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Home My WebLink About0577 WEST MAIN STREET - Health (2) 577 West M HyailciisV E R A= 269— 003 I I Address: 577 WEST MAIN STREET HYANNIS (Former Shell Service Station) VARIOUS REPORTS ON REMEDIATION STATUS AND GROUNDWATER SAMPLING RESULTS. • OCTOBER 2007 - 2011 DOCUMENTS IN STORAGE BOX # 41 A December 7,2021 Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601 Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Notice of Availability of Phase V Remedy Operation Status and Remedial Monitoring Report Former Shell-Branded Gasoline Station 577 West Main Street Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan(MCP) 310 CMR 40.1403 (3)(e),this correspondence serves as notification that a Phase V Remedy Operation Status &'Remedial Monitoring Report (ROS-RMR) was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location (the disposal site). The report summarizes activities conducted between June and December 2021. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site' is the operation of an air sparge and soil vapor extraction (AS/SVE)remediation system coupled with monitored natural attenuation(MNA) for the downgradient portion of the plume. The AS/SVE system operated continuously during this reporting period with minimal downtime. System operation will continue during the next reporting period. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conducted on a quarterly basis. A copy of the Phase V Remedy Operating Status Report as well as all other applicable documents pertaining to the subject site,are available for review on the MassDEP website: httl2s://eeaonline.eea.state.ma.us/EEA/fileviewer/Rtn.asl2x?rtn=4-0016772 If you have any questions,please call the undersigned at(508)339-3200. Sincerely, SOVEREIGN CONSULTING INC. Lklt l ii it Lisa M.Stone Rachel B.Leary,P.E.,LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Edward Henke,Shell(within report package) Sovereign File-2H874 9 Payson Road,Suite 1SO 0 Foxborough,MA 0203S • Tel:S08-339-3200 • Fax: S08-339-3248 SOVEREIGN CONSULTING INC . June 7,2021 Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601 Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Notice of Availability of Phase V Remedy Operation Status and Remedial Monitoring Report Former Shell-Branded Gasoline Station 577 West Main Street Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan(MCP)310 CMR 40.1403 (3)(e),this correspondence serves as notification that a Phase V Remedy Operation Status & Remedial Monitoring Report (ROS-RMR) was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location (the disposal site). The report summarizes activities conducted between December 2020 and June 2021. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site" is the operation of an air sparge and soil vapor extraction (AS/SVE)remediation system coupled with monitored natural attenuation(MNA) for the downgradient portion of the plume. The AS/SVE system operated continuously during this reporting period with minimal downtime. System operation will continue during the next reporting period. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conducted on a quarterly basis. A copy of the Phase V Remedy Operating Status Report as well as all other applicable documents pertaining to the subject site,are available for review on the MassDEP website: https://eeaonline.eea.state.ma.us/EEA/fileviewer/Rtn.aspx?rtn=4-0016772 If you have any questions,please call the undersigned at(508)339-3200. Sincerely, SOVEREIGN CONSULTING INC. Lisa M.Stone Rachel B.Leary,P.E.,LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Edward Henke,Shell(within report package) Sovereign File-2H874 9 Payson Road,Suite 150 0 Foxborough,MA 02035 0 Tel: 508-339-3200 • Fax:508-339-3248 577 SOVEREIGN CONSLILTING INC . t� C5 July 9,2019 Thomas A. McKean Town of Barnstable « Public Health Division 200 Main Street Hyannis,Massachusetts 02601 Thomas K. Lynch Barnstable Town Manager 387 Main Street =_ Hyannis,Massachusetts 02601 Re: Availability of Release Abatement Measure Completion Report Former Shell-Branded Gasoline Station 6, 577 West Main Street Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan(MCP) 310 CMR 40.0447(1), notification is hereby made that a Release Abatement Measure (RAM) Completion Report was prepared for the above-referenced disposal site. The report summarizes activities conducted during the removal of an oil-water separator. A copy of the RAM Completion Report as well as all other applicable documents pertaining to the subject site,are available for review on the MassDEP website: http://12ublic.dep.state.ma.us/SearchableSites2/Search.aspx. Sincerely, SOVEREIGN CONSULTING INC. Lisa M.Stone Rachel B. Leary,PE,LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO R.Rule,Equilon Sovereign File-2S874 9 Payson Road,Suite 150 0 Foxborough,MA 02035 9 Tel:508-339-3200 0 Fax: 508-339-3248 Health Master Detail Page 1 of 1 *. �. 86.E V'. 4 .ts6i xd6Y x 8.,. •A X/ � y�� d.p t 's' �; g Logged In As: TOWN\nickeant Health Master Detail Thursday,June 5 2014 Application Center Parcel Lookup Selection Items Reports Parcel Septic Perc Well i Fuel Tank Parcel: 269-003 .Location: 577 WEST MAIN STREET,HYANNIS Owner: ER&C ENTERPRISES,LLC Show 6 Removed Fuel Tanks Tank 7, 11/25/?010 Tank 8, 11/25/2010 Tank 9, 11/25/2010 New Fuel Tank... Tag number: Install date 11/25/2 110 112 Location:I B Below round I- Capacity(gallons) : 10000, Construction:I Select material] Meets 326-8(d)standards: r Leak detection: F Cathodic detection: r Not in ZOC on Split lot: r Fuel stored. G � Fuel storage reason: Select reason Removal company:I Select company Licensed Site Professional: Select name Unregistered removal: r Removal date : Removal notification date :F Leakage on removal: Abandon date :F— Abandon status: Select status i Variance date :�— Fa Variance granted: L 1 Release tracking number:�- Comments: [J Tank Install Date is date of application for permit to install issued by Hyan Delete Tank New Fuel Tank Test.. Notification date : Date : Result: Select result:` i Comments: Save Fuel Tank Changes I ;` Return to Lookup" http://issgl2/intranet/healthMaster/HealthMasterDetail.aspx?ID=269003 6/5/2014 Town of Barnstable Regulatory Services 6,9. °'f• '' Building Division 200 Main Street,Hyannis,MA 02601 508-862-4679 fax 508-862-4725 Initial Site Plan Review Issues & Concerns Applicant: West Main Gas SPR#: 016-14 Property Address: 577 West Main Street,Hyannis Map/Parcel: Map 269,Parcel 003 Zoning: HB, WP/GP Overlay Proposal: Applicant proposes to remove the existing carwash bay and convert the carwash space into retail space thereby expanding the retail space within the structure. This will result in addition of 940 s.f.to the retail use,namely the convenience store. The applicant also proposed the installation of a drive-up window in the rear of the structure. Plans for the above proposal were reviewed at a staff meeting held June 3, 2014 in preparation for the formal site plan review meeting scheduled June 5, 2014. The following initial comments were offered: ❖ Relief from the Zoning Board of Appeals will be required. ❖ Underground carwash related tanks and equipment must be removed. ❖ Request is made that the soil be tested for contamination upon removal of tanks and equipment. ❖ Update of the status of any previous EPA review or filing is requested. ❖ Consultation with the DPW regarding revision to water, sewer and grease trap installation will be required. ❖ According to the floor plans, it appears that a full service coffee shop is proposed. A coffee shop will require a grease trap as well as other Health Dept. requirements for food service. Consultation with the Health Department is recommended. ❖ A"right in only" from the westernmost West Main Street entrance is recommended with the closing of the easternmost entrance on West Main Street. Traffic will exit the site by the Old Craigville Road exit. ❖ Entrance to be closed must be filled with matching sidewalk and curbing. ❖ Consultation with DPW regarding landscaping will be required. ❖ Request is made for a drainage plan and for grading to be added to the plan. ❖ Hyannis FD has stated that if the full service fueling is proposed to be maintained, coffee shop staff may not also perform the fueling service. ❖ Question was raised as to how it is proposed to avoid conflicts with the drive through during fuel delivery to the underground tank. ❖ A road opening permit from DPW will be required. • A lighting plan depicting zero (0) spillage onto abutting property is requested. SCHEDULED FOR FORMAL SITE PLAN REVIEW JUNE 5, 2014. . 1 Health Master Detail , Page 1 of 1 "�' - _ Logged In As: TOWN\mckeant Health Master Detail Thursday,June 5 2014 Application Center Parcel Lookuo Selection Items Reports t Parcel Septic Perc Well Fuel Tank Parcel: 269-003 Location: 577 WEST MAIN STREET,HYANNIS Owner: ER&C ENTERPRISES,LLC Show 6 Removed Fuel Tanks F Tank 7,11/25/2010 1 Tank 8, 11/25/2010 Tank 9, 11/25/2010 1 New Fuel Tank... Tag number. Install date : 11/25/2010 { Location: B(Below ground) Capacity(gallons) : 10000:, Construction: Select material;' Meets 326-8(d)standards: r. Leak detection: ( } Cathodic detection: r Not in ZOC on Split lot: rl i j Fuel stored Select types='' Fuel storage reason: Select reason j Removal company: Select company — me Licensed Site Professional: Select na Unregistered removal: F w I Removal date : Removal notification date :F j Leakage on removal: Abandon date Abandon status: Select status I Variance date : Variance granted: I-1 Release tracking number: Comments: C—'—"Mete k Tank Install date"is the date of application for installation issued by Hyann� I Delete Tank) New Fuel Tank j Notification date :l Date : Result: Select result Comments: (� _------ ........_..._ _.......__. ..... — Save Fuel Tank Changes I Return to Lookup http://issgl2/intranet/healthMaster/HealthMasterDetail.aspx?ID=269003 6/5/2014 Health Master Detail i- Page 1 of 1 Logged In As: TOWN\mckeant Health Master Detail Thursday,Rine 5 2014 Application Center Parcel LOOkUD Selection Items Reports Parcel Septic Perc Well j Fuel Tank Parcel: 269-003 Location: 577 WEST MAIN STREET, HYANNIS Owner: ER&C ENTERPRISES,LLC €"""' Show 6 Removed Fuel Tanks Tank 7, 11/25/2010 Tank 8, 11/25/2010 Tank 9,11/25/2010 New Fuel Tank... _ _.. Tag number:F— Install date : 11/25/2910 Location: B(Below ground)! Capacity(gallons) : F77770000 Construction: Select matenal!` Meets 326-8(d)standards: F Leak detection: r! Cathodic detection: ri Not in ZOC on Split lot: r Fuel stored:f Select typed Fuel storage reason: Select reason; Removal company Select company Licensed Site Professional: lsoectnarne Unregistered removal: C I Removal date : Removal notification date :F— I Leakage on removal: r Abandon date : Abandon status: Select status Variance date :F--1 am Variance granted: r Release tracking number: Comments: S lit Tank 6,000/4,000 allons Install date"is the date of.application for Delete Tank ' New Fuel Tank Test... Notification date : Date : Result: Select result i Comments: l� ---- —— — —------ —_ ---- — �. Save Fuel Tank Changes f �Mf Return to Lookup http://issgl2/intranet/healthMaster/HealthMasterDetail.aspx?ID=269003 6/5/2014 ° '°` Town of Barnstable •"" '�� Regulatory Services 6JP �0 •�^�`' Building Division 200 Main Street,Hyannis,MA 0260.1 508-862-4679 fax 508-862-4725 Initial Site Plan Review Issues & Concerns Applicant: West Main Gas SPR#: 016-14 Property Address: 577 West Main Street,Hyannis Map/Parcel: Map 269,Parcel 003 Zoning: HB,WP/GP Overlay Proposal: Applicant proposes to remove the existing carwash bay and convert the carwash space into retail space thereby expanding the retail space within the structure. This will result in addition of 940 s.f.to the retail use,namely the convenience store. The applicant also proposed the installation of a drive-up window in the rear of the structure. Plans for the above proposal were reviewed at a staff meeting held June 3, 2014 in preparation for the formal site plan review meeting scheduled June 5, 2014. The following initial comments were offered: ❖ Relief from the Zoning Board of Appeals will be required. ❖ Underground carwash related tanks and equipment must be removed. ❖ Request is made that the soil be tested for contamination upon removal of tanks and equipment. ❖ Update of the status of any previous EPA review or filing is requested. ❖ Consultation with the DPW regarding revision to water, sewer and grease trap installation will be required. ❖ According to the floor plans, it appears that a full service coffee shop is proposed. A coffee shop will require a grease trap as well as other Health Dept. requirements for food service. Consultation with the Health Department is recommended. ❖ A"right in only" from the westernmost West Main Street entrance is recommended with the closing of the easternmost entrance on West Main Street. Traffic will exit the site by the Old Craigville Road exit. Entrance to be closed must be filled with matching sidewalk and curbing. ❖ Consultation with DPW regarding landscaping will be required. ❖ Request is made for a drainage plan and for grading to be added to the plan. ❖ Hyannis FD has stated that if the full service fueling is proposed to be maintained,coffee shop staff may not also perform the fueling service. ❖ Question was raised as to how it is proposed to avoid conflicts with the drive through during fuel delivery to the underground.tank. ❖ A road opening permit from DPW will be required. ❖ A lighting plan depicting zero (0) spillage onto abutting property is requested. SCHEDULED FOR FORMAL SITE PLAN REVIEW,TUNE 5;2014. 1 EKEIGN CONSULTING INC . July 23,2012 Ms. Cynthia Martin Hazardous Materials Specialist Barnstable Public Health Division 200 Main Street Hyannis,MA 02601 Thomas K. Lynch Acting Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Notice of Application for a Tier IC Permit Extension Former Shell-Branded Retail Station 577 West Main Street! Hyannis, Massachusetts RTN 4-16772 To Whom It May Concern: " In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.0703(8)(a)2, this letter serves as notification that a Tier IC Yermit Extension Application has been submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location. f In accordance with the MCP 310 CMR 40.0703(8)(a)2a, attached is a copy of the legal notice that will appear in the Cape Cod`Times on July 26, 2012 regarding the Tier IC Permit Extension Application and public involvement opportunities. If you have any questions or would like additional information please call the undersigned at(508) 339-3200. Sincerely,' SOVEREIGN CONSULTING,INC. Lisa M. Stone c Rachel B. Leary,P.E:; SP ^� a �a Project Manager Senior Project Engineer Attachments: .Notice of Application for Tier I Permit Extension � i} NJ ;$ cc: with Attachments: Robert Rule,Motiva £ € MassDEP SERO Sovereign File-2R874 t 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF APPLICATION FOR TIER I PERMIT EXTENSION Former Shell-Branded Retail Station 577 West Main Street Hyannis,Massachusetts 02601 RTN 4-167729 Permit No.W031981 A release of oil and/or hazardous materials has occurred at this location, which is a disposal site as defined by M.G.L. c. 21E, § 2 and the Massachusetts Contingency Plan,310 CMR 40.0000. On March 13,2003 the Department of Environmental Protection(MassDEP) issued a Tier IC Permit for Comprehensive Response Actions at the site. On July 30, 2012, Motiva Enterprises LLC intends to file an Application for a Tier 1 Permit Extension with MassDEP pursuant to 310 CMR 40.0703 and 40.0706. This Application will seek to extend the permit for this site from September 14, 2012 to July 30, 2013 based upon the following rationale: • To enable the continuation of Comprehensive Response Actions following the termination of Remedy Operation Status; Anyone interested in reviewing the Application for Tier I Permit Extension should contact Sovereign Consulting Inc., 16 Chestnut Street, Suite 520, Foxborough, MA, (508)-339-3200, to request a copy of the Application. Written comments related to this Application must be submitted within 20 days of the publication of this notice to: (1) MassDEP SERO, 20 Riverside Drive,Lakeville,Massachusetts 02347 by mail or by hand delivery during normal business hours; and (2) Sovereign Consulting Inc., 16 Chestnut Street, Suite 520, Foxborough,MA. Failure to provide written comments as set forth herein may affect your right,if any,to challenge MasSDEP'S permit decision. The Application and the disposal site file can be reviewed at MassDEP SERO,20 Riverside Drive,Lakeville,Massachusetts 02347,(508)-946-2714. Additional public involvement opportunities are available under 310 CMR 40.1403(9)and 310 CMR 40.1404. • CONSUL March 12,2013 Thomas A. McKean Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601.. Thomas K. Lynch Acting Town Manager 387 Main Street Hyannis,Massachusetts 02601 . Re: Availability of Phase IV Status Report Former Shell-Branded Retail Station 577 West Main Street Hyannis,Massachusetts RTN 4-16772 a To Whom It May Concern: . In accordance with the Massachusetts` Contingency Plan (MCP) 310 CMR 40.0874, this correspondence serves as notification that a Phase IV Status Report was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above-referenced location (the disposal site). This Phase ,IV Status,Report documents activities related to the remediation system installation as well as groundwater sampling events in August and December 2012. 1 " A copy of the Phase IV Status Report, as"well as other applicable documents pertaining to the disposal site, are available for review at the Massachusetts Department of Environmental Protection Southeast Regional Office in Lakeville, MA. If you have any questions please call the undersigned at(508) 339-3200 C7 I C> Z w ZZ Sincerely, ` SOVEREIGN CONSULTING INC. F Na Lisa M.Stone Rachel B. Leary,P.E.,LSP Project Manager X`' Senior Project Engineer cc: MassDEP SERO Y R.Rule-Motiva s Sovereign File-2E874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 i SOVFREIGN CONSLILTING INC . December 7,2018 f°` T�• Thomas A.McKean Town of Barnstablej' Public Health Division >a 200 Main Street Hyannis,Massachusetts 02601 Thomas K. Lynch Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Notice of Availability of Phase V Remedy Operation Status and Remedial Monitoring Report Former Shell-Branded Gasoline Station 577 West Main Street Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan(MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase V Remedy Operation Status & Remedial Monitoring Report (ROS-RMR) was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location (the disposal site). The report summarizes activities conducted between June and December 2018. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site' is the operation of an air sparge and soil vapor extraction (AS/SVE) remediation system coupled with monitored natural attenuation (MNA) for the downgradient portion of the plume. Currently the AS/SVE system is not in operation. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conducted on a quarterly basis. A copy of the Phase V Remedy Operating Status Report as well as all other applicable documents pertaining to the subject site,are available for review on the MassDEP website: h!!p://pubhc.dep.state.ma.us/SearchableSites2/Search.asl2x. If you have any questions please call the undersigned at(508)339-3200. Sincerely, SOVEREIGN CONSULTING INC. fZ:Y_ Lisa M.Stone Rachel B.Leary,P.E.,LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Robert Rule,SOPUS(within report package) Sovereign File-2S874 9 Payson Road, Suite 150 0 Foxborough,MA 02035 • Tel: 508-339-3200 • Fax: 508-339-3248 • V E R El I G N C • June 7,r'2018`� I-A Xh N3 Thomas A.McKean :k Town of Barnstable `J Public Health Division '€ 200 Main Street Hyannis,Massachusetts 02601 $, w Thomas K.Lynch w . ,,,M.. _}, Barnstable Town Manager - 387 Main Street Hyannis,Massachusetts 02601 DRemedy Re: once of Availability ofPhasetion Status and Remedial Monitoring Report Former Shell-Branded Gasoline 577 West Main Street H annis,Massachusetts MassDEP - 72, To Whom It May Concern: - In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase V Remedy Operation Status &Remedial Monitoring Report (ROS-RMR)was submitted to the Massachusetts Department of Environmental Protection(MassDEP) for the above referenced location (the disposal site). The report summarizes activities conducted between December 2017 and June 2018. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the,"disposal site' is the operation of an air sparge and soil vapor extraction (AS/SVE) remediation system coupled with monitored natural attenuation (MNA) for the downgradient portion of the plume. Currently the AS/SVE system is not in operation. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conducted on a quarterly basis. A copy of the Phase V Remedy Operating Status Report as well as all other applicable documents pertaining to the subject site,are available for review on the MassDEP website: h!!p://12ublic.del2.state.ma.us/SearchableSites2/Search.as]2x. If you have any questions please call the undersigned at(508)339-3200. Sincerely, SOVEREIGN CONSULTING INC. Lisa M.Stone Rachel B.Leary,P.E.,LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Marc Oler,SOPUS(within report package) Sovereign File-2S874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 • V E ' E I G N C • June 5, Thomas A.McKean Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601 r 4 00 Thomas K.Lynch Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Notice of Availability.of Phase V Remedy Operation Status and Remedial Monitoring Report_ Former Shell-Branded Gasoline Station \577 West Main Street Hyannis,Massachusetts 4 MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase V Remedy Operation Status &Remedial Monitoring Report (ROS-RMR) was submitted to the Massachusetts Department of Environmental Protection(MassDEP)for the above referenced location (the disposal site). The report summarizes activities conducted between October 2014 and May 2015. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site' is the operation of an air sparge and soil vapor extraction (AS/SVE) remediation system coupled with monitored natural attenuation (MNA) for the downgradient portion of the plume. Currently the AS/SVE system is in operation. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conducted on a quarterly basis. Copies of the report can be obtained at the MassDEP Southeast Regional Office in Lakeville, Massachusetts.If you have any questions please call the undersigned at(508)339-3200. Sincerely, - SOVEREIGN CONSULTING INC. Lisa M.Stone Rachel B.Leary,P.E.,LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr,Robert Rule,SOPUS(within report package) Sovereign File-2R874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 �f R,e_0 44�wd ' , r O 7;� June'7;$2016 Thomas A. McKean Town of Barnstable Public Health Division 200 Main Street Hyannis, Massachusetts 02601 Thomas K. Lynch Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Notice of Availability of Phase V Remedy Operation Status and Remedial Monitoring Report Former Shell-Branded Gasoline Station 577 West Main Street Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase V Remedy Operation Status & Remedial Monitoring Report (ROS-RMR) was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location (the disposal site). The report summarizes activities conducted between December 2015 and June 2016. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site' is the operation of an air sparge and soil vapor extraction(AS/SVE) remediation system coupled with monitored natural attenuation (MNA) for the downgradient portion of the plume. Currently the AS/SVE system is in operation. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conducted on a quarterly basis. ` I Copies of the report can be obtained at the MassDEP Southeast Regional Office in Lakeville, Massachusetts. If you have any,questions please call the undersigned at(508) 339-3200. Sincerely, SOVEREIGN CONSULTING INC. ltie• S .Lisa M.Stone Rachel B. Leary,P.E., LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Robert Rule,SOPUS(within report package) Sovereign File-2R874 16 Chestnut Street, Suite 520 0 Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 • ON December"7,2016 Thomas A. McKean Town of Barnstable Public Health Division 200 Main Street Hyannis, Massachusetts 02601 Thomas K. Lynch Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 �p Re: Notice of Availability of Phase V Remedy Operation Status and Remedial Monitoring Report Former Shell-Branded Gasoline Station 577 West Main Street Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance_with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase V Remedy Operation Status & Remedial Monitoring Report (ROS-RMR) was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location (the disposal site). The report summarizes activities conducted between June and December 2016. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site' is the operation of an air sparge and soil vapor extraction(AS/SVE) remediation system coupled with monitored natural attenuation (MNA) for the downgradient portion of the plume. Currently the AS/SVE system is off. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conducted on a quarterly basis. Copies of the report can be obtained at the MassDEP Southeast Regional Office in Lakeville, Massachusetts. If you have any questions please call the undersigned at(508) 339-3200. Sincerely; SOVEREIGN CONSULTING INC. / Lisa M.Stone Rachel B. Leary, P.E., LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Robert Rule,SOPUS(within report package) Sovereign File-2N874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 } SOVEREIGNs ; 16 Chestnut Street,Suite 520-Fo0orougti, MA 02035 rota Thomas A. McKean Town of Barnstable Public Health Division 200 Main Street Hyannis, MA 02601 _ i - J •�y. •(i:riiii:r rr7 ._�t,�rrs.e f�� 3 7.r� i �r 'e rx }� riil r-ri.i.'f it l Ci 114 1 tl 11 3i� itltl t 1111i lltil �l 4 Il t 11� 1 ... .. _,. �� ,,, ._ .. •� -- - - �- �- - - e ON Jurie 7,2017 Thomas A. McKean Town of Barnstable Public Health Division 200 Main Street Hyannis, Massachusetts 02601 Thomas K. Lynch Barnstable Town Manager 387 Main Street =, Hyannis,Massachusetts 02601 Re: Notice of Availability of Phase V Remedy Operation Status and Remedial Monitoring Report Former Shell-Branded Gasoline Station 577 West Main Street Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a.Phase V Remedy Operation Status & Remedial Monitoring Report (ROS-RMR) was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location (the disposal site). The report summarizes activities conducted between December 2016 and June 2017. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site' is the operation of an air sparge and soil vapor extraction (AS/SVE) remediation system coupled with monitored natural attenuation (MNA) for the downgradient portion of the plume. Currently -- the AS/SVE system is not in operation. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conducted on a quarterly basis. Copies of the report can be obtained at the MassDEP Southeast Regional Office in Lakeville, Massachusetts. If you have any questions please call the undersigned at(508) 339-3200. Sincerely, SOVEREIGN CONSULTING INC. Lisa M.Stone Rachel B. Leary,P.E., LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Marc Oler,Equilon(within report package) Sovereign File-2P874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 Aj Date: & / 7 TOWN OF BARNSTABLE TOXIC AND HAZARDOUS MATERIALS ON-SITE INVENTORY NAME OF BUSINESS: BUSINESS LOCATION: INVENTORY MAILING ADDRESS: TOTAL AMOUNT: TELEPHONE NUMBER: �8' �7�" `� ✓� 2.0 CONTACT PERSON: 41 :4&&U_1� EMERGENCY CONTACT TELEPHONE NUMBER: Cl": 2"Doo' '732 - 21YQ MSD ON SITE? TYPE OF BUSINESS: 41gs, U INFORMATION/REC MMENDATIONS: -9 1"AW Fire District: r Waste Transportation: Last shipment of hazardous.waste: Name of Hauler: Destination: Waste Product: Licensed? Yes No NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous materials use, storage and disposal of 111 gallons or more a month requires a license from the Public Health Division. LIST OF TOXIC AND HAZARDOUS MATERIALS The Board of Health and the Public Health Division have determined that the following products exhibit toxic or hazardous characteristics and must be registered regardless of volume. Observed/Maximum Observed/Maximum Antifreeze (for gasoline or coolant systems) Misc. Corrosive NEW USED Cesspool cleaners Automatic transmission fluid Disinfectants Engine and radiator flushes Road Salts (Halite) Hydraulic fluid (including brake fluid) Refrigerants Motor Oils Pesticides NEW USED (insecticides, herbicides, rodenticides) Gasoline, Jet fuel, Aviation gas Photochemicals (Fixers) Diesel Fuel, kerosene, #2 heating oil NEW USED Misc. petroleum products: grease, Photochemicals (Developer) lubricants, gear oil NEW USED Degreasers for engines and metal Printing ink Degreasers for driveways &garages Wood preservatives (creosote) Caulk/Grout Swimming pool chlorine Battery acid (electrolyte)/Batteries Lye or caustic soda Rustproofers Misc. Combustible Car wash detergents Leather dyes Car waxes and polishes Fertilizers Asphalt & roofing tar PCB's Paints, varnishes, stains, dyes Other chlorinated hydrocarbons, Lacquer thinners (inc, carbon tetrachloride) NEW USED Any other products with "poison" labels Paint &varnish removers, deglossers (including chloroform, formaldehyde, Misc. Flammables hydrochloric acid, other acids) Floor &furniture strippers Other products not listed which you feel Metal polishes may be toxic or hazardous (please list): Laundry soil & stain removers (including bleach) Spot removers & cleaning fluids (dry cleaners) Other cleaning solvents Bug and tar removers Windshield wash WHITE COPY-HEALTH DEPARTMENT/CANARY COPY-BUSINESS OIL WASTE OIL OIL FILTERS ANTIFREEZE WASTE ANITFREEZE GASOLINE WASTE GAS DIESEL FUEL W/W FLUID ATF HYDRAULIC/ MISC. MISC. MISC. 1VE[SC. BRAKE FLUE[) COMIVIBUSTIBLE FLAMMABLE CORROSIVE PETROLEUM (GEAR OIL/GREASE/ LUBRICANTS) FREON ACETYLENE CAR WASH CAR WASH PAINTS/ WAX DETERGENTS THINNERS SEALANT CLEANING BATTERIES/ POISION/TOXIC CAULK/GROUT SOLVENTS BATTERY ACID FERTALIZERS WASTE SOLVENT BLEACH DISH WASH AND MSDS DETERGENTS „\ MANIFESTS &Pbc �� •- nod J �c_ a03 Town of Barnstable �F'THE t Regulatory Services Thomas F. Geiler,Director Public Health Division BARNSTABLE, Thomas McKean,Director 1639. ,�,� 200 Main Street, Hyannis,MA 02601 ATfD MA'S A Phone: 508-862-4644 Email: health(a)town.barnstable.ma.us Fax: 508-790-6304 Office Hours: M-F 8:00—4:30 June 26,2007 Mr. Al Naoum West Main Gas C577 W.Mai�naSt% Hyannis, MA 02601 Dear Mr.Naoum: Thank you for your time and cooperation during the hazardous materials inventory and site visit at West Main Gas on June 25, 2007. This letter contains information from that visit that will help you become compliant with and remain compliant with the Town of Barnstable Ordinance Chapter 108: Hazardous Materials. Enclosed are copies of the Chapter 108: Hazardous Materials ordinance,the toxic and hazardous materials on-site inventory, a sample contingency plan,an application to store hazardous materials, and a list of licensed hazardous materials haulers. Please note the problems and the recommendations or orders identified at your place of business during the hazardous materials inspection: PROBLEM: • No MSDS on site. ORDER: • Please obtain MSDS for all products being used or sold at your place of business. PROBLEM: • No Hazardous Materials Permit for fiscal year 2007-2008. ORDER: • Obtain a Hazardous Materials Permit for the fiscal year 2007-2008 from the Town of Barnstable offices at 200 Main Street, Hyannis,MA 02601. PROBLEM: • No current plans of the facility on file showing a connection to the Town sewer line. ORDER: • Please obtain a plan from your engineer showing the plan of the property with sewer lines, monitoring wells, and all underground tanks. PROBLEM: • Underground tank on the site is full of an unknown substance. (Waste water or oil/water separator discharge etc.) ORDER: • If the tank is not connected to the sewer line,have the water in the tank tested. PROBLEM: • Monitoring wells number 9 and 10 show high levels of volatile organic compounds. ORDER: • Continue to monitor these wells. Your business is located in a wellhead protection area in which the groundwater feeds our drinking water supply. Monitoring will provide you with the environmental condition of your property. On Site Inventory Total The Toxic and Hazardous Materials On-Site Inventory from June 25, 2007 shows that you have approximately 178 gallons of toxic and hazardous materials being used, stored or sold at West Main Gas, 577 W.Main St.,Hyannis, MA(Please see enclosed Toxic and Hazardous Materials On-Site Inventory sheet). The Board of Health has determined that the using, storing, generating and disposing of over 111 gallons of hazardous materials per month requires businesses in the Town of Barnstable to obtain an annual Hazardous Materials License.You are required to purchase this license from the Town of Barnstable Town Offices,200 Main Street,Hyannis,MA 02601. Why are these recommendations being made for West Main Gas? • This information is intended to educate you, a business owner/operator in the Town of Barnstable,in order to keep.your business operations in compliance with local, state and federal toxic and hazardous materials laws so that you can avoid future regulatory problems. • Complying with the Town of Barnstable Ordinance, Chapter 108: Hazardous Materials can prevent contamination of Barnstable's existing and future drinking water supply, prevent environmental contamination which can bankrupt site owners, lower or destroy land values, drive out residents and industry, depress local economies and endanger public health. If you have any questions about these observations or you need further information, guidance or assistance,please do not hesitate to contact the Public Health Division. Si rely 'Ali ha L. Parker Hazardous Materials Specialist All orders to correct violations of Chapter 108 of the Town of Barnstable Ordinance: Hazardous Mateiials shall be completed upon receipt of this letter. as A. McKean,RS, CHO Director of Public Health CC: Donna Miorandi, Health Inspector Dave Anderson, Engineering Enc. On-Site Inventory(copy) Chapter 108 (copy) Contingency plan(copy) Application to store Hazardous Materials List of Licensed Hazardous Materials Haulers f Fire Department retains original application and issues duplicate as Permit- . Q, � �C?772�J2Q�YLL112C7�/fi�12 Q� 12��:5 aixGrrLenCa�(; 'i�xe CJ&a4*cee.— R3ocrOcz/ gDxe�� APPLICATION and PERMIT Fee: l0.a, for storage tank removal and transportation to approved tank disposal yard in accordance with the provisions of M.G.L. Chapter 148, Section 38A, 527 CMR 9.00, application is hereby made by: Tank Owner Name (please print) <; Co X s ar✓re p appryng ror pennrt/ _ Address o - . �P-G U=1 tT �q[ Slreer City Slags Zip Company Name �V�S L 1� HS-'(a-'k7b Co. or Individual C oUD PMr Paw Address 1 s 'Z 1�1.�1s�(��1;' ��z��l'+�MPc�� Address i L, L y AZZ�P �VK—_` `y DSnb� f applying or perm') Signature(if applying for permit) v CI'Certified Other 'IFCI`Certified O LSP;# Other on x �W o Tank Location � � )� l dy \� V E R- I L SteetAddfess Tank Capacityr(galfons)-6 U(�O Substance Last Stored 1 \ n Tank Dimensions(diameter x length) � t�D Q g( Remarks: >t , Firm transporting waste State Lic. It Hazardous waste manifest# E.P.A.# C1� Approved tank disposal yard J i S A Tank yard n D P Type of inert gas (-C V7-_ Tank yard address . City or Town FDID# U ( 1 ZCi Permit# I Date of issue Date of expiration Dig safe approval number. 7-00-2—�-J 1 0( (on g a Toll Free Tel. Number-800-322-4844 Signature/Title of Officer granting permit 1��I i di �� IRE pREVER RV IEAW' HYAfu IR FIR n[:PAPTMMT 4ri N f;N rrNn a � ��. After removal(s) ('Consumptive Use'fuel oil tanks exempted)send Form FP-29OR signs ocal ire Departrent`to'etfice of.t e'�T State Fire Marshal, UST Regulatory Compliance Unit`_ 1-025,,Stow,NA-0177-5:— ^ �--HYA i �AQ 60 *International Fire Code Institute 07 1f1;, ►ld�®C� —� 1 �� FP-292 ) revised 4/97 g ( �7 oy1 1 Fire Department retains original application and issues duplicate as Permit- 0- b. � �e��2x!irrae7cC d-11uXe CJ�a�scoea — �oaixc�a�C�axe �xvu�n�a Q �� J i APPLICATION and PERMIT Fee: for storage tank removal and transportation to approved tank disposal yard in accordance with the provisions of M.G.L. Chapter 148, Section 38A, 527 CMR 9.00, application is hereby made by: Tank Owner Name (please print) C-0 X r Signature Id appryrrg ru perrrur) Address Skew city Sv/e zip 1 Ml• • t'. .1 . - - r Company Name `�S t-�1Z NSa�u,�r"t .i 1�( Co. or Individual Pnrlt Pm1 Address`-�c(`� � s.«t (r��l;i� � �1'l�M�� Address 'L11J Pr" f applying or perm') `, Signature(if applying for permit) u V ' CI`Certified Other I '(FCI'Certified O LSP# Other Tank Location S/eetAacress Tank Capacity(gallons) A C Substance Last Stored_ 561�4�4 tre Tank Dimensions(diameter x length) Remarks: c ��L Vj k`-�— Firm transporting waste �' � � State Lic. # Hazardous waste manifest# E.P.A.# C1� D � l Approved tank disposal yard .J 'S �01� �l�� Tank yard x D OP Type of inert gas ��C- 7- Tank yard address . PO S V 0 14 t VV\ q�\-- City or Town FDID# �� I Z�— Permit# � Date of issue /491 le)-) Date of expiration �- Dig safe approval number. ��- 1 ` N0 ✓ l Sat oil Free Tel. Number-800-322-4844 Signature/Title of Officer granting permit ninMA"w1r NU r AI\f ll a.r,sr. r re�niv�wi� rlrliC tyr:.flWPtllVftt�l After removal(s) ("Consumptive Use"fuel oil tanks exempted) send Form FP-29OR signe Local Fire D6 all"`694hi 1 to(,�tfff'ceRoJ th,,e,'T - -- �__ State Fire Marshal, UST Regulatory Compliance Unit;P:0rBox-1025/;Stow;MA-01775. �� *International Fire Code Institute FP-292(revised 4/97) rive ueparimem reLZIMS vng,nat appncauUn ana ,ssucs uuNna:are as rannn. J T. 0,3054 APPLICATION and PERMIT Fee: !O•C)o for storage tank-removal and transportation to approved tank disposal yard in accordance with the provisions of M.G.L. Chapter 148, Section 38A, 527 CMR 9.00, application is hereby made by: Tank Owner Name(please print) - 01 C_0 X "'� Qnarure lit ru pemrrtJ Address 7 Z C`� l t_.�tV S ' "C' R G U �? V'�C�- �C=1— �Z�l Cb Street City Stare Zip t .i • r. .I t 111:4114 EIS l�C �� '1 .L bindividual �aLS7 GTL - U C2 � 5 Co.0r I a Z.,. 7companyme � � �rH � C _Pnnt PM1 �. Address 6-NL )li 1) 'W Address 0 MOtN Pmt �A� f applying or permi) , 1(� Signature (if applying for permit) �V � 77 CI`Certified Other '(FCI'Certified D LSP# Other � Tank Location 1`r` Sfeai Adcress City - -_ ----------------- 1 Tank Capacity(gallons) t��3�"O Substance Last Stored A Tank Dimensions(diameter x length) (2) t Y-- 01 Remarks: c�4—�G-VE—NO • • `1(7711 Firm transporting waste State Lic. # Hazardous waste manifest# E.P.A.It Approved tank disposal yard J N'nI�L-5 (a.4!��Iaa' Tank yard Type of inert gas {GFz _ Tank yard address . 0 \0 City or Town FDID# Permit# Date of issue / Date of expiration Dig sale approval number. Z-CX?-2 � 0� ✓ �� Safe Toll Free Tel. Number-800-322-4844I BUR Signature/Title of Officer granting permit "HYAN 'S FIRE PREVENTIQ �A Tr YAUN N FIRF I)FPARTMF T a� �Ir�1 �r.I�nn� �'i Ext After removal(s) ("Consumptive Use'fuel oil tanks exempted) send Form FP-290R signed by Local Fre Department 00 Office of the State Fire Marshal, UST Regulatory m Hanc_ Unit,_P.O.-Box 1025,Stow ..MA-01-775._ HYA NiS, MA 026 'International Fire Code Institufe FP-292(revised 4/97) Make application to local Fire Department Fire Department retains original application and issues duplicate as Permit APPLICATION and PERMIT Fee: for storage tank removal and transportation to approved tank disposal yard in accordance with the provisions of M.G.L. Chapter 148, Section 38A, 527 CMR 9.00, application is hereby made by: • // Tank Owner Name(please print) 9/if // �( L X �J _ tore pame Address �Qg-b A lf'`y-s f7 UC' Street City State zip Company Name �e-rok'e yf?l5T/5i/1#fielLS Co.or Individual �eV D�I'C -5�; 'U/C'e pry n f prtr Address �95&)�/Trdue Ave /9Pd11,4* Address / 5 �D�/P�f�7��/ l/e /9�l' yd soy Signature if applying forpermit) Signature(if applying for permit) PrW �( ❑ IFCI'Certified Other ❑ IFCI'Certified ❑ LSP# Other �G ? Tank Location s 7 LlJ/�/ %w 37pee% Steel Actress C;y�— Tank Capacity(gallons) //0IV -S Substance Last Stored /4�)1141.91iif Tank Dimensions(diameter x length) t Remarks: "Firmtransp Forting State Lic.# Hazardous waste manifest# E.P.A.# Approved tank disposal yard �ve--Tank yard# Type of inert gas Tank yard address /< S S I F� q,?-� Ave- �Oc O7 r City or Town FDID# Z Permit# V 3 CC-? Date of issue v .�u'� Date of expiration L'Lo Z Dig safe approval number 0.0 a y66 15-6 i oil Free Tel. Number-800-322-4844 Signature/Title of Officer granting permit ,� � ; N�I �� PREVENTION �11 � U HYANNIS FIRE DFPARTMFMT 95 HIGH SCH001 4n. FYT After removal(s) ("Consumptive Use'fuel oil tanks exempted)send Form FP-290A sign -ocal FirekDepartment to Office of the State Fire Marshal,UST Regulatory Compliance Unit, P.O.Box 1025, Stow,MA 01775. tIY�1NI�IIS, IVIA 02601 International Fire Code Institute 'P-292(revised 4/97) Lim March 27,2013 Via e-mail Cynthia Martin Hazardous Materials Specialist Barnstable Public Health Division 200 Main Street Hyannis,MA 02601 Re: Results of Groundwater Sampling Conducted February 19-20,2013 At and in the Vicinity of: Former Shell-Branded Service Station 577 West Main Street Hyannis, MA RTN 4-16772 Dear Ms. Martin; Pursuant to your authorization, Sovereign Consulting Inc. (Sovereign) personnel collected groundwater samples from monitoring wells associated with the above disposal site on February 19-20, 2013. This letter presents the analytical laboratory report summarizing the results of the sample collection and analyses consistent with 310 CMR 40.0017(3) of the Massachusetts Contingency Plan, as required by 310 CMR 40.1403(10)(b). Sovereign has conducted a data validation review of the laboratory results,and the laboratory report has been attached for your information, in addition to Massachusetts Department of Environmental Protection (MassDEP) Form BWSC-123. Please contact the MassDEP or the undersigned if you have any questions or require additional information. Please note that public involvement opportunities are available to you pursuant to 310 CMR 40.1404 for Tier classified sites. Motiva Enterprises LLC and Sovereign thank you for your cooperation in this matter. Sincerely, SOVEREIGN CONSULTING INC. Lisa M.Stone Project Manager Attachments: MassDEP Form BWSC-123 Laboratory Data Report cc: with attachments: Robert Rule,Motiva Enterprises LLC Sovereign File-2R874 16 Chestnut Street, Suite 520 • Foxborough,MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 September 11,2012 Thomas A. McKean Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601 Thomas K. Lynch Acting Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Availability&Summary of Phase III RAP Addendum Report&BWSC-108 Comprehensive Response Action Form Former Shell-Branded Retail Station 577 West Main Street Hyannis, Massachusetts RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase III Remedial Action Plan (RAP) Addendum Report was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above-referenced location (the disposal site). This Phase III RAP Addendum Report documents the planned remedial activities associated with RTN 4-16772. The selected remedial alternative (RA) for this disposal site is air sparging combined with soil vapor extraction to address residual groundwater impacts. A copy of the Phase III RAP Addendum Report, as well as other applicable documents pertaining to the subject site, are available. for review at the Massachusetts Department of Environmental Protection Southeast Regional Office in Lakeville, MA. If you have any questions please call the undersigned at (508) 339-3200. Sincerely, SOVEREIGN CONSULTING INC. re ,({; Lisa M.Stone Rachel B. Leary,P.E., LSP Project Manager Senior Project Engineer cc: MassDEP SERO D.Weeks-Motiva Sovereign File-2E874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 September 11,2012 Thomas A. McKean Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601 Thomas K. Lynch Acting Town Manager 387 Main Street - Hyannis,Massachusetts 02601 Re: Availability of Phase IV Remedy Implementation Plan Addendum Former Shell-Branded Retail Station 577 West Main Street Hyannis,Massachusetts RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.0874, this correspondence serves as notification that a Phase IV- Remedy Implementation Plan (Phase IV RIP) Addendum was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above-referenced location (the disposal site). This Phase IV RIP Addendum outlines the design, construction, and implementation of the Comprehensive Remedial Action as identified in the Phase III Remedial Action Plan (Phase III RAP) Addendum associated with RTN 4-16772. The selected remedial alternative for this disposal site is air sparging combined with soil vapor extraction to address residual groundwater impacts. A copy of the Phase IV RIP Addendum, as well as other applicable documents pertaining to the disposal site, are available for review at the Massachusetts Department of Environmental Protection Southeast Regional Office in Lakeville, MA. If you have any questions please call the undersigned at(508) 339-3200 Sincerely, SOVEREIGN CONSULTING INC. 12 Lisa M.Stone Rachel B. Leary, P.E., LSP Project Manager Senior Project Engineer cc: MassDEP SERO D.Weeks-Motiva Sovereign Fite-2E874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 SOVEP, EIGN CONSULTING June`7 2016 ` Thomas A. McKeany Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts.02601 Thomas K. Lynch. Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Notice of Availability of Phase V Remedy Operation Status and Remedial Monitoring Report Former Shell-Branded Gasoline Station 577 West Main Street Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase V Remedy Operation Status & Remedial Monitoring Report (ROS-RMR) was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location (the disposal site). The report summarizes activities conducted between December 2015 and June 2016. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site" is the operation of an air sparge and soil vapor extraction(AS/SVE) remediation system coupled with monitored natural attenuation (MNA) for the downgradient portion of the plume. Currently the AS/SVE system is in operation. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conducted on a quarterly basis. Copies of the report can be obtained at the MassDEP Southeast Regional Office in Lakeville, Massachusetts.If you have any questions please call the undersigned at(508) 339-3200. Sincerely, SOVEREIGN CONSULTING INC. Lisa M.Stone Rachel B. Leary,P.E.,LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Robert Rule,SOPUS(within report package) Sovereign File-2R874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 SOVEREIGN • P! 9 December 7,2015 Thomas A.McKean i Town of Barnstable tm,. Public Health Division C�I 200 Main Street Hyannis,Massachusetts 02601 Thomas K lynch " Barnstable Town 387 Main Street Hyannis,Massachusetts 02601 � ." � Re: Notice of Availability of Phase V Remedy Operation Status and Remedial Monitoring Reporter Former Shell,Brarid asolinel Station 577 West Main Street a n Hyannis,Massachusetts MassDEP RTN 4 16772 To Whom It May Concern. In accordance with the Massachusetts Contingency�Ptdri (MCP)2310 CMR_40.1403 (3)(e), this correspondence serves"as notification that a Phase V. Remedy ":Operation SMtus & Remedial Monitoring Report(ROS-RMR)was.",submitted to the Massachusetts Deparfin6t'of Environmental Protection (MassDEP)0-'for the,above referenced location (the disposal site). The report summarizes actrvit es conducted between June and November 2015 A summary of findmgs and conclusions for response-actions at` the disposal site have been provided in previous reports submitted to the Massachusetts epartment�_bf Environmental Protection (MassDEP). The selected remedial action alternativoJor the "disposal site' is the operation of an air,sparge and 5soil,,vapor extraction (AS/SVE) emediation system coupled with monitored natural"attenuation (MNA)for the',downgradient portion of the plume. Currently the AS/SVE system is'iri operation. Continued monitoring'of the dissolve-phase gasoline plume and geochemical conditions within the plume,.and up,and:downgradient of the.plume are being conducted on a quarter"1"y basis Copies of the report can be obtained at the MassDEP Southeast=Regional Office in Lakeville, Massachusetts. If you have any:questions please call the'undersi6ed at(508)339-3200. Sincerely, SOVEREIGN CONSULTING INC. Lisa M.Stone Rachel B.Leary,P.E.,LSP Senior Project Manager. Senior Project Manager cc: MassDEP SERO(within report package) Mr.Robert Rule,SOPUS(within report package) Sovereign File-2R874 16 Chestnut Street,Suite 520 Foxborough,MA 02035 Tel:508-339-32oo Fax:5o8-339-3248 a SOVEREIGN • June 6,12014' Thomas A.McKean Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601> , Thomas K.Lynch Barnstable Town Manager - 387 Main Street Hyannis,Massachusetts 02601' Re:. . Notice of Availability of Phase V Remedy Operation Status and Remedial.Monitoring Report Former Shell-Branded Gasoline Station 577 West Main Street Hyannis,Massachusetts - MassDEP RTN 4-16772 To Whom It May Concern:- a In accordance with, the -Massachusetts Contingency Plan (VCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification.that a Phase V Remedy Operqtion Status &Remedial Monitoring Report (ROS-RMR)was submitted to the Massachusetts Department of Environmental Protection(MassDEP)for the above referenced location (the disposal site). The report summarizes activities conducted between December 2014 and June 2014. A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site" is the operation of an air sparge and soil vapor extraction (AS/SVE) remediation system'coupled with monitored natural attenuation (MNA) for the.downgradient portion of the plume. Currently the AS/SVE system has been cycled off due to low influent concentrations. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the.plume, and up and downgradient of the plume are being conducted on a quarterly basis. Copies of the report can be obtained at the MassDEP Southeast Regional Office in Lakeville, Massachusetts.If you have any questions please call the undersigned at(508)339-3200. Sincerely, SOVEREIGN CONSULTING INC. Q i4 ZE Lisa M.`Stone Rachel B.Leary,P.E,-hSP a� fi Senior Project Manager'; Senior Project Manage cc: MassDEP SERO(within report package) ram" Mr.Robert Rule,SOPUS(within report package) Sovereign File-2R874 t 'tea 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339 3200 • Fax: 508-339-3248 OV E R E I G N CONS n M. December}112013 Thomas A.McKean Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601 John C.Klimm Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Notice of Availability of Phase V Remedy Operation Status and Remedial Monitoring Report Former Shell-Branded Gasoline Station - 577 West Main Street Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase V Remedy Operation Status &Remedial Monitoring Report (ROS-RMR) was submitted to the Massachusetts Department of Environmental Protection(MassDEP)for the above referenced location (the disposal site). The report summarizes activities conducted between June 2013 and December 2013. i A summary of findings and conclusions for response actions at the disposal site have been provided in previous reports submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action alternative for the "disposal site' is the operation of an air sparge and soil vapor extraction (AS/SVE) remediation system coupled with monitored natural attenuation (MNA) for the downgradient portion of the plume. Currently the AS/SVE system is being cycled on and off due to a high water table. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are beingconducted on a quarterly q Y basis. Copies of the report can be obtained at the MassDEP p p Southeast Regional Office in Lakeville, , Massachusetts.If you have any questions please call the undersigned at(508)339-3200. Sincerely, SOVEREIGN CONSULTING INC. x Lisa M.Stone Rachel B.Leary,P.E.,LSP Project Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Robert Rule,Motiva Enterprises LLC(within report package) Sovereign File-2R874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248 2 t Make application to local Fire Department. DO NOT make application to Department Services or State Fire Marshal. + APPLICATION FOR PERMIT To Maintain an Existing/New Undergrottnd Storage Tank Facility Regulated under 527 CMR 9.00 To: Head of Fire Department City,Town or District: -- fans Date: X -, S Application is hereby made for a permit to maintain an existing/new storage tank facility as required by 527 CMR 9.00: Location of Property: X S 7 7 Gy �' M B. n S — `�a 1 S Iyl 7 l Street address Owner of Property; Full name of person,firm or corporation Number of Storage Tanks:, 3 Underground Signature of Owner or Authorized Representative: Fee paid:$ �d n M.G.L Chapter 148, section 10A) Fire Department's copy—To be filed with FR290) --- ----------------------------.------------ - __ -=-- Vf2eo�n2�n2o�uG�e� o� )7k PERMIT . s To Maintain an Existing/New Storage Tank Facility for Underground Storage Tanks Regulated under 527 CMR 9.00 In accordance with the provisions of 527 CMR-9.00 this permit to maintain an existing/new storage tank facility is granted to: C Location of Property:_X 7-7 Lt l e's�� 0_1 W e tS� Street address J Owner of Property: X II'— } �". Full name of person,firm or corporation a5 Number of Storage Tanks: 3 Underground �� -(E�'� Facility to be maintained in accordance with the restrictions described below: rit55G?10� -- 2 10,000 Gal . Gasoline T nks 1 ( ._1 ) ~ 6,000 Gal. Gasoline. Tank / Split Tank / . ( 1 ) 4,000 Gal. Diesel Tank Fee paid:$ � (M.G.L. Chapter 148, section 10A) This permit will expire 12/31/2015 r Date Si ghatfftfakVHftdA6f FILID nt or p t esignee "�,gyi7ty.xF �:h c'F V 1�W 0 65'-L !1. 527 CMR 9.07(M)(1)issuance and renewal contigent upon passirig the inspection conducted PLAS a lati a27 G At I;�P�4{ (owner's copy—To be posted at the storage facility) 95 Hll;s.t VHVIOL RD, Er I FP-290 Permit(revised 05108) `h at I4, 3„ 0.2601 . The Commonwealth of Massachusetts FP-6 DEPARTMENT OF FIRE SERVICES P.O. Box 1025 - State Road - Stow, MA 01775 Hyannis, Ma 11/17/04 FUEL/GAS TANK INSTALL PERMIT In 005167 PERMIT TYPE In accordance with the provisions of: 148-section: 9-'to wit: 527 CMR 9.00, This permit is granted to: M.P. & SONS CONSTRUCTION. INC. for to to: INSTALL the following: FUEL TANKS at the following property: PropertyName WEST MAIN GAS. PHONE No.&Street 577 WEST MAIN STREET #110-889 FAX USE GROUP MAP I PARCEL CONTACT DESCRIBE INSTALL(2) 10,000 GAL. GASOLINE UST AND(1)6,000/4,000 GAL.SPLIT GAS/DIESEL UST PERMIT REF# PROJECT 611 RESTRICTIONS �*PER�PLANS SIJBMI�ED'. '� i REQUIREMENTS: CALL DISPATCHER PRIOR TO AND FOLLOWING WORK AND GIVE THE ABOVE PERMIT NO. NOTE ** CALL WHEN COMPLETED FOR FINAL INSPECTION ** APPLICANT INFO M.P. & SONS CONSTRUCTION, INC. 13 Russells Mills Rd. So. Dartmouth, Ma 02748 508-992-6609 LICENSE TYPE LIC.# EXPIRES APP. PHONE APP. FAX 508-984-4694 PRINT NAMEt � SIGNATURE PAID $30 RANTED,;: (,M+1Qi7/04 Will expire on LT. DONALD CHASE ;�GO ' LOGGED BY DL GRANTING FIR&0FFICI .L2) 1-1 INSPECTION INFO Hyannis Fire Department - #01922 508-775-1300 Fax 508-778-6448 Make application to local Fire Department. Fire Department refains original application and issues dupli-ate as Permit. �y %i; . �e�iiu�n�nCo�� 'iixe��a�icea— �c oa�xu�a��rixe ✓"�e�sCra�r� APPLICATION and PERMIT I Fee: for storage tank removal and transportation to approved tank disposal yard in accordance with the provisions of M.G.L. Chapter 148, Section 38A, 527 CMR 9.00, application is hereby made by: • Tank Owner Name(please print) 9 (f e ( L X /� i apptyvig orperma Address _.� D /7�r%/iIJS �7 UC' Signature U✓�G'U f dC�ali� { �� D p e .5— Suvat City State Zip • Kim, fi M. • • • Company Name _ JY ��ti%) 5 Co.or Individual P. n / Print // Address_ �� /Ji G' XP. /JE'c��Tfl-,* Address /S �DA��/�?c, �J.de- A lid sely Pran pn„t �/� Signature if applying for ermit) Signature(if applying for permit) ❑ IFCI'Certified Other ❑ IFCI'Certified ❑ LSP# Other Tank Location :S7 Ste/et-Address city Tank Capacity(gallons) 07� Z? 6 Substance Last Stored Tank Dimensions(diameter x length) Remarks: • . Firm transporting waste State Lic.# Hazardous waste manifest# E.P.A.# Approved tank disposal yard Tank yard# Type of inert gas Tank yard address /Ile 12r` City or Town FDID# L 2 Permit#, Date of issue V. [1.40 Date of expiration Dig safe approval number. 0 O 42 �1 o(v S� i oll Ffee Tel Nninber-800-322-4844 Fri Signature/Title of Officer granting permit y,�y After removal(s) ("Consumptive Use"fuel oil tanks exempted)send Form FP-29OR signs ylocal Fire Department to Office of the State Fire Marshal, UST Regulatory Compliance Unit, P.O.Box 1025, Stow,MA 01775. E 'International Fire Code Institutes P-292(revised 4/97) 'i r No 2 02: 19P Dav L. Bigelow 78opate 2G 3189 P. 5 Fire Department retains original application and issues du as Permit_ �Cli;�i7�'LQiJ'LLlJ2C�iL��'L O�C=�i�'u,u'Q�l'LLIdP�'l n � � e��aa G�nernC a1�i q,&CJ exvWe6— ✓30axd,�C-5 ixa Px�je 4zio APPLICATION and PERMIT Fee: LO.C) for storage tank removal and transportation to approved tank disposal yard in accordance with the provisions of M.G.L. Chapter 148, Section 38A, 527 CMF9 9.00, application is hereby made by. .i •M r Tank Owner Name (please print) < C X p—tv7a f appr.9 rd purmn/ Address > Z L t,�l� LV� �G U �1 V'�L� F=T-- r�Z� r✓� straw city sbta Zp Company Name ��5 l-�C --H S a�L► P�1�04, Co. or Individual 1-0 pmv nmt Address`-(n( � 1J1i1" t�(s�l PcM Address1`.�_��De�Qr Z7� H1� _\ 1yDSi PA Ptinr f applying or permi) ,` Signature(if applying for permit) rA JAr_ It CI"Certified Other P FCI- Certified ❑ LSP # Other Tank Location Slept Fdcless city t Tank Capar_ity(gallons) �� on Substance Last Stored t k � O ` 1 AcPDf'0 > Tank Dimensions(diameter x length) � _ )c Remarks: l Firm transporting waste � K��T�i � State Lic.# Hazardous waste manifest# E.P.A.# Approved tank disposal yard -J AMfL z> ��1�11 f� Tank yard 9 Q OA['� Type of inert gas R` -GFr_ Tank yard address _ 0 5 To 1 A r City or Town FDID# tJ (� Permit# ON Dale of issue d? Date of expiration Di safe approval number. Z-nO Z� 1 Q�✓ 1 g a Tdll',;Free�l'el".Number-800 322-4844 9 pp �� -�wp' .`.� Signature I Title of Officer granting permit + �`� ��O^� .aGX°` r ` VVV &'� (f Attar removals)("Can�umptive Use'fuel oil tanks exempted)send F�orrneFp"i' signe_w Deal Fire Department to Office of the Slate Fire Marshal, UST Regulatory ryCompliance Unit, P.O. Box 1025, Stow, M01ps.,� G a o a Fire Code Institute 'Inlem U n Iel ,FP-29�(revised 4/97) A 1 - L� � � ��C ��.� �SS � A '�IDS . Ne 02 02: 19p Da L. Bigelow 78f2G 3189 p. 3 r toV r i.fffldan./Ll we.L6 l Dye t..re rt o� Stu sma' a - d4w od the State 7tu X=4"' RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK ND E Fm FP 191 NAME AND ADDRESS OF APPROVED TANK YARD G.G n - 29 Y dell:" q,4., APPROVED TANK YARD NO. vvf Tank Yard Ledger 502 CMR 3.03(4)Number: Z 1{S-7 5L I cerby under penalty of law I have personally examined the underground steel storage tank delivered to this'approved tank yard'by firm,corporation or partnership K Fs�Lw-rs 31yT t 1-- and accepted same in conformance with Massachusetts Fire Prevention Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid penTul was issued by LOCAL Head of Fire Department. FDIO>f _ 2: 2 to transport this tank to this yard. me and o rtttle o p oved tank yard owner or owners auuthorizetl�esentative: SlCfATVRE TITLE Q{ DA E SIGNED This signed recb-ipeof disposal must be returned to the local head of the fire department FDID# 1 �— —pursuant to 502 CMR 3.00. EACH TANK MUST HAVE A RECEIPT OF DISPOSAL A ui TANK REMOVED FROM TANK DATA Gallonsco Previous Contents CA& � } '�' � 3 S .r Diameter 8 Length, Date Received I 62-Lo ®305 1 Fin Departmwt Permlt,# Serial#(if available) i Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form(FP290,or FP290R)to : UST Compliance, Office off the State Fire Marshal,P.O.BOX 1025 State Road,Stow, MA 017�5. TOWN OF ^BARE STABLE UNDERGRC7UND 'FUEL AN,D. CHEM I C _L;° STORAGE REGISTRATION 00 X, y MAP NO. PARCEL NO. ADDRESS OF: TANK 577 WE CRA1GV1LL s kP9A!N/OLD: I!r V i LL AGE MAILING ADDRESS ( I F D I FFERENT FROM .ABOVE) . 400 BLUE 44TT.T. DR. . idESTtr'OdD, t1A 02090 OWNER NAME:.. SF€ELL OIL doi TPANY' PHONE: 617-326-8210 INSTALLATION ATE: 1979 �3o BY _ a HLLSERt� c0 INSTALLER ADDRESS: sout GHELFISFORD s PIA -CERT.140. .TANK'LOCATIONb DGaQPt I DC TANK t_OQAT I ON -W S TH`pwmwFmCQT TQ ICU 2 LD I NO) CAPACITY 1QM TYPE OF TANK FIBERGLASS AGE. .10 YRS .'FUEL/CHEMICAL GASOLINE."_', TESTING CERTIFICATION Cx] PASS C ] FAIL DATE LEAK DETECTION Cy-7 CHECK IF N/A ^TYPE/BRAND RE JACKET ZONE OF CONTRIBUTION C YES C ] 'NO DATE TO BE REMOVED. F � PERMIT ISSUED [ ]: YES C ] NO DAT.;E r RE DEPT. CONSERVATION C ];CHECK IF N/A:' DATE BOARD OF HEALTH TAG N0. C ] DATE * PLEASE PROVIDE A SKETCH SHOWING THE, TANK LOCATION ON THE HACK OF THIS CARD . s?k A �f1r t t r MVA" s :..�,.� ,-r....•L.,l,+` i... `s,/.M-y _,n,x,_k'+G .-L ..�. ...�_.�.�..r.....�._.... ._..c _.o.�. Nov` 15 02 02. 20p Dav ' d L. Bigelow 78 2B 3189 p. 7 Fire Department retains original application and issues duplicate as permit_ APPLICATION and PERMIT' Fee: for storage tank removal and transportation to approved tank disposal yard in accordance with the provisions of M.G.L. Chapter 148, Section 38A, 527 CMR 9.00, application is hereby made by- Tank Owner Name (please print) X `1 '' II .rgeau�e; appgng iur Pnmw/ II Address Z L7 (V �tUS- pU��l��V�� Z-� us Sf/oa Cary Srar. ZAP Company Name �`��L � ��S�RLL?c l.�D(y ( Co.or Individual 6CoLj:)G, Pnnr - PM( -T AddressrV{'�� Address �� f�[.ZAP ��(Y�_ \-A:1DnIS�D N4 kgrr-atuK%--(f applying or permf)'° i u' ' Signature (it applying for permit) t V ' ( il AJA I CI"Certified Other XFCI-Certified ❑LSP# Other . r • Tank Location -S -7-7 �.J(� 5( dy\1'c Ll1 �„ '��(z { `-��} {,kkqA 1:—S - srear Aceress C+b Tank Capacity(gallons) r�Qn _-_ _ Substance Last Stored Tank Dimensions(diameter x length) t k_3 �_I [�I?_�rt>Sc Remarks: C`^i—�6-�L&— V-)IN`-I— Firm transporting waste-- 1:LC -l�!l� State Lic.4 Hazardous waste manifest# E.P.A. It Approved tank disposal yard Tank yard: _ 00 Type of inert gas'D P �C�7- -_Tank yard address . PC) 5 TO ►4l L City or Town FDIC)# ��l ZZ Permit# � Date of issue l /�; 4 y Date of expiration �� `�t �=(� L-- Z Z 0 U, ` Dig safe approval number. 1 1 sat oll,F4e"Tel Number-800-322-4844 Signature/Title of Officer granting permit After removal(s) ('Consumptive Use"fuel oil tanks exempted) send Fo�1FP-290R si he ;Local Fire Department to Office of me State Fire Marshal, UST Regulatory Compliance Unit, P.O. Box I025j1Stow,°MA 01 'Intemational Fire Code Institute =P-292(revised 4/97) t G- ALO Ndv 1!5 02 02: 19p David L. Bigelow 781 326 3189 p. 2 0 DG,luizt�Irl�it ;7uu Sew�ra - d�rie o� tAe Sid& ;ICu U401444l `C � _ RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK ' Fum FP 291 NAME AND ADDRESS OF APPROVED TANK YARD JI' C'� -�` �`'`' ei "' APPROVED TANK YARD NO. Tank Yard Ledger 502 CMR 3.03(4)Numbef: I certify under natty of law I ve personally examined the underground steel storage tank delivered to this'approved tank yard'by firm,corporation or partnershI — WT �"� and accepted same in conformance with Massachusetts Fire Prevention Regulation 502 CMR 3.00 Provisions for Approv g Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL Head of Fire Department. FDID# 0 �_ f 2 to transport this tank to this yard. n�olffilitlle of appro ed tank yard owner or owner uthonzed representative: IGN u E TITLE DAT EED This signed receipt f disposal must be returned to the local head of the fire department FOIDti pursuant to 502 CMR 3.00. EACH TANK MUST HAVE A RECEIPT OF DISPOSAL .TANK REMOVED FROM TANK DATA Gallons �i�` �� QT71 . AIA1 t4"4�.�,�R �tIA (Na and Strom) Previous Contents Gp,Sr�� (+1 ".4A gj Length - 'T S3 �NC��+ `*� (City or Turwn) Diameter a Date Received 11 12- 2. Fire Department Permit#.' Sarial#(if available) Tank IX.#(Form FP-290) ank IX.#(For or to mail revised copy of Notification Form(FP290,or FP290R)to : UST Compliance, 01775. Office of the State Fire.Marsb 1,P.O.BOX.1025 State Road,Stow,- MA.. L TOWN OF BARN.STABLE UNDERGROUND FUEL AND CHEMICAL`':STORAGE .REGISTRATION -MAP. N0. ( _PARCEL NO. ADDRESS F OF TANK. .577 JEST t`IAIVOLD-C_AlGVILL8 VILLAGE MAILING ADDRESS ( IF DIFFERENT FROM ABOVE) •,' ` 400`�LU '-�HItL DP.�. WESTWOOD, IVIA 02090 OWNER NAME., SHELL OIL :COMPANY. PHONE: 617-326-3210 INSTALLATION . DATE: .:. 1979 HY, J D.JLALLBERG . INSTALLER 'ADDRESS ('I 'CERT.NO.. *TANK LOCATION: 0K 620F4,I-321M ..TANK` l_OQAT 2 ON; ,W I'TH PtGflF�1mc-r TO' mU I LLD f NO) CAPACITY f m TYPE OF TANK YRS -F.UEL/CHEMICAL A CAT TMV TESTING CERTIFICATION :._.[ ] .PASS [ :] FAIL DATE LEAK: DETECTION; C ] CHECK "-IF N/A TYPE/BRAND RED ALtig y-. ZONE OF CO,NTR I BUT I ON L ] YES [ ] NO DATE TO HE REMOVED .] FIRE.,bEPT PERMIT .ISSUED ;[ ] YES C ] `:'NO DATE CONSERVATION CHECK IF. N/A: DATE ~ . .;.� .. BOARD :OF HEALTH TAG N0. [ ] DATES f * PLEASE RROVIDE A` SKETCH SNOWING THE TANK LOCATION DN THE BACK OF THIS CARD ' Nett' 15 02 02: 19p Da v L. Bigelow 78f2G 3189 p. G Fire Department retains original application and issues duplicate as Permit- -09�_ �, _ e end a �i�e C-J Diced— ✓c7 oa�r�o�C rixe 7�/ n o n V J•4 APPLICATION and PERMIT I Fee: for storage tank removal and transportation to approved tank disposal yard in accordance with the provisions of M.G.L. Chapter 148, Section 38A, 527 CMR 9.00, application is hereby made by: ,Tank Owner Name(please print) ��,r� t C- i tC-1 1 X, 1 a Address Z Cam. l L��ti lit(z . P R o U�t>EAgt'_, - , 10Z ` bb s Svaa COY Sias. Z'p ti ,Ir-I I I I r.1 i Company Name Co, or Individual PM Rot Address' i�f~ ��11i C�fi,l(r�it1t�_ � �i-��c�� Address 1 A k-Z7 iX_ 1 qr -"J 17S y �!gr at- Uf applying or penni) Signature (if applying for permit) CI`Cartified Other 'fFCI"Certilied O LSP# Other Tank Location -5 -7-7 �-J Y-�4 S 4I'=G F�T #,k-ktA T--S KP--I SIBBI Aticraas QY Tank Capacity(gallons) 1a on t7 Substance Last Stored Sr;l.'LIrV Tank Dimensions (diameter x length) c7 t� (`G 5C 1 Remarks: -- c'�(--t�6-L� ��-� �-�-��-C LC�A�� r�c4 IV, Firm transporting waste State Lic. Hazardous waste manifest# E.P.A # D 1 Approved lahk disposal yard -JY1�S �� ' ��i Tank yard R 0 D Type of inert gas {.� z _ Tank yard address zL Cityl•or Town U J� FDID# V Pemtit�� Date of issue (��160 of Date of expiration Z Lx1 Z� �� ✓ ICE`1 Safe TollpFree.Tel"Number-800-3P -4844 Dig safe approval number. � _ • �•�� T Signature/Title of Officer granting permit � --r.`_. After rernoval(s) ("Consumptive Use"fuel oil tanks exempted) send Form FP-290Rsignedsby Local Fire Dep ment to Office of the Slate Fire Marshal, UST Regulatory Compliance Unit, P.O. Box 1025, Stow, MA 01735. 'International Fire Code Institute �L(4'ei&t FP-292(revised 4/97) GAL ., ail N fv 15 02 02: 19p Da+ L. Bigelow 78JP26 3189 p. 4 RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK Fa FP 291 . NAME AND ADDRESS OF APPROVED TANK YARD APPROVED TANK YARD NO. 100 Tank Yard Ledger 502 CMR 3.03(4)Number- 2-Cl 2'45-Tt6 I certify undagpgnalty of law I have personally examined the underground steel storage tank delivered to this'approved tank yard'by firm,corporation or partnership VIP 55W.Q UNT t L. and accepted same in conformance with Massachusetts Fire Prevenuon Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL Head of Fire Department. FDID# C to transport this tank to this yard. Name and ffit5at title np ved tank yard owner or owners oozed r resentative: SI I RE TLE DATF SIGNED This signed receipt of disposal must be returned to the local head of the fire depanment FDID# V pursuant to 502 CMR 3.00. EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK DATA c",%� TANK REMOVED FROM Gallons 10AC80 MAN nt\)' (me.and SrrM) Previous Contents 1 � Diameter Length � 0 � (City or Towo) Date Received Fire Department Permit# Serial#(if.available) ` Tank I.D.#(Form FP-290) _ Owner/Operator to mail revised copy of Notification Form(FP290,or FP290R)to : UST Compliance, Once of the State Fire Marshal,P-O:Box 1025 State Road,Stow, MA 01775. f 1 } n • TOWN OF. BARNSTABLE UNDERGROUND FUEL AND CHEMI CAL. 'STORAGE REGISTRATION AA ,:� ... . MAP N0. . i PARCEL NO. f - ADDRESS OFTANK• 57 :TEST"`NAIN/O D.CIUMVILLE 'IV,ILLAGE.: f MAILING ADDRESS ( I F DIFFERENT FROM ABOVE) : 4a0 BLUE 1FII$.I DR. WSTWGOD i :ik 02030 . t OWNER NAME: SHELL OZL -coMPiwf PHONE: 617-326-8210 I NSTA.LLAT I ON DATE.: :197�3 BY•. J::.n, Pori?�,�' RG CQ .: INSTALLER `:ADDRESS: SOUTH lELMS' �,''�`� - 'CERT.iJO. *TANK `LOCATION: ' '1X=a CQFQ I Jost ",SANK: LOQAT.I ON,`:-WITH"�;14QOPCCT TO. mU i{-D i NO) CAPACITY 1(7M TYPE OF TANK = RGL55 :AGE _}_0_YRS °.FUEL/CHEMICAL 4.Act,Tn?7. . TESTING QERTIFICA T'IOML, [ 7 .;PASS. C ] FALL DATE' LEAK -:DETECTION; C CHECK <IF N/A TYPE/BRAND Rri� F?, f:iCET.. ZONE OF CONTRIBUTION [ ] YES [ ] NO DATE TO BE REMOVED F I RE..:DEP.T. PERMIT 'ISSUED [: ] :YES [ . ] :NO DATE CONSERVATION [ ] _CHECK IF N/A DATE HOPf ARD _OF HEAL?H TAG NO. DATE 1 s r, 7 :PLEASE PROVIbE A .SKETCH SHOWING THE TANK L':OCATION ON THE HACK ;OF TH.IS :CARD ..: i • f+lotMtea!!on for An se a1►Cloovrr Of In.'goa 61wmW Tanks Rsg{aud Under 527 Can "a rward completed forrn,signed by k=W to deparkrmK fo:Mug VSYComp/lance III PPL of Fire servloe j�P.Q p" to23-state Road stow,Mao 01773 tephone(978)387-3710 0 a�, •,��;` ate A.artved: . 11 VS. ri C""ment rehlru one copy of FP 2WR �Me DoM IDti Fire 04pt..%W kk' LE- is form is to be used for notNteation for removal of Underground Store Tank u A.a s/ storage facility has USTs which are to remain In�an entire amended FP-290 A- r"ft Mounter ty form) must be Ned. B. Date►Errtarsd to: "FaclUtY street address'must include both a street number and a street name, C. Clorwa Inulals it.office box numbers are not acceptable.VW wig cause a regiatratlon to be 0. Comments lined. If geographic location of facility Is not provided,please Mdcate distance ' I direction from closaet lei.xthngt of cam e.g.. (fsc ft at 199 Noah Stye®t le located) (lnt�rsectlon). 1. ®vinIIIERSNIP of TnawlK(s) lie LocATioa AF T1IIIK(S) sr Name(Carpocatlon,IndMdual,Putrtle soQanry,of Ofwr >f tmowrr,qh►a tla 9mgmPhk IoaadOn Of tanks by da9reax,+nWOS.and Mott ya Ertter'rues LLC OWWWR OXWnPW W 42,38,M N Long.$3.Zs,17W LaUtudo longftde $ctdd !nfieId BerZin Roard .er �s I. NJ �ws.r sa.lhrrr�n.uap�6r E 08034 -Sol 1 ls�C � � ) x awwgar...(►.Qasm1OMMMAM.,r„ Orole► �Cvnden 856-470-4015_ C+r aw. svcow 76-0262490 ��. T�wK�pnyN WIINOYED Fm b IN PILACM FC iVumber. TIU*Nn Tank Nam- Tank No. Tank No TanOc rdo. ank/Piping rsrrroved or fAled In plate narit'all that apply) .Substance fast stored .Tank capatacy iladtons IDDM) • Estkrt:atad data last u34d..{rrtDJ!laif/yr.} 14:Z14 4_ Tank was removed from,ground — .Tank s►as not iptttoved fr®m ground Tank was filled with inert Material ] oanstib"material Used., Pfp�Si was removed from ground .•. PfPft was not removed tMM gmund other, pluse spedly ipond�l -"'_".".� •-�-�--- -.-�.t� _..�...,..,.� . ov�A mber(cent.) Tank Nk„L Tar*No._.I— Tank Tank No. Tank No. rK closed in BCCotdBnCe 527 CMR 9.00 C Yes D No. 0 Yes 0 No Cl Yes tJ No O Yes n No O Yes I I No, A. Evidence of leak detected rn Yes 040 a Yes cyKO— rl Yes r� 0 Yes rj4o; Cl Yea I I No B.Mass. DEP notified i I Yes V06. p Yes &140 I !Yes Ia flo U Yes WW" 17 Yes I ! No 1. Mass.DEP tracking number 2.Agency or company performing contamination assessment' *627 CMR 9.07(4).see Vommmweam or , Masaaeleisam.Underground s"s Teak Closure Aseasa merit&%mar April 9,1998 DEP PWWY IWSC-402-96 I declare under penalty of perjury that 1 have personally examined and;am ramUlar with the information submitted in this and all attached documents,and that based on my Inquiry of those Individuals immediately responsible for obtaining the infornna- tion, i believe that the submitted information is true, accurate,and complete. Name and official tifle of owner or owner's Signature: Date: authorized representative(Print) Joan Trout, Permit Analyst D • I FP-noR((*A"d Seel 15� � o J ,; February 19 '2009 f Thomas A.McKean Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601 James F.Munafo,Jr. Barnstable Town Council - 387 Main Street Hyannis,Massachusetts 02601 Re: - Availability of Inspection&Monitoring Report for Phase V Remedy Operating Status -1 Former Shell-Branded Gasoline Station 577-Wesf Mairi Street, Hyannis;lVlassacliusetts Ivlas`sDEP RTN 446772 To Whom It May Concern: Y In accordance with ,the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as,notification that a Phase V Remedy Operating Status &Monitoring Report was submitted'to the Massachusetts'Department,of Environmental Protection (MassDEP) for the above referenced location (the disposal site).' The report summarizes activities conducted between August, 2008 and February 2009. co :x �. Continued activities on'site will include: '1 • Sorbent sock installation and monitoring; ca ' o • Quarterly groundwater gauging and sampling scheduled for May and August 2009;c� N • Submittal of ROS Status Report on August 1,2009. -v ; Copies of the report can be obtained at the Massachusetts Department of Environmen Prote& Southeast Regional Office in Lakeville, Massachusetts. if you have any questions ple se call'C'ffiI6 rn undersigned at(508)339-3200. Sincerely, SOVER N CONSULTING,INC. Jason Sherburne Eric D.Simpson,P.G.,LSP Project Manager ;° Operations Manager s p Vl cc: MassDEP SERO Mr.David Weeks,Motiva Enterprises LLC Mr.Craig Crocker,COMM Water'Board Ms..Donna Miorandi,Town of Barnstable,Health Inspector Mr.Gregory Moran,Dividend Capital Total Realty Trust Mr.Hans Keijser,Town of Barnstable Water Supply Division Mr.Kalil Naoum,K and E Plus Three Enterprises,LLC. Ms.Patti Grenier,Town of Barnstable,School Department Sovereign File-EQ874 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 t Message Page 1 of 1 Martin, Cynthia From: Miorandi, Donna Sent: Tuesday, February 24, 2009 9:36 AM To: Martin, Cynthia Subject: FW: Phase V I&M Report for 577 West main Street Hyannis -----Original Message--- From: Poliquin, Megan [mai Ito:MPoliquin@sovcon.com] Sent: Tuesday, February 24, 2009 9:31 AM To: Miorandi, Donna Subject: Phase V I&M Report for,,577-West main Street Hyannis Ms. Miorandi, Attached please find a PDF copy of our Phase V Status I&M Report dated February 19, 2009. Megan Poliquin Administrative Assistant I email: m_poliquin@sovcon.com phone: 508-339-3200 1 fax: 508-339-3248 Sovereign Consulting Inc. 905B South Main Street Mansfield, MA 02048 www.sovcon.com Science. Service. Solutions. PLEASE NOTE:All information transmitted with and contained in this correspondence contains confidential,proprietary or legally privileged information and is intended for use only by the person or entity to which it is addressed.Any review, retransmission,dissemination or other use of,or taking of any action in reliance upon this information by persons or entities other than the intended recipient is prohibited.If you received this communication in error, please notify the sender immediately.Thank you. all 2/24/2009 • V E K F • y' ,w January 8,2009 UPS# 1Z 969 64F 03 93551629 Ms. Donna Miorandi Town of Barnstable,Health Inspector 200 Main Street Hyannis,MA 02601 a Re: Groundwater Sampling Results,November 2008 In the Vicinity of: 'Former Shell Branded;;Service Station 577 West Malin Street: Hyannis,MA RTN 4-16772 Dear Ms. Miorandi; Pursuant to your authorization Sovereign Consulting Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH). A copy of the laboratory analytical is attached. 3 As always,we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, ;please feel free to contact the undersigned at 508-339-3200. Sincerely, SOV REIG CONSULTING,INC. I Jason Sherburne Project Manager Attachments: Laboratory Data Reports cc: with attachments: Dave Weeks,Motiva Enterprises LLC MassDEP SERO EQ874-File gw 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan BWSC 123 This Notice is Related to Release Tracking Number ® 16772 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 577 West Main Street City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Health Inspec. Donna Miorandi 2. Street Address: 367 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ✓❑ 1.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ✓❑3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address. 577 West Main Street City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 rt, Telephone: (508)339-3200 Email: Sherburne@sovcon.com 7 4 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling Will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass. oq v/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. e-Hardcopy 2.0 Automated Report 7 ;Y- New England La t o ra f uri es 12/15/08 ........... Technical,,Report for Shell Oil SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA x EQ 874 Accutest Job Number: M79097 f Sampling Dates: 11/25/08 - 11/26/08 Report to: Sovereign Consulting Inc. jsherburne@sovcon.com ATTN: Jason Sherburne Total number of pages in report: 99 4C�N ACCpROq�C� B L i S • , Test results contained within this data package meet the requirements /eza and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) ly E A R S NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England - 495 Tech Center West - Building 1 - Marlborough,MA 01752 - tel: 508-481-6200 - fax:508-481-7753 - littp://www.accutest.com Note:This report is password protected to disallow document modification or assembly. 1 of 99 A password to unlock this report is available from your client service representative. M79097 - - - Table of Contents Sections: -1- Section 1: Sample Summary 4 � Section 2: Case Narrative/Conformance Summary Section3: Sample Results ........................................................................................................ 8 3.1: M79097-1: MW-105S .................................................................................................. 9 3.2: M79097-2: MW-105D ..............................:....................................:.............................. 10 3.3: M79097-3: MW-6 ................................................. ....................................................... 11 3.4: M79097-4: MW-16 ....................................................................................................... 12 3.5: M79097-5: MW-3 ......................................................................................................... 13 3.6: M79097-6: MW-7 ......................................................................................................... 14 3.7: M79097-7: MW-10 ....................................................................................................... 15 3.8: M79097-8: MW-103D .................................................................................................. 16 3.9: M79097-9: MW-103S .................................................................................................. 17 3.10: M79097-10: MW-11 ................................................................................................... 18 3.11: M79097-11: MW-5 ..................................................................................................... 19 3.12: M79097-12: MW-1 R .................................................................................................. 20 3.13: M79097-13: MW-25 ................................................................................................... 21 3.14: M79097-14: MW-24D ................................................................................................ 22 3.15: M79097-15: MW-24 ................................................................................................... 23 3.16: M79097-16: MW-21 ................................................................................................... 24 3.17: M79097-17: MW-20 ................................................................................................... 25 3.18: M79097-18: MW-13 ................................................................................................... 26 3.19: M79097-19: MW-14 ................................................................................................... 27 3.20: M79097-20: MW-2 ..................................................................................................... 28 3.21: M79097-21: MW-104S .............................................................................................. 29 3.22: M79097-22: MW-4 ..................................................................................................... 30 3.23: M79097-23: MW-18 ................................................................................................... 31 3.24: M79097-24: MW-1011) .............................................................................................. 32 3.25: M79097-25: MW-lO1S .............................................................................................. 33 3.26: M79097-26: MW-102D ............................................................................................... 34 3.27: M79097-27: MW-102S .............................................................................................. 35 3.28: M79097-28: MW-104D .............................................................................................. 36 3.29: M79097-29: MW-15D ................................................................................................ 37 3.30: M79097-30: MW-17 ................................................................................................... 38 3.31: M79097-31: MW-15 ................................................................................................... 39 3.32: M79097-32: MW-19 ................................................................................................... 40 3.33: M79097-33: MW-23 ................................................................................................... 41 3.34: M79097-34: MW-22 ................................................................................................... 42 Section4: Misc. Forms ............................................................................................................ 43 4.1: Chain of Custody ........................................................................................................... 44 4.2: MCP Form ..................................................................................................................... 47 4.3: VPH Form ...................................................................................................................... 48 4.4: Sample Tracking Chronicle ........................................................................................... 82 M15 2 of 99 A UTEST. M79097 tor':"-> i Sections: Table of Contents -2- Section5: GC Volatiles - QC Data Summaries ..................................................................... 87 5.1: Method Blank Summary 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. ., 5.3: Surrogate Recovery Summaries ..................................................................................... 98 3of99 IMACCUTEBT. M79097 -' X Accutest Laboratories Sample Summary Shell Oil Job No: M79097 SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Project No: EQ 874 Sample C61lected Matrix Client ...:.....: Number Date Time By Received Code Type Sample ID .......... ..........__....._.......... M7909771 11/25/08 12:40 RD 12/02/08 AQ Ground Water MW-105S M79097-2 11/25/08 12:20 RD 12/02/08 AQ Ground Water MW-105D M7909.7-3 11/25/08 10:50 RD 12/02/08 AQ Ground Water MW-6 M79097-4 11/25/08 09:45 RD 12/02/08 AQ Ground Water MW-1'6 M79097-5 11/25/08 09:20 RD 12/02/08 AQ Grourd Water MW-3' M79097-6 11/25/08 10:40 RD 12/02/08 AQ Ground Water MW-7 M79097-7 11/25/08 11:20 RD 12/02/08 AQ Ground Water MW-10 M79097-8 11/25/08 12:15 RD 12/02/08 AQ Ground Water MW-103D M79097-9 11/25/08 12:35 RD 12/02/08 AQ Ground Water MW-103S_ M79097-10 11/25/08 10:00 RD 12/02/08 AQ Ground Water MW-11 M79097-11 11/25/08 09:30 RD 12/02/08 AQ Ground Water MW-5 M79097-12 11/26/08 12:05 RD 12/02/08 AQ Ground Water MW-lR M7909.7-13 11/26/08 11:35 RD 12/02/08 AQ Ground Water MW-25 4 of 99 A Accutest Laboratories Sample Summary (continued) Shell Oil Job No: M79097 SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Project No: EQ 874 Sample '•Collected ' Matrix Client Da te :ate Time 1.By Received Code Type Sample ID M79097x 14 11/26/08 11:20 RD 12/02/08 AQ Ground Water MW-24D M796045 11/26/08 11:05 RD 12/02/08 AQ Ground Water MW=24 M79097 16 11/26/08 10:30 RD 12/02/08 AQ Ground Water MW-21, M79097 17 . 11/26/08 09:55 RD 12/02/08 AQ Ground Water MW-20 M79097-18 11/26/08 09:25 RD 12/02/08 AQ Ground Water MW-13 M790. 0-19 11/26/08 09:00 RD 12/02/08 AQ Ground Water MW-14 M79097-20 11/26/08 08:25 RD 12/02/08 AQ Ground Water MW-2 M79097-21 11/26/08 12:00 RD 12/02/08 AQ Ground Water MW-104S M79097-22 11/26/08 08:20 RD 12/02/08 AQ Ground Water MW-4 M79097-23 11/26/08 09:00 RD 12/02/08 AQ Ground Water :MW-18 M79097 24 11/26/08 09:40 RD 12/02/08 AQ Ground Water MW-101D M7909.7-25 11/26/08 10:00 RD 12/02/08 AQ Ground Water MW-101S M79097-26 11/26/08 10:40 RD 12/02/08 AQ Ground Water MW402D MEN 5 of 99 A M79097 y Accutest Laboratories Sample Summary (continued) Shell Oil Job No: M79097 SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Project No: EQ 874 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M79097-27 11/26/08 11:00 RD 12/02/08 AQ Ground Water MW-102S ....... ......................_.. M79097-28 11/26/08 11:40 RD 12/02/08 AQ Ground Water MW-104D M79097-29 11/26/08 09:00 RD 12/02/08 AQ Ground Water MW-15D M79097-30 11/26/08 12:00 RD 12/02/08 AQ Ground Water MW-17 M79097-31 11/26/08 09:30 RD 12/02/08 AQ Ground Water MW-15 M79097-32 11/26/08 10:10 RD 12/02/08 AQ Ground Water MW-19 M79097-33 11/26/08 10:45 RD 12/02/08 AQ Ground ',Dater MW-23 M79097-34 11/26/08 11:20 RD 12/02/08 AQ Ground Water MW-22 6 of 99 @ACC. UTES'T M79097 -> L a b 0 r a t o r i e SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M79097 Site: SCMAW:97346878(REIMBMA)577 West Main Street Hyannis MA Report Date 12/12/2008 11:10:18 AM 34 Sample(s)were collected on between 11/25/2008 and 11/26/2008 and were received at Accutest on 12/02/2008 properly preserved, at 2 Deg.C and intact. These Samples received an Accutest job number of M79097.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control perfonnance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GAB2667 a All samples were analyzed within the recommended method holding time. a All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GBD1129 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. M79097-3:Elevated RL due to sample matrix. Matrix AQ Batch ID: GBD11130 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GBD1135 a All samples were analyzed within the recommended method holding time. 0 All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GBH148 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Note:Compounds whose QC limits are outside MCP criteria are designated by the lab as "Difficult".QC criteria for a"Difficult" compound may meet Accutest in-house generated QC criteria but exceed MCP criteria(compounds exceeding Accutest QC criteria are flagged on the QC summary).Refer to the QC summary pages. The Accutest Laboratories of New England certifies that all analysis were perfonned within method specification.Its further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M79097). Friday,December 12,2008 Page 1 of i 7of99 A M79097 -3- - f Y M New England 12ACCUTIS L a b i,r.1 tu r i e 5iA j„a: Section 3 Sample Results Report of Analysis 8 of 99 A M79097 - - s w- Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-105S Lab Sample ID: M79097-1 Date Sampled: 11/25/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23750.D 1 12/06/08 AF n/a n/a GBD1129 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene 3.0 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene 3.1 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9-C10 Aromatics(Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 74% 70-130% 615-59-8 2,5-Dibromotoluene 81% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME] 9 of 99 AC Y C Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-105D Lab Sample ID: M79097-2 Date Sampled: 11/25/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIINIBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23751.D 1 12/06/08 AF n/a n/a GBD1129 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene 'ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 78% 70-130% 615-59-8 2,5-Dibromotoluene 82% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME] 10 of 99 &3CC M79097 "= °e r 3 Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-6 Lab Sample ID: M79097-3 Date Sampled: 11/25/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 131323748.13 2 12/06/08 AF n/a n/a GBD1129 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 4.0 ug/I 100-41-4 Ethylbenzene 5.6 4.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene 27.2 6.0 ug/I 108-88-3 Toluene ND 4.0 ug/I m,p-Xylene 137 4.0 ug/I 95-47-6 o-Xylene 28.6 4.0 ug/I C5- C8 Aliphatics (Unadj.) 1930 100 ug/l C9-C12 Aliphatics (Unadj.) 5000 100 ug/l C9- C10 Aromatics (Unadj.) 4050 100 ug/I C5- C8 Aliphatics 1930 100 ug/I C9-C12 Aliphatics 785 100 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 76% 70-130% 615-59-8 2,5-Dibromotoluene 82% 70-130% (a)Elevated RL due to sample matrix. I ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 99 A M79097 e z c Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-16 Lab Sample ID: M79097-4 Date Sampled: 11/25/08 Matrix: AQ -Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West:Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 131323752.D 1 12/06/08 AF n/a n/a GBD1129 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND`,,. 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 74% 70-130% 615-59-8 2,5-Dibromotoluene 81% 70-130% ND= Not detected J Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ar Ej 12 of 99 M79097 '- i Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-3 Lab Sample ID: M79097-5 Date Sampled: 11/25/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23753.D 1 12/06/08 AF n/a n/a GBD1129 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene N:D. 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether Na:.'. 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene Nb , 2.0 ug/I m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) qND 50 ug/I C9-C10 Aromatics(Unadj.) 'ND 50 ug/1 C5- C8 Aliphatics ND . 50 ug/l C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene 83% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 99 M79097 r t Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-7 . Lab Sample ID: M79097-6 Date Sampled: 11/25/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23754.D 1 12/06/08 AF n/a n/a GBD1129 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q ......._....___.._-____-_. 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene 97 2.0 ug/I 95-47-6 o-Xylene 2.9 2.0 ug/1 C5-C8 Aliphatics (Unadj.) 175 50 ug/1 C9- C12 Aliphatics (Unadj.) 135 : 50 ug/I C9- C10 Aromatics (Unadj.) 98.3 50 ug/I C5- C8 Aliphatics 175 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 75% 70-130% 615-59-8 2,5-Dibromotoluene 80% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 14 of 99 M79097 - Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-10 Lab Sample ID: M79097-7 Date Sampled: 11/25/08 Matrix: AQ - Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23780.D 1 12/07/08 AF n/a n/a GBD1130 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene 9.7 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether N'Q 1.0 ug/I 91-20-3 Naphthalene 41 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene 56:8 2.0 ug/1 95-47-6 o-Xylene 18.2 2.0- ug/I C5- C8 Aliphatics (Unadj.) 185 50 ug/I C9- C12 Aliphatics (Unadj.) .236 50 ug/l C9- C10 Aromatics (Unadj.) 119 50 ug/l C5-C8 Aliphatics 185 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene 82% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 15 of 99 M79097 --- - - � f Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-103D Lab Sample ID: M79097-8 Date Sampled: 11/25/08 IND Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23779.D 1 12/06/08 AF n/a n/a GBD1130 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 82% 70-130% ND = Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 16 of 99 12ACCUTEBT. M79097 -a-0 r l } Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-103S Lab Sample ID: M79097-9 Date Sampled: 11/25/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23778.D 1 12/06/08 AF n/a n/a GBD1130 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q ............................__...._...__. 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene N>D 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene NO 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9-CIO Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 83% 70-130% I ND= Not detected =J Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 99 V M79097 - - -- 1 f Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-11 Lab Sample ID: M79097-10 Date Sampled: 11/25/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23777.D 1 12/06/08 AF n/a n/a GBD1130 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene N.D. 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene 82% 70-130% ND = Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M15 18 of 99 A T M79097 _aFo=sco: e> Accutest Laboratories s.a Report of Analysis Page 1 of 1 Client Sample ID: MW-5 Lab Sample ID: M79097-11 Date Sampled: 11/25/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23776.D 1 12/06/08 AF n/a n/a GBD1130 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................_....................... ... ........._.__. . . 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 82% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E = In _dicates value exceeds calibration range N Indicates presumptive evidence of a compound + min 19 of 99 M79097 "- Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-1R Lab Sample ID: M79097-12 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 Wes-Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3022.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) 360 50 ug/I C9- C12 Aliphatics (Unadj.) 229 50 ug/I C9- C10 Aromatics (Unadj.) 166 50 ug/I C5- C8 Aliphatics 360 50 ug/I C9- C12 Aliphatics 63.2 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 104% 70-130% 615-59-8 2,5-Dibromotoluene 103% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME 20 of 99 12AC CUTEST Accutest Laboratories Report of Analysis Page 1 of 1 , Client Sample ID: MW-25 Lab Sample ID: M79097-13 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3023.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q _..._..................._.._.... 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene 214 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene 20.5 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene 13:1 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) 894 50 ug/1 C9- C12 Aliphatics (Unadj.) 340 50 ug/I C9- C10 Aromatics (Unadj.) 270 50 ug/I C5- C8 Aliphatics 892 50 ug/I C9- C12 Aliphatics NO 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 104% 70-130% 615-59-8 2,5-Dibromotoluene 103% 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit =r g E3 Indicates zn2lyte found in associated methyl dank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M 21 of 99 T I 1 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-24D Lab Sample ID: M79097-14 Date Sampled: 11/26/08 = Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3027.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ,ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether NO 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5-C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 89% 70-130% 615-59-8 2,5-Dibromotoluene 88% 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 22 of 99 @ACCUTEErr. I Accutest Laboratories Report of Analysis Page I of 1 tA Client Sample ID: MW-24 Lab Sample ID: M79097-15 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BI13028.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........_............................__ ...._.... ......... .._. 71-43-2 Benzene NiO 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND : 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) .ND 50 ug/l C5-C8 Aliphatics ND 50 ug/I C9-C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 87% 70-130% 615-59-8 2,5-Dibromotoluene 86% 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 23 of 99 A M79097 • t Accutest Laboratories cs Report of Analysis Page 1 of I Client Sample ID: MW-21 Lab Sample ID: M79097-16 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3026.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene 14.9 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 'ND 1.0 ug/l 91-20-3 Naphthalene 9.1 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene 5.8 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) 50.5 50 ug/I C9- C12 Aliphatics (Unadj.) 88.3 50 ug/I C9-CIO Aromatics(Unadj.) 55.2 50 ug/I C5- C8 Aliphatics 50.5 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene 93% 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound EJEJ 24 of 99 @ACCLMEBM79097 e T Accutest Laboratories Report of Analysis Page 1 of 1 -: Client Sample ID: MW-20 Lab Sample ID: M79097-17 Date Sampled: 11/26/08 Matrix:. AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3024.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene 38.4 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 u9/1 91-20-3 Naphthalene 56 6 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene 50.1 2.0 ug/l 95-47-6 o-Xylene 5.1 2.0 ug/I C5- C8 Aliphatics (Unadj.) 1480 50 ug/1 C9- C12 Aliphatics (Unadj.) 774 50 ug/l C9- C10 Aromatics (Unadj.) 627 50 ug/1 C5- C8 Aliphatics 1480 50 ug/I C9- C12 Aliphatics 53.1 50 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 108% 70-130% 615-59-8 2,5-Dibromotoluene .109% 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 25 of 99 BT. M79097 --- - --- T Accutest Laboratories Report of Analysis Page 1 of 1 00 Client Sample ID: MW-13 Lab Sample ID: M79097-18 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REINIBMA) 577 West-\lain Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 131-13025.13 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) 484 50 ug/I C9- C12 Aliphatics (Unadj.) 310 50 ug/l C9- C10 Aromatics (Unadj.) 289 50 ug/I C5-C8 Aliphatics 484 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 100% 70-130% 615-59-8 2,5-Dibromotoluene 99% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M15 26 of 99 ACCUTEST M79097 r e Accutest Laboratories ca Report of Analysis Page 1 of 1 Client Sample ID: MW-14 Lab Sample ID: M79097-19 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3021.13 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ug/1 100-41-4 Ethylbenzene 170 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene 278 . 3.0 ug/I 108-88-3 Toluene 4.6 2.0 ug/I in,p-Xylene 1260 2.0 ug/I 95-47-6 o-Xylene 636 2.0 ug/I C5-C8 Aliphatics (Unadj.) 1670.. 50 ug/I C9- C12 Aliphatics (Unadj.) 5580 50 ug/I C9- C10 Aromatics (Unadj.) 3200 50 ug/I C5- C8 Aliphatics 1660 50 ug/I C9-C12 Aliphatics 306 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 117% 70-130% 615-59-8 2,5-Dibromotoluene 121% 70-130% ND = Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound [MEJ 27 of 99 A M79097 = "• --- Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-2 Lab Sample ID: M79097-20 Date Sampled: 11/26/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3029.1) 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5-C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5-C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 99% 70-130% 615-59-8 2,5-Dibromotoluene 98% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound E"a 28 of 99 AC CL EST M79097 Accutest Laboratories w Report of Analysis Page 1 of 1 ; Client Sample ID: MW-104S Lab Sample ID: M79097-21 Date Sampled: 11/26/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3030.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q ......._......._.._.__..._......._. .................... ............... ........... 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene N°D 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene N'D 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 106% 70-130% 615-59-8 2,5-Dibromotoluene W5% 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound l 29 of 99 M79097 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-4 Lab Sample ID: M79097-22 Date Sampled: 11/26/08 Matrix: AQ -Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West-'%lain Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3031.D 1 12/06/08 AP n/a n/a GBH 148 Run#2 Purge Volume Run 91 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2, Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) 'ND 50 ug/1 C9-C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#3 Limits 615-59-8 2,5-Dibromotoluene 83% 70-130% 615-59-8 2,5-Dibromotoluene 82% 70-130% ND = Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q 30 of 99 @AC CU TEST M79097 Accutest Laboratories Report of Analysis Page 1 of 1 w Client Sample ID: MW-18 Lab Sample ID: M79097-23 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3032.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q ..._......_...... ........ .. 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND:. 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene NO 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) N'D 50 ug/I C9- C10 Aromatics(Unadj.) ;.ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 100% 70-130% 615-59-8 2,5-Dibromotoluene 97% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MM 31 of 99 M79097 Accutest Laboratories Report of Analysis Page I of 1 K) Client Sample ID: MW-101D Lab Sample ID: M79097-24 Date Sampled: 11/26/08 ° Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3033.13 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND ; 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 83% 70-130% 615-59-8 2,5-Dibromotoluene 83% 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 32 of 99 &3A M79097 -' Accutest Laboratories Report of Analysis Page I of I NJ Ln Client Sample ID: MW-101S Lab Sample ID: M79097-25 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3034.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml I Run#2 MA-VPH List CAS No. Compound Result RL Units Q ................................................. 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) NO 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) NO 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene .77% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound as 33 of 99 12ACCLffUST Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-102D Lab Sample ID: M79097-26 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3035.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene NO 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9-C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 86% 70-130% 615-59-8 2,5-Dibromotoluene 84% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 34 of 99 UACCUMST. M79097 - Accutest Laboratories Report of Analysis Page 1 of I KJ Client Sample ID: MW-102S Lab Sample ID: M79097-27 Date Sampled: 11/26/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3036.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q _.................................... 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene N D 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95 47 6 o-Xylene .ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND. 50 ug/I C9-C12 Aliphatics (Unadj.) ND 50 ug/1 C9- CIO Aromatics (Unadj.) N.D 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 83%- 70-130% 615-59-8 2,5-Dibromotoluene 82% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B=. Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ffMffl 35 of 99 M79097 � '- Accutest Laboratories Report of Analysis Page 1 of 1 00 Client Sample ID: MW-104D ' Lab Sample ID: M79097-28 Date Sampled: 11/26/08 Matrix: AQ - Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BH3037.D 1 12/06/08 AP n/a n/a GBH148 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene NI) 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9-CIO Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9-C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 98% 70-130% 615-59-8 2,5-Dibromotoluene 96% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound Q15 36 of 99 13ACCUTEST. M79097 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-15D Lab Sample ID: M79097-29 Date Sampled: 11/26/08 Matrix: AQ -Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB47136.D 1 12/08/08 AP n/a n/a GAB2667 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 1 i 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene N-D, 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) NOD . 50 ug/1 C9- C10 Aromatics (Unadj.) ND, 50 ug/I C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 97% 70-130% 615-59-8 2,5-Dibromotoluene94% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range " N = Indicates presumptive evidence of a compound 37 of 99 M79097 _- Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-17 Lab Sample ID: M79097-30 Date Sampled: 11/26/08 � Matrix: AQ - Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 Wes-Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB47137.D 1 12/08/08 AP n/a n/a GAB2667 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene 87% 70-130% 615-59-8 2,5-Dibromotoluene 94% 70-130% I ND = Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 38 of 99 A Accutest Laboratories Report of Analysis Page 1 of 1 w Client Sample ID: MW-15 Lab Sample ID: M79097-31 Date Sampled: 11/26/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB47138.D 1 12/08/08 AP n/a n/a GAB2667 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene -ND _ =2.0 ug/1 100-41-4 Ethylbenzene 27.0 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene 17.7 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene 120 2.0 ug/I 95-47-6 o-Xylene 24.8 2.0 ug/I C5- C8 Aliphatics (Unadj.) 672 50 ug/1 C9- C12 Aliphatics (Unadj.) 519 50 ug/I C9- C10 Aromatics (Unadj.) 332 50 ug/1 C5- C8 Aliphatics 672 50 ug/I C9- C12 Aliphatics ND' 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 78% 70-130% 615-59-8 2,5-Dibromotoluene 87%` 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 39 of 99 3T M79097 a Accutest Laboratories ty.> Report of Analysis Page 1 of 1 w Client Sample ID: MW-19 Lab Sample ID: M79097-32 Date Sampled: 11/26/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23845.1) 1 12/09/08 AF n/a n/a GBD1135 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 75% 70-130% 615-59-8 2,5-Dibromotoluene 79% 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEM 40 of 99 ACCUTEST Accutest Laboratories cis Report of Analysis Page 1 of 1 Client Sample ID: MW-23 Lab Sample ID: M79097-33 Date Sampled: 11/26/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB47140.D 1 12/08/08 AP n/a n/a GAB2667 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene 64.7 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene 19.2 3.0 ug/1 108-88-3 Toluene 4.3 2.0 ug/I m,p-Xylene 70.2 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) 489 50 ug/I C9- C12 Aliphatics (Unadj.) 352 50 ug/I C9- C10 Aromatics (Unadj.) 203 50 ug/1 C5- C8 Aliphatics 485 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 73% 70-130% 615-59-8 2,5-Dibromotoluene 79% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Mel 41 of 99 T M79097 -'-- - Accutest Laboratories w Report of Analysis Page 1 of I Client Sample ID: M W-22 Lab Sample ID: M79097-34 Date Sampled: 11/26/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 577 Wes_Main Street Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23846.D 1 12/09/08 AF n/a n/a GBD1135 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 76% 70-130% 615-59-8 2,5-Dibromotoluene 81% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 42 of 99 ACCUTEBT. M79097 � "'=' `=' "'= . .�Fa New England s' Lz_ C,r.1IL �t�ri Section 4 =1VIisc Forms Custody Documents and Other Forms Includes the following where applicable: • Certification Exceptions • Parameter Certifications (MA) • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle a 43 of 99 A M79097 - Ih LAS(LOCATION) 4 Shell Oil Products Chain Of Custody Record -PleJse'Check APptop ald Be.! Print Bill To Contact Name: .:INCiDENTA(ENV:SERVIC ES)':❑rHrrx IF nn 11-5— PrrLL. Lh n- ', �Ifi ,. . �1s �acrul' Dave Weeks 9 7 3 4. 6 8[7 8 DA-[ b8 L•1 aae.r•,� flw lvA•Iur+ (l CJ wtt, ..' . .... I �-� S� 7 Imo. >" _. PO tl... ... 5AP:.�. :-..: PAcc—L_.___of i 7 3 7 71 71 0 Sovereign Consulting Inc ,•11>t..•l,e_1f1�Yy.,.,...I --- 577 West Main Street,[Hyannis.MA --90$e$OUlll Main Street,UBI1 202 CONSULTANT PROJECT CONTACT(RuPnrt hr):.lawn 51,elLurna I CONSULTANT PROJECT NO.'.E007a Mansfield,MA 02048 [rI;Za_r506 339 3200 _ ' VC y ler j lN1Y* us :� lMV47 � I. rl+nnPnsv:a I'J SiArlLnFO(ta D4r, ❑.nnvG I IJu>r, 111t r, ❑>+ REQUESTED ANALYSIS n uc ueuvLN;r t=_=: ❑__ pan— fd Ncr 1'1'." I ...._..-------- ' icooi«on SPECIAL INSTRUCTIONS OR NOTES SAMPLING Field Sample Identification N•*a�• = I comalaar Pm Ro.'al�y. DATE TIME ; L.iUeratary NOWu G. IIY Mw_ I 5D 122D - ,.. — /Nln/_16 vy; - I�w-� 1w Mw-7 � (olv 0ZO �4 T'IH/-fogy z(s — /'14J 3 5ILI 23s M79097: Chain of Custody Page 1 of 3 Q 44 of 99 RA M79097 =r a'-=' °o LAS(LOCATION) Shell Oil Products Chain Of Custody Record Please Check Appropriate Bo- Print Bill To Contact Name: INCIDENT.#(ENV SERVICES) 0 'ie I-- C] D 91 'i 610 9 I Da Week, 71 31 41 61 81 7 1 8 DATE, PO N SAP m:: iL 3 -T-11--TT—111T- 11 11 71 71 7TOT-T— Sovereign Consulting Inc 577 West Main Street,Hyannis,MA 905E South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Report to):Jason SherburneI CQ1111IAN1 PROJECI NO F0874 Mansfield,MA 02048 - 44� ""';8.339.3200 508.339.3248 r-`, i�1;177 27 a 1—1 LJ C:1»narxy REQUESTED ANALYSIS II... Ij—s I'll- 17 171 T-N—T-0—CE— SPECIAL INSTRUCTIONS OR NOTES Field Sample Identification DATE TIME n > 4L Kw-I K If/ 121)5' x IS P4 1135 -)y: MW z+4p Ilzv 925- D106 M5 :ZL ..MW.-q )D 10 oqqo -,3 It 1000 ll —5� ('1ST M79097: Chain of Custody Page 2 of 3 45 of 99 13ACCUTEST. M79097 r:I LAB(LOCATION) Shell Oil Products Chain Of Custody Record Please C�G"q ro riale:aox: Print Bjrl:ro Contact N—e- -na ta - . -1 INCIDENT H(ENV SERVICES) 71 xv,"T �6.on—r. I Dave Weeks 61 81,18 DATF D PO# �;AP:# 11A, �c 3 ........... I T .... .... 11 31 71 71 7 0 Soverel IT Consulting.Inc_ 577 West Main Street,_Hyannis,.MA - . 9058 South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(RepM In) She,1,,..e I CONSULTANT PROJECT NO:EO874 Mansfield,MA 02048 wo)IcM,5 ---- ----------508,339.3200 j-`-50-8-.-339.-324-H7 j�het_u ci)Z�OCO -t./w 0—, IIUAr. I I z—, REQUESTED ANALYST .111U,�(--'Y) 1-0 SPECIAL INSTRUCTIONS OR NOTES SAMPI INC Field Sample Identification DATE[TIME > 10q0 I Ll I Ix 1100 nw- 100 1190 t4w-15P OqX)I I I 3 raw i Mw— zz 1lz/j .... ...............— 1;V2,�'7g 3 A0 M79097: Chain of Custody Page 3 of 3 M15 46 of 99 j2ACC&rrEBT. M79097 Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 P. N Title: MADEP MCP Response Action Analytical Report Certification Form r� GP nat: Ica( thud e rt Gerd cation, P n s �: y "a a.... .._��. ..�?�``..':. ... ._ ' ..:: ��......: •".... :£ ._ + ... ,;;�:,. _Via:,. : �w - Laboratory Name: Accutest Laboratories of New England Project#: M79097 i Project Location: SCMAW:97346878(REIMBMA)577 West Main Street MADEP RTN None Hyannis MA This form provides certifications for the following data set: M79097-1 thruogh M79097-34 Sample Matrices: Groundwater X Soil/Sediment () Drinking Water () Other: () () MGP ' 6 � 8260E 8151 A 8330 6010E 7470A/1 A a. Qthcld5 ,,,;•;' 8270C 8081A VPH X 6020 9014M z As specifiedn tv1Ala P z 8082 8021 B EPH 7000 S 3 7196A Carty endium Analyttcaf Methods' "�2`� �. 8 6 hA�ttf�od 9 �4�or MgpEP Phj+sologic I y,4va�lable�Gyanide(PAS}�Niethod ,; =P �� C•;eCI4 at1 that a ly_:y 3 SPIV$46 Methods 7Ug0tSr LiS�t lnivid a�me#hod aanatyte �_. � An affirmative response to questions A, B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with Yes ❑ No ' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed, including the requirement to note and ❑ Yes ❑ No ' discuss in a narrative QC data that,did not meet appropriate performance standards or guidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty",as described in Section 2.0(a),(b), (c)and P1 Yes ❑No ' (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only: Was the VPH or EPH method run without 21 Yes ❑No '. significant modifications,as specified in Section 11.3? A response to questions E and Fbelow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the Yes El No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified El Yes LJ No method S reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. i the undersigned,attest under the pains and penalties of perjury that,based upon my personal r inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 12/12/2008 Q 47 of 99 M79097 MADEP VPH FORM Metrlx ... Aqueous n Soil 7 Sediment I-1 Other Containers Satisfactor n Broken F1 Leakin F1 ueotas Preservatives N/A H<=2 W pH>2 _ Tem �iature Received on Ice Received at 4 De- .C Other ✓ Rec'd at 2 deg C Methanol 71-71 ``"1 N/A P. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-103S Lab ID: M79097-1 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2003 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A Ug/l ND' 50 C9-C10 Aromatics(Unadj.) N/A Lg/I ND" 50 . C9-C12 Aliphatics(Unadj.) N/A Lg/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/1 3 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I 3.1 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A Jg/1 ND' 50 C9-C12 Aliphatics N/A -Ig/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 74 70-130% PID:2,5-Dibromotoluene % 81 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting n that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting n that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting n that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best cf my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 EJ 48 of 99 ,04 Bsl'T M79097 MADEP VPH FORM Matnx z .. A ueous n Soil Sediment F Other 11 Con-tai ers%,5 i Satisfactor n Broken n Leaking F-1 ueotisPreservattves N/A H<=2 DH>2 Tem er*ure ',� ... Received on Ice Received at 4 De C Other Rec'd at 2 deg C Meth na of ` N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-105D Lab ID: M79097-2 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes; Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-Cl 2 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND° 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 78 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range a Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 91Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 49 of 99 M79097 MADEP VPH FORM Matrix❑ ,. A ueous �I Soil ❑ Sediment Other ❑ Cohtainers31 � Satisfactory Broken F Leakin A:ueous Preserva Imes, N/A H<=2 ✓ H>2 v "Ternertur Received on Ice Received at 4 Deg.C Other Re�'d at 2 deg c Meth'a I N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-6 Lab ID: M79097-3 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/200E Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 2 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL (Q. C5-C8 Aliphatics(Unadj.) N/A ug/I 1930' 100 C9-C10 Aromatics(Unadj.) N/A ug/I 4050' 100 C9-C12 Aliphatics(Unadj.) N/A ug/I 5000, 100 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I 5.6 4 Toluene 108-88-3 C5-C8 ug/l ND 4 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 4 Naphthalene 91-20-3 N/A ug/I 27.2 6 o-Xylene 95-47-6 C9-C12 ug/I 28.6 4 m,p-Xylene C9-C12 Lg/I 137 4 Adiusted Ranges C5-C8 Aliphatics N/A vg/I 1930 B 100 C9-C12 Aliphatics N/A ug/I 785° 100 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 76 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting ii that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting ii that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑.i No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 ya 50 of 99 9ACCUTEST. MADEP VPH FORM Matrix Aqueous w Soil ❑ Sediment n Other Contafners Satisfactoryny Broken ❑ Leaking ueous Preservatl es N/A F1 DH <=2 W1 PH>2 Tem er�atu ' - Received on Ice Received at 4 Deg.C ❑ Other Read at 2 deg C Methanol ;_ N/A P Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-16 Lab ID: M79097-4 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugh ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 1 Benzene 71-43-2 C5-C8 ug/l ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ugh ND 2 m,p-Xylene C9-C12 ug/1 ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/1 ND a 50 C9-C12 Aliphatics N/A ug/1 ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 74 70-130% PID:2,5-Dibromotoluene % 81 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete, Signature Postition Laboratory Director Printed Name Reza Tan Date 12/11/2008 EM 51 of 99 M79097 a or;'or eo. MADEP VPH FORM Matrix Aqueous n Soil ❑ Sediment ❑ Other containe4s `' w Satisfactor Broken ❑ Leakin ❑ Abb"ods' Presefsvati ev N/A H<=2 W PH>2 Tefterat re' Received on Ice Received at 4 Deg. C 7 Other y Rec'd at 2 deg C Methanol# , , N/AP. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-3 Lab ID: M79097-5 w Date Collected: 11/25/2008 Date Received: 12/2/2008 Method for Target Analytes: MADEP VPH REV 1.1 �%.. VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Uiits Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/l ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/l ND' 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/l ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/1 ND 2 Adjusted Ranges C5-C8 Aliphatics N/A _lg/l ND a 50 C9-C12 Aliphatics N/A Jg/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting n that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 QR 52 of 99 @ACCUTEBT. M79097 - - - - - MADEP VPH FORM Matrix Aqueous ✓ Soil ❑ Sediment Other F Containers "` - Satisfacto Ivl Broken ❑ Leakin F1 ueou Presecuatives N/A ohl<=2 DH>2 Term t M era Received on Ice Received at 4 De .C Other ✓ Rec d at 2 deg c .... N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-7 Lab ID: M79097-6 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 175' 50 C9-C10 Aromatics(Unadj.) N/A ug/I 98.3 A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 135 A 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-Cl 2 ug/I 2.9 2 m,p-Xylene C9-C12 ug/I 9.7 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I 175 a 50 C9-C12 Aliphatics N/A ug/I ND° 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 75 70-130% PID:2,5-Dibromotoluene % 80 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range ` B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. fll C " Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 53 of 99 M79097 MADEP VPH FORM Matnx U"' Aqueous n Soil n Sediment n Other n C`ontalners ., Satisfacto Iv Broken n Leaking F ueous'Preservattves N/A El PH<=2 Fel PH>2 Tern erature Received on Ice Received at 4 Deg.C Other d Rec'd at 2 deg C Methanol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-10 Lab ID: M79097-7 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/7/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 185 A 50 C9-C10 Aromatics(Unadj.) N/A ug/I 119 A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 236' 50 Target Analytes; Ethylbenzene 100-41-4 C9-C12 i.'g/I 9.7 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I 4.1 3 o-Xylene 95-47-6 C9-C12 ug/I 18.2 2 m,p-Xylene C9-C12 ug/I 56.8 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I 185 6 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)end/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑.i No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 MED 54 of 99 @ACCAXrEBT. M79097 MADEP VPH FORM Ml,, A ueous I] Soil Sediment Other Con triers <. a Satisfactory W Broken ❑ Leakina ❑ ueausti04406 yr at yes N/A H<_2 Lyl PH>2 Teemp efturWa.,., Received on Ice El Received at 4 Deg. C D Other ✓ Rec'd at 2 deg C Methanol m N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-103D Lab ID: M79097-8 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 9 Y VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/1 ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/1 ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range k B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CSC8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 55 of 99 M79097 MADEP VPH FORM Matra A ueous - Soil 7 Sediment ❑ Other Containers SatisfactoryFy Broken ❑ Leakin "ous Pre a vativeW N/A pH<=2 W1 DH>2 Tem 0 bretu Received on Ice 0 Received at 41De . C Other Rec'd at 2 deg C M011a'nol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-103S Lab ID: M79097-9 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2003 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL 9 C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A t.g/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A l.g/I ND A 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/l ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A -Jg/l ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)end/or internal standards eluting n that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting n that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting n that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes;eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? -Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? -Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? -No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 56 of 99 MADEP VPH.FORM Matrix A ueous ✓ Soil F1 Sediment 7 Other ❑ Cant'aiiters.. '. Satisfactory✓ Broken FLeakinq ❑ AiiMiAr"es vative&' N/A 0 PH<=2 ✓ PH>2 Urn �attare 2q, Received on Ice F1 Received at 4 Deg. C F Other ✓ Rec'd at 2 deg C Or U N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-11 Lab ID: M79097-10 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 Ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 I Benzene 71-43-2 C5-C8 ug/I ND 2 1 Naphthalene 91-20-3 N/A Ug/l ND 3 o-Xylene 95-47-6 C9-C12 ug/l ND 2 m,p-Xylene C9-C12 ug/1 ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/l ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. . A Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 MEJ 57 of 99 M79097 ---- --- MADEP VPH FORM Matrix h,m A ueous Soil Sediment Other f Conitainers Satisfactory Broken F1 Leakin Adiieous Preservatives N/A El pH<=2 ✓ H>2 der •.erature ` .;. Received on Ice Received at 4 Deg. C F1 Other n Redd at 2 deg c Methanol N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-5 Lab ID: M79097-11 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/2E/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tent Butyl Ether 1634-04-4 C5-C8 ug/1 ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-Cl 2 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/l ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑d Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sec-.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 MID 58 of 99 ACCUTIEST M79097 - • -t MADEP VPH FORM Matr x 3..' A ueous W, Soil ❑ Sediment F Other Containers ❑.x...... MW Satisfactor Broken ❑ Leaking ❑ ueous Preservatives-, N/A El DH<=2 Fel DH>2 emP a utUt rye. Received on Ice Received at 4 Deg.C Other W Rec'd at 2 deg C MetH1i' hol W N/A � Method for Ranges: MADEP VPH REV 1 A Client ID: MW-1 R Lab ID: M79097-12 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 117-1 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/1 229' 50 C9-C10 Aromatics(Unadj.) N/A ug/l 166 A 50 C5-C8 Aliphatics(Unadj.) N/A ug/I 360 A 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/1 ND 2 o-Xylene 95-47-6 C9-Cl 2 ug/l ND 2 Naphthalene 91-20-3 N/A ug/l ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/1 ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ug/1 63.2° 50 C5-C8 Aliphatics N/A ug/I 360 a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 103 70-130% FID:2,5-Dibromotoluene % 104 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C&Ce Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 Ma 59 of 99 M79097 7 a^_._.._..- MADEP VPH FORM Matrix ' A ueous n Soil n Sediment Other f l Co.nteiners SatisfactorvFvl Broken FI Leaking ueous..Preservat.ives N/A L PH<=2 ✓ I H>2 t6m erature t,' Received on Ice Received at 4 De- .C Other ✓ Rec d at 2 deg c Mekhanol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-25 Lab ID: M79097-13 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Jnits Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I 340' 50 C9-C10 Aromatics(Unadj.) N/A ug/I 270 A 50 C5-C8 Aliphatics(Unadj.) N/A ug/I 894 A 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I 21.4 2 m,p-Xylene C9-C12 ug/I 13.1 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I 20.5 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND° 50 C5-C8 Aliphatics N/A ug/I 892 a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 103 70-130% FID:2,5-Dibromotoluene % 104 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes EJ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? C✓Yes U No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No 'Ll Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 60 of 99 @ACCArrEBT. M79097 = '= MADEP VPH FORM Matrix >;.': I A ueous n Soil 7 Sediment n Other n can ed's, Satisfacto nv Broken n Leakin f-1 'W ueoWOresemat O N/A PH <=2 ✓ H>2 T,, ftordtldre... Received on Ice L1 Received at 4 Deg.C Other ✓ Reed at 2 deg C Methanol _ N/A P. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-24D Lab ID: M79097-14 fa Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/l ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/1 ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/1 ND' 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 89 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 MEl 61 of 99 M79097 - -- - MADEP VPH FORM Matrixt A ueous n Soil Sediment ❑ Other Contain rs Satisfactory J Broken 7 Leakin ueous Preservatives N/A El PH<=2 J H>2 El Tem enure Received on Ice El Received at 4 Deg. C Other J Rec'd at 2 deg C Methanol „ N/A p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-24 Lab ID: M79097-15 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 ` VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND A 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 Ug/I ND 2 m,p-Xylene C9-C12 Ug/I ND 2 o-Xylene 95-47-6 C9-C12 Jg/I ND 2 Naphthalene 91-20-3 N/A Jg/1 ND 3 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND° 50 C5-C8 Aliphatics N/A Ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 86 70-130% FID:2,5-Dibromotoluene % 87 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. - C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? IVJ Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of ny knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 E 62 of 99 @ACCUTIES M79097 Y MADEP VPH FORM Matrix Aqueous n Soil R Sediment R Other C :;. Satjsfactor F-,l Broken n Leaking n u°eotr Preservat Ves N/A 7H<=2 H>2 Tetra .eratur�e„ I Received on Ice Received at 4 Deg.C F Other n Rec'd at 2 deg C Methanol ,,: .- N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-21 Lab ID: M79097-16 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I 88.3" 50 C9-C10 Aromatics(Unadj.) N/A ug/I 55.2 A 50 C5-C8 Aliphatics(Unadj.) N/A ug/I 50.5" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I 9.1 3 Benzene 71-43-2 C5-C8 ug/1 ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I 14.9 2 m,p-Xylene C9-C12 ug/I 5.8 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND' 50 C5-C8 Aliphatics N/A ug/I 50.5 B 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 92 70-130% FID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑d Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑d No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 63 of 99 M79097 . Y MADEP VPH FORM Matix Aqueous ICI Soil 7 Sediment P Other Containers.. . ., :, Satisfactor ✓ Broken ❑ Leaking du ea.us Pcese 44Wbs'W N/A ❑ DH<=2 kel PH>2 El Received on Ice Received at 4 Deg. C El Other [ Redd at 2 deg C Meth'aol' , N/A a Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-20 Lab ID: M79097-17 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/i 774 A 50 C9-C10 Aromatics(Unadj.) N/A ug/1 627 A 50 C5-C8 Aliphatics(Unadj.) N/A ug/I 1480 A 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I 38.4 2 o-Xylene 95-47-6 C9-C12 ug/I 5.1 2 Naphthalene 91-20-3 N/A ug/I 56.6 3 Benzene 71-43-2 C5-C8 ug/l ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 m,p-Xylene C9-C12 ug/l 50.1 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I 53.1° 50 C5-C8 Aliphatics N/A ug/l 1480 a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 109 70-130% FID:2,5-Dibromotoluene % 108 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Secr.11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 Mel 64 of 99 "P M79097 MADEP VPH FORM Matrix A ueous ✓ Soil Sediment 7 Other ❑ Contiffiers ,. ': Satisfactor ✓ Broken F Leaking u.e'ot s Pr se ervatives3: N/A PH<=2 ✓ PH>2 El Rec'd at 2 de Tem stature Received on Ice Received at 4 Deg. C Other ✓ s c Meth,anols ... N/A P. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-13 Lab ID: M79097-18 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 484" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 310 A 50 C9-C10 Aromatics(Unadj.) N/A ug/I 289 A 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 1 m,p-Xylene C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ugh 484 a 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 99 70-130% FID:2,5-Dibromotoluene % 100 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 7Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 Mel 65 of 99 M79097 �' - MADEP VPH FORM Matriz' A ueous W Soil Sediment ❑ Other tl;on-tainers n..�m ,a satisfactory7y Broken 7 Leaking ❑ A ueou:""§Preservatives. N/A p H<=2 [v DH>2 TemO Received on Ice Received at 4 Deg.C Other Rec�d at 2 deg C Methan'ol.. N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-14 Lab ID: M79097-19 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 1 1/2 612 0 08 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I 3200 A 50 C5-C8 Aliphatics(Unadj.) N/A ug/I 1670 A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 5580' 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I 4.6 2 Ethylbenzene 100-41-4 C9-C12 ug/I 170 2 o-Xylene 95-47-6 C9-C12 ug/I 636 2 Naphthalene 91-20-3 N/A ug/I 278 3 Benzene 71-43-2 C5-C8 ug/1 2.8 2 m,p-Xylene C9-C12 ug/I 1260 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I 1660 a 50 C9-C12 Aliphatics N/A ug/I 306° 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 117 70-130% PID:2,5-Dibromotoluene % 121 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CSCB Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑.i Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 ME] 66 of 99 ACCl.P EBT. M79097 =abar::±ore; Ir . MADEP VPH FORM Nlatnx. l -y,., �'�.' A ueous n Soil ❑ Sediment Other ❑ Containersz.5 Satisfactor Broken Leaking A'' ueoufr!-P-6eservatives N/A 0 PH<=2 W PH>2 El item eature�:. Received on Ice Received at 4 De . C Other W Rec'd at 2 deg C ethanol :.. �,I N/A P Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-2 Lab ID: M79097-20 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL (3 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/1 ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ug/I ND° 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 98 70-130% FID:2,5-Dibromotoluene % 99 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑.i Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 EMEJ 67 of 99 T. MADEP VPH FORM Matrix '........� 4 A ueous n Soil n Sediment 7 Other n Containers . SatisfactorvFvl Broken f 1 Leaking 7 Atiu". Preservatives N/A L pH<=2 Rv PH>2 Tem erature Received on Ice Received at 4 Deg. C F1 Other .I Rec'd at 2 deg C Methan.,o,l :,:: N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-104S Lab ID: M79097-21 W Date Collected: 11/26/2008 Date Received: 12/2/2008 Method for Target Analytes: MADEP VPH REV 1.1 P VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A t:g/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A t,g/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 Lg/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/1 ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 105 70-130% FID:2,5-Dibromotoluene % 106 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes U No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect 11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 68 of 99 ACC XrEST M79097 -a^.. ..._.._s MADEP VPH FORM Allatrix .° , Aqueous Soil F Sediment ❑ Other ❑ Con,tal,ners,,, ,, Satisfactory Broken F1 Leakin U 0e U S,:mob Preservatives" N/A H<=2 W H>2 El 0P6Mtwar ... '°; Received on Ice Received at 4 De .C ❑ Other J Rec'd at 2 deg C Metlajlnl, ,. N/A p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-4 Lab ID: M79097-22 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/l ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/l ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 1 Toluene 108-88-3 C5-C8 ug/l ND 2 Ethylbenzene 100-41-4 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/1 ND 2 Adjusted Ranges C9-C12 Aliphatics N/A u9/1 ND c 50 C5-C8 Aliphatics N/A ug/l ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 82 70-130% FID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓❑Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 69 of 99 IZACCUTEBT M79097 "= ` e MADEP VPH FORM Matnx A ueous ICI Soil n Sediment n Other C`oritainers. .: Satisfacto Broken n Leaking A ueou`s P.�eservatIves' N/A H<=2 H>2 Tempe6 Received on Ice Received at 4 Deg. C Other �/ Rec'd at 2 deg C ratur Methan;ola N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-18 Lab ID: M79097-23 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/l ND" 50 Target Analytes Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Adjusted Ranges C9-C12 Aliphatics N/A ug/1 ND° 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 97 70-130% FID:2,5-Dibromotoluene % 100 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? F�Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 M 70 of 99 AM79097 =3 C-1f 1,L^r i 2 0 MADEP VPH FORM Matrix Aqueous Soil Sediment Other ❑ Contait5ers- „ a _''`' Satisfactor .W Broken Leakin ueoti iPrese"rvative N/A I H<=2 ✓ H>2 Tem'erature., ' Received on Ice Received at 4 Deg. C D Other E. Rec'd at 2 deg C Wh U N/A P. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-101D Lab ID: M79097-24 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/1 ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND c 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 83 70-130% FID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 M 71 of 99 AC' M79097 -a. _.._,....e. MADEP VPH FORM Matrix A ueous f�l Soil ❑ Sediment ❑ Other ❑ con-tainers �. -- SatisfactoryFyl Broken 7 Leakina ❑ A u.eous Preservatives: N/A F1 PH<=2 P#1 PH>2 ❑ Tam' eratur® " Received on Ice Received at 4 Deg.C E Other Rec'd at 2 deg C Methanol . .. N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-101S Lab ID: M79097-25 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range units Result RDL g C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene, 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A Ug/1 ND 3 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND' 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 77 70-130% FID:2,5-Dibromotoluene % 77 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C6-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑d No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 Ma 72 of 99 A ST, MADEP VPH FORM Matrix. "W151 Aqueous ., Soil 7 Sediment n Other Co.ntalners.._w '. .. o ' Satisfactory 7 Broken f I Leaking u.et ipfes.ervatives N/A H<=2 W DH>2 Tem era`ture ... Received on Ice F1 Received at 4 Deg. C F Other J Rec'd at 2 deg C MaNdnWi� N/A P. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-102D Lab ID: M79097-26 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PiD: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 Target Analytes o-Xylene 95-47-6 C9-Cl 2 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tent Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/l ND 2 m,p-Xylene C9-C12 ug/l ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/1 ND° 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 84 70-130% FID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. _ C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑d No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 ME2 73 of 99 A M79097 MADEP VPH FORM Iatrlx A ueous n Soil Sediment ❑ Other ❑ ContainersN Satisfacto nI Broken ❑ Leaking r 1 Aciu,eous' Pr servatives� N/A H<=2 ✓ DH>2 fern eri"e n Received on Ice Received at 4 De . C Other W Rec'd at 2 deg C M' has N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-102S Lab ID: M79097-27 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/1 ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 82 70-130% FID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of thDse individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 M15 74 of 99 @ACCUTEST M79097 --- - MADEP VPH FORM Matrix. MA A ueous F.,] Soil ❑ Sediment F1 Other Containers ... Satisfactor W Broken F1 Leaking ueo&us Preser av tiV.es' N/A ❑ H<=2 PH>2 ... „F Received on Ice F1 Received at 4 Deg.C D Other ✓ Rec'd at 2 deg C Methanoh. _ N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-104D Lab ID: M79097-28 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/6/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 96 70-130% FID:2,5-Dibromotoluene % 98 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)end/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? r Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tan Date 12/11/2008 75 of 99 M79097 '- MADEP VPH FORM t x.; k Vlatn � �- A ueous Fy Soil ❑I Sediment ❑ Other Containietsm, Satisfacto n Broken ❑ Leaking ❑ ueoussPreservatives N/A H<=2 W PH>2 Tem enure Received on Ice Received at 4 De . C Other .e Rec'd at 2 deg C Me h not q'iM N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-15C• Lab ID: M79097-29 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2C08 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/8/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 1.1 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges 135-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 94 70-130% FID:2,5-Dibromotoluene % 97 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑d No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 Ma 76 of 99 93AMUTEST. M79097 3 r= r MADEP VPH FORM A ueous W Soil 7 Sediment F-1 Other ❑ ontairt�s SatisfactoryBroken Leakin Gs Preserva eou tives:; N/A H<=2 W1 PH>2 Tem eratureL, -. Received on Ice Received at 4 Deg. C Other d Rec'd at 2 deg C Meths o'I N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-17 Lab ID: M79097-30 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/8/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/1 ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 u9/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ug/1 ND° 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 94 70-130% FID:2,5-Dibromotoluene % 87 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 7i of 99 GACCUMWC M79097 MADEP VPH FORM Matrix Aqueous Soil ❑ Sediment ❑ Other ontairfers"""" Satisfactor Broken ❑ Leaking ❑ ueoas""P�eservat[ves N/A H<=2 ICI H>2 0" "- Rec'd at 2 de Tem etature, .. Received on Ice ❑ Received at 4 De .C ❑ Other n g Methanol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-15 Lab ID: M79097-31 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/8/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A -Jg/I 672" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 519' 50 C9-C10 Aromatics(Unadj.) N/A ug/I 332 A 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I 24.8 2 Naphthalene 91-20-3 N/A ug/I 17.7 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I 27 2 m,p-Xylene C9-C12 ug/I 120 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I 672 6 50 C9-C12 Aliphatics N/A ug/I ND° 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 87 70-130% FID:2,5-Dibromotoluene % 78 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? CYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 1;e No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 M" 78 of,g9 GACCUTEST M79097 --- - --- MADEP VPH FORM Matrt -"' A ueous Soil ❑ Sediment 7 Other Containers Satisfacto , Broken ❑ Leakjn t�eo s.,.Pr�e ervativee N/A D DH<=2 PH>2 Teem° da'ture „„- Received on Ice L Received at 4 Deg. C Other d Rec'd at 2 deg C Irethan.' : N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-19 Lab ID: M79097-32 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/9/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges - CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl.Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ug/I ND° 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 75 70-130% PID:2,5-Dibromotoluene % 79 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. - Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No '❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 79 of 99` M79097 _ - MADEP VPH FORM Matrix :" ..'m A ueous F.,-] Soil Sediment Other Containers Satisfactor J Broken ❑I Leaking A ueo.0'PreserVi ices.?, N/A F1 DH<=2 J DH>2 1-1 Teelr #ure.. Received on Ice nt:° Received at 4 Deg. C Other J Rec'd at 2 deg C Methanol .. N/A .p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-23 Lab ID: M79097-33 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/8/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I 203 A 50 C5-C8 Aliphatics(Unadj.) N/A ug/I 489 A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 352' 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I 19.2 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 1 Toluene 108-88-3 C5-C8 ug/I 4.3 2 Ethylbenzene 100-41-4 C9-C12 ug/I 64.7 2 m,p-Xylene C9-C12 ug/I 70.2 2 Adjusted Ranges C5-C8 Aliphatics N/A Jg/1 485 6 50 C9-C12 Aliphatics N/A Jg/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 79 70-130% FID:2,5-Dibromotoluene % 73 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑J Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑J No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of rry knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 M 80 of 99 T M79097 I MADEP VPH FORM Ifatrlx Aqueous n Soil F1 Sediment 7 Other Containers,. .. ' Satisfactory Broken 7 Leaking t"eou§Preservatives N/A L1 PH<=2 Fy PH>2 Tem°.e ature Received on Ice F1 Received at 4 Deg. C Other Rec'd at 2 deg C Methanol _ �- N/A Pa Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-22 Lab ID: M79097-34 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/9/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/l ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 1 Toluene 108-88-3 C5-C8 ug/1 ND 2 Ethylbenzene 100-41-4 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/l ND 2 o-Xylene 95-47-6 C9-C12 ug/l ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/1 ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/1 ND' 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 81 70-130% f FID:2,5-Dibromotoluene % 76 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/11/2008 r 81 of 99 A M79097 - Accutest Laboratories P. Internal Sample Tracking Chronicle Shell Oil j Job No: M79097 SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Project No: EQ 874 Sample Number Method Analyzed By Prepped By Test Codes v179097 1 Collected 25 NOV 08 12'40By'`RD Received 02-DEC 08By MW 105S M79097-1 MADEP VPH REV 1.106-DEC-08 03:55 AF VMAVPH M79097 2 Collected25 NOV 08 12 20 By: RD Receive d02-DEC-08;,'By: M79097-2 MADEP VPH REV 1.106-DEC-08 04:34 AF VMAVPH -. Iy179097 3 ollected: 25-NOV 08 10>S0 By: RD Received;,;02-DEC-08 By: ,x'N 1 MW-6 k - M79097-3 MADEP VPH REV 1.106-DEC-08 02:36 AF VMAVPH M79097-4 `Collected: 25-NOV-08 09 45;_by: RD Received: 02-DEC-08t.,By MW-1b E M79097-4 MADEP VPH REV 1.1 06-DEC-08 05:13 AF VMAVPH " M79097 5 ;'Collected: 25=NOV 08 09 20 .By: RD Rece-ived'-,"02-DEC-08,:,By: ,1W-3 : M79097-5 MADEP VPH REV 1.1 06-DEC-08 05:53 AF VMAVPH M79097-6 Collected: 25-NOV 08 10:40-"By: RD �; Received 02 DEC-08 By MW7 � M79097-6 MADEP VPH REV 1.106-DEC-08 06:33 AF VMAVPH M79097-7 Collected: 25-NOV 08 1 0.,...By; RD Received "02-DEG-08 By •„ � MW40 M79097-7 MADEP VPH REV 1.107-DEC-08 00:28 AF VMAVPH M79097 8 ,;C,ollected $ 12,I�S 25=NOV 0 Bys T�RD Rece ued 02 EOA8 By: � M79097-8 MADEP VPH REV 1.106-DEC-08 23:48 AF VMAVPH Page 1 of 5 MEJ 82 of 99 UACCUTEBT. M79097 r Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M79097 SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Project No: EQ 874 Sample Number Method Analyzed By Prepped By Test Codes 1I790 7 Collected 25 'NOS? 08 12 35 By ItD' ' 3 ecatve�` 02 DEC 8�� y � «� M79097-9 MADEP VPH REV 1.106-DEC-08 23:07 AF VMAVPH M79097�10 Collected 25 NOV 08�10 OO�By��RD�«��"Rece��ed 02 DEC08 �y x� �� , � �, M79097-10 MADEP VPH REV 1.106-DEC-08 22:27 AF VMAVPH M79097 11 CollectedN09 30 By hRDsF Received DEC08By � � RNT M79097-11 MADEP VPH REV 1.106-DEC-08 21:46 AF VMAVPH N17 0 7 12 Collected 26 N L'08 12 05 By�RD Received 02 DEC 08' By s �� 57111111 n M79097-12 MADEP VPH REV 1.106-DEC-08 13:47 AP VMAVPH M79�09�7 1�3 Collected 26 NOV 08I1�`35�By RD , Received02�DEC 08 By��,' � � � , a M79097-13 MADEP VPH REV 1.106-DEC-08 14:27 AP VMAVPH M79097 14 Collected2�6 N.O0 ®$ 11 20 B' RD Receiu2 DEC 08 �B�Y N- M79097-14 MADEP VPH REV 1.106-DEC-08 17:06 AP VMAVPH MW624 15 Collected O•-26 NU 08 11 05, B Receaved 02 DEC�08 Y a M79097-15 MADEP VPH REV 1.106-DEC-08 17:46 AP VMAVPH ON M M79097-16 MADEP VPH REV 1.106-DEC-08 16:27 AP VMAVPH Page 2 of 5 83 of 99 M79097 Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M79097 SCMAW:97346878 (REIMBMA) 577 West Main Str.-et Hyannis MA Project No: EQ 874 Sample Number Method Analyzed By Prepped By Test Codes -1111,111" -.. FZD- M7�9 97 17 Coll cted' 26 NOV 08 09553y Received 02-DEC 08 By MW 2 � fix_. z' M79097-17 MADEP VPH REV 1.106-DEC-08 15:07 AP VMAVPH M79097 18 C64ected:.26 NOV 08 09:25 By: RD Reeewgd 02-:DEC=08 By: ' MW 13 �. �5 . M79097-18 MADEP VPH REV 1.106-DEC-08 15:47 AP VMAVPH M7,9097-19 Collected: 26-NOV-08 09:00 By:x RD Received: 02-DEC-08 By: M W-14 M79097-19 MADEP VPH REV 1.106-DEC-08 13:07 AP VMAVPH M79097-26 Collected: 26 NOV-08 08:25 By RD Received: 02-DEC-08 By: M79097-20 MADEP VPH REV 1.106-DEC-08 18:26 AP VMAVPH M79097-21 Collected 26-NOV-0812:00 By:`RD Received: 02-DEC-08 By: ,MW i104S M79097-21 MADEP VPH REV 1.106-DEC-08 19:05 AP VMAVPH M79097-22 Collected; 26-NOV,'08 08:20 By:,RD Received: 02-DEC-08 By: MW-4 M79097-22 MADEP VPH REV 1.106-DEC-08 19:44 AP VMAVPH M79097-23 Collected: 26-NOV-08 09:00 By Received: 02-DEC-08 By: �vS�V-18 M79097-23 MADEP VPH REV 1.106-DEC-08 20:23 AP VMAVPH M79097-24 Collected: 26-NOV 08 09:46 By RD Received: 02-DEC-08 By: MW-1O1D M79097-24 MADEP VPH REV 1.106-DEC-08 21:03 AP VMAVPH Page 3 of 5 84 of 99 12A M79097 -'-- -- -- Accutest Laboratories P. Internal Sample Tracking Chronicle Shell Oil �. Job No: M79097 SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Project No: EQ 874 Sample Number Method Analyzed By Prepped By Test Codes Iu�7909725 CaliectBd , 6� 008� 0 00 B R*D ec d DE 08 - Y ,E M79097-25 MADEP VPH REV 1.106-DEC-08 21:42 AP VMAVPH M79097 26 Callected�"26 N®� 0810k0y RDA Received 02 DEC 08�Byfi ` ``� &k MW 102D . .x_. "� ...,...,_,, .• �....a......t.. _ M79097-26 MADEP VPH REV 1.106-DEC-08 22:21 AP VMAVPH 3 Ad 02 DE0�08 By RQ9727 Cll 6 eceiveM%74 MW 1®2S �� s011 NIX' M79097-27 MADEP VPH REV 1.106-DEC-08 23:00 AP VMAVPH M0907 28 Collected 26 NOW 0811 40 By'RD Recer�u�ed DEC 08`By µ77, � M79097-28 MADEP VPH REV 1.106-DEC-08 23:40 AP VMAVPH M79097 29 Collected 26 NOV O8 09 00 sBy •;RDA Received 02 DEC`08 By l 141 M M79097-29 MADEP VPH REV 1.108-DEC-08 20:32 AP VMAVPH M7 097 30 Collected 26 NOV 08 12:OO By RDA Received 02bhb-� 8 By "Emk ,�� M79097-30 MADEP VPH REV 1.1 08-DEC-08 21:13 AP VMAVPH M79�097 1 Collecte26 NOV 08 09 30 ,B,k-,R � Received 02,DEC 08 By z'' MWlS ...� ... ., ,... M79097-31 MADEP'VPH REV 1.108-DEC-08 21:52 AP VMAVPH M�7�097 32�Cgllected�26�NOV 0$ 10�10By�RD��Rece�ued02 DEC pBBy� ', '� � e M79097-32 MADEP VPH REV 1.109-DEC-08 14:43 AF VMAVPH Page 4 of 5 a 85 of 99 A r Accutest Laboratories Internal Sample Tracking Chronicle A Shell Oil Job No: M79097 SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Project No: EQ 874 Sample Number Method Analyzed By Prepped By Test Codes M79097 33 Cokkee ed 6 NO 08 10:45 By: RD Recaived�02,Q E fl$ By MW-__23 - xu ,--._ ... . .. M79097-33 MADEP VPH REV 1.108-DEC-08 23:12 AP VMAVPH M79097 34 Colkected:26 N4V 0$ k k 2fl By ;RD Reced 2 L1EC Q$ Bye ' MW 2 " , ;.: .. - _...... ` M79097-34 MADEP VPH REV 1.109-DEC-08 15:25 AF VMAVPH Page 5 of 5 86 of 99 @A M79097 - -- J f New EnglandJOACCU � �= n. r a t �r,e Section 5 . . GC~'Volatles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries I i 87 of 99 Method Blank Summary Page 1 of I Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1129-MB BD23730B.D1 12/05/08 AF n/a n/a GBD1129 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-1, M79097-2, M79097-3, M79097-4, M79097-5, M79097-6 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5-C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics(Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 86% 70-130% vaa 88 of 99 FaACCUTEBT M79097 a'r::::enree Method Blank Summary Page 1 of I Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBH148-MB BH3015.D 1 12/06/08 AP n/a n/a GBH148 cn The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-12, M79097-13, M79097-14, M79097-15, M79097-16, M79097-17, M79097-18, M79097-19, M79097-20, M79097-21, M79097-22, M79097-23, M79097-24, M79097-25, M79097-26, M79097-27, M79097-28 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 92% 70-130% 615-59-8 2,5-Dibromotoluene 91% 70-130% M 89 of 99 M79097 -'- -- -- Method Blank Summary Page 1 of 1 Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1130-MB BD23758.D 1 12/06/08 AF n/a n/a GBD1130 cn The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-7, M79097-8, M79097-9, M79097-10, M79097-11 CAS No. Compound Result RL Units Q ... .._. . ......... 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND ` 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND` 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 79% 70-13•D%0 615-59-8 2,5-Dibromotoluene 82% 70-130% 90 of 99 OACCLMEBT. Method Blank Summary Page 1 of 1 Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2667-MB AB47127.D 1 12/08/08 AP n/a n/a GAB2667 cse The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-29, M79097-30, M79097-31, M79097-33 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9-C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Limits ..... .._........ ....... 615-59-8 2,5-Dibromotoluene 94% 70-130% 615-59-8 2,5-Dibromotoluene 90% 70-130% f a 91 of 99 IRACCUrEffr. M79097 - -- - Method Blank Summary Page 1 of 1 Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch' GBD1135-MB BD23838.D 1 12/09/08 AF n/a n/a GBD1135 Cn :.a The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-32, M79097-34 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene 83% 70-130% ME] 92 of 99 M79097 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1129-BSP BD23731B.D1 12/05/08 AF n/a n/a GBD1129 GBD1129-BSD BD23732B.D1 12/05/08 AF n/a n/a GBD1129 iv The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-1, M79097-2, M79097-3, M79097-4, M79097-5, M79097-6 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/I % ug/1 % RPD Rec/RPD 71-43-2 Benzene 50 51.7 "103 51.2 102 1 70-130/25 100-41-4 Ethylbenzene 50 52.1 104 51.8 104 1 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 48.8 98 49.3 99 1 70-130/25 91-20-3 Naphthalene 50 45.1 90 45.8 92 2 70-130/25 108-88-3 Toluene 50 52.3 105 51.9 104 1 70-130/25 m,p-Xylene 100 104 104 104 104 0 70-130/25 95-47-6 o-Xylene 50 48.6 97 48.3 97 1 70-130/25 C5- C8 Aliphatics (Unadj.) 150 139 93 137 91 1 70-130/25 C9- C12 Aliphatics (Unadj.) 150 138 92 140 93 1 70-130/25 C9- C10 Aromatics (Unadj.) 50 48 96 48 96 0 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 80% 81% 70-130% 615-59-8 2,5-Dibromotoluene 87% 87% 70-130% Q 93 of 99 IRAC=LMEBT. M79097 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBH 148-BSP BH3016.D 1 12/06/08 AP n/a n/a GBH 148 GBH148-BSD BH3017.1) 1 12/06/08 AP n/a n/a GBH148 iv The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-12, M79097-13, M79097-14, M79097-15, M79097-16, N179097-17, M79097-18, M79097-19, M79097-20, M79097-21, M79097-22, M79097-23, M79097-24, N179097-25, M79097-26, M79097-27, M79097-28 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD 71-43-2 Benzene 50 53.1 106 53.4 107 1 70-130/25 100-41-4 Ethylbenzene 50 55.3 111 55.5 ill 0 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 54.6 109 54.3 109 1 70-130/25 91-20-3 Naphthalene 50 46.5 93 47.2 94 1 70-130/25 108-88-3 Toluene 50 53.4 107 53.6 107 0 70-130/25 m,p-Xylene 100 109 109 ill ill 2 70-130/25 95-47-6 o-Xylene 50 51.9 104 52.0 104 0 70-130/25 C5- C8 Aliphatics (Unadj.) 150 143 95 142 95 1 70-130/25 C9- C12 Aliphatics (Unadj.) 150 144 96 145 97 1 70-130/25 C9- CIO Aromatics (Unadj.) 50 55.3 ill 55.5 ill 0 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 86% 870/,, 70-130% 615-59-8 2,5-Dibromotoluene 85% 86% 70-130% gal 94 of 99 ACCL EST M79097 Blank Spike/Blank Spike Duplicate Summary Page I of 1 Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA)577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1130-BSP BD23759.D 1 12/06/08 AF n/a n/a GBD1130 GBD1130-BSD BD23760.D 1 12/06/08 AF n/a n/a GBD1130 iv The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-7, M79097-8, M79097-9, M79097-10, M79097-11 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD 71-43-2 Benzene 50 51.9 104 52.0 104 '' 0 70-130/25 100-41-4 Ethylbenzene 50 52.2 104 52.3 105 0 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 48.4 97 48.8 98 1 70-130/25 91-20-3 Naphthalene 50 43.2 86 44.4 89..' 3 70-130/25 108-88-3 Toluene 50 52.5 <'105 52.5 105 0 70-130/25 m,p-Xylene 100 104 10.4 105 105 1 70-130/25 95-47-6 o-Xylene 50 48.5 97 48.9 98 1 70-130/25 C5- C8 Aliphatics (Unadj.) 150 140 93 140 93 0 70-130/25 C9- C12 Aliphatics (Unadj.) 150 140 93 137 91 2 70-130/25 C9- C10 Aromatics (Unadj.) 50 48 96 48 96 0 70-130/25 CAS No. Surrogate Recoveries BSP BSD g S Limits 615-59-8 2,5-Dibromotoluene 80% 81% 70-130% 615-59-8 2,5-Dibromotoluene 86% 86%, 70-130% Nye 95 of 99 A Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2667-BSP AB47128.D 1 12/08/08 AP n/a n/a GAB2667 GAB2667-BSD AB47129.D 1 12/08/08 AP n/a n/a GAB2667 Ev The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-29, M79097-30, M79097-31, M79097-33 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/I °ro ug/I % RPD Rec/RPD 71-43-2 Benzene 50 47.7 �5 45.8 92 4 70-130/25 100-41-4 Ethylbenzene 50 48.8 S8 46.9 94 4 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 52.2 104 51.0 102 2 70-130/25 91-20-3 Naphthalene 50 50.0 100 47.7 95 5 70-130/25 108-88-3 Toluene 50 47.7 S5 45.9 92 4 70-130/25 m,p-Xylene 100 99.2 S°9 95.6 96 4 70-130/25 95-47-6 o-Xylene 50 47.6 S5 45.8 92 4 70-130/25 C5- C8 Aliphatics (Unadj.) 150 147 S`8 143 95 3 70-130/25 C9- C12 Aliphatics (Unadj.) 150 141 S'4 136 91 4 70-130/25 C9- C10 Aromatics (Unadj.) 50 ND 99 48 96 3 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 93% 87% 70-130% o 0 0 615-59-8 2 5-Dibromotoluene 90% 85ro 7 -1 0 30/o 96 of 99 AC=UTES'T M79097 = = e w 4 Blank Spike/Blank Spike Duplicate Summary Page 1 of I Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1135-BSP BD23839.D 1 12/09/08 AF n/a n/a GBD1135 GBD1135-BSD BD23840.D 1 12/09/08 AF n/a n/a GBD1135 w iv The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79097-32, M79097-34 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD 71-43-2 Benzene 50 51.8 104 52.2 104 1 70-130/25 100-41-4 Ethylbenzene 50 51.5 103 52.3 105 2 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 50.8 102 51.1 102 A 70-130/25 91-20-3 Naphthalene 50 44.5 i;89 45.1 90 1 70-130/25 108-88-3 Toluene 50 52.0 104 52.5 105. 1 70-130/25 m,p-Xylene 100 103 103 105 105 2 70-130/25 95-47-6 o-Xylene 50 48.2 9.6 48.6 97 r 1 70-130/25 C5- C8 Aliphatics (Unadj.) 150 145 9.7 147 98 1 70-130/25 C9- C12 Aliphatics (Unadj.) 150 138 92 140 93 1 70-130/25 C9- C10 Aromatics (Unadj.) 50 48 I95 48 96= 0 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 73% 760/. 70-130% 615-59-8 2,5-Dibromotoluene 84% 83% 70-130% I 97 of 99 1 at. 1 Volatile Surrogate Recovery Summary Page 1 of 2 Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method cs� w Lab Lab Sample ID File ID S1 a Sl b M79097-1 BD23750.D 74 0' 81.0 M79097-2 BD23751.D 78.0 82.0 ._....................... ........ .__............. ....._.._........... .... M79097-3 BD23748.D 76.0 82.0 ....... ....... ............ ......... ....... ... . . M79097-4 BD23752.D 74>0_,,,-.;`81.0 M79097-5 BD23753.D 77.0 83.0 M79097-6 BD23754.D 75 0_ _ ,;.I' 80.0 M79097-7 B1323780.D 79.0 82.0 M79097-8 BD23779.D 80.0 82.0 M79097-9 BD23778.D 80 0 83.0 M79097-10 BD23777.D 79.0 82.0 M79097-11 BD23776.D 80.0 82.0 M79097-12 BH3022.D 1'0kO 103.0 M79097-13 BH3023.D 104.0 103.0 M79097-14 BH3027.D .89.0 88.0 M79097-15 BH3028.D 87.0 86.0 M79097-16 BH3026.D 93.0 92.0 M79097-17 BH3024.1) 108.0 109.0 M79097-18 BH3025.D 100.0 99.0 M79097-19 BH3021.D 1170 121.0 M79097-20 BH3029.1) 99.0 98.0 M79097-21 BH3030.13 106.0 105.0 M79097-22 BH3031.D 83.0 82.0 M79097-23 BH3032.D 100;0 97.0 M79097-24 BH3033.D 83.0 83.0 M79097-25 BH3034.D 77.0 77.0 M79097-26 BH3035.D 86.0 84.0 M79097-27 BH3036.1) 83.0 82.0 M79097-28 BH3037.D 98.0 96.0 M79097-29 AB47136.D 97.0 94.0 M79097-30 A1347137.1) 87.0 94.0 M79097-31 AB47138.D 78.0 87.0 M79097-32 BD23845.D 75.0 79.0 M79097-33 AB47140.D 73.0 79.0 M79097-34 BD23846.D 76.0 81.0 GAB2667-BSD AB47129.D 8TO. 85.0 GAB2667-BSP A1347128.D 93.0 90.0 GAB2667-MB A1347127.D 94.0 90.0 GBD1129-BSD BD2373213.D 81.0 87.0 GBD1129-BSP BD23731B.D 80.0 87.0 GBD1129-MB BD23730B.D 80.10 86.0 Min 98 of 99 rT M79097 `-abort:; re Volatile Surrogate Recovery Summary Page 2 of 2 Job Number: M79097 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 577 West Main Street Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method w Lab Lab Sample ID File ID S1 a S1 b GBD1130-BSD BD23760.D 810 86.0 GBD1130-BSP BD23759.D 80.0 86.0 GBD1130-MB BD23758.D 79:0111.182.0 GBD1135-BSD BD23840.D 76:-0 83.0 GBD1135-BSP BD23839.D 78 0 84.0 .. . .............. .. ...... ... ...._... .... . ........_... . GBD1135-MB BD23838.D 79..0 83.0 GBH148-BSD BH3017.1) 86.0 ..............._..... .... ......._.....__._............. GBH148-BSP BH3016.D 86 0 85.0 . . ........... . GBH148-MB BH3015.D 92.0 ____' 91.0 Surrogate Recovery Compounds Limits Sl= 2,5-Dibromotoluene 70-130%` (a) Recovery from GC signal #1 (b) Recovery from GC signal#2 99 of 99 M79097 �t Message Page 1 of 1 Martin, Cynthia From: Miorandi, Donna Sent: Monday, April 27, 2009 9:10 AM To: Martin, Cynthia Subject: FW: Groundwater Sampling Results CCP 711--6 w j I&SLLi,:'rs l= CT3) K13) -----Original Message----- From: Poliquin, Megan [mailto:MPoliquin@sovcon.com] Sent: Friday, April 24, 2009 10:19 AM To: Miorandi, Donna Cc: Sherburne, Jason Subject: Groundwater Sampling Results Good Morning-here is out results letters for March Sampling for 577 West Main Street in7 Hyannis.) Thanks- Megan Poliquin Administrative Assistant I email: mpoliquin@sovcon.com phone: 508-339-3200 1 fax: 508-339-3248 Sovereign Consulting Inc. 905B South Main Street Mansfield, MA 02048 www.sovcon.com Science. Service. Solutions. PLEASE NOTE:All information transmitted with and contained in this correspondence contains confidential, proprietary or legally privileged information and is intended for use only by the person or entity to which it is addressed.Any review, retransmission,dissemination or other use of,or taking of any action in reliance upon this information by persons or entities other than the intended recipient is prohibited.If you received this communication in error,please notify the sender immediately.Thank you. z, 4/28/2009 r �QJ`XI K File Edit View Favorites Tools Actions Help Type a question for help '._l tie. -'� L'i �C �P4�Reply MReply to All (*C Forward ��Send/Receive I'�Find Type a contact to find Outlook Shortcuts ! 17 From I Subject [Received �,ze My Shortcuts y' 0 Peterson,Taryn Fuel Tank Mail Merge Letters Wed 411 J2009 10:09 AM 127 KB r LIJI 0 McKean,Thomas Full Fee Schedule)In Effect After Publication in Newspaper Only Thu 312612009 5:05 PM 117 KB IZ51 (5) Ll,) 0 McKean,Thomas FW:mileage rate Mon 1 J512009 6:10 AM 134 KB f=y 0 Crocker,Sharon let Underground Tanks 20 yrs Nov2008.DOC Tue 11 J2512008 4:24... 102 KB y f Outbox , 0 Peterson,Taryn Tank Letters Tue I112512008 10:5... 83 KB q2i Sent Items � 0 Dean Melanson Fwd:oil spill picts 27 Betty's Pond Road Hyannis 13-NOV-08 Mon I I11712008 3:32... 1 MB lif iC4, 0 Marilyn Lopes Business Prices for HHP Fri 212212008 2:22 PM 35 KB QJournal 0 Peterson,Taryn Fuel Tank Code Data Spreadsheet Thu 21712008 2:38 PM 44 KB ;Outlook Upda 0 Amy L,Wallace RE:templates&NOTES! Tue 1 J2912008 4:23 PM 174 KB f_y, 0 Peterson,Taryn Fuel Tank Codes-Test Status Codes added Thu 112412008 9:06 AM 22 KB 0 Miorandi,Donna FW:Phase V ROS&GW Sampling Results Mon 412712009 9:23 AM 5 MB 0 Miorandi,Donna FW:Groundwater Sampling Results _ Mon 412_712009,9:10 AM 695 KB G] 0 Miorandi,Donna FW:Groundwater Sampling Results - Mon 3J23J2009 8:14 AM 923 KB ^ 0 Miorandi,Donna FW:Groundwater Results Letter Thu 31512009 8:37 AM 1 MB 0 Miorandi,Donna FW:Phase V I&M Report for 577 West main Street Hyannis Tue 212412009 9:36 AM 5 MB Anderson,Robin Change of Address Fri 312OJ2009 2:59 PM 2 KB n it GO-D-0 r lan:r FW.Of�nne,c�cFem Mnn A i p-r r7Ano 4•Q 1 YR { From: Miorandi,Donna To: Martin,Cynthia Subject:FW:Groundwater Sampling Results Cc: Attachments:U'1GWS Results Letter-4-24-09.pdf(683 KB) -----Original Message----- From:Poliquin,Megan[mailto:MPoliquin@sovcon.com] Sent:Friday,April 24,2009 10:19 AM To:Miorandi,Donna Cc:Sherburne,Jason Subject:Groundwater Sampling Results i I _ t Good Morning-here is out results letters for March Sampling for 577 West Main Street in Hyannis. Thanks- I Megan Poliquin Other Shortcuts ' 60 Items,10 Unread I d iStart , »(Ipswitch IM , ®Inbox-Microsoft Outlook w 9 42 AM File Edit View Favorites Tools Actions HelpI T_+ e a uestion For h I P Q P New I Q=i X P40 Reply 04 Reply to All I C�SendJReceive f ID � [� t p y ��Forward _ � Find Type a contact to find � I low 0 Q o Outlook Shortcuts From I Subject I Received l'Size My Shortcuts �y' ® Peterson,Taryn Fuel Tank Mail Merge Letters Wed 41112009 10:09 AM 127 KB 0 McKean,Thomas Full Fee Schedule)In Effect After Publication in Newspaper Only Thu 312612009 5:05 PM 117 KB Drafts(5) f] 0 McKean,Thomas FW:mileage rate Mon 11512009 8:10 AM 134 KB y 0 Crocker,Sharon let Underground Tanks 20 yrs Nov2008.DOC Tue 1112512008 4:24... 102 KB Outbox Ey, 0 Peterson,Taryn Tank Letters Tue 1112512008 10:5... 83 KB i; Sent Items 0 Dean Melanson Fwd:oil spill Picts 27 Betty's Pond Road Hyannis 13-NOV-08 Mon 1111712008 3:32... 1 MB { 0 Marilyn Lopes Business Prices for HHP Fri 212212008 2:22 PM 35 KB 4 -a0'Journal 0 Peterson,Taryn Fuel Tank Code Data Spreadsheet Thu 217J2008 2:36 PM 44 KB t 0 Am L.Wallace RE:templates&NOTES! R Outlook Upda y P Tue 1 J29J2008 4:23 PM 174 KB r y 0 Peterson Taryn Fuel Tank Codes-Test Status Codes added Thu 112412008 9:06 AM 22 KB 0 Miorandi,Donna FW Phase V ROS&GW Sampling Results Mon 4J27J2009 9:23 AM 5 MB W, !� 0 Miorandi,Donna FW:Groundwater Sampling Results Mon 4127J2009 9:10 AM 695 KB 0 Miorandi,Donna FW:Groundwater Sampling Results Mon 3123J2009 8:14 AM 923 KB 6] 0 Miorandi,Donna FW:Groundwater Results Letter Thu 31512009 8:37 AM 1 MB 0 Miorandi,Donna FW:Phase V I&M Report For 577 West main Street Hyannis Tue 212412009 9:36 AM 5 MB Anderson,Robin Change of Address Fri 312012009 2:59 PM 2 KB .gin crooro. la..:c FW_Dk---c,.cFom M....A/7R./7flfl0�•� f VR From: Miorandi,Donna To: Martin,Cynthia Subject:FW:Phase V ROS&GW Sampling Results Cc: 4 Attachments:V,)EQ711-GWS Results•pdF(531 KB); tEQ71I-Phase V R05I&M-4-21-09.pdf(4 MB) 1 r Original Message----- From:Poliquin,Megan[mailtD:MPoliquin@sovcon.com] j Sent:Friday,April 24,2009 12:02 PM To:Miorandi,Donna E Cc:Sherburne,Jason Subject:Phase V ROS&GVV Sampling Results Hello-Here is the Phase V ROS Report dated 4121109 and our results letter for Groundwater Sampling done in March for the site located at 1140 Iyannough Road in Hyannis,MA Thank You Megan Poliquin J Other Shortcuts 60 Items,10 Unread h ! Start 1,�j Ipswitch IM ®Inbox-MicrosoFt Outlook V r}' 9:41 AM [ Town of Barnstable �pFiHE Tows Regulatory Services Thomas F. Geiler,Director BARNSTABLE, * MASS Public Health Division 059. 0 iOrFn Mop" Thomas McKean, Director 200 Main Street, Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 Application Fee: $100.00 ASSESSORS MAP AND PARCEL NO. DATE APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE MORE THAN 111 GALLONS OF HAZARDOUS MATERIALS FULL NAME OF APPLICANT NAME OF ESTABLISHMENT Q 1�(� �, /�� / W(?4 ADDRESS OF ESTABLISHMENT 7 Lcl�_ M Q S TELEPHONE NUMBERd S� SOLE OWNER: AYES NO t IF APPLICANT IS A PARTNERSHIP,FULL NAME AND HOME ADDRESS OF ALL o PARTNERS: } ao L, �� rn IF APPLICANT IS A CORPORATION:: FEDERAL IDENTIFICATION NO.� /STATE OF INCORPORATION A-SS FULL NAME AND HOME ADDRESS OF: PRESIDENT 7 6� (>?td Y (� TREASURER 4//, V-4 /i'/ 3 CLERK SIGNATURE OF APPLICANT RESTRICTIONS: HOME ADDRESS HOME TELEPHONE# 7 ?„? 9 Haz.doc/wp/q • • August 7,2009 Thomas A.McKean Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601 John C.Klimm Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 a Re: Availability of Inspection&Monitoring Report for Phase V Remedy Operating Status Former Shell-Branded Gasoline Station 577 West Main Street - Hyannis,Massachusetts MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase V Remedy Operating Status &Monitoring Report was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location(the disposal site). The report summarizes activities conducted between February 2009 and August 2009. Continued`activities on site will include: • Quarterly groundwater gauging and sampling scheduled for September and Dec'e'"inber 2009 • Submittal of ROS Status Report on February,2010. �- � r` -n Copies of the report can be obtained at the Massachusetts Department of Enviro�#r'ental PrZ@SctioT Southeast Regional Office in Lakeville, Massachusetts. If you have any questions please call they undersigned at(508)339-3200. ss Sincerely, r s'- SOVEREIGN CONSULTING,INC. M son Sherburne ( is15.Simpson,P.G.,LSP Project Manager Operations Manager cc: MassDEP SERO Mr.David Weeks,Motiva Enterprises LLC Sovereign File-EQ874 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 �a February 3, 2010 ups#_a.- jgj��o 01 g000 (y9 Thomas A. McKean Town of Barnstable Public Health Division 200 Main Street Hyannis,Massachusetts 02601 UPS# qy,� '�o John C. Klimm Barnstable Town Manager 387 Main Street Hyannis,Massachusetts 02601 Re: Notice of Availability of Phase V Remedy Operating Status and Remedial Monitoring Report Former Shell-Branded Gasoline Station '577 West Main Street V ' Hyannis, Massachusetts) MassDEP RTN 4-16772 To Whom It May Concern: In accordance with the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification that a Phase V Remedy Operating Status & Remedial Monitoring Report was submitted to the Massachusetts Department of Environmental Protection (MassDEP) for the above referenced location (the disposal site). The report summarizes activities conducted between August 2009 and February l 2010. A summary of findings and conclusions for response actions at the dispoal site have been provided in the March 2005 Phase If Comprehensive Site Assessment, Phase III Remdial Action Plan, Phase IV Remedy Implementation Plan and Final Insepction Report, the September 2005 Phase III Remedial Action Plan Addendum, Phase IV Remedy Implementation Plan Addendum, Phase V Remedy Operation Status Opinion and Substantial Hazard .-Evaluation, as well as subsequent status reports prepared for the disposal site. The selected remedial action alternative for the "disposal site' is utilization of monitored w natural_ attenuation (MNA) and removal of light non-aqueous phase liquid (LNAPL)via %active and passive methods. Continued monitoring of dissolve-phase gasoline plume size and geochemical conditions inside and outside of the plume are being obtained on a quarterly basis. Monitoring of LNAPL is performed concurrent with groundwater monitoring, and LNAPL removal is conducted when necessary. LNAPL was not detected in disposal site monitoring wells during this reporting period. 905B S. Main Street, Unit 202 - Mansfield, MA 02048 -Tel: 508-339-3200 0 Fax: 508-339-3248 c4 t Copies of the report can be obtained at the Massachusetts Department of Environmental Protection Southeast Regional Office in Lakeville, Massachusetts. If you have any questions please call the undersigned at(508) 339-3200. Sincerely, SOVEREIGN CONSULTING,INC. Jason E. Sher k-Sarah1 Le Boucher, LSP Senior Project Manager Senior Project Manager cc: MassDEP SERO (within report package) Mr. David Weeks, Motiva Enterprises LLC (within report package) Sovereign File - EQ874 I SOVEREIGN • Decemberk7,2017 Thomas A. McKean Y Town of Barrgtable Public Health Division 1 A 200 Main Street Hyannis,Massachusetts 02601 , E r: Thomas K. Lynch Barnstable Town Maiager 387 Main Street Hyannis,Massachusetts 02601: Re: Notice of Availabili.ty4 of Phase.. em:edy Operation Status and Remedial Monitoring"Report `"`1; Former Shell-Branded Gasoline Station 577 West Main Street Hyannis, Massachusetts MassDEP RTN'4-16772 To Whom It May Concern ` In accordance.with'{the Massachusetts Contingency Plan (MCP) 310 CMR 40.1403 (3)(e), this correspondence serves as notification 'that a Phase V Remedy Operation, Status. .£ Remedial Monitoring Report t,(ROS-RMR) was.' submitted to the Massachusetts Department of Environmental Protection(Mas9DEP) for the above referenced location (the disposal site). The report summarizes'activities conducted 2b,6tween June and December 2017. A summary of fin' gs and conclusions Ifor response actions at the disposal site have been provided in previ6us reports-'submitted to the Massachusetts Department of Environmental Protection (MassDEP). The selected remedial action.alternative for the "disposal site" is the operation of an air sparge and soil vapor extraction (AS/SVE) remediation system coupled with monitored natural attenuation (MNA) for the downgradient portion of the plume. Currently the AS/SVE system is not in operation. Continued monitoring of the dissolve-phase gasoline plume and geochemical conditions within the plume, and up and downgradient of the plume are being conductedon a quarterly basis."" :. _ .f; Copies of the report¢can be,obtained.at the MassDEP Southeast Regional Office in Lakeville, Massachusetts. If you have anyj questions,please call the undersigned.at(508) 339-3200. E Sincerely, SOVEREIGN CONSULTING INC C" Lisa M.Stone _ Rachel B.Leary,P.E;,LSP Senior'Project,Manager Senior Project Manager cc: MassDEP SERO(within report package) Mr.Marc Oler,SOPUS(within report package) Sovereign File-2S874 16 Chestnut Street, Suite 520 • Foxborough, MA 02035 •Tel: 508-339-3200 • Fax: 508-339-3248