABOVE NORMAL WATER LINE. i SANITARY SEWEROxl_O' 3'O' 2-6 MIN 8 S D•'. 6 'O•, 5 0 WHERE SUBJECT TO FROST OR CRUSHING .•. -� •' ie CONDITIONS, OUTLET SHALL BE AT LEAST THREE ',� ..E .. EE•T.BELOW THE SURFACE. . . .:•._...... :�.•. _. _ _. 1.>+ .,> xTRA HEAVY C I PIPE S 6 x5�� 4 fi S•0 fi 0 a 6.0. O•. 2:6 r - - THE NEW CATCH BASIN MUST BE FILLED _ / -•- 6 6� 3�6'j' '3�D WROUGH B'POURED IN PLACE CONCRETE S' 50�10 fi`6 a6.6 3 t7 •[•6 ' WITH CLEAN.WATER BEFORE USING, AND AFTER z IRCN i tt € — 6, ' * CONCRETE BLOCKS,WITH FULL MORTARED . NOTE.:,.... - �- BEING EMPTIED FOR PERIODIC.CLEANING.` STEPS JOINTS, HORIZONTAL` AND VERTICAL, c •, E4 r PLASSERED INSIDE AND OUTSIDE; OR RED FOR INLETS LAROER T -N 6 .. r� BRICK MASONRY CE7P'a+T MORTAR IuSED SHALL : TH ALL OIL AND GASOLINE MUST BE REMOVED E OES13N ANO ^IMCNS CN %,L e BEFORE CLEANING OUT THE BASIN, AND MUST : - - / pETFRMInEp t=OR EACH Pl9T-.C_I,ap ,,..5_..� iI NOT BE DISCHARGED INTO THE SEWEk SHROWH ' - CONSIST OF I PART CEMENT, 2 PARTS SANG - ' - I OTHER•FIXTURES. jsORTIANO',m .CONCRE E CIRCULAR,BASINS ARE RECOMMENCED - .• -.. .. ..... ... ..tEMENT BRICK,..HOLLOW CONCRETE, OR - - i SPECIFICATIONS FOR COVERING SPECIAL CASES CINDER BLOCK MASONRY MUST NOT BE USED OR CONDITIONS;.SMALL BE APPROVED BY THE I ^ LOCAL AUTHORITIES, AND THE AUTHORITIES OfTHE COMMONWEALTH OF MASSACHUSETTS. WROUGHT IRON STEPS SHALL BE SPACED ABOUT 18' APART. - . ;: :•" - :.•t .. .. - •, - BOTH VENTS SHALL BE EXTENDED INpEPEN•� l [ THE COMMONWEALTH. OF.,MASSACHUSETT, DENTLY 118"ABOVE THE ROOF, OR AS APPROVED METROPOLITAN DISTRICT COMMISSION I - AUTHORITIES, AND THE AUTHOR- BY THE LOCAL i 1TIES OF THE COMMONWEALTH OF MASSACHUSETTS. APPROVED BY Lk.PJ-E�j-dyj SEwEPAGE PI VI SIGN (�j/Q�. �.,...: DIRECTOR OF SEWERAGE DI SIGN - .-.,,. _ AND•CHIEF SEWERAGE EN EER - ' -.APPROVED BY �/GuL _.. CINl� (T 1t F IRE fnHALL ,l _ _ n f � . .. i k ~ , I � • , d ` r J O v SE 1, �'- r s .E : S y''`!�r.4, '} f .. --.....-....,..._ - _._._ - .,...._.._ � / ---- ' ---•---.___�------------__.." a o -Y- t *•-•-�• . --- '--- --i•- _. , tc �g - - -- - - -- - - - r-------- �' p-. . Al. �----- m 4 i - - - - - - GXis'tip,.7 9r-ou.7d Pt:ofi14L HX /O ?"/ 0V/ -- M �/2 SG �'9 Ho L ram: / L/ � ,QT. S G.9t_ � / : /C� —o—o—o—o- �roPostal 9rouno� Pro,fi/�. , ar Y SC H E-0. 40 i' ✓ C. Ole f G EQUAL 70 .5EP71G e"irwrntJ/r7 �¢ ce- -TANK-t•• - _ __-�a..tJ ✓NF Q r �P c� PLC xo 3-7 _�yj I A 1 r - � ® 6t? 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