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Home My WebLink About0810 WAKEBY ROAD - Health 810 WAKEBY ROAD' �I Fi 4 r 4 r� UPC 12934 ' N6.2-153LYro HA,STINQ,4 MN .. ��" ��' 1 �� O �� , �� "� C�y'� � � �� .� --�--�-- ��° �� C/Y �i� �� v � �\� �G�� '` � SITEC ' ENVIRONMENTAL Civil and Environmental Engineering,Land Use Planning,Hazardous and Solid Waste Consulting SITEC ENVIRONMENTAL, Inc. 769 Plain Street, Unit C 449 Faunce Corner Road ' Marshfield, MA 02050 Dartmouth, MA 02747 Tel. (781) 319-0100 FAX(781) 834-4783 Tel. (508) 998-2125 FAX(508)998-7554 ' November 8, 2018 Mr. Mark Dakers, Solid Waste Management Section Department of Environmental Protection ' 20 Riverside Drive Lakeville, Massachusetts 02347 Reference: 810 Wakeby Road, Barnstable Application for BWPSW25, Corrective Action Design (CAD) Transmittal No. W097656 Dear Mr. Dakers: As we discussed at our meeting of October 30, 2018, Gifford Brothers Sand & Gravel (Gifford Brothers)and TJA Clean Energy(TJA)would like to modify the Comprehensive Site Assessment Scope of Work(CSA-SOW)that was approved in the Department's January 30, 2007 Provisional Approval for the Corrective Action Design (CAD) for the referenced site. SITE CHARACTERIZATION iSince the CAD,dated October 26,2006,was issued,a significant amount of site clean up work has been accomplished by Gifford Brothers. The attached Figures 1 and 2,in plan and aerial photograph format,show the existing conditions of the site in 2005,respectively. As noted on the figures,there were potential contamination sites identified as a stump dump, a pile of an estimated 10,000 tires, a pile of unprocessed asphalt,brick and concrete(ABC),a pile of processed ABC and a substantial ' amount of junk vehicles. Between 2005 and 2007 Gifford Brothers excavated,ground and screened the stump dump and either sold off the product as mulch or soil and retained a portion of the processed material on site for use as top soil. The tire pile has been removed and sent to a tire recycler. The unprocessed ABC was processed(crushed)and removed from the site,along with the processed ABC,for reuse as aggregate. Figure 3,a 2007 aerial view,indicates how the site had been excavated and cleared in those areas, when compared to the 2005 aerial. Also in 2007, seven soil samples were taken in the areas that had previously been the site of the unprocessed and processed 1 ABC piles. The samples were analyzed for EPH, PCBs and metals. The results indicated no exceedances of MCP S-1 standards. The laboratory reports are attached. Figure 4 is a current t (February 2018)aerial photograph that shows the site as partially revegetated in the areas that were cleared in the 2007 aerial photograph and that there is a significant reduction in the number of junk vehicles from 2005. 810 Wakeby Road, Barnstable November 8, 2018 Page 2 PROPOSED CSA-SOW ' Gifford Brothers and TJA believe that the previous site remediation work has removed all potential contamination source materials and that the removal of the source material has mitigated the potential of impacting groundwater in the vicinity of 810 Wakeby Road. Consequently, Gifford Brothers and TJA are requesting MassDEP to approve a revised CSA-SOW that will update the site's environmental characterization,conduct a sampling and analysis program that will confirm the removal of potential contamination source material at identified locations and any currently unidentified locations that my indicate potential contamination and sample an existing on-site irrigation well. ' Environmental Site Characterization ' Using available information from MassDEP, the Town of Barnstable and the Town of Sandwich, potential environmental receptors and resources will be identified and characterized,to at least 500 feet from the site's perimeter. Information sources will include Massachusetts GIS mapping along with any GIS information that Barnstable and Sandwich may provide, relative to such things as resource protection districts and groundwater flow direction. The Towns' Board of Health and Water Department records will be reviewed to determine if there are any private wells and to confirm the presence of public water supply systems in the vicinity of the site. 1 Site Investigation The purpose of the site investigation work will be to confirm that the site remediation work, done to date, has removed potential contamination sources that could threaten environmental receptors 1 and that the site can be closed as a solid waste facility. Figure 5 shows a proposed soil sampling program in the identified areas where materials were previously stored and have been removed. The sample grids represent areas of approximately 2,500 square feet (50' x 50'). Samples will be composited from within the top two feet of each of the approximate grid areas. Each sample will be analyzed for metals, SemiVOCs, PCBs and TPH. In addition the rest of the site will be canvased for any signs of contamination, such as stained or odorous soils and pockets of stressed vegetation. ' Any of these areas will also be sampled and analyzed as described above,with the possible addition of analyzing for VOCs, where signs of potential contamination can be the result of fuel spills. Should soils analysis indicate the presence of contamination ofgreaterthan MCP S-1 criteria,further remediation,such as soils removal may be conducted in that area. Further sampling and analysis of ' residual soils will be conducted to confirm that contamination above MCP S-1 levels, has been removed. The excavated material will then be properly removed from the site for reuse or disposal, tusing either a Bill of Lading(BOL) or Material Shipping Record(MSR) procedure. In addition there is an irrigation well located on site,approximately where shown on Figure 5. The well will be purged and sampled for the parameters listed above and VOCs. Also, if any private wells are found to be located within 500 feet of the site, a request will be made to the well's owner to sample their well. 810 Wakeby Road, Barnstable November 8, 2018 Page 3 ' Site Assessment Report A Comprehensive Site Assessment Report will be prepared which will present the results of the Environmental Site Characterization and Site Investigation work described above. The report will summarize the findings of the Environmental Site Characterization by tabulating and graphically depicting locations of identified receptors and resources within a 500 foot radius of the site. Using that information the applicable groundwater criteria will be determined for the site. If there are critical receptors and resources in the vicinity of the site, possible mitigation measures, such as providing a public water supply connection and abandonment of a private well, may be proposed. The report will includ e de a description of all of the Site Investigation work that has been conducted. Activities will be documented with photographs,field logs and laboratory reports. Laboratory data will be tabulated and compared to the applicable standards that are developed in the Environmental Site Characterization summary,described above. Should any remedial action,such as soil removal be performed,that work and laboratory reports of removed and residual materials will be included ' and evaluated. Conclusions and recommendations will be developed and presented in the report, which will determine whether closure of the site as a solid waste facility is appropriate, or whether further action may be required to attain that status. The report will be submitted to MassDEP for its approval. ' Thank you for your consideration of the proposed modification to the CSA-SOW for the 810 Wakeby Road, Barnstable site. If you have any questions, please don't hesitate to contact me. Sincerely, A. Raymond Quinn, PE Senior Project Manager cc: Gifford Brothers Sand& Gravel TJA Clean Energy Town of Barnstable, .Board of Health Town of Sandwich, Board of Health 1 1 1 1 1 1 ' FIGURES i AiOA� h No. j2 AREA = +/— 19.32 ACRES APPROXIMATE AREA OF STUMP DUMP APPROXIMATE AREA OF 0 60 120 180 STOCKPILED TIRES r: APPROXIMATE AREA OF TOP SOIL STOCKPILE SS-2 SS-3 n SS-4 APPROXIMATE AREA OF ASPHALT, APPROXIMATE AREA OF BRICK AND CONCRETE (ABC) DISPOSAL PROCESSED ABC STORAGE WAKEBY ROAD ..•• 810 1/AKEBY ROAD `r V, SITEC . �ARSTONS MILLS �+ �► �. 2o,e 0 =� ENVIRONMENTAL Cla )� -----�� TJA CLEAN ENERGY FIGURE 4 ..r —W — FEBRUARY 2018 SITE IMAGE ..r...w. 1VIL a(M- PARC-Aj 1NJ. 5- AREA = +/- 19.32 ACREjF ilk— "'JRAI ' c ♦. c r ��Y{r'�yyY¢ G a 4 lat �3 3 .sir a ;v®r ,. ekfi APPROXIMATE AREA OF STUMP DUMP i APPROXIMATE AREA OF 60 120 180 STOCKPILED TIRES i k ' ' ° ,. _ .- y7;Sr _ tag t!•'�"• APPROXIMATE AREA OF a ss_1 ' TOP SOIL STOCKPILESS-2 A .t SS-3 mnj °1 SS-4 APPROXIMATE AREA OF ASPHALT, APPROXIMATE AREA OF BRICK AND CONCRETE (ABC) DISPOSAL PROCESSED ABC STORAGE SP-1-1 SP-1-2 SP-1-3 WAKEBY ROAD ..... 810 WAKEBY ROAD -r m mom w gob :� EC w�i,,,.:,,w� , MARSTONS xu.ts .. �.A 2010 : y I[NVIRONMENI'AL ■ ++ TJA CLEAN ENERGY "d" FIGURE 3 JULY 2007 SITE allGE •r.�" awl PARCEL No. 52 RE ' , vA�V Ilk w i " .� � ;' arm '~ � r , �► w 1iirI F. ' op 'K APPROXIMATE 4'y Y w•'i s AREA OF STUMP DUMP � V -APPROXIMATE AREA OF ! 1 400 STOCKPILED TIRES R t: APPROXIMATE . . . . • ' SOIL STOCKPILEi APPROXIMATEAW . . . . :- . . . . . : . .. . PROCESSED ABC -STORAGE- 1 810 WAKEBY ROAD VARSTONS MILTcm)swem NVIRONMFNTAI FIGURE 2 APRIL 20051 . �� PARCEL No. 52 ��<1 `', r '; r o AREA = +/- 19.32 ACRES -�—CU (/ �1 ,��Iltll�I'1 II __ '� 1 1 1\' \girl h•\ / ♦ J/� ' _ __ �__— \ \� ' a _ 'r'Inpull41111\1 It - �,�,�\ •_, \;\\\�\\�'♦ir`�\ f�I''�";:+� _ �- ;I/(.%j;l .tad,. _ •r, 1\, -• 'A, - - / ' br,) I \ \ ;.)1 �\1\\\`1\I\\♦ f`/ \\ '�, \ 1/^� s\ _ rid' ♦, �\I, al \\;;�\\\ 1 ' ` \ '� ,11 it t t 1l VI ill I/ /i / qq,, 1;,III I11 , ,l ♦ ////`\ / /// , 1 I I , !' / 'O - � ,l• +), - '.yY'I \I 1 i nlnl \i�,�P / � , 11 , ' �♦ �;�� , I 1 I.__ r / ; I'!,' 1 1'I'�IIII IlI1111 - 'I I i'Il .Il/l`I\� ,tl , 1 , _ (F, \ / � I r,,�11/11 I 1\ ,!q ; /.,iii� \ * 1 ,A I\\` / I \` tp \ 'P"li) ,i.11pN "Ill II 11 it i - `.'t`111`r�j/� "bF/ +Ip11\IIIIVIII II I III'll%\\\'t 1 \\y �1 - I III �11 - r Ali 1\`V PROPOSED SOIL SAMPLE LOCATIONS (TYP.) ,�," - APPROX. 50'x 50' GRID (+/-2,500 S.F. - METALS SVOCs TPH & PCBs ' ,JdF MMUqE AWA 1i1 NOTE: EXISTING CONptnONS BASED ON It ` '11`,I`I ili' _ , i' A PLM BY DOWN CAPE ENGINEERING.',, - hll INC:, DATED AUGYST 22, 2W5. _ _ - 111,Ii IIII r// ' ` `\ �`� 1 ' l '' \\ , l J ,�_� \ ,1 \' ` lIt- ,,�,�9T'// \ or-111) it �`\ :/I IIII/ / \ l/f ri / t`Il It \ ♦\ \`\ ♦,` {/ t\117 ��I 11\1\1\1 1\ ``\ Il illlj it \`` `\ ' � \``♦ � - �11.11`1,11, SAMPLE `EXISTING\ \ 1 itIt, / IRRIGATION WELL Y. PROPOSED CONFIRMATORY I / SOIL SAMPLES (TYP.) \III 1 11 II .1 t//.-,� /�-'1 \{1_�I ♦'' '%rlI 141 \ ,\\ /I l If 0 60 120 180 �♦ i \- I,i it" I I li;'tl.,/`,, , ,\_,,Iit \\\ , , ' ,, '3,\,/;:�- - , 1 I ,AI1F1RODalA7E AREA OF ASPWILT, AMMISM1E�,AREA,, :BRICK AMOONCPEIE (IBC) DISPOSAL ; Mp SOL SLOE' IC1I I` L._i It it RY It APPIWXM OF lE AREA OF PROCESSm ABC S'IORAOE l`2 j $ .,•. 810 WAKEBY ROAD -+ AS SHNM M. o� � or AV 7� 1� SITEC S pbbftillr�IPt 0 ronmenal,Inc. MARSTONS MEUS .4 Oct.n,2018 IY�K M� �Y ENVIRONMENTAL as ar0°w-ao --��I--�-�I- TJA CLEAN ENERGY ••�►�` FIGURE 5 - SITE PLAN '" —' — PROPOSED SITE ASSESSMENT \ _ = . 1 8 - 'I , 1 r PARCEL No. 52 o ' e AREA = +/— 19.32 ACRES �111 li �`($ \\`- `\\\�tN\\�.11.` I\1+.. - i' ou � , t' j / � \5�-�;1 '_\:♦ �1 r \\.\\\\`,\1\\�\��:f+-`\-� \ 'I ''_'^i i��\1�\j\\t\ 1\\ 1 !' I :J I 1 11 ': � _ \{Jf,�l' , f`1111\it 111 lti I I \ 4i\r l% 111 I I .1 04 17111 - - I' ♦`a '.1\\Illlj\�� \i� l ,�;�� r'Ii3 I �/, lal'ly \��\\1 I // ' � 1 � h _/ ' \ter r// 1 I L f�4�i' 1 \ I I \,11110,11'Inf - ' ,I/ /i/ \ ' ' I'/ I // ' \ 1 I ,I �u\ll,71 `` i+i/ �� f ' I lii ��4 i \\l i 1 t 1' l II -i111n11/!,1` 1/ � 4� 111 Illl l�h\h ' II 1}'I'/ i I \lV� I I I// -•' ,�II I 1 ,- \\ - • , Iil 1111�' -'\,I 11�1Jr 4V� `!l IUI\I 11,J.•.i \\\ ! 1`�IR'1r_11J, IIh ,I'I' �\riL �1 Q�,' 1\ __4 i.: `'\'\} \ l �' i/ i i'• /, . AREA Of QTvMp!WB\` i7+ %il if \1 it 1�V I \• 1 1\ 1' _ / , I ' _' i \\ . . - .$ i IIII\ Oi}�\V\ \'J 1 1 11.�. � 11�• , / 7 / ,' / \\\; : 1 i t i, \�U , / ♦ 1 I , t \\\ NOW- EXISIING CONOWNS BASED ON iiil -70 1 II III I!I/ i 1i \ A PUN BY DOWN CAPE ENGINEERING.\\ 1lt,l - ;Pi 111 J11 (r i 1\�i '`` ii ' Ir ' i \\��: INC.. WED AUWST 22. 2905. . i_, v„J7 a i q i \\\`I\, , t 1 1 `, \y.�. .per• .. 1' �''li!' j IF - yl^\i..:� �.1�'I __� i/' �`�� \ � I 1\ •\ �Syyy/p�M11C 403 ' I�fi .IIII lliiil �\ /1/raj I'd, SOIL SAMPLES TAKEN 1 IN 2007 (INP.) lb U 120 19U \I I Ti3 � S$ y.' i 1 1 OAPPPIRIMVu1WE AAREEA OAF ASPNALLT.d�cA Tr/RpVA�/OyO��Iy�f�i.A�^. � VW IAA/ OONCWE O/' WSPOSL \}\ TOP SOIL STOCKPLE Ir I` 11 I ' 4'_ .,\\\ .\♦ —_ �i\�.''�;j / Ss- J II I - . SOIL SAMPLES TAKEN pp/A�/P�PROX�YATE AREA OF it, Hb PROCESSm ABC 51ptA0E Pit} I fill j1 1 ttt \ All lam+ 810 WAHEBY ROAD ad* AS s� we Dab FAokbn DNagal SI JI,'HCEn.-"4111cmal.Inc � MARSTONS JMJ .�, .U.wig TEC ENVIRONMENTAL sal0"a"= +� TJA CLEAN ENERGY dm`as FIGURE i — ME PLAN - 2005 K SMG CONDITIONS �� 1 1 1 1 1 1 1 1 SOIL SAMPLE RESULTS I � 4 1 WOODS H E LASS ANALYTICAL REPORT Lab Number: L0710600 Client: Sitec Environmental, Inc. 769 Plain Street Unit C Marshfield, MA 02050 ATTN: Geoff Souza ' Project Name: WAKEBY ROAD, CAD Project Number: SE01-615-1 ' Report Date: 09/28/07 Certifications&Approvals: MA(M-MA086),NY NELAC(11148),CT(PH-0574),NH(200305),NJ(MA935),RI(LA000065),ME(2006012), ' PA(Registration#68-03671),USDA(Permit#S-72578),US Army Corps of Engineers,Naval FESC. ' Eight Walkup Drive,Westborough, MA 01581-1019 508-898-9220 (Fax)508-898-9193 800-624-9220 -www.alphalab.com Fage 1 of 52 �___. . vvwv. .�.vv ' Project Name: WAKEBY ROAC, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 Alpha Sample ID Client ID Sample Location L0710600-01 Sh-1-1 810 WAKEBY ROAD L0710600-02 SR-1-2 810 WAKEBY ROAD L0710600-03 S`.?-1-3 810 WAKEBY ROAD L0710600-04 S3-1 810 WAKEBY ROAD ' L0710600-05 S3-2 810 WAKEBY ROAD L0710600-06 S3-3 810 WAKEBY ROAD II Cage 2 of 52 ----- 1-- Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 1 MADEP MCP Response Action Analytical Report Certification ' This form provides certifications for all samples performed by MCP methods. Please refer to the Sample Results and Container Information sections of this report for specification of MCP methods used for each analysis. The following questions pertain only to MCP Analytical Methods. An affirmative response to questions A, B, C & D is required for"Presumptive Certainty" status ' A Were all samples received by the laboratory in a condition consistent with those described on YES their Chain-of-Custody documentation for the data set? ' B Were all QA/QC procedures required for the specified analytical methods(s) included in this YES report followed, including the requirement to note and discuss in a narrative QC data that did not meet appropriate erformance standards orguidelines? C Does the analytical data included in this report meet all the requirements for"Presumptive YES Certainty", as described in section 2.0 of the MADEP document CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only: Was the VPH or EPH method run without significant modifications, YES asspecified in Section 11.3? A response to questions E and F is required for"Presumptive Certainty" status E Were all QC performance standards and recommendations for the specified method(s) YES achieved? ' F Were results for all analyte-list compounds/elements for the specified method(s)reported? NO ' For any questions answered "No", please refer to the case narrative section on the following page(s). ' Please note that sample matrix information is located in the Sample Results section of this report. IP age 3 of 52 Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 Case Narrative The samples were received in accordance with the chain of custody and no significant deviations were encountered during preparation or analysis unless otherwise noted below. MCP Related Narratives: ' PCB L0710600-01 through -06 were re-extracted within holding time due to a Quality Control failure. Re- extraction was within method acceptance criteria; therefore, the re-extracted data is reported. Metals ' In reference to question F: At the client's request, all submitted samples were not analyzed for the full MCP list of compounds specified for the Method. 1 I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: UWAA` + Title: Technical Director/Representative Date: 09/28/07 r; age 4 of 52 ! -.,- 1 1 1 ORGANICS ALPWA tage 5 of 52 1 1 1 1 1 1 1 PETROLEUM HYDROCARBONS Page 6 of 52 P N tProject Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-01 Date Collected: 07/23/07 08:20 Client ID: SP-1-1 Date Received: 07/24/07 ' Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 61,EPH-04-1 Extraction Date: 07/27/07 12:30 ' Analytical Date: 07/30/07 14:35 Analyst: BN Percent Solids: 96% QualFfy Control Information Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method � I Parameter Result Qualifier Units RDLJ Dilution Factor Extractable Petroleum H drocarbons Y ' C9-C18 Aliphatics ND mg/kg 6.94 1 CA-C36 Aliphatics ND mg/kg 6.94 1 C11-C22 Aromatics ND mg/kg 6.94 1 C11-C22 Aromatics,Adjusted ND mg/kg 6.94 1 Naphthalene ND mg/kg 0.347 1 2-Methylnaphthalene ND mg/kg 0.347 1 ' Acenaphthylene ND mg/kg 0.347 1 Acenaphthene ND mg/kg 0.347 1 Fluorene ND mg/kg 0.347 1 _._.. Phenanthrene ND mg/kg 0.347 1 A nth racene ND mg/kg 0.347 1 Fluoranthene ND mg/kg 0.347 1 Pyrene ND mg/kg 0.347 1 Benzo(a)anthracene ND mg/kg 0.347 1 Chrysene ND mg/kg 0.347 1 Benzo(b)fuoranthene ND mg/kg 0.347 1 Benzo(k)fluoranthene ND mg/kg 0.347 1 Benzo(a)pyrene ND mg/kg 0.347 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.347 1 Dibenzo(a,h)anthracene ND mg/kg 0.347 1 - -_ -- --_. - - - - --- . ---. - _ Benzo(ghi)perylene ND mg/kg 0.347 1 I i Page 7 of 52 vvwv �.vv Project Name: WAKEBY ROAD,CAD Lab Number: L0710600 ' Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-01 Date Collected: 07/23/07 08:20 Client ID: SP-1-1 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Extractable Petroleum Hydroc#lons ,. Acceptance Surrogate % Recovery Qualifier Criteria 1 Chloro-Octadecane 73 40-140 o-Terphenyl S3 40-140 ' 2-Fluorobiphenyl 76 40-140 2-Bromonaphthalene 74 40-140 II II 1 I �A&kA 'Page 8 of 52 Project Name: WAKEBY ROAD,CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-02 Date Collected: 07/23/07 08:40 Client ID: SP-1-2 Date Received: 07/24/07 ' Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 61,EPH-04-1 Extraction Date: 07/27/07 12:30 ' Analytical Date: 07/30/07 11:33 Analyst: BN Percent Solids: 95% 7'717W NQ W!4 Control nformation�-' ' Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Extracted Per the Method Sample Extraction method: r . Parameter Result Qualifier Units RDL Dilution Factor =ffactable Petroleum Hydrocarbons T. . C9-C18 Aliphatics ND mg/kg 7.02 . . C197C36 Aliphatics ND mg/kg 7.02 1 C11-C22 Aromatics ND mg/kg 7.02 1 C11-C22 Aromatics,Adjusted ND mg/kg 7.02 1 Naphthalene ND mg/kg 0.351 1 2-Methylnaphthalene ND mg/kg 0.351 1 Acenaphthylene ND mg/kg 0.351 1 Acenaphthene ND mg/kg 0.351 1 Fluorene ND mg/kg 0.351 1 Phenanthrene ND mg/kg 0.351 1 A nth racene ND mg/kg 0.351 1 _ .... - ._.. ....... Fluoranthene ND mg/kg 0.351 1 Pyrene ND mg/kg 0.351 1 Benzo(a)a nth race ne ND mg/kg 0.351 1 Chrysene ND mg/kg 0.351 1 Benzo(b)fluoranthene ND mg/kg 0.351 1 Benzo(k)fluoranthene ND mg/kg 0.351 1 Benzo(a)pyrene ND mg/kg 0.351 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.351 1 Dibenzo(a,h)anthracene ND mg/kg 0.351 1 Benzo(ghi)perylene ND mg/kg 0.351 1 Fage 9 of 52 ' Project Name: WAKEBY ROAD,CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-02 Date Collected: 07/23/07 08:40 Client ID: SP-1-2 Date Received: 07/24/07 Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EctractablePetroleum Mydrocarbort Acceptance Surrogate % Recovery Qualifier Criteria ' Chloro-Octadecane 60 40-140 o-Terphenyl 78 40-140 ' 2-Fluorobiphenyl 81 40-140 2-Bromonaphthalene 78 40-140 !r e z 'Page 10 of 52 vawvi i�.vv ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS ' Lab ID: L0710600-03 Date Collected: 07/23/07 08:55 Client ID: SP-1-3 Date Received: 07/24/07 Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 61,EPH-04-1 Extraction Date: 07/27/07 12:30 Analytical Date: 07/30/07 13:58 Analyst: BN Percent Solids: 96% a ra �- Quality Control Information , "' Ur Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method 7 e, t- P Parameter Result Qualifier Units RDL Dilution Factor Eztractable.Petroleum Hytlrocart�ons�� &.�� - .� �. ��,` ' C9-C18 Aliphatics - ND mg/kg 6.94 1 C19-C36 Aliphatics ND mg/kg 6.94 1 C11-C22 Aromatics ND mg/kg 6.94 1 C11-C22 Aromatics,Adjusted ND mg/kg 6.94 1 Naphthalene ND mg/kg 0 347 1 2-Methyl naphthalene ND mg/kg 0.347 1 Acenaphthylene ND mg/kg 0.347 1 Acenaphthene ND mg/kg 0.347 1 Fluorene ND mg/kg 0.347 1 Phenanthrene ND mg/kg 0.347 1 Anthracene ND mg/kg 0.347 1 Fluoranthene ND mg/kg mg/kg 0.347 1 Pyrene ND mg/kg 0.347 1 Benzo(a)anthracene ND mg/kg 0.347 1 Chrysene ND mg/kg 0.347 1 Benzo(b)fuoranthene ND mg/kg 0.347 1 Benzo(k)fluoranthene ND mg/kg 0.347 1 Benzo(a)pyrene ND mg/kg 0.347 1 _ .- Indeno(1,2,3-cd)Pyrene ND mg/kg 0.347 1 Dibenzo(a,h)anthracene ND mg/kg 0.347 1 Benzo(ghi)perylene ND mg/kg 0.34.7 1 'Page 11 of 52 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-03 Date Collected: 07/23/07 08:55 Client ID: SP-1-3 Date Received: 07/24/07 ' Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Extractable'Petroleum;Hydrocarbons Ale Acceptance Surrogate % Recovery Qualifier Criteria Chloro-Octadecane 58 40-140 o-Terphenyl 78 40-140 2-Fluorobiphenyl 76 40-140 2-Bromonaphthalene 77 40-140 1�t+r :A 'Page 12 of 52 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS ' Lab ID: L0710600-04 Date Collected: 07/23/07 09:18 Client ID: SS-1 Date Received: 07/24/07 ' Sample Location: 810 WAKEBY RCAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 61,EPH-04-1 Extraction Date: 07/27/07 12:30 ' Analytical Date: 07/30/07 12:09 Analyst: BN Percent Solids: 98% Quality;t6iii rdl`n,form,ati;n Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method a ' Parameter Result Qualifier Units RDL Dilution Factor Eictractible Petroleum Hy4r6carbwts ' C9-C18 Aliphatics ND mg/kg 6.80 1 C19-C36 Aliphatics ND mg/kg 6.80 1 C11-C22 Aromatics ND mg/kg 6.80 1 C11-C22 Aromatics Adjusted ND mg/kg 6.80 1 Naphthalene ND mg/kg 0.340 1 2-Methyl naphthalene ND mg/kg 0.340 1 Acenaphthylene ND mg/kg 0.340 1 Acenaphthene ND mg/kg 0.340 1 Fluorene ND mg/kg mg/kg 0.340 1 - _- - Phenanthrene ND mg/kg 0.340 1 Anthracene ND mg/kg 0.340 1 Fluoranthene ND mg/kg 0.340 1 Pyrene ND mg/kg 0.340 1 Benzo(a)anthracene ND mg/kg 0.340 1 Chrysene ND mg/kg 0.340 1 Benzo(b)fuoranthene ND mg/kg 0.340 1 Benzo(k)fluoranthene ND mg/kg 0.340 1 Benzo(a)pyrene ND mg/kg 0.340 1 Indeno(1 2 3-cd)Pyrene ND mg/kg 0.340 1 Dibenzo(a,h)anthracene ND mg/kg 0.340 1 Benzo(ghi)perylene ND mg/kg 0.340 1 _.._. . _....__... ----.._._ _._...... . -_.. .._. ._ _.......... A 'Page 13 of 52 ' Project Name: WAKEBY ROAD,CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-04 Date Collected: 07/23/07 09:18 Client ID: SS-1 Date Received: 07/24/07 ' Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Extractable'Petroleum Hydrocar"6ons Acceptance Surrogate % Recovery Qualifier Criteria Chloro-Octadecane 55 40-140 o-Terphenyl 74 40-140 ' 2-Fluorobiphenyl 83 40-140 2-Bromonaphthalene 84 40-140 li i age 14 of 52 N Project Name: WAKEBY ROAD,CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-05 Date Collected: 07/23/07 09:31 Client ID: SS-2 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 61,EPH-04-1 Extraction Date: 07/27/07 12:30 ' Analytical Date: 07/30/07 12:45 Analyst: BN Percent Solids: 98% Quality Con tro3�1lnformation ' Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method ' Parameter Result Qualifier Units RDL Dilution Factor Eztractabte'Petroleum Hydroearbofi 7M.: ' C9-C18 Aliphatics ND - mg/kg 6.80 1 - _. -_. _..-_ _. - ._. ... .. ... _.._ -_.._ .. ..._ .. ...P... C19-C36 Aliphatics ti-( 3,00�I 17 8 mg/kg 6.80 1 C11-C22 Aromatics ND mg/kg 6.80 1 ' C11-C22 Aromatics,Adjusted ND mg/kg 6.80 1 Naphthalene ND mg/kg 0.340 - 1 ----...._... ..-_ - - - ----._.._. 2-Methylnaphthalene ND mg/kg 0.340 1 Acenaphthylene ND mg/kg 0.340 1 Acenaphthene ND mg/kg 0.340 1 Fluorene ND mg/kg 0.340 1 Phenanth ND mg/kg 0.340 Ant hracenrene ND mg/kg 0.340 .. .. 1 Fluoranthene ND mg/kg 0.340 1 Pyrene ND mg/kg 0.340 1 Benzo(a)anthracene ND mg/kg 0.340 1 _. ... _. - — - _._..... ---- . .... Chrysene ND mg/kg 0.340 1 Benzo(b)fluoranthene ND mg/kg 0.340 1 ----- - --- _._ Benzo(k)fluoranthene ND mg/kg 0.340 1 Benzo(a)pyrene ND mg/kg 0.340 1 Indeno(12,3-cd)Pyrene ND mg/kg 0.340 1 Dibenzo(a,h)anthracene ND mg/kg 0.340 1 Benzo(ghi)perylene ND mg/kg 0.340 1 �7'o< Fage 15 of 52 Project Name: WAKEBY ROAD,CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-05 Date Collected: 07/23/07 09:31 Client ID: SS-2 Date Received: 07/24/07 Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Extractable'PetrioleumkHydrocarbor}rs ° - , Acceptance Surrogate % Recovery Qualifier Criteria ' Chloro-Octadecane 54 40-140 o-Terphenyl 78 40-140 ' 2-Fluorobiphenyl 80 40-140 2-Bromonaphthalene 80 40-140 age 16 of 52 vvr-vv r r c.vv Project Name: WAKEBY ROAD,CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-06 Date Collected: 07/23/07 09:42 Client ID: SS-3 Date Received: 07/24/07 ' Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 61,EPH-04-1 Extraction Date: 07/27/07 12:30 tAnalytical Date: 07/30/07 13:22 Analyst: BN Percent Solids: 98% Quality'Control16rbrmatiort , ' Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method ,x. Parameter Result Qualifier Units RDL Dilution Factor Extractable'Petroleum`Hydrocarbons ' C9-C18 Aliphatics ND mg/kg 6.80 1 C19-C36 Aliphatics ND mg/kg 6.80 1 C11-C22 Aromatics ND mg/kg 6.80 1 C11-C22 Aromatics,Adjusted ND mg/kg 6.80 1 Naphthalene ND mg/kg 0.340 1 2-Methylnaphthalene ND mg/kg 0.340 1 _ _ Acenaphthylene ND mg/kg 0.340 1 Acenaphthene ND mg/kg 0.340 1 Fluorene ND mg/kg 0.340 1 Phenanthrene ND mg/kg 0.340 1 Anthracene ND mg/kg 0.340 1 _ ._.. __ ___. ........ -- Fluoranthene ND mg/kg 0.340 1 Pyrene ND mg/kg 0.340 1 Benzo(a)anthracene ND mg/kg 0.340 1 Chrysene ND mg/kg 0.340 1 Benzo(b)fluoranthene ND mg/kg 0.340 1 Benzo(k)fluoranthene ND mg/kg 0.340 1 Benzo(a)pyrene ND mg/kg 0.340 1 Indeno(1 2 3-cd)Pyrene ND mg/kg 0.340 1 Dibenzo(a,h)anthracene ND mg/kg 0.340 1 Benzo(ghi)perylene ND mg/kg 0.340 1 Page 17 of 52 Project Name: WAKEBY ROAD,CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-06 Date Collected: 07/23/07 09:42 Client ID: SS-3 Date Received: 07/24/07 tSample Location: 810 WAKEBY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor ' Extractable Petraleurn Hyd coca n a Acceptance Surrogate % Recovery Qualifier Criteria Chloro-Octadecane 59 40-140 o-Terphenyl 77 40-140 ' 2-Fluorobiphenyl 80 40-140 2-Bromonaphthalene 81 40-140 I Page 18 of 52 vvwv �.vv Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 ' Method Blank Analysis Batch Quality Control rAnalytical Method: 61,EPH-04-1 Extraction Method: EPA 3546 Analytical Date: 07/30/07 09:44 Extraction Date: 07/27/07 12:30 ' Analyst: BN Parameter Result Qualifier Units RDL ' Extractable Petroleum Hydrocarbons for sample(s): "01=06 Batch: WG289 87-1 C9-Cl8 Aliphatics ND mg/kg 6.67 ' C19 C36 Aliphatics ND mg/kg 6.67 C11-C22 Aromatics ND mg/kg 6.67 C11-C22 Aromatics,Adjusted ND mg/kg 6.67 ' Naphthalene ND mg/kg 0.333 2-Methy Ina pInth ale ne ND mg/kg 0.333 Acenaphthylene ND mg/kg 0.333 Acenaphthene ND mg/kg 0.333 Fluorene ND mg/kg 0.333 Phenanthrene ND mg/kg 0.333 Anthracene ND mg/kg 0.333 Fluoranthene ND mg/kg 0.333 Pyrene ND mg/kg 0.333 Benzo(a)anthracene ND mg/kg 0.333 Chrysene ND mg/kg 0.333 Benzo(b)fluoranthene ND mg/kg 0.333 Benzo(k)fluoranthene ND mg/kg 0.333 Benzo(a)pyrene ND mg/kg 0.333 ' Indeno(1 2 3 cd)Pyrene ND mg/kg 0.333 Dibenzo a,h anthracene ND mg/kg mg/kg 0.333 Benzo(ghi)perylene ND mg/kg 0.333 Acceptance ' Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 59 40-140 ' o-Terphenyl 71 40-140 2-Fluorobiphenyl 73 40-140 2-Bromonaphthalene 73 40-140 Page 19 of 52 I a Man M r M i i r M M M M M M air M 09280712:58 Lab Control Sample Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits Extractable Petraieum Hydrocarbons ssoci ted'sampie{s ; 01�06 _ Bauch: WG28 3 7-2; WG2883 C9-C18 Aliphatics I 40-140 2 25 --- ........... ----------------.... _..._..--------- -- - - _._. _._.__...-.... - - - - - - ---------------.._..__.------.__....... C19-C36 Aliphatics- - -_............-. ___ 75 ---- --- - 9 `7 40-140 8 25 _.. ..._................_..._.... _....__...... . -_ -- _.......... C11 C22 Aromatics $ ®� -- 8 _..._...._._._--._ 40,140 -----------------__ 25 - Naphthalene 75 64 40-140 25 - 2-Meth Ina hthalene74 64ti ; __._......._._......_.......__40-140 _.____..__...........__ �1 ___..._.......__.._........_._..25 .. ._ ---._._... ..._Y._ _P----- ------- -- -- ---------------------------- - -- Acenaphthylene 7"3: 40-140 t4} 25 ........_P_._......- ................__ ........_.. ...........__._..... ........_..... _.._..._.. - - -.... -.........__. -__-_-------------------- -......_......-._...-... ----------------- --- Acena hthene 78 � 9 40-140 10 25 �� -- -- - -- - Fluorene 1 '8 73 a?w 40-140 7;_ 25 --------------------------------___-------.___..._....._._..__._.......--....-----...._..._.. - ....__...__..__... -------- ------- Phenanthrene U 87= �81 40-140 7• 25 -... . -------- ---- - ----- --- --- ----- ------- - - - -- -- ---- ....__._...__..__.....-—---------------- Anthracene 91 40-140 8 f... 25 ------------------ ---._._.... -- - -------------- - _ - _..... ....- - ..._.._... - ---- --- Fluoranthene 91" 40-140 9 25 -....._...........---------------------------------.__-- ......_._.._...._....... - � Pyrene 92 84 40-140 $ 25 ..._...---- - ----- _......._..................__............_ r, ------- .... .........._.........._....._... ----. ._.............. ....__... ...._........ Benzo(a)anthracene r F "` 40-140 9 25 -- ---------- _...... -... -_.._.__- --- -- -- --....... - -..._.. _... _ - ._.._......._....__......._.._........_....... ...._ Chrysene -_`, 40140 9 ---._..-._...._........._......_..._25 -- ----------------------_.. Benzo(b)fluoranthene 94 -84 40-140 11 25 -- _......--......._..._.... ----- ------ ._..............------------------- ---- - ._....._...- - -._.-._......_..._... - ---- ...._.._.. ........_.. - --- -... --- -------.... -- - - Benzo(k)fluoranthene 9i7 82 40-140 25 - ----------- ------ -- -- -- -- ---._..__.._.._....._..__._.....---------- -------------------- ._-.... -------------- ....... -- - Benzo(a)pyrene St3 �78 3; 40-1 40 10 ,, 25 Indeno(1,2,3-cd)Pyrene 83 74r 40-140 i1 25 s-4Qd•,r ._Dibenzo(a,h)anthracene ....._....................._.-_....--__- -...----- $s} --_....--_._....._...............� T'' _-........_.._.................40-140__---- - -..._..._....._............._ 0 _._._.-..........__......---_.. 25...- ------......._..........._.... ,, 1- - -----------------------....._.........-_._.............._......- - ----------- --------- ---- -- ._........_....__... _- --- _. _Benzo(ghi)perylene $8 " 80 p�_, 40-140 14 ; - -25- ----- _. -- -----.....__._.... -- ...........- - ---- ..._.. -------------.........._........ Nonane(C9) 1 "$ I 30-140 4 25 Page 20 of 52 ,ram ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! ! 09280712:58 Lab Control Sample Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits Extractable Petroleum Hydrocarbons,,Associated same e(s): U8=06 Batch: �WG28838Z2 WG288987-3 m.. .. Decane(C10) 64 �"�'66-"� 40-140 3 25 - - -- - ......._.._..-..._.__....._... - --- ....... _........._..... ..... - _...- ....._. Dodecane(C12) � 70 %y, 40-140 fr 1 25 ------.._.........._.....- ----------- --- ................_._... -._.........._._..---------- Tetradecane(C14) 7270 40 140 3 25 ..- --------------......--- ..__.......... _- --_.. --- __.......... - L _ - ...._.. - --.._..... - ..._...-._._.. -- - _....._........._.... -... Hexadecane(C16)-....._....._.....--------._._..........__... -------------_ '.� , 72 a'�; - .... --- 68 __.._...- 40-140.._...._ - - 6 , -25 - Ar, t+ t Octadecane(C18) 7 40-140 T= 25 --------- -.. ....._..._.. Nonadecane(C19) 4 ! - ------------- ._.. ~�-- ......- -- 40_140.... -- - --------- ...._.._..... --25- - - - Eicosane(C20) 76 88® `� 40 140 113. 25 Docosane(C22) 76 40-140 11 25 _.--....-------- _._..... -...__...._._....--p ...._.......__..- ---- - - - ._.._....._ ... _ _---1. TeVacosane(C24) _.._...---- 74 -.._._.._.._-----... 1 6 -- - - -- —40 140 - - - ._.._.... - - - ....- -----..... 25 - - — - Hexacosane(C26) 75.` "�0�� 40-140 7 , 25 --------- _ .;,,r. Octacosane(C28) 75~ 70: 40-140 7 25 - --------........_..._....._._.__...._..----.-.- - -.._.._._.__.._..........__..._.._......_.._.. _ -- - .� -------- - _-..._... ...---- - — ---....__._..__ _ --- ----------------------------- --... Triacontane(C30) 75 1 40-140 7 25 .--------------....._..-- - - - --------- -----_------------------------------- _._.__..------------ - ------._...._.. _--- - -...._....._..-- -- _ ...-- - ----...._..........------------ Hexatriacontane(C36) 76 s 70'r`� 40-140 5 s 8 25 - --- -- ........--- --...._...................... ......_..._.._....--- '.� -...._.-.... _..__._.........._ - .- _. ---------------------......_... LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Chloro-Octadecane 67 58 40-140 o-Terphenyl 91 83 40-140 2-Fluorobiphenyl 78 70 40-140 2-Bromonaphthalene 80 73 40-140 •Naphthalene Breakthrough 0 0 •2-Methylnaphthalene Breakthrough 0 0 Page 21 of 52 vvwv �.vv ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 Fractionation Check Standard Quality Control Fractionation check standard;fo F1SH061149b:„ "u 3 74 Parameter % Recovery QC Criteria ' C9-C18 Aliphatics 60 40-140 C19-C36 Aliphatics 72 40-140 - — - -------- - - - C11-C22 Aromatics 83 40-140 - - ----- Na phthalene 77 40 140 2-Methylnaphthalene 72 40-140 Acenaphthylene 72 40 140 Acenaphthene 74 40-140 Fluorene 74 40-140 Phenanthrene 77 40-140 Anthracene 72 40-140 Fluoranthene 82 40-140 Pyrene 82 40-140 Benzo(a)anthracene 82 40-140 Chrysene 82 40-140 Benzo(b)fluoranthene 81 40-140 Benzo(k)fluoranthene 84 40-140 ' Benzo(a)pyrene 76 40 140 Indeno(1,2,3 cd)Pyrene 76 40-140 Dibenzo(a,h)anthracene 80 40-140 .._... Benzo(g h i)perylene 80 40-140 Nonane 54 30-140 ' Decane 58 40 140 Dodecane 62 40-140 Tetradecane 62 40-140 Hexadecane 63 40-140 - -....._ - Octadecane 64 40-140 Nonadecane 64 40-140 Eicosane 66 40-140 Docosane 70 40-140 Tetracosane 73 40-140 Hexacosane 76 40-140 Octacosane 77 40-140 Triacontane 78 40-140 Hexatriacontane 82 40-140 }r Cage 22 of 52 V VLVVI IL.VV ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 Fractionation Check Standard Quality Control FracCionation,check standard for flSH061�149 r Surrogate % Recovery QC Criteria Chloro-Octadecane 52 40-140 ' o-Terphenyl 77 40-140 2-Fluorobiphenyl 76 40-140 2-Bromonaphthalene 76 40-140 fr tDff_i7dF+dFr..�ai Page 23 of 52 I 1 1 PCBS 1 1 1 1 1 1 ALPE;a (Page 24 of 52 ..Op. .. ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-01 RE Date Collected: 07/23/07 08:20 ' Client ID: SP-1-1 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 ' Anaytical Method: 64,8082 Extraction Date: 07/30/07 18:00 Analytical Date: 07/31/07 10:51 Cleanup Methodl: EPA 3665A Analyst: JB Cleanup Datel: 07/31/07 ' Percent Solids: 96% Parameter Result Qualifier Units RDL Dilution Factor Polychlorinated Biphenyls by MCP,8082 ' Aroclor 1016 ND ug/kg 34.7 1 Aroclor 1221 ND ug/kg 34.7 1 A roc lor 1232 ND ug/kg 34.7 1 Aroclor 1242 ND ug/kg 34.7 1 - -----.... - Aroclor 1248 ND ug/kg 34.7 1 Aroclor 1254 ND ug/kg 34.7 1 Aroclor 1260 ND ug/kg 34.7 1 Aroclor 1262 ND ug/kg 34.7 1 Aroclor 1268 ND ug/kg 34.7 1 ' Acceptance Surrogate % Recovery Qualifier Criteria Column 2,45,6-Tetrachloro-m-xylene 83 30-150 A Decachlorobiphenyl 78 30-150 A 2,45,6-Tetrachloro-m-xylene 76 30-150 B Decachlorobiphenyl 66 30-150 B 'Page 25 of 52 vvwv �.vv ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 ' SAMPLE RESULTS Lab ID: L0710600-02 RE Date Collected: 07/23/07 08:40 ' Client ID: SP-1-2 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 64,8082 Extraction Date: 07/30/07 18:00 Analytical Date: 07/31/07 11:20 Cleanup Methodl: EPA 3665A Analyst: JB Cleanup Datel: 07/31/07 ' Percent Solids: 95% Parameter Result Qualifier Units RDL Dilution Factor ,Pol7rhlor'inatediBipheny1s by MCP,8OE2 5W, ' Aroclor 1016 ND ug/kg 35.1 1 Aroclor 1221 ND ug/kg 35.1 1 ' Aroclor 1232 ND ug/kg 35.1 1 Aroclor 1242 ND ug/kg 35.1 1 Aroclor 1248 ND ug/kg 35.1 1 Aroclor 1254 ND ug/kg 35.1 1 Aroclor 1260 ND ug/kg 35.1 1 Aroclor 1262 ND ug/kg 35.1 1 Aroclor 1268 ND ug/kg 35.1 1 ' Acceptance Surrogate % Recovery Qualifier Criteria Column 2,45,6-Tetrachloro-m-xylene 76 30-150 A ' Decachlorobiphenyl 79 30-150 A 2,4,5,6-Tetrachloro-m-xylene 70 30-150 B Decachlorobiphenyl 69 30-150 B XV Page 26 of 52 I Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-03 IRE Date Collected: 07/23/07 08:55 Client ID: SP-1-3 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 64,8082 Extraction Date: 07/30/07 18:00 Analytical Date: 07/31/07 11:48 Cleanup Methodl: EPA 3665A Analyst: JB Cleanup Datel: 07/31/07 ' Percent Solids: 96% ' Parameter Result Qualifier Units RDL Dilution Factor �Polyehlorinated Biphenyis by MCP 8082 p g ' Aroclor 1016 ND ug/kg 34.7 1 Aroclor 1221 ND ug/kg 34.7 1 Aroclor 1232 ND ug/kg 34.7 1 Aroclor 1242 ND ug/kg 34.7 1 Aroclor 1248 ND ug/kg 34.7 1 Aroclor 1254 ND ug/kg 34.7 1 Aroclor 1260 ND ug/kg 34.7 1 Aroclor 1262 ND ug/kg 34.7 1 Aroclor 1268 ND ug/kg 34.7 1 Acceptance Surrogate % Recovery Qualifier Criteria Column 2,4,5,6-Tetrachloro-m-xylene 75 30-150 A Decachlorobiphenyl 72 30-150 A 2,45,6-Tetrachloro-m-xylene 69 30-150 B Decachlorobiphenyl 62 30-150 B 'Page 27 of 52 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 ' SAMPLE RESULTS Lab ID: L0710600-04 RE Date Collected: 07/23/07 09:18 Client ID: SS-1 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 64,8082 Extraction Date: 07/30/07 18:00 Analytical Date: 07/31/07 12:17 Cleanup Method 1: EPA 3665A 1 Analyst: JB Cleanup Date1: 07/31/07 Percent Solids: 98% ' Parameter Result Qualifier Units RDL Dilution Factor Polychlorinated Biphenyls_ by MCP 8082 „" Aroclor 1016 ND ug/kg 34.0 1 Aroclor 1221 ND ug/kg 34.0 1 Aroclor 1232 ND ug/kg 34.0 1 Aroclor 1242 ND ug/kg 34.0 1 Aroclor 1248 ND ug/kg 34.0 1 - - - - -. . Aroclor 1254 ND ug/kg 34.0 1 Aroclor 1260 ND ug/kg 34.0 1 Aroclor 1262 ND ug/kg 34.0 1 Aroclor 1268 ND ug/kg 34.0 1 ' Acceptance Surrogate % Recovery Qualifier Criteria Column 2,4,5,6-Tetrachloro-m-xylene 67 30-150 A ' Decachlorobiphenyl 68 30-150 A 2,45,6-Tetrachloro-m-xylene 61 30-150 B Decachlorobiphenyl 60 30-150 B I 1 xga�� Page 28 of 52 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 tSAMPLE RESULTS Lab ID: L0710600-05 RE Date Collected: 07/23/07 09:31 Client ID: SS-2 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 ' Anaytical Method: 64,8082 Extraction Date: 07/30/07 18:00 Analytical Date: 07/31/07 12:45 Cleanup Method1: EPA 3665A Analyst: JB Cleanup Date1: 07/31/07 Percent Solids: 98% Parameter Result Qualifier Units RDL Dilution Factor PolyehtorinatQ@J0h4 n—? dry M F�8'Cla Aroclor 1016 ND ug/kg 34.0 1 Aroclor 1221 ND ug/kg 34.0 1 ' Aroclor 1232 ND ug/kg 34.0 1 Aroclor 1242 ND ug/kg 34.0 1 Aroclor 1248 ND ug/kg 34.0 1 Aroclor 1254 ND ug/kg 34.0 1 Aroclor 1260 ND ug/kg 34.0 1 ' Aroclor 1262 ND ug/kg 34.0 1 Aroclor 1268 ND ug/kg 34.0 1 Acceptance Surrogate %Recovery Qualifier Criteria Column 2,4,5,6-Tetrachloro-m-Wene 75 30-150 A 1 Decachlorobiphenyl 77 30-150 A 2,4,5,6-Tetrachloro-m-xylene 69 30-150 B Decachlorobiphenyl 67 30-150 B i i Page 29 of 52 Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-06 iRE Date Collected: 07/23/07 09:42 Client ID: SS-3 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 64,8082 Extraction Date: 07/30/07 18:00 Analytical Date: 07/31/07 13:14 Cleanup Method1: EPA 3665A Analyst: JB Cleanup Date1: 07/31/07 Percent Solids: 98% Parameter Result Qualifier Units RDL Dilution Factor 6lyeht3rinated,,Biphenj4_ MGP 8032 7 ' "` 'IFAW Aa ' Aroclor 1016 ND ug/kg 34.0 1 Aroclor 1221 ND ug/kg 34.0 1 Aroclor 1232 ND ug/kg 34.0 1 Aroclor 1242 ND ug/kg 34.0 1 Aroclor 1248 ND ug/kg 34.0 1 Aroclor 1254 ND ug/kg 34.0 1 Aroclor 1260 ND ug/kg 34.0 1 ' Aroclor 1262 ND uglkg 34.0 1__. Aroclor 1268 ND ug/kg 34.0 1 Acceptance Surrogate % Recovery Qualifier Criteria Column 2,45,6-Tetrachloro-m-xylene 70 30-150 A Decachlorobiphenyl 78 30-150 A 2,45,6-Tetrachloro-m-xylene 64 30-150 B Decachlorobiphenyl 67 30-150 B 1 ,Page 30 of 52 Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 Method Blank Analysis Batch Quality Control rAnalytical Method: 64,8082 Extraction Method: EPA 3546 Analytical Date: 07/31/07 C9:25 Extraction Date: 07/30/07 18:00 Analyst: JB Cleanup Method1: EPA 3665A Cleanup Date1: 07/31/07 Parameter Result Qualifier Units RDL ' f,glychlorinated:Biphenyyls E�y MCP 8082�for camp e(s}: 01 206 Batck>; WG B883 1. Aroclor 1016 ND ug/kg 33.3 ' Aroclor 1221 ND ug/kg 33.3 Aroclor 1232 ND ug/kg 33.3 Aroclor 1242 ND ug/kg 33.3 Aroclor 1248 ND ug/kg 33.3 Aroclor 1254 ND ug/kg 33.3 Aroclor 1260 ND ug/kg 33.3 Aroclor 1262 ND ug/kg 33.3 Aroclor 1268 ND ug/kg 33.3 Acceptance Surrogate %Recovery Qualifier Criteria Column 2,45,6-Tetrachloro-m-xylene 74 30-150 A Decachlorobiphenyl 75 30-150 A 2,45,6-Tetrachloro-m-xylene 67 30-150 B Decachlorobiphenyl 66 30-150 B Page 31 of 52 a■� �■s a i a■� ,, ,�■� >• M M M M rye MI M 09280712:58 Lab Control Sample Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits Poiychlorihated BipheFy-Is by MC 8 2 Associated sample(s)701-0 ,Batch: G288 39-2 W02-98839=3 -Aroclor 1016 ---------------------------------------I ----------.-.....- - }'P '8': ? ...............-......_40 140_...-----------......... 6 -.-..._........... _....-30----- -..._--- .............. Aroclor 1260 �88�°"�" t�' 90 ." 40-140 30 LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Column 2,45,6-Tetrachloro-m-xylene 75 77 30-150 A Decachlorobiphenyl 81 81 30-150 A 2,45,6-Tetrachloro-m-xylene 70 72 30-150 B Decachlorobiphenyl 71 71 30-150 B Page 32 of 52 METALS 1 1 Page 33 of 52 Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-01 Date Collected: 07/23/07 08:20 Client ID: SP-1-1 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 96% Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst Total�Metais by MCP 6000/7000 seiies Arsenic,Total 2.0 mg/k,g 0.41 1 07/27/07 13:50 07/30/07 12:52 tEPA 3050B 60,6010B MG Barium,Total 7.5 mg/kg 0.41 1 07/27/07 13:50 07/30/07 12:52 EPA 3050B 60,6010E MG Cadmium,Total ND mg/kg 0.41 1 07/27/07 13:50 07/30/07 12:52 EPA 3050B 60,6010E MG Chromium,Total 4.1 mg/kg 0.41 1 07/27/07 13:50 07/30/07 12:52 EPA 3050E 60,6010B MG Lead,Total 7.0 mg/kg 2.1 1 07/27/07 13:50 07/30/07 12:52 EPA 3050E 60,6010B MG Mercury,Total ND mg/kg 0.09 1 07/26/07 19:30 07/27/07 14:48 EPA 7471A 64,7471A RC Selenium,Total ND mg/kg 2.1 1 07/27/07 13:50 07/30/07 12:52 EPA 3050E 60,6010B MG Silver,Total ND mg/kg 0.41 1 07/27/07 13:50 07/30/07 12:52 EPA 3050E 60,6010B MG 'Page 34 of 52 vvwvr i�.vv Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-02 Date Collected: 07/23/07 08:40 Client ID: SP-1-2 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 95% Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst TotafWtalsby4MCP 6000/7000 serie< 3� - r Arsenic,Total 1.7 mg/kg mg/kg 0.42 1 07/27/07 13:50 07/30/07 12:55 EPA 3050B 60,60106 MG Barium,Total 8.5 mg/kg 0.42 1 07/27/07 13:50 07/30/07 12:55 EPA 3050B 60,6010E MG Cadmium,Total ND mg/kg 0.42 1 07/27/07 13:50 07/30/07 12:55 EPA 3050E 60,60106 MG Chromium,Total 5.3 mg/kg 0.42 1 07/27/07 13:50 07/30/07 12:55 EPA 3050E 60,6010E MG ' Lead,Total 3.6 mg/kg 2.1 1 07/27/07 13:50 07/30/07 12:55 EPA 3050E 60,60106 MG Mercury,Total ND mg/kg 0.08 1 07/26/07 19 30 07/27/07 14:50 EPA 7471A 64,7471A RC Selenium,Total ND mg/kg 2.1 1 07/27/07 13:50 07/30/07 12:55 EPA 3050B 60,6010B MG ' Silver,Total ND mg/kg 0.42 1 07/27/07 13:50 07/30/07 12:55 EPA 3050B 60,6010E MG t 1 I AKA ,Page 35 of 52 vv�vv i�.vv Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-03 Date Collected: 07/23/07 08:55 Client ID: SP-1-3 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 96% Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst Total Metals by MCP 6000/7000 series AL ' Arsenic,Total 2.1 mg/kg 0.41 1 07/27/07 13:50 07/30/07 12:57 EPA 3050E 60,60106 MG Barium,Total 6.3 mg/kg 0.41 1 07/27/07 13:50 07/30/07 12:57 EPA 3050B 60,60106 MG Cadmium,Total ND mg/kg 0.41 1 07/27/07 13:50 07/30/07 12:57 EPA 3050E 60,601013 MG Chromium,Total 4.5 mg/kg 0.41 1 07/27/07 13:50 07/30/07 12:57 EPA 3050E 60,601013 MG Lead,Total 4 1 mg/kg 2.1 1 07/27/07 13:50 07/30/07 12:57 EPA 3050B 60,601013 MG Mercury,Total ND mg/kg 0.08 1 07/26/07 19 30 07/27/07 14:51 EPA 7471A 64,7471A RC Selenium,Total ND mg/kg 2.1 1 07/27/07 13:50 07/30/07 12:57 EPA 3050B 60,6010E MG Silver,Total ND mg/kg 0.41 1 07/27/07 13:50 07/30/07 12:57 EPA 3050B 60 60106 MG i Lage 36 of 52 vvwv i�.vv Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-04 Date Collected: 07/23/07 09:18 Client ID: SS-1 Date Received: 07/24/07 ' Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 98% ' Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst Total M&41s by;MCP 6 000/7000'series Arsenic,Total 0.91 mg/kg 0.40 1 07/27/07 13:50 07/30/07,12:59 EPA 3050B 60,6010B MG Barium,Total 2.4 mg/kg 0.40 1 07/27/07 13:50 07/30/07 12:59 EPA 3050E 60,6010B MG Cadmium,Total ND mg/kg 0.40 1 07/27/07 13:50 07/30/07 12:59 EPA 3050E 60,6010E MG Chromium,Total 1.8 mg/kg 0.40 1 07/27/07 13:50 07/30/07 12:59 EPA 3050B 60,6010E MG Lead,Total ND mg/kg 2.0 1 07/27/07 13:50 07/30/07 12:59 EPA 3050E 60,60108 MG Mercury,Total ND mg/kg 0.08 1 07/26/07 19 30 07/27/07 14:53 EPA 7471A 64 7471A RC Selenium,Total ND mg/kg 2.0 1 07/27/07 13:50 07/30/07 12:59 EPA 3050B 60,6010E MG Silver,Total ND mg/kg 0.40 1 07/27/07 13:50 07/30/07 12:59 EPA 3050B 60,6010B MG ZI . A 'Page 37 of 52 vvwv �.vv Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-05 Date Collected: 07/23/07 00:31 Client ID: SS-2 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 98% Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst Tot llMetals y MCP 6000/7,000 series Arsenic,Total 0.93 mg/kg 0.41 1 07/27/07 13:50 07/30/07 13:02 EPA 30506 60,6010B MG Barium,Total 3.4 mg/kg 0.41 1 07/27/07 13:50 07/30/07 13:02 EPA 3050E 60,6010E MG Cadmium,Total ND mg/kg 0.41 1 07/27/07 13:50 07/30/07 13:02 EPA 3050E 60,6010E MG Chromium,Total 1.7 mg/kg 0.41 1 07/27/07 13:50 07/30/07 13:02 EPA 3050B 60,6010E MG Lead,Total 5.3 mg/kg 2.0 1 07/27/07 13:50 07/30/07 13:02 EPA 3050B 60,6010E MG Mercury,Total ND mg/kg 0.08 1 07/26/07 19:30 07/27/07 14:55 EPA 7471A 64,7471A RC Selenium,Total ND mg/kg 2.0 1 07/27/07 13:50 07/30/07 13:02 EPA 3050E 60,6010E MG Silver,Total ND mg/kg 0.41 1 07/27/07 13:50 07/30/07 13:02 EPA 3050B 60,6010E MG _... - -. _ ....... i � r Page 38 of 52 Project Name: WAKEBY ROAD,CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 1 Lab ID: L0710600-06 SAMPLE RESULTS Date Collected: 07/23/07 09:42 Client ID: SS-3 Date Received: 07/24/07 ' Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 98% Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst Total Mktalo by,MCP 6000/7000 series _ Arsenic,Total 1.1 mg/kg 0.40 1 07/27/07 13:50 07/30/07 13:04 EPA 3050E 60,6010E MG Barium,Total 2.3 mg/kg mg/kg 0.40 1 07/27/07 13:50 07/30/07 13:04 EPA 3050E 60,6010E MG ' Cadmium,Total ND mg/kg 0.40 1 07/27/07 13:50 07/30/07 13:04 EPA 3050B 60,6010E MG Chromium,Total 1.6 mg/kg 11 0.40 1 07/27/07 13:50 07/30/07 13:04 EPA 3050B 60,6010E MG Lead,Total ND mg/kg 2.0 1 07/27/07 13:50 07/30/07 13:04 EPA 3050B 60,6010B MG Mercury,Total ND mg/kg 0.08 1 07/26/07 19:30 07/27/07 14:57 EPA 7471A 64,7471A RC Selenium,Total ND mg/kg 2.0 1 07/27/07 13:50 07/30/07 13:04 EPA 3050E 60,6010E MG __. . .Silver, - Total ND mg/kg 0.40 1 07/27/07 13:50 07/30/07 13:04 EPA 3050E 60,6010B MG 1 t Cage 39 of 52 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 ■ Method Blank Analysis ■ Batch Quality Control Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst tal Metals by MZ P�6000/7000 series for sample(s): "01=06 `Batch: l o WG2$8484-1 V. Mercury,Total ND mg/kg 0.08 1 07/26/07 19:30 07/27/07 14:09 64,7471A RC ' Prep Information Digestion Method: EPA 7471 A Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Lotal Metals by MCP 6000/7000 series for samp e(s): 01 6 atch: WG. `8615-1 Arsenic,Total ND mg/kg 0.40 1 07/27/07 13:50 07/30/07 12:31 60,601013 MG Barium,Total ND mg/kg mg/kg 0.40 1 07/27/07 13:50 07/30/07 12:31 60,601013 MG ' Cadmium,Total ND ND - mg/kg 0.40 — 1 -- 07/27/07 13:50 07/30/07 12:31 60,601013 MG Chromium,Total mg/kg 0.40 1 07/27/0713:50 07/30/0712:31 60,60106 MG ' Lead,Total ND mg/kg 2.0 1 07/27/07 13:50 07/30/07 12:31 60,601013 MG Selenium,Total ND mg/kg 2.0 1 07/27/07 13:50 07/30/07 12:31 60,60106 MG Silver,Total ND mg/kg 0.40 1 07/27/07 13:50 07/30/07 12:31 60,60106 MG Prep Information Digestion Method: EPA 3050E II 'Page 40 of 52 09280712:58 Lab Control Sample Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: 1-0710600 Project Number: SE01-615-1 Report Date: 09/28/07 0 LCS LCSD /oRecove ry Parameter %Recovery %Recovery Limits RPD RPD Limits ata Metals Icy 70 s Ins s o'►ate. s ' �e(st 0 , s�lta : UG288- 4- W :2 5 Mercury,Total 75-125 30 otal eteis Arsenic,Total------------ -------___._.__-_.._.__._.._.__...-._...----._....._-....__._._ 75-125 9, .e 30 Banum,Total 5 75-125 1 30 - ---- _..._... _ - ..._......__.._. _....__.... Cadmium,Total ? _ 75-125 i 1; 30 ------------- -------- ._...._- .... ---------------- u ---- --- - - - Chromium,Total $, $„ 75-125a 30 ---_ .-- ---- ------ _. ..... ----------------------._._...... ............. . -- - _.. Lead,Total > 75-125 30 __..---'-'--- maxi._., Selenium,Total pl 75-125r 30 __. ._._ ... - ............ ....... _.... ._....._.__.... - - --- -- _._..__. _............. - 11111M Silver,Total _ .. - . 75-125....................... 30 Page 41 of 52 sinu t � IN O RGA NICS 1 & � MISCELLANEOUS 1 1 i 1 i 1 i 1 1 Lage 42 of 52 vvwv, ir-.vv ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-01 Date Collected: 07/23/07 08:20 ' Client ID: SP-1-1 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst General"Chernistry Solids,Total 96 % 0.10 1 07/25/07 14:55 30,2540G NM I ALP14A Page 43 of 52 Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-02 Date Collected: 07/23/07 08:40 ' Client ID: SP-1-2 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst `General Chemistry;-,. n Solids,Total 95 % 0.10 1 - 07/25/07 14:55 30,2540G NM 'Page 44 of 52 vvc.vv. .�.vv Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-03 Date Collected: 07/23/07 08:55 Client ID: SP-1-3 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst G'erneralChemistry Solids,Total 96 % 0.10 1 07/25/07 14:55 30,2540G NM I I III `ALP14A Page 45 of 52 Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-04 Date Collected: 07/23/07 09:18 1 Client ID: SS-1 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil 1 Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst 1 GenealChemistry h . ; p Solids,Total 98 % 0.10 1 07/25/07 14:55 30,2540G NM 1 1 1 1 1 1 1 1 1 ALPHA� Page 46 of 52 vvcw i i-.vv ' Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-05 Date Collected: 07/23/07 09:31 Client ID: SS-2 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst 'GeneraiCherrrtstry I - zamm27•. �. Solids,Total 98 % 0.10 1 07/25/07 14:55 30,2540G NM r Page 47 of 52 Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 SAMPLE RESULTS Lab ID: L0710600-06 Date Collected: 07/23/07 09:42 Client ID: SS-3 Date Received: 07/24/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst General Chemistry - Solids,Total 98 % 0.10 1 07/25/07 14:55 30,2540G NM ' AL;4,A Page 48 of 52 Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 Sample Receipt and Container Information Were project specific reporting limits specified? YES Cooler Information Cooler Custody Seal A Absent E Container Information Container ID Container Type Cooler pH Temp Pres Seal Analysis L0710600-01A Amber250m1 unpreserved A N/A 2.9C Y Absent EPH-DELUX-04,MCP-8082-04 L0710600-016 Amber 250ml unpreserved A N/A 2.9C Y Absent MCP-7471T,MCP-AG- 6010T,M CP-AS-6010T,MCP-BA- 6010 T,MCP-C D-6010T,M C P-C R- 6010T,MCP-PB-6010T,M CP-SE- 6010T,TS L0710600-02A Amber 250ml unpreserved A N/A 2.9C Y Absent EPH-DELUX-04,MCP-8082-04 L0710600-02B Amber 250ml unpreserved A N/A 2.9C Y Absent MCP-7471T,MCP-AG- ' 6010T,MCP-AS-6010T,MCP-BA- 6010T,MCP-CD-6010T,MCP-C R- 6010T,MCP-PB-6010T,MCP-SE- 6010T,TS L0710600-03A Amber 250ml unpreservec A N/A 2.9C Y Absent EPH-DELUX-04,MCP-8082-04 L0710600-03B Amber 250ml unpreserved A N/A 2.9C Y Absent MCP-7471T,MCP-AG- 6010 T,M C P-AS-6010T,MCP-BA- 6010 T,M C P-C D-6010T,MCP-C R- ' 6010T,MCP-PB-6010T,MCP-SE- 6010T,TS L0710600-04A Amber 250ml unpreserved A N/A 2.9C Y Absent EPH-DELUX-04,MCP-8082-04 L0710600-04B Amber 250ml unpreserved A N/A 2.9C Y Absent MCP-7471T,MCP-AG- ' 6010T,MCP-AS-6010T,MCP-BA- 6010T,MCP-CD-6010T,MCP-C R- 6010T,MCP-PB-6010T,MCP-SE- 6010T,TS ' L0710600-05A Amber 250ml unpreserved A N/A 2.9C Y Absent EPH-DELUX-04,MCP-8082-04 L0710600-05B Amber 250ml unpreserved A N/A 2.9C Y Absent MCP-7471T,MCP-AG- 6010T,MCP-AS-6010T,MCP-BA- 6010T,M CP-C D-6010T,M C P-C R- ' 6010T,MCP-PB-6010T,MCP-SE- 6010T,TS L0710600-06A Amber 250ml unpreserved A NIA 2.9C Y Absent EPH-DELUX-04,MCP-8082-04 L0710600-06B Amber 250ml unpreserved A N/A 2.9C Y Absent MCP-7471T,MCP-AG- 6010T,MCP-AS-6010T,MCP-BA- 6010T,MCP-CD-6010T,MCP-CR- 6010T,MCP-PB-6010T,MCP-SE- 6010T,TS II T-, I Page 49 of 52 i Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 GLOSSARY Acronyms EPA - Environmental Protection Agency. LCS - Laboratory Control Sar-tple: A sample matrix,free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. LCSD- Laboratory Control Sample Duplicate: Refer to LCS. MS - Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sampie for which an independent estimate of target analyte concentration is available. MSD - Matrix Spike Sample Duplicate: Refer to MS. NA - Not Applicable. NI - Not Ignitable. NC - Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. ND Not detected at the reported detection limit for the sample. RDL - Reported Detection Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. RPD - Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as ' relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. I Terms Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260E is shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum. 1 Data Qualifiers The following data qualifiers have been identified for use under the CT DEP Reasonable Confidence Protocols. tA- Spectra identified as "Aldo) Condensation Product". B -The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte. E- Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. J- Estimated value. The analyte was tentatively identified; the quantitation is an estimation. (Tentatively identified compounds only.) Standard Qualifiers H -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. Report Format: Data Usability Report d�L?i;A Page 50 of 52 Project Name: WAKEBY ROAD, CAD Lab Number: L0710600 Project Number: SE01-615-1 Report Date: 09/28/07 REFERENCES 30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-WPCF. 18th Edition. 1992. 60 Quality Assurance and Quality Control Requirements and Performance Standards for SW- 846 Methods. MADEP BWSC. WSC-CAM-IIA(Revision 4),WSC-CAM-V C (Revision 2), WSC-CAM-IIIA(Revision 5). May 2004. 61 Method for the Determination of Extractable Petroleum Hydrocarbons(EPH). Massachusetts Department of Environmental Protection, DEA/ORS/BWSC. May 2004, Revision 1.1. 64 Quality Assurance and Quality Control Requirements and Performance Standards for SW- M 846 Methods. MADEP BWSC.WSC-CAM-IIA(Revision 4),WSC-CAM-V C (Revision 2), WSC-CAM-IIIA(Revision 5).August 2004. r i 1 1 LIMITATION OF LIABILITIES Alpha Woods Hole Labs performs'services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Woods Hole Labs shall be to re-perform the work at it's own expense. In no event shall Alpha Woods Hole Labs be held liable for any incidental, consequential o;special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Woods Hole Labs. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. AU44A Lage 51 of 52 G� CHAIN Off' CUSTODY PAGE OF � r r r KA bate Rec d In Lab ALPHA Job d LASS WESTBORO,MA RAYNHAM,MA Project • • �'. • •n-Data Deliverables, Billing Inf• ... i • TEL:SOM98-9220 TEL:508-822-9300 FAX;508 898-9193 FAX:508-822-3288 Project Name: WAV—e6Y ?,OAb Ly4J ElFAX D EMAIL ❑.Sams as Client info InformationClient Project Location: SIO W,A �3Y �Od`� I DEX ❑Add'I Deliverables Wb14e3Y . 'ROAD rt Limits Client: St'T-i;(� GNViaflI•!) 6/4 LMC. Regulatory • • P74L Project#: Address: +Fr State/Fed Program Criteria �'� UM r,T C� Project Manager: RAY (�i�t-1 t.( MR MC%}� c5-1 MA42St-1 ifie-t> ALPHA Quote M. MA MCP PRESUMPTIVE CERTAINTY • •NFIDENCE PROTOCO LS Phone: aitt Of 0Q ❑Yes ❑No Are MCP Analytical Methods Required? Fax: , 4 $9 1. ❑Yes ❑No Are CT RCP(Reasonable Confidence Protocols)Required? T— Filtrationndard ❑ RUSH(oniycor&maCUpre-approveen Email: {�SCrIySLrirC.- Due: f Time:❑ These samples have been previously analyzed by Alph3AMPLEHANDLING Other Project Specific Requirements/Comments/Detection Limits: ❑Done Q Not needed A (k; Q Lab to do Preservation yr ti.1 CI Lab to do "ALPHA L I�tIfS� t Collection Sample Sampler's !r Pless••pedry below) (Labs JJsO )jrr Sample ID Date Time Matrix Initials Do Sample Specific Comments A*' 0 8.q o� S m SS` 23 0� `I't S S r+1 ✓ ✓ 2 n {r1'} t'lR1J . lti,C,:i:Y(�v PLEASE ANSWER QUESTIONS ABOVE! Container? Es YPa v rs�pleass��rlat dariy legrf�i4. yrand IS YOUR PROJECT Preservative J�' A I omplQtey ; amp!es can not'ti� oggetl rn ajtf{iirna ou�d time clock Relinquished By: Dateffime Received By: Date/Time r °ril not start until an}r`tairtblguitlas are MA MCP or CT RCP? �1l E �s57� a�l.�l T� 'r� i (,E !i/1 ,� resviVxed All SemplQs sttk!ta(itecf are. subiect to Alphas nPay ientTe4ins LO RMNO:01-01(rev.10-OCT-05) ` ` } 5pe:reverse side` 'r 1 HA WOODS H B LABS 1 ANALYTICAL REPORT Lab Number: L0717845 Client: Sitec Environmental, Inc. 769 Plain Street Unit C Marshfield, MA 02050 ATTN: Geoff Souza Project Name: WAKEBY ROAD, CAD Project Number: SE01-615-1 Report Date: 12/07/07 r Certifications&Approvals: MA(M-MA086),N"NELAC(11148),CT(PH-0574),NH(200305),NJ(MA935),RI(LA000065),ME(2006012), PA(Registration#68-03671),USDA(Permit#S-72578),US Army Corps of Engineers,Naval FESC. Eight Walkup Drive, Westborough, MA 01581-1019 508-898-9220 (Fax) 508-898-9193 800-624-9220 -www.alphalab.com Page 1 of 44 �� ® 1 Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 Alpha Sample ID Client ID Sample Location L0717845-01 SS-4 810 WAKEBY ROAD L0717845-02 SS-5 810 WAKEBY ROAD L0717845-03 SS-6 810 WAKEBY ROAD L0717845-04 SS-7 810 WAKEBY ROAD i Page 2 of 44 -1 v. -- Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 MADEP MCP Response Action Analytical Report Certification This form provides certifications for all samples performed by MCP methods. Please refer to the Sample Results and Container Information sections of this report for specification of MCP methods used for each analysis.The following questions pertain only to MCP Analytical Methods. An affirmative response to questions A, B, C& D is required for"Presumptive Certainty" status A Were all samples received by the laboratory in a condition consistent with those described on YES their Chain-of-Custody documentation for the data set? B Were all QA/QC procedures required for the specified analytical methods(s) included in this YES report followed, including the requirement to note and discuss in a narrative QC data that did not meet appronriatp nerformance standards orguidelines? C Does the analytical data included in this report meet all the requirements for"Presumptive YES Certainty", as described in section 2.0 of the MADEP document CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only: Was the VPH or EPH method run without significant modifications, YES asspecified in Section 11.3? A response to questions E and F is required for"Presumptive Certainty" status E Were all QC performance standards and recommendations for the specified method(s) YES achieved? F Were results for all analyte-list compounds/elements for the specified method(s) reported? NO ' For any questions answered "No", please refer to the case narrative section on the following page(s). Please note that sample matrix information is located in the Sample Results section of this report. LPkA woori ad..♦...a `Page 3 of 44 Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 1 Case Narrative The samples were received in accordance with the chain of custody and no significant deviations were encountered during preparation or analysis unless otherwise noted below. MCP Related Narratives: Metals In reference to question F: At the client's request, all submitted samples were not analyzed for the full MCP list of compounds specified for the Method. 1 III i 1 I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: QwwAt�+ Title: Technical Director/Representative Date: 12/07/07 r� III Page 4 of 44 "•. i � ORGANICS 1 1 1 1 1 1 1 1 i 1 Lage 5o,aa "'�' � PETROLEUM � HYDROCARBONS ALPHA 'Page 6 of 44 1 1 1 1 i 1 f 1 1 1 1 1 1 1 1 1 i i Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-01 Date Collected: 11/30/07 07:10 Client ID: SS-4 Date Received: 11/30/07 Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3545 1 Analytical Method: 61,EPH-04-1 Extraction Date: 12/03/07 10:00 Analytical Date: 12/05/07 19:42 Analyst: AJ Percent Solids: 98% Qua�ity,CiAr6 hformat onlow- r ' Condition of sample received: Satisfactory 'Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method gn Parameter Result Qualifier Units RDL Dilution Factor Extrac#able�Petrofeum Hydrocarbons `. a, ®� ,�. ' C9-C18 Aliphatics ND mg/kg 6.80 1 C19-C36 Aliphatics 19.1 mg/kg 6.80 1 C11-C22 Aromatics 6.98 mg/kg 6.80 1 1� C11-C22 Aromatics,Adjusted 6.98 mg/kg 6.80 1 Naphthalene ND mg/kg 0.340 1 2-Methylnaphthalene ND mg/kg 0.340 1 �. Acenaphthylene ND mg/kg 0.340 1 Acenaphthene ND mg/kg 0.340 1 Fluorene ND mg/kg 0.340 1 Phenanthrene ND mg/kg 0.340 1 Anthracene ND mg/kg 0.340 1 Fluoranthene ND mg/kg 0.340 1 Pyrene ND mg/kg 0.340 1 Benzo(a)anthracene ND mg/kg 0.340 1 Chrysene ND mg/kg 0.340 1 Benzo(b)fluoranthene ND mg/kg 0.340 1 Benzo(k)fluoranthene ND mg/kg 0.340 1 Benzo(a)pyrene ND mg/kg 0.340 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.340 1 Dibenzo(a,h)anthracene ND mg/kg 0.340 1 Benzo(ghi)perylene ND mg/kg 0.340 1 t� ,Page 7 of 44 Project Name: WAKEBY ROAD,CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-01 Date Collected: 11/30 07 07.1/ 0 Client ID: SS-4 Date Received: 11/30/07 Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Eztractabte Petroleam;Hydrocarbons .r . Acceptance Surrogate % Recovery Qualifier Criteria Chloro-Octadecane 69 40-140 o-Terphenyl 85 40-140 2-Fluorobiphenyl 77 40-140 2-Bromonaphthalene 78 40-140 ,Page 8 of 44 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-02 Date Collected: 11/30/07 07:10 Client ID: SS-5 Date Received: 11/30/07 ' Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3545 Analytical Method: 61,EPH-04-1 Extraction Date: 12/03/07 10:00 Analytical Date: 12/05/07 11:09 Analyst: AJ ' Percent Solids: 989/6 ' Quality:Con Condition of sample received: Satisfactory "Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor Extractfible Petroleum Hydrocarbons` " C9-C18 Aliphatics ND mg/kg 6.80 1 C19 C36 Aliphatics ND mg/kg 6.80 1 C11-C22 Aromatics ND mg/kg 6.80 1 C11-C22 Aromatics,Adjusted ND mg/kg 6.80 1 Naphthalene ND mg/kg 0.340 1 2-Methylnaphthalene ND mg/kg 0.340 1 ' Acenaphthylene ND mg/kg 0.340 1 Acenaphthene ND mg/kg 0.340 1 Fluorene ND mg/kg 0.340 1 Phenanthrene ND mg/kg 0.340 1 Anthracene ND mg/kg 0.340 1 ' Fluoranthene ND mg/kg 0.340 1 Pyrene ND mg/kg 0.34.0 1 Benzo(a)anthracene ND mg/kg 0.340 1 Chrysene ND mg/kg 0.340 1 Benzo(b)fluoranthene ND mg/kg 0.340 1 Benzo(k)fluoranthene ND mg/kg 0.340 1 Benzo(a)pyrene ND mg/kg 0.340 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.340 1 Dibenzo(a,h)anthracene ND mg/kg 0.340 1 Benzo(ghi)perylene ND mg/kg 0.340 1 ox 1 'Page 9 of 44 z Aft Project Name: WAKEBY ROAD,CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS ' Lab ID: L0717845-02 Date Collected: 11/30/07 07:10 ' Client ID: SS-5 Date Received: 11/30/07 Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Extractable.Petroleum Hydrocarbons y 5 : w° r Acceptance Surrogate % Recovery Qualifier Criteria Chloro-Octadecane 67 40-140 o-Terphenyl 77 40-140 2-Fluorobiphenyl 81 40-140 2-Bromonaphthalene 79 40-140 1 i 1 1 1 1 1 1 1 ' Page 10 of 44 ' Project Name: WAKEBY ROAD,CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS ' Lab ID: L0717845-03 Date Collected: 11/30/07 07:10 ' Client ID: SS-6 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3545 ' Analytical Method: 61,EPH-04-1 Extraction Date: 12/03/07 10:00 Analytical Date: 12/05/07 11:45 Analyst: AJ Percent Solids: 97% x Quality Control:lnfom atior 77 Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor Extractable:Petroleum Hydrocarbons '.$i a ' C9-C18 Aliphatics ND mg/kg 6.87 1 C19-C36 Aliphatics ND mg/kg 6.87 1 C11-C22 Aromatics ND mg/kg 6.87 1 ' C11-C22 Aromatics,Adjusted ND mg/kg 6.87 1 Naphthalene ND mg/kg 0.344 1 2-Methylnaphthalene ND mg/kg 0.344 1 Acenaphthylene ND mg/kg 0.344 1 Acenaphthene ND mg/kg 0.344 1 Fluorene ND mg/kg 0.344 1 ' Phenanthrene ND mg/kg 0.344 1 Anthracene ND mg/kg 0.344 1 Fluoranthene ND mg/kg 0.344 1 1 Pyrene ND mg/kg 0.344 1 Benzo(a)anthracene ND mg/kg 0.344 1 Chrysene ND mg/kg 0.344 1 Benzo(b)fluoranthene ND mg/kg 0.344 1 Benzo(k)fluoranthene ND mg/kg 0.344 1 Benzo(a)pyrene ND mg/kg 0.344 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.344 1 Dibenzo(a,h)anthracene ND mg/kg 0.344 1 ' Benzo(ghi)perylene ND mg/kg 0.344 1 'Page 11 of 44 f ' Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-03 Date Collected: 11/30/07 07:10 Client ID: SS-6 Date Received: 11/30/07 ' Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor ExtfactablI Petroleum Acceptance Surrogate % Recovery Qualifier Criteria Chloro-Octadecane 63 40-140 o-Terphenyl 81 40-140 2-Fluorobiphenyl 86 40-140 2-Bromonaphthalene 84 40-140 i 1 1 1 1 ' /� . 'Page 12 of 44 Project Name: WAKEBY ROAD,CAD Lab Number: 1-0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS ' Lab ID: L0717845-04 Date Collected: 11/30/07 07:10 Client ID: SS-7 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3545 ' Analytical Method: 61,EPH-04-1 Extraction Date: 12/03/07 10:00 Analytical Date: 12/05/07 12:21 Analyst: AJ Percent Solids: 98% ��, z. Quality„Controlinfor�nation b �. Condition of sample received: Satisfactory -Sample Temperature upon receipt: Received on Ice ' Sample Extraction method: Extracted Per the Method ¢+; a ' ft- Parameter Result Qualifier Units RDL Dilution Factor Extractable Petroleum Hydrocarbons .'C9-C18 Aliphatics ND mg/kg 6.80 1 C19-C36 Aliphatics ND mg/kg 6.80 1 C11-C22 Aromatics ND mg/kg 6.80 1 ' C11-C22 Aromatics,Adjusted ND mg/kg 6.80 1 Naphthalene ND mg/kg 0,340 1 2-Methylnaphthalene ND mg/kg 0.340 1 ' Acenaphthylene ND mg/kg 0.340 1 Acenaphthene ND mg/kg 0.340 1 Fluorene ND mg/kg 0.340 1 ' Phenanthrene ND mg/kg 0.340 1 Anthracene ND mg/kg 0.340 1 Fluoranthene ND mg/kg 0.340 1 Pyrene ND mg/kg 0.340 1 Benzo(a)anthracene ND mg/kg 0.340 1 Chrysene ND mg/kg 0.340 1 Benzo(b)fluoranthene ND mg/kg 0.340 1 Benzo(k)fluoranthene ND mg/kg 0.340 1 Benzo(a)pyrene ND mg/kg 0.340 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.340 1 Dibenzo(a,h)anthracene ND mg/kg 0.340 1 Benzo(ghi)perylene ND mg/kg 0.340 1 'N Page 13 of 44 Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-04 Date Collected: 11/30/07 07:10 Client ID: SS-7 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor ------------- ' Extlractable;Petroleum Hydrocarbons � � , . _�� .- � �,� _ p�= Acceptance Surrogate % Recovery Qualifier Criteria Chloro-Octadecane 81 40-140 o-Terphenyl S0 40-140 ' 2-Fluorobiphenyl 86 40-140 2-Bromonaphthalene 85 40-140 t 1 i Page 14 of 44 zo Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 Method Blank Analysis Batch Quality Control rAnalytical Method: 61,EPH-04-1 Extraction Method: EPA 3545 Analytical Date: 12/03/07 18:06 Extraction Date: 12/03/07 10:00 Analyst: AJ Parameter Result Qualifier Units RDL i� €xtractable,PetroleurnlHydrocarbons for sainpfei;�,): ;01-04 Batch: ,WG304144-1 F C9-Cl8 Aliphatics ND mg/kg 6.67 ' C19-C36 Aliphatics ND mg/kg 6.67 C11-C22 Aromatics ND mg/kg 6.67 C11-C22 Aromatics,Adjusted ND mg/kg 6.67 Naphthalene ND mg/kg 0.333 2-M ethyl naphthalene ND mg/kg 0.333 Acenaphthylene ND mg/kg 0.333 ' Acenaphthene ND mg/kg 0.333 Fluorene ND mg/kg 0.333 Phenanthrene ND mg/kg 0.333 Anthracene ND mg/kg 0.333 Fluoranthene ND mg/kg 0.333 Pyrene ND mg/kg 0.333 Benzo(a)anthracene ND mg/kg 0.333 Chrysene ND mg/kg 0.333 Benzo(b)fluoranthene ND mg/kg 0.333 Benzo(k)fluoranthene ND mg/kg 0.333 Benzo(a)pyrene ND mg/kg 0.333 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.333 Dibenzo(a,h)anthracene ND mg/kg 0.333 Benzo(ghi)perylene ND mg/kg 0.333 Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 66 40-140 ' o-Terphenyl 95 40-140 2-Fluorobiphenyl 106 40-140 2-Bromonaphthalene 108 40-140 z Page 15 of 44 r r a ar r M M r r r M M M M 12070716:11 Lab Control Sample Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits Extractable PY-e ole m Kkyd�roca'rbons�Asocieteci sapke.�} Dy04' Bate V1FG304144-2 1NG3Q4�144-3- x s � ; C9-Cl8 Aliphatics 40-140 T8x� 25 _- ..._.._ .. ..... .........._.... ................ -----.. r _C19 C36 Aliphatics - '. s,61 59 40 140.............. ....... . .. ..."�A +ter _ 25- C11-C22 Aromatics •i�, M1 5B 40-140 i $ , 25 __. -. ._.... _.. ..... -- _.._ _ .. .. ._..... ......... ..._........._ _.. Naphthalene frla dt" 52 40-140 25 25 _......... ...._... ...._._.... _. ..... . 2-M ethyl naphthalene 63 "" 50 40-140 23 25 ..._..... ....._.. .. .........__. ..._.... ......._. ........ ......._ .... ...... _ ...... ....._._.......... ........ ...... .... Acenaphthylene. 59, �y4 46 40-140 2'1 25 _ ._.. - .......- _........... _. _....... .... - ...._._ .. _..... _.............. Acenaphthene 64 _ 50 40-140 25: 25 ._.--------------- _ .........- .._......... ......... .... _ ................. --- .. . ._...._.. .. ........_ . .......... .-......_. _...... _........_... ......._ Fluorene _.._......_.__ 59 54 40-140 _...... rt►24 - _.. _ _25. Phenanthrene... 7;1, 5 40-140 (Y; 25 ... _......._.. -_- _..... ...._.... .. . -- _...... .......- _ Anthracene 67 56'"� 40140 f8. 41, 25 ..........--..................._.. .. -..._._ ........ Fluoranthene �. 71' 6T 40-140 ".t5 25 _ __... - _------- -. ....._....__.........._ . .... - ..... .... Pyrene r 70., �, 40 140 .......... ............. ._......_... 14 25 Benzo(a)anthracene a,. 68 61. 40140 ;T1:N 25 Chrysene 40-140 4e 44', n 25 __ __. ............._...- ... _........._......-..._...... -._....- -- ... Benzo(b)fluoranthene ,f70' 63 40-140 1T 25 _. __. _.. ....... .,�.,, Benzo(k)f----- then 69" 63' 40 140 ti 9; ., 25 Benzo(a)pyrene �° 60. . 5T. 40 140 5; r. 25 .Indeno(-,2,3-cd)Pyrene 66: , 60"`:s.� 40-140. ..... ........... T 25 Dibenzo(a,h)anthracene .. `n° 66 61 40 140 „ 8''S, 25 ..............._.._.._.... ...._... ........... -.--.. _.-- - _------ _ ._. _..... _ _._.... Benzo(ghi)perylene 7Q's 63 40.140 ........................_...... ......... §K 1:T � 25 _ _......_. ...__... .........._.................. .......... _........ Nonane(C9) "'"',52 44 30 140*cs ... 1,7 25..._.......... ........xr. , . Page 16 of 44 12070716:11 Lab Control Sample Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits E�xtractak f9PetroleunraFC etroearbonsssoc':.Aiated saris le s : _ 01-04 Batch , WG3Q4144 2 .VVG304 44-,3. =.Y Decane(C10) �. 8Q„ V 56 4 40-140 , i8y 25 - -__......... ...._ _ --.... -_ ._...-.. . .... ........... ...... ..........._. ._..... ..... Dodecane(C 12) 6 )� + 54 .a 40-140........... ---_._ _._. .�.� :•.' 25 Tetradecane(C14) 68 { 55 40-140.. �•21 25 _...__ ........... ....._._........ --- -- _.._....---------------------- -----------.. ...... v Hexadecane(C16) 68 40-140 " 19V 25 Octadecane(C18) 68: 57 s 40 140......_.... ..__ ..... 18P: _........_..... _.25.. ....__... ._... Nonadecane(C19) 58 40-140 DEB' „, 25 _. _ .... _...._- .._.._ -- -- _ ........ ....... Eicosane(C20) I *• ' t.6a 40-140 13>. 25 ....................... .._.._.._......._.._. .._ ._ Docosane(C22) 67: ..._ 40-140 eta 25 .......... ..._........ .._._ .. Tetracosane(C24) 66s t 60' 40-140 (:0'., 25 _.._.. _ .. --.--_ _.. ... Hexacosane(C26) a� 65, �60L 40-140 25 ....... - .... ...... _ Octacosane C28( ) .��, ."64 � " 53,• 40-140 -,8" ,�"; 25 Triacontane(C30) 6 ' 45 8. 40-140 -. . - - 6 25.... ......... ....... ................... ry s k .n i - Hexatriacontane(C36) ' fil R" 56- 40-1409 25 %Naphthalene Breakthrough x U W y6, %2-Methylnaphthalene Breakthrough - 0 0• ti rz r NG; ---..----------- ._..._. .... ....._..... ..._.__............ ....... . .........- .........._ ........._.. _._.. . ._..... .. ....... t� Page 17 of 44 r \ � 12070716:11 Lab Control Sample Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits Extractabler troleut�tHy:4rocarbons Associatetl sam,ple(s): 01=04 . Ba ct h: ,,W 3G fI O VI/G30414403; }',� ,�� n' ° -� LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Chloro-Octadecane 43 38 40-140 o-Terphenyl 52 48 40-140 2-Fluorobiphenyl 88 76 40-140 2-Bromonaphthalene 90 78 40-140 •Naphthalene Breakthrough 0 0 %2-Methylnaphthalene Breakthrough 0 0 Page 18 of 44 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 Fractionation Check Standard Quality Control ' Fractionation checkr�tanda�d fog FISHQ61149s .+x 4Md.ir%�Jr.:."J."3��i+hi,�:.J`i'V✓i"w�%k".�.+X'� .5+ 1� '`\..li. ' Parameter % Recovery QC Criteria C9-Cl8 Aliphatics 60 40-140 C19-C36 Aliphatics 72 40-140 C11-C22 Aromatics 83 40-140 Naphthalene 77 40-140 2-Methylnaphthalene 72 40-140 ' Acenaphthylene 72 40-140 Acenaphthene 74 40-140 Fluorene 74 40-140 Phenanthrene 77 40-140 Anthracene 72 40-140 ' Fluoranthene 82 40-140 Pyrene 82 40-140 Benzo(a)anthracene 82 40-140 Chrysene 82 40-140 Benzo(b)fluoranthene 81 40-140 Benzo(k)fluoranthene 84 40-140 ' Benzo(a)pyrene 76 40-140 Indeno(1,2,3-cd)Pyrene 76 40-140 Dibenzo(a,h)anthracene 80 40-140 Benzo(g,h,i)perylene 80 40-140 Nonane 54 30-140 ' Decane 58 40-140 Dodecane 62 40-140 Tetradecane 62 40-140 Hexadecane 63 40-140 Octadecane 64 40-140 Nonadecane 64 40-140 ' Eicosane 66 40-140 Docosane 70 40-140 Tetracosane 73 40-140 Hexacosane 76 40-140 Octacosane 77 40-140 ' Triacontane 78 40-140 Hexatriacontane 82 40-140 'i Page 19 of 44 Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 Fractionation Check Standard Quality Control Fractionation check 4tandartl for;FISH061.149 CrcYia.+tv�;+y"r-�'s'!ca�;:t,•�sr;x..--as5 �"` ,�'. Surrogate % Recovery QC Criteria Chloro-Octadecane 52 40-140 o-Terphenyl 77 40-140 2-Fluorobiphenyl 76 40-140 2-Bromonaphthalene 76 40-140 Lli i Page 20 of 44 ve PCBS 1 I � 1 a Page 21 of 44 Oe. i Project Name: WAKEBY ROAD. CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-01 Date Collected: 11/30/07 07:10 Client ID: SS-4 Date Received: 11/30/07 Sample Location: 810 WAKEB:' ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 64,8082 Extraction Date: 12/03/07 21:00 Analytical Date: 12/06/07 21:11 Cleanup Method1: EPA 3665A Analyst: JB Cleanup Date1: 12/04/07 Percent Solids: 98% Parameter Result Qualifier Units RDL Dilution Factor Polchlorinat dBpeny sy i Aroclor 1016 ND ug/kg 34.0 1 Aroclor 1221 ND ug/kg 34.0 1 Aroclor 1232 ND ug/kg 34.0 1 Aroclor 1242 ND ug/kg 34.0 1 Aroclor 1248 ND ug/kg 34.0 1 Aroclor 1254 ND ug/kg 34.0 1 Aroclor 1260 ND ug/kg 34.0 1 Aroclor 1262 ND ug/kg 34.0 1 Aroclor 1268 ND ug/kg 34.0 1 Acceptance Surrogate %Recovery Qualifier Criteria Column 2,45,6-Tetrachloro-m-xylene 70 30-150 A Decachlorobiphenyl 77 30-150 A 2,45,6-Tetrachloro-m-xylene 65 30-150 B Decachlorobiphenyl 79 30-150 B i t 1 1 P kA bi M2 fhH Page 22 of 44 ' Project Name: WAKEBY ROAD, CAD Lab Number: 1-0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-02 Date Collected: 11/30/0707:10 Client ID: SS-5 Date Received: 11/30/07 Sample Location: 810 WAKEB( ROAD Field Prep: Not Specified 1 Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 64,8082 Extraction Date: 12/03/07 21:00 Analytical Date: 12/06/07 21:39 Cleanup Methodl: EPA 3665A Analyst: JB Cleanup Datel: 12/04/07 Percent Solids: 98% Parameter Result Qualifier Units RDL Dilution Factor Rolychlorinated;Biphenyls.byaMCP,BC Aroclor 1016 ND ug/kg 34.0 1 Aroclor 1221 ND ug/kg 34.0 1 Aroclor 1232 ND ug/kg 34.0 1 Aroclor 1242 ND ug/kg 34.0 1 Aroclor 1248 ND ug/kg 34.0 1 Aroclor 1254 ND ug/kg 34.0 1 Aroclor 1260 ND ug/kg 34.0 1 Aroclor 1262 ND ug/kg 34.0 1 Aroclor 1268 ND ug/kg 34.0 1 Acceptance Surrogate % Recovery Qualifier Criteria Column 2,45,6-Tetrachloro-m-xylene 72 30-150 A Decachlorobiphenyl 80 30-150 A 2,45,6-Tetrachloro-m-xylene 67 30-150 B Decachlorobiphenyl 83 30-150 B r kat HA r;WgS Page 23 of 44 ' Project Name: WAKEBY ROAD CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-03 Date Collected: 11/30/07 07:10 Client ID: SS-6 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Anaytical Method: 64,8082 Extraction Date: 12/03/07 21:00 Analytical Date: 12/06/07 22:08 Cleanup Methodl: EPA 3665A Analyst: JB Cleanup Datel: 12/04/07 Percent Solids: 97% ' Parameter Result Qualifier Units RDL Dilution Factor Polychiorinated E iphenyls by,MCF' 082 . , Aroclor 1016 ND ug/kg 34.4 1 Aroclor 1221 ND ug/kg 34.4 1 Aroclor 1232 ND ug/kg 34.4 1 Aroclor 1242 ND ug/kg 34.4 1 Aroclor 1248 ND ug/kg 34.4 1 ' Aroclor 1254 ND ug/kg 34.4 1 Aroclor 1260 ND ug/kg 34.4 1 Aroclor 1262 ND ug/kg 34.4 1 Aroclor 1268 ND ug/kg 34.4 1 ' Acceptance Surrogate % Recovery Qualifier Criteria Column 2,45,6-Tetrachloro-m-xylene 82 30-150 A ' Decachlorobiphenyl 89 30-150 A 2,4,5,6-Tetrachloro-m-xylene 67 30-150 B Decachlorobiphenyl 80 30-150 B tt t Y}or �asst� ,Page 24 of 44 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 ' SAMPLE RESULTS Lab ID: L0717845-C4 Date Collected: 11/30/07 07:10 ' Client ID: SS-7 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 ' Anaytical Method: 64,8082 Extraction Date: 12/03/07 21:00 Analytical Date: 12/06/07 22:37 Cleanup Method1: EPA 3665A Analyst: JB Cleanup Date1: 12/04/07 ' Percent Solids: 98% tParameter Result Qualifier Units RDL Dilution Factor Polychlorinated°tiphenyls'by MGF''8082 ' Aroclor 1016 ND ug/kg 34.0 1 Aroclor 1221 ND ug/kg 34.0 1 ' Aroclor 1232 ND ug/kg 34.0 1 Aroclor 1242 ND ug/kg 34.0 1 ' Aroclor 1248 ND ug/kg 34.0 1 Aroclor 1254 ND ug/kg 34.0 1 Aroclor 1260 ND ug/kg 34.0 1 ' Aroclor 1262 ND ug/kg 34.0 1 Aroclor 1268 ND ug/kg 34.0 1 ' Acceptance Surrogate % Recovery Qualifier Criteria Column 2,4,5,6-Tetrachloro-m-xylene 79 30-150 A i' Decachlorobiphenyl 83 30-150 A 2,4,5,6-Tetrachloro-m-xylene 72 30-150 B ' Decachlorobiphenyl 89 30-150 B y �v 'Page 25 of 44 Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 ' Method Blank Analysis Batch Quality Control Analytical Method: 64,8082 Extraction Method: EPA 3546 Analytical Date: 12/04/07 15:02 Extraction Date: 12/03/07 21:00 Analyst: JB Cleanup Method1: EPA 3665A Cleanup Date1: 12/04/07 Parameter Result Qualifier Units RDL Polychlorinated E3iphenyl'slby l�tCP°8082.for samples) 01-04TF Ba#ch -WG304272 1 -I e`7 - } Aroclor 1016 ND ug/kg 33.3 Aroclor 1221 ND ug/kg 33.3 Aroclor 1232 ND ug/kg 33.3 Aroclor 1242 ND ug/kg 33.3 ' Aroclor 1248 ND ug/kg 33.3 Aroclor 1254 ND ug/kg 33.3 Aroclor 1260 ND ug/kg 33.3 1 Aroclor 1262 ND ug/kg 33.3 Aroclor 1268 ND ug/kg 33.3 i Acceptance ' Surrogate %Recovery Qualifier Criteria Column 2,4,5,6-Tetrachloro-m-xylene 57 30-150 A Decachlorobiphenyl 73 30-150 A 2,45,6-Tetrachloro-m-xylene 76 30-150 B Decachlorobiphenyl 75 30-150 B i sA! Page 26 of 44 i w iw a aw w �w w ilw■ MEli w w w w i M w w M 12070716:11 Lab Control Sample Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits RolychlorinatedTBiphenyfsabyMCP8082 AssocratedYsample(s} 01 04 ,Batch:: V1/G304272-2k.WG304272 Aroclor 1016 79.,. 98 40-140 21, 30 Aroclor 1260 72 $3 40 14014 30 ......... .. .. _......_.................... _. ; _ _.....__......._....._ _ . LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Column 2,4,5,6-Tetrachloro-m-xylene 56 70 30-150 A Decachlorobiphenyl 70 83 30-150 A 2,4,5,6-Tetrachloro-m-xylene 72 91 30-150 B Decachlorobiphenyl 73 88 30-150 B Page 27 of 44 METALS �N$6if�d8�9k�Aai Page f g 28 0 44 f ' Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 ' Lab ID: L0717845-01 SAMPLE RESULTS Date Collected: 11/30/07 07:10 Client ID: SS-4 Date Received: 11/30/07 ' Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 98% ' Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst TotalMetals by MCP.,6000/7000rseries: 4 $. ' Arsenic,Total v 0.78 mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:38 EPA 3050B� 60,6010E MG Barium,Total 3.4 mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:38 EPA 3050E 60,6010B MG ' Cadmium,Total ND mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:38 EPA 3050E 60,6010B MG Chromium,Total 2.4 mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:38 EPA 3050E 60,60106 MG ' Lead,Total 4.0 mg/kg 2.4 1 12/06/07 18:30 12/07/07 11:38 EPA 3050B 60,6010E MG Mercury,Total ND mg/kg 0.07 1 12/06/07 20:00 12/07/07 12:44 EPA 7471A 64,7471A DM Selenium,Total ND mg/kg 2.4 1 12/06/07 18:30 12/07/07 11:38 EPA 3050E 60,6010E MG ' Silver,Total ND mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:38 EPA 3050B 60,6010E MG II �� II 'Page 29 of 44 -1- 1 v. . Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-02 Date Collected: 11/30/07 07:10 Client ID: SS-5 Date Received: 11/30/07 ' Sample Location: 810 WAKE BY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 98% Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst T_ Total Metals l y MCP 6Q00/7000,series'I�� r` a y p ��r . , ' Arsenic,Total 2.8 mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:43 EPA 3050E 60,6010E MG Barium,Total 5.0 mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:43 EPA 3050B 60,6010E MG ' Cadmium,Total ND mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:43 EPA 3050E 60,6010B MG Chromium,Total 2.6 mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:43 EPA 3050B 60,6010B MG Lead,Total 3.1 mg/kg 2.4 1 12/06/07 18:30 12/07/07 11:43 EPA 3050B 60,6010E MG Mercury,Total ND mg/kg 0.08 1 12/06/07 20:00 12/07/07 12:45 EPA 7471A 64,7471A DM Selenium,Total ND mg/kg 2.4 1 12/06/07 18:30 12/07/07 11:43 EPA 3050E 60,6010E MG Silver,Total ND mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:43 EPA 3050E 60,6010E MG i 'Page 30 of 44 Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 ' Lab ID: L0717845-03 SAMPLE RESULTS Date Collected: 11/30/07 07:10 Client ID: SS-6 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 97% Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst TotaLMetals;by"MCR6000/7000 eries ' Arsenic,Total 0.73 mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:46 EPA 3050E 60,6010E MG Barium,Total 2.2 mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:46 EPA 3050B 60,6010B MG Cadmium,Total ND mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:46 EPA 3050E 60,6010E MG Chromium,Total 1.5 mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:46 EPA 3050E 60,6010B MG Lead,Total 5.5 mg/kg 2.4 1 12/06/07 18:30 12/07/07 11:46 EPA 3050B 60,6010E MG Mercury,Total ND mg/kg 0.09 1 12/06/07 20:00 12/07/07 12:47 EPA 7471A 64,7471A DM Selenium,Total ND mg/kg 2.4 1 12/06/07 18:30 12/07/07 11:46 EPA 3050E 60,6010B MG ' Silver,Total ND mg/kg 0.48 1 12/06/07 18:30 12/07/07 11:46 EPA 3050B 60,6010E MG I r � 'Page 31 of 44 Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 ' Lab ID: L0717845-04 SAMPLE RESULTS Date Collected: 11/30/07 07:10 Client ID: SS-7 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Percent Solids: 98% Dilution Date Date Prep Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Method Analyst Total.Metals,ffMCP=6000/7000<sefies <1 , -�: ' Arsenic,Total 0.70 mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:49 EPA 3050B 60,6010E MG Barium,Total 2.4 mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:49 EPA 3050E 60,6010E MG Cadmium,Total ND mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:49 EPA 3050B 60,6010B MG Chromium,Total 2.1 mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:49 EPA 3050B 60,6010E MG Lead,Total ND mg/kg 2.4 1 12/06/07 18:30 12/07/07 11:49 EPA 3050E 60,6010E MG Mercury,Total ND mg/kg 0.08 1 12/06/07 20:00 12/07/07 12:49 EPA 7471A 64,7471A DM Selenium,Total ND mg/kg 2.4 1 12/06/07 18:30 12/07/07 11:49 EPA 3050E 60,6010E MG Silver,Total ND mg/kg 0.49 1 12/06/07 18:30 12/07/07 11:49 EPA 3050E 60,6010E MG 1 1 Page 32 of 44 � Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 Method Blank Analysis Batch Quality Control Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst ' TotalvMetals by MCP 600Ql7000 series,for sample(s):�01�04 Batch: V1IG3Q4790=1 :v � hF�4 =r ` Arsenic,Total ND mg/kg 0.50 1 12/06/07 18:30 12/07/07 11:21 60,6010B MG Barium,Total ND mg/kg 0.50 1 12/06/07 18:30 12/07/07 11:21 60,6010B MG Cadmium,Total ND mg/kg 0.50 1 12/06/07 18:30 12/07/07 11:21 60,6010E MG ' Chromium,Total ND mg/kg 0.50 1 12/06/07 18:30 12/07/07 11:21 60,6010E MG Lead,Total ND mg/kg 2.5 1 12/06/07 18:30 12/07/07 11:21 60,6010E MG Selenium,Total ND mg/kg 2.5 1 12/06/07 18:30 12/07/07 11:21 60,6010E MG ' Silver,Total ND mg/kg 0.50 1 12/06/07 18:30 12/07/07 11:21 60,6010B MG ' Prep Information Digestion Method: EPA 3050B Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst otal`MetaI- by MCP 6000/7000 series:for sample(s): 101=04 Batch: WG304794M1. - ..�.: �.. Mercury,Total ND mg/kg 0.08 1 12/06/07 20:00 12/07/07 12:10 64,7471A DM Prep Information ' Digestion Method: EPA 7471A 1 1 1 'Page 33 of 44 i 12070716:11 Lab Control Sample Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits �atal�Metals�by�itit1�CP'6 0 =40Uzs�ries so�:►at d sampPe � �: '�1�-�4' Bad�i� YVE330479(?-2 'C3 ��9.(�-3 Arsenic,Total $ al 75-125 5 30 - --- Barium,Total 75-125 30 _. Cadmium Total $ 75-125 - 30_._ ..... _... . Chromium Total 9 S- 75 125 30 _.. --- -- Lead,Total 8a a5 75-125i, 30 Selenium,Total8 75-125 t5�,y 30 aa '`' _... . . _ ...-._._ Silver,Total 9 75-125 f 30 �o al. `eta stay�![� , (7:.::� se:r S Ass G e s�r?r►pte � � a d� h: E3 . ,. , �,� Mercury,Total - q6 14 75-1254 30 ..._- Page 34 of 44 rLW I_ _aoT LBtr.A � INORGANICS 1 & � MISCELLANEOUS tage 35 of 44 1 i 1 1 i 1 1 1 1 1 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 �. SAMPLE RESULTS Lab ID: L0717845-01 Date Collected: 11/30/07 07:10 Client ID: SS-4 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil r Dilution Date Date Analytical 1 Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst GeneralChemistry �: Solids,Total 98 % 0.10 1 12/04/07 18:00 30,2540G NM i r 'Page 36 of 44 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 ' SAMPLE RESULTS Lab ID: L0717845-02 Date Collected: 11/30/0707:10 Client ID: SS-5 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Gsnecai Chemistry. WERE Solids,Total 98 % 0.10 1 12/04/07 18:00 30,2540G NM 'Page 37 of 44 ' Project Name: WAKEBY ROAD,CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-03 Date Collected: 11/30/07 07:10 Client ID: SS-6 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst ,General Chemistry Solids,Total 97 % 0.10 1 12/04/07 18:00 30,2540G NM r Page 38 of 44 Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 SAMPLE RESULTS Lab ID: L0717845-04 Date Collected: 11/30/07 07:10 Client ID: SS-7 Date Received: 11/30/07 Sample Location: 810 WAKEBY ROAD Field Prep: Not Specified ' Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst � Gen it Chemistry. ., � , r � - y t �� ` Solids,Total 98 % 0.10 1 12/04/07 18:00 30,2540G NM 1 II t i I Page 39 of 44 12070716:11 Lab Duplicate Analysis Project Name: WAKEBY ROAD, CAD Batch Quality Control Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 Parameter Native Sample Duplicate Sample Units RPD RPD Limits Associated sampie(s,): '01-04. QC Batch iD ,,WG304378 1'� QC Sample: 'L07.17,785-09 Client tD. DUP.Sample =s �, M G Solids,Total 94 94 % 0 u? 20 Page 40 of 44 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 Sample Receipt and Container Information Were project specific reporting limits specified? YES ' Cooler Information Cooler Custody Seal ' A Absent Container Information ' Container ID Container Type Cooler pH Temp Pres Seal Analysis L0717845-01A Amber250m1 unpreserved A N/A 3C Y Absent EPH-DELUX-04,MCP- ' 7471 T,MCP-8082-04,MCP-AG- 6010T,M C P-AS-6010T,M C P-BA- 6010T,MCP-CD-6010T,MCP-CR- 6010T,M CP-PB-6010T,MCP-SE- 6010T,TS ' L0717845-02A Amber250ml unpreserved A N/A 3C Y Absent EPH-DELUX-04,MCP- 7471 T,MCP-8082-04,MCP-AG- 6010T,MCP-AS-6010T,MCP-BA- 6010T,M CP-CD-6010T,MCP-C R- ' 6010T,MCP-PB-6010T,MCP-SE- 6010T,TS L0717845-03A Amber 250m1 unpreserved A N/A 3C Y Absent EPH-DELUX-04,MCP- 7471 T,MCP-8082-04,MCP-AG- 6010T,MCP-AS-6010T,MCP-BA- 6010 T,M C P-C D-6010 T,M C P-C R- 6010T,M C P-PS-6010T,MCP-SE- 6010T,TS ' L0717845-04A Amber 250ml unpreserved A N/A 3C Y Absent EPH-DELUX-04,MCP- 7471 T,MCP-8082-04,MCP-AG- 6010 T,M C P-AS-6010T,M C P-BA- 6010 T,M C P-C D-6010T,MCP-C R- 6010 T,M C P-P B-6010T,M C P-S E- 6010T,TS Container Comments L0717845-01A Temp Probe L0717845-02A Temp Probe ' L0717845-03A Temp Probe L0717845-04A Temp Probe Page 41 of 44 `" .�.. Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 GLOSSARY Acronyms EPA - Environmental Protection Agency. LCS - Laboratory Control Sample:A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. r LCSD- Laboratory Control Sample Duplicate: Refer to LCS. MS - Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. t MSD - Matrix Spike Sample Duplicate: Refer to MS. NA - Not Applicable. NI - Not Ignitable. NC - Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. ND Not detected at the reported detection limit for the sample. RDL - Reported Detection Limit: The value at which an instrument can accurately measure an analyte at a ' specific concentration. The RDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. RPD - Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily ' designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. ' Terms Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers The following data qualifiers have been identified for use under the CT DEP Reasonable Confidence Protocols. A- Spectra identified as "Aldol Condensation Product". ' B-The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte. E- Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. J - Estimated value. The analyte was tentatively identified; the quantitation is an estimation. (Tentatively identified compounds only.) Standard Qualifiers H -The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time ' of sample collection. Report Format: Not Specified 'Page 42 of 44 ' Project Name: WAKEBY ROAD, CAD Lab Number: L0717845 Project Number: SE01-615-1 Report Date: 12/07/07 ' REFERENCES ' 30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA-WPCF. 18th Edition. 1992. 60 Quality Assurance and Quality Control Requirements and Performance Standards for SW- 846 Methods. MADEP BWSC.WSC-CAM-IIA(Revision 4),WSC-CAM-V C(Revision 2), WSC-CAM-IIIA(Revision 5). May 2004. ' 61 Method for the Determination of Extractable Petroleum Hydrocarbons(EPH). Massachusetts Department of Environmental Protection, DEA/ORS/BWSC. May 2004, Revision 1.1. 1 64 Quality Assurance and Quality Control Requirements and Performance Standards for SW- 846 Methods. MADEP BWSC.WSC-CAM-IIA(Revision 4),WSC-CAM-V C(Revision 2), WSC-CAM-IIIA(Revision 5). August 2004. i ' LIMITATION OF LIABILITIES Alpha Woods Hole Labs performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Woods Hole Labs ' shall be to re-perform the work at it's own expense. In no event shall Alpha Woods Hole Labs be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Woods Hole Labs. ' We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. Page 43 of 44 _ CHAIN OF CUSTODY PAGE OF Date Rec'd In Lab: !I ALPHA Job#: 1Proje-A Informletion Report Information-Data Deliverables. Billing Informatiol 0? �� WESTBORO,MA MANSFIELD,MA i TB-:508.898-0220 TEL:508-822-9300 Projecl Name: pN<E$Y R ❑FAX ❑EMAIL ❑Same as Client info I PO#: _— - FAX:508-898-9193 FAX:508-822-3288 .... _. t�b t ��... /-' ---- . Project Location: �� Why Po4fl 13?SDEx ❑Add'I Deliverables w+43Y Rotaj7 �Ii (- ANC' . —. . .. - ments"Report Limits Client: Project#: _ Stale/Fed Program Criteria Acdress: / � ._.� Projec:Manager: - - 4&CL t? I S tY C. RAY QVIn1 ' 14 t2S 1 ►L�Lr r1gr4 j'20 ALPHA Quote#: - • .; ► e ••• • • Phone: 'I ,31�( Q�DD ❑Yes ❑No Are MCP Analytical Methods Required^ Fax: ? ' g�U �g3 ❑Yes ❑No Are CT RCP(Reasonable Confidence Protocols)Required? l �� — ....-- Standard ❑ RUSH•oelycof—d#peanoroved.9 Fslail: rrJs2V ��'cT&L-FNCP _ to Due: Time: i SAMPLEHANDLING i— � / ;' , ❑ These samples have been previously analyzed by Alpha - t/ Z� ——— FJtration .// ' CI Done Other Project Specific Requirements/Comments/Detection Limits: ,r. U Q; „ i 1W Oaa` o Not to a o /�,1 ,' j'�•, ! P.•eservation T �r ❑Lab to do i ems, v ;, (P4ase specify below) ALPHA Lab ID Collection Sample Sampler's iLab Use Only) SamplelD Date Time Matrix Initials Z Sample SpecHicComments 1-7 Us- — - _ . � 7 t Z o rs S /4wt � 13 i 1 Sg (A II 30 0� Zo 5M I PLEASE ANSWER QUESTIONS ASOVEI Container Type (� I release print clearly,legibly and Preservative )i i completely. Samples cannot be i IS YOUR PROJECT logged in and turnaround time clock Relinquished y: ! Date(rima ecei;Vw- - lme will not start until any ambiguities are MA MCP or CT RCP? tM;>� ( II.55 If _ subjecttoAipnas Payment- � I I pies sum are -•-•.- _ .. See reverse side. Pa O 'FORMNO:01-01(w.30-JUL-07) - / -- _. N w 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 MONDAY, JANUARY 3, 2011 Marstons Mills shed fire kj JkLl CHRISTINE HOCHKEPPEIICAPE COb TIMES A storage shed at a former Junk yard In Marstons Mills was destroyed by fire Sunday after- noon, according to the Centerville-Osterville-Marstons Mills Fire Department. A neighbor near 810 Wakeby Road who heard an explosion and saw the flames reported the fire shortly before 4 p.m.The cause of the fire remained under investigation Sunday night,a fire depart- ment official said., A6 B�LDCape Cod Times 1 qua' ke '-. t rattles Chil power were knocked out in doning'some shopping cen- � the Araucania region where ters entirely: �� ERU>' SRA. the quake was centered, 370 In the communities of La BOL - miles south-southwest of the Araucania,Puerto Saavedra, � �# r capital;Santiago. Tolteri andTeodoro Smith,anOq f� PAt The U.S.Geological Survey estimated 50,000 people vol- said the epicenter was about untarily evacuated to higher 45 miles from the provincial ground;according to Nunez. ;.a UR capital ofTemuco,which has a Hundreds of tourists spend- k ARG. population of about 250,000. ing the New Year's holiday:at . z : MI i° The quake struck at.a depth the resorts of Villarica and AJcea t of 11 miles, the USGS said, Pucon cut their trips short and there was at least one and headed north, clogging ° aftershock of 5.0 magnitude. roads and toll stations. When the first temblor Residents of the region have SOURCES:ES RI;USGS AP struck; people in several fresh memories of the magmi coastal cities quickly moved tude-8.8 quake and resulting away from,the ocean;.aban tsunami on Feb.27,2010. Austral" ia Citizen Web Request Page 1 of 1 Citizen Request Management Request ID: 33305 Created: 1/4/2011 4:03:45 PM ' Status: — Closed Assigned To: Miorandi, Donna Health Office Anonymous: No Category: Chapter 108Hazardous Materials E.C. Date: 1/19/2011 Created By: Parvin, Lindsay Citations: BuildingDept 4 Time Worked: 3.00 Response Time: 0.50 "i Request Location: 810 WAKEBY ROAD Marstons Mills, Ma 02648 Parcel Number: Map: 013 Block: 052 Lot: 000 Request: 4:45pm 1/03/2010-COMM Fire Department requested a Health Inspector at the scene of an explosion/fire at 810 Wakeby Road, Marstons Mills. Request Work History: Entered on 1/5/2011 8:23:37 AM DZM responded and took pictures. It was a shed fire that was caused by an unknown factor. It is in ZOC-no wetlands nearby. It is a 16 acre parcel formerly owned by Gifford and known as the "Gifford Pit". It is now owned by Wakeby Road Realty Trust/Christopher Keyes, phone 3508-888- 3400. Captain Eldredge of COMM Fire Dept was the Incident Commander and many fire dept personnel were on the scene including cotuit for assistance. Wakeby Road was shut down for this period of time. DZM called DEP and spoke to Julie Hutcheson. Julie went to the site on 1/4/2011 with Cynthia Martin, Hazardous Material Inspector of Barnstable Health. No imminent problems- premise was that anything that was on site went up in air with the fire. Cynthia Martin shall follow up with later inspections. http://itsqldb/CitizenRequest/WRequestPrintPub.aspx?ID=33305 8/27/2018 Bk 22107 Ps259 -35414 06-14-200 7 a 1 1 2 20ct QUITCLAIM DEED Property Address: Wakeby Road,Marston$ Mills,MA I,Harriet P. Hayward,Trustee of The Overlord Realty Trust u/d/t 11/13/95 recorded with the Barnstable County Registry of Deeds in Book 9928, Page 122 and l s`Amendment dated 12/17/99 recorded in Book 12731, Page 128,of 49 East Road,P.O. Box 425,Forestdale,MA 02644 for consideration paid in full of Two Thousand and 00/100 ($2,000.00)dollars Grant to Wakeby Road Realty, Inc. a Massachusetts Corporation of 72 Pine Street, Hyannis,MA 02601 With Quitclaim Covenants All of the Trusts remaining right title and interest to the land with the buildings thereon situated on Wakeby Road,Marstons Mills,Barnstable County,Massachusetts and shown on a plan of land entitled "Plan of Land in Newtown,Barnstable Mass. For Priscilla E. Maynard T. & William C. Gifford by Charles Savery Inc. Registered Engineers and Surveyors, Hyannis,Mass Scale: 1 inch= 100 feet dated August 26, 1974" and recorded with the Barnstable County Registry of Deeds in Plan Book 288, Page 75,one being marked "16.66 acres",meaning and intending to convey the property shown on the plan and any and all of my interest from any source in that property of Joseph Landers referenced by a deed recorded_December 18, 1857 in Book 66, Pages 107 & 108. For title see deed recorded at Barnstable County Registry of Deeds in Book 9928, Page 127. 1 further certify as follows: I am the sole trustee; the Declaration of Trust has not been altered, modified,amended or terminated since its recording,except as may already appear of record at said Registry of Deeds; no beneficiary is a minor, incompetent, a corporation selling all or substantially all of its assets,or a personal representative of an estate subject to tax liens; All the beneficiaries of the Trust, being Cape Cod Organization for the Rights of the Disabled (CORD) and Hospice & Pallative Care of Cape Cod,Inc. successor to Hospice of Sandwich,Massachusetts have authorized and directed the Trustee to execute.this Quitclaim Deed. BARNSYABLETCOUNTYTREGISTRY OFxDEEDS Date: 06--14--2007 0 11:20am CtIAV: 906 Doc*: 35414 Fee: $6.84 Cons: $2000.00 BARNSTABLE COUNTY EXCISE TAX BARNSTABLE COUNTY REGISTRY OF DEEDS Date: 06-•14-2007 a 11:20am MA: 906 Doct: 35414 Fee: $4.56 ions: QrO00.00 Bk 22107 Pg 260 #35414 Witness my hand and seal this `day of June,2007 The Overlord Realty Trust Harriet P. Hayward, rustee COMMONWEALTH OF MASSACHUSETTS Barnstable, ss �Zlke, /�3 ,2007 Then personally appeared before me, the undersigned notary public, the above-named Harriet P. Hayward,Trustee of The Overlord Realty Trust who proved to me through satisfactory evidence of identification, which were 7z(',C, 121 who is known by me and to me known to be, the person whose name is signed on the preceding or attached document, and acknowledged to me that she signed it voluntarily for its stated purpose. No ary Public Y commission expire: 1111-31"1 JANICE R.ORENIER NOTARY PUBLIC COMMONWEALTH of MASSACHUSETTS2+,^6 My COMMISSION EXPIRE NOVEMBER 13,2009 Deeds\W akeby.mm.deed.doc BARNSTABLE REGISTRY OF DEEDS Bk 22107 Pg 259 JL35414 06-14-2007 a`i 1 1 2 2JDCL QUITCLAIM DEED Property Address: Wakeby Road,Marstons Mills,MA I, Harriet P. Hayward,Trustee of The Overlord Realty Trust u/d/t 11/13/95 recorded with the Barnstable County Registry of Deeds in Book 9928, Page 122 and 1"Amendment dated 12/17/99 recorded in Book 12731, Page 128,of 49 East Road,P.O. Box 425,Forestdale,MA 02644 for consideration paid in full of Two Thousand and 00/100 ($2,000.00)dollars Grant to Wakeby Road Realty, Inc. a Massachusetts Corporation of 72 Pine Street,Hyannis,MA 02601 With Quitclaim Covenants All of the Trusts remaining right title and interest to the land with the buildings thereon situated on Wakeby Road,Marstons Mills,Barnstable County,Massachusetts and shown on a plan of land entitled "Plan of Land in Newtown,Barnstable Mass. For Priscilla E. Maynard T. & William C. Gifford by Charles Savery Inc. Registered Engineers and Surveyors, Hyannis,Mass Scale: 1 inch= 100 feet dated August 26, 1974" and recorded with the Barnstable County Registry of Deeds in Plan Book 288,Page 75, one being marked ".16.66 acres",meaning and intending to convey the property shown on the plan and any and all of my interest from any source in that property of Joseph Landers referenced by a deed recorded December 18, 1857 in Book 66, Pages 107 & 108. For title see deed recorded at Barnstable County Registry of Deeds in Book 9928,Page 127. I further certify as follows: I am the sole trustee; the Declaration of Trust has not been altered, modified, amended or terminated since its recording,except as may already appear of record at said Registry of Deeds; no beneficiary is a minor, incompetent, a corporation selling all or substantially all of its assets, or a personal representative of an estate subject to tax liens; All the beneficiaries of the Trust, being Cape Cod Organization for the Rights of the Disabled (CORD) and Hospice & to Hospice of Sandwich Massachusetts have authorized f Cape Cod Inc. successor , Pallative Care o Capp and directed the Trustee to execute this Quitclaim Deed. MASSAC:HUSETTS STATE EXCISE TAX BARNSTABLE COUNTY REGISTRY OF DEEDS Date: 06--14-2007 8 11:20an Ctl:: 906 Doc:: 35414 Fee: $6.84 Cons: $2r000.00 BARNSTABLE COUNTY EXCISE TAX BARNSTABLE COUNTY REGISTRY OF DEEDS Date: 06-14-2007 a 11:20an Ctl*: 906 DOCAT: 35414 Fee: $4,56 Cons: $2000.00 r Bk 22107 Pg 260 #35414 ` Witness my hand and seal this day of June,2007 The Overlord Realty Trust Harriet P. Hayward, rustee COMMONWEALTH OF MASSACHUSETTS Barnstable, ss �2/", /.3 , 2007 17— Then personally appeared before me, the undersigned notary public, the above-named Harriet P. Hayward,Trustee of The Overlord Realty Trust who proved to me through satisfactory evidence of identification, which were A'.c. ��l C�r_iC�sL C; who is known by me and to me known to be, the person whose name is signed on the preceding or attached document, and acknowledged to me that she signed it voluntarily for its stated purpose. No ary Public *commission expire;: ////I/�'/ JANICE R.GRENIER t< NOTARY PUBLIC COMMONWEALTH of MASSACHUSETTS�',i } My COMMISSION EXPIRES V A „ NOVEMBER 13,2009 Deeds\W akeby.mm.deed.doc BARNSTABLE REGISTRY OF DEEDS Bk 21095 Ps202 T3 r 227 4f3--14-2006 of 1 1 x 38u MASSACHUSETTr� STAT EXCISE TAX BARNSTABLE COUNTY 'EGISTRY OF DEEDS RELEASE Date: 06-14-2006 a 11:38am CtI`.: 997 Doc:: 37227 Fee: $171.00 Cons: WP000.00 Property Address: 810 Wakeby Road,Marstons Mills,MA I, Patricia L. Gifford,of 30 Cedar Street, Cotuit, Massachusetts for consideration paid in full consideration of Fifty Thousand and 00/100($50,000.00)Dollars Give, Grant and Release to Wakeby Road Realty Inc.,a Massachusetts Corporation,of 72 Pine Street, Hyannis,Massachusetts - All my right title and interest(if any)in and to a certain parcel of land situated on Wakeby Road in Newtown/Marstons Mills, Barnstable,Barnstable County, Massachusetts and shown on a plan of land entitled"Plan of Land in Newtown,Barnstable Mass. For Priscilla E. Maynard T. &William C. Gifford by Charles Savery Inc. Registered Engineers and Surveyors,Hyannis,Mass Scale: 1•inch= 100 feet dated August 26, 1974" and recorded with the Barnstable County Registry of Deeds in Plan Book 288, Page 75,one being marked "16.66 acres",meaning and intending to convey the property shown on the plan and any and all of my interest from any source in that property of Joseph Landers referenced by a deed recorded December 18, 1857 in Book 66,Pages 107& 108. For other title references see, inter alia, a deed from Lorenzo T. Gifford to Maynard T. Gifford and William C. Gifford(my deceased husband)recorded in Book 1350,Page 14, and a deed dated April 30, 1992 in Book 7996,Page 107 to Patricia L. Gifford;the Estate of William C. (Coleman) Gifford, Barnstable County Probate Court Docket No. 96PO23I AD-1,date of death October 18, 1991; and the Petition to Partition action filed in said Probate Court as Docket#99E-0067-PP1. By recording this deed the grantee agrees to assume any and all obligations of the grantor that relate to the premises, including but not limited to past,present or future real estate taxes,and any claims of whatever nature,past,present or future of any cotenants with regard to the grantor's ownership in the premises. BARNSTABLE COUNTY EXCISE TAX Witness my hand and seal this 14th day of June,2006 Date: 6�-14--2006taF:11:33am OF DEEDS CtIT: 497 Doct: 37227 Fee: Cons: $Soro00. o J i Patricia L. Gifford i COMMONWEALTH OF MASSACHUSETTS Barnstable,ss June 14,2006 Then personally appeared before me,the undersigned notary public,the above-named Patricia L. Gifford❑ who proved to me through satisfactory evidence of identification,which were a MV Operator's License No. 0 7 G1/ , who is known by me and to me known to be, the person whose name is signed on the preceding or attached d cument and acknowledged to me that she signed it voluntarily for its s Notary Public M co mmission omrrussion expires: ZARA WL RAMW R�,,•,,�.,�j� NOTARY Ping ,�* �fi.• -7vgEALTH OF l iR00" �. . 40 ,Ss�o�Ems eln$ BARNSTABLE REGISTRY OF DEEDS i Map Page 1 of 1 Town of Barnstable Geographic Information System New Search Home Help Parcel Viewer Custom Map Abutters Map Size ® Zoom Out In Turn map layers on/off by gym, vt ;R rs c i E). .— -- ® JPG selecting check boxes below L F. Town Boundaries = ?� ` ' r Road Names P a �� Y � > �� ,- X, I r Voter Precincts �. °p � �� 4 �>>>> Y>4�, ��; F'_ Map&Parcel Numbers �k Z�1:�^ F. Parcels x F t*vs 13 r. FEMA Q3 Flood Zones(01d Maps)Willd m 2010 be Superced �i AE(100 yr flood) . AO(100 yr flood) ��•. VE(100 yr flood w/wave action) 4: 00.(500 yr flood) `L I ONy k r Neighboring Towns Water _ \ e r Streams sr�wnr i 4. c 4 a �� tia Set Scale 1" = 1016 Aerial Photos lj MAP DISCLAIMER copyright 2005-2010 Town of Barnstable,MA All rights reserved.Send questions or comments to GIS BarnstableMA V1.2.4015 [Production] http://66.203.95.236/arcims/appgeoapp/map.aspx?propertyID=013... 1/3/2011 Map Page 1 of 1 Town of Barnstable Geographic Information System New Sear Parcel Viewer Custom Map Abutters ■■ Zoom Out"„'J",In tp m f Ja)Pr.' Map: 013 Parcel: 052 ol3o3g 1 Location: 810 WAKEBY ROAD 443 013M 1 - •` at30 i� 2t Owner: WAKEBY ROAD REALTY INC .. ��'. ��fff •:�' Oi7C10 ' nt Location Information Map&Parcel 013052 Y t2 Location 810 WAKEBY ROAD 013035 Acreage 16.66 acres 1 " 1140 ' Mailing Address WAKEBY ROAD REALTY 1 •—, .'013023 PO BOX 485 • 1131, CRESENT,GA 31304 Appraised Value(FY 2011) a, Extra Features $0 Out Buildings $0 Y,i s ' •.f � Land $414,400 Buildings $0 r Y,•, FK 0145 Total Appraised $414,400 w -. i _ 013052 3 -sled Value(FY 2011) t r y y ��•�,, y a} t Extra Features $0 y Out Buildings $0 r. ! Land $414,400 Buildings $0 Total Assessed $414,400 MAP DISCLAIMER- ---_ •• �;• t306a This map is for planning only.It is not adequate I - boundary determination Interpretation.This map 19003 t• represent an on-the-gro Enlargements beyond a 1"=100'may not meet e map accuracy standards 010004 Mtt Parcel lines on this map graphic representations tax parcels.They are no property boundaries and Set Scale 1"= 100 I April 2008 J I MAP DISCLAIMER represent accurate relati physical objects on the r Copyright 2005-2010 Town of Barnstable.MA All nghts reserved Send Questions or comments to GIS BarnstableMA v1.2.4015 [Production] http://66.203.95.236/arcims/appgeoapp/map.aspx?propertyID=013... 1/3/2011 Map Page I of 1 Town of Barnstable Geographic Information System New sear Parcel Viewer custom Map Abutters Map size ■ Zoom Out"„l„"In 7PG Map: 013 Parcel: 052 Location: 810 WAKEBY ROAD io f. g1xp= 017021` Owner: WAKEBY ROAD REALTY INC Yg : r nn atal7s Location Information 012 Map R Parcel 013052 01121 Location 810 WAKEBY ROAD ti 17M6 Acreage 16.66 acres Current Owner - 1 Mailing Address WAKEBY ROAD REALTY I PO BOX 485 4 +I CRESENT,GA 31304 •r Appraised Value(FY 2011) > - Extra Features $0 ocoo; , Out Buildings $0 x 4 Land $414,400 Buildings $0 L2 01*3M Total Appraised $414,400 W ' c •.'^• '� +,. Assessed Value(FY 2011)-- ------_. I _ Extra Features $0 _.___.. Out Buildings $0 � *.+'�aeA'•� • Land $414,400 FFii'"''B�l�Etc�II ' ►, � Buildings $0 ji - � •'- Total Assessed $414,400 FmAP DISCLAIMER This map is for planning only.It is not adequate I_ a' Y boundary determination y +, •, interpretation.This map ot0000 .a. Ls represent an on-the-gro Enlargements beyond a 40 I"=100'may not meet e f,. map accuracy standards ` Ot s Parcel lines on this map graphic representations $ ---------- - tax parcels.They are no property boundaries and Set Scale 1" =�100 I April 2008 J I MAP DISCLAIMER represent accurate relati physical objects on the r Copyright 2005.2010 Town of Barnstable.VA All rights reserved Send questions or comments to GIS BarnstableMA V1.2.4015 [Production] http://66.203.95.236/arcims/appgeoapp/map.aspx?propertyID=013... 1/3/2011 I I Map Page 1 of 1 Town of Barnstable Geographic Information System New Search i Home i Help Parcel Viewer F Custom Map Abutters Map Size [3 „ Zoom Out Turn map layers o by JPG selecting check boxes below Town Boundaries .... s. ..........................................:................... ............................................................... .........;f r. Road Names ..�4::::: r r' Voter Precincts i............iiiiiir ` 13 ::::Siaitr!eir:¢�::�:..... ... .......... a ........... : ....,...... ,. ..� .:. [� Map&Parcel Numbers r Parcels (f .......................... ... ...,....._ :.::•:':-:':'.': 17- FEMA Q3 Flood Zones(Old Maps) Will'be Superceded in 2010 , ................ AE(100 yr flood) .... .......... .................... ... 13 AO............................ ... � .: � .. 0 yr flood) 13 VE(100 yr flood w/wave action) , .............. ' ........... �. •.•�..�"�:�4�� X500(500 yr flood) , Neighboring Towns S ... Y bR............�•::.. ...,.......q'::�e:{:..:ik;..i:,.� '•;.:.' � Water 0ppjj�' K [ Streams Set Stale 1"= 1016j r__Aenal Photos MAP DISCLAIMER Copyright 2005-2010 Town of Barnstable,MA All rights reserved.Send questions or comments to GIS . BarnstableMA V1.2.4O15 [Production] http://66.203.95.236/arcims/appgeoapp/map.aspx?propertyID=013... 1/3/2011 Barnstable Assessing Search Results Page 1 of 2 k-Z ER � rec-w X' rc Home:Departments:Assessors Division:Property Assessment Search Results New Search New Interactive Maps >> Owner: 2011 Assessed Values: WAKEBY ROAD REALTY INC 810 WAKEBY ROAD 2011 Appraised Value 2011 Assessed Value Past Comparisons Map/Parcel/Parcel Extension Building Value: $0 $0 Year Total Assessed Value 013 /052/ Extra Features: $0 $0 2010-$414,400 Outbuildings: $0 $0 2009-$838,500 Mailing Address Land Value: $414.400 $414,400 2008-$243,700 WAKEBY ROAD REALTY INC 2007-$243,700 2011 Totals $414,400 $414,400 2006-$251,600 PO BOX 485 CRESENT,GA.31304 2011 REAL ESTATE Tax Information: Tax Rates: (per$1,000 of valuation) Community Preservation Act Tax $90.50 Fire District Rates Town Residential Barnstable FD-All Classes $2.31 $8.05 C.O.M.M.-All Classes $1.33 Town Commercial C.O.M.M.FD Tax(Commercial) $551.15 Cotuit FD-All Classes n/a $7.28 Hyannis-Residential $2.04 Town Tax(Commercial) $3,016.83 Hyannis-Commercial $3.24 W Barnstable-Residential $2.65 W Barnstable-Commercial $2.34 Community Preservation Act 3%of Town Tax Total: $3,658.48 Construction Details Property Sketch & ASBUILT Cards Building Construction info N/A Property Sketch Legend A sketch is not available for this parcel. Land AsBuilt Card N/A CODE 4000 Lot Size(Acres) 16.66 iew Interactive Maps >> UP Appraised Value $414,400 Assessed Value $414,400 Sales History: Owner: Sale Date Page: Sale Price: WAKEBY ROAD REALTY INC Jun 14 2007 12:OOAM 22107/2 $2,000 WAKEBY ROAD REALTY INC Jun 14 2006 12:OOAM 2 $50,000 HAYWARD,HARRIET P TR& Jan 19 2005 12:OOAM 19452/283 $0 BARNSTABLE,TOWN OF(MUN) Jun 112001 12:OOAM 13920/113 $ HAYWARD,HARRIET P TR& Mar 15 1996 12:OOAM 10105/202 $40,000 HAYWARD,HARRIET P TR Nov 15 1995 12:OOAM 9928/127 $1 GIFFORD,MAYNARD&WILLIA Oct 15 1995 12:OOAM 9897/177 $4,000 GIFFORD,MAYNARD&WILLIA Oct 15 1995 12:OOAM 98781174 $4,000 GIFFORD,MAYNARD&WILLIA Oct 15 1995 12:OOAM 98781173 $4,000 GIFFORD,MAYNARD&WILLIA 1370/386 $0 COMM ELECTRIC ESMT 6584/007 $0 Extra Building Features http://www.town.barnstable.ma.us/assessing/2011/displayparcel l I... 1/3/2011 Barnstable Assessing Search Results Page 2 of 2 Code Description Units/SO ft Appraised Value Assessed Value Property Sketch Legend BAS First Floor,Living Area FST Utility Area(Finished Interior) UAT Attic Area(Unfinished) BMT Basement Area(Unfinished) FTS Third Story Living Area(Finished) U HS Half Story(Unfinished) CAN Canopy FUS Second Story Living Area(Finished) UST Utility Area(Unfinished) FAT Attic Area(Finished) GAR Garage UTQ Three Quarters Story(Unfinished) FCP Carport GRN Greenhouse UUA Unfinished Utility Attic FEP Enclosed Porch PTO Patio UUS Full Upper 2nd Story(Unfinished) FHS Half Story(Finished) SFB Semi Finished Living Area WOK Wood Deck FOP Open or Screened in Porch TQS Three Quarters Story(Finished) http://www.town.barnstable..ma.us/assessing/2011/displayparcel l I... 1/3/2011 r Barnstable Assessing Search Results Page 1 of 2 Home:Departments:Assessors Division:Property Assessment Search Results New Search ; New Interactive Maps >> Owner: 2011 Assessed Values: WAKEBY ROAD REALTY INC 810 WAKEBY ROAD 2011 Appraised Value 2011 Assessed Value Past Comparisons Map/Parcel/Parcel Extension Building Value: $0 $0 Year Total Assessed Value 013 /052/ Extra Features: $0 $0 2010-$414,400 Outbuildings: $0 $0 2009-$838,500 Mailing Address Land Value: $414,400 $414,400 2008-$243,700 WAKEBY ROAD REALTY INC 2007-$243,700 2011 Totals $414,400 $414,400 2006-$251,600 PO BOX 485 CRESENT,GA.31304 2011 REAL ESTATE Tax Information: Tax Rates: (per$1,000 of valuation) Community Preservation Act Tax $90.50 Fire District Rates Town Residential Barnstable FD-All Classes$2.31 $8.05 C.O.M.M.-All Classes $1.33 Town Commercial C.O.M.M.FD Tax(Commercial) $551.15 Cotuit FD-All Classes n/a $7.28 Hyannis-Residential $2.04 Town Tax(Commercial) $3,016.83 Hyannis-Commercial $3.24 W Barnstable-Residential $2.65 W Barnstable-Commercial $2.34 Community Preservation Act 3%of Town Tax Total: $3,658.48 Construction Details Property Sketch & ASBUILT Cards Building Construction info N/A Property Sketch Legend A sketch is not available for this parcel. Land AsBuilt Card N/A CODE 4000 Lot Size(Acres) 16.66 R V iew Interactive Maps »� Appraised Value $414,400 Assessed Value $414,400 Sales History: Owner: Sale Date Book/Page: Sale Price: WAKEBY ROAD REALTY INC Jun 14 2007 12:OOAM 22107/259 $2,000 WAKEBY ROAD REALTY INC Jun 14 2006 12:OOAM 21095/202 $50,000 HAYWARD,HARRIET P TR& Jan 19 2005 12:OOAM 19452/283 $0 BARNSTABLE,TOWN OF(MUN) Jun 11 2001 12:OOAM 13920/113 $ HAYWARD,HARRIET P TR& Mar 15 1996 12:00AM 10105/202 $40,000 HAYWARD,HARRIET P TR Nov 15 1995 12:OOAM 9928/127 $1 GIFFORD,MAYNARD&WILLIA Oct 15 1995 12:OOAM 9897/177 $4,000 GIFFORD,MAYNARD&WILLIA Oct 151995 12:OOAM 9878/174 $4,000 GIFFORD,MAYNARD&WILLIA Oct 151995 12:OOAM 98781173 $4,000 GIFFORD,MAYNARD&WILLIA 1370/386 $0 COMM ELECTRIC ESMT 6584/007 $0 Extra Building Features http://www.town.barnstable.ma.us/assessing/2011/displayparcel l I... 1/3/2011 Barnstable Assessing Search Results Page 2 of 2 Code Description Units/SQ ft Appraised Value Assessed Value Property Sketch Legend BAS First Floor,Living Area FST Utility Area(Finished Interior) UAT Attic Area(Unfinished) BMT Basement Area(Unfinished) FTS Third Story Living Area(Finished) U HS Half Story(Unfinished) CAN Canopy F US Second Story Living Area(Finished) UST Utility Area(Unfinished) FAT Attic Area(Finished) GAR Garage UTQ Three Quarters Story(Unfinished) FCP Carport GRN Greenhouse UUA Unfinished Utility Attic FEP Enclosed Porch PTO Patio UUS Full Upper2nd Story(Unfinished) FHS Half Story(Finished) SFB Semi Finished Living Area WDK Wood Deck FOP Open or Screened in Porch TQS Three Quarters Story(Finished) http://www.town.barnstable.ma.us/assessing/2011/displayparcel l 1... 1/3/2011 Health Master Detail Page 1 of 1 Logged In As: Health Master Detail Monday, January S TOW N\miorandd 2011 Application Center Parcel Lookup Selection Items Parcel I Septic Perc I Well I Fuel Tank Parcel: 013-052 Location: 810 WAKEBY ROAD, MARSTONS MILLS Owner: WAKEBY ROAD REALTY INC Business name: Business phone: Rental property: r Deed restricted: 1] Number of bedrooms : __ ; Contaminant released: r Fuel storage tank permit: r Save Parcel Changes ( Return toLookup �� { _ --A Parcel Info Parcel ID: 013-052 Developer lot: Location:810 WAKEBY ROAD Primary frontage: 115 Secondary road: Secondary frontage: Village: MARSTONS MILLS Fire district:C-O-MM Sewer acct: Road index: 1773 Interactive map HIM— Town zone of contribution:GP (Groundwater Protection State zone of contribution:IN Overlay District) Owner Info Owner: WAKEBY ROAD REALTY INC Co-Owner: Streetl: PO BOX 485 Street2: City:CRESENT State:GA Zip: 31304 Country: Deed date:06/14/2007 Deed reference:22107/259 Land Info Acres: 16.66 Use: FACTORY Zoning: RF Neighborhood: M DL-00 CI03 Topography: Road: Utilities: Location: Construction InfolBuilding No ear Buil Gross ArealLiving Area BedroomsBathrooms Buildings value:tt0.00 Extra features: oO.00 Land value: rx414,400.00 http://issgl2/intranet/healthMaster/HealthMasterDetail.aspx?ID=O... 1/3/2011 TOWN OF BARNSTABLE COMPLIANCE: CLASS: 1. Marine,Gas Stations,Repair 2. Printers BOARD OF HEALTH 0 satisfactory 3.Auto Body Shops unsatisfactory- 4.Manufacturers COMPANYCIVVC_ � _>(51. � O (see"Orders") 5.Retail Stores `t-7 6.Fuel Suppliers ADDRESS 2<10 t la S: 1" SRN VC 7.Miscellaneous QUANTITIES AND STORAG (IN= indoors;OUT=outdoors) MAJOR MATERIALS Case lots Drums Above Tanks Underground Tanks NJ IN OUT IN OUT IN OUT #&gallons Age Test Fuels: Gasoline Jet Fuel (A) Diesel, rosene, #2 (B) Heavy Oils: waste motor oil (C) new motor oil (C) transmission/hydraulic Synthetic Organics: degreasers Miscellaneous: DISPOSAIJR.ECLAMATION REMARKS: 1. Santa wage 2.Water Supply O Sewer OPublic On-site J&Private 3. Indoor Floor Drains YES NO O Holding tank:MDC_ O Catch basin/Dry well O On-site system 4. Outdoor Surface drains:YES NO ORDERS: O Holding tank:MDC O Catch basin/Dry well O On-site system 5.Waste Transporter Narne of Hauler Destination Waste Product Licensed?, NO 2. on(s) Interviewe V Inspector Date °�TMEr°,+ti Town of Barnstable • BARNSTAMA,QaBIZ Department of Health, Safety, and Environmental Services . ,�� Public Health Division AlEDN1A'�A P.O.Box 534, Hyannis MA 02601 Office: 508-790-6265Thomas A.McKean,RS,CHO FAX: 508-790-6304 Director of Public Health } RECORD OF VERBAL COMMUNICATION PM i(n l l 1q91b 1 c 1. G.r�` ��. a�;� c,.�n� �a t,.�.�►� of r v G O <r-.nc-(t �� c L � � o g we c o ICE J Q to (( (5p8) L4 verbcomm.doc P►�C - C—ui c CAL S nC!c • _ .. III Town of Barnstable * sn MSTAB i6gq.LE 9 M^ g Department of Health, Safety, and Environmental Services �A A�0 rFOMa� Public Health Division P.O. Box 534, Hyannis MA 02601 Office: 508-862-4644 Thomas A.McKean,RS,CHO FAX: 508-790-6304 Director of Public Health November 30, 1999 Paul Taurasi, Regional Director Department of Environmental Protection Southeast Region 20 Lakeside Drive Lakeville, MA 02347 Re: Gifford Brothers Sand and Gravel, Inc. 810 Wakeby Road Marstons Mills, MA Dear Mr. Taurasi: I am writing to seek the Department's assistance in investigating possible violations of the Department's regulations regarding the recent disposal of asphalt concrete, stumps, tree branches and soil, at a sixteen-acre parcel located at 810 Wakeby Road, Marstons Mills, Massachusetts. This site is found in the town's groundwater protection overlay district and therefore, is of particular sensitivity and concern to the Board of Health. By way of brief background, the site in question as been the subject matter of litigation in the Barnstable Superior Court based on a cease and desist order issued by Building Commissioner ,prohibiting all activities on the site, except for residential use and the salvage operations, consistent with previously issued permits. After a trial held in April of 1999, the Court sustained the Zoning Board of Appeals and Building Commissioner, except for the removal of sand and gravel in a five-acre area of the property closest to Wakeby Road. The Court acknowledged that there may be no more sand and gravel to mine in that area. (The superior court decision is on appeal). It is my understanding that there has been no removal of gravel from the specified area for several years. f In addition, I am advised that the Department has been in discussions since 1997 with Christopher Keyes, the president of Gifford Brothers Sand and Gravel Inc., regarding the entry of an administrative consent order regarding the property. As far as I know, there has been no such consent decree executed. However, Mr. Keyes has raised his discussions with the Department as a justification for continuing to engage in activities which the town and now the superior court have determined are impermissible but which Mr. Keyes has claimed are required by the Department as part of a cleanup of the premises. Based upon an investigation undertaken by the Barnstable Police Department regarding continuing zoning violations on the property, the Board of Health has been made aware that broken asphalt and concrete have been disposed on the property with some frequency. Additionally, stumps, tree branches and other like materials have been brought into the property as well. (See copy of affidavit of Paul Everson enclosed herewith). No prior notice or approval was provided to or given by the Barnstable Board of Health for the commencement of these activities. Particularly because of the parcel's location in a groundwater protection overlay district, the Board requests the Department's assistance in evaluating whether the dumping of concrete and asphalt as well as stumps, brush and other materials is in conformance with the Department's regulations and state law. I look forward to discussing this matter at your earliest convenience. Sincerely, 2as A. McKean Director of Public Health MIBIT 5 COMMONWEALTH OF MASSACHUSETTS BARNSTABLE, ss: SUPERIOR COURT C.A. No. 98-87 GIFFORD BROTHERS SAND AND GRAVEL, INC., AFFIDAVIT OF Plaintiff, DETECTIVE V. PAUL EVERSON IN SUPPORT OF EMMETT F. GLYNN, RON S. JANSSON, COMPLAINT FOR GENE BURMAN, RICHARD L. BOY, GAIL CIVIL CONTEMPT. NIGHTINGHALE, ELIZABETH NILSSON, ) THOMAS A. DERIEMER, DAVID RICE, ) and KEVIN MINNIGERODE, as they are ) Members and Alternate Members of the TOWN OF BARNSTABLE ZONING ) BOARD OF APPEALS, Defendants.) I, Detective Paul Everson, being duly sworn, depose and say: 1) 1 have full knowledge of the facts stated herein and am competent to testify to these facts. 2) 1 hold the position of detective in the Barnstable Police Department. I have been employed by the Barnstable Police Department for approximately 20 years. 3) On or about September 24, 1999, 1 met with Barnstable Town Attorney Robert D. Smith concerning the Gifford Brothers Sand and Gravel, Inc. case and was asked to investigate complaints that Gifford Sand and Gravel Inc. was not complying with the Findings of Fact, Rulings of Law and Order of Judgment, dated June 25, 1999 issued in Gifford Sand and Gravel Inc. v. Zoning Board of Appeals, Town of Bamstable, Case No. 98-87. As a result of this (98A361everwnaffldavd] 1 - - 1 meeting, I conducted an investigation into the activities being undertaken at the property located at 810 Wakeby Road, Marstons Mills. 4) As part of my investigation, on or about September 25, 1999, 1 spoke with Patricia Gifford of 800 Wakeby Road, regarding the operation at the location. Patricia Gifford relayed to me a history of the property as it pertained to her family. Patricia Gifford stated that she was no longer involved in the daily operation of the property. However, she stated that she retained an ownership interest in the property. According to Mrs. Gifford, whatever business enterprises are being undertaken at the site located at 810 Wakeby Road, Marstons Mills are being initiated and run by Mr. Keyes. 5) On September 25, 1999, I also interviewed a Mr. James P. McDonough of 111 Mockingbird Lane, Marstons Mills. Mr. McDonough showed me where his property abuts the rear of 810 Wakeby Road. Mr. McDonough showed me where the property of 810 Wakeby Road had been cleared up to his property line as well as the adjacent abutters. 6) On October 12, 1999, 1 viewed the processing of what appears to be a loam pile on the 810 Wakeby Road property from the property of the McDonoughs. 7) On or about October 15, 1999, 1 observed an 18-wheel tractor trailer, Child's Trucking, South Dennis, transporting materials to the 810 Wakeby Road property. 8) On October 26, 1999: 1 again met with Patricia Gifford at her home at 800 Wakeby Road. At this time, I observed a front-end loader working just 198-00361eversonaHldavOl 2 behind the Gifford residence. The operator of the machine was actively screening and processing various piles of loam and earth, loading it into a green sifting machine, which mechanically processed this material. Patricia Gifford showed me the pile of concrete and tar dumped on the 810 Wakeby Road, Marstons Mills, MA property by Child's Trucking and Deco Trucking on October 14, 1999 and October 15, 1999. 1 also observed the Sky Frog Tree Service truck and trailer enter the premises and deposit a construction trailer. 9) On or about October 27, 1999, 1 spoke with Mr. Charles Childs, owner of Child's Trucking. I asked Mr. Childs about the dumping of debris on the property at 810 Wakeby Road. Mr. Childs, upon checking his records, reports to me that he did have a truck working a "sub-contract" for RH Construction on the dates in question. Upon contacting the driver who operated the truck on these dates, Mr. Childs confirmed that his truck did deposit materials at 810 Wakeby Road. The driver, a Mr. Warren Crooker, confirmed that he picked up three loads of concrete and tar from a Falmouth construction site and dumped them at 810 Wakeby Road, Marstons Mills. RH Construction is run by Randy Harnois. Mr. Crooker further adds that the demolition of materials came from a site on Bridge Street in Falmouth. Signed under the pains and penalties of perjury this day of November 1999. � / J Cidl� tec K e Paul Everson TowrY of Barnstable Police Department (98-00361eversonaf 1daAl 3 Sa� I sa�� 6r �� f�c �� S � �� s� b� � c�� O �r� ��-- .fir .�/�;. �1� ^- o� l.l� �� _ � !!! Cam_C� Massachusetts Department of Environmental Protection "> Bureau of Resource Protection v 1r fr " Well Completion Reports �t J Well Driller Please specify work performed: Address at well location: ............................................. ......_.. New Well Street Number: Street Name: 810 WAKEBY ROAD Please specify well type: Building Lot#: Assessor's Map#: Monitoring 013 Assessor's Lot#: ZIP Code: Number Of Wells: 052 02648 4 City/Town: Well Location BARNSTABLE In public right-of-way: GPS (GPS for the deepest well) f Yes f: No North: West: 41.66776 70.45284 Subdivision/Property/Description: Mailing Address: I click here if same as well location a d d r e s ................_......._............_.__..........................................._......_................._............................. Property Owner: Street Number: Street Name: CHRISTOPHER KEYES 485 PO BOX City/Town: State: Engineering Firm: CRESCENT GEORGIA ZIP Code: Board of health permit obtained: r Yes f Not Required Permit Number: Date Issued: Massachusetts Department of Environmental Protection Bureau of Resource Protection—Well Driller Program Well Completion Reports(Monitoring) ............... ............ .................................................................................. ................................. ........... ................. .................. ................................ .................... .................... Well Driller - Monitoring Form DRILLING METHOD Overburden Auger �edrock C ose Bedrock- WELL LOG OVERBURDEN LITHOLOGY LF ... ........... _......-.........._....._._._..........__............ _..............................-._.....................................__...................................,............._......................rom(ft) To(ft) Code Color Comment Drop in drill Extra fast or Loss or addition stem slow drill rate 1 of fluid ......._ ............... .... .. i020 Fine To Coarse San !�.Brownmmm�� - YE Fast Slow Loss Addition ( f C t 20 =[3� Fine To Coarse San :Brawn { [YES NO Fast Slow Loss Addition i..........................................................-..............!....................................._..._.............................................................................._..._....... ......._.......................................................................... ..!.......................................................... PERMIT INFORMATION DEP 21E RTN# DEP Groundwater Discharge# ADDITIONAL WELL INFORMATION Developed ( Yes f';No Are these wells nested? Yes i-No Surface Seal Type Concrete Area of group(sq.ft) 43560 Total Well Depth 32 Depth to Bedrock CASING From:2To:0 From To Type Thickness Diameter Casing above 0w 22 (P�olyv n�yl Chlodde ! Schedule 40 + j2 ground? C _ _ C - L i SCREEN No Screen ___ ..._.._ From'5 To Type i Slot Size Diameter 122 ;32 — Slotted PVC 0.010 2 WATER-BEARING ZONES .................................................................. From To Yield(gpm) i-237 ANNULAR SEAL/FILTER PACK Water From To Material 1 Weight Material 2 !Weight Batches Method Of Placement 9 al I is ) ................................. ........................................................................................................_....._...............................................................................................i............................................................................................................................................................................................ 16 .......... i22...._... Sand '' ' ChooseMatenal ( .............„ (' ........ .... _Gravity ......... .. ..., __ .. 16 22 Bentonite Chips/Pellets Choose Matenal 3 ( j (Gravity _ i _ __.; WATER LEVEL FatMeasured Static Depth BGS(ft) Flowing Rate(gpm) 10/07/2020... �23............................................................... I......_...._....................... ._............................_...I .............._.._.................................----..-.........._.._......,.........................-_......._................---........ COMMENTS Massachusetts Department of Environmental Protection - Bu reau of Resource Protection—Well Driller Program Well Completion Reports(Monitoring) WELL DRILLERS STATEMENT This well was drilled or altered under my direct supervision,according to the applicable rules and regulations,and this report is complete and accurate to the best of my knowledge. DESMOND WILLIAM Monitoring[M] Supervising Driller Signature III, DrillerURQUHART Registration# 764 THOMAS,E DESMOND WELL Date Job Complete Firm DRILLING INC. Rig Permit# 0551 i10/07/2020 NOTE:Well Completion Reports must be filed by the registered well driller within 30 days of well completion. I v pb • Y , ' as. " • f'I Y "RR � W F g r r f' qq A ' 1 ' m SITE MAP OF ASSESSOR'S MAP Oil 3 PARCEL 52 FIGURE PREPARED BY TOWN OF BARNS'TABLE F� �•.. ,k.. Y G. '�P GEOGRAPHIC C INFORMATION SYSTEMS UNIT Ak a � r a ,c a r , i 1 , 2 �c r" Tik r r• , I 4 , Y r " IU rW r. , t ti " : r a �t a rc " i' p„ 5 • 6`I f I f�l l FILE: it3.d n p g Z49�7 5 r i I VEGETATION TOPOGRAPHY AND PLANIMETRIC A INTERPRETED FROM 1989 AERIAL OVERFLIGHTS PHOTOGRAPHYAT 1I-800 MAPPED AT 1 100 PARCEL DATA DIGITIZED FROM 1 lOq, I I ENGINEERING ASSESSORS MAPS 1995 i Y H `I M41 R W. 7 I ' � ! NOTE:THE PARCEL LINES ARE ONLY GRAPHIC REPRESENTATIONS 0f PROPERTY BOUNDARIES,THEY ARE NOT TRUE LOCATIONS cmh 8-3-94 11-1 Y!p:: �.... :.. ay a 44�— l' , A °�''' E p t. STANDARD LEGEND �,•, note. not all symbols will appear on a map 41 1400 , , MARSH AREA r , „ , , , , , J III i : EDGE OF WATER •w i DIRT ROAD - , I � can r %4 DRIVEWAYS z, PARKING LOT PAVED ROAD Yid DITCHES a I k J y ` k 0 u C , " PATH TRAI L PROPERTY LINES r , ,- p If . r n .. " ; .�----- LOT A C REAGE15.85 AC� NUMBER HOUSE NUMBER ,L I I, 1� �I k rt sr 2 FOOT CONTOUR LINE , > h s v 10 FOOT CONTOUR LINE TM , X4.9 SPOT ELEVATION h, STONE WALL �F -41 , , FENCE K ...... .... : . ��.. RETAINING WALL " - r, RAIL ROAD TRACK Y <;y , TELEPHONE POLE �I to v -_- STONE E JETTY I r. _ . Y oo� _ SWIMMING POOL } ' w PORCH / DECK . . J { M : BUILDING T �- / STRUCTURES f S 1 DOCK/ PI ER J ETTY I r. ASSESSOR'S MAP BOUNDARY 1 . : . f ar �� r