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HomeMy WebLinkAbout0450 SOUTH STREET - Health .450 South Stteeta-', Hyannis A- 3084E 122 e I "Expect the Best" Ogg, CHAM PO N Builders o Developers • Contractors O B U I L D E R S , I N C. (781) 826-3800 FAX: (781) 829-0000 www.championbuilders.com February 2, 2007 Thomas McKean, Director of Public Health Town of Barnstable, Public Health Division 200 Main Street , Hyannis, MA 02601 RE: 450 SOU TREET TH S -HYANNIS MA L` LIMITED REMOVAL Dear Mr. McKean: � Enclosed herewith please find a copy of the report prepared by Enviro- Safe Corporation for the above referenced location of 450 South Street in Hyannis. This location is the Law Office of John Manoog; and Enviro-Safe Corporation performed a limited removal action on a oil/water separator as outlined in the enclosed report. Their findings were that the site has been r remedied to levels that are well below any standards as necessary, as indicated in their Conclusions under Section 3.0. j Thank you for your attention to this matter; and if you have any questions, please do not hesitate to contact the Site Engineers at Enviro-Safe Corporation or myself. Since ly, an rat att ew J. Dacey ° President - MJD/pr —° Enclosure r° cc: Attorney John Manoog (w/Enclosure) Specializing in Affordable Single Family Custom Homes Corporate Park • 300 Oak Street • Suite 155 • Pembroke, Massachusetts 02359 Envlro-Safe Corporation. Environmental Services Field Service Center January 26,2007 Mr.Matthew J..Dacey Champion Builders, Inc. .300 Oak Street; Suite 155e Pembroke;MA 02359 1 RE: Limited Removal Action Report ' .450 South Street Hyannis,MA Job # 7513 ' Dear Mr.'Dacey: Enviro Safe Corporation (ESC) is submitting the following report to address the release - of petroleum located at°the 350 South Street Hyannis; Massachusetts (herein referred-to as "the Site"), This document provides a Limited Removal Action (LRA) Report ' summarizing actions conducted at`the site for the remediation of: etroleum impacted soil associated with the removal of the oil%water separator. Please refer to Figures 1 and 2:in. Attachment A for.a depiction,of the site.and surrounding area. + LO RELEASE.DESCRIPTION ' On December 1,2006, an ESC representative eollectedj samples for laboratory analysis as part of.a pre-characterization for the disposal of impacted soils related to. the removal of an. oil/water,separator. The laboratory 'analytical results revealed the presence of Total ' Petroleum Hydrocarbons in,the pre-characterization. soil sample at a concentration.in excess of the•applicable reporting>category.RCS-.1 standard. Based on these' release concentrations, .a condition requiring 2 hour or 72 hour notification to the Massachusetts'Department of Environmental Protection(MA DEP) did ` not exist, pursuant to 310 CMR*40.0361. However, it was assumed that the release would ' require notification to the:MA DEP within 120.days of the release date, pursuant to 310 CMR 40.0360 and310 CMR.4o.1600; 2.0 ASSESSMENT AND REMOVAL ACTIVITIES Based on the assessment data,collected on,January 11 2007, ESC recommended that'.a 1` `Limited Removal Action be conducted as the:'most direct means to achieve regulatory, closure.for. the impacted soil associated with the,historic operations of the oil/water. ' separator. An LRA is a removal action that is limited in size and scope in which' -notification to the MA DEP would not be required. Pursuant to 310 CMR 40.0000, the Massachusetts Contingency Plan (MCP), specifically 310 CMR 40.0318, the 31 .Granite Street Milford, MA 01757 PH ('508) 634 9800 FX (508) 634 8259 ' Limited Removal Action Report 450 South Street Hyannis,MA Page 2 of 3 ' requirements for co an LRA.are: q g • That conditions requiring either a 2 hour'notification or 72 hour notification to the' ' MA DEP are not present; Y • Response actions are completed within 1.20 days of obtaining knowledge of the 120 day release condition; ' • The release condition is limited to soil only;and • The removal action is limited,to less than 100 cubic yards for releases of petroleum hydrocarbons. The description of the assessment and remediation activities described below demonstrate that response actions were conducted within'the requirements for conducting a LRA and that notification to the MA DER is not required. t' 2.1 Assessment, Soil Sampling and Soil Removal Activities On January 12, 2007, ESC representatives supervised ,the removal of the oil/water separator and the excavation of'impacted soils! The structural integrity of the oil/water ' separator,_composed of brick and mortar, appeared to be in good condition and intact with an approximate depth of seven feet. - It should be noted that during excavation activities a concrete foundation and inactive underground conduits were within the ' footprint of the excavation. Please refer-to Attachment B for photo-documentation of the site excavation activities. During excavation.activities, personnel from ESC conducted field screening of soils for the presence of petroleum hydrocarbons using headspace.screening methodologies. A ' photoionization detector(PIO) was calibrated to read volatile organic compound (VOC) concentrations on a parts per million by volume (ppm' v) basis, benzene referred. The PID readings for in-situ samples ranged from 0.0ppmv to 3.5 ppmv. Personnel from ESC and Robert Childs Inc.,excavated impacted soil to a maximum depth of approximately twelve feet. The size of the completed excavation was approximately 20 feet by 15 feet, with a depth of approximately 12 feet. The size of the completed excavation is shown on Figure ESC transported impacted soil (approximately 36.83 tons) under a Bill-of-Lading (BOL) to Aggregate Industries in South Dennis, MA. Following soil removal activities in the release area, ESC collected two in-situ samples (ES and Bottom), and one composite soil sample (Comp SW). The composite soil sample was made up of multiple.aliquots collected from the north, west, and east. The ' PID Field Screening results'of each post excavation soil sample PID did not exhibit and VOCs above the instrument detection limit. The soil samples were kept cool and delivered by courier to Alpha Woods Hole Labs of Westborough, MA, for analysis of, extractable petroleum hydrocarbons (EPH) and volatile petroleum hydrocarbons (VPH) by MA DEP Method 04-1 and Method 04-1.1 respectively, RCRA 8 metals, volatile organic compounds by MA DEP Method 8260B, and/or PCBs by MA DEP Method 8082. Laboratory analysis indicated that the target petroleum analytes were non-detect and/or ' Limited Removal Action Report 450 South Street Hyannis,MA Page 3 of 3 ' detected at concentrations less than the reportable concentrations. The complete p p laboratory analytical report is included in Attachment C. 2.2 Remediation Waste Management As previously noted, approximately 36.83 tons of petroleum-impacted soil (as measured by the receiving facility) was transported to the Aggregate Industries facility under a Bill of Lading (BOL) on January 12, 2007. A complete copy of the BOL is included as ' Attachment D. 3.0 CONCLUSIONS Based on the results of completed LRA.activities, petroleum-impacted soil associated with the removal of the oil/water separator at the Site has been remediated to levels that iare well below the reportable RCS-1 soil standards within the 120 days required for the execution of a LRA. Accordingly, no further response actions are required in association with the.removal of the oil/water separator. Pursuant to 310 CMR 40.0318 (7)(b) the Responsible Party undertaking the Limited Removal Action shall retain this LRA document for a minimum of five years. If you have any questions regarding the information presented herein, please do not . hesitate to contact the undersigned at(508) 634-9800, Very truly yours, I ' Enviro-Safe Corporation Bridget Sullivan Michael C. Bricher, P.G., LSP Environmental Scientist Senior Environmental Engineer LIST OF ATTACHMENTS''-, Attachment A= Figure 1 Locus Plan , Figure 2 Site Plan ' Attachment B- Photo Documentation Attachment C- Laboratory Analytical Results Attachment D- Disposal Documentation and Pre-Characterization Laboratory Y 1 : Analytical Results APPENDIX A tw ppu4a,g� ` yy+�5 p'.'•�F Z s. e `R. yv't� a_ y �vielw„� 'ss = , ' g5[�' :. T' s y 3 St " r ' � �;!'�.. 76, E � FfE.,I+ '�.'SY- `�" �� � �c a t' � ;� •• � t . ,. g t� i .r� �. lr�' .} ���`�, e 'r. ..... •T'. _ h rsv, 'y ,v,,.'"x"J¢��• .w • ,,-� � 4. .3'�.� ��'{{� -�. �� �;._ ,�� C:: fit. � v _ '! .a ' �'� ,wS6 ?' .�e�l° .s^c �, f; s V;°^ R `f tij \• Pi.. ■ v ' Y �w•� � vi ti` � r��i+ .fs;*1c � �1 ��,^x. �A �� �r '':. _ s �� VFW an k g * h r B Orb n t � Q." 1W :; KatfnusLit ..t� FIGURE 1: USGS'Locus Man 1 450 South Street Hyannis, MA Excerpt from the USGS Topographic Map ' Hyannis, MA Quadrangle, 1979 Scale: 1 to 25,000 N01 ENVIRO-SAFE Corporation ' 31 Granite Street, Suite 8, Milford, MA 01757 Phone: (508) 634-9800 Fax: (508) 634-8259 \ In-Situ Sample Location 6-7, Sample Depths Residence \NJ #20 Sea Street — = Property Lies \ OWS Oil/Water Seperotor Former OWS BOH:11-a• Residence EV6-7:, #450 South Street W:6-7 Note: Lot lines generated from the Hyannis Assessors M.P. Field checked by ESC by tape survey. NI locations are Limits of Excavation approximate' ee. /h-w ome Enviro-Safe Corporation N 31 Granite Street, Suite 8 Milford, MA 01757 Phone: (5W) 634-9800 Far. (508) 634-8259 Figure 2: Site Plan Champion Builders ` v 450 South Street Hyannis. MA 7513 °` January 12, 2006 7O ax. 1 to 20 ' 01220714:11 4 � SY y F • ,aNO.O.DS�'H:�t6E'•4ABS 'ANALYTICAL REPORT t t 1 Lab Number: Client: -EnviroSafe 31 Granite Street ' Milford;MA 01757~: _..1 t . - ATTN: Mike Bricher ' Project Name: CHAMPION.BUILDERS Project Number: 7513 ' Report Date: " 01/22/07. ,.,Certifications&Approvals: MA(M-MA086),NY NELAC(11148),CT(PH-0574),NH(200305),NJ(MA935),RI(LA000065),ME(2006012). PA(kegistration*68-03671),USDA(Permit#S-72578),US Army Corps of Engineers,.Naval FESC. Eight WalkuDrive,Westborough, MA 01581-1019 9 P 9 � 50&898-9220 (Fax)508-898-9193 800-624-9220-www.alph6lab.com l� Page 1 of 55 �r 01220714:11 1 Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 1 1 Alpha Sample ID Client ID Sample Location 1 L0700683-01 ES HYANNIS, MA L0700683-02 BOTTOM HYANNIS, MA 1 L0700683-03 COMP SW HYANNIS, MA 1 1 1 1 1 1 1 1 1 i 1 1 /'rL1Lt�7 Page 2 of 55 ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number:. _0700683 Project Number: 7513 Report Date: 01/22/07 I MADEP•MCP.ResponseAction"Analytical.Report Certification This form provides certifications for all samples performedby MCP methods. Please refer to the Sample Re ' suits and Container Information sections of_this'fireport for specification of MCP methods used for each analysis:The in only.•to'MCP following�questions perta AnalyticalUetkiods. ' 'An affirmative response to questions A •B,'C' D is required.for."Presumptive Certainty"status A . Were all samples received by the laboratory in a condition consistent with those described on YES their Chain-of-Custodydocumentation for the data set? ' B Were all`QA/QC procedures required for the specifiedpanalytical methods(s) included in this YES report followed, including the requirement to note and discuss in a narrative QC data that did not meet appropriate erformance standards or guidelines. ' C 'Does the analytical data included in this report meet all the-requirements for"Presumptive YES Certainty", as described in section 2.0 of the'MADEP document CAM VII A, "Quality Assurance and Quali Control Guidelines for the A64uis.ition'and Ae*ortin of Analytical Data"? D VPH;and.EPH methods only: Was tkie VPH or EPH method run without significant moditications, YES ' ;.as specified in Section 11.3? A response to,questions,E and'F is required,for"Presumptive Certainty".status ' E Were all QC performance standards and recommendations for the specified P p method(s) NO achieved? F Were results for all analyte-list compounds/elements for the specified method(s)reported? NO tFor,an uestions;answered"No please`refer•to,thecase`narrative section on_the,following page(s): Please notethat sample"matrix_ information islocated in theSample'Results section of this report. Page 3 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' Case Narrative The samples were received in accordance with the chain of custody and no significant deviations were encountered during preparation or analysis unless otherwise noted below. MCP Related Narratives: ' Volatile Organics L0700683-01 and 02 were processed against a calibration curve that utilized a quadratic fit for vinyl chloride, ' 1,1-dichloroethene, methyl tert butyl ether, ethyl tert butyl ether, 2,2-dichloropropane, and tertiary-amyl- methyl-ether. In reference to question E: ' The WG268205-1,2 LCS,LCSD have high recoveries for Ethyl-Tert-Butyl-Ether,Tertiary-Amyl-Methyl- Ether, methyl tert butyl ether(in the LCSD). ' VPH L0700683-01,02 exceeded the recommended 1:1 methanol : soil ratio. Metals ' In reference to question F: At the client's request, all submitted samples were not analyzed for the full MCP list of compounds specified for ' the Method. I,the undersigned,attest under the pains and penalties of perjury that,to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained ' in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: Title: Technical Director Date: 01/22/07 ' Page 4 of 55 '''F"� 1 01220714:11 'is Fs" Ic I'MiG A-i 11-M., 1 1 1 1 1 . Page 5 of 55 1 , 01220714:11 ' VOLATILES Page 6 of 55 ' 01220714:11 Project Name:' CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 SAMPLE RESULTS. ' Lab ID: L0700683-01 Date Collected: 01/12/07 10:55 Client ID: ES Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified ' Matrix: Soil Anaytical Method: 60,8260B Analytical Date: 01/19/07 16:32 ' Analyst: RY Percent Solids: 96% Parameter `4111esult Qualifier Units RDL Dilution-Factor .. {(sCf�leS�.�`�G��X�-�T 4F3m8,���1�U•�' �7��"�'G ���""�a° "•`. '�+wa w4.G•*. �x'� � ` ,� � '- 'i c.°s•- 3 i Methylene chloride NO ug/kg 190 1 1,1-Dichloroethane No-, ug/kg 29 1 tChloroform ND ug/kg 29 1 Carbon tetrachloride ND ug/kg 19 1 1,2-Dichloropropane ND ug/kg 68 1 ' Dibromochloromethane ND_ ug/kg 19 1 1,1,2-Trichloroethane ND ug/kg 29 1 r Tetrachloroethene NO ug/kg 19 1 Chlorobenzene NO ug/kg 19 1 Tnchlorofluoromethane'' ND ug/kg 97 1 1,2-Dichloroethane NO ug/kg 19 1 ' 1,1,1-Trichloroethane ND` ug/kg 19 1 r Bromodichloromethane ND ug/kg 19 1 trans-1,3-Dichloropropene r NO ug/kg 19 1•. cis-1,3-Dichloropropene NO, ug/kg 19 1 1,1-Dichloropropene ND - ug/kg 97 1 Bromoform NO ug/kg 77 1 1,1,2,2-Tetrachloroethane NO ug/kg 19 1 Benzene ND ug/kg 19 1 ' Toluene NO ug/kg 29 1 Ethylbenzene RD ug/kg 19 1 Chloromethane NO ug/kg 97 1 ' Bromomethane No. ug/kg 39 1 Vinyl chloride NO ug/kg 39 1 'Chloroethane { NO ' ug/kg 39 1 ' 1,1-Dichloroethene NO ug/kg 19 1 r trans-1;2-Dichl0'roethane `.ND ug/kg 29 1 Tnchloroethene NO ug/kg 19 1 ' 1,2-Dichlorobenzene NO ug/kg 97 1 1,3-Dichlorobenzene ND ug/kg 97 1 I�A`' ' Page 7 of 55 01220714:11 Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project.Number: 7513 Report Date: 01/22/07 SAMPLE RESULTS Lab ID: L0700683-01 Date Collected: 01/12/07 10:55 Client ID: ES Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor 1,4-Dichlorobenzene NO ug/kg 97 1 Methyl tert butyl ether NO ug/kg 39 1 p/m-Xylene NO ug/kg 39 1 o-Xylene NO ug/kg 39 1 cis-1,2-Dichloroethene NO ug/kg 19 1 Dibromomethane NO ug/kg 190 1 1,2,3-Trichloropropane NO ug/kg 190 1 Styrene NO ug/kg 39 1 Dichlorodifluoromethane NO ug/kg 190 1 Acetone NO ug/kg 190 1 Carbon disulfide NO ug/kg 970 1 2-Butanone NO ug/kg 190 1 4-M ethyl-2-pentanone NO ug/kg 190 1 2-Hexanone NO ug/kg 190 1 Bromochloromethane NO ug/kg 97 1 Tetrahydrofuran NO ug/kg 390 1 2,2-Dichloropropane NO ug/kg 97 1 1,2-Dibromoethane NO ug/kg 77 1 1,3-Dichloropropane NO ug/kg 97 1 1,1,1,2-Tetrachloroethane NO ug/kg 19 1 Bromobenzene NO ug/kg 97 1 n-Butylbenzene NO ug/kg 19 1 sec-Butylbenzene NO ug/kg 19 1 tert-Butylbenzene NO ug/kg 97 1 o-Chlorotoluene NO ug/kg 97 1 p-Chlorotoluene NO ug/kg 97 1 1,2-Dibromo-3-chloropropane NO ug/kg 97 1 Hexachlorobutadiene NO ug/kg 97 1 lsopropylbenzene NO ug/kg 19 1 p-Isopropyltoluene NO ug/kg 19 1 Naphthalene NO ug/kg 97 1 n-Propylbenzene NO ug/kg 19 1 1,2,3-Tdchlorobenzene NO ug/kg 97 1 1,2,4-Tdchlorobenzene NO ug/kg 97 1 1,3,5-Trimethylbenzene NO ug/kg 97 1 1,2,4-Trimethylbenzene NO ug/kg 97 1 Ethyl ether NO ug/kg 97 Page 8 of 55 Project Name: CHAMPION BUILDERS 01220714:11 Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 SAMPLE RESULTS' -r ' Lab ID: L0700683-01 Date Collected: 01/12/07 10:55 Client ID: ES Date Received: 01/15/07 Sample Location: HYANNIS,MA Field Prep: Not Specified ' Parameter Result Qualifier Units RDL Dilution Factor ' Isopropyl Ether rr ND ug/kg 77 1 Ethyl-Tert-Butyl-Ether ND ug/kg 77 1 Teruary-Amyl Methyl Ether ND ug/kg 77 1 ' 1,4-Di6xane ND ug/kg 9700 1 Acceptance ' 7gateurro %'Recovery Qualifier Criteria 2-Dichloroethane-d4 94. 70-130 Toluene-d8 `110 70-130 ' 4-Bromofluorobenzene 103 70-130 Dibromofluoromethane 90 70-130 ' Page 9 of 55 �+� 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 I SAMPLE RESULTS ' Lab ID: L0700683-02 Date Collected: 01/12/07 11:2.5 ' Client ID: BOTTOM Date Received: 01/15/07 Sample Location: HYANNIS,MA Field Prep: Not Specified Matrix: Soil ' Anaytical Method: 60,8260B Analytical Date: 01/19/07 17:08 Analyst: RY ' Percent Solids: 97% Parameter Result r Qualifie Units tts RDL Dilution Factor Methylene chloride ND ug/kg 250 1 ' 1,1-Dichloroethane NO ug/kg 38 1 Chloroform NO ug/kg 38 1 ' Carbon tetrachloride NO ug/kg 25 1 1,2-Dichloropropane NO ug/kg 88 1 ' Dibromochloromethane NO ug/kg 25 1 1,1,2-Tnchloroethane NO ug/kg 38 1 Tetrachloroethene NO ug/kg 25 1 Chlorobenzene NO ug/kg 25 1 Trichlorofluoromethane NO ug/kg 120 1 1,2-Dichloroethane NO ug/kg 25 1 , 1,1,1-Trichloroethane NO ug/kg 25 1 Bromodichloromethane NO ug/kg 25 1 trans-1,3-Dichloropropene ND ug/kg 25 1 ' cis-1,3-Dichloropropene ND ug/kg 25 1 1,1-Dichloropropene ND ug/kg 120 1 Bromoform ND ug/kg 100 1 ' 1,1,2,2-Tetrachloroethane ND ug/kg 25 1 Benzene NO ug/kg 25 1 Toluene NO ug/kg 38 1 ' Ethylbenzene NO ug/kg 25 1 Chloromethane NO ug/kg 120 1 Bromomethane NO ug/kg 50 1 ' Vinyl chloride NO ug/kg 50 1 Chloroethane ND ug/kg 50 1 1,1-Dichloroethene ND ug/kg 25 1 ' trans-1,2-Dichloroethene NO ug/kg 38 1 Trichloroethene ND ug/kg 25 1 1,2-Dichlorobenzene ND ug/kg 120 1 , 1,3-Dichlorobenzene ND ug/kg 120 1 Z_.m.... a.._...:: Page 10 of 55 ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 SAMPLE RESULTS Lab ID: L0700683-02 Date Collected: 01/12/07 11:35 Client ID: BOTTOM Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor ' 1,4-Dichlorobenzene NO ug/kg 120 1 Methyl tert butyl ether ND ug/kg 50 1 p/m-Xylene ND ug/kg 50 1 ' o-Xylene ND ug/kg 50 1 cis-1,2-Dichloroethene NO ug/kg 25 1 Dibromomethane .- NO` ug/kg 250 1 ' 1,2,3-Tdchloropropane ND ug/kg 250 1 Styrene x NO ug/kg 50 1 Dichlorodifluoromethane NO ug/kg 250 1 ' Acetone NO ug/kg 250 1 Carbon disulfide ND ug/kg 1200 1 2-Butanone ND„ . ug/kg 250 1 ' 4-Methyl-2-pentanone ND ug/kg 250 1 2-Hexanone ND ug/kg 250 1 Bromochloromethane NO "ug/kg 120 1 L , Tetrahydrofuran NO. ug/kg 500 1 . 2,2-Dichloropropane NO ug/kg 120. 1 1,2-Dibromoethane NO ug/kg 100 1 1,3-Dichloropropane NO ug/kg 120 1 1,1,1,2-Tetrachloroethane NO ug/kg 25 1 Bromobenzene NO, ug/kg 120 1 n-Butylbenzene NO ug/kg 25 1 sec-Butylbenzene ND ug/kg 25 1. tert-Butylbenzene NO ug/kg 120 1 o-Chlorotoluene NO ug/kg 120 1 p-Chlorotoluene ND r ug/kg 120 1 ' 1,2-Dibromo-3-chloropropane ND. ug/kg 120 1 Hexachlorobutadiene ND ug/kg 120 1 Isopropylbenzene ND ug/kg 25 1 ' p-Isopropyltoluene ND ug/kg 25 1 Naphthalene ND, ug/kg 120 1 -' n-Propylbenzene ND. ug/kg 25 1 1,2,3-Trichlorobenzene NO ug/kg 120 1 1,2,4-Trichlorobenzene NO ug/kg 120 1 .: f. 1,3,5-Trimethylbenzene NO ug/kg 120 1 1,2,4-Trimethylbenzene NO ug/kg 120 1 Ethyl ether ND ug/kg 120 1 ' Page 11 of 55 01220714:11 , Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 SAMPLE RESULTS ' Lab ID: L0700683-02 Date Collected: 01/12/07 11:35 ' Client ID: BOTTOM Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified. Parameter Result Qualifier Units RDL Dilution Factor �fi»a to Or amcs by MEP 826q�15035-M,, h Isopropyl Ether ND ug/kg 100 1 ' Ethyl-Tert-Butyl-Ether ND ug/kg 100 1 Tertiary-Amyl Methyl Ether ND ug/kg 100 1 1,4-Dioxane ND ug/kg 12000 1 ' Acceptance Surrogate %Recovery Qualifier Criteria ' 1,2-Dichloroethane-d4 95 70-130 TolueneA8 109 70-130 ' 4-Bromofluorobenzene 100 70-130 Dibromofluoromethane 90 70-130 1 Page 12 of 55 t ' 01220714:11 Project Name: CHAMPION.BUILDERS Lab Number: L0700683 ' Project Number: 7513' ; Report Date: 01/22/07 , Method Blank3Analysis Batch Quality Control x •1 Analytical Method: 60,8260B , Analytical Date: 01/19/07 10:40 ' Analyst: RY. Parameter f Result Qualifier Units RDIL ' _ Y'���4'�K����� �4"'Y�����'y4�si���✓��S���y ` ??9��yv�,�E7G(?�� �$ "vaM ��.'��u��v..1�.�...� ..�......r.-.�..e✓v" - Methylene chloride ND ug/kg 500 1,1-Dichloroethane ND ug/kg 75 Chloroform ND ug/kg 75 Carbon tetrachloride- ND ug/kg 50 ' 1,2-Dichloropropane NDt , ug/kg 180 Dibr6mochloromethane ND ug/kg 50 1,1,2-Trichloroethane ND ug/kg 75 ' Tetrachloroethene ND , ug/kg 50 Chlorobenzene ND ug/kg 50 Tdchlorofluoromethane ND ug/kg 250 ' 1,2-Dichloroethane ND ug/kg 50 a 1,1,1-Trichloroethane ND ug/kg 50 Bromodichloromethane ND ug/kg 50 trans-1,3-Dichloropropene ND ug/kg 50 cis-1;3-Dichloropropene ND ug/kg 50 1,1-Dichloropropene ND „ ug/kg 250 ' Bromoform ND . ug/kg 200 1,12,2-Tetrachloroethane ND ug/kg 50 Benzene _ 14D ug/kg 50 ' Toluene ND ug/kg 75 Ethylbenzene ND ug/kg 50 Chloromethane ND ug/kg. 250 ' Bromomethane ND ug/kg 100 Vinyl chloride ND x ug/kg 100 Chloroethane .` -- ND ug/kg 100 I ' 1,1-Dichloroethene ND, ug/kg 50 trans-1,2-Dichloroethene 11 ND ug/kg 75 Trichloroethene ND ug/kg 50 1,2-Dichlorobenzene ND ug/kg 250 ' 1,3-Dichlorobenzene ND ug/kg 250 ' 1,4-Dichlorobenzene ND ug/kg 250 LEI.?1��1 Page 13 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' Method Blank Analysis Batch Quality Control ' Analytical Method: 60,8260E Analytical Date: 01/19/07 10:40 ' Analyst: RY Parameter Result Qualifier Units RDL Methyl tert butyl ether ND ug/kg 100 p/m-Xylene ND ug/kg 100 ' o-Xylene ND ug/kg 100 cis-1,2-Dichloroethene NO ug/kg 50 Dibromomethane NO ug/kg 500 ' 1,2,3-Trichloropropane NO ug/kg 500 Styrene NO ug/kg 100 Dichlorodifluoromethane ND ug/kg 500 ' Acetone NO ug/kg 500 Carbon disulfide NO ug/kg 2500 2-Butanone ND ug/kg 500 ' 4-Methyl-2-pentanone NO ug/kg 500 2-Hexanone NO ug/kg 500 Bromochloromethane NO ug/kg 250 ' Tetrahydrofuran NO ug/kg 1000 2,2-Dichloropropane NO ug/kg 250 1,2-Dibromoethane NO ug/kg 200 ' 1,3-Dichloropropane NO ug/kg 250 1,1,1,2-Tetrachloroethane NO ug/kg 50 Bromobenzene NO ug/kg 250 ' n-Butylbenzene NO ug/kg 50 sec-Butylbenzene NO ug/kg 50 tert-Butylbenzene NO ug/kg 250 ' o-Chlorotoluene NO ug/kg 250 p-Chlorotoluene ND ug/kg 250 1,2-Dibromo-3-chloropropane NO ug/kg 250 ' Hexachlorobutadiene NO ug/kg 250 Isopropylbenzene NO ug/kg 50 p-Isopropyltoluene NO ug/kg 50 ' Naphthalene NO ug/kg 250 n-Propylbenzene NO ug/kg 50 ' J, L&PHA Page 14 of 55 ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number: L0700683 ' Project Number: 7513 Report Date: 01/22/07 1&'.Methodtlank An.,.alysis :Batch Quality Control ' Analytical Method: 608260B Analytical Date: 01/19/07 10:40 Analyst: RY 1 Parameter Result Qualifier Units RDL ._rm^•:::...,s s v ma.:_...,...._v4:...•_.,...,e�.�.�i'v.......�..S,.s�.sy.5,.+„t..�a_,ems '�. ,�.x�.,.:.,ro-e..r,_,...,., A..e.',s...�.,°,k _.._..,..._ �„ r-_...95»,.,.»..,s..-,....... .., 1,2,3-Trichlorobenzene ND -Ug/kg 250 1,2,4-Trichlorobenzene ND ug/kg 250 1,3,5-Trimethylbenzene " ND ug/kg 250 1,2,4-Trimethylbenzene ND ug/kg 250 ' Ethyl ether ND ug/kg 250 Isopropyl Ether ND ug/kg 200 Ethyl-Tert-Butyl-Ether ND ug/kg 200 ' Tertiary-Amyl Methyl Ether ND ug/kg 200 1,4-Dioxane ND ug/kg 25000 F - Acceptance Surrogate %Recovery Qualifier Criteria ' 1,2-Dichloroethane-d4 100 70-130 Toluene-d8 107 70-130 ' 4-Bromofluorobenzene 106 70-130 Dibromofluoromethane 94 70-130 Page 15 of 55 01220714:11 Lab Control Sample Analysis Project Name: CHAMPION BUILDERS Batch Quality Control Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits ...... >e. ..-.._:., L.L t 1 e r �,„.;. >'L 9 ,.,. .L> �i . .... .,LaL •! :'}.�p,`., txpE _'�" LS LyLYc �y,.�.." �L _`ix i 9 - .. 1._.,.:a: : [� ..., 4 �i�.1. .@. .. `".}:. .".:. '.0 y�:� 3 L iF� �e�P' LLY 44 ��✓.P F S� .t L, � l.X�_ r, � � M4,L�.. .. : ,L•„•�+i�:.�+ � S .X?n E. .Lx n:Lu L Ltp F _.K:�e..r..............u.« .,_..,........................La.8 ..,.....,:.u...,.:�...._.._,..k'�:.s_..z.:.�.a.*w...<.....,,..:,.�v,...eY,....w...3.v..,..._,,..m..�a4:.._..,s.,,E.,.«ni��s«:.....:.�.,av*�.....:;:a,e..nx..,.se.,:,..s.�,..,_..�,_.. , ,,.._.,_ ,a.,_.,...._.. ,_:ae.,.., .._..... <.__:,.... .�._ .....r.., .. . Methylene chloride `ca >E�s `"aL� ,xss` 70-130 t,e < i v<„`t. 25 1,1-Dichloroethane ;MINI " 70-130 °LL+ . 1 i, 25 .,.,....:MIa ..._t.w.L�.°v3 �L.x`a.°�•G m...s'3."«?°�sro „`.v..,,xu.>_.,t.c.,..r.. Chloroform 70-130 25 1*1 Carbon tetrachloride t n as"(�# 'Y2 �{5t` a`trti 70-130xY , ;`u 25 1,2-Dichloropropane y #fi�4:' L ,..ra. hj ' 70-130 vµ L 25 Dibromochloromethane 70-130 �' L Q ' �a 25 'Y�n,... 1,1,2-Trichloroethane YI�� -3 70-130 ; # 25 Tetrachloroethene 70-130 25 ....tip,.. Chlorobenzene v ytiO4! �, Y, t7Q tktz°: 70-130 4 25 Trichlorofluoromethane , ,jBJ 4G's�lp4* tX _" 70-130L ,N 7 25 1,2-Dichloroethane `r r v $ + x+ 70-130 2 25 1,1,1-Trichloroethane ,FJ + fQaa 70-130 *rt XL 25 Bromodichloromethane e 6$ j n �S t'j t sL;` 70-130 t 0 25 trans-1,3-Dichloropropene 3a #1 a ` 1 .�F`a 70-130 2 > t 25 cis-1,3-Dichloropropeneo( Q _ NYLt #(3 `�Lkt 70-130 x��L, '$ 25 e,>_-3 L,Sa�vrtStk:�'Lw..:n.. _:3::d. .........✓..r+ _.N. +Y su...n..�"..i,. .. 1,1-Dichloropropene 'II "N r xti. 70-130 ��-.1 25 Bromoform Xcdrn9., ey` PEA"fir � xMvti 70-130tpikt £q 50 ':3t��,y�_.e: `53.�.L>��=xm .,,.. °+. ... s..,...._ f......_ 1,1,2,2-Tetrachloroethane 70-130 25 Benzene` xa. tWC2 4s��5: # °kx3°6z 70-130 �uax >x ` s 25 Toluene s '#�8 « 70-130 x tLx F'k 25 Ethylbenzene 70-130 tt �} XLrt� 25 Page 16 of 55 � P14A 01220714:11 LabgControi Sample'Ana lysis- PlrojectW rne: CHQMPION'B�UILDERS +•Batch Quality Control z , m Lab Nuber: L0700683 ;Project;Number: 7513 -o�eRepolrt Date: 01/22/07 ,LCS LCSD %Recovery Parameter %Recovery `%Recovery Limits RPD RPD Limits Y 4 �j Y a � �y���+V• �e t• E<,+�k t� '.*: S <t:::* i t 1�# �i �/ *(lip Ft .i S' �.�i�� � �`J'A [«�y�7��,�.yy yy� a`.�. ��✓', <>.L° `�� o- :+�... �as� e s� i `s <..��a. .�..' . .. T1 'u�/�,....< : .�.>, � '..�.. L a" F ,� . Y'° 9?•t,: .. � f�#,*.,,.. ��'w. u.`n,:-: .:. _._.aYh:>_,e#'!«�*....Ea.s .....d....ew,.+at' .sr'..* <LeC.1-..-.._.a:.7e.�,..,e<6"e:,....,'?Se.,..,....,..,c^« .,�*..,*,.<.<.,a,...tc.,e'�aea..:.,S:Saaa,., .....on<,?es.<*v.,r.< tr:;?XsB.rn<:.,..:'u<.'i*<,e� -.':ras.,��*e<L...,..,.GE.,rri e.,r.S•..,e.:e.,.�...,:,e,x-.. ....,�_..,... ..v .._,,.,, _. ..,_. ..,, ..... < Chloromethane ` ... '� wee ?uor° ° <'�°i k�@?� 70-130. 3,a I2 ° I 50 ` Bromomethane 70-130 ' 1S ° 50 Vinyl chloride 08-!a s� � h<w4a J; F$r1w. n 70-130 3 ,>s_.v.N:: 25 Chloroethaney75°' 70-130 Y &�? s<< 25 1.1-Dichloroethene ti ax �«` ?s# u${� 70-130 tct L ,°, 25. AN,WINWARC,NNW trans-1,2-Dichloroethene 70-130 aq L 25 x _ . Trichooroethene `<< $1 s}<< a 70-130 4xs Q 25 1,2-Dichlorobenzene r 4<e °9QBx ;` <L e9}9 ° n 70-130 as, ?y 25 1,3-Dichlorobenzene 47, , l s°t°< i#? 70-130 ,<° to a.25 1,4-Dichlorobenzene1 a gut 1t 9 �t '` 70-130 s;# 4 25 Methyl tert butyl ether t� < rE. ° �53 } < 70-130 '19 25 >.,Y.<r....vr.<iyit.,.:,...,Sr.. .. ..n-. ..... ......r..S..xn-.. .. ,n.,..v...... p/m-Xylene ✓ < �415�<° ?@s<<p,fi°(boa ?a�R ' 70-130 25 O-Xylene o,w 70-130 < 3F 25 y cis-1,2-Dichloroethene 70-130 a ;Yl 25 +.�?<Q_a ``.._,e.e r..<_•,i'_°' .r..4, >:.9 t «.:,?ia,m<r.,? Dibromomethane Fti< < 8 1 , e` °t<4t '8 ' ae 70-130 tE° R # L 25 ..;*ca., ..;�: .`.'saw..,Nil? c * 1,2,3-Trichloropropane ?<# � o°� .�" s,5°4w �1 , <FSR ` 70-130 t, 25 ...;5,5w.., ..,..!?v655.,;>-°r.,,<,...,... Styre.n@ 70-130 a < L 0 <#r9 a } 25 # 98 a . v Dichlorodifluoromethane 70-130 50 Ys , i < i u H N 4 ° Acetone "t6ses Q L s t ti,c B F n "#, 70-130 0 7< 50 Carbon.dlSUlfide r a< �q? Y6t '4i7s° 70-130 ni< 4e 25 }� tt a..,...;:#F,TM._Witr2<..N_.r.:4$ .3_St.s,_.:t t_,x...e;s�x.«_, _ 2-Butanone 9fi 70-130 # 50 Page 17 of, 5 �tia 01220714:11 Lab Control Sample Analysis Project Name: CHAMPION BUILDERS Batch Quality Control Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits 4-Meth I-2- entanone fez " t`F £?z* ' ' Y P `� � � ,. 98, F c, 70-130 ,`� �� 50 2-Hexanone ilG e`tt* :" `' 70 130 � atk Vie', z. 50 �,� ta: .. ��r&t._,�t•,.u8t„S.«..w..s?`3°e"v' Yk6s w.ksAS�, .... Bromochloromethane tFt� 70-130 .` 1� ? 25 131 1-- Tetrahydrofuran Room 70-130eFu1n4;0 t 25 2,2-Dichloropropane 4�A t �4 � 4 ``s3 70-130 for 50 1,2-Dibromoethane �ttttysEx `eryi �eFa .fs 70-130 SF r' 25 1,3-Dichloropropane *ht �2 { ©G :* 70-130 °�4W w 25 1,1,1,2-Tetrachloroethane yKSFfQ$`'�Yt s`� ' 07 ?iron 70-130 st 25 Bromobenzene 70-130z 3 25 n-Butylbenzene 4F r�F rs� '�1,4 ss 70-130 r' 3 + ` 25 sec-Butylbenzene „';` p$���e_ F41 wF19x 70-130 3 ; 25 tert-Butylbenzene 1 des g' 70-130 " Q+ 25 S.A.-=F \.._w.,a-..rG�xS. �,�...�:...... .�_...._. �: o-Chlorotoluene ' t#(�i,x E � F 70-130 9 25 p-Chlorotoluene ° 4 .•` '1 F�.Y,v.;� 70-130 sRti�.._,._,q 25 1,2-Dibromo-3-chloropropanetY $�FL 'M, t' V$ Q5 z LL µ 70-130 y`µ 7 50 : Hexachlorobutadiene 70-130 s 6 25 ..�...b .,.:..z3W .�... ,,..1F...ew:',i:....,a::w:..>:::s.;ab'. ..o?.....:......:..o...:.a.....�_. Isopropylbenzene E` ,+ `v ' x r' .. 2g'� �'r 70-130 3 0$ 25 _....a',..6"rrt.t...'�n .m..,... `..EFAt.`..zwAtaA p-Isopropyltoluene �� 'IFS ¢� � 7Tt 70-130 ` ' 25 .:e-z Naphthalene 70-130 25�Fz a, �__ °.,..,...z.: n-Propylbenzene t T �tF .'~L1$s % 70-130 £ s 25 1,2,3-Trichlorobenzene w' t1° ' x, Fw 70-130y 25 Page 18 of 55 01220714:11 'Lab Contrd1,Sample Analysis -Batch"Quaiity Control Project Name: CHAMPION BUILDERS = 1 Lab Number: L0700683 Project'.Number: 7513 - Report Date: 01/22/07 •.:LCS LCSD %Recovery Oarariieter %Recovery; %Recovery- Limits ROD RPD Limits '+ t. �t 4n �.: .o-�i*» t h«1 _o✓. :..__.:"b_„F� �t t .2 A G,+ :�.G4 4 ..L .y4 C b. '1.. � �, y �. St,. 4 r <'w ,F, •C. t. io Y.. !. .fie �-t tG F. 1,2,4-Trichlorobenzene °T" t,4 ,y ty, Q`r 4t t; 70-130 t 4 25 ,.v. ...,.E.... ;...,,.,�.,^ :...t.....,�s. E, t..<t,,..«... ,...E..c.:..c•..,. 1,3,5-Trimethylbenzene r etm tG� « T ��tt 5 70-130 trx t`:s3 25' 1,2,4-Trimethylbenzene . a ';'yz yL ,: kr ;` �1414t t t 70-130 F? 4t GS 25. : Ethyl ether «< c� s'f 4�t <° g�4t xx J 70-130 25 Isopropyl Ether d < f00 G t. G1flt�GG 70-130 g 25 Ethyl-Tert-Butyl-Ethert1t t� ' <=+ 'y e 70-130" F2�2r i 25 _ iv.,'z7 -.,.rr...,nv... c�"...• t�.5ht„si£�P..._�e..,.,. .. ,.. - x..,F._,.ov,...,e.. ,_._.. Tertiary-Amyl Methyl Ether .tot1 � EGtrt��,tE{y;^s v' 707130 t1044 25 .'..t.' 1,4-DI X ne 70-130 �'<^...::....: as_...n.... 50 _ Lids L•CSD Acceptance Surrogate %Recoyery`Quaiifier %Recovery .Qualifier Criteria 1,2-Dichloroethane-& 98 96 70-130 Toluene-O 112 108 70-130 4-Bromofluorobenzene 101 103 70-130 Dibromofluoromethane 97- 96 70-130 -,Page 19 of 55 �H.a' 01220714:11 ' 1 PETROLEUM HYDROCARBONS Page 20 of 55 ' ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' SAMPLE,RESULTS Lab ID: L0700683-01 Date Collected: 01/12/07 10:55 ' Client ID: ES Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified. Matrix: Soil ' Anaytical Method: 59,VPH-04-1.1 Analytical Date: 01/16/07 13:25 Analyst: TT ' Percent Solids: 96% ' "`' ..'",�,'; � � .._,..,'� u, sr � � �ia�Cifl1�F�YQ�R>�flfl1#1tlflRl.� ',+..�.a."u,�. ., .."A j,• ate,..�.....'.':. ..,3 Condition of sample received. °' '" Satisfactory Sample Temperature upon receipt: Received on Ice ' Were samples received in methanol? Covering the Soil Methanol ratio: 1:2.4 �:.u�.z�;':......z'w.i'�? ...,?�.➢,�. ... a....'::'y..';ap}u�.. ..sw.._.,°..�a a�.�;e '�:';aas?."k ..'a... ;o?.. ...5.;:�? � -:t�' .,c.,«_...,�" .,-:aa 4:.a....:..�,s�m.:.3 Parameter Result Qualifier Units RDL Dilution Factor C5 C8 Aliphatics ND„ mg/kg 1.24 1 C9-C12 Aliphatics, „ 2.84 mg/kg 1.24 1 ' C9-C10 Aromatics s ND mg/kg 1.24 1 C5-C8 Aliphatics,Adjusted ND ` mg/kg 1.24 1 C9-C12 Aliphatics,Adjusted 2.84 mg/kg 1.24 1 ' Benzene ND mg/kg 0.050 1 Toluene ND mg/kg 0.050 Ethylbenzene ND mg/kg 0.050 1 p/m-Xylene ND; r mg/kg 0.050 1 o-Xylene ND mg/kg 0.050 1 Methyl tert butyl ether ND mg/kg 0.025 1 Naphthalene ND mg/kg 0.249 1 Acceptance Surrogate �' %°Recovery Qualifier. Criteria 2,5-1)ibromotoluene-13I1) 100 70-130 2,5-Dibromotoluene-FID 98 70-130 1 f - ',a.. ' Page 21 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 SAMPLE RESULTS ' Lab ID: L0700683-01 Date Collected: 01/12/07 10:55 ' Client ID: ES Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3545 ' Anaytical Method: 61,EPH-04-1 Extraction Date: 01/16/07 04:00 Analytical Date: 01/19/07 18:21 Analyst: BN Percent Solids: 96% ' Condition of sample received. Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method ' .....»...., ...�""' ..,..,.e.... 5.;�'"d...l..b �,.w .r....>...,.... .t... ..........+L Et is...,...✓..,,r..... ..l..v.,...'?..r .0 S.,a` . ,...e.n✓..,x. .._S..`'..,o- . ...,.... .M .v.....�4...,r.,e e:l.i Parameter Result Qualifier Units RDL Dilution Factor ' C9-Cl8 Aliphatics ND mg/kg 6.94 1 , C19-C36 Aliphatics 19.2 mg/kg 6.94 1 C11-C22 Aromatics ND mg/kg 6.94 1 C11-C22 Aromatics,Adjusted ND mg/kg 6.94 1 ' Naphthalene ND mg/kg 0.347 1 2-Methylnaphthalene ND mg/kg 0.347 1 Acenaphthylene ND mg/kg 0.347 1 ' Acenaphthene ND mg/kg 0.347 1 Fluorene ND mg/kg 0.347 1 Phenanthrene ND mg/kg 0.347 1 ' Anthracene ND mg/kg 0.347 1 Fluoranthene ND mg/kg 0.347 1 Pyrene ND mg/kg 0.347 1 ' Benzo(a)anthracene ND mg/kg 0.347 1 Chrysene ND mg/kg 0.347 1 Benzo(b)fluoranthene ND mg/kg 0.347 1 ' Benzo(k)fluoranthene ND mg/kg 0.347 1 Benzo(a)pyrene ND mg/kg 0.347 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.347 1 ' Dibenzo(a,h)anthracene ND mg/kg 0.347 1 Benzo(ghi)perylene ND mg/kg 0.347 1 /,ALPHA ' Page 22 of 55 ' f ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date.' 01/22/07 ' SAMPLE RESULTS Lab ID: L0700683-01 Date Collected: 01/12/07 10:55 ' Client ID: ES Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified ' Parameter Result Qualifier Units RDL Dilution Factor Ex>lractable Petroleum.Hydtocacbor�s- x t ,� , Acceptance ' Surrogate %Recovery Qualifier Criteria Chloro-OctadeGane fi0 40-140 o-Terphenyl 45 40-140 ' 2-Fluorobiphenyl 58 40-140 2-Bromonaphthalene 60 - 40-140 �T,L?I•;r1' ' Page 23 of 55 01220714:11 , Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 SAMPLE RESULTS ' Lab ID: L0700683-02 Date Collected: 01/12/07 11:35 ' Client ID: BOTTOM Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Matrix: Soil ' Anaytical Method: 59,VPH-04-1.1 Analytical Date: 01/16/07 14:17 Analyst: TT Percent Solids: 97% , 'GY G5 G-: G�5 ;✓5 G�'SC G �t 6. GGA„4 Y y A... py ;�4����A1I ����,sl��?����n 0. A G G�: ✓a. n. � 0. aA w'�.�"nA•:.. N .s... ._A._........... .,;�..._nz...J .....,»-.. ..xtc✓...!4+.Y . i.....a_...... .`5:....✓.J:? ..4+ .......m.» ....r ... .. .... Condition of sample received. Satisfactory Sample Temperature upon receipt: Received on Ice Were samples received in methanol? Covering the Soil , Methanol ratio: 1:2.6 s...,... ,�»`..G...b.n i :G.`.•,..:0.+:.✓,,.SG.�.....� ..•,.H..,J�ee� ",G'.F'C w.n.G'3?..w"''...+_....».'.Y..e_.ai0.�J?Gw0.0.•nY h.G;4iee. >J 5......5... ..».+..T.»�.'�M1....<3K a.. vi_v�F.A0.i.t"G '1 5 Parameter Result Qualifier Units RDL Dilution Factor �•OI.tG���0.1�I�.�I�V.4wl 4 55 J>SLNy 0.Y'cGi1NG`G�5 J;?� 6G ^yeG ,»+.G 50.�0.G �J G S y. .� G GN G :4 C � ,G� 0.C CY S 5..csG»»:�'...,v.......,..Jw...t�'.�e.._:>ews...»:v....WJ,..G..:'....a5:....w.Jx......?J.._s.?s...�::�_.tG.�. 3e.. ..w._... .xh,.;.N.$,.... ... .... �r,s�.......:.:�`..,.... t.N. . ..,..�._,..m._. J.,.,r;_._ . ._. C5-C8 Aliphatics ND mg/kg 1.15 1 C9-C12 Aliphatics ND mg/kg 1.15 1 C9-C10 Aromatics ND mg/kg 1.15 1 ' C5-C8 Aliphatics,Adjusted ND mg/kg 1.15 1 C9-Cl2 Aliphatics,Adjusted ND mg/kg 1.15 1 Benzene ND mg/kg 0.046 1 ' Toluene ND mg/kg 0.046 1 Ethylbenzene ND mg/kg 0.046 1 p/m-Xylene ND mg/kg 0.046 1 ' o-Xylene ND mg/kg 0.046 1 Methyl tert butyl ether ND mg/kg 0.023 1 Naphthalene ND mg/kg 0.230 1 ' Acceptance Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 110 70-130 ' 2,5-Dibromotoluene-FID 09 70-130 1 Page 24 of 55 ' 01220714:11 Project Name: CHAMPION BUILDERS 1 Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 I ' SAMPLE RESULTS Lab ID: L0700683-02 Y Date Collected: 01/12/07 11:35 ' Client ID: BOTTOM Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3545 ' Anaytical Method: 61,EPH-04-1 Extraction Date: 01/16/07 04:00 Analytical Date: 01/19/07 18:55 Analyst: BN ' Percent Solids: 97% ' �_._«ati✓._,...._o a�c.'�,._ ,�_,",.wc �t.µ?.�x""�c4 a;F scy_"s«�K �{v�l��Q.ItJ�©��a����s`� c °'"'t °. �"c< c rdc �.. ..� a M1,..+.a*•g:. �' s.,. .. Condition of sample received. Satisfactory Sample Temperature upon receipt: Received on Ice ' Sample'Extraction method: Extracted Per the Method "•._.;,; .. cc .?., ''"..h� �:: c ,c:5,. c}° tits;'� 9 n`'�:r. ° i..,' F..., ,�.?v, =t~ .4t a ca �v ,}�tt3 Paramlete4rJ Result Qualifier Units RDL Dilution Factor z�iii�L1�74.«� S���Y�����- � ..-.. CiC St L 1Gt. -:..s^5, � t i. ,. h t t Ct t y.�,• i y :•"�m'SspsY,.��.,�;«.,t;'��..�`e.s�.�Win.._..-�.�•eq�':..ess;��^"e?^u,.,-.c.'��'?'1`.�...... .a s _ sc,._ - �`"�y R 5'}�t cY- Rt Rcc' �.`c '�' ' C9-Cl8 Aliphatics 14.5 mg/kg 6.87 1 C19-C36 Aliphatics 47.0 mg/kg 6.87 1 C1 1-C22 Aromatics 247 mg/kg 6.87 1 ' C11-C22 Aromatics,Adjusted , 24:7 `« mg/kg 6.87 1 Naphthalene ND mg/kg 0.344 1 2-Methyl naphthalene ND mg/kg 0.344 1 Acenaphthylene ND mg/kg 0.344 1 Acenaphthene ND mg/kg 0.344 1 . Fluorene -ND mg/kg 0.344 1 ' Phenanthrene ND mg/kg 0.344 1 Anthracene ND mg/kg 0.344 1 Fluoranthene ND mg/kg 0.344 1 ' Pyrene ND mg/kg 0.344 1 Benzo(a)anthracene ND mg/kg 0.344 1 Chrysene ND mg/kg 0.344 1 ' Benzo(b)fluoranthena ND mg/kg 0.344 1 Benzo(k)fluoranthene ND mg/kg 0.344 1 Benzo(a)pyrene ND mg/kg 0.344 1 ' 1ndeno(1,2,3-cd)Pyrene ND`., mg/kg 0.344 1 Dibenzo(a,h)anthracene. ND mg/kg 0.344 1 Benzo(ghi)perylene ND-* mg/kg 0.344 1 rl�L?F, ' Page 25 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 SAMPLE RESULTS ' Lab ID: L0700683-02 Date Collected: 01/12/07 11:35 ' Client ID: BOTTOM Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor ' Extractable Petroleum>F�ydrocarbons Acceptance ' Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 54 40-140 o-Terphenyl B1 40-140 ' 2-Fluorobiphenyl 80 40-140 2-Bromonaphthalene 81 40-140 ,11L'?Ivi Page 26 of 55 , ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 SAMPLE.RESULt$!. ' Lab ID: 1-0700683-03 Date Collected: 01/12/07 12:00 Client ID: COMP SW Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3545 Anaytical Method: 61,EPH-04-1 Extraction Date: 01/16/07 04:00 Analytical Date: 01/19/07 19:28 Analyst: BM tPercent Solids: 93% "� `,,,,,,e,. s y s' .ra u. >;, ,a` «+.«P ,m "e�����i���o�Y.♦�t��flF�lattt�� . 1� 9i» `v G r+ 5 � 5 .-_F5�.._r a,:` ...»_.''..»`�i' .�i._✓3 _✓..:r. .,. «,... .,*�»».a^ 2'. '+.aA...� },?,.:.5»K"«,.«..,:5.�« u.i. ✓`,"�1 H�`»i ,.,t Condition of sample received. Satisfactory Sample Temperature upon receipt: _ Received on Ice Sample Extraction method: Extracted Per the Method. Parameter Result Qualifier Units RDL Dilution Factor ' C9-Cl8 Aliphatics 8.21 mg/kg 7.17 1 C19-C36 Aliphatics 46.6 mg/kg 7.17 1 C11-C22 Aromatics 8.40 mg/kg 7.17 1 ' C11-C22 Aromatics,Adjusted 8.40 i mg/kg 7.17 1 Naphthalene NO mg/kg 0.358 1. 2-Methylnaphthalene NO mg/kg 0,358 1 ' Acenaphthylene NO m mg/kg 0.358 1 Acenaphthene NO mg/kg 0.358 1 Fluorene NO mg/kg 0.358 1 ' Phenanthrene NO mg/kg 0.358 1 Anthracene NO mg/kg 0.358 1 Fluoranthene - NO mg/kg 0.358 1 ' Pyrene NO mg/kg 0.358 1 Benzo(a)anthracene NO mg/kg 0.358 1 Chrysene NO mg/kg 0.358 1 tBenzo(b)fluoranthene — NO mg/kg 0.358 1 Benzo(k)fluoranthene NO mg/kg 0.358 1 Benzo(a)pyrene NO , mg/kg 0.358 1 ' Indeno(1,2,3-cd)Pyrene ND' mg/kg 0.358 1 Dibenzo(a,h)anthracene 4 NO mg/kg 0.358 1 Benzo(ghi)perylene NO mg/kg 0.358 1 1 fix Page' Page 27 of 55 r 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' SAMPLE RESULTS Lab ID: L0700683-03 Date Collected: 01/12/07 12:00 ' Client ID: COMP SW Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Extractable Petroleum t4" drocarb' * ,.., Acceptance ' Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 62 40-140 o-Terphenyl 54 40-140 ' 2-Fluorobiphenyl B9 40-140 2-Bromonaphthalene 7' 40-140 t 1 ;'-ILL?Fill ' Page 28 of 55 ' ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number: L0700683 ' Project Number: 7513 Report Date: 01/22/07 Method Blank`Analysis Batch Quality Control Analytical Method: 61,EPH-04-1 Extraction Method: EPA 3545 Analytical Date: 01/17/07 19:07 Extraction Date: 01/16/07 04:00 ' Analyst: BN 1 Parametepr' T Result* ' Qualifier bUnits R�D�L('�f� ' � r��b�V���e� �� t�1 ir�t'Le•`a.+1iw�+. ��,�5y tl��� �"�7��� t���1..,4''Vt7�',•� � ��Y��."1 X� ,M .. 5"G�. C9-C18 Aliphatics ND mg/kg 6.67 ' C19-C36 Aliphatics ND mg/kg 6.67 C11-C22 Aromatics ND mg/kg 6.67 C11-C22 Aromatics,Adjusted ND mg/kg 6.67 ' Naphthalene ND mg/kg 0.333 2-Methylnaphthalene ND mg/kg 0.333 F , Acenaphthylene ND mg/kg 0.333 ' Acenaphthene " ND mg/kg 0.333 Fluorene ND mg/kg 0.333 Phenanthrene ND mg/kg 0.333 ' Anthracene ND mg/kg 0.333 Fluoranthene ND mg/kg 0.333 Pyrene ND mg/kg 0.333 Benzo(a)anthracene ND mg/kg 0.333 Chrysene ND mg/kg 0.333 Benzo(b)fluoranthene ND mg/kg 0.333 Benzo(k)fluoranthene ND ,, ti mg/kg 0.333 1 Benzo a rene ND m /k 0.333 OPY 9 9 Indeno(1,2,3-cd)Pyrene NDI mg/kg 0.333 ' Dibenzo(a,h)anthracene ND mg/kg 0.333 Benzo(ghi)perylene ND mg/kg 0.333 Acceptance Surrogate %Recovery 'Qualifier Criteria ' Chloro-Octadecane 63 40-140 o-Terphenyl 56 40-140 ' 2-Fluorobiphenyl 79 40-140 2-Bromonaphthalene 81 40-140 HA1 ' Page 29 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' Method Blank Analysis Batch Quality Control ' Analytical Method: 59,VPH-04-1.1 Analytical Date: 01/16/07 09:37 ' Analyst: TT Parameter yyyyyyy Result Qualifier Uniitt�Ysf" RDL y C5-C8 Aliphatics ND mg/kg 2.67 C9-C12 Aliphatics ND mg/kg 2.67 ' C9-C10 Aromatics ND mg/kg 2.67 C5-C8 Aliphatics,Adjusted ND mg/kg 2.67 C9-C12 Aliphatics,Adjusted ND mg/kg 2.67 ' Benzene ND mg/kg 0.107 Toluene ND mg/kg 0.107 Ethylbenzene ND mg/kg 0.107 ' p/m-Xylene ND mg/kg 0.107 o-Xylene ND mg/kg 0.107 Methyl tert butyl ether ND mg/kg 0.053 ' Naphthalene ND mg/kg 0.533 Acceptance , Surrogate %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 86 70-130 1 2,5-Dibromotoluene-FID 82 70-130 L�L-FAA ' Page 30 of 55 01220714:11 Lab Control Sample Analysis f Batch Quality Control Project Name: CHAMP.ION'BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits ,::�.. ..,:.., r- '..,a A�...:...«.«..« e}�:... ,. :...L V...-..a...i w � ,...R rw � <•«««.« .« «,,.r„•• gF:LttS: .ul- '3 LLt 7r L. .A � t �� �.y, ,�• }L.yq, x'� }C is q•BL..xbri"S`E+.'' qp �p Y,t.x�'G `�-. �Ci Y `a 1��y■ (yet. �P I� :, ., f�i�.� y(�]. .. «, - .S � �. >,. .., ��. �x- .�:;�«« _�;. ...« � - «:.; «« t .;� . . � «.<�,.c t.- h �•1!}ry' -�.?.. !6�'..t��..�1[1 .�f'?t• S«f < .4« � [R.+ E« ««« «.« A. F < «..« :«� « �n (vim ,« t4 :Ct E t «4+««.:•.t«"i «`a..5 �^ .'�^.}} �.« _«Ao�., ..t<�«{ 5 � «t«i t�^.«�tL�.«{.�4 � L,+««„« �4�y�«,@n+,q <.q�, t ?•.2,«,r««««q V tl t• x«+;� q+ ?C�t'n< S« q.,..«q. 1.x B ,§ .}c.Lc `+ey ..,« .t"C'..Lcq« }}.� «':c'q q ,sq« 4«a i��y. .,•t t 0«}x«> «<.t«•�;. .tt.. x ',::.�.e;�,aM.t�:.,>.:c>.,,t�r.,,...x,.?.;stw...o At.:�.:..,...�ea:85':�»sv„a«.....'...a'�ex,c�,e.S< .e t...h.,.x uza.:Lx••.tr*a°�.`r}..r.........r:.n �r.LL2Lde..:.<n<^<'Y3L<c5«en»es«:.».,..L.re B,c..:cL;Exi=:�.,e.�s�?.,eq.•q,:L....x.«e .L@.e.6 ..,�tl'�ow, ex«...tr.t..g5rto.,.q.. .....„t�,.�,c... �._.,,sa..:'A.e.,..c_. .....«..ti... . ... .<.., . ,.,,. C9-C18AIiphatiCS ;.. ., a }ttc aL R is ai F 40-140 Sii}t' 25 C19-C36Ali hatic$ _ 40-140 25 µ ; C11-C22 Aromatics 4c L3 4Z4c` �L t`4 Q c 40- 40 LL e1 25 'A - sA_.s...nS]4.....s.•...,-.•Yt Naphthalene i. ccuxrYtF amcx3 L� �yat - 40-140 9xY� n: 25 .. CIS,!I 2-Methylnaphthalene 01.si � ;40 140 25 Acenaphthylene 'r LNL'st' us@ _. e ;e AM+vX`L} 40-140 x.<14 -,25 r Acenaphthene ?Lx°e ,6`gt° ;ttp1��Ltt; �R';q'{ " ,e 40-140 25 `Eu.. • x..x.L..,A...,„.0.++..... - - Fluorene _ ...LL<}Lt 'c}'n£L s� `Jx t c'''« t'""o-yscL}s'x"•x 40-140- �.,� `n`£h�J uY ,. 25 Phenanthrene 40-140 },F °t4 25 - E,:...R•a .¢.,.s..�.�`�es..n.v.. �'::�:�e.�.:�t,.L;l.«.?3,�a:}.:M:"=. - _ u. .,.�@},:c«._.._�,�, . . Anthracene s Nis 11.111 x�txk"q q�LLse : 40-140 °iI4 25 Fluoranthene LL r xLt°k}. } xax xxhC a 40-140 FeL x 25 P rene a"x} en iaSe LL.:, E}cc@vtc� }fit' 40-140 mi L@c} 4 25 Y .. �r'�'.q»rw` �`t�.t.rary.., � }�c,r ... tY}'�...,._. r 1 .. �',f•it.r 'Yx i Benzo(a)anthracene ;V.fityt , ,1Lr'r L=° §8 3x 40-140 A >A> 25 ChrySene � c@ ,' y"xF�E�a*LE� caF a 40-140 L'F' 4 25 Benzo(b)fluoranthene H r #i6` na }tc4t "SSghN#r; 40-140 °,; 25 Benzo(k)fluoranthene pL?GG}`` c }a 4L7;�q;' 9Lwe « 40-140L"16 25 3;�e:SnJ >x..,�.x,2.,.Z• xta,x+.:�..,«...�.,, hd5.4:d.:-'a e,.,.4 we ep. Benzo(a)pYrene 4 c L c 5V 9ZtLt 4 u}Lti* q 8$x ct cs 1 40-140 }c°18 25 ..:c.::.i }.«..�. Indeno1,2,3-cd P rene ( ) Y aa siE;n �xLSLeu. 40-140 25 Dibenzo(a,h)anthracene ± @ };� $ � }oaa;L $lay"4 40-140 }' �} 3 25 .n.h.Na_ .. .L t�s S... ...... . .x..r.,...*_. «_L.:2_...r. Benzo(ghi)perylene n�`v ` 'L yt �w_w, xq ° . 40-140 y 31F9 25 Nonane(C9) 30-140- wkg4' 25 Page 31 of 55 4 01220714:11 Lab Control Sample Analysis Project Name: CHAMPION BUILDERS Batch Quality Control Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits ,... .v...- .E _',..,«.'�.• :'. :r p��' `.s; Y ti -�.•o+r � t tt Ys t ,4 - l�t �- R��'Y . .•. � t....-..«t�la3�.,.x+.s'�« « -.�t.y...,.^' ..y...,m.v..•*� ,? «.. ,...« � ... .Gas. 4.... . �:«_£. � .. .. . �.nt�R Y« ..� :. .A....�fit,.W✓. f 1-. S. �• 4 ( f- .t tt• «.t.,, u,=t. . ..4y...._.._.«....«.w..e.«_�GG,..".e...... ,„tat.Y.�ue.««t«...�..�.....:......0..«...... ..,, .-_.... ...,._ ,«.,, ... ., ..,.....M. ..t....zu:cst.GS.,,•._F�.._....�.z..n,G..G 40.«.. _.«.._...� ,.b..n..T_.«�,r♦,..,..:,_c<.. ,o..s.,..«e,..«nt:.....,.is...r.;n.«ee:.�'s;`eatw...e.. .«.t..t�scG.« ..,....r....,A5^^ r Decane(C10) si$ z�G �tFxEte3�Et�l�x a °e 40-140 3 a 2 2F g5 25 Dodecane(C12) qYi 40-140 a 0 5 25 Tetradecane(C14) z £$$u IN 8+ µ` 40-140 N u O, 25 Hexadecane(C16) `x sett <tt `1�4 40-140p 3 st 25 4 t`f�..GG.a.>.x.z,.._«... k,..nna5 n.5xt r.s,.,..«...:,tr:' Octadecane(C18) i? ,eg3} 40-140 k '� 5 25 n.a t`as«_..:.• _Y. ..r h.*'trx.G }.,p,_,._>r...c, .T....,..,u..Zi >_ Nonadecane(C19) 40-140 s`U G` 2b Eicosane(C20) 40-140 25 r=u✓.«,k. t:, ..:u...i., a.. r.,.. Docosane(C22) uw iete p £G G `y° $G t 40-140 M w eQi t 25 Tetracosane(C24) `. .... c. 40-140 25 Hexacosane(C26) •*YRG� �7 - °a`v"'¢7G 40-140 0 25 ttl a et a v 40-140 2 25 Octacosane(C28) Triacontane(C30) °° G 40-140 0'S 25 G z✓.•_ _, „G s ttt _t_= 40-140 s.-A G 25 Hexatriacontane(C36) �$IcG _ ,4'$8 _.e., LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Chloro-Octadecane 64 64 40-140 o-Terphenyl 64 71 40-140 2-Fluorobiphenyl 75 80 40-140 2-Bromonaphthalene 77 82 40-140 •Naphthalene Breakthrough 0 0 •2-Methylnaphthalene Breakthrough 0 0 Page 32 of 55 % .PH r I� I� � II• � I� � � � I� � lip � I� I� II• I� II• 01220714:11 Lab.Control,. 6n le Analy§is Batch Quality Coritrol Project Name: CHAMPIONIBUILDERS Lab`Number: L0700683 Project Number: 7513 R"e ort Date: 01/22/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits ' .:a a...�•k».4�,.�,': �»e.p...,p.}: n4A:...:'S A.h.x a:':..w...A..1 h.. ..^.Y Y��., a to ,,,n,t ,t.,. '.tt.- kt>-i 4 A.. 'x`YS ti � k...,..;-. :-at ., ;�;s-, -�...; ;Etat`wA .,r,•. k�ai`aa•,�aAAAA^A.^"Aaip aA 3^-at "Ea'�At t;°EA Ea�< aaA ,.� R'., E t', F � 4 Y. .^.a .,.✓».,..A,.. .$t>.. >S>. ..n.n .. ......,,.. e:r^..+. .+ >,,..�.. ... $.. ,a„^. t» > . t `a A `A f-. ::.,.::� '..:.....i .::.Ynt,elR,..AS .wwt.,AS.-:.C..ea..Lto i3.,.n:ti..A.:a..:..,t..,..✓...v..wC.+..,....>w".e...i.wtw.Gw.�b.w..n.»E.o..ar.tw.w..wmetn..atii..r.a..n..�.�`.LN,a.e.,uxU-..:,..xa,tl,11,5-.w.T.....w.4:x:, S...v...:.wC....nv..n x1r rt.^. �x»ati.'i.xS :Ate::. E..," .s .. ., .. ., 70-130 C5-C8 Aliphatics :,;k 4t 4. Q tA�A �5 ( 25 C9-C12Aliphatics 70-130 Ra a 25. C9-C10 Aromatics a`A �5a 5xx tr r4,s ¢ xt A.5 70-130 A 25 Y5,,. - Benzene ray ytA�sA ° a 4 `a 70-130 9Y t�E 1 Aa i " 25 Toluene S° 70-130. d E s° to 4 x 5 25 .. a M P?kk Ethylbenzene A`l aAjai E�tiEE'.t'C:•,ea'aA Am.n3a, 70-130 ,<s`t�''hi':p nA�`a 25 IMPRINT-,.,_ ASz,.6x...�zstitzx.,@k�`?ix:�x..x_; p/m-Xylene <aAa` �t: jz @ a @ ``ate ,. 70-130 a a 3 0 25 O-Xylene .;>` 4E', .cam...F.,. ka.,a �,�i esAx3ww%. .. 70-130 -. i., ° a 25 IMI Y Y `i ` '. s ° ' 70-130 ``.a :t..., . Methyl tent butyl ether �� ��� s � 25 Naphthalene 4 "` t a` w w 70-130 ata t=, ar 4 - 25 1,2,4-Trimethylbenzene `r : .x ; ;4 a "j4 k,`AFu 70-130 9t 25 Pentane k.,. $6i a` At 70-130 !` k 25 a O 2-Meth I entane YAY 4 A Et 8a faEt as a 70-130 °t 25 2,2,4-Trimeth I entane 70-130 25 n-Nonane 30-130 25 al 4s slogan . 25 n-Decane �`1 ..r�:_, � A..^..,5 n-Butylcyclohexane 70-130 a4 25 Page 33 of 55 '�' 01220714:11 Lab Control Sample Analysis Project Name: CHAMPION BUILDERS Batch Quality Control Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits .,:.v ✓:. -i '.:...+.. 'o.-,.'..: ^..... ..�:`t`. .R^*t,'... :..... Y is .., 0...;... .4?. -L^*' x�a _ .•L44V-t ...i -a .:S:K✓'i.:•.H• ,-aii x _uxi :ai'!: �' ,-6r .15� .S ....., ,>. ��yFyj. , ..., .. ,.,+r�•.",t.. ...^...;.`t^,x i. �. ,�..•'.",t'..^...i..,,v "kt C .}.•,..,.t^.,,.LS,, Y„t x-.i: $ ,Pk :'�_ t5 t i .�..✓.�Yu'ii ...,*.�.-*Y��`...�c"w�:^G'Oe.Ott...5 u..14o. S e5e�1'c..a.EaOu..�4%�,,C.�� :i�..ni ..�:utixSci..Bar.OY.nwSw�"..+iSO^ee�.:di.a0..."+...:n b.+Y Aidc.rznctn�wc^n..+.uw....o.e�ot LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria 2,5-Dibromotoluene-PID 95 98 70-130 2,5-Dibromotoluene-FID 90 93 70-130 Page 34 of 55 ! Pti� A ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number: L0700683 ' Project Number: 751.3. N Report Date: 01/22/07 Fractionation Check*,Standard ' Quality Control Fractionation check standard for FISH526'f8 `' ' Parameter % Recovery QC Criteria C9-Cl8 Aliphatics .'62- 40-140 C19-C36 Aliphatics _ 71 40-140 ' C11-C22 Aromatics 80 40-140 Naphthalene 74 40-140 2-Methylnaphthalene 70 40-140 ' Acenaphthylene 69 40-140 Acenaphthene 72 40-140 Fluorene 72 40-140 ' Phenanthrene 72 40-140. Anthracene 77 40-140 ' Fluoranthene" 75 40-140 Pyrene 75 40-140 Benzo(a)anthracene 74 40-140 ' Chrysene 88 40-140 Benzo(b)fluoranthene 72 40-140 Benzo(k)fluoranthene 74 40-140 ' Benzo(a)pyrene 73 40-140 Indeno(1,2,3-cd)Pyrene 72 40-140 Dibenzo(a,h)anthracene 73 40-140 ' Benzo(g,h,i)perylene 73 40-140 Nonane 57 30-140 Decane 62 40-140 ' Dodecane 65 40-140 Tetradecane 63 40-140 Hexadecane 64 40-140 1 Octadecane 64 40-140 Nonadecane' 64 40-140 ' Eicosane 67 40-140 Docosane 71 40-140 Tetracosane 72 40-140 ' Hexacosane 72 40-140 Octacosane 73 40-140 Tnacontane 73 40-140 1 Hexatriacontane 76 40-140 ' Page 35 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' Fractionation Check Standard Quality Control ' Fractionation cheek sfandard for`FtSH52618 Surrogate % Recovery QC Criteria t Chloro-Octadecane 57 40-140 o-Terphenyl 78 40-140 ' 2-Fluorobiphenyl 72 40-140 2-Bromonaphthalene 72 40-140 ' i 1 1 r,L L?HA Page 36 of 55 _ ' ' 01220714:11 { i • ,. f" rr d�, a, q y I �L�L?Fib ' Page 37 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' SAMPLE RESULTS Lab ID: L0700683-02 Date Collected: 01/12/07 11:35 ' Client ID: BOTTOM Date Received: 01/15/07 Sample Location: HYANNIS,MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 64,8082 Extraction Date: 01/17/07 13:00 ' Analytical Date: 01/18/07 17:53 Cleanup Methodl: EPA 3665A Analyst: JB Cleanup Datel: 01/18/07 ' Percent Solids: 97% Parameter Result Qualifier Un its RDL Dilution Factor cp � iV� �)�b� ✓ C a 5,✓sy�"`r' ... '� a ,.e,S Y.'af as'+G «�i.4 Wa S � `� 2 a �a �.� c°_,_.��_,,,. ,?,.:.* _2_,sc<.. a sa��.. ?c_:...�.r...z. ?:.;.r°�..�-.�. ..a.�.'3'.. ..n.«..,r° .. ...,_a,.,..., . ..s:5�w.�_�-.._... ...s.,...,;�..a:..,..,..:�...�^...cs�:._,?.�.,';a" Aroclor 1016 ND ug/kg 34.4 1 Aroclor 1221 ND ug/kg 34.4 1 ' Aroclor 1232 ND ug/kg 34.4 1 Aroclor 1242 ND ug/kg 34.4 1 Aroclor 1248 ND ug/kg 34.4 1 ' Aroclor 1254 ND ug/kg 34.4 1 Aroclor 1260 41.1 ug/kg 34.4 1 Aroclor 1262 ND ug/kg 34.4 1 ' Aroclor 1268 ND ug/kg 34.4 1 Acceptance ' Surrogate %Recovery Qualifier Criteria Column 2,4,5,6-Tetrachloro-m-xylene 80 30-150 A Decachlorobiphenyl 70 30-150 A ' 2,45,6-Tetrachloro-m-xylene 79 30-150 B Decachlorobiphenyl 75 30-150 B Page 38 of 55 ' ' 01220714:11 Project Name: CHAMPION BUILDERS .F Lab Number: L0700683 ' Project Number: 7513 Report Date: 01/22/07 Method Blank Analysis Batch Quality ControV Analytical Method: 64,8082 Extraction Method: EPA 3546 Analytical Date: 01/18/07 13:04 Extraction Date: 01/17/07 13:00 ' Analyst: JB Cleanup Method1: EPA 3665A Cleanup Date1: 01/18/07 f � Parameter -Result 'Qualifier UnitsL RDL v»� +at:»�H Y .'»» ! "tA 4 i'} � `w{."✓ Y SS A�L. "� i 6 Aroclor 1016 NO ug/kg 33.3 ' Aroclor 1221 'ND Y ug/kg 33.3 Aroclor 1232 _ND - � ug/kg 33.3 Aroclor 1242 ND ug/kg 33.3 ' Aroclor 1248 NO ug/kg 33.3. Aroclor 1254 NO ug/kg 33.3 Aroclor 1260 ND . ug/kg 33.3 Aroclor 1262 ND ug/kg 33.3 ' Aroclor 1268 ND ug/kg 33.3 ' AcceP tance , Surrogate '%Recovery, Qualifier. "Criteria Column ' 2,4,5,6-Tetrachloro-m-xylene 68 30-150 A Decachlorobiphenyl 62 30-150 A 2,45,6-Tetrachloro-m-xylene- 68 30-150 B Decachlorobiphenyl 75 30-150 B I ter..._ ' Page 39 of 55 01220714:11 Lab Control Sample Analysis Project Name: CHAMPION BUILDERS Batch Quality Control Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits ... ..:........ a'. ::.. ;. ...,.:..,.a,» >a.A< a _: ..�+• .. ...F < e. .a,,.a. ,r.:^, a ZK •Wr�F` ..... :.aaa.. -.. ,,... �> .yZ i�yc,���,� Ca 33ea�a� L r, a `� L,: C C .: � L:L. 'F,. tl ,Lt�F^�'+S�it�'.>.�Sy'S✓e: 4 Y �f Nk Y�R(L.,. 5 d"3t .� M��. � L E, S�k ..•.L�L..•. Z.• FZ. .... .. ... .,.t "`kZL •.�a��yr � ,..0 a 3.-: � e 's ae 5*.a..c. .a m,.,:,.Y e.,..,.u..,nL;:.,3.......,<.,.....e.^,..............<,e..,s,� 3.,..,....�;.�:_.,.,v,.:a.L...S..,..»-T,: »:;.......aa��Z.Sz..e�A4�4*u.:L,�.*r......:x:.....o.<Fe......�,:dn,...r.,.,. ...........h..v:.:.-.e. ?L...M.......a....;�L..,<L."�zi ?1...iv.:.... .,.K..»:5..,....., ..,..,<_ ..., ...., ,. .......a.�.. . . .�. . .. . Aroclor 1016 Rom��"IIL�`eZ x 40-1409 a 30 Aroclor 1260LZsY dye s n �as<�°Zz< 40-140 $ 30 LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Column 2,4,5,6-Tetrachloro-m-xylene 70 74 30-150 A Decachlorobiphenyl 61 65 30-150 A 2,45,6-Tetrachloro-m-xylene 71 72 30-150 B Decachlorobiphenyl 75 76 30-150 B Page 40 of 55 r '+ FHA t01220714:11 .f „ a ;y ..METALS , ' Page 41 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' SAMPLE RESULTS Lab ID: L0700683-02 Date Collected: 01/12/07 11:35 Client ID: BOTTOM Date Received: 01/15/07 ' Sample Location: HYANNIS, MA Field Prep: Not Specified Matrix: Soil Percent Solids: 97% ' Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst Tdtat Metats b�MCP`6QQOJ7lx0a�4°Se>1�s , u � , a )� � ' Arsenic,Total 2.0 mg/kg 0.40 1 01/18/07 17:00 01/19/07 10:05 EPA 3051 60,6010E Al Barium,Total 2.3 mg/kg 0.40 1 01/18/07 17:00 01/19/07 10:05 EPA 3051 60,6010E Al Cadmium,Total NO mg/kg 0.40 1 01/18/07 17:00 01/19/07 10:05 EPA 3051 60,601013 Al ' Chromium,Total 2.5 mg/kg 0.40 1 01/18/07 17:00 01/19/07 10:05 EPA 3051 60,6010E Al Lead,Total 3.4 mg/kg 2.0 1 01/18/07 17:00 01/19/07 10:05 EPA 3051 60,6010E Al , Mercury,Total ND mg/kg 0.08 1 01/18/07 20:00 01/19/07 14:30 EPA 7471A 64,7471A DM Selenium,Total ND mg/kg 2.0 1 01/18/07 17:00 01/19/07 10:05 EPA 3051 60,6010E Al Silver,Total ND mg/kg 0.40 1 01/18/07 17:00 01/19/07 10:05 EPA 3051 60,6010E Al ' t t ---'�dc••.va Page 42 of 55 ' ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number:,, L0700683 - Project Number: 7513 Report Date: 01/22/07 Method Blank Analysis Batch Quality Control Dilution Date Date Analytical ' Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst iota{Met�ls�by MCP 60�a171)U©.�s�rtes for sample{s}�.02 Batch xxldjG2679�4� " .,.�. Mercury,Total ND mg/kg 0.08 1 01/18/07 20:00 01/19/07 14:09 64,7471A DM 'Prep Information ' Digestion Method: EPA 7471A Dilution Date Date Analytical ' Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst �l,?�'�js:� 'ik��.f�•. I �t�Q���r�e;;,fo�af� ���'' - ` ��� ��.��'` ,�;`�`�> � ��.�� a¢��� � ��°s� ,� I, Arsenic,Total ND mg/kg 0.40 1 01/18/07 17:00 01/19/07 09:51 60,60108 Al Barium,Total No mg/kg- 0.40 1 01/18/07 17:00 01/19/07 09:51 60,60108 Al ' Cadmium,Total ND mg/kg 0.40 1 01/18/07 17:00 01/19/07 09:51 60,6010E Al Chromium,Total No mg/kg 0.40 1 01/18/07 17:00 01/19/07 09:51 60,6010E AI Lead,Total ND mg/kg 2.0 1 01/18/07 17:00 01/19/07 09:51 60,6010E AI Selenium,Total ND mg/kg' F2.0 1 01/18/07 17:00 01/19/07 09:51 60,6010B 'Al Silver,Total ND mg/kg 0.40 ` 1 `. 01/18/07 17:00 01/19/07 09:51 60,6010E Al, Prep Information- Digestion Method: . EPA 3051 I,L?I-ion° ' Page 43 of 55, 01220714:11 Lab Control Sample Analysis Project Name: CHAMPION BUILDERS Batch Quality Control Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits n}�� "x+`�". ��: L�.�'^C�tT .,. .a4' �'G".v � � Q.x ,..,.« ... e a _.<..y?. ,x k,e k.., k,�.:,«,•{a3c�xix x ,..,.�, +;".s5 w.„�„ x e s a 'i ... '.,..-e_.n:Y.:..*,.....��.:e.ix«...e.;- "d.x` ^�r.^.:-:��$a"r� .2�h�:`'xev�'.�sw,:..,.e,� �.r.�.ka,3a,:.,.,�.vr�FNe,,.,..t«'�Fmu...:..nuFk...w.�c1�.8�a.<..x�......<^._:f'r..esx:..<�5+vc.<..,.�ed.-a.:a��,.., Mercury,Totals ao: ssd 75-125 i � .._.... 30 - ->„.. :, .>•.w_.., 3�.. .�,.., ,.. .• �w.« w..-C:�.,...� «w;�....:;i. „< ...,4. e}FT 3 .a«, ,,pai:. �. •... .>^>..15 >.x: a .'F f! w2 , i `z'.-.t.,�:.,.» ....au.�'<«. ..'.«.::.:.:.... ....:.....:.,::«...:,F,....,-:...'3z.,:«,n3:.,�.,x:4.�<.:•.,..�.L'•.'�c,�^.:3:.v«..,..,.:,.,:wxxm_....Ka,�;:w.c.,.,,r..:..-a�..�.,:w....a,.a_-,ors'"S:Fa.,«�. -x..«,F..,,:wv...$,.�.->..-._v>.:..�r�....,.�.:E,. ..:.,,.fie,.,...'EF..«>.r._w� .:.,;c'.: ;::4_...:: .-..,,.,.... ,....>.. .,.. .. .,..... _..-.. Arsenic,Total F='z, ;�F , { °� 17 k 75-125 " 2 30 Barium,Total Asa n �lnSx c F .�}x° D 75-125 D a 30 -„_M.wz�,_ >....�.>. Cadmium, total ON _x�EF•x�x4�l)FStLx e1 tixsti'+c i"x�xe4as ^t5 _. 75-125 F+s:� ''„y--` 30 ,.<_:`' ?ma..a ,✓_..,,.,_ :s .�a_v-7kx; Chromium,Total xer OFFc $ x qa�„ 75-125 30 Lead,Total 75-125 x8 30 Selenium,Total F s<Sa9g4�1x ev < �9s F 75-125 r Q 'xh 30 Silver,Total 75-125 x< .Q 30 -�e3zse.,-�:;.a..:£ae. .,.w-. •aaFa ��..aa�.�.L.:,, -,:.<...,«,. ...:..._.. Page 44 of 55 ' 01220714:11 M�LSCEL.LAL EG� UaS 3Y 1 ' Page 45 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' SAMPLE RESULTS Lab ID: L0700683-01 Date Collected: 01/12/07 10:55 ' Client ID: ES Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Matrix: Soil ' Dilution Date Date Analytical ' (P aaramet/e'r Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Solids,Total 96 % 0.10 1 01/15/07 16:30 30,2540G PD ' t 1 1 HA Page Page 46 of 55 ' t01220714:11 Project Name: CHAMPION BUILDERS . Lab:Number: L0700683 Project Number: 7513 Report Date: 01/22/07 SAMPL"E'RESULTS ' Lab ID: L0700683-02 Date Collected: 01/12/07 11:35 Client ID: BOTTOM Date Received: 01/15/07 Sample Location: HYANNIS,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical ' Parameter Result Qualifier Units. RDL Factor. , Prepared Analyzed Method Analyst Solids,Total 97 % 0.10 .: 1 01/15/07 16:30 30,2540G PD y 1 r 1 s f Ah:��a ' Page 47 of 55 01220714:11 , Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 , SAMPLE RESULTS Lab ID: L0700683-03 Date Collected: 01/12/07 12:00 ' Client ID: COMP SW Date Received: 01/15/07 Sample Location: HYANNIS, MA Field Prep: Not Specified Matrix: Soil ' Dilution Date Date Analytical ' Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst �Yf✓1.Q1�herral;—.•J s ....._... ....., .._.:.. .. n. ��.. c ti.1... _ .... �..... .., .ry-. �.. ,.i ..a_.v.....?.a n ....,v... . .. 1. �...,..✓+�. .r..r..,.�.�w.� h �5 Solids,Total 93 % 0.10 1 01/15/07 16:30 30,2540G PD t HA Page Page 48 of 55 ' 01220714:11 Lab Duplicate Analysis Project Name: CHAMPION,BUILDERS s, Batch Quality Control Lab Number: L0700683 Project Number': 7513 Report Date: 01/22/07 Parameter Native Sample Duplicate Sample Units ROD RPD Limits Solids,Total 93 93 % 4` U 20 i LPHA Page 49 of 55 '/� 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L07OO683 Project Number: 7513 p P Report Date: 01/22/07 ' Sample Receipt and Container Information Were project specific reporting limits specified? YES , Cooler Information Cooler Custody Seal ' A Absent Container Information Container ID Container iner Type Cooler pH Temp Pres Seal Analysis ' L0700683-01A Vial McOH preserved A N/A 2.1C Y Absent MCP-8260H-04 L0700683-01B Vial water preserved A N/A 2.1C Y Absent MCP-8260H-04 , L0700683-01C Vial water preserved A N/A 2.1C Y Absent MCP-8260H-04 L0700683-01D Vial McOH preserved A N/A 2.1C Y Absent VPH-DELUX-04 ' L0700683-01E Amber 250ml unpreserved A N/A 2.1C Y Absent EPH-DELUX-04 L0700683-01 F Amber 250ml unpreserved A N/A 2.1C Y Absent TS P .1 Y Absent MCP-8260H-04 L0700683-02A Vial McOH reserved A N/A 2 C P ' L0700683-02B Vial water preserved A N/A 2.1C Y Absent MCP-8260H-04 L0700683-02C Vial water preserved A N/A 2.1 C Y Absent MCP-8260H-04 L0700683-02D Vial McOH preserved A NIA 2.1C Y Absent VPH-DELUX-04 ' L0700683-02E Amber250ml unpreserved A NIA. 2.1C Y Absent EPH-DELUX-04,MCP-8082-04 L0700683-02F Amber 250ml unpreserved A N/A 2.1C Y Absent MCP-7471T,MCP-AG- ' 6010T,MCP-AS-601 OT,MCP-BA- 601 OT,MCP-CD-6010T,MCP-CR- 601 OT,M C P-P B-601 OT,M C P-S E- 601OT,TS L0700683-03A Amber250ml unpreserved A N/A 2.1C Y Absent EPH-DELUX-04 ' L0700683-03B Amber 250ml unpreserved A N/A 2.1C Y Absent TS t I i'ALPHA Page 50 of 55 ' 01220714:11 Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' GLOSSARY . ' Acronyms EPA - Environmental Protection Agency.' . LCS - Laboratory Control Sample:A sample matrix,free from the analytes of interest, spiked with verified known amounts of analytes or a-material containing known and verified amounts of analytes. LCSD- Laboratory Control Sample Duplicate:'Refer to LCS. MS - Matrix Spike Sample:A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. MSD - Matrix Spike Sample Duplicate: Refer to MS. - ' NA - Not Applicable. NC - Not Calculated: Term is utilized when one'or'more of the results utilized in the calculation are ' non-detect at the parameter's reporting unit. ND - Not detected at the reported detection limit forthe sample. RDL --Reported Detection Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RDL includes any adjustments from dilutions, concentrations or moisture ' content, where applicable. RPD - Relative Percent Difference: The results'from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference(RPD). Values which are less than five times the reporting limit for any ' individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. Terms Analytical Method:Both the document from which:the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.)The codes for the,reference method documents are provided in the ' References section of the Addendum. ' Data.Qualifiers The following data qualifiers have been identified for use under the CT DEP Reasonable Confidence Protocols. ' A-Spectra identified as"Aldo) Condensation Product". B The analyte was detected above the reporting limit in"the associated method blank. Flag only applies to associated field samples.that have detectable concentrations.of the analyte. E-Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. ' J -Estimated value.The analyte was tentatively identified;the quantitation is an estimation. (Tentatively identified compounds only.) ' Report Format: Not Specified L10HA Page 51 of 55 01220714:11 ' Project Name: CHAMPION BUILDERS Lab Number: L0700683 Project Number: 7513 Report Date: 01/22/07 ' REFERENCES 30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-WPCF. ' 18th Edition. 1992. 59 Method for the Determination of Volatile Petroleum Hydrocarbons(VPH). Massachusetts , Department of Environmental Protection, DEA/ORS/BWSC. May 2004, Revision 1.1. 60 Quality Assurance and Quality Control Requirements and Performance Standards for SW- ' 846 Methods. MADEP BWSC.WSC-CAM-IIA(Revision 4),WSC-CAM-V C(Revision 2), WSC-CAM-IIIA(Revision 5). May 2004. 61 Method for the Determination of Extractable Petroleum Hydrocarbons(EPH). Massachusetts ' Department of Environmental Protection, DEA/ORS/BWSC. May 2004, Revision 1.1. 64 Quality Assurance and Quality Control Requirements and Performance Standards for SW- 846 Methods. MADEP BWSC.WSC-CAM-IIA(Revision 4),WSC-CAM-V C(Revision 2), ' WSC-CAM-IIIA(Revision 5).August 2004. LIMITATION OF LIABILITIES Alpha Woods Hole Labs performs services with reasonable care and diligence normal to the analytical testing ' laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Woods Hole Labs shall be to re-perform the work at it's own expense. In no event shall Alpha Woods Hole Labs be held liable for any incidental,consequential or special damages, including but not limited to, damages in any way ' connected with the use of, interpretation of, information or analysis provided by Alpha Woods Hole Labs. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. ' Page 52 of 55 ' CHAIN OF CUSTODY PAGE�OF� Date Rec'd in Lab: - /I i ALPHA Job i ALPHA w0 eaf.D:r °♦ri ` i Project Information Report Information-Data Deliverables Billing Information I WEST8ORO.MA RAYNHAMNA 508-898-9220;g+ TEL:508-822-9300 -�„ ° 7 FAX:50B•898-9193°'•Y FAX:50e-822-3288: ''rr„v ?• -`•� Project Name:C -w ��� y 1 s ❑FAX MAIL _ _. -_ .--_-.. O_#:�1 _71713 pJ aIg ❑Same as Client info P t` S 1 �ADEx El Deliverables N Information Project Location: j nos l /t lV - -.... Regulatory RequirementsReport Limitso Client' Project#— '75 j--1 -- _ V _A - ,C 1 1- State/Fed-Program Criteria Address:. , �. AIv � ! T1 Project Manager: t�e �AA (11�- ALPHA Quote#: MA MCP PRESUMPTIVE CERTAINTY---CT REASONABLE CONFIDENCE PROTOCOLS IP-hone: 11CV Ol - ' es ❑No Are MCP Analytical Methods Required? ❑Yes ❑No Are CT RCP(Reasonable Confidence Proto,ols)Required? !Fax: 1 j} p b _ -- - - /V ` -/ -�V1 �� Standard ❑RUSH(."y-f-drr,a-a—edn Email: I._�-1L`+� t�i' 5a /t@� f / ate Due: Time: y / / / SAMPLEHANDLING ❑ These samples have been previously analyzed by Alpha 49 S`�(r Vir - - -- -- — - — --- _ �' /� / Q/ i Filtration Other Project Specific Requirements/Comments/Detection Limits: Q i El Done 1 / /' G;'� �%r ld J /'/ �flot needed ^ C % / ❑Lab to do , Preservation / r. 1 V• ! / i (Please specify below) y3 , ALPHA Lab"ID''"' Collection , ; .Sample Sampler's !/ SamplelD trix a k � � l*i f ` i°` Sample Specific Comments (Lab Use Only) Date Time r lniti I 2 a` _. —.. X .. _ j l PLEASEANSWEROUESTIONS ABOVEI Container Type A _ 'Please print clearly,legibly and Preservative A �( l<completely. Samples can not be YOUR PROJECT - turnaround m ReLqu!,Td y *' Date/Tlme - Received By: F any ambiguiti U)logged in and tur clock les MA M or CT RCP? , > an, 'l3�) � t ��D.tr�subJe Ito Alpha s pPaym nt TQmsf e 'I L: I /'a.Q See reverse side: (FORM NJ:Oi-Ot(rev.10-OCT-05) LO a CHAIN OF CUSTODY PAGE---t-OF J— Date Reed In Lab: ALPHA Job ALPHA #: .•....s., ,.,. e Deliverables r/EST80R0,}AA RAYNFAMMA Project TEL!soe-ere-922e TEL:sted Project 2z-9300 Pct Name 4 FAX MAIL 0 Some as Cl'lent YAo PO H�'� 1SI� Q W.:saearearea FAX:ste-azz3zee (d _M!C/ ------ r- . . Project Locaton A NN E �� p ADE� O Add! Deliveebtes CV Reg ulatc,ryReq (V :lien!: Project r4: t'?) o Q __... - -- Stale/Fed Program Criteria \ddress - 2� ' Project Manager 1 MICfI/ l - _ - - --- - � l F(7 ALPHA Quote IM: • t • e • • • —�.._ 'hone: �OjLfa gop • CYes O No Are NCP Analytical Methods Required? r'08 /�� _ O Yes ❑No Are CT RCP(Reasonable Confidence Protocols)Required? am:�� W andard a RUSH —.h �dAe.-.J,,,,,,rs w$ Date Due: Time: J/ //SAMPLEtiANDLING ] These sample;have bean previously anelyLed by Alpfie { F none Other Project Specific Requirements/Comments/Detection Limits: o oone J �#lol needed / ❑Lab to do , / Preserealion / O Lab to do ALPI�ALab 110 Collection Sample s e�' (Lab Use Onty► SamplelD Dale lime Matrix r O �q Sarnale SpecificCommenis -- -� - - - -------- - -- - - - - - `EASEANSWERQUESTIONSABOVEI Container Type J JklikPlease print dearly,legibly and Preservative completely. Samples asn not be 1U R PROJECT logged In and turnaround time clock Relinquished By: Date:Time Receh*d By: Dalernme will not start until any amblguites are OI CT RCP? -,$-y resolrad. All samplessubmilledare LO t"xid `Q�' I JrJ� __ subject to Alpha's Pa/marl Terms. LO _T -- - - -_ -- -- See reverse side. o ,�-- - - — M m d ' 01220714:11 Alpha Analytical Labs Sample Delivery Group Form ' I 3 Reviewer Revi Laboratory Job No. L, SDG e Client: Date/Time: 5 �_ ' Preliminary Review 1. Samples Delivered via: 2. Chain of Custody: 3. Custody Seal: 41A-11ph,Courier ❑Express Mail Present Absent ❑Client ❑Other ❑Absent ❑Present/Intact 3. All Containers Accounted for El Present/Broken : Yes ❑No ' 4. Sam les received: Intact ❑Extra: ' ❑spoken Sample IDs ❑Leaking Sample IDs : . t5. Temperature Blank: Present Temperature(in Celsius): =6'Celsius degrees ' ❑other l ❑Absent Is th ice blue ice) present? P�71 Cooler Temp: ❑No* Secondary Review �� s `�^ 1� 0 /8 1. Do-the samples)°labels and Chair'of Custody agree? Pes ❑No 2. Are the samples in appropriate containers? Ep s []No ' 3. Are the samples properly preserved? !_es ❑No* Initial pH= Preserved In-House wl ' 4. Are thEj samples within hold; ti s? V s . No* ' * Contact client and attach the phone log ' Form No.:0 1-02 uUunzuus Page 55 of 55 1 ' Massachusetts Department otEnvironmental Protection BWSC-012A Bureau of Waste Site Cleanup + Release Tracking Number* BILL OF LADING (pursuantto 310 CMR 40.0030) 1 A. LOCATION OF SITE OR DISPOSAL SITE WHERE REMEDIATION WASTE WAS GENERATED: ' Release Name(optional), Law Offices of-'John Manoog Street: 450 South Street Location Aid: City/Town: Hyannis ZIP Code: 02601 ' Date/Period of Generation: 1/11/2 0 0 7 to: 1/12/2 0 0'7 Additional Release Tracking Numbers Associated with this Bill of Lading: t *Note If this Bill of Lading is the result of a Limited Removal Action(LRA) taken prior to Notification, a Release Tracking Number is not needed. B. PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF LADING: Name of Organization: Law Offices of John Manoog ' Name of Contact: John Manoog Title: Attorney Street: 450 South Street Hyannis - MA 02601 City/Town: State: ZIP Code: 1 Telephone: 508 775-0088 Ext.: C. RELATIONSHIP TO RELEASE OF PERSON CONDUCTING RESPONSE'ACTION ASSOCIATED WITH BILL OF LADING: ® RP or PRP Specify: ® Owner ❑ Operator ❑ Generator T] Transporter Other RP or PRP: ' ❑ Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.'21 E,s.2) ❑ Agency or Public Utility on a Right of Way(as defined by M.G.L.c 21 E,s.50)) " ❑ Other.Person: " ' If an owner and/or operator is not conducting the response actioA associated with the Bill of Lading,provide on an attachment the name, contact person,address and telephone number,including any area code and extension,for each,if known. D. TRANSPORTER OR COMMON CARRIER INFORMATION:: Transporter/Common Carrier Name: Enviro-Safe Corporation Contact Person: Heather Atwood k Title: General Manager Street: 14B Jan Sebastian Drive , 1 Sandwich `, MA 02563 City/Town: State: ZIP Code: Telephone: (5 0 8) 8 8 8-5 4 7 8 Ext.: E. RECEIVING FACILITY/TEMPORARY STORAGE LOCATION: Operator/Facility Name: Aggregate. Industries ° Contact Person: William Reinhardt Title: Manager ' Street: 230 Great Western Road South Dennis .� ZIP Code: 02660 City/Town: State: ' Telephone: (5 0 8) 3 41-5 5 0 0 Ext.. Type of Facility: Asphalt Batch/Cold Mix Landfill/Disposal Incinerator Temporary Storage (check one) Asphalt Batch/Hot Mix ❑,Landfill/Daily Cover ❑ Other: Thermal'Processing Landfill/Structural Fill .f ' � EPA Identification#: Division of Hazardous Waste/Class A Permit#: S-01-0 2 7 Division of Solid Waste Management Permit#: MAD 9 8 5 2 8 6 3 8 4 ' Actual/Anticipated Period of Temporary Storage(specify dates if applicable): to: Reason for Temporary Storage: Revised 10/3/94 Page 1 of 3 Massachusetts Department of Environmental Protection BWSC-012A Bureau of Waste Site Cleanupl� + Release Tracking Number* ' BILL OF LADING (pursuant to 310 CMR 40.0030) LRA E. RECEIVING FAC(LITY/rEMPORARY STORAGE LOCATION(continued): ' Temporary Storage Address: Street: r.. City/Town: State: ZIP Code: ' F. DESCRIPTION OF REMEDIATION WASTE: (check all that apply) Contaminated Media(check all that apply): Soil .0 Groundwater 0 Surface Water 0 Other:_ ' o Contaminated Debris(check all that apply): 0 Vegetation,or Organic Debris Demolition/Construction Waste 0 Inorganic Absorbent Materials 0 Other: Non-hazardous Uncontainerized Waste(check all that apply): '0 Non-aqueous Phase Liquid 0 Other ' ❑ Non-hazardous Containerized Waste(check all that apply): O- Tank'Bottoms/Sludges 0 Containers 0 Drumsk 0 Engineered Impoundments O. Other ' Type of Contamination(check all that apply): �'Gasoline, .,Diesel Fuel. #2 Oil E] #4 Oil #6 Oil Waste Oil Kerosene 0 Jet Fuel 0 Other. ' Estimated Volume of Materials: .Cubic Yards: 10 Tons: Other: Contaminant Source(check one/specify): 11 Transportation Accident, ; E1 Underground Storage Tank Other: OWs Response Action Associated with Bill of Lading(check one): E] Immediai4'Response Action El Release Abatement Measure ' Utility-Related Abatement Measure WJ Limited Removal Action Comprehensive Response Action Other " Remediation Waste Charcterization Support Documentation attached Site History Information Sampling and Analytical Methods and Procedures Laboratory Data Field Screening Data If supporting documentation is not appended,provide an attachment stating thedate and in connection with what document such information was previously submitted to DER ' G. LICENSED SITE PROFESSIONAL(LSP)OPINION Name of Organization: Enviro-Safe Corporation LSP Name: Robert Berger 'Title: Technical Services Manager ' Telephone: (508) 634-9800 Ext.: I attest under the pains and penalties of perjury that I have personally examined and am familiar with this submittal, including any and all documents ' accompanying this submittal. In my professional opinion and judgment based upon application,of (i)the standard of care in 309 CMR 4.02(1), (ii)the applicable provisions of 309 CMR 4.02(2)and(3),and ' (iii)the provisions of 309 CMR 4.03(5), % to the best of m,y knowledge,information and belief,the assessment actions undertaken to characterize the Remediation Waste which is(are)the subject of this submittal for acceptance at the facility identified in this submittal comply with the applicable provisions of 310 CMR 40.0000,and such facility is permitted to accept Remediation Waste having the characteristics described in this submitta).+N.:Aarn,aq%are that significant penalties may result, ' including;but not Ii ,possible fines and,imprisonment,if I submit inbrmation which I kpbwto be false inaccurate or materially incomplete. ;7 alp 3' LSP Signature: Seal: a �I Date: License Number: Y'ri v J J V Revised 10/3/94 Page 2 of 3 01/08/2007 14:01 FAX 5087750176 0 008 ' . Protection sWSG-D1 ZA MassachUrwtts Department of Environmental Bureau of Waste Site Cleanup- Rime2se Tfaanng Number ' BILL OF LADING(pursuant to 310 CMR 40.0030) 1 M. CF.RTIFICATION 01:PSRSON CONDUCTING KMNSIS ACTION ASSOCIATED VOW THIS 8II.1.OF LADING: I certify under pew of law that t have personally milted and am%Shier whit tfl@ mfprtn2lion ootttdined In Sibt boor obmtn g int IncludIng h offman,me aocumerds acaen►PanYav - caruecaeen,and drat based on my inquiry of tease lr*w* %imm�layeryr recpon h is,Sp the 4�t Of my knowledge and bellef,true,awjWe and wmplele. f am a*aee that tllere ant signiflCant ffmwdai irdormeBon or incron+Wele inforrnatian. ' penaitlas.Including.but not ta,poesltde fin4S 8nd imptis°nmi for willfully submitting%Ise.inewmate, Signs4ire; Data: 0 , Name of Person(Prft • i F i - Page 3 of 3 ' Revised 900% Massachusetts Department of Environmental Protection BWSC-0129 ' Bureau of Waste Site Cleanup BILL OF LADING(pursuant to.310 CMR 40.11030) Release Tracoring Number ' SUMMARY SHEET OF I. LOAD INFORMATION: Sign71� /� o/� r Load 1: ' f h i'Receiving Faaldy � Representative: Storage Repentative: � i ' Date of Shipment � Time of Shipment. •�°:, ..� J��`�;/C� / -f Z- - / / :• L, l Date of Receipt Time of Recei t AM ❑ PM' is F AM PM Trudcrrra cjR;Reg istratlon: Trailer Registration(if any): i�."�L ��7'� r/� b ❑ r Load Size(cu,ydeJtone): (,r )/^ Load 2: Signatiure of Transporter Representative: 1 RecelvI Faci Re �8 ib mP Storege F?eprtbentative: i Date of Shipnnent; Time of Shipment: []'AM ❑ PM Date of Receipt: Time of Receipt: ' [:] AM ❑ PM. Truck/Tractor Registration: Trailer Registration(d any): 1 i f .Toad Size(cu.yds.Rons): i Load 3: Signaatiure of Transporter Representative: Receiving Faditty/r"rery Storage Representative: Date of Shipment: Time of Shipment: ❑ AM PM i Date of Receipt ' � H Time of Receipt: 1 ❑ AM ❑ PM.' 7ruck/'Tractor Registration; Trailer Re9isbati0n(if any): 1 . 1 Load Size(Cu.ydsitons): { Load 4: Signatiure of Transporter Representative: i i Receiving Facilityrremporary Storage Representative: i ' Date of Shipment; Trine of Shipment t -Date of Receipt: Time of Receipt: ❑ AM ❑ PM i ❑ AM ❑ PM Truclu Tractor Registration: Trailer Registration(if any): i t I Load,Size(cu.ydsJtons): Load 5: Signature of Transporter Representative: p ceiving Facility/remporary Storage Representative: 4 Gate of Shipment: Time of Shipment: t pate of Receipt Time of Receipt: ❑ AiM ❑�PM i ., ❑ AM ❑ PM ' Truck.Tractor Registration: Trailer R stration if an 1 egi ( any): 1 Load Sae(Cu.ydsAons): Load 6: Signatiure of Transporter Representatm: i Receiving Fadlity/rempoy"Storage Representative: r• Date of Shipment; Time of Shipment Date of Recelpt Time of Receipt ❑.AM ❑ PM i ❑ AM ❑ PM Ttudrfrractor Registration: Trailer Registration(if airy): i Load Size(cu.yds,rmns); J. LOG SHEET.VOLUME INFORMATION: Total Volume Recorded This Page(cu.y&,Aons) Total Carried Forward(cu.yds,/oorrs); - ' Total Carried Forward and This Page(cu.yd"ns): nAvlsed 10/3/94 Page 1 of 1 Massachusetts Department of Environmental Protection BWSC-012C Bureau of Waste Site Cleanup ' BILL OF LADING(pursuant to 310 MR 40.0030) Release Tracking Number SUMMARY SHEET OF_ - K. SUMMARY OF SHIPMENTS: _. Daily Volume Shipped ' Date of Shipment: Date of Receipt: Number of Loads Shipped: (cu.yds Iton� : e a Summary Sheet Total Shipped: Bill of Lading Total Shipped � --- ------------ _ --- -- ' (only if different): Revised 10/3/94 Page 1 of 2 Massachusetts Department of Environmental Protection BWSC-012C Bureau of Waste Site Cleanup BILL OF LADING(pursuant to 310 CMR 40.0030 Release Tracking Number SUMMARY SHEET _L ONLY COMPLETE ONE COPY OF THIS PAGE AND ATTACH TO THE FINAL COPY OF THE SUMMARY SHEET. L. ACKNOWLEDGMENT OF RECEIPT OF REMEDIATION WASTE AT.RECEIVING FACILITY OR TEMPORARY STORAGE: Receiving Facility/Temporary Storage Representative(print); ;< William R. Reinhardt Title: Manager ' --- � ,,// ---- ---- --�7 ----------- ate: Signature: — ------ M. ACKNOWLEDGMENT OF SHIPMENT AND RECEIPT OF REMED / ION WASTE BY PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING: I certify under penalties of law that I.ave personally examined and am familiar with the information contained in this submittal,including any and all ' documents accompanying this ce cation,and that,based on my inquiry of those individuals immediately responsible for obtaining the information,the , material information contained in er m is,to the best of my knowledge and belief,true,accurate and complete, I am aware that there are significant penalties,including,but not Iirn d t possible fines and imprisonment,for willfully submitting false,inaccurate,orincomplete information. Signature: Date: Name of Person(print): - A n Revised 10/3194 Page 2 of 2 4 2Q0-6 DEC 14 PN 3* 41 GwLabs,Inc. Monday, December 11, 2006 007L EO GeoLabs, Inc. 45 Johnson Lane John Bailey Braintree MA 02184 Enviro-Safe Corp. Tele: 781 848 7844 31 Granite Street, Suite 8 Fax: 781 848 7811 Milford, MA 01757 TEL: (508) 634-9800 FAX: (508) 634-8259 Project: 7513. - Location: C450 South St, Hyannis, MA Order No.: 0612023 Dear John Bailey: GeoLabs, Inc. received 1 sample(s) on 12/4/2006 for the analyses presented in the following report. There were no problems with the analyses and all data for associated QC met EPA or laboratory specifications. Analytical methods and results meet requirements of 310CMR 40.1056(J) as per MADEP Compendium of Analytical Methods (CAM)., If you have any questions regarding these tests results, please feel free to call. Sincerely, Jim Chen 'Laboratory Director AN p GeoLabs, Inc. Date: 11-Dec-06 CLIENT: Enviro-Safe Corp. Project: 7513 CASE NARRATIVE Lab Order: 0612023 MADEP MCP Response Action Analytical Report Certification Form Laboratory Name: GeoLabs, Inc. Project#7513 Project Location: 450 South Street,Hyannis MA MADEP RTN#: This form provides certification for the following data set: 0612023-001 Sample Matrix: Soil MCP SW-846 Methods Used: EPH,VPH, 6010B, 7471A An affirmative answer to questions A,B and C are required for "Presumptive Certainty" status A. Were all samples received by the laboratory in a condition consistent with that described on the Chain of custody documentation for the data set? YES B. Were all QA/QC procedures required for the specified method(s) included in this report followed,including the requirement to note and discuss in a narrative QC data that did not meet appropriate standards or guidelines? YES C. Does the analytical data included in this report meet all the requirements for"Presumptive Certainty" as described in Section 2.0 of the MADEP documents CAM VII A "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? YES D.VPH and EPH Methods only: Was the VPH or EPH Method conducted without significant modifications(see Section 11.3 of respective Methods) YES A response to questions E and F are required for"Presumptive Certainty" status E. Were all QC performance standards and recommendations for the specified methods achieved? YES F. Were results for all analyte-list compounds/elements for the specified method(s)reported? YES All NO answers need to be addressed in an attached Environmental Laboratory case narrative. GeoLabs,Inc. Date: 11-Dec-06 CLIENT: Enviro-Safe Corp. Project: 7513 CASE NARRATIVE Lab Order: 0612023 CASE NARRATNE Physical Condition of Samples The project was received by the laboratory in satisfactory condition. The sample(s)were received undamaged, in appropriate containers with the correct preservation. Project Documentation The project was accompanied by satisfactory Chain of Custody documentation. Analysis of Sample(s) No analytical anomalies or non-conformances were rioted by the laboratory during the processing of these samples. I,the undersigned, attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is,to he best of my knowledge and belief, accurate and complete. Signature: Position: Lab Director Printed Name. Jim Chen Date: 12/11/06 GeoLabs,Inc. Date: 11-Dec-06 CLIENT: Enviro-Safe Corp. Project: 7513 Lab Order: 0612023 EPH Methods Method for Ranges: MADEP EPH 04-1.1 Method for Target Analytes: 8270 GC/MS Carbon Range data exclude concentrations of any surrogate(s) and/or internal standards eluting in that range C I 1-C22 Aromatic Hydrocarbons exclude concentrations of Target PAH Analytes CERTIFICATION: Were all QA/QC procedures REQUIRED by the EPH Method followed? YES Were all performance/acceptance standards achieved? YES Were any significant modifications made to the EPH method? NO I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. SIGNATURE: L LAB DIRECTOR PRINTED NAME: Jim Chen DATE: 12/11/06 GeoLabs,Inc. Date: 11-Dec-06 CLIENT: Enviro-Safe Corp. Project: 7513 Lab Order: 0612023VPH Methods Method for Ranges: MADEP VPH 04-1.1 Method for Target Analytes: MADEP VPH 04-1.1 Carbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range: (MTBE,Benzene, Toluene) C9-C12 Aliphatic Hydrocarbons exclude concentration of Target Analytes eluting in that range (Ethylbenzene,m&p-Xylenes,o-Xylene)AND concentration of C9-C10 Aromatic Hydrocarbons. CERTIFICATION Were all QA/QC procedures REQUIRED by the VPH Method followed? YES Were all QA/QC performance/acceptance standards achieved? YES Were any significant modifications made to the VPH method,as specified in Sec. 11.3? NO I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge,accurate and complete. SIGNATURE: POSITION: LAB DIRECTOR PRINTED N Jim Chen DATE: 12/11/06 GeoLabs, Inc. Date: 11-Dec-06 Original Date Reported: 11-Dec-06 CLIENT: Enviro-Safe Corp. Client Sample ED: S-1 Lab Order: 0612023 Collection Date: 12/1/2006 Project: 7513 Date Received: 12/4/2006 Lab ED: 0612023-001 Matrix: SOIL Analyses Result DeL Limit Qual Units DF Date Analyzed EPH RANGES MADEP EPH (MADEP EPH) Analyst: KH Adjusted C11-C22 Aromatics 227 10.8 mg/Kg-dry 1 12/5/2006 C09-C18 Aliphatics 455 53.8 mg/Kg-dry 5 12/5/2006 C19-C36 Aliphatics 386 10.8 mg/Kg-dry 1 12/5/2006 Unadjusted C11-C22 Aromatics 228 10.8 mg/Kg-dry 1 12/5/2006 Surr:1-Chlorooctadecane 72.0 40-140 %REC 1 12/5/2006 Sun.c-Terphenyl 104 40-140 %REC 1 12/5/2006 TOTAL SILVER SW6010B (305013) Analyst: BF Silver NO 1.05 mg/Kg-dry 1 12/4/2006 MERCURY SW 7471A (SW7471A) Analyst: BF Mercury NO 0.0978 mg/Kg-dry 1 12/6/2006 RCRA METALS W/O HG SW6010B (SW3050B). Analyst: CIS Arsenic NO 7.19 mg/Kg-dry 1 12/5/2006 Barium 29.3 3.70 mg/Kg-dry 1 12/5/2006 Cadmium ND 1.54 mg/Kg-dry 1 12/5/2006 Chromium 8.42 7.46 mg/Kg-dry 1 12/5/2006 Lead 104 9.00 mg/Kg-dry 1 12/5/2006 Selenium ND 7.80 mg/Kg-dry 1 12/5/2006 EPH TARGET ANALYTES MADEP EPH_P (EPH_SPR) Analyst: ZYZ Naphthalene NO 0.0538 mg/Kg-dry 1 1217/2006 4:06:00 PM 2-Methylnaphthalene 0.916 0.0538 mg/Kg-dry 1 12/7/2006 4:06:00 PM Acenaphthene NO 0.108 mg/Kg-dry 1 12/7/2006 4:06:00 PM Phenanthrene NO 0.0538 mg/Kg-dry 1 1217/2006 4:06:00 PM Acenaphthylene NO 0.0538 mg/Kg-dry 1 1217/2006 4:06:00 PM Fluorene NO 0.0269 mg/Kg-dry 1 12/7/2006 4:06:00 PM Anthracene NO 0.0538 mg/Kg-dry 1 1217/2006 4:06:00 PM Fluoranthene NO 0.215 mg/Kg-dry 1 12/7/2006 4:06:00 PM Pyrene NO 0.215 mg/Kg-dry 1 12/7/2006 4:06:00 PM Benzo(a)Anthracene NO 0.108 mg/Kg-dry 1 12/7/2006 4:06:00 PM Chrysene NO 0.108 mg/Kg-dry 1 12/7/2006 4:06:00 PM Benzo(b)Fluoranthene ND 0.161 mg/Kg-dry 1 12/7/2006 4:06:00 PM Benzo(k)Fluoranthene NO 0.108 mg/Kg-dry 1 12/7/2006 4:06:00 PM Benzo(a)Pyrene ND 0.108 mg/Kg-dry 1 12/7/2006 4:06:00 PM Indeno(1,2,3-cd)Pyrene NO 0.0538 mg/Kg-dry 1 12/7/2006 4:06:00 PM Dibenz(a,h)Anthracene NO 0.108 mg/Kg-dry 1 12/7/2006 4:06:00 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit S Spike Recovery outside accepted recovery limits 4 Page 1 of 2 GeoLabs,Inc. Date: 11-Dec-06 Original Date Reported: { CLIENT: Enviro-Safe Corp. Client Sample ID: S-1 Lab Order: 0612023 Collection Date: 12/1/2006 Project: 7513 Date Received: 12/4/2006 Lab ID: 0612023-001 Matrix: SOIL Analyses Result Det.Limit Qual Units DF Date Analyzed EPH TARGET ANALYTES MADEP EPH_P (EPH_SPR) Analyst: ZYZ Benzo(g,h,i)Perylene ND 0.108 mg/Kg-dry 1 12/7/2006 4:06:00 PM Total PAH Target Concentration 0.916 0 mg/Kg-dry 1 12/7/2006 4:06:00 PM Surr:2,2'-Difluorobiphenyl 71.4 40-140 %REC 1 12/7/2006 4:06:00 PM Surr:2-Fluorobiphenyl 75.1 40-140 %REC 1 12/7/2006 4:06:00 PM VOLATILE PETROLEUM HYDROCARBONS VPH Analyst: MR Adjusted C5-C8 Aliphatic ND 6.99 mg/Kg-dry 1 12/8/2006 Hydrocarbons Adjusted C9-C12 Aliphatic 13.8 6.99 mg/Kg-dry 1 12/8/2006 Hydrocarbons Benzene ND 0.538 mg/Kg-dry 1 12/8/2006 C9-Cl0 Aromatic Hydrocarbons 4.05 1.61 mg/Kg-dry 1 12/8/2006 Ethylbenzene ND 0.538 mg/Kg-dry 1 12/8/2006 m,p-Xylene ND 0.538 mg/Kg-dry 1 12/812006 Methyl Tert-Butyl Ether ND 0.108 mg/Kg-dry 1 12/8/2006 Naphthalene ND 1.08 mg/Kg-dry 1 12/8/2006 o-Xylene ND 0.538 mg/Kg-dry 1 12/8/2006 Toluene ND 0.538 mg/Kg-dry 1 12/8/2006 Unadjusted C5-C8 Aliphatic ND .6.99 mg/Kg-dry 1 12/8/2006 Hydrocarbons Unadjusted C9-C12 Aliphatic 17.9 6.99 mg/Kg-dry 1 12/8/2006 Hydrocarbons Surr 1,2-Dichloroethane-d4 96.2 70-130 %REC 1 12/8/2006 Surr:2,5-Dibromotoluene 99.6 70-130 %REC 1 12/8/2006 Surr:Bromofluorobenzene 101 70-130 %REC 1 12/8/2006 Surr:Toluene-d8 121 70-130 %REC 1 12/8/2006 Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit S Spike Recovery outside accepted recovery limits Page 2 of 2 GeoLabs, Inc. Date: 11-Dec-06 CLIENT: Enviro-safe Corp. ANALYTICAL QC SUMMARY REPORT Work Order: 0612023 Project: 7513 BatchID: 6011 Sample ID: MB-6011 SampType: MBLK TestCode: 6010b_S Units: mg/Kg Prep Date: 12/5/2006 RunNo: 14073 Client ID: 777.77 Batch ID: 6011 TestNo: SW6010B (SW3050B) Analysis Date: 12/5/2006 SegNo: 122849 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Arsenic ND 7.00 Barium ND 3.60 Cadmium ND 1.50 Chromium ND 6.90 Lead ND 8.76 Selenium ND. 7.59 Sample ID: LCS-6011 SampType: LCS TestCode: 6010b_S Units: mg/Kg Prep Date: 12/5/2006 RunNo: 14073 Client ID: 77777 Batch ID: 6011 TestNo: SW6010B (SW3050B) Analysis Date: 12/5/2006 SegNo: 122850 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Arsenic 113.3 7.00 133.3 0 85.0 75 125 Barium 122.7 3.60 133.3 0.08667 91.9 75 125 Cadmium 112.0 1.50 133.3 0 84.0 75 125 Chromium 113.3 6.90 133.3 0 85.0 75 125 Lead 112.7 8.76 133.3 0 84.5 75 125 Selenium 110.7 7.59 133.3 2.06 81.5 75 125 Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits ts ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery Iii Page 1 of I s Date: 11-Dec-06 GeoLabs, Inc. CLIENT: Enviro-safe Corp. ,,ANALYTICAL QC SUMMARY REPORT Work Order: 0612023 P TestCode: AG_S Project: 7513 Sample ID: MS-6002 SampType: MBLK TestCode:AG S Units: mg/Kg Prep Date: 12/412006 RunNo: 14031 Client ID: 77777 Batch ID: 6002 TestNo: SW6010B (3050b) Analysis Date: 12/4/2006 SegNo: 122517 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Silver ND 1.00 Sample ID: LCS-6002 SampType: LCS TestCode: AG_S Units: mg/Kg Prep Date: 1 2/4120 0 6 RunNo: 14031 Client ID: 777.77 Batch ID: 6002 TestNo: SW6010B (3050b) Analysis Date: 12/4/2006 SegNo: 122518 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Silver 5.900 1.00 6.66 0 88.6 80 120 Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded 1 Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Page 1 of 6 I CLIENT: Enviro-Safe Corp. ANALYTICAL QC SUMMARY REPORT Work Order: 0612023 Project: 7513 TestCode: EPHP_S Sample ID: MB-6006 SampType: MBLK TestCode: EPHP_S Units: mg/Kg Prep Date: 12/5/2006 RunNo: 14081 Client ID: 7777 Batch ID: 6006 TestNo: MADEP EPH_ (eph_Spr) Analysis Date: 12/5/2006 SegNo: 122930 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Naphthalene ND 0.0500 2-Methylnaphthalene ND 0.0500 Acenaphthene ND 0.100 Phenanthrene ND 0.0500 Acenaphthylene ND 0.0500 Fluorene ND 0.0250 Anthracene ND 0.0500 Fluoranthene ND 0.200 Pyrene ND 0.200 Benzo(a)Anthracene ND 0.100 Chrysene ND 0.100 Benzo(b)Fluoranthene ND 0.150 Benzo(k)Fluoranthene ND 0.100 Benzo(a)Pyrene ND 0.100 Indeno(1,2,3-cd)Pyrene ND 0.0500 Dibenz(a,h)Anthracene ND 0.100 Benzo(g,h,i)Perylene ND 0.100 Total PAH Target Concentration ND 0 Surr:2,2'-Difluorobiphenyl 4.056 0 5 0 81.1 40 140 Surr:2-Fluorobiphenyl 3.852 0 5 0 77.0 40 140 Sample ID: LCS-6006 SampType: LCS1 TestCode: EPHP_S Units: mg/Kg Prep Date: 12/5/2006 RunNo: 14081 Client ID: 77777 Batch ID: 6006 TestNo: MADEP EPH_(eph_Spr) Analysis Date: 12/5/2006 SegNo: 122931 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Naphthalene 2.242 0.0500 5 0 44.8 40 140 2-Methylnaphthalene 2.474 0.0500 5 0 49.5 40 140 Acenaphthene 2.668 0.100 5 0 53.4 40 140 Phenanthrene 3.172 0.0500 5 0 63.4 40 140 Acenaphthylene 2.360 0.0500 5 0 47.2 40 140 Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Page 2 of 6 CLIENT: Enviro-safe Corp. ANALYTICAL QC SUMMARY REPORT Work Order: 0612023 TestCode: EPHP_S Project: 7513 Sample ID: LCS-6006 SampType: LCS1 TestCode: EPHP_S Units: rng/Kg Prep Date: 12/5/2006 RunNo: 14081 Client ID: 7777 Batch ID: 6006 TestNo: MADEP EPH_ (eph_Spr) Analysis Date: 12/5/2006 SegNo: 122931 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit .Highlimit RPD Ref Val %RPD RPDLimit Qual Fluorene 2.694 0.0250 5 0 53.9 40 140 Anthracene 3.290 0.0500 5 0 65.8 40 140 Fluoranthene 3.246 0.200 5 0 64.9 40 140 Pyrene 2.194 0.200 5 0 43.9 40 140 Benzo(a)Anthracene 2.748 0.100 5 0 55.0 40 140 Chrysene 5.670 0.100 5 0 113 40 140 Benzo(b)Fluoranthene 3.978 0.150 5 0 79.6 40 140 Benzo(k)Fluoranthene 2.824 0.100 5 0 56.5 40 140 Benzo(a)Pyrene 2.826 0.100 5 0 66.5 40 140 Indeno(1,2,3-cd)Pyrene 2.768 0.0500 5 0 55.4 40 140 Dibenz(a,h)Anthracene 2.824 0.100 5 0 56.5 40 140 Benzo(g,h,i)Perylene 2.930 0.100 5 0 58.6 40 140 Total PAH Target Concentration 50.91 0 Sum 2,2'-Difluorobiphenyl 3.942 0 5 0 78.8 40 140 Surr.2-Fluorobiphenyl 3,590 0 5 0 71.8 40 140 Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Page 3 of 6 CLIENT: Enviro-Safe Corp. ANALYTICAL QC SUMMARY REPORT Work Order: 0612023 TestCode: EPHT_S Project: 7513 Sample ID: MB-6006 SampType: MBLK TestCode: EPHT_S Units: mg/Kg Prep Date: 1215/2006 RunNo: 14086 Client ID: 77_777 Batch ID: 6015 TestNo: MADEP EPH (MADEP EPH Analysis Date: 12/5/2006 SegNo: 122973 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Adjusted C11-C22 Aromatics ND 10.0 C09-C18 Aliphatics ND 10.0 C19-C36 Aliphatics ND 10.0 Unadjusted C11-C22 Aromatics ND 10.0 Surr: 1-Chlorooctadecane 37.50 0 50 0 75.0 40 140 Surr:o-Terphenyl 38.00 0 50 0 76.0 40 140 Sample ID: LCS-6006 SampType: LCS TestCode: EPHT_S Units: mg/Kg Prep Date: 12/5/2006 RunNo: 14086 Client ID: 77771 Batch ID: 6015 TestNo: MADEP EPH (MADEP EPH Analysis Date: 12/5/2006 SegNo: 122974 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Hlghl-imit RPD Ref Val %RPD RPDLimlt Qual C09-C18 Aliphatics 35.20 10.0 50 0 70.4 40 140 C19-C36 Aliphatics 47.40 10.0 50 0 94.8 40 140 Unadjusted C11-C22 Aromatics 31.90 10.0 50 0 63.8 40 140 Surr:1-Chlorooctadecane 40.00 0 50 0 80.0 40 140 Surr:o-Terphenyl 41.50 0 50 0 83.0 40 140 Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Page 4 of 6 CLIENT: Enviro-Safe Corp. ANALYTICAL QC SUMMARY REPORT Work Order: 0612023 TestCode: HG 7471A S Project: 7513 Sample ID: MS-6034 SampType: MBLK TestCode: HG_7471A S Units: mg/Kg Prep Date: 12/6/2006 RunNo: 14102 Client ID: 7777Z Batch ID: 6034 TestNo: SW 7471A (SW7471A) Analysis Date: 12/6/2006 SegNo: 123092 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Mercury ND 0.100 Sample ID: LCS-6034 SampType: LCS TestCode: HG_7471A S Units: mg/Kg Prep Date: 121612006 RunNo: 14102 Client ID: 77777 Batch ID: 6034 TestNo: SW 7471A (SW7471A) Analysis Date: 1 2/612 0 0 6 SegNo: 123093 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Mercury 2.730 0.100 2.5 0 109 80 120 Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Page 5 of 6 CLIENT: Enviro-Safe Corp. ANALYTICAL QC SUMMARY REPORT Work Order: 0612023 TestCode: VPH_S4 Project: 7513 Sample ID: MB-R14160 SampType: MBLK TestCode: VPH_S4 Units: mg/Kg Prep Date: RunNo: 14160 Client ID: 7777 Batch ID: R14160 TestNo: VPH Analysis Date: 12/8/2006 SegNo: 123740 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Benzene ND 0.500 Ethylbenzene ND 0.500 m,p-Xylene ND 0.500 Methyl Tert-Butyl Ether ND 0.100 Naphthalene ND 1.00 o-Xylene ND 0.500 Toluene ND 0.500 Surr:1,2-Dichloroethane-d4 109.4 0 100 0 109 70 130 Surr:2,5-Dibromotoluene 109.7 D 100 0 110 70 130 Surr:Bromofluorobenzene 112.6 0 100 0 113 70 130 Surr:Toluene-d8 85.70 0 100 0 85.7 70 130 Sample ID: LCS-R14160 SampType: LCS TestCode:VPH_S4 Units: mg/Kg Prep Date: RunNo: 14160 Client ID: 77777 Batch ID: R14160 TestNo: VPH Analysis Date: 12/8/2006 SegNo: 123741 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Benzene 106.5 0.500 100 0 106 70 130 Ethylbenzene 117.0 0.500 100 0 117 70 130 m,p-Xylene 228.2 0.500 200 0 114 70 130 Methyl Tert-Butyl Ether 92.10 0.100 100 0 92.1 70 130 Naphthalene 80.70 1.00 100 0 80.7 70 130 o-Xylene 110.8 0.500 100 0 111 70 130 Toluene 113.4 0.500 100 0 113 70 130 Surr:1,2-Dichloroethane-d4 95.80 0 100 0 95.8 70 130 Surr:2,5-Dibromotoluene 89.80 0 100 0 89.8 70 130 Surr:Bromofluorobenzene 101.2 0 100 0 101 70 130 Surr:Toluene-d8 101.0 0 100 0 101 70 130 Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Page 6 of 6 CHAIN OF CUSTODY GeoLabs CHAIN NUMBER: 0(014093 D `P ''''`1rWEOKED'S1TE S MUST'B :FILLED 1I�#?, 24/ 8 MOUR"RtJS .ES ONL�(S1 fIT 1;APRROA/A!... RAF'"D I FYLER ORpiU4BjrD1.„LCTaO �a ;..'ly.".:'�:{m s- M.. GeoLabs, Inc. TurnaMUR �tlme Page I of I Environmental Laboratories SPECIAL INSTRUCTIONS M"" �STAND RUS .4IRD �iX s nra u u ,,i+'�rNl al!4 uM a ylsity °1iNi7� , .I� 45 Johnson Lane Braintree, MA 02184 Cy 4�11 N S7jM G' M Office: 781-848-7844 UI,fi 1 it i r i .aq +firi { w .i rt ry.J9 l , r 4iu�yi t. Fax: 781-848-7811 Note: JOBS WITH INCOMPLETELY FILLED OUT CHAINS WILL NOT BE RUN. CHAIN WILL BE RETURNED TO CLIENT FOR COMPLETION TYPE OF CLIENT: BUS__._LAB HOMEOWNER NOTE: HOMEOWNERS, LAW FIRMS MUST PAY WHEN DROPPING OFF SAMPLES Client: X - gmifmy C O Project Number: X 1 '3 CHANGES REQUESTED? Y N Address: X ' I S+NO P.O. BOXES Project Location: X LI 0 50 BY DATE P 1TS� Phone: X 50 (..;3 6 o Fax: g �'� S" Purchase Order#: (j - Contact: X 6 P Collected By: X Received on ice? c ANALYSES REQUESTED COLLECTION CONTAINER W S Q M � L D T M T U A C G P GEOLABS cr7 C Q~Q A SAMPLE A i P B SAMPLE Y A T O R R SAMPLE W B ID T M Y LOCATION P R M A E � Z IL E E L E N I P B S NUMBER "I-v ✓� 2 P E T x N r,z-) 9 UJ H D S—l iah a6 r A.� `— G SX 1"6"17 - 0 I x x X Verbal results given to byl(date/initial MATRIX CODES: CONTAINER CODES: PRESERVATIVE CODES: R linq ished By: Date/Time Received By. DatelTime: GW=Ground Water A=Amber B=Bag 1 = HCI 5= NaOH V'X4-t rr-11 f o) �► W l W=Wastewater G=Glass P= Plastic 2= HNO3 6= McOH PRINT; I C.�—�`Z v b 6 d DW=Drinking Water S=Summa Canister 3= HZSO4 7= ICE Relinq jished By. Received By: SL=Sludge O=Other V=VOA 14= Na2S203 S=Soil A=Air Terms: Payment due within 30 days unless other arrangements are made. R Wed B Re Ived B GeoLabs: O=Oil OT=Other Past due balances subject to interest and collection costs. y( " l�+ Certified: MA, NH, RI,CT, NY, NJ, PA COMMONWEALTH OF MASSACHUSETTS EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS d DEPARTMENT OF ENVIRONMENTAL PRO COPY SOUTHEAST REGIONAL OFFICE S. 20 RIVERSIDE DRIVE, LAKEVILLE, MA 02347 508-946-2y 1ANE SWIFT BOB DURAND Goumor Secretary Y 1 20'0� LAUREN A.LISS 1 Commissioner �rOF BARNSTABLE May 15, 2001 aLTH.DEPT. Mr. David L. Columbo,Trustee RE: BARNSTABLE -BWSC/ASM Olive Oil Realty Trust Property 478 South Street 484 South Street Hyannis, Massachusetts 02601 RTN 4-01301 RETURN TO COMPLIANCE/ NOTICE OF AUDIT COMPLETION Dear Mr. Columbo: On February 21, 2001, the Massachusetts Department of Environmental Protection, Bureau of Waste Site Cleanup (the Department), issued a Notice of Audit Findings/Notice of Noncompliance (NOAF/NON)in response to conditions existing at the site mentioned above which were in violation of the terms of the Activity and Use Limitation (AUL). The NON requested that you (as used in this Notice, "you" refers to "Olive Oil Realty Trust") take certain steps to correct those violations. In a document received by the Department on April 26, 2001, the LSP-of-Record,. Mr. Nathaniel Finsness, indicated that.a condition of No Significant Risk had been achieved at the site without the need for an AUL and therefore, the AUL was not necessary. Subsequently, a Notice of Termination of the Activity and Use Limitation was recorded with the appropriate Registry of Deeds and a copy forwarded to the Department on April 26,2001. The Department now considers the audit initiated for this site on January 22, 1999 to be complete. LIMITATIONS The Department relies upon the certainty of the information reviewed during the audit, including information submitted during the course of the audit, to make these findings. These findings do not: (1) apply to actions or other aspects of the site that were not reviewed in the audit, (2) preclude future audits of past, current, or future actions at the site, (3) in any way constitute a release from any liability, obligation, action or penalty under M.G.L. c.21E, 310 CMR 40.0000, or any other law, regulation, or requirement, or (4) limit the Department's authority to take or arrange, or to require any Responsible Party or Potentially Responsible Party to perform, any response action authorized by M.G.L. c.21E which the Department deems necessary to protect health, safety,public welfare or the environment. This information is available in alternate format by calling our ADA Coordinator at(617)574-6872. DEP on the World Wide Web: http://www.state.ma.usidep i�a Printed on Recycled Paper Barnstable,484 South Street 2 Return to Compliance/Notice of Audit Completion RTN 4-01301 If you have any questions regarding this Notice, please call Kathryn Carvalho at (508) 946- 2742. Please reference Release Tracking Number 4-01301 in any correspondence regarding this site. Very truly yours, Joseph F. Kowal, Chief Audit & Site Management Section JFK/KC/ka CERTIFIED MAIL# Z 240 877 061 RETURN RECEIPT REQUESTED cc: Mr. Michael B. Stusse 25 Mid Tech Drive West Yarmouth,Massachusetts 02673 Barnstable Board of Health P.O. Box 534 Hyannis,Massachusetts 02601 Barnstable Selectmen's Office Town Hall 367 Main Street Hyannis,Massachusetts 02601 Mahoney&Douglas, Ltd Environmental Services Post Office Box 473 Falmouth,Massachusetts 02541 ATTN: Ms. Katherine A. Mahoney,President DEP-Boston ATTN: Tom Potter DEP-SERO ATTN: Regional Enforcement Office(2) Data Entry 1 COMMONWEALTH OF MASSACHUSETTS Z EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS d DEPARTMENT OF ENVIRONMENTAL PROTECTIONG vE� e 20 RIVERSIDE DRIVE, LAKEVILLE,MA 02347 508-946-27 p�CjG, ARGEO PAUL CELLUCCI J AN D Governor RpNEP S etary JANE SWIFT � D TOW NEpySLISS Lieutenant Governor LAUREN A.Commissioner January 22, 2001 Mr. Eric Errico RE: .BARNSTABLE--BWSC/ASM as Exxon Company, USA I-Former,Exxon Facility 52 Beacham Street "404 Soutii Street Everett, Massachusetts 02149 RTN 4-01301 RETURN TO COMPLIANCE/ NOTICE OF AUDIT COMPLETION NON SE-00-3A-022 Dear Mr. Errico: On November 15, 2000, the Massachusetts Department of Environmental Protection, Bureau of Waste Site Cleanup .(the Department) issued a Notice of Audit Findings/Notice of Noncompliance that identified response action violations at the above referenced site. The Notice requested that you ("you refers to "Exxon Company, USA") take certain steps to correct those violations The Department has received your, response dated January 12, 2001, prepared and certified by Mr: Bruce Ross, the Licensed Site Professional (LSP)-of Record for this site, which contains information indicating that the steps requested by the Department have been taken. The information you submitted is adequate and the Department now considers the audit initiated for this site on January 22, 1999 to be complete. LIMITATIONS The Department relies upon the accuracy of the information reviewed during the audit, including information submitted during the course of the audit, to make these findings. These findings do not: (1) apply to actions or other aspects of the site that were not reviewed in the audit, (2) preclude future audits of past, current, or future actions at the site, (3) in anyway constitute a release from any liability, obligation, action or penalty under M.G.L. c.21E, 310 CMR 40.0000, or any other law, regulation, or requirement, or (4) limit the Department's authority to take or arrange, or_to require any Responsible Party or Potentially Responsible Party to'perform, aft y response action authorized by M.G.L. c.21E which the Department deems necessary to protecthealth, safety;public welfare or'the environment. This information is available in alternate format by calling our ADA Coordinator at(617)574-6872. DEP on the World Wide Web: http://www.magnet.state.ma.us/dep Zia Printed on Recycled Paper Barnstable-BWSC/ASM Page 2 of 2 RTN 4-01301 Return to Compliance/Notice of Audit Completion If you have any questions regarding this Notice, please call Kathryn Carvalho at (508) 946- 2742. Please reference Release Tracking Number 4-01301 in any correspondence regarding this site. Very truly yours, aseph F. Kowal, Chief Audit& Site Management Section K/KC/rr CERTIFIED MAIL # Z 240 877 547 RETURN RECEIPT REQUESTED cc: Barnstable Board of Health DEP-BOSTON P.O. Box 534 Attn: Thomas Potter r Hyannis, MA 02601 DEP-SERO Barnstable Selectman's Office. Attn: Data Entry Town Hall Regional Enforcement Office (2) 367 Main Street Hyannis, MA 02601 Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mr. Bruce Ross,LSP ' COMMONWEALTH OF MASSACHUSETTS EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS > d DEPARTMENT OF ENVIRONMENTAL PROTECTION ti< 20 RIVERSIDE DRIVE; LAKEVILLE, MA 02347 508-946-2700 �1M spa ARGEO PAUL CELLUCCI BOB DURAND Governor Secretary JANE SWIFT LAUREN A.LISS Lieutenant Governor Commissioner COPY November 15, 2000 Ms. Melissa K. Winsor RE: BARNSTABLE--BWSC/ASM Exxon Company, USA ;Former Exxon Facility 52 Beacham Street 4 484 South Street Everett, Massachusetts 02149 RTN 4-001301 s NOTICE OF AUDIT FINDINGS NOTICE OF NONCOMPLIANCE NON-SE-00-3A-022 Dear Ms. Winsor: On January 22, 1999, Exxon Company,,USA (hereafter referred to as "you") were notified that the Massachusetts Department.of Environmental Protection (the Department) had begun to audit response actions conducted to address the release Of oil at the location identified above. In particular,the audit focused on the Activity and Use Limitation (AUL) at this site and subsequent Response Action Outcome (RAO). This Notice informs you of the results of the Department's audit. DETERMINATION RAO Violations Identified which Require Correction As a result of the audit, the Department has determined that. response actions were not performed in compliance with the requirements of the Massachusetts Contingency Plan (MCP). Violations were identified that require additional actions to be taken under the supervision of a Licensed Site.Professional (LSP)in order to come into compliance with the MCP and other permits or approvals enforced by the Department. The additional actions must be taken within sixty days of receipt of this Notice. The attached Notice of Noncompliance (Attachment A) describes: (1) each activity identified during the audit which is in noncompliance, (2) the requirements violated, (3) the action the Department now wants you to take, and (4) the deadline for taking this action. An administrative 4 penalty may be assessed for every day from now on that you are in noncompliance. The Audit Memorandum (Attachment B) describes the activities Department personnel performed during the audit and summarizes relevant site information. This information is available in alternate format by calling our ADA Coordinator at(617)574-6872. DEP on the World Wide Web: http://www.state.ma.us/dep Z�'a Printed on Recycled Paper Facility,Hyannis,4-1301 2 Notice of Audit Findings No AUL Errors Identified which Require Correction The audit of the AUL did not identify any errors that require correction. Further information concerning the results of the AUL review is addressed in Attachment C. You do not need further Department approval to take the actions the Department has specified. However, to avoid further enforcement actions, you must complete the additional actions and submit a Post-Audit Completion Statement`in accordance with 310 CMR 40.1170 (Attachment D). DO NOT IGNORE T HIS NOTICE. Failure to address the vio lations and provide documentation of such action to the Department may subject you and your officers to further enforcement action by the Department. The Department may conduct a follow-up audit to determine whether the required response action has been taken. LICENSED SITE PROFESSIONAL A copy of this notice has been sent to Mr. Donald Pomeroy, LSP#3053, the LSP-of-Record for the Disposal site. However, you, not your-LSP, are responsible for correcting any identified violations and/or errors. LIMITATIONS The Department's findings were based upon the certainty of the information reviewed during the audit. These findings do not: (1) apply to actions or other aspects of the site that were not reviewed in the audit, (2) preclude future audits of past, current, or future actions at the site, (3) in any way constitute a release from any liability, obligation, action or penalty under M.G.L. c. 21E, 310 CMR 40.0000, or any other law, regulation, or requirement, or (4) limit the Department's authority to take or arrange; or to require any Responsible Party or Potentially Responsible Party to perform,any response action authorized by M.G.L. c. 21E which the Department deems necessary to protect health,safety,public welfare,or the environment. If you have any questions regarding this Notice, or any requirements it contains, please contact Kathryn Carvalho at 508-946-2742. Please reference the Release Tracking Number 4-1301 in any future correspondence to the Department regarding the site. Very truly yours, ?sepph F. Kowal, Chief Audit& Site Management Section K/KC/re Attachments: A. Notice of Noncompliance B. Audit Memorandum C. Summary of AUL Compliance Review D. Post Audit Completion Statement-BWSC Form 111 Facility,Hyannis,4-1301 3 Notice of Audit Findings CERTIFIED MAIL#Z 240 878 091 RETURN RECEIPT REQUESTED cc: Barnstable Board of Health P.O. Box 534 Hyannis, MA 02601 Barnstable Selectmen's Office Town Hall 367 Main Street Hyannis,MA 02601 Geologic Services Corporation. 15 Bonazzoli Avenue Hudson,Massachusetts 01749 ATTN: Mr. Donald L. Pomeroy,LSP DEP-Boston ATTN: Tom Potter DEP-SERO ATTN: Regional Enforcement Office (2) Data Entry: IRA/PH-II/RAO/AUL Former Exxon Facility,Hyannis,4-1301 1 Noncompliance Summary ATTACHMENT A NONCOMPLIANCE SUMMARY NON-SE-00-3A-022 Donald L. Pomeroy,Licensed Site Professional,#3053 ENTITY IN NONCOMPLIANCE . Exxon Company,USA 52 Beacham Street Everett,Massachusetts 02149 LOCATION WHERE NONCOMPLIANCE OCCURRED OR WAS OBSERVED Former Exxon Station 484 South Street Hyannis,Massachusetts DATES WHEN NONCOMPLIANCE OCCURRED OR WAS OBSERVED AND DESCRIPTION OF ACTIVITY IN NONCOMPLIANCE 1. The Phase II Report/Class A-3 RAO dated December 1997, failed to utilize the appropriate laboratory analytical test method approved by the Department for testing soils contaminated with petroleum compounds. This is a violation(Class II)of 310 CMR 40.0191(2). 2. During a site visit on October 16, 2000, conditions were observed at the site that failed to comply with the terms of the Activity and Use Limitation. This is a violation (Class I).of 310 . CMR 40.1070(2). DESCRIPTION OF REQUIREMENTS NOT COMPLIED WITH 1. In Section 1.2 of the Department's policy "Characterizing Risks posed by Petroleum Contaminated Sites: Implementation of MADEP VPH/EPH Approach" the following is clearly stated"On and after October 31, 1997, MADEP expects that all sites that have not been closed out in accordance with MCP provisions will be characterized using the VPH/EPH approach. There are no grandfathering provisions applicable to sites currently under evaluation." Pursuant to 310 CMR 40.0191(2),RAPS shall be employed during the performance of response actions conducted pursuant to 310 CMR 40.0000, and shall include, without limitation, the following: (a) consideration of relevant policies and guidelines issued by the Department and EPA; (b) use of accurate and up-to-date methods, standards and practices, equipment and . technologies which are appropriate, available and generally accepted by the professional and trade communities conducting response actions in accordance with M.G.L.. c. 21E and 310 CMR 40.0000 under similar circumstances; and (c) investigative practices which are scientifically defensible, and of a level of precision and accuracy commensurate with the intended use of the results of such investigations. Former Exxon Facility,Hyannis,4-1301 2 Noncompliance Summary 2. Section 3.0 of the Notice of Activity and Use Limitation recorded for the Property, sets forth Obligations and Conditions in order to maintain a condition of No Significant Risk. Obligations and Conditions set forth for the Property include "The prompt repair and maintenance of any pavement cracks or frost heaves". Pursuant to 310 CMR 40.1070(2), Activity and Use Limitations imposed pursuant to 310 CMR 40.1012 shall be implemented and adhered to by the owner and holders of interest in the property and/or a license to use the property subject to the Activity and Use Limitation, and/or the RP, PRP, or Other Person conducting response actions at the disposal site or portions of a disposal site in accordance with the procedures established in 310 CMR 40.1070 through 310 CMR 40.1099. DEADLINE AND DESCRIPTION OF ACTIONS TO BE TAKEN Within sixty (60) days of receipt of this Notice you are required to: 1 a) Conduct further assessment with analytical data provided from an appropriate test methodology and submit a revised Risk Characterization for the Class A-3 RAO that supports a conclusion of No Significant Risk; or, 1 b) Retract the Class A-3 RAO and continue response actions until an RAO is resubmitted that accurately characterizes the impact of the site to human health and the environment,and demonstrates that a condition of No Significant Risk has been achieved. NOTE: If you can document the achievement of a Class A-1 or A-2 RAO at the site you may then terminate the existing AUL,utilizing Form 108413. 2) Repair the cracks and frost heaves observed in the pavement and submit documentation detailing the repair. FAILURE TO COMPLY MAY RESULT IN FURTHER ENFORCEMENT If you fail to correct the violations identified above and provide documentation of such action to the Department,you may be subject to further enforcement action by the Department. The Department may conduct a follow-up audit to determine whether the required actions have been taken. If the Department finds that the violations have not been corrected,then the Department may issue a Notice of Intent to Assess a Civil Administrative Penalty (PAN), administrative enforcement order, Notice of Responsibility (NOR), Notice of Intent to take Response Action (NORA), Administrative Consent Order, Unilateral Order, or seek a Judicial Judgement as appropriate. You may also be subject to cost recovery under 310 CMR 40.1200 for failure to perform response actions at the disposal site. Former Exxon Facility,Hyannis,4-1301 1 Audit Memorandum ATTACHMENT B AUDIT MEMORANDUM . BWSC-4-1301 I. RESPONSE ACTIONS AUDITED The Audit included a review of the following: • The Phase I Site Investigation, the Phase II Comprehensive Site Assessment and A-3 Response Action Outcome (RAO) Statement and the Immediate Response Action (IRA) Completion Statement. • Notice of Activity and Use Limitation(HAUL) U. AUDIT ACTIVITIES The Audit consisted of the following activities: • A Notice of Audit(NOA)dated January 22, 1999. • Site walkovers that occurred on February 5, 1999 and October 16, 2000. • A Barnstable County Registry of Deeds file review on November 9, 1999. A review of documents contained in the Department's file for this location, including but not limited to: + The report titled "Massachusetts Contingency Plan, Phase I Site Investigation, Exxon Retail Facility #'-5751, 484 South Street, Hyannis, Massachusetts" prepared by Geologic. ` Services Corporation dated January, 1993. • The report titled "Tank Excavation Assessment Report, Former Exxon R/S #3-5751, 484 South Street, Hyannis, Massachusetts" prepared by Geologic Services Corporation and dated October, 1993. • The document titled "Phase II-Comprehensive Site Assessment Scope of Work, Former Exxon Facility R/S #3-5751, 484 South Street, Hyannis, Massachusetts" prepared by Geologic Services Corporation and dated September, 1996. • The report titled "Immediate Response Action Completion Report, Former Exxon Facility R/S #3-5751, 484 South Street, Hyannis, Massachusetts" prepared by Geologic Services and dated April 1995. � J • The report titled"Phase-II Comprehensive Site Assessment Report With Method 1 Risk Characterization and Class A-3 Response Action Outcome Statement, Former Exxon Facility R/S #3-5751, 484 South Street, Hyannis, Massachusetts"'prepared by Geologic Services Corporation and dated December, 1997. Former Exxon Facility,Hyannis,4-1301 2 Audit Memorandum III. SITE SUMMARY\SITE INSPECTION The property is located at 484 South Street in Hyannis, Massachusetts. It is comprised of 0.42 acres of land containing an unoccupied single-story building that was formerly operated as a gasoline retail and service station. The site is zoned for business use. Nearby properties include residential buildings to the south across South Street, commercial buildings to the north, residential homes, commercial businesses to the west and also to the east and across Sea Street. The site is located within an area of Hyannis where the groundwater resources are classified as "NON Potentially Productive Aquifer"i.e. GW-3. (Massachusetts GIS Map Quadrangle for Hyannis). In the direction of groundwater flow(south), the NON Potentially Productive Aquifer extends a distance of approximately 3400 feet. Located within this GW-3 area is a narrow band(approximately 100 feet) of GW-1 groundwater that surrounds the Oak F Grove Cemetery approximately 1600 feet to the south. Groundwater depth at the site ranges from 17' to 24'. When in operation the facility stored 26,000 gallons of gasoline in one 10,000 gallon and two 8000 gallon Underground Storage Tanks (USTs); 1,000 gallons of fuel oil in one 1,000 gallon UST and waste oil in one 1,000 gallon UST. The site was first listed as a confirmed disposal site on October 1, 1993, as a result of petroleum contaminated groundwater identified in a Phase I Site Assessment. The Phase I investigation revealed elevated concentrations of benzene,toluene, ethylbenzene and xylenes in monitoring wells MW-1 and MW-4. Positive PID readings were obtained in soils from the MW- i boring; the highest being 452 ppm obtained from a depth of 14'-16'. Positive PID responses Were not obtained from soils tested from the remaining borings. The concentrations of total benzene,toluene, ethylbenzene and xylenes (BTEX)ranged from 5,923 ug/1 in groundwater from MW-l.to,less than the Method Detection Limit(MDL)in MWs 2, 3 and 5. MW-4 exhibited only slightly elevated levels of BTEX. Analytical results from soil samples obtained from the monitoring well borings exhibited total BTEX concentrations ranging from 6,672 ug/kg at the MW-1 location to less than the MDL in the remaining borings. In July 1993 the USTs were removed from the site under the supervision of Geologic Services Corporation(GSC). The UST removal activities, documented in the October 1993 UST excavation report, described each of the USTs as being in good condition. Soil samples obtained from the UST grave were screened for VOCs. The readings ranged from None Detected (ND)to 95 ppm.PID readings from excavated soils ranged from ND to 183 ppm. However, laboratory analyses of soil samples obtained from the tank grave revealed no detectable concentrations of VOCs by EPA Method 8020. t The site was granted a waiver of approvals on May 3, 1994. In April 1995, an Immediate Response Action(IRA)was undertaken to "evaluate subsurface conditions at the downgradient portion of the subject property, and to document past and present site activities and uses in the vicinity of the site." The results of the IRA revealed that BTEX compounds had,migrated off the property and exceeded Method 1 GW-1 standards in several monitoring wells. However,the entire area of the site is classified as GW-3 due to its redesignation as a"NON Potentially Productive Aquifer". A Substantial Release Migration(SRM) evaluation was also conducted Former Exxon Facility,Hyannis,4-1301' 3 Audit Memorandum and revealed that the groundwater velocity at the site was approximately 704 feet per year. A SRM condition is considered to exist when it is determined that the groundwater velocity at the site exceeds or is likely to exceed 200 feet per year. Since no sensitive receptors were identified in the vicinity of the site and Method 1 GW-3 had not been exceeded the SRM condition was not considered significant. In December 1997 the Phase II-Comprehensive Site Assessment was completed at the site. A contaminant plume was identified extending southward from the property approximately 600 feet(within the"Non Potentially Productive"aquifer). Concentrations of benzene, ethylbenzene, xylenes, and MTBE were identified at the leading edge of the plume at levels below Method 1 GW-1 standards. Concentrations of toluene were above Method 1 GW-1 standards but below Method 1 GW-2 /GW-3 groundwater standards. Since the concentrations of benzene, ethylbenzene,xylenes and MBTE had significantly attenuated well below Method 1 GW-1 groundwater standards, and the concentration of toluene was below Method-1 GW-2 standards, no additional wells were installed. During the Phase II investigation, three monitoring wells on the former Exxon Station property were also evaluated for the presence of EDB and lead. None was identified at a concentration above the method detection limits of 0.02 ug/l.and 0.005 mg/l, respectively. Laboratory analyses of soil samples obtained from the tank excavation that were tested by EPA Method 8020 revealed no detectable concentrations of petroleum compounds in excess of Method 1, S-1 soil standards, Therefore, based on these analytical results, an AUL was not specifically required to maintain a condition of no significant risk. However, since the property was for sale at the time the Phase H was completed, a Class A-3 RAO was filed for the property to "impose the A UL for internal risk management purposes, thereby limiting ground intrusive activities and future uses at the former Exxon property". The Activity and Use Limitation.was recorded at the Barnstable Registry of Deeds on July 18'', 1996. It should be noted that prior to the completion of the Phase H in December 1997,the Department had already implemented the VPH\EPH test method in lieu of EPA Meth 2 p Y p Method 80 0 for analyzing soils contaminated with petroleum compounds. The effective date for the implementation of the VPH\EPH test method(October 31, 1997)was clearly indicated in Section 1.2 of the Policy. The Policy states that sites that had not closed out pursuant to 310 CMR 40.0000 by this date were expected to use the EPH\VPH test methodology for soils contaminated with petroleum compounds. On February 3, 1998 the Department received a report titled"Monitoring Well Abandonment Site.Closure Activities" indicating that all the monitoring wells used for the Phase I and Phase II investigations had been decommissioned. On February'5, 1999, Mr. Mark Panni of the Department conducted a site walkover. During this site visit it was observed that the.entire surface of the property was either paved or covered by the former gas station building. During a follow-up site visit on October 16, 2000, Mrs. Kathryn Carvalho noted that although the site was covered by pavement, it had not been maintained, as required in the Activity and Use Limitation. Cracks and frost heaves were observed in the northwestern corner of the property. Former Exxon Facility,Hyannis,4-1301 4 Audit Memorandum IV. DETERMINATION On the basis of the information reviewed during the audit and-in reliance upon the certainty of that information,the Department makes the following Determination. RAO Violations were identified that require further action Please refer to-the Notice of Noncompliance (Attachment A)relative'to the activities in noncompliance and the actions the Department wants you to take to come into compliance. J Former Exxon Facility,Hyannis,4-1301 1 Summary of AUL Compliance Review ATTACHMENT C SUMMARY OF AUL COMPLIANCE REVIEW Chapter 206 of the Acts of 1998p(The Brownfields Act) requires that the Department conduct an audit of all sites with Activity and Use Limitations (AULs). In carrying out this mandate, the Department has established special procedures for reviewing AULs recorded on or before October 29, 1999, including the ALL submitted as part of the Response Action Outcome (RAO) for your site. Please note that these procedures do not apply to AULs recorded on or after October 30, 1999, and this Summary of AUL Compliance Review should not be relied upon to predict audit results for such AULs. Applying the procedures described above,the Department has not identified any errors in the AUL that require correction. In order to ensure that the public is aware of the restrictions that the AUL imposes at the site,the Department may issue a public notice identifying the site and the location of the AUL at the Registry of Deeds. Such notice may be published in a local newspaper and/or on the Internet. I COMMONWEALTH OF MASSACHUSETTS EXECUTIVE OFFICE OF ENVIRONMENTAL AFFAIRS w .: DEPARTMENT, OF ENVIRONMENTAL PROTECTION �d SOL7THEAST , REGIONAL OFFICE 1 ARGEO PAUL CELLUCCI BOB DURAND Governor _ Secretary JANE SWIFT x DAVID B.STRUHS Lieutenant Governor Commissioner January 22, 1999 . ;Ms.Karen M.Daly 'RE: HYANNIS—B_W_SC/ASM-401301 Exxon Company,USA Former Gasoline Station , 52 Beacham Street 484 South Street Everett;'Massachusetts 02149, NOTICE'OF AUDIT/REQUEST FOR Y} •.� SITE INSPECTION NOTICE OF AUDIT .This is an important Notice. Promptly respond toany requests contained herein. x Dear M`s.Daly ,< Massachusetts General Law Chapter 21 E requires the Massachusetts Department of Environmental Protection;Bureau of Waste Site Cleanup(the "Department"),to audit response actions not approved by the Department4t sites`'of releases of oil of hazardous material to ensure that these actions are being conducted. according to M.G.L.c. 21E,the Massachusetts Contingency Plan(the"MCP' ,and other relevant laws and >regulations.."The MCP at'310.CMR 40.1.100,establishes procedures for conducting such audits. s The site::referenced above has been selected by the Department for an audit- The audit will be ' conducted by Department staff of the Southeast Regional Office in Lakeville. The audit will initially focus on the Class A-3 Response Action Outcome (RAO) Statement and Activity and Use Limitation (AUL) prepared on your behalf by Donald L. Pomeroy,°LSP#3053,of Geologic Services Corporation. Additional response actions may also be evaluated as appropriate. This Notice describes the scope of the audit and the _. . e f audit activities the Dell aitment initially. intends to perform, along with our responsibilities and o . type r Y. r g Y r , relevant deadlines. A fact sheet and flow chart that"describe the audit process are also included'as part of this Notice. Note that, during an audit response actitins:can proceed as planned unless you are otherwise notifiedby,the Depaitment. Y' 20 Riverside Drive•Lakeville.Massachusetts 02347 FAX(508)947-6557•Telephone(508)946-2700 This information is available in alternate format by calling our ADA Coordinator.at(617)574-68721. DEP on the World Wide Web: http://wwwmugnet.state.ma.us/dep i'J Printed on Recycled Paper r tia 2 REQUEST FOR SITE INSPECTION Pursuant to M.G.L.c.21E §§ 2,4,and 8,310 CMR 40.0166, and 310 CMR 40.1120(1;),employees, agents, and contractors of the Department may enter any site or vessel to;investigate,,sample,or-;inspect any documents, conditions, equipment, practice, or property as part of the audit. The Department requests an appointment to inspect the site on February 5, 1999, at 1:30 p.m.,,to"discuss issues relevant to this-audit. The inspection will be conducted by Mark Panni of th'e Audif-and-Site Management Section. Your LSP is requested to attend. Please call Mark Panni within seven(7)days of receipt of this Notice at(508)946-2848 if you will need to arrange an alternative date or time. Please submit any additional documentatnn associated with the response actions performed at the site not previously submitted to the Department which you would like to be included as part of the audit within seven (7) days from receipt of this Notice. Any submittal made in response to this Notice must contain the enclosed Certification of Submittal per-310 CMR/--0.0009. At the completion of this phase of the audit,the Department may: (1) Issue a Notice of Audit Findings that may in::lude a statement of violations or deficiencies and steps to correct those violations or deficiencies. (2) Request a meeting with you,and if you choose,a representative,to discuss response actions and other supporting evidence to demonstrate compliance and then issue a Notice of Audit Findings. (3) Conduct further site investigations and then issue a Notice of Audit Findings. (4) Issue a Notice of Audit Findings that sets an Interim Deadline to correct violations or deficiencies or to prepare an Audit Follow-up Plan. (5) Initiate enforcement actions listed at 310 CMR 40.1140(2) if violations of M.G.L. c. 21 E or the MCP have been identified. If you have any questions regarding this Notice or any of the requirements contained in it,or believe that you cannot comply with its requirements, please contact Mark Parini at (508) 946-2848. The Department appreciates your anticipated cooperation in this matter. Very truly yours, � MV4 <; K hief �osephF. o wal.C Audit and Site Management Section K/MEP/ka Enclosures: Fact Sheet Flow Chart Certification of Submittal CERTIFIED MAIL#Z 598 884 917 RETURN RECEIPT REQUESTED cc: Warren J. Rutherfo� rd;Town-Manager ;, Barnstable Board of Selectmen.' Town Hall 367'Maln"'Street Hyaniis;`1VIassacliusetts'02601 y, ° �� , ;"` ,^- �, yK3Y i cif t�k: 3�t1, J r'F 'lad �r s tc1 f t x a fi t is a i E Hs. :^�'� N �6 z. f. r'if S „e✓f _.r'W'. :Lk�, �;X d.T I y:..si �,.Stxu.,C4a . p - �..£ .F'1 s.. ,^a r ,c .L�:d a.,,YT•+•a., 9r F..% t Barnstable Board of Health __- Post Office Box 534.; Hyannis,Massachusetts 02601 {m Geologic Services Corporation 15 Bonazzoli Avenue , Hudson,Massachusetts,.01749. 4 t Attn. Donald L.Pomei•oy;'LSP , DEP-SERO.; Attn: 'Data Entry i DEP-Boston Attn: Tom Potter`_, ». .. tk1;.+- ,,,z _ �-i. tt. Y. c .t * 1•{ t .kW . !" w .. (t'." ..,..+»n ' '^�k,'•3..ea3t 6aF�. !�.'c .s y .�,fr',f L` 4' —4 M ''i7F e='£zC7 ',Sz" ,',."tars%�st.�1 a"�'•s..'.:- � 3>r «',, - `:? r "# t ! ,_* ',? 4 i k . r r `2 .. rr.'".� �'#".5•.' a j•.:�'�.�+ hi��'zA1•�.,�lt> ��S �1} � t...�.>"� ..F t .+ ..•zi-. - t �.k RR.":G fit' firsGEOLOGIC SERVICES CORPORATION CJ Hydrogeologlsts and Environmental Scientists March 24, 1998 Mr. Jim Tinsley Town Manager Hyannis Town Hall 367 Main Street Hyannis, MA 02601 Re: Former Exxon Facci ty FVS#3-57.51. 484 South Street r Hyannis,Massachusetts Dear Mr. Tinsley: Pursuant to 310 CMR 40.1403(3)(e),and(f),Geologic Services Corporation(GSC)on behalf of Exxon Company,USA(Exxon)hereby notifies your office of the availability of the following document for the above referenced site: Phase II Comprehensive Site Assessment Report with Method 1 Risk Characterization and Class A-3 Response Action Outcome. This document is available for review at the Massachusetts Department of Environmental Protections Southeast Regional Office located at 20 Riverside Drive,Lakeville,Massachusetts. If you have any questions please feel free to contact us. Sincerely, Geologic Services Corporation Scott K. Parker Project Manager a cc: Karen M. Daly, Exxon Company, USA Tom McKean,Hyannis Board of Health SKP/sml Ref#900803-3.06 r M. 15 Bonazzoli Ave. • Hudson, MA 01749%, (978) 568-8740 (978) 568-9316 Recycled Paper GEOLOGIC SERVICES CORPORATION Hydrogeologlsts and Environmental Scientists May 18,.1994 Ms. Susan G. Rask - Chair Person Hyannis Board of Health Town Hall 367 Main Street Hyannis, MA 02601 Re: Exxon Station RAS #3-8751 484 South Street Hyannis, MA DEP Site`No. 4-1301 Dear Ms. Rask: Enclosed please find a copy of the Waiver Application Disposition Form approved by the Massachusetts Department of Environmental Protection.(DEP).on April 29, 1994 for the above referenced site. Pursuant to 310 CMR 40.537, the Department of Environmental Protection (DEP) has granted a waiver of the approval requirements set forth in 310.CMR 40.536 to:Exxon Company, USA. In . conjunction with this waiver, the DEP has classified the above site 'Non Priority.' The,purpose of a Waiver of Approvals is to allow a potentially responsible party (PRP) of a non-priority disposal site to proceed through the phases of 310 CMR 40.000 the Massachusetts Contingency Plan(MCP), and with remedial activities in a timely manner, without direct DEP oversight. The waiver does. not, however, alleviate a PRP from his or her obligations to comply with the MCP and MGL Chapter,21 E. Should you have any questions relative to this matter, please contact us at your convenience. Very truly yours, .Geologic Services Corporation Scott K. Parker Zrnia Pomer �0,2 Project.Manager Operations Manager SKP/DLP/sml attachments cc: Charles M. Beck von Peccoz, Exxon Company, USA Jacalyn A. Barton, Chairperson, Hyannis Board of Selectmen Deborah A. Marshall,'Department of Environmental Protection ref# 920820A.16 15 Bonazzoli Ave. • Hudson, MA 01749 (508) 568-8740 • FAX (508) 568-9316 Recycled Paper SECTION VIII WAIVER ' APPLICATION DISPOSITION (For DEP Use Only) 1. , Application, Number: , . 93-4-1301-1 Date Application Received: 8124193 2. Applicant Name: Exxon Company, USA Address: 52 'Beacham .Street . (STREET) Everett MA - 02149 (CITY/TOWN) (STATE) (ZIP CODE) 3 . Site Name: Exxon- Service Station 13-5751 4. Site ID Number: 4-1301 5. Disposition Waiver Application Determination. (Check one) XXXX Approved• Conditions of Approval: The Department shall be notified in writing, if work is terminated prior to fulfillment of the MCP and Waiver Requirements. Additional Conditions are specified in the Waiver Application (Section IV) and the approval letter.. This form, the waiver application and the approval letter constitute the . complete. waiver approval. t Denied Basis for denial: Application Reviewed by: a4' 9y !r - dS 5y Signature: Date: Acceptance of Waiver Application Disposition I understand and agree .to any -and''all additional conditions specified for an approved application. (Signature o Applicant) (Date) To be completed by applicant for approved waiver applications. Sign and return this page to the Department for all approved waiver applications, regardless of whether any .additional ,l conditions have been specified. R.. Commonwealth of Massachusetts Executive Office of Environmental Affairs Department of Environmental Protection Willem F. Weld Governor Daniel S.Greenbaum Commissioner Board of Health A U G 0 51993 P.O. Box 534 Hyannis, MA 02601 RE: Hyannis 14x84 xon Service Statio IS C South Street` DEP Site ID # 4-1301 WAIVER APPLICATION NOTIFICATION Dear Local Official: This letter is to inform you that the Department has received an application for "Waiver of Approvals" for the above referenced disposal site. The application was submitted by Exxon Company, USA. The Massachusetts Contingency Plan (310 CMR, 40.00) establishes procedures for assessing and remediating sites where there has been a release of oil or hazardous materials. The Massachusetts Contingency Plan requires that six specific reports be submitted to the Department during the response action process. The Department must approve each of the reports before the next phase of work can be conducted (310 CMR 40. 536) . The Massachusetts Contingency Plan also allows those conducting response actions at non-priority sites to apply to the Department for a waiver of required approvals (310 CMR 40.537) . When such a waiver is granted, remedial response actions must still meet all of the other requirements of M.G.L. c. 21E and The Massachusetts Contingency Plan, including submittal of documents to the Department. However, no Department approvals of reports, plans, or other documents will be required as long as the waiver remains in effect. A waiver of approvals will expedite the performance of a -remedial response action. At this time, the Department is focusing its limited resources on the disposal sites which present the greatest and most immediate threats to public health y One Winter Street •. Boston,Massachusetts 02108 • FAX(617)556-1049 a Telephone(617)292-5500 Page 2 of 2 BOH Letter and to the environment. These are generally sites classified as priority, based on specific criteria in the Massachusetts Contingency Plan. At non-priority sites, contamination does not threaten public health or the environment, but may at some time in the future if no action is taken. A waiver of approvals allows assessment and cleanup of non-priority sites which otherwise would have to wait until the Department has staff available to oversee response actions. The DEP expects to complete its review of this waiver application and all other relevant information within 60 days of receipt of the application in the regional office. The waiver application and any other information submitted to the department may be reviewed by appointment. To make an appointment, please contact the assigned DEP staff person at the phone number listed in the closing of this correspondence. In deciding whether to grant a waiver of approvals for this , site, The Department welcomes any additional information that you may wish to be considered for this case. Please submit any information and comments to the Waiver Unit of the DEP regional Office listed above. Information must be submitted on or by thirty days from the date of this letter so that we may include it in our review of this application. The Department will notify you as to the decision made on this waiver application. For specific information regarding this particular waiver application, please refer all inquiries to Joseph Kowal of the Southeast Regional Office, (508) 946-2862. We appreciate any assistance that you may offer in this matter. l Sinc e , Robert P. Kalag Chief Cost Recovery Section Waiver Program, ti Bureau Of Waste Site Cleanup cc: Charles Beck von Peccoz, Exxon Company, USA Joseph Kowal, SERO 1