HomeMy WebLinkAbout1780 MAIN ST./RTE 6A(W.BARN.) - Health 1780 Main St
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Ja�SED Siq�s ENVIRONMENTAL PROTECTION AGENCY
s. >W REGION 1—NEW ENGLAND
�3'+7 PROZF•ESO
Lynne A. Hamjian
Deputy Director
Office of Ecosystem Protection
5 Post Office Sq. Suite 100 Phone: (617)918-1601
Mail Code: OEP06-5 Fax: (617)918-0601
Boston,MA 02109-3912 hamjian.lynne@epa.gov
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' UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
OFFICE OF INSPECTOR GENERAL
290 BROADWAY
NEW YORK,NY 10001
i
November 8, 2017
a
Lynne Hamjian
Acting Division Director «L fit ti=� Y?z
Office of Ecosystem Protection
U.S. EPA, Region 1
5 Post Office Square, MC.OEP06-5
Boston, MA 02109-3912
Dear Ms. Hamjian:
The EPA Office of the Inspector General (OIG), Office of Investigations (01), New York
Field--Office has received numerous complaints from Patrick Page, private citizen, 1780 Main
Street, West Barnstable, MA 026% 508-280-7243 relative to environmental issues/concerns
with his property in the Town of Barnstable, MA (the Town). Mr. Page has had a long standing
dispute with the Town, the County, the Massachusetts Department of Environmental Protection
(MADEP), the Massachusetts Department of Transportation (MADOT), and the United States
Army Corps of Engineers (ACOE) Mr;#Page`:has�made�numerousallegatr'ons concerning a
discharge pipe on his-property that he claims is havingian:adverse effectonlas water
The EPA OIG 01 previously made a referral to your office on December 27, 20T6-,
relative to numerous issues raised by Mr. Page.The EPA OIG 01 was recently provided with
additional water test results related to Mr. Page's property. Enclosed with this referral are copies
of two Memoranda of Activity related to the receipt and review of those results.
The EPA OIG 01 has no direct nexus in the matters raised by Mr. Page. There will be no
further action taken by the EPA Office of Inspector General concerning these allegations. As the
alleged violations are outside the jurisdiction of this office, we are referring this matter to your
office for any action you deem appropriate. This letter will serve as official notice of the referral
to your office. An identical letter will be sent to the Office of Ground Water and Drinking Water,
EPA, Washington, DC. Prior to contacting Mr. Page directly, please contact this office for
important information regarding these allegations. If yoti.have any,gtiesti hs:or wish to discuss„
this matter in further detail,please contact me at,(2-12)637 3033_ f
I
Sincerely, _
Paul A. Brezins i
Resident Agent in Charge
New York Post of Duty
Enclosures
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
OFFICE OF INSPECTOR GENERAL
290 BROADWAY
NEW YORK,NY 10007
CASE #: COMP-2018-0003 CROSS REFERENCE #: COMP-2014-0153,
COMP-2016-0088
TITLE: ENVIRONMENTAL ISSUES, BARNSTABLE, MA
INTERVIEWEE (if applicable):
PREPARED BY: RAC PAUL A. BREZINSKI
MEMORANDUM OF ACTIVITY
DOCUMENT REVIEW
NARRATIVE:
On October 31, 2017, Resident Agent in Charge Paul A. Brezinski, U.S. Environmental .
Protection Agency, Office of Inspector General, Office of Investigations, 290 Broadway, Suite
1520,New York; NY completed a review of various test results provided by Ronald J. Saari,
President, Envirotech Laboratories, Inc. (ELI), 8 Jan Sebastian Drive, Unit 12, Sandwich, MA
02563. The results were sent on behalf of his client, Patrick Page, private citizen, 1780 Main
Street, West Barnstable, MA. Page previously made allegations about a discharge pipe on his
property. The following was derived in substance:
Saari sent page a letter dated September 27, 2016. Saari advised that on September 22, 2016, two
water samples were collected by ELI at the trench located on Page's property. It was noted that
the trench is an extension of the outfall pipe that is located on the property (Attachment 1, page
1). It was noted that the applicable EPA Method was 1603. A Chain of Custody Form
accompanied the report. The test results follow:
Results: E coli were detected at the bridge location: 1,900 cfull00ml.
E coli were detected at the ditch location: 140,000 efull00ml.
Comment: E coli counts are significant for sample sites.
CASE: COMP-2018-0003 INTERVIEWEE(if applicable):
DATE OF ACTIVITY: October 31, DRAFTED DATE: October 31,2017 AGENT(S): Brezinski
2017 and November 3,2017
RESTRICTED INFORMATION This report and any attachments are the property of the EPA Office of Inspector General,Office of Investigations and is
Page I of 4 loaned to your agency. It and its contents may not be reproduced or disclosed without written permission. "Phis report
contains information protected by the Privacy Act and is FOR OFFICIAL USE ONLY. Disclosure of this report to
unauthorized persons is prohibited. See 5 U.S.C.552a.
Saari sent page a second letter dated October 26, 2016. Saari advised that on September 28,
2016, two water samples were collected by ELI at the trench located on Page's property. It was
noted that the trench is an extension of the outfall pipe that is located on the property
(Attachment 1, page 4). It was noted that the applicable EPA Method was 1603. A Chain of
Custody Form accompanied the report. The test results follow:
Results: E coli were detected at the bridge location: 68,000 efull00ml.
E coli were detected at the ditch location: 1,600 cfull00ml.
Comment: E coli counts are significant for sample sites.
Saari sent page a letter dated September 18, 2017. Saari advised that on August 29, 2017, a
sample for algae was collected by ELI at the ditch located on Page's property. It was noted that
the ditch is an extension of the outfall pipe that is located on the property. The sample was
collected at the bridge location of the ditch. Saari stated "The material consists of large amounts
of filamentous bacteria." (Attachment 2, page 1).
The actual testing was conducted by Northeast Laboratories, Inc. (NLI), 129 Mill Street, Berlin,
CT 06037. The documents include a summary of the test results and a Chain of Custody Form
from ELI (Attachment 2, pages 3-4).
Saari sent page a letter dated September 12, 2017. Saari advised that on August 7,'2017, water
samples were collected by ELI at the ditch located on Page's property. It was noted that the ditch
is an extension of the outfall pipe that is located on the property. The sample was taken at the
bridge location of the ditch (Attachment 3, page 1). It was noted that the applicable EPA Method
was 200.7 (for the water sample). The test results follow:
There was found 1,800 ug/L of petroleum that most closely resembles 50w motor oil.
Also, amounts of Lead, Copper, Chromium, Aluminum, Iron, and Manganese were
detected.
Sample.for Algae Identification was taken at the ditch located at the large boulder.
Genus Aphanocapsa and Nostoc belong to the Cyanobacteria group.
The analysis of the "Petroleum Fingerprint" was conducted by R.I. Analytical (RIA), 41 Illinois
Avenue, Warwick, RI 02888. The documents included a summary of test results and chain of
custody documents. (.Attachment 3, pages 3-6) The analysis of the"Algae Identification" was
conducted by NLI. The documents included an analytical report and chain of custody documents
(Attachment 3, pages 7-9).
CASE: COMP-2018-0003 INTERVIEWEE(if applicable):
DATE OF ACTIVITY: October 31, DRAFTED DATE: October 31,2017 AGENT(S): Brezinski
2017 and November 3,2017
RESTRICTED INFORMATION This report and any attachments are the property of the EPA Office of Inspector General,Office of Investigations and is
Page 2 of 4 loaned to your agency. It and its contents may not be reproduced or disclosed without written permission. This report
contains information protected by the Privacy Act and is FOR OFFICIAL USE ONLY. Disclosure of this report to
unauthorized persons is prohibited. See 5 U.S.C.552a.
An ELI report related to sample(s) taken on August 27, 2013 of discharge pipe A located on
Page's property indicated E coli 5,000 cfu/100m1, Total Petroleum hydrocarbons 850 ug/L, C19-
C36 Aliphatics 210 ug/L, Di-n-butyl phthalate 15 ug/L. Several of the analyses were conducted
by RIA and the documents included a certificate of analysis and the test results (Attachment 4).
An ELI report related to sample(s) taken on August 1, 2013 of outfall A located on Page's
property yielded results for a"Petroleum Fingerprint". The analysis was conducted by RIA
which noted: "Fingerprint: Chromatogram best matches weathered biodiesel fuel, possibly from
vegetable oil sources."The sample type was identified as "Drinking".
Agent's Note: The attachment titles and file names were provided by Saari and not changed by
the Reporting Agent.
Attachments:
1. Trench 9-22 & 9-28-17
2. 8-29-17 outfall bact
3. 8-7-17 ditch
4. 8-13-17 discharge pipe
5. 8-1-13 outfall
CASE: COMP-2018-0003 INTERVIEWEE(if applicable):
DATE OF ACTIVITY: October 31, DRAFTED DATE: October 31,2017 AGENT(S): Brezinski
2017 and November 3,2017
RESTRICTED INFORMATION This report and any attachments are the property of the EPA Office of Inspector General,Office of Investigations and is
Page 3 of 4 loaned to your agency. It and its contents may not be reproduced or disclosed without written permission. This report
contains information protected by the Privacy Act and is FOR OFFICIAL USE ONLY. Disclosure of this report to
unauthorized persons is prohibited. See 5 U.S.C.552a.
Attachments:
1. Trench 9-22 & 9-28-17
Trench 9-22&
9-28-17.pdf
2. 8-29-17 outfall bact
8-29-17 outfall
bact.pdf
3. 8-7-17 ditch
Uj
8-7-17 ditch.pdf
4. 8-13-17 discharge pipe
8-13-17 discharge
pipe.pdf
5. 8-1-13 outfall
8-1-13 outfall.pdf
CASE: COMP-2018-0003 INTERVIEWEE(if applicable):
DATE OF ACTIVITY: October 31, DRAFTED DATE: October 31,2017 AGENT(S): Brezinski
2017 and November 3,2017
RE'STRIC'FED INFORMATION This report and any attachments are the property of the EPA Office of Inspector General,Office of Investigations and is
Page 4 of 4 loaned to your agency. It and its contents may not be reproduced or disclosed without written permission. This report
contains information protected by the Privacy Act and is FOR OFFICIAL USE ONLY. Disclosure of this report to
unauthorized persons is prohibited. See 5 U.S.C.552a.
Envir®tech Laboratodes, 8 Jan Sebastian Dr Unit 12
Sandwich, MA 02563
Inc Sandwich,
888-6460
Fax(508)888-6446
September 27,2016
Patrick Page
1780 Main Street
W. Barnstable, MA
Dear Patrick,
On September 22,2016, two water samples were collected by Envirotech Laboratories at the trench
located at 1780 Main Street West Barnstable, MA. The trench is an extension of the outfall pipe that is
located on the property.
Results: E coli were detected at the bridge location: 1,900 cfu/100ml.
E coli were detected at the ditch location: 140,000 cfu/100ml.
Comment: E coli counts are significant for sample sites.
i
Sincerely you ,
4
.�2on J. Saari �
Pre ' ent
PH:508 888 6460
rsenviro@comcast.net
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ENVIR0TECH LABORA TORIES INC.
MA CERT. NO: M MA 063
8 Jan Sebastian Drive .
Sandwich, MA 02563
(508)888-6460 1-800-339-6460
FAX(308)888-6446
Tuesday,Seplernber 27, `2016 ;
Page, Patrick
1780,Ifain D
1V Bejrnstahle, A,1
ProjectName: 1780 Main St Comments:
Project Number:
Collection Date: 09122/16 Collection Time: 14:50
Sampled By: R Saari
Lab Order Numbers TYGY-161984
Date Received: 091221.16
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Parantders Units Test Results Reportable Limits DareAnalyted Analyst ,11ed,od
E.11 coli CFU/100ML 1,900 NA 09/22/16 RS EPA 1603
4SamplrTYpe p T ,.� SamplrDate a
-,_ar a1n rS
Parameters Units Test Results Reportable Limits Dare t»niyzed tnalysl tledmrl
E soli CFU/100mL 140,000 NA 09/22/16 RS EPA 1603
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`s•ee attaches!
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Page 1 of 1
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CHAIN OF CUSTODY FORM ENVIROTECH LABS, IN
Client: Patric Page
8 Jan Sebastian Dr., Unit
Proj. No, Project Name: Ecoli
Sandwich, MA 02563 Address: 1780 Main St
I it � S (508)888-6460./1-800-339-6460
Sampler: Ron Saari/Env W. barnstable,MA 02668
FAX(508)888-6446 Phone#: 508 280 7243
Lab ID# Date Time Comp Grab Fax#:
P Sample location container Pres.
11g2& 9/22/16 (4,(1 )�,k I Analysis Requested
t E coil
Relinquished: / Oat ime
Rec eve r ERelinquished:
Date/Time
Received:
Relinquished: Da e/Time
i R ei Date/Time
Received:
Envi otech Laboratories, 8 Jan Sebastian Dr Unit 12
Sandwich, MA 02563
Inc (508) 888-6460
Fax (508) 888-6446
October 26,2016
Patrick Page
1780 Main Street
W.Barnstable, MA
Dear Patrick,
On September 28,2016,two water samples were collected by Envirotech Laboratories at the trench
located at 1780 Main Street West Barnstable, MA.The trench is an extension of the outfall pipe that is
located on the property.
Results: E coli were detected at the bridge location:68,000 cfu/1 poml.
E coli were detected at the ditch location: 1,600 cfu/100011.
Comment: E coli counts are significant for sample sites.
Sincerely yours,
Ronal Saari
Presi nt
PH:s508 888 6460
rsenviro@comcast.net i
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ENVIROTECHLABORATORIES, INC.
MA CERT. NO.: M-MA 063
8.Ian Sebastian Drive
Sandwich,MA 02563
(508)888-6460 1-800-339-6460 "
FAX(50b)888-6446
Alonday,October 03,2016
Page, Patrick
1780 Alain St
1Y Barnstable, M
ProjeclNume: Trench Comments;Project Number:
Collection Data: 09128116 Collection Time;
Sampled By: R Scrari
Lab Order Number: WIY-162032
Dale Received: 09128116
Safi p!e T�pe} Sum"!e Inte
• ,� r 09/28/16
III ... ... ... •_ ' { ;l� Y '
-- ...,.., w.,...., ._�,:..� • .,-r.. .. ... a � .. Dredge;.Badge �
Parameters Writs Tesl Resrr/ts Repvrtnb/e Lnnits Dare A1rn/nzed Ann/psl t ilelhor/p
E coli CFUr100mL 68 000
NA 09128/16 RS EPA 1603
Sau1�lc Type,� r t ��; �Sr»�rpl4g,�Tinret Srunple Datc '' r, ��
Trench B63
14 50 09/28/16 k` , Dre ge=Di- c
Parameters Units Test Results ReparluGle Linrils DrrleAnrrlpzed Analyst ,11e1/rod
E coli CFU/ OOmL 1,600 NA Os/28/16 RS EPA 1603
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Page 1 of 1
CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. Client: Patrick Page
8 Jan Sebastian Dr., Unit 12
Proj. No. Project Name: 1780 Main St W Barnstable Sandwich, MA 02563
Address: 1780 Main St
� NL(+ (508)888-6460/1-800-339-6460 W. barnstable,MA 02668
Sampler:
FAX(508)888-6446 Phone#: 508 280 7243
Fax#:
Lab ID# Date Time Comp Grab Sample location container Pres.
Analysis Requested
l NEC, ITT 0
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I Relinquis ed Date ime (,l( Recei4e
I / Reliquished: Daterrime Received:
JU -VI A 14 Z'
Refi"nquisEied: Da e�me Rec .iv d:
Relinquished: Date/Time Received:
I ,
Envirotech Laboratories, 8 Jan Sebastian Dr Unit 12
Sandwich, MA 02563
Inc (508) 888-6460
Fax (508) 888-6446
September 18,2017
Patrick Page
1780 Main Street
W.Barnstable, MA
Dear Patrick,
On August 29,2017,a sample for algae was collected by Envirotech Laboratories at the ditch located
at 1780 Main Street West Barnstable,MA.
The ditch is an extension of the outfall pipe that is located on the property.The sample was collected at
the bridge location of the ditch.
The results are attached.
The material consists of large amounts of filamentous bacteria,
Sincerely yours,
onald J. ari
President
PH: 508 8 6460
rsenvirc comcast.net
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ENVIROTECH LABORATORIES, INC.
MA CERT. NO.: 1-MA 063
8 Jan Sebastian Drive
Sandwich, BIA 02S63
(S08)88.8-6460 1-800-339-6460
FAX(.508)888-6446
Ahmilay,September 18,2017
F'nge, Patrick
17,90,d Inin S/
FP Ban isloble, A
ProjectNatne: Continents:
Project Number:
Collection Date: 08129117 Collection Time: 12.20
Sampler!BY: R Saari
Lab Order Number: TVTV-171903
Date Received: 08129117
Sample Type Smriple Trrne Sample Mfg Co»mienls
Ditch at t3ndge A 1220 08/29/17 Filamentous bacteria
Parameters Units Test Results Reportable Limits Date Anal-ed Analpst Method
Algae Identification #/ml see comment NA 09/08/17 INortheast Lab
BRI.=belom reportable lit ti s
'see attached
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Roilald J aari
. Laborat y Director
Page 1 of 1 .
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4- Northeas't
Laboratories Inc. ANALYTICAL REPORT Pa e 1 of 1.
Report To: ENVIROTECH LABORATORIES, INC.
Attn: Ronald Saari, President EMAIL ADDRESSEE: rsenviro@comcast.net.
8 Jan Sebastian Dr= Unit#12
Sandwich MA 02563
Report Date: 9/13/2017 Date Sampled: 8/29/2017
Laboratory 1D#: N1771449 Date Received: 9/06/2017
Envirotech's iD#: DW— 171903 Date Tested: 9/08/2017
MICROSCOPIC EXAMINATION: Raw Water—SITE: Ditch Bridge
ORGANISM #/ml ORGANISM #/ml ORGANISM ##/ml ORGANISM #/ml
Diatomaceae Chloro h ceae C ano h ceae Protozoa
Amphora Actinastrum Anabaena* Actinophrys
Asterionella* Arthrodesmus Anabaeno sis Amoeba
Am hiprora Ankistrodesmus A hanoca sa Arcella
Cocinodiscus Chorelta A hanizomenon* Bursaria*
C clotella* Closterium A hanothece Ceratium
C mbella Coelastrum Aulosira lCercornonas
Diatoma* Cosmarium Arthros ira IChilomonas
Frustulia Dictyos haerium* Chroococcus IChlarnydornonas
Fra ilaria Eudorina* Clathroc stis* I Codonella
Gyrosigma Elakatothrix Coelosphaerium* C tomonas*
Gom honema Gleoc stis C lindros ermum Difflugia
Melosira Micrasterias Cus idothrix Dinob on*
Meridion* Mougeotia Dact lococco sis Euglena
Navicula Pandorina* Euca sis Glenodinium*
Nitzschia Pediastrum Gleoca sa Gonium
Pleurosigma Protococcus Galucocystis Halteria
LSt
nulada Quadri ula Gloeothece Mallomonas*
hanodiscus Scenedesmus Gom hos haeria Monas
phanodiscus S haeroc stis Hydrocoleum Peridiniuin*
rella Sphaerozosma Microcystis S nura*edra Spirogyra Merismo edia Trachelomonas
Tabellaria* Staurastrum Nostoc Uro leno sis*
Tetras ora Nodularia Vorticella
Rotifera Westella Oscillatoria
Anuraea Ulothrix Pseudanabaena
As lanchna Volvox* S irulina
Brachionus Xanthidium Rivularia*
Conochilus Zygnema Xenococcus SchizoTi
Euchlanis Euastrum Crenot
Keratella
Notholca Xenococcus Miscellaneous
Pol arthra Acarina
Rotifer Anguillula
S nchaeta Miscellaneous - Bosmina
Canthocam tus *Odor
Palmella Anac stis Cyclops
Phacus Golenkinia Daphnia
Diaptomus x
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Conclusions: Total Natural Unit Count: 0 per mL F
Comments: Results are based on sample, as submitted to Northeast Laboratories, Inc. on: 8/08/2017. Large number of
filamentous bacteria noted in sample. Approved by: Laboratory Director
Northeast Laboratories,Inc. .129 Mill Street Berlin, CT 06037 wwwaielabset.corn
Telephone: 860-828-9787 Toll Free(hi State)800-826-0105 (Out of State)800-654-1230 Fat: 860-829-1050
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CT Ca•f.#PFI-OJOa SPA Cerl.#CT=024 USDA Cer1.g097G P'DA Rcg.g086650a88 CT CSL#0000624 E;
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CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. Client: Patrick Page
8 Jan Sebastian Dr., Unit 12
Proj. No. Project Name: 1780 Main St W Barnstable Sandwich, MA 02563 Address: 1780 Main St
(508)888-6460/1-800-339-6460 W. barnstable,MA 02668
Sampler: FAX (508)888-6446 Phone#: 508 280 7243
-- lFax#:
Lab ID# Date Time Comp Grab Sample location container Pres. Analysis Requested
I
Relinquish Date/Time Rece ed: Reliquished: Date/Time Received:
�1
Relinqui ed: Date/Time Received: Relinquished: Date/Time Received:
3 � s
Enviratech Laboratodes, 8 Jan Sebastian Dr Unit 12
Sandwich, MA 02563
Inc (508)888-6460
Fax (508)888-6446
September 12,2017
Patrick Page
1780 Main Street
W. Barnstable, MA
Dear Patrick,
On August 7,2017,water samples were collected by Envirotech Laboratories at the ditch located at
1780 Main Street West Barnstable,MA.
The ditch is an extension of the outfall pipe that is located on the property.The sample was collected at
the bridge location of the ditch.
The results are attached.
There was found 1,800 ug/L of petroleum that most closely resembles 50w motor oil.Also,amounts of
Lead,Copper,Chromium,Aluminum,Iron,and Manganese were detected.
Sample for Algae Identification was taken at the ditch located at the large boulder.Genus
Aphanocapsa and Nostoc belong to the Cyanobacteria group.
Sincerely yours,
onald J.S�ri
President
PH:508 88 6460
rsenviro@com cast,net
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ENVIR 0 TECH LA B ORA TORIES, INC
MACERT NO.eMMA063
8 Jan Sebastian Drive
Sandivich,MA 02563
(508)888-6460 1-800-3.39-6460
F,4V(508)888-6446
Wednesday,September 06,2017
Page, Patrick
178011ain St
IF Barnstable,All
ProjectName: Comments:
Project Number:
Collection Date: 08107117 Collection Time: 12:45
Sampled By: Saari/Envirotech
Lab Order Number: WW-171705
Date Received: 08107117
�.'Sart p, Trine � .Sm»•'te Dates. .,� .«£ M.Z x =c J.,+t 4:F �y�{ '.�.4e.�t".¢ti�..,:�.�r2, �f+c.,'*'�'�'�p��K"'+'e rs,'z"'T:
Y � � F4•• �.,�+.;a--,��i�,�� s�3 c.,g�-�..�,7�. "�a.,,�.r�COlfllftelltS�5 �7 r ' t t i.ti�.. S �: x,,.. " a .� yam;_
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Parameters Units Test Results Reportable Lindis Date Analyzed Analyst Method
Total Iron mg/L 33 0,01 08/10/17 MC EPA 200.7
Manganese mg/L 0.237 0.005 08/10/17 MC EPA 200.7
Aluminum mg/L 3.75 0.010 08/10/17 MC EPA 200.7
Barium mg/L 0.197 0.002 08/10/17 MC EPA 200.7
Chromium mg/L. 0.019 0.002 08/10/17 MC EPA 200.7
Nickel mg/L 0.009 0.005 08/10/17 MC EPA 200.7
Lead mg/L 0.037 0.006 08/10/17 MC EPA 200.7
Copper mg/L 0.024 0.003 08/10/17 MC EPA 200.7
Zinc mg/L 0.209 0.004 08/10/17 MC EPA 200.7
Petroleum Fingerprint' 1,800 08/18/17 RIA*
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BRL=below reporlabte limits
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'see anacle'd
By:
LX
Ronal J. Saai
Lab ratory Dtre for
Page 1 of 1 ;;
Page 2 of 3
R.I.Analytical Laboratories,Inc.
Laboratory Report
Envirotech Laboratories, Inc.
Work Order#:1708-17187
Project Name: 1780 MAIN STREET, W.BARNSTABLE MA
Sample Number: 001
Sample Description: WW-171705 DITCH a OUTFALL BRIDGE
Sample Type: GRAB
Sample Date/Time: 8/07/2017 @ 12:45
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
TPH �7
TPH GC/F1D 1800 ]40 ug/I SW-846 8100M 8/18/2017 12:53 CCS
Surrogate RANGE SW-84681OOM 8/18/2017 12:53 CCS
2-Fluorobiphenyl 53 40-140% SW-846 BLOOM 8/18/2017 12:53 CCS
Extraction Date SW-846351OC 8/11/2017 9:55 JBW
TPH Fingerprint=Chromatogram most closely resembles 50w motor oil.
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CHAIN OF CUSTODY FORM ENVIROTECH LABS,INC. RI Analytica;
8 Jan Sebastian Dr Unit 12 M RI 015
PWS: Project Name: 1780 Main St, W Barnstable Sandwich,MA 02563 Address 41 Illinois Avenue
(508)888-6460 Warwick,RI 02888
Sampler. R SaarUEnvirotech 1-800-339-6460 ahone# 401-737-8500
FAX(508)888-6446 Fax# 401-738-1970
Lab ID# Date Time, Comp Grab Station location DEP ID Container Pres. Sample pe Analysis requested
WW-171705 08/07/17 1246 X Ditch Ig Outfall Bridge Glass HCl Petroleum Scan
---------------
Relinauished: \�1 I DateMme,
! Race] Reiiauished: Datemme R 2 eve
Nye
Relinaulshed• j'I DatoMme Received: Relinquished; Ft M-e eco ved•
S,s
Pagel of 3
R.I. ANALYTICAL
Specialists in Environmentel Services
LABORATORY REPORT
Envirotech Laboratories, Inc. Date Received: 8/9/2017
Attn: Mr. Ron Saari Date Reported: 8/18/2017
8 Jan Sebastian Drive P.O.Number
Sandwich,MA 02563
Work Order#: 1708-17187
Project Name: 1780 MAIN STREET, W.BARNSTABLE MA
Enclosed are the analytical results-and Chain of Custody for your project referenced above. The sample(s)
were analyzed by our Warwick,RI laboratory unless noted otherwise. When applicable,indication of
sample analysis at our Hudson,MA laboratory and/or subcontracted results are noted and subcontracted
reports are enclosed in their entirety.
All samples were analyzed within the established guidelines of US EPA approved methods with all
requirements met, unless otherwise noted at the end of a given sample's analytical results or in a case
narrative.
The Detection Limit is defined as the lowest level that can be reliably achieved during routine laboratory
conditions.
i
These results only pertain to the samples submitted for this Work Order#and this report shall not be
reproduced except in its entirety.
We certify that the following results are true and accurate to the best of our knowledge, If you have
questions or-need further assistance,please-contact our Customer Service.Department.
Approved by:
Melissa A.Manamon
QA/QC Officer
b
Laboratory Certification Numbers(as applicable to sample's origin state):
Warwick RI*RI LA100033,MA M-RI015,CT PH-'0508,ME R100015,N142070,NY 11726
Hudson MA*M-MA1117,RI LA000319 K
41 Illinois Avenue,Warwick,RI 02888 www,rianalytical.com 131 Coolidge Street,Suite 105,Hudson MA01749 r
Phone:401-737-8500 Fax:401-7,38-1970. Phone:978-568,0041 Fax:978-568-0078
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CHAIN OF CUSTODY FORM ENVIROTECH LABS,INC. Client: Patrick Page r
8 Jan Sebastian Dr.,Unit 12
Proj.No. Project Name: 1780 Main St W.Bamstable Sandwich,MA 02563 Address: 1780_MaimSt
(508)888-646011-800-339-6460 W.barnstable,MA 02668
Sampler: qVV FAX(508)888-6446 Phone#: 508 280 7243
Fax#:
Lab ID:; Date 7ime/Comp Grab I Sample location container Pres. Analysis Requested
�' 1 g C; tN-c_e Petroleum Scan
' i metals
I _
Relinquis *atem -1UJRe i ed: Reliquished: Dater lore Received:
1TRelinquishe e Received: Relinquished: DatelTime Received:
II
ENVIROTECHLABORATORIES, INC.
MA CERT. NO.: M MA 063
8 Jan Sebastian Drive
Sandwich,MA 02563
(,508)888-6460 1-800-339-6460
FAX(508)888-6446
Tuesday,September 12,2017
Page, Patrick
1780 t1,1ain St
IY Barnstable,All ,
ProjeciName: 1780 Main St., W..-Barn, Comments:
Project Number: NA
Collection Date: 817117 Collection Time: 12:20
Sampled By: RS/Envirotech
Lab Order Number: WW-171706
Date Received: 08107117
a�` �`' �San ple�ype'"''�'� 'k1"Sam'�leTinei�' �.S'�°` leDate,� � ���;�.,,,,���.� �� -•�- x w�: ��.�Y ��, ��
-
Parameters Units Test Results Reportable Limits Datertnat)Ized Analprr 4lerhod
Algae Identification #/ml see attached NA 08/08/17 INortheast Lab
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BRL=below reportabl
`see attached
j
Rol ld J. Sa 1
Ldborato y irector
Page 1 of 1
i
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Northeast Laboratories, Inc. .ANALYTICAL REPORT Page 1 of 1.
Report To: ENVIROTECH LABORATORIES, INC.
Attn: Ronald Saari, President EMAIL ADDRESSEE: rsenviro@comcast.net
8 Jan Sebastian Dr= Unit#12
Sandwich MA 02563
Report Date: 8/14/2017 Date Sampled: 8/07/2017
Laborato ID#: N1771079 Date Received: 8/08/2017
Envirotech's ED#: DW— 171706 Date Tested: 8/08/2017
Raw Water—SITE: 1780 Main St. West Barnstable MA, Ditch @
MICROSCOPIC EXAMINATION: Boulder
ORGANISM #/ml ORGANISM #/ml ORGANISM #/ml ORGANISM #/ml
Diatomaceae lChlorophyceae C ano h ceae Protozoa
Am hora Actinastrum Anabaena* Actino h s
Asterionella* Arthrodesmus Anabaeno sis Amoeba
Am hi rora Ankistrodesmus A hanoca sa 1,900.. Arcella
Cocinodiscus Chorella jAphanizomenon*
Bursaria*
C clotella* Closterium A hanothece Ceratium
C mbella Coelastrum Aulosira ' Cercomonas
Diatoma* Cosmarium Arthros ira Chilomonas
Frustulia Dict os haerium* Chroococcus Chlam dorrionas
Fra ilaria Eudorina* Clathroc stis* Codonella
G rosi ma Elakatothrix Coelos haerium* C tomonas*
Gom honema Gleoc stis C lindros ermurh Difflu is
Melosira Micrasterias Gus idothrix Dinob on*
Meridion* Mou eotia Dact lococco sis Eu Jena
Navicula 15,000 Pandorina* Euca sis Glenodinium*
Nitzschia Pediastrum Gleoca sa Gonium
Pleurosi ma Protococcus Galucoc stis Haiteria
Pinnularia Quadri ula Gloeothece Mallomonas*
Ste hanodiscus Scenedesmus Gom hos haeria Monas
Ste hanodiscus S haeroc stis H drocoleum Peridinium*
Surirella S haerozosma Microc stis S nura*
lBrachionus
Spirogyra 3,900 Merismo edia Trachelomonas
ia* Staurastrum Nostoc 960 Uro leno sis*
Tetras ora Nodularia Vorticella
Westella Oscillatoria
Ulothrix 5,800 IPseudanabaena
hna Volvox* S irulina
Xanthidium Rivularia*
us Z nema Xenococcus Schizom cetes
s Euastrum Crenothrix
Keratella
Notholca Xenococcus Miscellaneous _
Pol arthra Acarina
Rotifer An uillula
S nchaeta Miscellaneous Bosmina
Canthocam tus *Odor Producin
Palmella Anac stis Cyclops
Phacus Golenkinia Daphnia
Dia tomus
Conclusions: Total Natural Unit Count: 28,000 per mL k,
Comments: Results are based on sample, as submitted to Northeast Laboratories, Inc. on: 8/08/2017 (rounded). .
c
Approved by: Laboratory Director
Northeast Laboratories,Inc. 129 Mill Street Berlin,CT 06037 N«vw.nelabsct.com a
Telephone: 860-828-9787 Toll Free(In State)800-826-0105 (Out of State) 800-654-1230 Fax: 860-829-1050
CT Cert.#PH-0404 EPA Cert.#CT-024 USDA Cert.#0976 FDA Reg.#086650488 CT CSL 90000624 F.
CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. Client: Patrick Page
8 Jan Sebastian Dr.,Unit 12
Proj.No. Project Name: 1780 Main St W Barnstable Sandwich,MA 02563 Address: 1780 Main St
(508)888-6460l1-800-339-6460 W.bamstable,MA 02668
Sampler. FAX(508)888-6446 Phone#: 508 280 7243
Fax#:
Lab ID# Date Time Comp crab Sample location container Pres. Analysis Requested
77—
G 6 i q ice° Algae ID
(specifically cyanobacteria)
Relinquish D im Jtl Rece' e : Reliquished: DatelTime Received:
Relinquished: i DateTime Received: Relinquished: DateTime Received:
I
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ENVIROTECH LABORATORIES, INC.
MA CERT. NO.: M.-MA 063
8 Jan Sebastian Drive
Swidwicb,NIA 02563
(508)888-6460 1-800-33 9-6460
FAX(508)888-6446
r FridaY,September 27, 2013
Page, Pnh•ick
l780 114ah?S1
17"/3arnstable, Al
Projec/Nante: 1780 Hwin St lY Bcnwslable Conunellis: Rain event in AM
Project Number:
Collection Date: 08127113 Collection Time: 12:05
Salnpled Bp: R Saari
Lab Order Ntrnrber: WTV-132030
Date Received: 08127113
Sn»tple T}pe''_ Sample Trme Siurple Datc:
� 2G Comments �
DrScharge Prpe A h 2:05 08127/13 T,. 4m r 5, s,, �w
- .W �-»-�u
aranrelers Unite Tect Results`~ Reportable Limits Date Analyzed Analyst Alet/rod
FEcoli
ium mg/L 11.4 1.0 08/29/13
/PAH MC 200.7
ug/L 210 os/o4I13 RIA* MADEP
ug/L None Detected oa/2s/13 RIA* MADEP
/100 5,000i-volatile Compounds ug/L 15 RS EPA 1603
*' * 09/05/131 RIA* EPA 625
Dioxin pg/L None Detected 09/16/13
Summit EPA 16136
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Page 2 of 2
R.I . ANALYTICAL Page I of 7
Specielists in Environmental Services
,
CERTIFICATE OF ANALYSIS
Envirotech Laboratories, Inc. Date Received: 8/28/2013
Attn: . Mr. Ron Saari Date Reported: 9/6/2013
8 Jan Sebastian Drive P.O. #:
Sandwich, MA 02563 Work Order#: 1308-18481
DESCRIPTION: PAGE, PATRICK
Subject sample(s) has/have been analyzed by our Warwick,R.I. laboratory with the attached results.
Reference: All parameters were analyzed by U.S. EPA approved methodologies.
The specific methodologies are listed in the methods column of the Certificate of Analysis.
Data qualifiers (if present) are explained in full at the end of a given sample's analytical results.
The Certificate of Analysis shall not be reproduced except in full, without written approval of R.I. Analytical.
Results relate only to samples submitted to the laboratory for analysis.
Test results are not blank corrected.
Certification#: RI-033, MA-RI015, CT-PH-0508, ME-RIO15
NH-253700 A& B, USDA 5-41844
F
If you have any questions regarding this work, or if we may be of further assistance,please contact 1
our customer service deimilment.
Approved b ;
r
Sharon Baker i
MIS/Data Reporting
enc: Chain of Custody z
V
1 i
t
41 Illinois Avenue,Warwick,RI 02888 131 Coolidge Street,Suite 105,Hudson,MA 01749
Phone:401.737.8500 Fax:401.738.1970 wwwAanalytical.com Phone:978.568.0041 Fax:978.568.0078
I a
Page 2 of 7
R.I. Analytical Laboratories, Inc.
CERTIFICATE OF ANALYSIS
Envirotech Laboratories;Inc.
Date Received: 8/28/2013
Work Order#: 1308-18481
Sample# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST. W.BARNSTABLE
SAMPLE TYPE: GRAB SAMPLE DATE/TIME: 8/27/2013 @ 12:05
SAMPLE DET. DATE/TIIYIE
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
TOC 15 5 mg/l SM-5310B 8/29/2013 12:45 EC
IPH
TPH GC/FID 850 100 ug/l SW846 8100M 9/4/2013 19:37 THP
Surrogate RANGE SW-846 8100 9/4/2013 19:37 Tf-
2-Fluorobiphenyl 86 40-140% SW-846 8100 9/4/2013 19:37 THP
Extraction date Extracted SW8463510 9/1/2013 10:15 RJL
PCB
Aroclor-1016 <0.5 0.5 ug/l EPA 608 9/4/2013 10:10 JEB
Aroclor-1221 <0,5 0.5 ug/l EPA 608 9/4/2013 10:10 JEB
Aroclor-1232 <0.5 0.5 ug/I EPA 608 9/4/2013 10:10 JEB
Aroclor-1242 <0.5 0.5 ug/l EPA 608 9/4/2013 10:10 JEB
Aroclor-1248 <0.5 0.5 ug/l EPA 608 9/4/2013 10:10 JEB
Aroclor-1254 <0.5 0.5 ug/l EPA 608 9/4/2013 10:10 JEB
Aroclor-1260 <0.5 0.5 ug/l EPA 608 9/4/2013 10:10 JEB
Surrogate RANGE 9/4/2013 10:10 JEB
Tetrachloro-m-aylene(TCMX) 70 30-150% EPA 608 9/4/2013 10:10 JEB
Decachlorobiphenyl 30 30-150% EPA 608 9/4/2013 10:10 JEB
Extraction date Extracted EPA 608 9/1/2013 10:15 RD.,
VPH
Unadjusted C5-C8 Aliphatics(FID) <150 150 ug/l MADEP 8/29/2013 11:38 *ET
Unadjusted C9-C12 Aliphaties(FID) <150 150 ug/1 MADEP 8/29/2013 11:38 *ET
Methyl-tert-butylethcr <1.5 1.5 ug/l MADEP 8/29/2013 11:38 *ET
Benzene <1,5 1.5 ug/I MADEP 8/29/2013 11:38
Toluene <5.0 5.0 ug/l MADEP 8/29/2013 11:38 *ET p
Ethylbenzene <5.0 5.0 ug/l MADEP 8/29/2013 11:38 *ET
m,p-Xylenc <10.0 10.0 ug/l MADEP 8/2.9/2013 11:38 *ET
o-Xylene <5.0 5.0 ug/l MADEP 8/29/2013 11:38 *ET
Naphthalene <5.0 5.0 ug/1 MADEP 8/29/2013 11:38 *ET
Adjusted C5-C8 Aliphatics(FID) <150 150 ug/l MADEP 8/29/2013 11:38 *ET
3
Adjusted C9-C12 Aliphatics(FID) <150 150 ug/1 MADEP 8/29/2013 11:38 *ET-. ..
C Momatics(PID) <100 100 ug/1 MADEP. 8/29/2013 11:38 *ET
Surrogate
te RANGE 8/29/2013 1138 *ET
2,5-Dibromotoluene(PID) 100 70-130% MADEP 8/29/2013 11:38 *ET
2,5-Dibrontotoluene(F1D) 92 70-130% MADEP 8/29/2013 11:38 *ET
EPH/PAH .
C9-C18 Aliphatics <100 100 ug/1 MADEP 9/4/2013 16:32 THP
C19-C36 Aliphatics 210 100 ug/1 MADEP 9/4/2013 16:32 THP
Cl l-C22 Aromatics <100 100 ug/l MADEP 9/4/2013 16:32 THP
TARGET PAH ANALYTES 9/4/2013 16:32 THP
Page 3 of 7
R.I. Analytical Laboratories, Inc.
CERTIFICATE OFANALYSIS
Envirotech Laboratories Llc.
Date Received: 8/28/2613
Work Order#: 1308-18481
Sample# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST. W. BARNSTABLE
SANIPLE TYPE: GRAB SAMPLE DATE/TIME: 8/27/2013 @ 12:05
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
Naphthalene <5 5 ug/l MADEP 9/4/2013 16:32 1'14I'
2-Methylnaphthalene <5 5 ug/I MADEP 9/4/2013 16:32 THY
Acenaphthylene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Acenaphtheue <5 5 ug/l MADEP 9/4/201.3 16:32 THP
Fluorene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Phenanthrene <5 5 ug/l MADEP 9/4/2U13 1632 THP
Anihracene <5 4-Ar�r41' gE4.11914 14.32 TIIP
Fluoranthene <5 5 ug/1 MADEP 9/4/2013 16:32 THP
Pyrene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Bcnzo(a)amlhracenc <5 5 ug/l MADEP 9/4/2013 16:32 THP
Chrysene <5 5 ug/1 MADEP 9/4/2013 16:32 THP
Benzo(b)fluorantliene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Benzo(k)fluoranthene <5 5' ug/l MADEP 9/4/2013 16:32 THP
Benzo(a)pyrene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Jndcno(1,2;3-cd)pyrenc <5 5 ug/i MADEP 9/4/2013 16:32 THP
Di ben•zo(a,h)amthracene <5 5 , ug/l MADEP 9/4/2013 16:32 THP
Benzo(g,h,i)perylene <5 5 uM A4ADEP 9/4/2013 16:32 THP
Extraction Surrogates RANGE 9/4/2013 16:32 THP f
5-alpha-Androstane 87 40-140% MADEP 9/4/2013 16:32 THP
Ortho-terphenyl 79 40-140% MADEP 9/4/2013 16:32 THP
Fractionation Surrogates RANGE 9/4/2013 16:32 THP
2-Fluorobiphenyl 78 40-140% MADEP 9/4/2013 16:32 THP }
2-Bromonaphthalene 63 40-140% MADEP 9/4/2013 16:32 THP
Extraction date Extracted MADEP 9/3/2013 16:37 MMM
s
Semi-Volatile Organic Compounds
Acenaphthene <5. 5 ug/l EPA 625 9/5/2013 15:11 KF
Acenaphthylene <5 5 ug/l EPA625 9/5/2013 I5:11 KF
Anthracene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Benzidine <$
5 ug/I EPA 625 9/5/2013 15:11 KF
Benzo(a)anthracene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Benzo(b)fluoranthene <5 5 ug/l EPA 625. 9/5/2013 15:11 KF
Benzo(k)fluoranthene <5 5 ug/l EPA625 9/5/2013 15:11 KF
Benzo(g,h,i)perylene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Benzo(a)pyrene <5 5 ug/l EPA625 9/5/2013 15:11 KF 1
bis(2-Chloroethyl)Ether <5 5 ug/1 EPA 625 9/5/2013 15:11 KF ! �
Bis(2-Chloroethoxy)mcthane <5 5 ug/l EPA625 9/5/2013 15:11 KF
Bis(2-chloroisoprop),l)ether <5 5 ug/l EPA625 9/5/2013 15:11 KP
Bis(2-ethylhexyl)phthalate <5 5 ug/l EPA625 9/5/2013 15:11 KF l
4-13romophcnyl phenyl ether <5 5 ug/l EPA625 9/5/2013 15:11 KF
it
Butylbenzyl phthalate <5 5 ug/) EPA625 9/5/2013 15:11 KF
2-Chioronaptlialene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
5
I
Page 4 of 7
R.I. Analytical Laboratories, Inc.
CERTIFICATE OF ANALYSIS'
Envirotech Laboratories, hie.
Date Received: 8/28/2013
Work Order#: 1308-18481
Sample# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST. W.BARNSTABLE
SAMPLE TYPE: GRAB SAMPLE DATE/TIME: 8/27/2013 a, 12:05
SAMPLE DET. DATE/TIll4E
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
4-Chlorophenyl phenyl ether <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Chrysene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Dibenzo(a,h)anthracene <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
Di-n-butyl phthalate 15 5 ug/1 EPA 625 9/5/2013 15:11 KF
1,2-Dichlorobenzene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
1,3-Dichlorobenzene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
3,Y-Dichlorobenzidine <5 5 ug/l
g/ EPA 625 9/5/2013 15:11 KF
Diethyl phthalate <5 5 ug/l EPA 625 9/5/2013 15:1 I KF
Dunethyl phtlialate <5 5 ug/l EPA 625 9/5/2013 15:11 KF
2,4-Dinitrotoluene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
2,6-Dinitrotoluene <5 5. ug/l EPA 625 9/5/2013 15:11 KF
Di-n-octyl phthalate <5 5 ug/l EPA 625 9/5/2013 15:11 KF
1,2-Diphenylhydra7ine <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Fluoranthene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Fluorene <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
Hexachlorobenzene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Hexachlorobutadiene <5 5 118/1 EPA 625 9/5/2013 15:11 KF
Hexachlorocycl open todiene <5 5 no EPA 625 9/5/2013 15:11 KF .
Hexachloroethane <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Indeno(1,2,3-ed)pyrene <5 S ug/1 EPA 625 9/5/2013 15:11 KF
Isophorone <5. 5 ugA EPA 625 9/5/2013 15:11 KF
Naphthalene <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
Nitrobenzene <5 S ug/l EPA 625 9/5/2013
I5:11 KF
N-nitrosodimet hylamino <5 5 ug/1 EPA 625 9/5l2013 I5;11 KP
N-nitrosodiphenylamine <5 5 ug/l EPA 625 . 9/5/2013 15:11 Kh
N-nilrosodi-n-propylamine <5 5 ug/l EPA 625 9/5/2013 I5:11 KF
Phenanthrene €
<5 5 ug/l EPA 625 .9/5/2013 15:11 KF i
Pyrene <5
5 ug/l EPA 625 9/5/2013 15:11 KF
1,2,4-Trichlorobenzene <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
4-Cliloro-3-methylphenol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
2-Chlorophenol <5 5 ug/l EPA 625 9/5/2013 '15:11 KF I
2,4-Dichlorophenol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF (:
2,4-Dimethylphehol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
2-Methyl-4,6-dinitrophenol <5 5 ug/l EPA 625 9/5/2013 15:11 KF.
2,4-Dinitrophenol <5 5 ug/l EPA 625 9/5/2013 15:11
2-Nitrophenol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
4.Nitrophenol <5
5 ug/1 EPA 625 .9/5/2013 15:11 ICI'. f
Pentachlorophenol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF - 4
Phenol <5 r'
5 ugn EPA 625 9/5/2013 15:11 KF .
2,4,6-1'richlorophenol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
Surrogates RANGE EPA 625 9/5/2013 15:11 KF
- r>
Page 5 of 7
R.I. Analytical Laboratories, Inc.
CERTIFICATE OF ANALYSIS
Envirotecll Laboratories, Ine.
Date Received: 8/28/2613
Work Order#: 1308-18481
Satliple# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST'. W.BARNSTABLE
SAATPLE TYPE: GRAB SAMPLE DATE/TIME: 8/27/2013 @ 12:05
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIATIT UNITS METHOD ANALYZED ANALYST
Phenol-d5 29 15-110% EPA 625 9/5/2013 15:1 J KF
2-Fluorophenol 36 15-110% EPA 625 9/5/2013 15:11 KF
2,4,6-Tribromoplienol 91 15-110% EPA 625 9/5/2013 15:11 KF
Nitrobenzene-d5 89 30-130%. EPA 625 9/5/2013 15:11 KF
2-Fluorobiphenyl 69 30-130% EPA 625 9/5/2013 ISAI KF
P-Terphenyl-dI4 85 30-130% EPA 625 9/5/2013 15:11 KF
Volatile Organic Compounds
Benzene <l 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
Bromobenzene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
Bromochloromethane <1 1 ug/J SW-846 8260B 8/31/2013 15:29 KAC
Bromodichloromethane <1 I ug/l SW-846 8260B 8/31/2013 15:29 KAC
Bromofonn <1 ] ug/1 SW-8468260B 8/31/2013 15:29 KAC
Bromomethane <5 5 ug/l SW-846 8260B 9/31/2013 15:29 KAC
n-Butylbenzene <1 I ug/l SW-846 8260B 8/31/2013 15:29 KAC
Sec-butylbenzene <1 I ug/l SW-846 8260B 813 t/2013 15:29 KAC
tert-Butyl benzene <1 I ug/l SNV-846 8260B 8/31/2.013 15:29 KAC
Carbon Tetrachloride <1 I ug/1 -SW-846 8260B 8/31/2013 15:29 KAC
Chlorobenzene <1 1 ug/l SW-846 8260B 3/31/2013 15:29 KAC
Chloroethane <5 5 ugh SW-846 8260B 8/31/2013 15:29 KAC
Chlorofonn <1 I ug/1 SW-846 8260B 8/31/2013 15:29 KAC
r
Chloromefhane <5 5 ug/l SW-846 8260B 8/31/2013 15:29 KAC
2-Chlorotoluene <1 I ug/I SW-846 8260B 8/31/2013 15:29 KAC
4-Chlorotoluene <1 I ug/l SW-846 8260B 8/31/2013 15:29 KAC
Dibromochloromethane <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
1,2-Dibromo-3-Chloropropa»c <2 2 ug/1 SW-8.46 8260B 8/31/2013 15:29 KAC r
l,2-Dibromoethmlc(EDB) <1. I ug/l SW-846 8260E 8/31/2013 15:29 KAC w
Dibromomethanc <2 2 ug/1 SW-8468260B 8/31/2013 15:29 KAC
1,2-Dichlorobenzene <1 I ug/1 SW-8468260B 8/31/2013 15:29 KAC j
1,3-Dichlorobenzene <1 1 ug/l SW-8468260B 8/31/2013 15:29 KAC
1,4-Dichlorobenzene <l. 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC R
DichlorodiJluoromethane <5 5 ug/1 SW-846 8260B 8/31/2013 15:29 KAC 4
1,1-Dichloroethane <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
1,2-Dichloroethane <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
],I-Dichloroethene <I I ug/1 SW-846 8260B 8/31/2013 15:29 KAC
cis-1,2-Dichloroethene <1 I ug/l SW-846 8260B 8/31/2013 15:29 KAC
trans-l,2-Dichloroeth,lene <2 2 u��1 SW-846 3260E 8/31/2013 15:29 KAC
1,2-Dichloropropane <1 1 ug4 SW-846 8260B 8/31/2013 15:29 KAC
1,3-Dichloropropane <I 1 ug l SW-846 8260B 8/31/2013 15:29 KAC
2,2-Dichloropropane <1 I ug/1 SW-846 8260B 8/31/2013 15:29 KAC
1,1-Dichloropropene <1 1 ug/1 SW-8468260B 8/31/2013 15:29 KAC
Ethylbenzene <l 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
k
I
Page 6 of 7
R.I. Analytical Laboratories, Inc.
CERTIFICATE OF ANALYSIS
Envirotech Laboratories, hie.
Date Received: 8/28/2613
Work Order#: 1308-18481
Sample# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST. W.BARNSTABLE
SAMPLE TYPE: GRAB SAMPLE DATE/TIME: 8/27/2013 @ 12:05
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
1-lesachlorobuladieue <I 1 ug/l SW-8468260B 8/31/2013 15:29 KAC
Lsopropylbenzcne <1 I u8/1 SW-8468260B 8/31/2013 15:29 1CAC
p-lsopropyltoluene <1 I ug/I SW-846 8260B 8/31/2013 15:29 KAC
Methylene Chloride <5 5 ug/l SW-846 8260B 8/31/2013 15:29 KAC
Naphthalene <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
n-Propylbenzene <1 I ug/
l SW-846 8260B 8/31l2013 15.29 KAC �
Slvrei e <I I
1,1,1,2-Tetrachloroethane <1 1 ug/l SW-8468260B 8/31/2013 15:29 KAC
1,1,2,2-Tetrachloroethane <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
Tetrachloroethene <1 I ug/1 SW-846 8260B 8/31/2013 15:29 KAC
Toluene <1 ] ug/l SW-846 8260B 8/31/2013 15:29 KAC
1,2,3-Trichlorobenzene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
1,2,4-Trichlorobenzene <1 1 ug/l SW-846 8260E 8/31/2013 15:29 KAC
1,1,1-Trichloroethane <1 1 ug/1 SW-8468260B 8/31/2013 , 15:29 KAC
1,1,2-Trichlorocthane <1 1 ug/l SW-8468260B 8/31/2013 15:29 KAC
Trichloroethene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
rrichloro[luoromethane <I I ug/1 SW-846 8260B 8/31/2013 15:29 KAC i
1,2,3-1'ricliloropropane <2 2 ug/l SW-846 8260E 9/31/2013 15:29 KAC j
1,2,4-Trimediy1benzene <] 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
1,3,5-Trimelhylbenzene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC e
Vinyl Chloride <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
o-Xylene <1 1 ug/l SW-846 8260B 3/31/2013 15:29 KAC
m,p-Xylene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
MTBE <2 2 ug/l SW-846 8260E 8/31/2013 15:29 KAC
Acetone <10 10 ug/l SW-846 8260B 8/31/2013 15:29 KAC
Surrogates RANGE SW-846 8260B 8/31/2013 15:29 KAC
Dibromofluoromethane 107 86-118% SW-846 8260B 8/31/2013 15:29 KAC
Toluene-d8 97 88-110% SW-846 8260B 8/31/2013 15:29 KAC
4-Bromofluorobenzene 94 86-115% SW-846 8260B 8/31/2013 15:29 KAC a
1,2 Dichloroethanc-d4 97 80-120% SW-846 8260B 8/31/2013 15:29 KAC
i
Total Metals
Mercury <0.0005 0.0005 mg/1 EPA 245.1 8/30/2013 9:31 YJC w
Mercury Digestion EPA 245.1 8/30/2013 9:12 JL
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Page 7 of 7
R.I. Analytical Laboratories,Inc.
CERTIF'ICArE OF'ANALYSIS
Envirotech Laboratories,Inc.
Date Received: 8/28/2013
Work Ordet•#: 1308-18481
VPH method was analyzed by a subcontracted laboratory,ESS Laboratory.
A.II QA/QC procedures required by the EPH Method were followed.
All Performance/Acceptance Standards for the required QA/QC procedures were achieved or
othei"vise stated.
No significant modifications were made to the EPH Method.
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ENVIR O TECH LABORA TORIES, INC.
MA CERT. NO.: lid-MA 063
8 Jan Sebastian Drive
Sandwich,MA 02563.
(508)888-6460 1-800-339-6460
FAX(508)888-6446
Wednesday,September 18,1013
Page, Patrick
1780 Alain St
1•J�13arnslahle, A,1
ProjectName: 1780 Main Streel Continents:
Project Number.
Collection Date: 08101113 Collection Time: NA
Sampled By: P. Page
Lab Order Number: WTv-131905
Dale Received: 08115113
Sample Type: Spniple Tirue Sntirp/ Dnl ee Coiinterr/s
Outfall. A 08/09/13
Parameters Units Test Results Reportable Limits Dare Analyzed Analyst A4erhod
Petroleum Fingerprint" See Attached 08/23/13 RIA'
i
i t
r
BRL=below reportable limits
*see attached
J P,611ald J. Iri
Laborato Director
Page 1 of 1
f
Page 2 of 2
R.I.Analytical Laboratories; Inc.
CERTIFICATE OFANALYSIS
III
Enviroteeb Laboratories,Inc.
Date Received: 8/20/2013
Work Order 4: 1308-1.7844
Sample# 001
SAMPLE DESCRIPTION: WW-131905 OUTFALL
SAMPLE TYPE: GRAD SAMPLE DATE/TIME: 8/01/2013
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
TPH
TPH GUM 450 - 110 ug/1 SW846 8100M 8/2YNN 16:45 TRIP
Surrogate RANG13 SW-846 8100 8/23/20.13 16:45 THP
2-Fluorobiphenyl 66 40-140% SW-846 8100 8/23/2013 16:45 THP
Extraction date Extracted SW846 3510 8/22/2013 21:00 IviN1M
The sample was received at the laboratory outside of the recommended hold time for the TPH analysis.
Fingerprint:Chromatogram best matches weathered biodiesel fuel,possibly from vegetable oil sources.
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CHAIN OF CUSTODY FORM ENVIIaOTECIi LABS, INC.
RI Analytical
8 Jan Sebastian Dr Unit 12 M Ri 015
PWS: Project Name: Sandwich,MA 02563 Address 41 Illinois Avenue
(508)888-6460 Warwick, RI 02888
Sampler: P. Page 1-800-339-6460 Phone# 401-737-8500
FAX(508)808-6446 Fax# 401-738-1970
Lab ID# Date Time Comp Grab Station location DEP ID Container Pres. Sample p type Analysis requested
WW-131905 0801113. NA X Outfall Glass H2SO4 Drinking Petroleum Fingerprint
------------------
Reifn uiahed: DateMrne Received: Reliauished: DateMme
Received:
In u hed
Gm` Rceived• Relinquished: bate/time ' Received:
�J Lam' �i... �/Ww•
CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC.
Client: C ices
8 Jan Sebastian Dr., Unit 12
Proj. No. Project Name:
+ U , Sandwich, MA 02563 Address: o d sPark
(508)888-6460/1-800-3 6460
Sampler: el N e A 02031
FAX(50B)888-6446
Phone#: ;
Fax#:
Lab ID# Date_„ - Time Comp Grab _ Sample location container Pres,
Qv_13iR6� g�� l3 Analysis Requested
I
Relinquished: DatelT'me
Receive Reliquished: DateTme
/5 )3 - Received:
Relinquished: DafeTime � —
Received: Relinquished: DateTme
Received:
Town of Barnstable
�oF114e t � Town Council
367 Main Street,Village of Hyannis,MA 02601
508-862-4738 • 508-862-4770 g® 4`uv\
BARNSTABLE, * E-mail: council@town.barnstable.ma.us W bitim�
MASS. www.town.barnstable.ma.us
i639• 1�
ArEpMp�a�
Councillors:
October 12, 2016
Jessica Rapp Grassetti
President Dr. Paul Canniff, DMD
Precinct 7
Eric R.Steinhilber Chair, Barnstable Board of Health
Vice President 200 Main Street
Precinct 2 Hyannis, MA 02601
John G.Flores Dear Dr. Canniff.
Precinct 1
Paul Hebert Precinct 3 q The Barns requested p
Barnstable Town Council has re ted that the enclosed report from Envirotech
Frederick Chirigotis Laboratories , Inc. dated September 22, 2016 be sent to the Board of Health. It was presented by
Precinct 4 Mr. Patrick Page to the Town Council at its October 6, 2016 meeting.
James H.Crocker Jr.
Precinct 5 Thank you for your consideration.
William Crocker Jr.
Precinct 6 Sl eerel ,
Dr.Debra S.Dagwan
Precinct 8 nthia Love 1
James M.Tinsley Administrator,
Precinct 9 Barnstable Town Council
Sara Cushing
Precinct 10
Enc.
Philip Wallace
Precinct 11
John T.Norman
Precinct 12
Jennifer L.Cullum
Precinct 13
Admnustrator:
Cynthia A.Lovell
Administrative Ad 9T&tiT 130
Assistant:
Kelly Crahan
232' 2
f�
yi. Hamblin dated pebruary 21, 1927 recorded with Barnstable Deeds Book
440 page 33'.-Said promisee are conveyed subject to a mortgage for
$1000000 held by the�{�ellflsat Savings Bank and takes for current year.
Witness my hand and gaal�thia s_ ixth day
,o September 1997
iota H. King (TA)
pommon:jo,m
alt .o Maeeaohusattah
Suffolk ea. Boston, Sp 1987 Thou personally appeared the
above-named John He King and sokaowledged the foregoing instrument to
be his free act and deed, before me
j J Ralph WellMan Justice of the Paaoe
yj commission expires 1%y 8 1930
Barnstable, no. Received September 13, 19E7 and is recorded.
IO'oW all-Men by these preaente, That I Victor-beeman,-being mevried,-
and of Barnstable, in the County of Barnstable and Commonwealth of
Maesaohusette, for myself, my heirs, exeoutora, administrators and
V� aeaigns, in consideration of the gum of one Dollar paid by the Common-
wealth of Massachusetts, through its Department of public Works, astob-
jIlahed under the provisions of Chapter 16 of the General Laws and acts
in amendment thereof and in addition thereto, the receipt whereof Is
n
hereby acknowledged, do hereby grant unto the acid Commonwealth of
Massachusetts and its assigns forever the right .to discharge into an •
Jexisting ditch upon my land, situated on the north-westerly side of
the proposed State highway in the town of Barnstable, water from a
�j drainage system to be oonatruated within the limits of eaid highway
between about stations 179.60 and 1934,00, to carry water away from
said highway and over and through my land above described, for public
convenience and for the proper construction and ogre of said highway,
and to enter upon my land at-any time for the purpose of constructing,
repairing and maintaining said drainage system and an outlet bhereof,
under the provisions of Section 4, Chapter 83 of the General jaws and
note in amendment thereof and in addition thereto; the proposed looation
�.!J of eaid drainage system and outlet being as shown on plan drawn by
J
Ar W. Dean, Chief gnginear, dated Aug. 31, 19U, and entitled: 01The
Commonwealth of Massachusetts, Department of public Works. Town of
Barnstable Plan of proposed Drainage System and outlet About Sta.
179t80 on the proposed State Highway, Scale: 40 feat to the inch e
certified copy of which is,to be recorded herewith. And for the oon-
sidoration aforesaid, I do ocoept said gum in full payment of said
easement and for myself and my hairs, executors, administratore and •
assigns do hereby release the eaid Commonwealth Of Massachusetts and
herearte
all other persona from all damages. that,have arisen or may^ar ao ty
reason of the construction of eaid.draivage system and the carrying Of
o ,
T , •_ . . •. .. 233
water away from the said highway and over or through any of the land here-
• inbefore desoribed. And I do hereby, for myself and my heirs, executors, ;
administrators and assigns covenant with the grantee and its assigns
that I am lawfully seined in fee simple of the granted premises, and
that I have good right to grant the within described easement. And, I,
acpemia Leeman, wife of said grantor, release to said grantee all rights
of curtsey, dower and homestead and other interests therein. In Witne88
Whereof, we bareunto set our hands and goals this let day of September
in the year nineteen hundred and twenty-seven-
victor Leeman (13)
Eapemia Leeman
The Commonwealth of gaseachoo tte
Barnstable as. Sept 1- 1927, Then personally appeared the above-named
Victor Leeman and aoknowl.edged the foregoing instrument to be his free
act and deed. Before me,
W. Nowell Wade Justioe of the Peace.
W Commiseion Expires may 4- 1928
Barnstable, Be. Received September 13', 1927 and is reoorded.
2pnox all Lien by these Presents, that Y John Loki. Doing married, and of--- --
Barnstable, in the County of Barnstable and Commonwealth of M84achuaette,
for myself my heirs, executors, administrators and assigns, in ooneid-
• oration of the snm of One MUM paid by the Commomwealth of Liaasachu-
setts, through its Department of Public Worka; eatabliehed undei the
��provieiong of chapter 16 of the General Laws and note 132 amendment
1 ry thereof and in addition thereto, the reoeipt whereof in hereby so)mowl-
edged, do hereby grant unto the said Commonwealth of Masachueette and
its assigns forever.the right to discharge into an existing ditch upon
jmy land, situated on,the north-weeterly aide of the proposed State
highway in the town of Barnstable, water from a drainage system to be
' oonstruote4 within the limits of said highway between about stations
179e80 and 193f00. to oarry water away from said highway and over and
\f `� through my land above described, for public convenience and for the
proper construction and care of said highway, and to enter upon my land
at say time for the purpose of constructing,.repairing and maintaining
eaid drainage system and an outlet thereof, under the provisions of
Section 4, Chapter 83 of the General jAwe and note in amendment thereof
=4 is addition thereto; the proposed location Of 6414 drainage system '
and outlet being an shown on plan drawn by A. W. Dean, 0410f Engineer,
dated Aug. 31, 1927, and entitled: "The commonwealth of NAaaachusette.
. Department of Public Wor):a. Sown of Barnstable plan of proposed Drainage
System and Outlet about Sta. 179t80 on the propose4 State Highway. Scaler
40 feet to the ingh " a certified copy of which is to be recorded here-
with. And for tha oonaiderstion aforesaid, I do accept amid sum in fu11
L •
I
10
t34
payment of said easement and for myself and my heirs, executors, admin-
ietratore and assigns do hereby release the said Commonwealth of Haaaa- •
ohusette and all other persona from all damages that have arisen or
may hereafter arise by reason of the construction of said drainage
system and the carrying of water away from said highway and over or
through any of the land hereinbefore described. And I do hereby, for
myself and my heirs, executors, administrators and assigns covenant
with the grantee and its assigns that I am lawfully seised in tee
simple of the granted premises, and that I have good right to grant
the within described easement. And, I, Johnna $ski wife of said
grantor, release to said grantee all rights of curtsey, dower and
homestead and other intereata therein. In Witness Whereof, we hereunto
set our hands and seals this let day of Sept in the year nineteen
hundre4 and twenty-seven.
John Maki. (KS)
Johnny Haki c�•�a)
The Commonwealth of ]4assa0husetts
Barnstable us. Sept 1- 19g7, Then personally appeared the above-named
John Uaki and acknowledged the foregoing instrument to be his free act
and deed. Before me,
W. Newell Wads Juetioe of the Peace.
My Commission Expires May 4- 1928
Barnstable, ea. Reoeived September 13, 1927 and is reoorded.
y -
X, Jessie-G+-B000aokof Boaton, Suffolk County, being
unmarried, for ooneideration paid, grant to Killian P. Butterfield of
177 St. Botolph St Boston Uaae. with %uitolaim covenants the land in
Eastham in Barnstable County itaeeaohueetto at North Eastham bounded
V and described as follows:- On the north by my other land 318 feet; on
4,th* east by my other land.293 feet; on the south by land of the heirs
'i of Isaiah H Horton 321 feet and on the west by the State Highway B50
feet and containing an area of 0ne'andl99/100 acres be the•eame more
p or leas, all as shown on a "Plan of 1,ana in Eastham scalee.100 :root to
an inch from the office of A. L. Sparrow So+ r_ sans Aug. 1927" to be
' filed herewith, to whloh reference may be made,�granted premises are
a part of the land conveyed to me by deed of Oraog•w. Doyle, Trustee,
dated October 1, 1918 and recorded with Barnet#b(le County Deeds in
Book 365 page 115. Witness my hand and seal.-hie twelfth day of
September 1987.
Jessie G• Booaoak (YiS) ,
Commonwealth of Massachusetta
Barnstable as. September 12, 1927• Then personally appeared the above-
named Jessie G. B00000k and acknowledged the foregoing inetxuwent to
be her free act and deed, before me
John H. Paine Justice of the peace
My oommieaion expires Oct. 23 1930.
THE COMMONWEALTH OF MABekACHU9ETT8
vzpAraTMFNr OF'PUBLIC W04116
TOWN. OF'-BARNSTABLE "
R=Z Of Phoposed DrnirZotge sum.arLd Outlet
ABOUT STA.179+eO ON THE: P20POSED STATE H01WAY
• J�tE:4D FLCt"t0 TTi t►r!i
AUI9.31,WZ7. /c'�//1
VICT02 LEEMAN i t
IDI{
> *
poi ►1p�
`, �+RPe ;yi��•'�,,.,re-..,��+T-3rp ��e�,�r�----- I` � �.. ape - �� '..
�HN MAKI
t -e;- G.�1
lHT;L7 Fr
t�
i t ELL +
ce+c:
.� tw 'X1 ;'i2 e k 2 P{• ca+5r. /Y'Hp7 cbtct. �
/ i2 Plpr /2 PZ-.� L �e -- ,'Is- .p�2-o-_---^- �2---
`� iei tt�2 as 'teA tas r♦ 166 tar tet3vY :,►�9 ��i90 t91 t i
Fr' i py
f t - I r-pe eldispe \o'r/o'Rpe �i0'Ftpo�,�p�i rb�_- = b
Skeith showing corr+plfOe drainage sgdterr?,
•Z' t�'^L, . . ,y^V;•• a., _ - .r ..�.y, -. _- .. ,.;:L�Li_. - , _ - :v
• �' .n �r' 'ja- YY,c�.• .r ' r
- - - - +%:'i�..- i Nr Ohl..-.•e*•':; ;��
+•�.. :l�]?. J'el"•_ - ''1 I vile':.: �� +'-!:+`y':!ir`• - '�it7:•t L4 ..F..:.T= .1~!� = y�� •, '3. �f '+ ."��4• _
_.r ':%r? .'a_ _:fwr,3•r -' ��• .. '.+ttTn. a�.7s-w �rt ..., r:- - - =i.. �i`+( a.-:' i -
7i
F-�6'1 T' \
ElM L ibomhNieS, 8 Jan Sebastian Dr Unit 12 !
Sandwich, MA 02563
Inc (508)888-6460
Fax(508)888-6446
September 27,2016
Patrick Page
1780 Main Street
W. Barnstable, MA
Dear Patrick,
On September 22,2016,two water samples were collected by Envirotech Laboratories at the trench
located at 1780 Main Street West Barnstable,MA.The trench is an extension of the outfall pipe that is
located on the property.
Results:E coli were detected at the bridge location: 1,900 cfu/100m1.
E coli were detected at the ditch location: 140,000 cfu/100m1.
Comment E coli counts are significant for sample sites.
Sincerely yo
on J.Saari
Pre ' ent
PH:508 888 6460
rsenvim@comcast.net
i
ENVIROTECH LABORATORIES, INC.
MA CERT. NO.: M-MA 063
8 Jan Sebastian Drive
Sandwich,MA 02563
(508)888-6460 1-800-339-6460 "
FAX(508)888-6446
Tuesday,September 27,2016
Page,Patrick
1780 Main St
W Barnstable,M
ProjedName: 1780 Main St Comments:
Project Number:
Collection Date: 09122116 Collection 27me: 14:50
Sampled By: R Saari
Lab Order Number: War-161984
Dale Received: 09122116
F
Saar �'L?e Sarnpit-Time Sar+ ile 1�de Causmeasis 77
t '
4 `
T-
i a 45 09122I16
Trench_et 6ndge,±A ,:, ,; .:.: _ _•;' .. ,
Parameters Units Teo RGu1Ls Reportable Litadi s OaueAnaly<ed Anal4w ,1lahod
E coli (CFU/100/^mL 1,900]-]\ NA 09/2211116 RS EPA 1603
Parameters t�nicr TestResulis Reportable Limit nafi.lral�.ed anal}n nrz d y
E coii CFU/100mL 140,000 NA o9n2+16 RS EPA 1503
BRL=below reportable limits
4tee aKached
Ronald J. Saari
LaboratorJ !)' ector Page 1 of 1
CHAIN OF CUSTODY FORM ENVIRCTECH LABS, IN Client: Patrick Rage
8 Jan Sebastian Dr., Unit
Proj. No. Project Name: Ecoli Sandwich, MA 02563 Address: 1780 Main St
It S (508).888-6460/1-800-339-6460 W. barnstable,MA.02668
Sampler: Ron Saari/Env FAX (6:08)888-6446 Phone#: 508 280 7243
Fax#:
Lab ID# Date Time Comp Grab Sample location container Pres. Analysis Requested
' c4� 9/22/16 t�tgl yrze�iL Vf E coli
Relinquished: Date/Time, Received: Reliquished: DaterTime Received:
Relinquished: Date rime Received: Relinquished: Dater rime Received:
Official Website of The Town of Barnstable - Property Lookup Page 1 of 4
Select Language(v
Assessing Division Property Lookup Results - 2016
367 Main Street,Hyannis,MA.02601
BACK TO SEARCH<< Print Friendly
Owner Information-Map/Block/Lot:217/004/-Use Code:1010
Owner
Owner Name as of SAUNDERS,JANE D Map/Block/Lot GIS MAPS
1/1/15 1780 ROUTE 6A 217/004/
Property Address
WEST BARNSTABLE,MA. 1780 MAIN ST./RTE 6A(W.BARN.)
02668
Co-Owner Name
Village:West Barnstable
Town Sewer At Address:No
GIS Zoning Value:RF
Assessed Values 2016-Map/Block/Lot:217/0041-Use Code: 1010
2016 Appraised Value2016 Assessed Value Past Comparisons
Building $66,900 $66,900 Year Total Assessed
Value: Value
Extra $23,200 $23,200 2015-$276,100
Features: 2014-$276,200
2013-$280,500
Outbuildings:$2,400 $2,400 2012-$299,200
2011-$300,600
Land Value: $177,700 $177,700
2010-$392,400
2009-$394,000
2008-$430,200
2016 Totals $270,200 $270,200
2007-$448,000
Residential Exemption Received=$90,000
Tax Information 2016-Map/Block/Lot:217/004/-Use Code:1010
Taxes
W.Barnstable FD Tax $724.14
(Residential) Fiscal Year 2016 TAX RATES HERE
Community Preservation $50.33
Act Tax
Town Tax(Residential) $
1,677.66
$
2,462.13
http://www.townofbamstable.us/Assessing/propertydisplaysc.reenl 6.asp?ap=O&searchpar... 10/14/2016
Official Website of The Town of Barnstable - Property Lookup Page 2 of 4
Sales History-Map/Block/Lot:217/004/-Use Code: 1010
History:
Owner: Sale Date Book/Page: Sale Price:
I SAUNDERS,JANE D 1989-07-05 6797/163 $145000
1 WEBER,ROBERT A&BARBARA D 1987-05-04 5700/346 $0
1
I WEBER,ROBERT A&MARTHA J&BARBARA D1960-01-01. 1086/348 $0 I
(I Photos 217/004/-Use Code:1010 ---------�
Sketches-Map/Block/lot:217/0041-Use Code:1010
2
! WDK" FTQ
p ,,FER" 1� z.410
20rr 10'
1FH91 �.
BMi
�0*
AS Built Cards:Click card#to view:Card#1
Constructions Details-Map/Block/Lot:217 1 004/-Use Code: 1010
Building Details Land
Building value $66,900 Bedrooms 2 Bedrooms USE CODE 1010
Replacement Cost $111,553 Bathrooms 1 Full-0 Half Lot Size(Acres) 3.16
Model Residential Total Rooms 5 Rooms Appraised $177,700
Value
Style Cape Cod Heat Fuel Oil Assessed $
Value 177,700
Grade Average Heat Type Hot Water
Year Built 1935 AC Type None
Effective 40 Interior Floors Hardwood
depreciation
Stories 1 1/2 Interior Walls Plastered
Stories
Living Area sq/ft 990 Exterior Walls Wood Shingle
Gross Area sq/ft 2,480 Roof Gable/Hip
Structure
Roof Cover
http://www.townofbamstable.us/Assessing/propertydisplayscreenl 6.asp?ap=0&searchpar... 10/14/2016
Official Website of The Town of Barnstable - Property Lookup Page 3 of 4
Asph/F
GIs/Cmp
Outbuildings&Extra Features-Map/Block/Lot:217/004/-Use Code:1010
Code Description Units/SO ft Appraised Value Assessed Value
FEP Enclosed porch- 200 $7,000 $7,000
roof,ceiling
BMT Basement- 660 $12,900 $12,900
Unfinished
PAT1 Patio-Average 100 $600 $600
FPL2 Fireplace 1.5 1 $3,300 $3,300
I
stories
WDCK Wood Decking 200 $1,800 $1,800
w/railings
Sketch Legend
Property Sketch Legend
62N Bam-any 2nd story area FPC Open Porch Concrete Floor REF Reference Only
BAS First Floor,Living Area FTS Third Story Living Area(Finished) SOL Solarium
BMT Basement Area(Unfinished)FUS Second Story Living Area SPE Pool Enclosure
(Finished)
BRN Barn GAR Garage TQS Three Quarters Story(Finished)
CAN Canopy GAZ Gazebo UAT Attic Area(Unfinished)
CLP Loading Platform GRN Greenhouse UHS Half Story(Unfinished)
FAT Attic Area(Finished) GXT Garage Extension Front UST Utility Area(Unfinished)
FCP Carport KEN Kennel UTQ Three Quarters Story
(Unfinished)
FEP Enclosed Porch MZ1 Mezzanine,Unfinished UUA Unfinished Utility Attic
FHS Half Story(Finished) PRG Pergola UUS Full Upper 2nd Story
(Unfinished)
FOP Open or Screened in Porch PRT Portico WDK Wood Deck
PTO Patio
` Print Friendly
I
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i
f Director of Assessing
!Jeffrey Rudziak
1
`P 508-862-4022
I
F 508-862-4722
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Assessing Division Property Lookup Results - 2016
367 Main Street,Hyannis,MA.02601
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Owner Information-Map/Block/Lot:217/031/-Use Code: 1300
Owner
Owner Name as of PAGE,PATRICK F TR Map/Block/Lot GIS MAPS
1/1115 1780 MAIN ST/ROUTE 6A 217/031/
Property Address
WEST BARNSTABLE,MA. 21 BUTTON WOOD LANE
02668
Co-Owner Name JDS REALTY TRUST
Village:West Barnstable
Town Sewer At Address:No
GIS Zoning Value:RF
Assessed Values 2016-Map/Block/Lot:217/031/-Use Code:1300
2016 Appraised Value2016 Assessed Value Past Comparisons
Building $0 $0 Year Total Assessed
Value: Value
Extra $0 $0 2015-$154,500
Features: 2014-$154,500
2013-$160,700
Outbuildings:$0 $0 2012-$154,500
2011 -$154,500
Land Value: $155,300 $155,300
2010-$290,500
2009-$163,900
2008-$170,900
2016 Totals $155,300 $155,300
2007-$170,900
I Tax Information 2016-Map/Block/Lot:217 1 031/-Use Code:1300'
Taxes
f W.Barnstable FD Tax $416.20
(Residential) Fiscal Year 2016 TAX RATES HERE
Community Preservation $43.38
Act Tax I
I
j Town Tax(Residential) $
1,445.84
$
1,905.42
Sales History-Map/Block/Lot:217/031/-Use Code:1300
http://www.townofbarnstable.us/Assessing/propertydisplayscreenl6.asp?ap=0&searchpar... 10/14/2016
Official Website of The Town of Barnstable - Property Lookup Page 2 of 3
History:
Owner: Sale Date Book/Page: Sale Price:
PAGE,PATRICK F TR 2002-04-04 15016/164 $15000
FOLLETT,HELENA C 1981-07-13 3322151 $0
Photos 217/0311-Use Code: 1300
There are not any photos for this parcel _
_ I
Sketches-Map/Block/Lot:217/031/-Use Code:1300
i
A sketch is not available for this parcel.
AsBuilt Card N/A
Constructions Details-Map/Block/Lot:217/031/-Use Code:1300
Land
USE CODE 1300
Lot Size(Acres) 0.97
1 Appraised Value $155,300
Assessed Value $155,300
Construction details are not available for this parcel.
I Outbuildings&Extra Features-Map/Block/Lot:217/031/-Use Code:1300
There are not any extra building features on record at this time. i
Sketch Legend
Property Sketch Legend
B2N Barn-any 2nd story area FPC Open Porch Concrete Floor REF Reference Only
BAS First Floor,Living Area FTS Third Story Living Area(Finished) SOL Solarium
BMT Basement Area(Unfinished)FUS Second Story Living Area SPE Pool Enclosure
(Finished)
BRN Barn GAR Garage TQS Three Quarters Story(Finished)
CAN Canopy GAZ Gazebo UAT Attic Area(Unfinished)
CLP Loading Platform GRN Greenhouse UHS Half Story(Unfinished)
FAT Attic Area(Finished) GXT Garage Extension Front UST Utility Area(Unfinished)
FCP Carport KEN Kennel UTQ Three Quarters Story
(Unfinished)
FEP Enclosed Porch MZ1 Mezzanine,Unfinished UUA Unfinished Utility Attic
FHS Half Story(Finished) PRG Pergola UUS Full Upper 2nd Story
(Unfinished)
IFOP Open or Screened in Porch PRT Portico WDK Wood Deck
PTO Patio
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i
Official Website of The Town of Barnstable - Property Lookup Page 3 of 3
� u
iContact
!Director of Assessing
iJeffrey Rudiiak
1P 508-862-4022
F 508-862-4722
8:30a.m.to 4:30p.m.
Helpful Links to
'Downloads
I Abatements
SALES LISTINGS
I
Barnstable FD
Residential
C.O.M.M FD Residential
Commercial-Industrial-
Mixed Use
1
Cotuit FD Residential
Hyannis FD Residential ;
Townwide Condominium i
W.Barnstable FD #
Residential
r
Department of Revenue
Exemptions
Parcel Consolidation
x
Questions about values
i
Town Tax Rates i
Town Land Use Codes
;Helpful Maps
r
All Town Maps s
Flood Insurance Maps
i Property Maps
r b The Town of Barnstable-Information Technolo
Owned and Operated y ov
Home Departments&Services I Boards&Committees I Residents&Visitors I Doing Business I Town
Calendar I Phone Directory I Employment I Email Town Hall
http://www.townofbamstable.us/Assessing/propertydisplayscreenl 6.asp?ap=0&searchpar... 10/14/2016
_ . - . ,�... . • 4- it
. . !O !iYMZ1.
03/26/2013® o ®0 7.2 5!
} ZIP 02109
® 041PV11127900E
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0AIM:!C[-A-0V UNITED STATES C)"04 I�
ENVIRONMENTAL PROTECTION AGENCY
'
REGION 1
5 POST OFFICE SQUARE
SUITE 100
BOSTON,MASSACHUSETTS 02109-3912
OFFICIAL BUSINESS
PENALTY FOR PRIVATE USE,$300
AN EQUAL.OPPORTUNITY EMPLOYER r "
Thomas A. McKean
Barnstable Board of Health Director
Barnstable Town Hall w,*
367 Main Street
Hyannis, MA 02601 P
4
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
OFFICE OF INSPECTOR GENERAL
Y 290 BROADWAY
y NEW YORK,NY 10007
CASE #: COMP-2018-0003 CROSS REFERENCE #: COMP-2014-0153,
COMP-2016-0088
TITLE: ENVIRONMENTAL ISSUES, BARNSTABLE, MA
INTERVIEWEE (if applicable):
PREPARED BY: RAC PAUL A. BREZINSKI
MEMORANDUM OF ACTIVITY
DOCUMENT REVIEW
f i
NARRATIVE:
On October 19, 2017, Resident Agent in Charge (RAC) Paul A. Brezinski, EPA Office of
Inspector General (OIG), Office of Investigations (01), New York,NY sent copies of lab test
results (Attachments 1 to 9) to Dr. Bruce Woods, Chemist, EPA OIG, 01, Electronic Crimes
Division, Seattle, WA for a review. The lab reports were based on samples taken frpm a ditch
and outfall pipe located on the private property of Patrick Page and Jane Saunders, 1780 Main
Street, West Barnstable, MA 02668, 508-280-7243. The purpose of the request for review was to
get Dr. Woods' insight into what had been reported. The following was provided:
Dr. Woods sent the Reporting Agent an email (Attachment 10) this same date indicating that two
primary things jumped out at him from a review of the reports— (1) the concentration of E. coli
found and (2) the Total Petroleum Hydrocarbon (TPH) test. Dr. Woods wrote:
1 think the most striking information is for E. coli bacteria in the Trench report. E. coli is
a specific indicator of human or animal waste being present somewhere to get into the
water, i.e.,.farm, septic tank, ????, etc. It is stated in the report that the E. coli
concentrations are significant, i.e., 1,900 CFU and 140,000 CFUper.100 milliliters (or
about 3 ounces). CFU's is short-hand for Colony Forming Units, which can replicate
and increase the bacteria.concentration. The reason I say that this appears to be a
discharge of human/animal waste is the samples tested positive for E. coli. For
CASE: COMP-2018-0003 INTERVIEWEE(if applicable): .
DATE OF ACTIVITY: October 11, DRAFTED DATE: October 13 & 16, AGENT(S): Brezinski
2017 2017
RESTRICTED INFORMATION This report and any attachments are the property of the EPA Office of Inspector General,Office of Investigations and is
Page I of 4 loaned to your agency. It and its contents may not be reproduced or disclosed without written permission. This report
contains information protected by the Privacy Act and is FOR OFFICIAL USE ONLY. Disclosure of this report to
unauthorized persons is prohibited. See 5 U.S.C.552a.
comparison, Total Coliform limits in drinking water is < I CFUper 100 ml sample. The
test for Total Coliforms would be higher than a test for fecal coliforms, which would be
higher than a specific test for E. Coli.
With respect to the TPH test, Dr. Woods wrote:
I did not check for a regulatory limit for the Total Petroleum Hydrocarbon test, to
compare with their result o 1,800 u /l. But the two different re orts or these tests
p f gp f
tentatively identified the pattern as 50 weight motor oil and weathered biodiesel.
Because I don't know anything about this area, I don't,know if this might be run-off from
a road or parking lot.
On this same date, the RA and Dr. Woods spoke in further detail. The RA explained the history
with the complainants, the issues with the property, the attempts to get remedies/responsibilities
and the fact that the property was residential. Dr. Woods utilized Google Maps to get a better
understanding of the property and the approximate location of the tests. The RA advised he was
not sure of the exact source(s) of the materials that are reportedly emanating from the outfall pipe
nor the location as to where the pipe begins. In addition, the RA added that some of the materials
found in the ditch.could be runoff from the local roads. Dr. Woods agreed that this is a matter
that would fall under the jurisdiction of either the Agency or the Commonwealth of
Massachusetts.
Attachments:
1. Trench 9-22 & 9-28-17
2. 8-29-17 outfall bact
3. 8-7-17 ditch
4. 8-13-17 discharge pipe
5. 8-1-13 outfall
6. cover letter 8-8-16
7. 12-25-15 stone well
8. 8-27-13 discharge pipe
9. 8-27-13 cranberry bog
10. Email from Dr. Woods, dated October 19, 2017.
CASE: COMP-2018-0003 INTERVIEWEE (if applicable):
DATE OF ACTIVITY: October 11, DRAFTED DATE: October 13 & 16, AGENT(S): Brezinski
2017 2017
RESTRICTED INFORMATION This report and any attachments are the property of the EPA Office of Inspector General,Office of Investigations and is
Page 2 of 4 loaned to your agency. It and its contents may not be reproduced or disclosed without written permission. This report
contains information protected by the Privacy Act and is FOR OFFICIAL USE ONLY. Disclosure of this report to
unauthorized persons is prohibited. See 5 U.S.C.552a.
Attachments:
1. Trench 9-22 & 9-28-17
Trench 9-22&
9-28-17.pdf
2. 8-29-17 outfall bact
8-29-17 outfall
bact.pdf
3. 8-7-17 ditch
8-7-17 ditch.pdf
4. 8-13-17 discharge pipe
8-13-17 discharge
pipe.pdf
5. 8-1-13 outfall'
8-1-13 outfall.pdf
6. cover letter 8-8-16
MMM
cover letter
8-8-16.pdf
CASE: COMP-201.8-0003 INTERVIEWEE(if applicable):
DATE OF ACTIVITY: October 11, DRAFTED DATE: October 13 & 16, AGENT(S): Brezinski
2017 2017
RES'T'121011)INFORMA110N This report and any attachments are the property of the EPA Office of Inspector General,Office of Investigations and is
Page 3 of 4 loaned to your agency. It and its contents may not be reproduced or disclosed without written permission. This report
contains information protected by the Privacy Act and is FOR OFFICIAL USE ONLY. Disclosure of this report to
unauthorized persons is prohibited. See 5 U.S.C.552a.
� K
t
7. 12-25-15 stone well
12-25-15 stone
well.pdf
8. 8-27-13 discharge pipe
8-27-13 discharge
pipe.pdf
9. 8-27-13 cranberry bog
8-27-13 cranberry
bog.pdf
10. Email from Dr. Woods, dated October 19, 2017.
Email.Woods.190ct
17.pdf
CASE: COMP-2018-0003 tNT ERV I EW EE(if applicable):
DATE OF ACTIVITY: October 11, DRAFTED DATE: October 13 & 16, AGENT(S): Brezinski
2017 2017
RESTRICTED INFORMATION This report and any attachments are the property of the EPA Office of Inspector General,Office of Investigations and is
Page 4 of 4 loaned to your agency. It and its contents may not be reproduced or disclosed without written permission. This report
contains information protected by the Privacy Act and is FOR OFFICIAL USE ONLY. Disclosure of this report to
unauthorized persons is prohibited. See 5-U.S.C.552a.
Enviif Otech Laboratones, 8 Jan Sebastian Dr Unit 12
Sandwich MA 02563
Inc Sandwich,
888-6460
Fax(508)888-6446
September 27,2016
Patrick Page
1780 Main Street
W. Barnstable, MA
Dear Patrick,
On September 22,2016,two water samples were collected by Envirotech Laboratories at the trench
located at 1780 Main Street West Barnstable,MA.The trench is an extension of the outfall pipe that is
located on the property.
Results: E coli were detected at the bridge location: 1,900 cfu/100ml.
E coli were detected at the ditch location: 140,000 cfu/100ml.
Comment: E coli counts are significant for sample sites,
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Sincerely you
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PH:508 888 6460
rsenviro@comcast.net
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ENVIR 0 TECH LA B ORA TOMES, INC.
MA CERT NO.: M-MA 063
8 Jan Sebastian Drive
Sandwich, AM 02563
(508)888-6460 1-800-339-6460
F (568)888-6446
Tuesday,September 27, 2016
page,Patrick
1750 Alvin.9
IV Bornstable, Al
ProjectNnme: 1780 rbicrin St C.vnnnents:
Project Number:
Collection Date: 09122i16 Collection Time: 14:50
Sampled By: R Saari
Lab Order Number: PVTV-161984
Date Received: 09122116
rar
T�Yrenc h
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a.k,.,.5.,,..� F" �.6K at ��'M^,�;°��+:ra^A3�`�� H{�wx^-:5� rs..a?;�'k�Pt'�.,..3`,::���'^.: ;'����,�ls �' '�"�'a�c� -�s3'�'!..3��e�a� .$.r����'" k,� ^�' �tT'rY'��cam"A�" "'.•.
¢v... '�a..rK..,�i,....r.. 2s,'2C",� �.��n, �'!k:i.5 '.aaYa,�r, y� msa..s i�•ti� ,-}Parameters Units Test Results Reporfnble Limits Dare,4»nlj,zed A,mlpsr tleilmd
E coif CFU/100mL 1,900 NA O9122116
Sam¢le T e � T ram* S : '€ S EPA 1603
i.Tlme,. a ..r�x''[R, is e 4 4 uH'
Comnienlr a�ay"4r w. w uti' h
Onoav ` �£�:>
x �c,-� ".z.,.a&,.+w aa� s�z..•as.;
�x TrenchsDilch3s B � t4:5009123I16a r � 3
!+ =w"`"?fi x'*..; - 4Yio_.a�a..+�.:,"�..P. .,. " ,�,,�; �i�. v: - 'a� '�' t„ rZ •"ram• `#"'D. t�.' *rsU.4."� NI
Parameters Units Test Results ReLortable Limits Dale Analyzed Analyst Method
E coli CFU/100mL 140,000 NA 09/22/16 IRS EPA 1603
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I3IU_=belory repnrlaGle lurrits
'see attached
.Ronald,l. Saari
Labor Pori,/D' ector
Page 1 of 1 v
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CHAIN OF CUSTODY FORM ENVIROTECH LABS, IN
Client: Patrick Page
8 Jan Sebastian Dr., Unit
Proj. No. Project Name: Ecoli Sandwich, MA 02563
S Address: 1780 Main St
I (508)888-6460/1-800-339-6460 W. barnstable,MA 02668
Sampler: Ron Saari/Env FAX(508)888-6446
Phone#: 508 280 7243
Fax#:
Lab ID# Date Time Comp Grab Sample location container Pres.
Analysis Requested
l�& 9i22/16 /��(i t3,-�� t E cold
Relinquished: Dat ime
n�7 Rec ve Reliquished: Date/Time
'C,l%i1J, ,-, (JJ Received:
Relinquished: f Da e/Time R tei
Relinquished: Date/Time Received:
{ t
a. En � 8 Ja virotech Labo n Sebastian Dr Unit 12
® �� Sandwich, MA 02563
Inc (508) 888-6460
Fax (508)888-6446
October 26, 2016
Patrick Page t
1780 Main Street
W.Barnstable,MA
Dear Patrick,
On September 28,2016,two water samples were collected by Envirotech Laboratories at the trench
located at 1780 Main Street West Barnstable, MA.The trench is an extension of the outfall.pipe that is
located on the property.
Results: E coli were detected at the bridge location:68,000 cfu/100ml.
E coli were detected atthe ditch location: 1,600 cfu/100ml.
Comment:E coli counts are significant for sample sites.
Sincerely yours,
Ronal /.Saari
Presi nt
PH: 508 888 6460
rsenviro@comcast.net
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EN VIR 0 TECH LA B ORA TORIES, INC.
MA CERT. NO.: 1V1-MA 063
8 An Sebastian Drive
Sandwich, AIA 02563
(.508)888-6460 1-800-339-6460
FAX(508)888-6446
Alonday,October 03,2016
Page, Palrick
1786 Moin Sl
H/Barnslable, M
ProjeclNreme: Trench Comments:
Projecl Number:
Collection D(ile: 09/28/16 Collection Time:
Sampled.By: R Saari
Lab Order Number: W111-I62032
Date Received: 09128116
�,�- � Srunple�j pe '` 3r'�ln Ie�`+Tuire Simi le Date ;
-
i'sr�
14 45< Q9/28/16
�,•� ,.T�e�=�h _.�:A w , v �� � .��
Parameters Units Test Results Reportable Limits Date Analyzed Anal)w Alelhorl k
E coli CFUJ100mL 68,000 NA 09/28/16 RS EPA 1603
Sa»rp1J Tjpe SnnrpleRTrine SairleDa1� Conimen(s �� � c:
Trench B �Y'50 09J28/ 6 �; ;Dredge DitchwL <,a+a +
�....;.. ...� � .•.,
Parameters Units Test Results Reportable Limits Dote Analyzer) Armful ,lletlrod
E coli CFU/t 00mL 1,600 NA 09/28/16 RS EPA 1603
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c
BRL=below reportable limits
i
*see attached
Rona il. aari
Laborrlo 1 Director
Page 1 of 1
ik
CHAIN OF CUSTODY FORM EN 4 VIROTECH LABS, INC. Client. Patrick Page
8 Jan Sebastian Dr., Unit 12
Proj. No. Project Name: 1780 Main St W Barnstable Sandwich, MA 02563
Address: 1780 Main St
tlL�� (508)888-6460
Sampler: /1-800-339-6460 W. barnstable,MA 02668
FAX(508)888-6446' Phone#: 508 280 7243
Lab ID# Date Time Comp Grab Fax#:
Sample location container Pres.
� � ��� Analysis Requested
-71
1
Relinqtsed.�! J '
e
/ Date ime (((,t tl Receiv
I' '] Reliquished: Date/Time Received:
Refin-quistkd: Da eTme Recliv
Relinquished: Daterrime
I'
Received:
Ci)
Envirotech Laboratories, 8 Jan Sebastian Dr Unit 12
Sandwich, MA 02563
Inc (508) 888-6460
Fax (508) 888-6446
September 18,2017
Patrick Page
1780 Main Street
W.Barnstable, MA
Dear Patrick,
On August 29,2017,a sample for algae was collected by Envirotech Laboratories at the ditch located
at 1780 Main Street West Barnstable,MA.
The ditch is an extension of the outfall pipe that is located on the property.The sample was collected at
the bridge location of the ditch.
The results are attached.
The material consists of lame amounts of filamentous bacteria.
Sincerely yours,
onald J. a
President
PFi: 508 8 6460
rsenviro comcast.net
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ENVIROTECH LABORATORIES, INC.
MA CERT. NO.: M MA 063
8 Jan Sebastian Drive
SandWeh,111A 02S63
(508)888-6460 1-860-339-6460
FAX(508)888-6446
Monday,September 18,2017
Page. Palricic
1780Aloilt Sl
IF Barreslable, Al
ProjectNante: Comments:
Project Number:
Collection Date: 08129117 Collection Time: 12:20
'Sampled BY: R Saari
Lah Order Number: WTTr-171903
Date Received: 08129117
Ditch atlBndge A 1220 ` 08/29/17 M Filamentous bacte`na <
Parameters Units Test Results Reportable Limits nareefrmly.ed fnnlyst .Ilcthod
Algae Identification NMI see comment NA 09/08/17 Northeast Lab
i
13R1=belong reportable lirl}i s
,see attached
s
R iald J aart
r
Laboral y Director
Page 1 of 1 I?
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JI.
Northeast Laboratories, Inc. ANAL=Y'TICAL RI PORT Page 1 of 1
Report To: ENVIROTECH LABORATORIES, INC.
Attn: Ronald Saari, President EMAIL ADDRESSEE: rsenviro@comeast.net
8 Jan Sebastian Dr= Unit#12
Sandwich MA 02563
Report Date: 9/13/2017 Date Sampled: 8/29/2017 .
Laboratory ID#: N1771449 Date Received: -9/06/2017
Envirotech's 10#: OW— 171903 Date Tested: 9/06/2017
MICROSCOPIC EXAMINATION: ' Raw Water=SITE: Ditch @ Bridge
ORGANISM #/ml ORGANISM #/ml ORGANISM #/ml ORGANISM #/ml
Diatomaceae Chloro h ceae C ano h ceae Protozoa
Amphora Actinastrum Anabaena* Actino hrys
A sterionella* Arthrodesmus Anabaenopsis Amoeba
iAm hi rota Ankistrodesmus A hanoca sa Arcella
Cocinodiscus Chorella A hanizomenon* Bursaria*
C clotella* Closterium A hanothece Ceratium
Cymbella Coelastrum Aulosira Cercomonas
Diatoma* Cosmarium Arthros ira Cfiilomonas
Frustulia Dictyos haerium* Chroococcus Chlam domonas
Fra ilaria Eudodna* Clathroc stis* Codonella
G rosigma Elakatothk Coelosphaerium* C ptomonas*
Gom honema Gleoc stis Cylindros ermum Difflugia
Melosira Micrasterias . Cus idothrix Dinob on*
Meridion* Mougeotia Dact lococcopsis Euglena77
Navicula Pandorina* Euca sis Glenodinium*
Nitzschia Pediastrum Gleoca sa Gonium
Pleurosigma Protococcus Galucocystis Halteria
Pinnularia Quadri ula Gloeothece Mallomonas*`
Ste hanodiscus Scenedesmus Gom hos haena Monas
Ste hanodiscus S haeroc stis Hydrocoleum Peridinium*
Surirella S haerozosma Microc stis S nura*
S nedra Spirogyra Merismo edia Trachelomonas
Tabellaria* Staurastrum Nostoc Urogleno sis*
Tetras ora Nodularia Vorticella
Rotifera Westella Oscillatoria
Anuraea Ulothrix Pseudanabaena
Asplanchna Volvox* S irulina
Brachionus Xanthidium Rivularia*
Conochilus Z gnema Xenococcus Schizom cetes j
Euchfanis Euastrum Crenothrix
Keratella
Notholca Xenococcus Miscellaneous
Polyarthra Acarina `
Rotifer Anguillula
S nchaeta Miscellaneous Bosmina
Canthocam tus *Odor Producin
Palmella Anac stis C cl0 s
Phacus Golenkinia Da hnia
J(Diaptomus
d
Conclusions: Total Natural Unit Count: 0 per mL
Comments: Results are based on sample,as submitted to Northeast Laboratories, Inc. on:8/08/2017, Large number of
filamentous bacteria noted in sample. Approved by; Laboratory Director P.
Northeast Laboratories,Inc. 1.29 Mill Street Berlin, CT 06037
a «�i w.ne}a6sct.con,
Telephone: 960-828-9787 Toll Free(hi State)800-826-0105 (Out of State)800-654-1230 Fax:860-829-1050
CT Cerl.#PH-0404 EPA Cerf.ftCT-024 USDA Cerf.90976 FDA Rcg.N086650488 CT CSLt/0000624
CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. Client: Patrick Page
8 Jan Sebastian Dr., Unit 12
Proj. No.. Project Name: 1780 Main St W Barnstable Sandwich, MA 02563 Address: 1780 Main St
(508)888-6460/1-800-339-6460 W. bamstable,MA 02668
Sampler: f� FAX(508)888-6446 Phone#: 508 280 7243
Fax#:
Lab ID# Date Time Comp Grab Sample location container Pres. Analysis Requested
Relinquish Daterrime Rece ed: Reliquished: DateTme Received:
01
Relinqui ed: Date/Time Received:
Relinquished: Date/Time Received: ~
. r
S
Enviro$ech Laboratories, 8 Jan Sebastian Dr Unit 12
Sandwich, MA 02563
Inc (508)888-6460
Fax (508)888-6446
September 12,2017
Patrick Page
1780 Main Street
W. Barnstable,MA
Dear Patrick,
On August 7,201-7,water samples were collected by Envirotech Laboratories at the ditch located at
1780 Main Street West Barnstable, MA.
The ditch is an extension of the outfall pipe that is located on the property.The sample was collected at
the bridge location of the ditch.
The results are attached.
There was found 1,800 ug/L of petroleum that most closely resembles 50w motor oil.Also,amounts of
Lead, Copper,Chromium,Aluminum, Iron,and Manganese were detected.
Sample for Algae identification was taken at the ditch located at the large boulder.Genus
P 9 9
Aphanocapsa and Nostoc belong to the Cyanobacteria group.
Sincerely yours,
AonalldJ.S�ri
President
PH:508 88 6460
rsenviro@comcast.net
t
ENYMOTECHLABORATORIES, INC.
MA CERT. NO.: M MA 063
8 Jan Sebastian Drive
Sandwich,MA 02563
(508)888-6460 1-RQ0-3:39-6460
FAX(508)888-6446
IYednesday,Septetnher 06,2017
Page, Pafrick
1780 A,tairt Sf
IF Barrrslable, Ad
ProjeciName: Comments:
Project Number:
Collection Date: 08107117 Collection Time: 12:45
Sampled By: Saari/Envirofech
Lab Order Number: WW-171705
Date Received: 08107117
-,.a ��i��t�'� � �s-fy�'�. �,�` �i'�. .,�� s,�Y�s3.�� x � �,�z. � �—�bti� zS" ri:".'� � �� �s��-•a� '3 ,��-�'�'e +" t;
r� '3�3�bs� D�tCtl����1 A��, �',, i 12•,95�-x �"�.� 08/07/17�" :5 h... :.,4 � � 3'�� i� Dltch�outfall bndge�,��'�4�""t�' s„ sGi ` .•-,'
Parameters Units Test Results Reportable Limits Date Analyzed Atta4ut w Method
Total Iron mg/L 33 0.01 08/10/17 MC EPA 200.7
Manganese mg/L 0.237 0.005 08/10/17 MC EPA 200.7
Aluminum mg/L 3.75 0.010 08/10/17 MC EPA 200.7
Barium mg/L 0.197 0.002 08/10/17 MC f EPA 200.7
Chromium mg/L 0.019 0.002 08/10/17 MC EPA 200.7
Nickel mg/L 0.009 0.005 08/10/17 MC EPA 200.7
Lead mg/L 0.037 0.006 08/10/17 MC EPA 200.7
Copper mg/L 0.024 0.003 08/10/17 MC EPA 200.7
Zinc mg/L 0.209 0.004 08/10/17 MC EPA 200.7
Petroleum Fingerprint' 1,800 ' 08/18/17 RIA' '
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BRL=below reportable limits
'see attached
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Ronal J. Saari
Lab ratory Dire for
Page 1 of 1 r
Page 2 of 3
R.I.Analytical Laboratories,Inc.
Laboratory Report
Envirotech Laboratories, Inc,
Work Order 4:1708-17187
Project Name: 1780 MAIN STREET, W. BARNSTABLE MA
Sample Number: 001
Sample Description: WW-171705 DITCH @ OUTFALL BRIDGE
Sample Type: GRAB
Sample Date/Time: 8/07/2017 @ 12:45
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
TPH
TPH GUM 1800 140 ug/l SW-846 8100M 8/18/2017 12:53 CCS
Surrogate RANGE SW-8468100M 8/18/2017 12:53 CCS
2-Fluorobiphenyl 53 40-140% SW-846 8100M 8/18/2017 12:53 CCS
Extraction Date SW-846 3510C 8/11/2017 9:55 JBW
TPH Fingerprint=Chromatogram most closely resembles 50w motor oil.
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CHAIN OF CUSTODY FORM ENV6ROTECH LABS, INC.
RI Analytical!
8 Jan Sebastian Dr Unit 12 PWS: M RI 015
Project Name: 1780 Main St, W Barnstable Sandwich,MA 02563
Address 41 Illinois Avenge®
(508)888-6460 Warrick, RI 02888
Sampler. R Saari/E.nvirotech
1-800-339-6460 Phone# 401-737-8600
FAX(508)88"446
Lab ID aex 401-735-19►70
Date Time re
Comp Grab Station location DEP ID Container Pres. Sample
WW-171705 08/07/17 1245 X Ditch Outfall Bride type Analysis requested
9 Glass HClNCI Petroleum Scare
a '
Rellnauished Da me
Received: Reiiauished• D
Al
lTime
Q cf' 5 Re eve
R Iin I hod: Da
Received: kRofln'�uls7hhod:
15',ze; �� 1 Datem— Received;
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Page I of 3
R.I. ,ANALYTICAL
Specialists in Environmental Services
3 '
LABORATORY REPORT
Envirotech Laboratories,Inc. Date Received: 8/9/2017 '
Attn: Mr. Ron Saari N Date Reported: 8/18/2017
8 Jan Sebastian Drive P.O.Number
Sandwich,MA 02563
Work Order#: 1708-17187
Project Name: 1780 MAIN STREET, W. BARNSTABLE MA
Enclosed are the analytical results and Chain of Custody for your project referenced above. The sample(s)
were analyzed by our Warwick,RI laboratory unless noted otherwise. When applicable, indication of
sample analysis at our Hudson,MA laboratory and/or subcontracted results are noted and subcontracted.
reports are enclosed in their entirety.
All samples were analyzed within the established guidelines of US EPA approved methods with all
requirements met, unless otherwise noted at the end of a given sample's analytical results or in a case
narrative.
The Detection Limit is defined as the lowest level that can be'reliably achieved during,routine laboratory.
conditions.
These results only pertain to the samples submitted for this Work Order#and this report shall not be
reproduced except in its entirety. s
1
We certify that the following results are.true and accurate to the best of our knowledge. If you have
questions or need further assistance,please contact our Customer Service Department.
Approved by:
i
r`
Melissa A.Manamon
QA/QC Officer is
x
Laboratory Certification Numbers(as applicable to sample's origin state): .
Warwick RI*RI LAI00033,MA M-R1015,CT PH-0508,ME RI00015,NH 2O70,NY 11726
Hudson MA*M-MAI 117,RI LA000319
41 Illinois Avenue,Warwick,RI 02888 www.rianalytical.com 131 Coolidge Street,Suite 105,Hudson MA 0174.9 .19
Phone,401-737-8500 Fax:401-7,U-1970, Phone:978-56870041 Fax:978-56870078
K
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CHAIN OF CUSTODY FORM
ENVIROTECH LABS, INC.
Client: Patrick Page
Proj. No. Project Name: 0 Jan Sebastian Dr., Unit 12
1780 Main St W Barnstable sandwich, MA 02563
i Address: 1780,Mairu St
Sampler: (508)888-6460/1-800-339-6460 W. barnstable,MA 02668
FAX (508)888-6446 Phone#: 5082807243
Lab ID.._# Date Time/ Comp Grab (�
Sample location Fax#:
container Pres.
Analysis Requested
i n Petroleum Scan
i metals
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Relinquis Date m'
,I L�UU Re ate/TiAme
i Reliquished: D
j��' ( Received:
Relinquished: Dat /Time
!t Received: Relinquished: Date/Time
Received:
t ,
ENVIROTECII LABORATORIES, INC.
MA CERT. NO.: M-MA 063
8"Jan Sebastian Drive
Sandrvich,MA 02563.
(,508)888-6A60 1-800-339-6460
FAX(508)888-6446
Tuesday,September 12,2017
Page, Patrick
1780 A,1oin,S1
IYBarnstable,Al
ProjectName: 1780 Main St., W. Barn. Comments:
Project Number: NA
Collection Date: 817117 Collection Time: 12:20
Sampled By: RS/Envirotech
Lab Order Number: WW-171706
Date Received: 08107117
Boultler��.kA
Parameters. Units Test Results Reportable Llerits Dare Analyzed Analyst Method
Algae Identification #/ml see attached NA 68108/17 Northeast Lab
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BRL=belowreportabl '
'see attached
13y:
Rol Id J. Sa i r`
Ldhorato y irector
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Page 1 of 1
1 C Y
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L
.00 Northeast Laboratories, Inc. ANALV T I(;Al, REPORT Page 1 of 1
Report To: ENVIROTECH LABORATORIES, INC.-
.Attn: Ronald Saari, President ( EMAIL ADDRESSEE: rsenviro@comcast.net
8 Jan Sebastian Dr= Unit#12
Sandwich MA 02563
Report Date: 8/14/2017 Date Sampled: t 8/07/2017
Laborato ID#: N1771079 Date Received: 8/08/2017
Envirotech's 6D#. DW— 171706 Date Tested: 8/08/2017
Raw Water-SITE: 1780 Main St. West Barnstable MA, Ditch @
MICROSCOPIC EXAMINATION: Boulder
ORGANISM #/ml I ORGANISM #/ml ORGANISM #/ml ORGANISM #/ml
Diatomaceae Chloro h ceae C ano h ceae I jProtozoa _
Amphora Actinastrum Anabaena* Actinophrys
Asterionella* lArthrodesmus jAnabaenopsis jArnoeba
Am hi rora lAnkistrodesmus jAphanocapsa 1,900 Zrsaria*
cella
Cocinodiscus Chorella A hanizomenon*
C clotella* Closterium A hanothece Ceratium
C mbella lCoelastrurn Aulosira Cercomonas
Diatoma* Cosmarium Arthros Ira IChilomonas
Frustulia Dici os haerium* Chroococcus Chlam domonas
Fra ilaria Eudorina* Clathroc stis* Codonella
G rosi ma Elakatothrix Coelos haerium* C tomonas*
Gornp honema Gleoc stis C lindros ermum jDifflugla
Melosira Micrasterias Cus idothrix Dinob on*
Meridion* Mou eotia Dact lococco sis Eu lena
Navicula 15,000 Pandorina* Euca sis Glenodinium*
Nitzschia Pediastrum Gleoca sa Gonium
Pleurosi ma lProtococcus Galucoc stis Halteria
Pinnularia IQuadrigula Gloeothece Mallomonas*
Ste hanodiscus IScenedesmus 11 Gom hos haeria I IMonas
Ste hanodiscus ISphaerocystis I H drocoleum Peridinium*
Surirella ISphaerozosma Microc stis S nura*
S nedra ISpirogyra 3.900 IMerismopedia I iTrachelomonas
Tabellaria* IStaurastrurn Oodularia
ostoc 960 Uro leno sis`
Tetras ora Vorticella
Rotifera Westella Oscillatoria
Anuraea �Ulothrix 5,800 Pseudanabaena
As lanchna Volvox* S irulina
Brachionus Xanthidium Rivularia*
Conochilus Zygnema Xenococcus Schizom cetes
Euchlanis Euastrum Crenothrix
Keratella
Notholca Xenococcus Miscellaneous
Pol arthra A
Acarina l
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Rotifer n uillula
S nch,aeta Miscellaneous Bosmina
Canthocam tus *Odor Producing
Palmella Anac stir Cyclops
Phacus Golenkinia Daphnia
z
Dia tomus F
i
Conclusions: ITotal_Natural Unit Count: 28,000 per mL
Comments: Results are based on sample, as submitted to Northeast Laboratories, Inc, on: 8/08/2017 (rounded)
Approved by: Laboratory Director
Northeast Laboratories,Inc. 129 Mill Street Berlin, CT 06037 Nvivw.nelabsct.com
Telephone: 860-828-9787 Toll Free(In State)800-826-0105 (Out of State)800-654-1230 Fax: 860-829-1050
CT Cert.#PH-0404 EPA Cert.#CT-024 USDA Cert.#0976 FDA Reg.#086650488 CT CSL#0000624 E
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{
CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. Client: Patrick Page
8 Jan Sebastian Dr., Unit 12
Proj. No. Project Name: 1780 Main St W Barnstable Sandwich, MA 02563
Address: 1780 Main St
(508)888-6460/1-800-339-6460 W. barnstable,MA 02668
Sampler: r FAX 508 888-6446
( ) Phone#: 508 280 7243
Fax#:
Lab ID# Date Time Comp Grab Sample location
p container Pres.00- 17 /706, Analysis Requested
Algae ID
(specifically cyanobacteria)
Relinquish D irno Ido Rece" e
Retiquished: Date/Time Received:
Relinquished: DateM6 Received:
Relinquished: Daterrime Received:
- 'J
ENVIROTECH LABORATORIES, INC. `
3M CERT. NO.: M MA 063
8 Jan Sebastiaii Drive
Sandwich,AL1 02563
(508)888-6460 1-800-33 9-6460
FAX ffb8)888-6446
rrie iy,September 27,2013
Page, Palrick
/780 Xfahi St
Pi,'13arnslable, Al
Projec/Name: 1780 AlAd17 St lY Brn astable Comments: Rain event in AM
Project Number.
Collection Date: 08127113 Collection Time: 12:05
Sampled BN: R Saari
Lab Order Number: W7,Y 132030
Dale Received: 08/27/13
Samp/e T}pe Soliple 77me Sainple,Dai� 777,
Comments
,r 4
Dischatge Pipe ;A 12 05 08/27/13 s s
*y.D `
i n butylphthalate,
Parameters nits Test Results Reportable Limits Date Analyzed Analyst Alethod
Sodium mg/L 11.4 1.0 08/29/13 MC 200.7
EPH/PAH ug/L 210
09ro4/13 RlT7__T MADEP
VPH ug/L None Detected 08/29/13 RIA* MADEP
E coli 1100 5,000 NA 08/27/13 RS E_ PA 1603 ,
Semi-volatile Compounds ug/L 15— 09/05/13 RIA* EPA 625
Dioxin pg/L None Detected * 09/16/13 Summit EPA 16136
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Laborat *Director
Page 2 of 2
•} 1
R.I . ANALYTICAL Page i of
Specialists in Environmental Servic®s
CERTIFICATE OF•ANALYSIS
Envirotech Laboratories, Inc. Date Received: 8/28/2013
Attn: Mr. Ron Saari Date Reported: 9/6/2013
8 Jan Sebastian Drive P.O.#:
Sandwich, MA 02563 Work Order#: 1308-18481
DESCRIPTION: PAGE, PATRICK
Subject saniple(s) has/have been,analyzed by our Warwick,R.I. laboratory with the attached results.
Reference: All parameters were analyzed by U.S. EPA approved methodologies.
The specific methodologies are listed in the methods column of the Certificate of Analysis.
Data qualifiers (if present) are explained in full at the end of a-given sample's analytical results.
The Certificate of Analysis shall not be reproduced except in full, without written approval of R.I. Analytical.
Results relate only to samples submitted to the laboratory for analysis.
Test results are not blank corrected.
fY
Certification#: RI-033, MA-RI015, CT-PH-0508, ME-R.I015
NH-253700 A&B, USDA 5-41844
If you have any questions regarding this work, or if we may be of further assistance,please contact 1
ot.ir Customer service department.
r
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• B
Approved b i
Sharon Baker
MIS/Data Reporting
enc: Chain of Custody
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41 Illinois Avenue,Warwick,RI 02888 4,
131 Cooifd e Sheet Suite
ui e t 105
www.rianalytical.com
9 Hudson,MAo1799 .
Phone:401:737.8500 Fax:401.738.1970 Y Phone:978.568.00 41 Fax:978.568.0078
s
Page 2 of 7
R.I. Analytical Laboratories, Inc.
CERTIFICATE OF ANALYSIS
Envirotech Laboratories Inc.
Date Received: 8/28/2613
Work Order#: 1308-18481
Sample# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST. W.BARNSTABL.E
SAMPLE TYPE: GRAB 'SAMPLE DATE/TIME: 8/27/2013 @ 12:05
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
TOC 15 5 mg/I SM-5310B 8/29/2013 12:45 EC
TPH
TPH GC/FID 850 100 ug/I SW846 8100M 9/4/2013 19:37 THP
Surrogate RANGE SW-846 8100 9/4/2013 19:37 THP
2-Fluorobiphenyl 86 40-140% SW-846 8100 9/4/2013 19:37 THP
Extraction date Extracted SW8463510 9/l/2013 10•I5 RJI
PCB
Aroclor-1016 <0.5 0.5 ug/i EPA 608 9/4/2013 10:10 JEB
Aroclor-1221 <0.5. 0.5 ug/I EPA 608 9/4/2013 10:10 JEB
Aroclor-1232 <0.5 0.5 ug/l EPA 608 9/4/2013 10:10 JEB
Aroclor-1242 <0.5 0.5 ug/I EPA 608 9/4/2013 10:10 JEB
Aroclor-1248 <0.5 0.5 ug/I EPA 608 9/4/2013 10:10 JEB
Aroclor-1254 <0.5 0.5 ug/I EPA 608 9/4/2013 10:10 JEB
Aroclor-1260 <0.5 0.5 ug/I EPA 608 9/4/2013 10:10 JEB
Surrogate RANGE 9/4/2013 10:10 JEB
Tetrachloro-m-xylene(TCMX) 70 30-150% EPA 608 9/4/2013 10:10 JEB
Decachlorobiphenyl 30 30-150% EPA 608 9/4/2013 10:10 JEB j
Extraction date Extracted EPA 608 9/l/2013 10:15 RJL
VPH I
Unadjusted CS-C8 Aliphatics(FID) <150 150 ug/I MADEP 8/29/2013 11:38 *ET 1
Unadjusted C9-C12 Aliphatics(FID) <150 150 ug/I MADEP 8/29/2013 11:38 *ET }
Methyl-tert-butylelher <1.5 1.5 ug/I MADEP 8/29/2013 11:38 *ET
Benzene <1.5 1.5 ug/l MADEP 8/29/2013 11:38 *ET
Toluene <5.0 5.0 ug/I MADEP 8/29/2013 11:38
Elhylbenzene <5.0 5.0 ug/I MADEP 8/29/2013 11:38 *ET G
m,p-Xylene <I0.0 10.0 ug/I MADEP 8/29/2013 11:38 *ET
o-Xylene <5.0 5.0 ug/I MADEP 8/29/2013 11:38 *ET
Naphthalene <5.0 5.0 ug/I MADEP 8/29/2013 11:38 *ET
Adjusted CS-C8 Aliphatics(FID) <150 150 ug/I MADEP. 8/29/2013 11:38 *ET
Adjusted C9-C12 Aliphatics(FID) <150 150 ug/I MADEP 8/29/2013 11:38 ET.-
C9-C10 Aronlatics(PID) <100 100 ug/I MADEP 8/29/2013 11:38 *ET
Surrogate RANGE 8/29/2013 11:38 *ET k
2,5-Dibromotoluene(PID) 100 70-130% MADEP 8/29/2013 11:38 *ET
2,5-Dibronlololuene(FID) 92 70-130% MADEP 8/29/2013 11:38 *ET
EPH/PAH
C9-C18 Aliphatics <100 100 ug/l MADEP 9/4/2013 16:32 THP 4
C19-C36 Aliphatics 210 100 ug/I MADEP 9/4/2013 1.6:32 THP
C11-C22 Aromatics <100 100 ug/I MADEP 9/4/2013 16:32 THP s
TARGET PAH ANALYTES 9/4/2013 16:32 THP .
I.
C
Page 3 of 7
R.I. Analytical Laboratories, Inc.
CERTIFICATE OF ANALYSIS
> nvirotech Laboratories Iuc,.
Date Received: 8/28/2613
Work Order#: 1308-18481
Sample# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST. W, BARNSTABLE
SAMPLE TYPE: GRAB SAMPLE DATE/TIME: 8/2-7/2013 cr 12:05
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
Naphthalene <5 5 ug/1 MADEP 9/4/2013 16:32 THP
2-Methyinaphthalene <5 5 ugft MADEP 9/4/2013 16:32 TIP
Acenaphthylene <5 5 ug/1 MADEP 9/4/2013 16:32 THP
Acenaphthene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Fluorene <5 5 ug/1 MADEP 9/4/2013 16:32 THP
Phenanthrcnc <5 5 ug/l MADEP 9/4/2013 16:32 THP
Anihracene <L s g/t ADD R14/2913 1.63-2 Tlfp
Fluoranthene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Pyrene <5 5 ugh MADEP 9/4/2013 16:32 THP
Benzo(a)anthracene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Chrysene <5 5 ug/1 MADEP 9/4/2013 16:32 THP
Benzo(b)fluoranthene <5 5 u8/1 MADEP 9/4/2013 16:32 THP
Benzo(b)fluoranthene <5, 5 ug/l MADEP 1 9/4/2013 16:32 THP
Benzo(a)pyrene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Indeno(1,2;3-ed)pyrene <5 5 ug/l MADEP 9/4/2013 16:32 THP
Dibenzo(a,h)anthracene <5 5 ug/l MADEP 9/4/2013 MR THP
Be.nzo(g,h,i)perylenc <5 5 UM MADEP 9/4/2013 16:32 THP
Extraction Surrogates RANGE 9/4/2013 16:32 THP
5 alpha-Androstane 87 40-140% MADEP 9/4/2013 16:32 THP
Ortho-terphenyl 79 40-140% MADEP 9/4/2013 16:32 THP
Fractionation Surrogates RANGE 9/4/2013 16:32 THP a
2-Fluorobiphenyl 78 46-140% MADEP 9A/2013 16:32 THP `
t
2-Bromonaphtltalenc 63 40-140% MADEP 9/4/2013 16:32 TI-W
Extraction date Extracted MADEP 9/3/2013 16:37 MMM
t
Semi-Volatile Organic Compounds .
Acenaphthene <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
Acenaphthylene <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
Anihracene <5 5 ug/1 EPA625 9/5/2013 15:11 KF
Benzidine <5 5 ug/1 EPA625 9/5/20H 15:11 KF
Benzo(a)anthracene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Benzo b Buoranthene <5 r'
O 5 ug/l EPA 625 9/5/2013 15:11 KF
Benzo(b)Duoranthene <5 5. ug/l EPA 625 9/5/2013 15:11 KF 5
Benzo(g,h,i)perylene <5 5 ug/1 EPA625 9/5/2013 15:11 KF $
Benzo(a)pyrene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
bis(2-Chloroethyl)Ether <5 5 ug/l EPA625 9/5/2013 15:11 KF
Bis 2-Chloroethox methane <5
( Y) 5 ug/l } EPA 625 9./5/2013 15:11 KF
Bis(2-ell loroisopropyl)ether <5 5 ug/1 1 EPA625 9/5/2013 15:11 KF
Bis(2-et.hy1hcxyl)phthalate <5 5 ugh EPA625 9/5/2013 15:11 KF
4-Bromophenyl plienyl ether <5 5 ug/l EPA625 9/5/2013 15:11 KF
Butylbenzylphthalate <5 5 ug/1 EPA625 9/5/2013 15:11 KF.
2-Chloronapthalene <5 5 ug/l EPA 625 9/5/2013 15:11 KF.
h.;
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Page 4 of 7
R.L Analytical Laboratories, Inc.
CERTIFICATE OF ANALYSIS
Envirotech Laboratories hic.
Date Received: 8/28/2613
Work Order 4: 1308-18481
Sample# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST. W.BARNSTABLE
SAMPLE TYPE: GRAB SAMPLE DATE/TIME: 8/27/2013'@ 12:05
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS, METHOD ANALYZED ANALYST
4-Clilorophenyl phenyl ether <5 5 ug/l EPA625 9/5/2013 15:11 KF
Chrysene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Dibenzo(a,h)anthracene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Di-n-butyl phthalate 15 5 ug/1 EPA625 9/5/2013 15:11 KF
1,2-Dichlorobenzene <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
1,3-Dichlorobenzene <5 5 ugll EPA 625 9/5/2013 15:11 KF
l.4-tlirhlnrnhrn7rnr $ S 6511 E- A626 9f5,99H Hii fe
3,3'-Dichlorobenzidine <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Dietlryl phthalate <5 5 ug/1 EPA 625 9/5/2013 15:1 I KF
Dimethyl phthalate <5 5 ug/l EPA 625 9/5/2013 15:11 KF
2,4-Dinitrotoluene <5 5 ug/1 EPA625 9/5/2013 15:11 KF
2,6-Dinitrotoluene <5 5 ug/l EPA 625 9/5/2013 15:l 1 KF
Di-n-octylphthalate <5 5 ug/1 EPA625 9/5/2013 15:1I KF
1,2-Dipheny1hydra7ine <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Fluoranthene <5 5 ug/l EPA625 9/5/2013 15:11 KF
Fluorene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Hexachlorobenzene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Hexachlorobutadiene <5 5 ug/1 EPA625 9/5/2013 15:11 KF
Hexachlorocyclopentadiene <5 5 ug/l EPA625 9/5/2013 15:11 KF
Hexachloroethane <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
lndeno(1,2,3-cd)pyrcnc <5 5 ug/I EPA625 9/5/2013 15:11 KF j
Isophorone <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
i
Naphthalene <5 5 ug/l EPA 625 9/5/2013 15:11 KF i
Nitrobenzene <5 5 ug/l EPA625 9/5/2013 15:11 KF
I
N-nitrosodimethylamine <5 5 ug/l EPA625 9/5/2013 15:11 KF
N-nitrosodiphenylamine <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
N-nitrosodi-n-propylamine <5 5 ug/1 EPA625 9/5/2013 15:11 KF s
Phenanthrene <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
Pyrene <5 5 ug/1 EPA 625 9/5/2013 15:11 KF '
1,2,4-Triclilorobenzene <5 5 ug/l EPA 625 9/5/2013 15:11 KF
4-Chioro-3-methylphenol <5 5 ug/1. EPA 625 9/5/2013 15:11 KF
2-Chlorophenol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
a'
2,4-Dichlorophenol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
2,4-Dimethylphenol <5 5 ug/l EPA 625 9/5/2013 15:11 KF
2-Mcthyl-4,6-dinitrophenol <5 5 ug/l EPA 625 9/5/2013 15:11 KF
2,4-Dinitrophenol <5 5 ug/l EPA625 9/5/2013 15:11 KF
2-Nitrophenol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
4-Nilrophenol <5 5 ug/l EPA625 9/5/2013 15:11 KF .
Pentachlorophenol <5 5 ug/l EPA 625 9/5/2013 15:11 KF
Phenol <5 5 ug/1 EPA625 9/5/2013 15:11 KF
2,4,6-Trichlorophenol <5 5 ug/1 EPA 625 9/5/2013 15:11 KF
Surrogates RANGE EPA 625 9/5/2013 15:11 KF
h
Page 5 of 7
R.I. Analytical-Laboratories, Inc.
CERTIFICATE OF ANALYSIS
Envirotech Laboratories,Lic.
Date Received: 8/28/2013
Work Order#: 1308-18481
Sample# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST. W.BA- NSTABLE
SAMPLE TYPE: GRAB SAMPLE DATE/TIME: 8/27/2013 @ 12:05
SAMPLE DET, DATE/TIME
PARAMETER RESULTS LIMIT UNITS ATE,THOD ANALYZED ANALYST
Phevol-d5 29 15-110% EPA 625 9/5/2013 15:11 KF
2-Fluorophcnol 36 15-110% EPA 625 9/5/2013 15:11 KF
2,4,6-Tribromophenol 91 15-110% EPA 625 9/5/2013 15:11 K.F
Nitrobenzene-0 89 30-130%, EPA 625 9/5/2013 15:11 KF
2-I-luorobiphcnyl 69 30-130% EPA 625 9/5/2013 15:11 KF
P-Terphenyl-d14 85 30-130% EPA 625 9/5/2013 15:11 KF
Volatile Organic Compounds
Benzene <1 1 ug/l SW-846 8260E 8/31/2013 15:29 KAC
Bromobenzene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
Bromochloromethane <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
Bromodichloromethane <1 I ug/l SW-8468260B 8/31/2013 15:29 KAC
Bromoform <1 1 ug/l SW-8468260B 8/31/2013 15:29 KAC
Bromomethane <5 5 ug/l SW-846 8260B 8/31/2013 15:29 KAC
n-Butylbenzene .<1 1 ug/l SW-8468260B 8/31/2013 15:29 KAC
Sec-butylbenzene <1 I ug/1 SW-846 8260B 8/31/2013 15:29 KAC
tert-Butylbenzene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
Carbon Tetrachloride <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
Chlorobenzene <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
Chloroethane <5 5 ug/l SW-846 8260B 8/31/2013 15:29 KAC
C:hloraform <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC t
Chloromethane <5 5 ug/1 SW-8468260B 8/31/2013 15:29 KAC
2-Chlorotoluene <I 1 ugll SW-8468260B 8/31/2013 15:29 KAC
4-Chlorotoluene <1 1 ug/1 SW-846 8260E 8/31/2013 15:29 KAC 3
Dibromochloromethane <1 l ug/1 SW-846 8260B 8/31/2013 15:29 KAC
1,2-Dibionio-3-Chloropropane <2 2 ug/l SW-846 8260B 8/31/2013 15:29 KAC .
l,2-Dibrom0ethane(EDB) <1 I ug/l SW-846 8260B 8/31/2013 15:29 KAC
Dibromomethane <2 2 ug/l SW-846 8260B 8/31/2013 15:29 KAC
k
1,2-Dichlorobenzene <I I ug/1 SW-846 8260E 8/31/2013 15:29 KAC
1,3 Dichlorobenzene <] 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
1,4-Dichlorobenzene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC `
Dichlorodilluoromethane <5 5 ug/1 SW-846 8260E 8/31/2013 15:29 KAC
s
I,1-Dichloroethane <1 I ug/1 SW-846 8260B 8l31/2013 15:29 KAC .
1,2-Dichloroethane <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
],I-Dichloroethene <1 I ug/1 SW-8468260B 8/31/2013 .15:29 KAC `
1:
cis-1,?_-Dichloroethene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
trans-1,2-Dichloroethylene <2 2 ug/1 SW-846 8260E 8/31/2013 15:29 KAC
1,2-Dichloropropane <1 1 ug/I SW-846 8260B 8/31/2013 15:29 KAC
1,3-Dichloropropane <1 1 110 SW-846 8260B 8/31/2013 15:29 KAC I
2,2-Dichloropropane <I I ug/l SW-846 8260B 8/31/2013 15:29 KAC k
1,1-Dichloropropene <1 I ugh SW-846 8260B 8/.31/2013 15:29 KAC
Ethylbenzene <I 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
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Page 6 of 7
R.I. Analytical Laboratori'es;,Inc:
CERTIFICATE OF ANALYSIS
Envirotech Laboratories, Ina
Date Received: 8/28/2013
Work Order 0: 1308-18481
Sample# 001
SAMPLE DESCRIPTION: WW-132030 1780 MAIN ST. W.BARNSTABLE
SAMPLE TYPE: GRAB SAMPLE DATE/TIME: 8/27/2013 a 12:05
SAMPLE DET. DATE/TIME
PARAMETER IZESULTS LIMIT UNITS METHOD ANALYZED ANALYST
llexachlorobutadiene <1 1 ug/l SW-8468260B 8/31/2013 15:29 -KAC
Isopropylbenzene <1 1 ug/I SW-8468260B 8/31/2013 15:29 KAC
p-Isopropyltoluene <1 I ug/l SW-846 8260B 8/31/2013 15:29 KAC
Methylene Chloride <5 5 ug/I SW-846 8260B 8/31/2013 15:29 KAC
Naphdialene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
n-Propylbenzene <1 I ug/l SW-846 8260B 8/31/2013 15:29 KAC
Styrene <1 1 o/I etzr-84AR-)611i3-8/31/Z913 15-20- Yet:
1,1,1,2-Tetrachloroethane <1 1 ug/1 SW-8468260B 8/31/2013 15:29 KAC
1,1,2,2=retrachloroethane <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
Tetrachloroethene <1 I ug/1 SW-846 8260B 8/31/2013 15:29 KAC
Toluene <1 1 ug/1 SAT-846 8260B 8/31/2013 15:29 'KAC
1,2,3-Trichlorobenzene <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
1,2,4-Trichlorobenzene <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
1,1,1-Trichloroetlrane <1 1 ug/1 SW-8468260B 8/31/2013 15:29 KAC
1,1,2-Trichloroethane <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
Trichloroethene <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
Trichlorofluoromethane <1 1 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
1,2,3-Tricliloropropane <2 2 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
1,2,4=rrimethylbenzeue <1 1 ug/1 SW-8468260B 8/31/2013 15:29 KAC
1,3,5-Trimethylbenzene <1 I ug/1 SW-846 8260B 8/31/2013 15:29 KAC s
Vinyl Chloride <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
o-Xylene <1 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
m,p-Xylene <7 1 ug/l SW-846 8260B 8/31/2013 15:29 KAC
MTBE <2 2 ug/1 SW-846 8260B 8/31/2013 15:29 KAC
Acetone <10 10 ug/l SW-846 8260B 8/31/2013 15:29 KAC
Surrogates RANGE SW-846 8260B 8/31/2013 15;29 KAC
Dibromofluoromethane 107 86-118% SW-846 8260B 8/31/2013 15:29 KAC
Toluene-d8 97 88-110% SW-846 8260B 8/31/2013 15:29 KAC
4-Bromofluorobenzene 94 86-115% SW-846 8260B 8/31/2013 15:29 KAC
1,2 Dichloroethane-d4 97 80-120% SW-846 8260B 8/31/2013 15:29 KAC i
Total Metals
Mercury <0.0005 0.0005 mg/1 EPA245.1 8/30/2013 9:31 PJC
Mercury Digestion EPA245.1 8/30/2013 9:12 JL 1
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R.I.Analytical.Laboratories, Inc,
CERTIFICATE OFANALYSIS
Envirotech Laboratories, Inc.
Date Received: 8/20/2613
Work Order#: 1308-17844
Sample# 001
SAMPLE DESCRIPTION: WW-131905 OUTFALL
SAMPLE TYPE: GRAB SAMPLE DATE/TIME: 8/01/2013
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
TPH
TPH GUM 450 110 ug/l SW846 8100M 8/23/2013 16:45 THY
Surrogate RANGE SW-846 8100 8/23/2013 16:45 11113
2-Fluorobiphenyl 66 40-140% SW-846 8100 8/23/2013 16:45 THP
Extraction date Extracted SW8463510 8/22/2013 21:00 MMM
The sample was received at the laboratory outside of the recommended hold time for the TPH analysis.
Fingerprint:Chromatogram best matches weuthered biodiesel fuel,possibly from vegetable oil sources.
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CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. RI Analytical
8 Jan Sebastian Dr Unit 12 M Rl 015
PWS: Project Name: Sandwich,MA 02563 Addn3ss 41 Illinois Avenue
Sampler: P. Page (508)888-6460 Warwick, RI 02888
9 1-60039-6460 Phone# 401-737-8500
FAX(508)888-64" Fax 401-738-1976
Lab ID# Date :: Time Comp Grab Istation location DEP ID Container ' Pres: ._ Sample type Analysis requested
WW-131905 0901113 NA X of ttail Glass H2SO4 Drinking Petroleum Fingerprint
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Relin uiahed: pl;acm
Received: Datelfime Received:in u hed• Received: Relinquished: Datel7ime Received:
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. . ices
8 Jan Sebastian Dr., Unif 12
Proj. No. Project Name:
Sandwich, MA 02563 Address: o d- Park
(508)888-6460%1-800- 3n-6460
Sam ler: � - N e :, A 02031 '
p 'e @1 �'L _ FAX{50B1888-6446 Phone#:
Fax#:
Lab ID# Date: Time Comp GrabA. Sample Location container Pres. `
13Igb� Analysis Requested
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Reli uished:
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Relinquished: Dat1 /5
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Rec6 ived:
I
Envirotech Laboratories, 8 Jan Sebastian Dr Unit 12
Sandwich, MA 02563
Inc (508) 888-6460
Fax(508) 888-6446
August 8, 2016
Patrick Page
1780 Main Street
W.Barnstable, MA
Dear Patrick,
Samples taken by Envirotech Laboratories at different locations from sites located at 1780 Main Street
West Barnstable, MA.
Results:
8/27/13:Sample at discharge pipe located at 1780 Main Street showed E.coli 5,000 cfu/100ml,Total
Petroleum hydrocarbons 850 ug/L,C19-C36 Aliphatics 210 ug/L, Di-n-butyl phthalate 15 ug/L.
8/27/13:Solid sample from old cranberry bog showed detection of Cadmium 0.14 mg/Kg dry wt.,
Chromium 7.90 mg/Kg dry wt.and Barium 13.7 mg/Kg dry wt.
12/24/15: Sample at Stone Well located off of route 6A at 1780 Main Street showed nitrate 3.49 mg/L,
Total Nitrogen 6.1 mg/L,Aluminum 19.8mg/L.
Results indicate that further investigation is recommended by a qualified environmental organization
(i.e. DEP or EPA)or qualified environmental engineering company.
Sincerely your ,
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ENVIROTECHLABORATORIES, INC.
MA CERT. .NO.: M-MA 063
8 Jtttt Sebastian Drive
Saadlvich, 41A 02563
(508)888-6460 1-800-339-6460
FAX(508)888-6446
Friday,January 08,2016
Page, Patrick
1780 Alain St
by Bat•nslable, bf
ProjectNarne: 1780 Main.A W Barnslable Comments:
Project Number:
Collection Date: 12124115 Collection Time: 09:55
Sampler/By: R Saari
Lab Order Number: WTV-153151
Date Received: 12124115
r W�$-:,.'^.� !xL'.?,�`' �`+,�rfi-{t�,y��:rSf .� 7 ?s -Yiai`� k } ' w r� k`,b:,tij'" 'F't+.�"'S�"�.A''•Z?��'*' ww"'. Gx
sr r �� t Rs� 3� �� �"� �"�t �,•fix � � �-� '�} 'rr :. a-y. � � � s �s` � 9 �y`z"� z" _ �, �rk�,.�a�;�
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Parameters Units Test Results Reportable Limits Date Analyzed Attalj+.rt A4et/iod
Kjeldhal Nitrogen mg/L 2.6 0.6 01/06/16 KB SM4500 NH3 C
Ammonia-N mg/L BRL 0.5 ol/05/16 KB SM4500 NH3 C
Nitrate-N mg/L 5.49 0.01 12/24/15 RL 300.0
Nitrite-N mg/L BRL 0.006 12/24/15 RL 300.0
Total Nitrogen mg/L 6:1 NA 01/07/16 KB Calculation
Total Phosphorous(P) mg/L 0.025 0.005 01/08/16 MC 4500-P
Sodium-grab I mg/L 12.3 1.0 12/30/15 MC 200.7
Total Iron mg/L 24.1 0.01 12/30/15 MC 200.7
Manganese mg/L 0.55 0.005 12/30/15 MC 200.7
Aluminum mg/L 19.8 0.010 12/30/15 MC 200.7
Barium mg/L 0.15. 0.002 12/30/15 MC 200.7
Zinc mg/L 0.19 0.004 12/30/15 MC 200.7
Potassium mg/L 8.8 0.1 12/30/15 MC 200.7 .
Magnesium mg/L 10.5 0.1 12/30/15 MC 200.7
EPFI/PAH ug/L ND* 01/05/16 RIA" MADEP
VPH ug/L ND* 12/30/15 RIA` MADEP:
BRL=below reportable/halts s
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`'see attached t
Ronald J. Sa7iri 7
Laboratory Director
Page 1 of 1
R.I. ANALYTICAL Pagel of3
Specialists in Environmental Services
CERTIFICATE OF ANALYSIS
Envirotech Laboratories, Inc. Date Received: 12/28/2015
Attn: Mr. Ron Saari Date Reported: 1/7/2016
8 Jan Sebastian Drive P.O.#:
Sandwich, MA 02563 Work Order#: 1512-28061
DESCRIPTION: PAGE, PATRICK 1780 MAIN STREET, W BARNSTABLE MA
Subject sample(s)has/have been analyzed by our Warwick, RI laboratory with the attached results.
Reference: All parameters were analyzed by U.S. EPA approved methodologies.
The specific methodologies are listed in the methods column of the Certificate of Analysis,
Data qualifiers (if present) are explained in full at the end of a given sample's analytical results.
The Detection Limit is defined as the lowest level that can be reliably achieved during routine laboratory
conditions.
The Certificate of Analysis shall not be reproduced except in full,without written approval of R.I. Analytical.
Results relate only to samples submitted to the laboratory for analysis.
Test results are not blank corrected.
Certification#(as applicable to the,sample's origin state):
RI LAI0033,MA'M-RI015, CT PH-0508, ME RI00015, NH 2537,NY 11726
If you have any questions regarding this work, or if we may be of further assistance,please contact
our customer service department.
Approved by:
t
.enc: Chain of Custody
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41 Illinois Avenue,Warwick,RI 02888 131 Coolidge Street,Suite 105,Hudson,MA 0174.9
Phone:401.737.8500. Fax:401.738.19 www.
.70 rianal Ytical.com Phone:978.568.0041 Fax:978.568.0078
r:
Page 2 of 3
R.I. Analytical Laboratories,Inc.
CERTIFICATE OF ANALYSIS
Envirotech Laboratories,Inc.
Date Received: 12/28/2015
Work Order#: 1512-28061
Sample# 001 '
SAMPLE DESCRIPTION: WW-153151 STONE WELL
SAMPLE TYPE:GRAB SAMPLE DATE/TIME: 12/24/2015 a 09:55
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
TPH
TPH GC/F1D <100 t00 ug/l SW-846 8100M 1/6/2016 8:51 KS
Surrogate RANGE SW-846 8100M 1/6/2016 8:51 KS
2-Fluorobiphenyl 63 40-140% SW-846 8100M 1/6/2016 8:51 KS
Extraction Date SW-8463510C 12/30/2015 13:15 JPB
VPH
Unadjusted C5-C8 Aliphaties(FID) <100 100 ug/1 MADEP VPH-04-1.1 12/30/2015 16:02 KF
Unadjusted C9-C12 Aliphatics(FID) <100 100 ug/1 MADEP VPH-04-1.I 12/30/2015 16:02 KF
Adjusted C5-C8 Aliphatics(F1D) <100 100 ug/l MADEP VPH-04-1.1 12/30/2015 16:02 KF
Adjusted C9-C12 Aliphaties(FID) <100 100 ug/1 MADEP VPH-04-1.1 12/30/2015 16:02 KF
C9-CI0 Aromatics(PID) <100 100 ug/l MADEP VPH-04-1.1 12/30/2015 16:02 KF
Target Aromatic Analytes 12/30/2015 16:02 KF
Methyl-tert-butylether <5 5 ug/l MADEP VPH-04-1.1 12/30/2015 16:02 KF
Benzene <5 5 ug/l MADEP VPH-04-1.1 12/30/2015 16:02 KF
Toluene <5 5 ug/l MADEP VPH-04-1.1 12/30/2015 16:02 KF
Ethylbenzene <5 5 ug/l MADEP VPH-04-1.1 12/30/2015 16:02 KF
m,p-Xylene <5 5 ugA MADEP VPH-04-1.1 12/30/2015 16:02 KF
o-Xylene <5 5 ug/1 MADEP VPH-04-1.1 12/30/2015 16:02 KF
Naphthalene <5 5 ug/l MADEP VPH-04-1.1 12/30/2015 16:02 KF
Sun-ogate RANGE 12/30/2015 16:02 KF
2,5-Dibroinotoluene(PID) 95 70-130% MADEP VPH-04-1.1 12/30/2015 16:02 KF
2,5-Dibroinotoluene(FID) 100 70-130% MADEP VPH-04-1.1 12/30/2015 16:02 KF
EPH/PAH
C9-C18Aliphalics <120 120 ug/1 MADEPEPH-04-1.1 1/5/2016 17:58 KS
C19-C36 Aliphatics <120 120 ug/I MADEP EPH-04-1.1 1/5/2016 17:58 KS
Unadj.CI1-C22 Aromatics <100 100 ug/l MADEP EPH-04-1.1 1/5/2016 17:58 KS 1
Adj.CI I-C22 Aromatics <100 100 ug/l MADEP EPH-04-1.1 1/5/2016 17:58 KS s
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TARGET PAH ANALYTES r
Naphthalene <5 5 ug/1 MADEP EPH-04-1.1 1/5/2016 17:58 KS
2-Methylnaphthalene <5 5 ug/l MADEP EPH-04-1.1 1/5/2016 17:58 KS
Acenaphthylene <5 5 ug/l MADEP EPH-04-1.1 1/5/2016 17:58 KS
Acenaphthene <5 5 ug/l MADEP EPH-04-1.1 1/5/2016 17:58 KS
Fiuorene <5 5 ug/l MADEP EPH-04-1.1 1/5/2016 17:58 KS
Phenanthrene <5 5 ug/l MADEPEPH-04-1.1 I/5/2016 17:58 KS
Antluacenc <5 5 ug/1 MADEP EPH-04-1.1 1/5/2016 17:58 KS
Fluoranthcne <5 5 ug/l MADEP EPH-04-1.1 1/5/2016 17:58 KS '
Pyrene <5 5 ug/1 MADEP EPH-04-1.1 1/5/2016 17:58 KS
Benzo(a)anlhraccne <5 5 ug/l MADEP EPH-04-1.1 1/5/2016 17:58 KS
Cluysene <5 5 ug/l MADEP EPH-04-1.1 1/5/2016 17:58 KS
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Page 3 of 3
R.I. Analytical Laboratories, Inc.
CERTIFICATE OF ANALYSIS
l;nvirotech Laboratories, Inc.
Date Received: 12/28/2015
Work Order#: 1512-28061
Sample#. 001
SAMPLE DESCRIPTION: WW-153151 STONE WELL .
SAMPLE TYPE:GRAB SAMPLE DATE/TIME: 12/24/2015 L 09:55
SAMPLE DET. DATE/TIME
PARAMETER—' RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
Benzo(b)f]uoranthene <5 5 ug/1 MADEP EPH-04-1.1 1/5/2016 17:58 KS
Benzo(k)fluoranthene <5 5 ug/1 MADEP EPH-04-I.1 1/5/2016 17:58 KS
Benzo(a)pyrene <5 5 ug/1 MADEP EPH-04-1.1 1/5/2016 17:58 1(S
Indeno(1,2,3-cd)pyrene <5 5 ug/1 MADEP EPH-04-1.1 1/5/2016 17:58 KS
Dibenzo(a,h)antlu-acetic <5 5 ug/l� MADEP EPH-04-1.1 1/5/2016 17:58 KS
Benzo(g,h,i)perylene <5 5 ug/1 MADEP EPH-04-1.1 1/5/2016 17:58 KS
Extraction Sunogates RANGE
5-alpha-Androstane 73 40.140% MADEP EPH-04-1.1 1/5/2016 17:58 KS
Ortho-terphenyl 85 40-140% MADEP EPH-04-I.I 1/5/2016 17:58 KS
Fractionation Swrogates RANGE
2-Fluorobiphenyl 86 40-140% MADEP EPH-N-1.1 1/5/2016 17:58 KS
2-Bromonaphthalene 89 40-140% MADEP EPH-04-1.1 1/5/2016 17:58 KS
TPH:Samplc does not exhibit a hydrocarbon pattern.
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CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. RI Analytical
8 Jan Sebastian Dr Unit 12 M Rl 015 -
Project Name: Page, Patrick Sandwich, MA 02563 Address 41 Illinois Avenue
1780 Main Street,W. Barnstable, MA (508)888-6460 Warwick, RI 02888
Sampler: R. Saari 1-800-339-6460 Phone# 401-737-8500
FAX(508)888-6446 Fax# 401-738-1970
Lab ID# Date ITime Coml Grab Station location Container Pres. Sample
p typ Analysis requested
WW-153151 12/24/15 0955 X Stone Well I Glass H2SO4 Groudwater TPH fingerprint
2 VOA WC Groudwater VPH
2 Glass HCL Groudwater EPH/PAH
Relinquished: Date/Time Received:
12-)&/s ilia � Contact lab with any exceeded MCL
Relinquished: Datemme Received:
CHAIN OF CUSTODY FORM EN1ilROTECH LABS, INC.
RI Analytical
8 Jan Sebastian Dr Unit 12 M RI 016
Project Name: Page, Pabick Sandwich,MA 02563
Address 41 Illinois Avenue
I 1780 main Street,W.Barnstable,MA (508)888-6460 Warwick, RI 02888
Sampler. R. Saari 1-800�39-6460
Phone# 401-737-8500
fAX(508)888-6446 Fax# 401-738-1970
Lab ID Date Time Come Grab Station location
Container Pros... Sample typ Anal sis requested
WW 1±53151 12/24H`5 0955 X Stone Well 1L Glass, H2SO4 Groudwater
4 TPH fingerprint
I 2 VOA HCL Groudwater
VPH
2 Glass HCL Groudwater EPH/PAH
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CHAIN OF CUSTODY FORM ENWIROTECH LABS, INC. Client: Patrick Page
8 Jan Sebastian Dr., Unit 12
Proj. No. Project Name: 1780 Main St W Barnstable Sandwich, MA 02563 Address: 1780 Main St
(508)888-6460/1-800-339-6460 W. barnstable,MA 02668
Sampler: FAX(508)888-6446 Phone#: 608 280 7243
Fax M
Lab ID# . , Dat Time Comp Grab Sample location container Pres. Analysis Requested
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Relinquis Vd Date/Tim Receive Reliquished: Date/Time
/ Received:
Relinquish d: Daterrime Received' Relinquished: Daterrime
Received:
ENVIROTECH LABORATORIES, INC.
1V1A CERT. NO.: M-MA 063
8 Jan Sebastian Drive
Slnidwich,AZ4 02563
(508)888-6460 1-800-339-6460
FAX(508)888-6446
l,rirlay,September 27, 2013
Page, Palrick
l 780 Adaln Sl
W Barnstable, A4
Project'Natite: 1780 Mahe St YYBmislable Colttrnents: Rain event in AM
Project Nnntber:
Collection Dale: 08127113 Collection Tinte: 12:05
Saliipled By: •R Saori
Lab Order Nianber: WTV-132030
Date Received.• 08/27/13
Sam le Type Sanpli Timex _ Sam 1c Dnte '�� ` t V s
Con�unent� Y r T r
t '
Discharge Pipe A 12 05` 08/27113 { a ` p`u ate' '
y lkn�butylPhthalate s
Parameters Ullits, Test Results y Reportable Limits Date Analyzed Analyst A1ethod
BOD 5-Day mg/L 4.1 3.0 08/28/13 MC 5210 B
Kleldhal Nitrogen mg/L 0.8 0.6 09/09/13 KB SM4500 NH3 C
Ammonia-N mg/L BRL 0.5 08/29/13 KB SM4500 NH3 C
Nitrate-N mg1L 0.70 0.05 08/27/13 LL 300.0
Nitrite-N mg/L BRL 0.020 08/27/13 LL 300.0
Total Nitrogen mg/L 1.5 NA 09/23/13 RIA* Calculation
Total Phosphorous(P) mg/L 0.20 0.013 09/25/13 MC 4500-P
Chemical Oxygen Demand mg/L 63.8 5.0 09/04/13 MC Hach 8000
Total Organic Carbon` mg/L 15 D.5 08/29/13 RIA* SM 5310 C
Volatile Organic Compounds" ug/L None Detected 0e/31/13 RIA*
Total Iron mg/L 0.59 0.01 08/29/13 MC 200.7
Manganese mg/L 0.11 0.008 09/13/13 MC 200.7
Aluminum mg/L 0.99 0.010 09/13/13 MC .200.7
Silver mg/L BRL 0.002 09/13/13 MC 200.7 i
Barium mg/L 0.018 0.002 09/13/13 MC 200.7 1
Cadmium mg/L BRL 0.001 Os/1.3I13 MC 200 7 [
Chromium mg/L BRL. 0.002 09/13/13. MC 200 7
Mercury' mglL <0.0005.. 0,0005: 08/30,/13 RIA* . .`: 2451
Selenium mg/L BRL 0.006 09/13/.1,3 MC 200.7 t
Lead. mg/L BRL 0.006 'OW13/13 MC. 200.7
Copper mg/L 0.025 0.003- ;P5/29/13: .. ...... MC. 200.7
Zinc mg/L 0.098 0.004 09/13/13 d MC 20.0.7.:. f.
Arsenic mg/L BRL 0.010 09/13/13 ;MC. 200.7
Petroleum Fingerprint` 850 o9/04/13 RIA* *.
PCB 8080` "None Detected 09/04/13 "RIA SW-846 8082
BRL=heloiv reportable lindts
*.Tee attaehed .
By.
Ron ilt/J`Sr ri
Laborat r ireclor t
Page 1 of 2
_ /i
i ESS Laboratory BAL Laboratory
Division of Thielscli Engineeting,Inc. ' -The ATicrobiologj,Division
1� \ ofThielsch Engineering,Inc. A
CERTIFICATE OF ANALYSIS
Data Reporting
RI Analytical Laboratories, Inc.
41 Illinois Avenue
Warwick,RI 02888
RE: RIAL Sampling-MCP(1308-18481)
ESS Laboratory Work Order Number: 1308604
This signed Certificate of Analysis is our approved release of your analytical results. These results are
only representative of sample aliquots received at the laboratory. ESS Laboratory expects its clients to
follow all regulatory sampling guidelines. Beginning with this page, the entire report has been paginated.
This report should not be copied except in full without the approval of the laboratory. Samples will be
disposed of thirty days after the final report has been delivered. If you have any questions or concerns,
please feel free to call our Customer Service Department.
'� 'By ESS Laborat ry�at�20 amzS p�0�4,���'`0,1,,3R,
Laurel Stoddard yt ...
Laboratory Director
Analytical Summary
The project. as described above has been analyzed in accordance with the ESS Quality Assurance Plan.
This plan utilizes the following methodologies: US EPA S W-846, US EPA Methods for Chemical
Analysis of Water and Wastes per 40 CFR Part 136, APHA Standard Methods `for, the Examination of
Water and Wastewater, American Society for Testing and Materials (ASTM), .and other recognized
methodologies. The analyses with these noted observations are in conformance to the Quality Assurance
Plan. In chromatographic analysis, manual integration is fi•equently used instead of automated
integration because it produces more accurate results.
The test results present in this report are in compliance with NELAC Standards, A2LA and/or client
Quality Assurance Project Plans (QAPP). The laboratory has reviewed the following: Sample t
Preservations, Hold Times, Initial Calibrations, Continuing Calibratins, Method Blanks, Blank Spikes, s
Blank Spike Duplicates, Duplicates, Matrix Spikes, Matrix Spike Duplicates, Surrogates and internal
Standards. Any results which were found to be outside of the recommended ranges. stated in our SOPs h
will be noted in the Project Narrative.
- F
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Pam I of 12 fir.
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ESS Laboratory BAL Laboratory
Division ofTbielseb Engineeting,Inc. The11ficrobiologyDivision -
1 ofTbidsch En-Lucering,Inc.
CERTIFICATE OF ANALYSIS
Client Name: RI Analytical Laboratories,Inc.
Client Project lD: RiAL Sampling-MCP ESS Laboratory Work Order: 1308604
SAMPLE RECEIPT
The following samples were received on August 29,2013 for the analyses specified on the enclosed Chain of Custody Record.
To achieve CAM compliance for MCP data, ESS Laboratory has performed and reviewed all QA/QC Requirements and
Performance Standards listed in each method. Holding times and preservation have also been reviewed. All CAM
requirements have been achieved unless noted in the project narrative.
Each method has been set-up in the laboratory to reach required MCP standards. The methods for aqueous VOA and Soil
Methanol VOA have known limitations for certain analytes. The regulatory standards may not be achieved due to these
limitations. In addition, for all methods, matrix interferences, dilutions, and %Solids may elevate method reporting . limits
above regulatory standards. ESS Laboratory can provide, upon request, a Data Checker (regulatory standard comparison
spreadsneet)e ec ronic deliverable w plc i will highlight ttiese excee antes.
For EPH soil samples, the aromatic range results have been corrected for identified cartridge contaminant in accordance with
the CAM protocol.
Lab Number SamnleName Matrix Analysis
1308604-01 1308-18481-001 Waste Water MADEPNPH
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E S S Laboratory BAL Laboratory
The_Microbiol d Division
Division ofThielsch Engineering, Inc. °2'
of T6ie/sch Lo giueerirg,Inc. AA -
CERTIFICATE OF ANALYSTS
Client Name: RI Analytical Laboratories,Inc.
Client Project ID: RIAL Sampling-MCP ESS Laboratory Work Order: 1308604
PROJECT NARRATIVE
No unusual observations noted.
End of Project Narrative.
DATA USABILITY LINKS
Definitions ofOuality Control Parameters
Semivolatile Organics Internal Standard Information
Semivolatile Organics Surrogate Tnformation
Volatile Organics Internal Standard Information
Volatile Organics Surrogate Information
EPH and VPH Alkane Lists
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185 Frances Avenue,Cranston,RI 02910-2211 Tel:401461-7181 Fax:401-461-4496 httn:/hw%,Nv.ESSI,aboratory.com t
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. Division ofThielsch Engineering,Inc, The blicrobiolosj,Division -
of Thiels-ch Ena incerin5,Inc.
CERTIFICATE OF ANALYSIS
Client Name: RI Analytical Laboratories,Inc,
Client Project ID: RIAL Sampling-MCP ESS Laboratory Work Order: 1308604
CURRENT SW-846 METHODOLOGY VERSIONS
Analytical Methods Prep Methods
I O1 OA-Flashpoint 3005A-Aqueous ICP Digestion
6010C-ICP 3020A-Aqueous Graphite Furnace/ICP MS Digestion
6020A-1CP MS 3050B-Solid ICP/Graphite Furnace/ICP MS Digestion
7010 -Graphite Furnace 3060A-Solid Hexavalent Chromium Digestion
7196A-Hexavalent Chromium 3510C-Separatory Funnel Extraction
7470A-Aqueous Mercury 3520C-Liquid/Liquid Extraction
7471 B-Solid Mercury 3540C-Manual Soxhlet Extraction
3011 -EDB/DBCP/TCP 3541 -Automated Soxhlet Extraction
3015C-GRO/DRO 3580A-Waste Dilution
3 08 1 B-Pesticides 5030B-Aqueous Purge and Trap
9082A-PCB 5035 -Solid Purge and Trap
3100M-TPH '
—3I 5 tr'
3260B- VOA
3270D-SVOA
3270D SIM-SVOA Low Level
9014-Cyanide
9038-Sulfate
9040C-Aqueous pH
9045D-Solid pH(Corrosivity)
9050A-Specific Conductance
9056A-Anions(IC)
9060A-TOC ,
9095E-Paint Filter
MADEP 04-1.1 -EPH/VPH
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Dependability 4 Quality 4 Service
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F ESS Laboratory. BAL Laboratory
Division ofThiclsch Eiigiijeeting,lac. The Microbiology Division
( 7 S ofThie/sch Engineering,Inc. A
CERTIFICATE OFANALPSIS
Client Name: RI Analytical Laboratories,In(;.
Client Project ID: RIAL Sampling-MCP. ESS Laboratory Work Order: 1308604
MassDEP Analytical Protocol Certification Forty
MADEP RTN:
Phis form provides certification for the following data set:1308604-01
Matrices: (X)Ground Water/Surface Water O Soil/Sediment ( )Drinking Water O Air O Other:
CAM Protocol (check all that apply below):
( ) 8260 VOC ( ) 7470/7471 I-Ig (X) MassDEP VPH ( )8081 Pesticides ( ) 7196 Hex Cr ( ) MassDEP APH
CAM 11 A CAM IIi B CAM IV A CAM V B CAM VI B CAM IX A
( ) 8270 SVOC ( ) 7010 Metals ( ) MassDEP EPH ( ) 8151 Herbicides ( ) 8330 Explosives ( ) TO-15 VOC
CAM Il B CAM Ill C CAM IV B CAM V C CAM VII1 A CAM 1X B
( ) 6010 Metals ( ) 6020 Metals ( ) 8082 PCT3 (. ) 6860 Perchlorate ( ) 9014 Total C',yanide./PAC
CAM ITT A CAM III D CAM V A CAM VIII B CAM VI A
Affirmative responses to questions A through Fare required for Presumptive Certainty Vatus
A Were all samples received in a condition consistent with those described on the Chain-of-Custody,properly Yes(X) No( )
preserved(including temperature)in the field or laboratory,and prepared/analynd within method holding times?
B Were the analytical method(s)and all associated QC requirements specified in the selected CAM protocol(s) Yes(X) No( )
followed?
C Were all required corrective actions and analytical response actions specified in the selected CAM protocol(s) Yes(X) No( )
implemented for all identified performance standard non-conformances?
D Does the laboratory report comply with all the reporting requirements specified in the CAM VII A,"Quality Yes(X) No( )
Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"?
C a.VPH,EPH,APH and TO-15 only:Was each method conducted without significant modification(s)?(Refer Yes(X) No( )
to the individual method(s)for a list of significant modifications).
b.APH and TO-15 Methods only:Was the complete analyte list reported for each method? Yes( ) No( )
F Were all applicable CAM protocol QC and performance standard non-conformances identified and evaluated Yes(X) No( )
in a laboratory narrative(including all"No"responses to Questions A through E)?
Responses to Questions C,H and I below are required for Presrutrptive Certair:ty'Ratus
G Were the reporting limits at or below all CAM reporting limits specified in the selected CAM protocols(s)? Yes(X) No( )*
Data User Note:Data that achieve Presumptive Certainty'Statuspiay not necessarily meet the data usability and
representativeness requirements described in 310 CMR 40. 1056(2)(k)and TYSG07--350.
H Were all QC performance standards specified in the CAM protocol(s)achieved? Yes(X) No( )*
I Were results reported for the complete analyte list specified in the selected CAM protocol(s)? Yes(X) No( )*
*A11 negative responses mist be addressed in an attached laboratory narrative.
I,the undersigned,attest raider thepains and penalties ofperjnry that,based upon my personal inquiry of those responsible
for obtaining the information,the material contained in this analytical report is,to.lhe.bestsof my knowledge and belief,
accurate and complete
Signature:
Date: September 04,2013
Printed Name:Laurel Stoddard Position:Laboratory Director
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185 Frances Avenue,Cranston,RI 02910-2211 Tel:401461.7181 Fax:401-4614486 htto://h�rnNv.ESSLaboratorv.coni
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s 4 ESS Laboratory BAL Laboratory
Division of Engineering,Inc. The Microbio/000yDivision
o' o
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CERTIFICATE OF ANALYSIS
Client Name: RI Analytical Laboratories,Inc.
Client Project ID: RIAL Sampling-MCP ESS Laboratory Work Order: 1308604
Client Sample ID: 1308-18481-001 ESS Laboratory Sample ID: 1308604-01
Date Sampled: 08/27/13 12:05 Sample Matrix: Waste Water
Percent Solids: N/A Units:ug/L
Initial Volume: 5 Analyst: NS
Final Volume: 5
Extraction Method: 5030B
MADE,P-VPH.Volatile Petroleum Hydrocarbon
Anal to Results(MRL) MDL Method Limit DF Analyzed Sequence Batch
C9-C10Aromatics ND(100) MADEP-VPFI 1 08/29/13 I1:38 CWH0374 CH32847
C5-C8 Aliphaticsl,2 ND(150) MADEP-VPH 1 08/29/13 11:38 [CALCJ
CS-C8 Unadjusted Aliphatics ND(150) MADEP-VPH 1 08/29/13 11:38 CWH0374 CH32847
C9-C]2 Aliphatics2,3 ND(150) MADEP-VPH 1 08/29/13 11:38 [CALCJ
C9-C12 Unadjusted Aliphatics ND(ISO) MADEP-VPH 1 08/29/13 11:38 CWH0374 CH32847
Benzene ND(1.5) MADEP-VPH 1 08/29/13 I1:38 CWH0374 CH32847
Glhylbenzene ND(5.0) MADEP-VPH 1 08/29/13 11:38 CWH0374 CF132847
Metliyl tert-Butyl Ether ND(1,5) MADEP-VPH 1 08/29/13 11:38 CWH0374 CH32847
Naphthalene ND(5.0) MADEP-VPH 1 08/29/13 11:38 CWH0374 CH32847
Toluene ND(5.0) MADEP-VPH 1 08/29/13 11:38 CWH0374 CH32847
Xylene 0 ND(5.0) MADEP-VPH 1 08/29/13 11:38 CWH0374 CH32847
Xylene PM ND(10.0) MADEP-VPH 1 08/29/13 11:38 CWH0374 CH32847
Preservative: pH<=2 MADEP-VPH CH32847
%Recovery QualiRer umlts
Surrogate:2,5-Dibromotoluene-FID 92% 70-130
Surrogate:2,5-Dlbromotoluene-PID 100% 70-130
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Dependability 4 Quality 4 Service
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Division of 7hielsch 1 Engineering, lix. The AficrobiologyDAdsion e ofThielsch E �ineerin -
Inc.
4, K
CERTIFICATE OF ANALYSIS
Client Name: RI Analytical Laboratories,Tne.
Client Project ID: RIAL Sampling-MCP ESS Laboratory Work Order: 1308604
Quality Control Data
Spike Source %REC RPD
Arialyte Result MRL Units Level Result %REC Limits RPD Limit Qualifier
MADEP-VPH Volatile Petroleum Hydrocarbon
Batch CH32847-503013
Blank
1,2,4-Trlmethylbenzene ND 5.0 y ug/L
2,2,4-Trimethylpentane NO 5.0 ug/L -
2-Methylpentane NO 5.0 ug/L
Benzene NO 1.5 - ug/L
:5-C8 Unadjusted Allphatics NO 150 ug/L
-9-C10 Aromatic NO 100 ug/L
-9-C12 Unadjusted Allphabc NO ISO ug/L
Ethylbenzene NO 5.0 ug/L
Methyl tert-Butyl Ether NO 1.5 ug/L "
MD 5.0 UYJL
rBuycyclohexane 5.8 5.0 ug/L
i-Decane 6.3 510 ug/L
Nonane(0) 8.6 5.0 ug/L
Pentane NO 5.0 ug/L
roluene NO 5.0 ug/L ,
Kylene 0 NO 5.0 ug/L
Kylene P,M NO 10.0 ug/L
Surrogate:2,5-Dlbromotoluene-FID 47.9 - ug/L 50.00 96 70.130
Surrogate 2,5-Dlbromotoluene-PID 51.7 ug/L 50.00 103 70-130
LCS
1,2,4-Trimethylben2ene 110 ug/L 100.0 110 70-130
2,2,4-Trimethylpentane 143 ug/L 150.0 95 70-130
2-Methylpentane 156 ug/L 15010 104 70-130
Benzene 53.8 ug/L 50.00 108 70-130 {
-5-C8 Unadjusted Allphatics 399 ug/L 400.0 100 70-130
-9-CIO Aromatics 109 ug/L 100.0 109 70-130 j
.t
�9-C12 Unadjusted Allphatic 257 ug/L 300.0 86 70-130 ;2
Ethylbenrene 54.8 ugJL 50.00 110 70.130
Methyl tert-Butyl Ether 166 ug/L 150.0 111 70-130
Naphthalene 108 ug/L 100.0 108 70.130, }
rButylcydohexane 77.7 ug/L 100.0 78 70-130
I'
r Dea'me 88.1 ug/L 100.0 88 70.130 e
Nonane(C9) 81.3 ug/L 100.0 81 30-130
Pentane 102 ug/L 100.0 102 70-130
roluene - 167 ug/L 150,0 111 70.130
i
Kylene 0 112 ug/L 100.0 112 - 70-130
Kylene P,M 219 ug/L 200.0 110 70-130
Sumzgate:2,5 Dibromohzluene-FID 48.6 ug/L 50.00 97 70-130
57raogale:2,5-Dlbromotoluene-PID 53.7 ug/L 50.00 107 70-130
k'
LCS Dup F
7
1,2,4-Trimethylbenzene 109 ug/L 10010 109 70-130 1 25
2,2,4-Trimethylpentane 139 ug/L 150.0 92 70-130 3 25
185 Frances Avenue,Cranston,RI 02910-2211 Tel:401461-7181 Fax:401-461-4486 httD://RM,Nv.ESSLaboratory cons
Dependability # Quality 4 Service
Paee 7 of 12
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ESS Laboratory BAL Laboratory
Division ofThic1sch Engineering,Inc. The Microbiology,Division
l nl of Thielsch Engineering,Inc. *AB
CERTIFICATE OFANALESIS
Client Name: RI Analytical Laboratories,Inc.
Client Project ID: RIAL Sampluig-MCP ESS Laboratory Work Order: 1308604
Quality Control Data
Spike Source %REC RPD
Analyte Result MRL Units Level Result %REC Limits RPD Limit Qualifier
MADEP-VPH Volatile Petroleum Hydrocarbon
Batch CH32847-5030B
2-Methylpentane ISO ug/L 150.0 100 70.130 3 25
Benzene 52.8 ug/L 50.00 106 70-130 2 25
-5-C8 Unadjusted Allphatics 384 ug/L 100.0 96 70-130 4 25
-9-C10 Aromatics 104 ug/L 100.0 104 70-130 4 25
-9-C12 Unadjusted Allphattcs 238 ug/L 300.0 79 70.130 8 25
Ethylbenzene 54.7 lug/L 50.00 109 70-130 0.2 25
Methyl tert-Butyl Ether 161 ug/L 150.0 107 70-130 3 25.
Naphthalene 101 ug/L 100.0 104 70.130 4 25
i-Butylcyclohexane 70.9 ug/L 100.0. 71 70-130 9 25
t-Decane 76A ug/L 100.0 76 70.130 15 25
nnan J[9,1 77 F q/1 inn n 7e 30 r30 rn 29
-
Pentane 101 Ug/L 100.0 101 70-130 1 25
roluene 161 ug/L 150.0 109. 70.130 2 25
Xylene 0 112 ug/L 100.0 112 70-130 0.2 25
<ylene P,M 220 ug/L 200.0 110 70-130 0.1 25
Surrogate:1,5-Dtbromota/uene-FID Sl.l ug/L 50.00 101 70-130
5urra3a1e:7,5-0tbramotoluene-PID 59,5 ug/L S0.00 109 70-130
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Division ofThielscb Engineeting, Inc. TheAlicrobiolo��Division
ofThieisch Eggincermg,Inc. A
CERTIFICATE OF ANAL 3'SIS
Client Name: RI Analytical Laboratories, Inc.
Client Project rD: RIA.L Sampling-MCP ESS Laboratory Work Order: 1308604
Notes and Definitions
G-06 pH<=2
(i Analyte included in the analysis, but not detected
ND Analyte NOT DETECTED at or above the MRL(LOQ),LOD for DoD Reports,MDL for J-Flagged Analytes
dry Sample results reported on a dry weight basis
RI)D Relative Percent Difference
MDL Method Detection Limit
MRL Method Reporting Limit
LOD Limit of Detection
LOQ Limit of Quantitation
DL Detection Limit
UV Initial Volume
F/V Final Volume
§ Subcontracted analysis;see attached report
1 Mange result excludes concentrations of surrogates and/or internal standards eluting in that range.
2 Range result excludes concentrations of target analytes eluting in that range.
3 Range result excludes the concentration of the C9-C'10 aromatic ranvP
Avg Results reported as a mathematical average.
Mt. No Recovery
[CALL] Calculated Analyte
SUB Subcontracted analysis;see attached report
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185 Frances Avenue,Cranston,RI 02910-2211 Tel:401-461-7181 Fax:401461-4486 htta_/_/ii,�%,Nv.ESSLaboratory,com
Dependability 4 Quality 4 service
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Division ofThic1sch Engineering, Inc. The Microbiolob-3,Division
1 A130I of Thielsch&Wr b Bering,Inc. A
CERTIFICATE, OFANALYSIS
Client Name: RI Analytical Laboratories;Inc.
Client Project 1D: R1AL Sampling-MCP ESS Laboratory Work Order: 1308604
ESS LABORATORY CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL
Department of Defense(DoD)Environmental Laboratory Accreditation Program(FLAP)
A2LAAccredited:Testing Cert#2864.01
http•//www a2la ore/scopee6df/2864-01 pdf
Rhode Island Potable and Non Potable Water:LAI00179
bttp://iv%viv.heaIth.r-i.gov/1abs/ivaterlabs-instate.plip
Connecticut Potable.and Non Potable Water,Solid and Hazardous Waste:PH-0750
http://wwNv.ct.gov/dplVlib/dph/environmental health/environmental laboratories/pdf/OutofStateCommercialLaboratories pdf
Maine Potable and Non Potable Water,and Solid and Hazardous Waste: RI0002
http://wivNv.maine.gov/dep/blwg/topie/vesseU[ab list pdf
Massachusetts Potable and Non Potable Water:M-RIO02
http://Public.dep.st,,ate.ma.us/labcert/labeert.aspx
New Hampshire(NELAP accredited)Potable and Non PotableWater,Solid and Hazardous Waste:2424
http://www4.e og v.rJi gov/des/nhelap/narnesea.rch asp
New York(NELAP accredited)Non Potable Water,Solid and Hazardous Waste: 11313
http://www.wads%voiih org/labcert/elap/comm html
New Jersey(NELAP accredited)Non Potable Water,Solid and Hazardous Waste:R1.006
http://datainine2.state.ni.us/dep/DEP OPRA/ `
United States Department of Agriculture Soil Permit:S-54210
Maryland Potable Water:301
http://vvwiv.mde.state.md.us/assets/documentfWSP labs-2009apr20_pdf
CHEMISTRY H
I
A2LAAccredited:Testing Cert#2864,01 {
Lead in Paint,Phthalates,Lead in Children's Metals Products(Including Jewelry)
http://iv%v%Y.A2LA.org/dirsearchneFv/neivsearch.cfm
CPSC ID# 1141
Lead Paint,Lead in Children's Metals Jewelry
hM.'/hvNvw.cpsc.pov/cgi-bin/labapolist ash
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Attachment B
>arnple and Cooler Receipt Checklist SOP 10_0001
Client: RIAL ESS Project ID: 13080604
Client Project ID: Date Project Due: 9/3/13
t 3
Shipped/Delivered Via: Client Days For Projec D:47
[teens to be checked upon receipt: j
1. Air Bill Manifest Present? *No 10. Are the samples properly preserved: Yes
Air No.: 11. Proper sample containers used? Yes
2. Were Custody Seals Present? No 12. Any air bubbles in the VOA vials? No
3. Were Custody Seals Intact? F-Ni-A-1 13. Holding times exceeded? No
4. Is Radiation count < 100 CPM? Yes 14. Sufficient sample volumes? Yes
5. Is a cooler present? Yes 15, Any Subcontracting needed? No
Cooler Temp: 3.4 16. Are ESS labels on correct container aflNo
Iced With: Ycepacks 17. Were samples received intact? a No
6, Was COC included with samples? Yes ESS Sample iDs:
7. Was COC signed and dated by client? Yes Sub Lab:
8. Does the COC match the sample Yes Analysis:
9. Is COC complete and correct? Yes TAT:
18, Was there need to call project manager to discuss status? If yes, please explain.
Who was called?: By whom?
Sample Number Properly Preserved Container Type #of Containers Preservative
1 Ye 40 ml-VOA 2 HCL }
Completed By, DateMme: OZ'
Reviewed By: Date/Time: a'
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A-ni viieal:Laborat6fi-,s=
41 Illinois Avenue 131 Coolidge St, Suite 105
Warwick, RI 02888-3007 Hudson,MA 01749-1331 Ei
Te1:401-737-8500 Te1: 978-568-0041 0
Fax: 401-738-1970 Fax: 978-568-0078 0 0 v
:':': •_: - . :. . ...:. .. •
Collected: 'Coilected Our Sample IderitifIcatioiis'. Chi a
l 8/27/13 12:05 1308-18481-001 vUW-132030 1780 Main St W
Barnstable G 2V H WW X
;Send Re ort and Invoice To. _ _
Company: R,I. Anal ical Laboratories Inc.
Subcontractor In;foxmation
Address: 41 111inois Avenue Sub° °tractor: ESS Laboratory
Cityl State I Zip: Warwick, RI 02888 Addre sLine 1: 185 Frances Ave
Telephone: 8OO-937-2580 Addre s Line 2:
Fax: 401-738-1970
Report To: Data Reporting city: Cranston state: R1 Zip: 02910-2211
Email: datareporting@rianalyticai.com T lephone: 401-461-7181 FAX:
Coaraet for quetmioas Kristin Phelan ext: 116 401-461-4486
Emil: kphelan@rianalytical.corn
R iagiiished By ...:-..
te:
Received By_
: . .
g Date Time.:._
r 3 _. Turn:Arotm d Time
ro a� ad Norman:
Z �730 X RUSH: 3-4 Business Days
-,rTOject.Commenfs`' :..
NDtiSh
Notes to e ;_...
Subcontract (:p# 'Zg9.$Z r> Results due 9/4/13. Thank you. �, �-j Courier �S
Laboratory:
�� p�. DHL
stainers:P=Poly,G=Gass,AG=Amber Glass,l/=Val,St=Sterile Presemat;vecq=g4=NH<CI,H=HCI, =MeOH N=Matri x Codes•GW=Groundwater,SW=Surface Water,WW=Wastewater, DW=Drinking Water,S=Soil,SL=Sludge,A=AIr ell,6=B'N=H O N=Swab,p= l=Narkordo: 0 ; ; , ;
HNO�,NP-None,S=H2S0,,SB=NaHSOa,SH=NaOH,T=NazSiOa,Z=ZnOAc
---.------ Page 1 of 1 .
330-253-4489 02:32:06 p.m. 09-18-2013 6/7
m mmmly
ENVIRONMENTAL TECHNOLOGIES, INC. September 17,2013 '
Analytical,Laboratories Client: Envirotech Laboratories,Inc.
Address: 8 Jan Sebastian Dr unit 12
Sandwich,MA 02563
Received:8/30/2013
Project#:WW 132030
Client TDO Lab(Dt# Collected Anal a Result Units Matrix Method DF LOB( Run Analyst
WW132030 1780 1314637-01 16-Jun-13 2,3,7,8-TCDD ND pg/1 L 1613B 2 1 16-Sep-13 CM
Main St
Page 4.
t
"Analytical Integrity-" EPA Certified NELAP Certified
3310 Win Street Cuyahoga Falls, Ohio 44223 • Phone:330-253-8211 • Fax: 330-253-4489 S
Web Site:weww.settek.com
y
9
i
330-253-4489 02:32:17 p.m. 09-18-2013 7/7
Summit Environmental Technologies, Inc.
Method 1613
QC Report
Batch ID: 1109 . ICAL Date : 5/2/2013 Extraction Date: 9/4/2013
Blank Results: 2,3,7,8-TCDD<1.0 pg/L
Labeled Unlabeled
Compound Compound
% Recovery %Recovery
13C-2,3,7,8- 2,3,7,8- Analysis
Parameter TCDD TCDD Date
LCS 57.3 74.3 9/8/2013
Acceptance Limits 25-141 73-146
CCV1 99.5 95.8 9/16/2013
CCV2 102.6 107.9 9/16/2013
Acceptance Limits 85-117 82-123
Blank 48.4 9/8/2013
Acceptance Limits 25-164
Sample
1314637-01 39.1 9/16/2013
Acceptance Limits 25- 164
- I
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4
330-253-4489 02:30:54 p.m, 09-18-2013 2/7
Rev. 12 I I�IIIII IIIIu III�I llll�lll�fill!u llll I��IIII III��IIIII IIIII IIIII IIIIIIIIIII(ll llll
Date: 07/27/13
Summit Environmental Techr Order ID: 1314637 COOLER-
Cooler Receipt For,,,
r Initials of person Inspecting cooler and samples.--L
Client:!'11 (11 1^e3� y�7 Order Number:
Date Received:T Time Received: lc.L' cz c7 Date cooler(s)opened and samplesiinspected: L o�
Number of Coolers/Boxes:_ N/A
Shipper: FED EX UP$ DHL Airborne US Postal Walk-in Pickup Other:
Packaging: Peanuts ubble Wrap Paper Foam None Other:
Tape on cooler/box: ` ✓ N N/A
Custody Seals Intact Y N/A
C-O-C in plastic ( N N/A
Ice lue Ice present / absent / etnl ted • N/A
Sample Temperature IR Gun#16020459 CF C 16 .5 `°C N/A
N/A
(see page 2 for scan results)
"*Use 1 sheet per sample for Radiological Testing, if sample is HOT,the Radiological Safety Officer must be notified
Immediately.
C-O-C filled out properly N N/A
Samples In separate bags 6y�> N N/A
Sample containers intact* ( Y� N N/A
*If no,list broken sample(s):
Sample label(s)complete(ID,date,etc.) OY N N/A
Label(s)agree with C-O-C \ " N N/A
Correct containers used N N/A
Sufficient sample received N N/A
Bubbles absent from 40 mL vials** Y N N/A
:)
**Samples with bubbles<6mm are acceptable. Indicate bubble size if>6mm.
Was client contacted about samples Y N
Will client send new samples Y N
' Client contact:
i
k
Date/Time:
I{:
Logged In by:
Comments:
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en M 11 4e e_. n___ • -rn
330-253-4489 02:31:14 p.m. 09-18-2013 3/7
I E I ENVIRONMENTAL TECHNOLOGIES,INC.
Analytical Laboratories
LABORATORY REPORT
Client
Envirotech Laboratories, inc.
8 Jan Sebastian Dr unit 12
Sandwich, MA 02563
Order Number
1314637
B rej e n tumbe r
WW132030
issued
Tuesday, September 17, 2013
Total Number of Pages
4 (excluding C.O.C. and cooler receipt form)
a
G
Approved By :
a
QA Manager
4
Certifications; A2LA/DOD 0724.01,Alabama 41600,Arkansas 88-0735,California 07256CA,Colorado,Connecticut PH-0105, .
Delaware,Florida NELAC E87688,Georgla E87688 and 943,Idaho OH00923,Illinois 200061 and Reg.5,Indiana
C-OH-13,Kansas E-10347,Kentucky(underground Storage Tank)3,Kentucky 90146, Louisiana 04001 and
LA12004,Maine 2012015,Maryland 339,Massachusetts M-OPH923,Michigan(Reg.S),Minnesota 409711,
Montana CERT0099,New Hampshire 2996,New Jersey 01-1006,New York 11777,North Carolina 39705 and
631,Ohio 4170,Ohio VAP CL0052,Oklahoma 9940,Oregon OH2O0001,Pennsylvania 68-01335,Rhode Island
tA000317,South Carolina 92016001,Tennessee TN04018,Texas T104704466-11-5,Region 5 WG-15J,Region E
8 8TMS-L,USDA/APHIS P330-11-00244,Utah OH009232011-1,Vermont VT-87688,Virginia 00440 and 1581, '
Washington C891,West Virginia 248 and 9957C and E87688,Wisconsin 399013010
"Analytical Integrity" EPA Certified - NELAP Certified
3310 Win Street CuyahogaTalis, Ohio 44223 • 'Phone: 330-253.8211 Fax:330.253-4489
Web Site:www.settek.com
p
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330-253-4489 02:31:33p.m. 09-18-2013 4/7
wmMMIT
LijENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
2
Sample Summary
Client: Envirotech Laboratories Inc.
Order Number: 1314637
Laboratory ID Client ID Matrix Sampling Date
1314637-01 WWI 32030 1780 Main Liquid 6/16/2013
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"Analytical integrity" EPA-Certified_'• NELAP Certified
3310 Win Street Cuyahoga-Falls, Ohio 44223 • Phone:330-253-8211 • Fax: 330-253-4489
Web Site:www.settek.com F
4
fa
330-253-4489 02:31:42 p.m. 09-18-2013 5/7
U A11h Agh
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8 1 1 ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
3
Report Narrative
Client: Envirotech Laboratories, Inc.
Order Number: 1314637
No problems were encountered during analysis of this order number, except as noted.
Method numbers, unless specified as SM or ASTM, are EPA methods.
Method of analysis for TCLP Volatiles is 1311/8260B
Method of analysis for TCLP Metals is 1311/6010B and 1311/7471A
Method of analysis for TCLP BNA is 1311/8270C
Data Quallfiers:
B=Analyte found in the method blank
J=Estimated concentration of analyte between MDL(LOD)and Reporting Limit(LOQ)
C=Analyte has been confirmed by another instrument or method
E=Analyte exceeds the upper limit of the calibration curve. Matrices:
D=Sample or extract was analyzed at a higher dilution A=Air
X=User defined data qualifier. C=Cream
S=Surrogate out of control limits DW=Drinking Water
U=Undetected L=Liquid
a=Not Accredited by NELAC o=Oil
St.=Sludge
ND= Non Detected at LOQ SO=Soil
DF=Dilution Factor S=Solid
T=Tablet
TC=TCLP Extract
Limit Of Quantitation(LOQ)=Laboratory Reporting Limit(not adjusted for dilution factor) WW=Waste Water
Limit Of Detection(LOD)=Method Detection Limit W=Wipe
Practical Quantitation Limit(PQL)=(same as LOQ) !
Method Detection Limit(MDL)=(same as LOD).
Reporting Detection Limit(RDL)=(same as LOD)
Estimated uncertainty values are available upon request.
The test results meet the requirements of the NELAC standard,except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies,Inc.and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental .echn.ologies, Inc.or..the.client.for.which this
report was issued. The results contained in this report are only representative of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies,Inc.Is not
responsible for use or Interpretation of the data included herein,
"Analytical Integrity" EPA Certified • NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 • Phone: 3307253-8211 • Fax: 330-253-4489
Web Site;www.settek.com
1. 1
ATSDR-ToxFAQsTM:Di-n-butyI Phthalate Page I of 4
Agency for Toxic Substances & Disease Registry
ToxFAQsTM for Di-n-butyl Phthalate
(Di-n-butil ftalato)
September 2001
CAS# 84-74-2
i PDF Version, 2s KB
This fact sheet answers the most frequently asked health questions about di-n-
butyl phthalate. For more information, you may call the ATSDR Information
Center at 1-888-422-8737. This fact sheet is one in a series of summaries about
hazardous substances and their health effects. This information is important
because this substance may harm you. The effects.of exposure to any hazardous
substance depend on the dose, the duration,how you are exposed,personal traits
and habits, and whether other chemicals are present.
Highlights
Di-n-butyl phthalate is a iffdhufactured chemical that is added to plastics, paint, glue, hair
spray,another household products..It is commonly found in the environment, and most
people are exposed to low levels in the air, water, and food. No harmful effects have been found
in humans. In laboratory animals, oral exposure to very high levels can cause impaired
reproduction and developmental effects. This substance has been found in at least 471 of the
1,585 National Priorities List sites identified by.the Environmental Protection Agency(EPA).
What is di-n-but phthalate?
y. p
Di-n-butyl phthalate is a manufactured chemical that ioes..not occur naturally. It is an odorless`
and oily liquid that is colorless to faint yellow in color. It is slightly soluble in water-and does
not evaporate easily.
Di-n-butyl phthalate is used to make plastics more flexible-acid is also�in carpet backings,
pantulue�insect ieellenta.,rhair_spray--nail polsh,and_rocket fuel'.
What happens to di-n-butyl phthalate when it enters the
environment?
. Di-n-butyl phthalate is released to air as a vapor.It can react.with other chemicals in . .
the air and is usually broken down within a few days. Di-n-butyl phthalate can also
attach to particles in the air and eventually settle to the land and water.
. Most of the di-n-butyl phthalate in water attaches to sediment and settles out of the
water or is broken down by bacteria. Small amounts may evaporate to the air.
When released to the soil, it attaches to soil particles and is broken down by bacteria.
. There is no evidence that it builds up in the food chain. .
s
http://www.atsdr.cdc.Rov/toxfags/tf.asp?id=858&tid=167 9/23/2013
ATSDR-ToxFAQsTM: Di-n-butyl Phthalate Page 2 of 4
How might I be exposed to di-n-butyl phthalate?
e Most people are probably exposed to low levels of di-n-butyl phthalate in the air
because it is used in so many household products.
People who use products which contain di-n-butyl phthalate, such as nail polish,
may be exposed by breathing it in the air or getting it on their skin.
. The general population.may also be exposed by eating food containing di-n-butyl
phthalate, such as fish and shellfish, or food which is packaged or stored in materials
containing di-n-butyl phthalate.
. If you work or live near a factory where di-n-butyl phthalate is made or used,you
could be exposed to higher than usual levels.
o People living near uncontrolled hazardous waste sites may also be exposed to higher
than usual levels of di-n-butyl phthalate.
How can di-n-butyl phthalate affect my health?
Di-n-butyl phthalate appears to have relatively low toxicity.Adverse effects have not been
reported in humans as a result of exposure to di-n-butyl phthalate..
In laboratory animals, studies show that eating large amounts of di-n-butyl phthalate can affect
their abilityto reproduce Sperm produc:Uap-can decrease,but r-au-irps to p.aar normal le-vels
when exposure stops. Large amounts of di-n-butyl phthalate repeatedly applied to the skin for
a long time can cause mild irritation.We do not know if similar effects would occur in humans.
How likely is di-n-butyl phthalate to cause cancer?
There have been no cancer studies in humans and the one study in laboratory animals is
inadequate. The EPA has determined that di-n-butyl phthalate is not classifiable as to human
carcinogenicity based on inadequate evidence in both humans and animals.
How can di-n-butyl phthalate affect children?
It is likely that health effects seen in children exposed to high levels of di-n-butyl phthalate will
be similar to the effects seen in adults. We do not know_ whether-children differ from adults in
their susceptibility to di-n-butyl phthalate.
We do not know if exposure to di-n-butyl phthalate will result in birth defects or other
developmental effects in people. Birth defects have been observed in laboratory animals
exposed to high levels of di-n-butyl phthalate during development. Death,low body weights,
skeletal effects, cleft palate, and damage to the testes have been observed in animals exposed
during development.
How can families reduce the risk of exposure to di-n-butyl
phthalate?
Di-n-butyl phthalate is used in many household products.The level of di=n-butyl phthalate in a
product is higher when the product is new than when the product is old. Because di-n-butyl
phthalate may be in some toys, children chewing on such toys could be exposed; however, no
measurements have yet been made to show whether children are exposed in this way. E
httt)://www.atsdr.cdc.Qov/toxfaas/tfasr)?id=858&tid=l67 9/23/2013 w
ATSDR- ToxFAQsTM: Di-n-butyl Phthalate Page 3 of 4
Children should avoid playing in soils near uncontrolled hazardous waste sites where di-n-
butyl phthalate may have been discarded.
Is there a medical test to show whether I've been exposed to di-n-
butyl phthalate?
Tests are available to measure di-n-butyl phthalate in blood and body tissues, and its major
breakdown products in urine. However, these tests cannot determine whether you will
experience health effects or be used to predict the nature or severity of any effects. Because
special equipment is needed, these tests are not usually done in the doctor's office.
Has the federal government made recommendations to protect
human health?
The EPA recommends that levels of di-n-butyl phthalate in lakes and streams should be limited
to 34 parts of di-n-butyl phthalate per million parts of wate (34�,ppm),,to prevent possible
human health effects from drinking water or eating fish contaminated with this chemical.
The Occupational Safety and Health Administration (OSHA)has set a limit of 5 milligrams of
di-n-butyl phthalate per cubic meter of g/
ace air(5 workplace m ma)for 8 hour shifts and 4o hour
work weeks.
References
Agency for Toxic Substances and Disease Registry(ATSDR). 2001.Toxicological Profile for Di-
n-butyl phthalate. Update.Atlanta; GA: U.S. Department of Health and Human Services,
Public Health Service.
Where can i get more information?
If you have questions or concerns, please contact your community or state health or
environmental quality department or:
For more information, contact: ,
Agency for Toxic Substances and Disease Registry
Division of Toxicology and Human Health Sciences
1600 Clifton Road NE, Mailstop F-57
Atlanta, GA 30333
Phone: 1-800-CDC-INFO . 888-232-6348 (M)
Fax: 1-770-488-4178
Email: cdcinfo@cdc.gov
r
ATSDR can also tell you the location of occupational and environmental health clinics. These
clinics specialize in recognizing, evaluating, and treating illnesses resulting from exposure to 4
hazardous substances.
b
Information line and technical assistance:
Phone: 888-422-8737 z
FAX: (770)-488-4178. .
To order toxicological profiles, contact:
Fs.
i3
ki
httn://www.atsdr.edc.gov/toxfaos/tf.asn?id=R5R&tid=167
ATSDR-ToxFAQSTM: Di-n-butyl Phthalate Page 4 of 4
National Technical Information Service.
5285 Port Royal Road
Springfield,VA 22161
Phone: 800-553-6847 or 703-605-6000
Disclaimer
All ATSDR Toxicological Profile, Public Health Statement and ToxFAQs PDF files are
electronic conversions from paper copy or other electronic ASCII text files. This conversion
may have resulted in character translation Or format errors. Users are referred to the original
paper copy of the toxicological profile for the official text, figures, and tables. Original paper
copies can be obtained via the directions on the toxicological profile home-page, which also
contains other important information about the profiles.
• Page last revievved:March 3,2011
• Page last updated:October 21,2oii
• Content source:Agency for Toxic Substances and Disease Regis
........................................................................................................................................................................................................................................................................................................:..............................
Agency for Toxic Substances and Disease Registry,477o Buford Hwy NE,
Atlanta,GA 30341 SA 90V �
Contact CDC:800-232-4636/TTY: 888-232-6348 U}}Government Made Easy
i
http://www.atsdr.cd.e.gov/toxfaqs/tfasp?id=858&tid=l 67 9/23/2013
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1l4rE of MA`�'c UNDERSTANDING EXTRACTABLE PETROLEUM HYDROCARBONS and
VOLATILE PETROLEUM HYDROCARBONS WATER TEST RESULTS
The purpose of this informational handout is to help you understand petroleum test results for your drinking
water. The Maine Department ,of Environmental Protection [DEP] relies on laboratory tests called EPH
[Extractable Petroleum Hydrocarbons] and VPH [Volatile Petroleum Hydrocarbons] to test for the presence of
gasoline or fuel oil in drinking water. These tests provide information needed to determine if drinking water
supplies near petroleum spills are contaminated with petroleum above health-based guidelines.
Petroleum does not contain just one single compound [for example benzene], but many hundreds of
compounds, all based on the chemistry of carbon and hydrogen. That is why petroleum compounds are
commonly referred to as "hydrocarbons.". Some of the compounds contained in petroleum [again, for example
benzene] are more harmful than others. The EPH and VPH tests identify concentrations of the more harmful
compounds and those that are more abundant in fuels [called target compounds) and also identify all of the
remaining petroleum hydrocarbons by grouping compounds with similar chemical properties and toxicity into
"fractions" as shown on the table below. Each fraction has its own health guideline.
EPH/VPH Defined Hydrocarbon Fractions
Hydrocarbon Fraction - Analytical Method
C9-C18 aliphatics EPH
C19-C36 aliphatics EPH
C11-C22 aromatics EPH
C5-C8 aliphatics VPH
C9-C12 ali hatics VPH
C9-C10 aromatics VPH
To determine the health risk from petroleum contamination i
r n your water, DEP may have to use one or both
tests. Our recommendations for testing depend on the type of petroleum product spilled as outlined in the t
table below.
Recommendations for EPH and VPH Testing
Petroleum Product VPH EPH
Gasoline X i
Fresh diesel/#2 fuel oil X X
Weathered diesel/#2 fuel oil X r
#3-#6 fuel oils X
Waste oil X X
Jet fuels/kerosene X X r
Mineral oil/dielectric oils X
Unknown oils or sources X X
i
I
To determine if a water supply is safe to use, the DEP compares sample results from these tests to a list of
I
health-based guidelines developed by the Maine Center for Disease Control and Prevention's [CDC's] I
Environmental Toxicology Program. These guidelines are conservative and assume you will drink u
approximately two quarts of water from this particular water supply every day for 70 years. Although EPH/VP,H
test results are detailed and require explanation, these test methods do a better job of addressing the health
implications of petroleum releases than previous [simpler] testing and allow the DEP to better determine
appropriate actions.for protecting drinking water based on human health concerns.
Below are explanations of the various sections of most laboratory reports.
Result: Numbers contained in this column represent the concentration of target compounds and fractions
detected in our water.v Compare these numbers to the drinking water guidelines in'the table below. Results
above the guidelines indicate that the water may not be safe for regular use without treatment. Results less
than the guidelines are generally considered to be safe for use. When test results are close to the drinking
water guideline, the DEP may still wish to take measures to address the petroleum found.
GUIDELINES FOR TARGET COMPOUNDS AND FRACTIONS
Test Target Compound Guideline[ug/L or PPB]
Benzene 4
Eth (benzene 30
Meth I-tert-but I ether MTBE 35
VPH Naphthalene 10
Toluene 600
Total x lenes 1,000
TEST Fractions:
C5-C8 Aliphatic Hydrocarbons 300
C9-C12 Aliphatic Hydrocarbons 700
C9-C10 Aromatic Hydrocarbons 200
2-Meth ilLaphthalene 30
Acena hthene 1 400
Acena hth lene 400
Anthracene 2,000
PBeEnzo(g,hEj)peryIene
oa ne 0.0 5
obanthene 0.5
200
EPH
Benzo k fluoranthene 15
Chrysene 1 50
Dibenz a,h anthracene 0.05
�Fluoranthene 300TEST
Fluorene 300
Indeno 1,2,3-cd rene 0.5
Na hthalene 10
Phenanthrene 200
P rene 200 `
Fractions:
C9-C18 Aliphatic Hydrocarbons 700
F-
C19-C36 Aliphatic Hydrocarbons 14,000 i k
C11-C22 Aromatic Hydrocarbons 200 I G
The analytical results section also contains the following information:
• Range/Target Analyte: This is a list of the parameters that are included on the test. Note that unadjusted
results should be iqnored. They are included only for DEP information purposes.
• Surrogate %Recovery. Surrogate chemicals are added to the sample in the laboratory to determine the
accuracy of the test. These chemicals were not found in your water.
• RL [Reporting Limit]: The minimum concentration of a compound or a hydrocarbon fraction that the.
laboratory will report. Concentrations less than this RL are reported out in the result column as "U"
(undetected) or < [less than] the reporting limit, In some cases the laboratory will report an estimated
concentration lower than the RL and flag the result with a "J"to indicate the number is estimated.
• Units: How the sample was measured, usually in micrograms per liter [ug/1] or parts per billion [ppb] for r
water samples. Micrograms per liter are comparable to parts per billion.
For Further Assistance: If you have questions or need assistance understanding your petroleum
test results and what they mean, please'call the DEP chemist at 207-287-7878.
MITAn-Allysis Request / Chaiift -®f Cyst®d '° 'EtdVIROAIMENTALTECIiNOLpGtES, INC. � �
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Order ID:_ 1314637 COC
8 Jan Sebastian D F
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02563 1780 Main St W.Barnstable,MA.
t Client Phone Report To
5088886460 Ron Saari
Clicnt Par No. to Receive Results by Fnx PO Number
506 8886446 082713
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Contact Person
Quote Number
Ron Saari :; "'~::. , : 2
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CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. RI Analytical
8 Jan Sebastian Dr.Unit 12 M RI 015 _
PWS: Project Name: Page, Patrick Sandwich, MA 02563 Address 41 Illinois Avenue
(508)888-6460 Warwick, RI 02888
Sampler: R. Saari 1-800-339-6460 Phone# 401-737-8500
FAX(508)888-6446 Fax# 401-738-1970
Lab ID# Date Time Comp Grab IStation location DEP ID. Container Pres. Sample type Analysis requested
WW-132030 08/27/13 1205 X 1780 Main St. W Barnstable Wastewater EPA 625
2� ;-'';.�` Wastewater EPFi with PAH
C !i Wastewater PCB 608
P6,,+i<- YzSc Wastewater -TOC
C LaA-� 45-4 Wastewater Petroleum Scan
Z Ups}- Wastewater EPA 8260
PIa� G /j�D .Wastewater Hg
ZU04 tkZ. _ Wastewater VPH
Call._Lab with any
'Exceeded;MCL -
Relinquished: Date/T' a Recei d: Religuished: Date/Time Received:
13 �3"
Relin uishe / Date/Time Received: Relinquished: Date/Time Received:
CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. Client: Patrick Page
8 Jan Sebastian Dr., Unit 12
Proj. No. Project Name: 1780 Maid St W Barnstable Sandwich, MA 02563 I Address: 1780 Main St
(508)888-6460/1-800-339-646 W. bamstable,MA 02668
Sampler: ` FAX 508 8884446
P�71
Phonet€: 508 280 7243
a
Fax#:
dab°ID. , Dake Time comp Grad ati
Sample locon` container Pros. Analysis Requested f
-12Q EPA 625
L EPH with PAH
PC
B
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Total N� BOD CO
D T C
U
C�ZS I� Petroleum Scan
VDL �Ct EPA 8260
I) RECRA 8 metals
I CA
(( r
Relingiished' Datofrlm Received- Reliquished: Datefrime
' f _ Received:
IqID
RelinGujShed: % DatelFime Received: Relinquished: Datefrime Received:
Attachment B
;ample and Cooler Receipt Checklist SOP 10_0001
Client: RIAL ESS Project ID: 13080604
Client Project ID: Date Project Due: 9/3/13
Shipped/Delivered Via; Client Days For Projec€�
items to be checked upon receipt:
1. Air Bill Manifest Present? FT No 10. Are the samples properly preserved, Yes
Air No.: 11. Proper sample containers used? FYes
2. Were Custody Seals Present? No 12. Any air bubbles in the VOA vials? No
3. Were Custody Seals Intact? NIA 13. Holding times exceeded? No
4. Is Radiation count < 100 CPM? Yes 14. Sufficient sample volumes? Yes
5. Is a cooler present? Yes 15. Any Subcontracting needed? No
Cooler Temp: 3.4 16. Are ESS labels on correct container e lNo
Iced With: Ice packs 17. Were samples received intact? a No
6. Was COC Included with samples? Yes ESS Sample IDs:
7. Was COC signed and dated by client? Yes Sub Lab:
8. Does the COC match the sample Yes Analysis:
9. Is COC complete and correct? Yes TAT:
18. Was there need to call project manager to discuss status? If yes, please explain.
Who was called?: By whom?
Sample Number Properly Preserved Container Type #of Containers Preservative
1 Ye 40 ml-VOA 2 HCL
Completed By: Date/Time: 0�
Reviewed By: Date/Time: 'p- L15P O
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Page I of 12 4
330-253-4489 02:31:14 p.m. 09-18-2013 3/7
SUMMIN
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
LABORATORY REPORT
Client
Envirotech Laboratories, Inc.
8 Jan Sebastian Dr unit 12
Sandwich, MA 02563
Order Number
1314637
Project Number
WW132030
Issued
Tuesday, September 17, 2013
Total Number of Pages,
4 (excluding C.O.C. and cooler receipt form)
Approved By :
i
QA Manager
k
Cerfifications; A2LA/DOD 0724.01,Alabama 41600,Arkansas 88-0735,California 07256CA,Colorado,Connecticut PH-0105,
Delaware,Florida NELAC E87688,Georgia E87688 and 943,Idaho OH00923,Illinois 200061 and Reg.5,Indiana
C-OH-13,Kansas E-10347,Kentucky(underground Storage Tank)3,Kentucky 90146, Louisiana 04061 and =.
LA12004,Maine 2012015,Maryland 339,Massachusetts M-OPH923,Michigan(Reg.5),Minnesota 409711,
Montana CERT0099,New Hampshire 2996,New Jersey OH006,New York 11777,North Carolina 39705 and
631,Ohio 4170,Ohio VAP CL0052,Oklahoma 9940,Oregon OH2O0001,Pennsylvania 68-01335,Rhode Island
LA000317,South Carolina 92016001,Tennessee TN04018,Texas T104704466-11-5,Region 5 WG-15J,Region
8 8TMS-L,USDA/APHIS P330-11-00244,Utah OH009232011-1,Vermont Vr-87688,Virginia 00440 and 1581,
Washington C891,West Virginia 248 and 9957C and E87688,Wisconsin 399013010
k
"Analytical Integrity" - EPA Certified - NELAP'Certified
3310 Win Street Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 Fax: 330-253-4489
Web Site:www.settek.com
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330-253-4489 02:31:33 p.m. 09-18-2013 4/7
K;M00PI am Am am Am IT
ENVIRONMENTAL TECHNOLOGIES, INC.
LLJ Analytical Laboratories
2
Sample Summary
Client: Envirotech Laboratories, Inc.
Order Number: 1314637
Laboratory ID Client ID Matrix Sampling Date
1314637-01 WW132030 1780 Main Liquid 6/16/2013
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"Analytical Integrity" EPA Certified NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 . Phone:330-253-8211 Fax: 330-253-4489
Web Site;www.settek.com
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330-253-4489 02:31:42p.m. 09-18-2013 5/7
sp—qu, ISUMMIMT
III I ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
3
Report Narrative
Client: Envirotech Laboratories. Inc.
Order Number: 1314637
No problems were encountered during analysis of this order number, except as noted.
Method numbers, unless specified as SM or ASTM, are EPA methods.
Method of analysis for TCLP Volatiles is 1311/8260B
Method of analysis for TCLP Metals is 1311/6010B and 1311/7471A
Method of analysis for TCLP BNA is 1311/8270C
Data Qualifiers:
B=Analyte found in the method blank
J=Estimated concentration of analyte between MDL(LOD)and Reporting Limit(LOQ)
C=Analyte has been confirmed by another instrument or method
E=Analyte exceeds the upper limit of the calibration curve. Matrices:
D=Sample or extract was analyzed at a higher dilution A=Air
X=User defined data qualifier. C=Cre
am
S=Surrogate out of control limits DW=Drinking Water
U=Undetected L=Liquid
a=Not Accredited by NELAC O=oil
SL=Sludge
ND= Non Detected at LOQ SO=Soil
DF=Dilution Factor S=Solid
T=Tablet
TC=TCLP Extract
Limit Of Quantitation(LOQ)=Laboratory Reporting Limit(not adjusted for dilution factor) W/y=Waste Water
Limit Of Detection(LOD)=Method Detection Limit W=Wipe
Practical Quantitation Limit(PQL)=(same as LOQ)
Method Detection Limit(MDL)=(same as LOD)
Reporting Detection Limit(RDL)=(same as LOD)
Estimated uncertainty values are available upon request.
The test results meet the requirements of the NELAC standard,except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies,Inc.and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc.or the client for which this
report was Issued. The results contained in this report are only representative.of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies,Inc,is not
responsible for use or Interpretation of the data included herein. '
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"Analytical Integrity" EPA Certified NELAP Certified
3310 Win Street Cuyahoga Falls, Ohio 44223 • Phone:330-253-8211 • Fax: 330-253-4489
Web Site:www.settek.com
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330-253-4489 02:32:06 p.m. 09-18-2013 6/7
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r=0012 SummIT
ENVIRONMENTAL TECHNOLOGIES, INC. September 17,2013
Analytical Laboratories Client:Envirotech Laboratories,Inc.
Address: 8 Jan Sebastian Dr unit 12
Sandwich,MA 02563
Received:8/30/2013
Project#:WW 132030
Client D Lab IMi/ cQiiecte Anal Result Units Matrix Method DF LOg Run Analyst,
WW132030 1780 1314637-01 16-)un-13 2,3,7,8-TCDD ND pg/I L 1613B 2 1 16-Sep-13 CM
Main St
Page 4 E
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"Analytical Integrity" EPA Certified NELAP Certified
3310 Win Street • Cuyahoga Falls, Ohio 44223 • Phone: 330-253-8211 • Fax: 330-253-4489
Web Site:wwwsettek.com
Y
330-2531-4489 02:32:17 p.m, 09-18-2013 7/7
Summit Environmental Technologies, Inc.
Method 1613
QC Report
Batch ID: 1109 ]CAL date : 5/2/2013 Extraction Date: 9/4/2013
Blank Results: 2,3,7,8-TCDD < 1.0 pg/L
Labeled Unlabeled
Compound Compound
% Recovery % Recovery
13C-2,3,7,8- 2,3,7,8- Analysis
Parameter TCD'D TCDD Date
LCS 57.3 74.3 9/8/2013
LCSD 58.8 75.2
Acceptance Limits 25-141 73-146
CCV1 99.5 95.8 9/16/2013
CCV2 102.6 107.9 9/16/2013
Acceptance Limits 85-117 82-123
Blank 48.4 9/8/2013
Acceptance Limits 25- 164
Sample
1314637-01 39.1 9/16/2013
Acceptance Limits 25- 164
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Rev. 12 II�IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII�I� IIIIIIIIIIIIIII�IIIIIIIIfIIIIIIIIIIIIIIIIIII
Date: 07/27/13
Order I®: 1314637 COOLER
Summit Environmental Techr
CooW Receipt Force,
( Initials of person inspecting cooler and samples:_
Client:�(,Jj r0l�ed%
'V� �s_e Order Number:
Date Received:$/ 4 Time Received: (rJ ' 0 Date cooler(s)opened and samples inspected:-�_
Number of Coolers/Boxes: N/A
Shipper: FED EX UPS DHL Airborne US Postal Walk-in Pickup Other:
Packaging: Peanuts ubble Wrap Paper Foam None Other:
Tape on cooler/box: Y N N/A
Custody Seals intact Y N/A
C-O-C in plastic N N/A
Ice lue ice present / absent / elted N/A
Sample Temperature IR Gun#16020459 CF c-t- lzo 'C 1 6 1 °C N/A
Radiological Testing Instrument serial#35127 Y N N/A
(see page 2 for scan results)
Use 1 sheet per sample for Radiological Testing, If sample is HOT,the Radiological Safety Officer must be notified
Immediately.
C-O-C filled out properly l N N/A
Samples in separate bags t Y> N N/A
Sample containers Intact* t N NIA
*If no,list broken sample(s):
Sample label(s)complete(ID,date,etc.) t Y N N/A
Label(s)agree with C-O-C \ ' N N/A
Correct containers used N N/A
Y
Sufficient sample received ` V N N/A
Bubbles absent from 40 mL vials** Y N N/A
**Samples with bubbles<6mm are acceptable. Indicate bubble size if>6mm.
Was client contacted about samples Y N
Will client send new samples Y N
Client contact:
Date/Time:
Logged in by:
I
Comments:
i
i
f.
G:\QC SHARED\Document Control Templates-Tracking\Cooler receipt form Rev. 12 07-27-13.doc Page 1 of 2. (S
330-253-4489 02:30:54 p.m. 09-18-2013 2/7
Rev. 12 IIIIIIIIIIIIIIIIIIIIIIIIIiiII�IIINIIII Illllllllllllllllllilllllillllll�illllllll
Date:07/27/13
Summit Environmental Techr Order ID: 1314637 COOLER
Cooler Receipt Fors„ 0
Initials of person Inspecting cooler and samples: L O
Client:Cn ,��r�csa��/P,,L���� Order Number:
Date Received Time Received: !2 ' 0y Date cooler(s)opened and samples Inspected: _
Number of Coolers/Boxes:. I I WA
Shipper: FED FCC UPS DHL Airborne US Postal Walk-In Pickup, Other:
Packaging: Peanuts ubble Wrap Paper .Foam None Other:
Tape on cooler/box: ` ✓ N NIA
Custody Seals Intact YY N/A
C-O-C in plastic (lr N�� N/A
Ice lue Ice > present / absent / rid ' N/A
Sample Temperature IR Gun#16020459 CF m- °C °C N/A
Radiological Testing Instrument serial#f35127 Y N N/A
(see page 2 for scan results)
"Use 1 sheet per sample for Radiological Testing, If sample is HOT,the Radiological Safety Officer must be notified
Immediately.
C-O-C filled out properly 1 ✓ N N/A
Samples in separate bags t✓ N NIA
Sample containers Intact' ' / > N NIA
'If no,list broken sample(s):
Sample label(s)complete(ID,date,etc.) `✓ N N/A
Label(s)agree with C-O-C l ' N N/A
Correct containers used Y N N/A I,
Sufficient sample received N N/A
I
Bubbles absent from 40 mL vlals" Y N N/A
Samples with bubbles<6mm are acceptable. Indicate bubble size if>6mm. a
Was client contacted about samples .Y N
Will client send new samples Y N
Client contact:
Date/Time:
Logged In by:
Comments:
f
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-C: N O]F': CIT _ ECZS
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ical:Laboratores Iris
41 Illinois Avenue w
131 Coolidge St, Suite 105 o
Warwick, RI 02888-3007 Hudson,Iv1A 01749-1331 E u x
Tel:401-737-8500 Tel: 978-568-0041 UI o j
Fax: 401-738-1970 Fax: 978-568-0078 v X
Date :::::.:•:::;Time:'. •`r..' i ``:,';. ...` . •'.:. .• o _ I
Collected "Collected Oiir Sample Identifications .: �! a IL
8127113 12:05 1308-18481-001 ww-132030 1780 Main St 2V H vvvv Barnstable X
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-Send Re drt and Invoice To.
Subcontractor Information'::'company: R.I. Analytical Laboratories Inc. subcontractor: ESS Laboratory
Address: 41 Illinois Avenue- _ Address Line 1: 185 Frances Ave
City/State/Zip: Warwick, RI 02888 Address Line 2:
Telephone: 800-937-2580 Fax 401-738-1970 city: Cranston state:
Report To: Data Reporting RI zip: 02910_2211
p g Email: data repo Telephone: 401-461-7181 FAx: 401-461-4486
Contact for questions: Krisfin Phelan ext: 116 Emaik, kphelan@rianalytical.com
R inquished By ... ._..
D.
ate: Time, Received By. .' : Date'- Time.:' Turn:AroundTiine ,
odd Normal: Business Days
ro
a4 ,3a z 5130 X RUSH: 3-4 Business Days
X oject.Comments'
:.. :..
Date Shipped::---
Notes to X Courier UPS
Subcontract p Q#'; g:9'$2`'<>` Results due 9/4/13. Thank you. 2, q '`� P``�
Laboratory: c�
:..................... 1' FedEx DHL
8t2�f r? I X On Ice
1 ; ;
Containers P=Poly,G=Glass,AG=Amber Glass,V=Vial,St--Sterile Preservatives: Workorder No:
A=Ascorbic Acid,NH4=NH4CI,H=HCI,M=MeOH,N=HNO3,NP=None,S=H2SO4,SB=NaHSO4.SH=NaOH,T=Na2SZ03,Z=ZnOAc
Matrix Codes:GW=Groundwater,SW=Surface Water,WW=Wastewater,DW=Drinking Water,S=Soil,Sl-=Sludge,A=Alr Cell,B=Bulk/Solid,SB=Swab,O=
Page 1 of 1 .
mMMIT �
analysis Request / Chain of Custod
ENVIRONMENTAL TECHNOLOGIES. INC. y
331 O WIn Sireet For Summit Environmental Technologies,Inc.use only
Cuyahoga falls,Ohio 44223
e00_2713_0140 Illlllllllllllilllllllll IIIIIIIIIIIIIIIIIIlIIIIIIIIIIIIIIIIIIIIIII
Client Name Project Identification
Envirotech Laboratories, Inc WWI32030 IIIIIIIIIIIIIIIIIIII
Client Address Projecl Address
8 Jan Sebastian Dr unit 12 Sandwich, MA ', Order ID: 1314637 co
02563 1780 Main St W.Barnstable, MA.
Client Phone Report To
508 888 6460 Ron Saari ;®
Client Fax No. V to Receive Results by Pax PO Number
508 888 6446 ❑ 082713
Contact Person �.
Quote Number
Ron Saari .� c
•o
Sampled By
R Saari ❑ if Ohio VAP Samples o ,.
Date
# �, Samplel}denttcatlon Tlmc x
C'nllected
WW132030 1780 Main St 06/16/26. 12:06 XL _ ice 2
XX
by . Da a :Time "Rccei�cel,9w Date. I itnc ._, Notes/Cor,nncnts:
1-S IZ7 v Q �
Rec'elved,tn:LaU by"_ '.Date Tune r,Rush Requested: DaY(s).
Must be approved by Lab Manager
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ENVIROTECHLABORATORIES, INC.
MA CER T. NO.: M-MA 063
8 Jan Sebastian Drive
Sandivicltr MA 02563
(508)888-6460 1-800-339-6460
FAX(508)888-6446
Trresda,,September 24, 2013
Page, Patrick
1780 11,fain Si
W Barnstable, M
ProjectNrnne: 1780 Merin St TV Bcn'nstable Corrrnrerrls:
Projecl Number
Collection Date: 08127113 Collection Pine: 12:15
Sanipled By: R Saor•i
Lab Order Nlnnber: TYW-132032
Date Received: 08127113
Sample Type Santple.Tilire. Snriile Dale Conriuerrts
Old Cranberry bog exiA 12 1.5 08/27/13.,.. Mud Sample
Parameters Uilits Test Results Reportable Limits Dare Analyzed Analyst Method
PCB 8080` ND` 08/31/13 RIA` SW-846 8082
Lead mg/Kg dry BRL 0.6 09/20/13 MC 200.7
Cadmium mg/Kg dry 0.14 0.2 O9I20/13 MC 200.7
Chromium mg/Kg dry 7.90 0.2 09/20/13 MC 200.7
Mercury` mg/Kg dry <0.070" 08/29/13 RIA`
Sliver mg/Kg dry BRL 0.2 09/20/13 MC 200.7
Selenium mg/Kg dry BRL 1.0 09/20/13 MC 200.7
Arsenic mg/Kg dry BRL 1.0 09/20/13 MC 200.7
Barium mg/Kg dry 13.7 0.2 09/20/13 MC 200.7
Total Petroleum Hydrocarbons" mg/Kg dry 100' 08/30/13 RIA' SW 8468100M
BRL=below reportable limits
*see adached
�
By:
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Rona d J. Saadl
Laboratory D rector I
Page 1 of 1
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� ®I . NALYT' AL Page 1 of
Specialists in Environmental Services
CERTIFICATE OF ANALYSIS
Envirotech Laboratories, Inc. Date Received: 8/28/2013
Attn: Mr. Ron Saari Date Reported: 9/3/2013
8 Jan Sebastian Drive P.O. #:
Sandwich, NIA 02563 Work Order#: 1308-18482
DESCRIPTION: PAGE, PATRICK
Subject sample(s) has/have been analyzed by our Warwick, R.I. laboratory with the attached results.- /
Reference:-All parameters were analyzed by U.S.`EPA approved methodologies.
The specific methodologies are listed in the,methods column of the Certificate of Analysis,
Data qualifiers (if present) are explained in fill at the end of a given sample's analytical results.
Me Certificate of Analysis shall not be reproduced except in full,without written approval of R.I. Analytical.
Results relate only to samples submitted to the laboratory for analysis.
Test results are not blank corrected:
Certification#: RI-033, MA-RIO15, CT-PH-0508,ME-RI015
NH-253700 A& B, USDA 5-41844
If you have any questions regarding this work, or if we may be of further assistance, please contact
our customer e deU ent.
Approv d by:
Sh ron B ker i
MI' /Da eporti r
en.c: Chain of Custody
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4
41 Illinois Avenue,Warwick,RI 02888 131 Coolidge Street,Suite 105,Hudson,MA 01749
www.rianaly�ical.com Phone:401:737.8500.Fax:401.738.1970 y Phone:978.568.0041 Fax;978.568.0078
Page 2 of 2
R.I. Analytical Laboratories, Inc.
CERTIFICATE OF ANALYSIS
Envirotech Laboratories,Inc.
Date Received: 8/28/2013
Work Order#: 1308-18482
Sample# 001
SAMPLE DESCRIPTION: WW-132032 1780 MAIN ST. W.BARNS'IABLF
SAMPLE TYPE: GRAB SAMPLE DATE/TIME: 8/27/2013 @ 12:15
SAMPLE DET. DATE/TIME
PARAMETER RESULTS LIMIT UNITS METHOD ANALYZED ANALYST
TPH
TPH GC/FID l00 14 mg/kg dry SW846 8,100M 8/30/2013 13:39 THP
Surrogate RANGE SW-846 8100 8/30/2013 13:39 THP
2-Fluorobiphenyl 65 40-140% SW-846 8100 8/30/2013 13:39 THP
Moisture 30 % SM2540 G. 8/29/2013 13:58 JRW
Aroclor-1016 <0.1 0.1 mg/kg dry SW-846 8082 8/31/2013 16:59 JEB
Aroclor-1221 <0.1 .0.1 mg/kg dry SW-846 8082 8/31/2013 16:59 JEB
Aroclor-1232 <0.1 0.1 mg/kg dry SW-846 8082 8/31/2013 16:59 JEB
Aroclor-1242 <0.1 0.1 mg/kg dry SW-846 8082 8/31/2013 16:59 JEB
Aroclor-1248 <0.1 0.1 mg/kg dry SW-846 8082 8/31/2013 16:59 JEB
Aroclor-1254 <0.1 0.1 mg/kg dry SW-846 8082 8/31/2013 16:59 JEB
Aroclor-1260 <0.1 0.1 mg/kg dry SW-846 8082 8/31/2013 16:59 JEB
I
Surrogate RANGE SW-846 8082 8/31/2013 16:59 JEB
Telrachloro-nrxylene(TCMX) 76 30-150% SW-846 8082 8/31/2013 16:59 JEB
Decachlorobiphenyl 79 30-150% SW-846 8082 8/31/2013 16:59 JEB
Extraction date SW8463540 8/29/2013 9:25 JRG t
TOTAL METALS
Mercury <0.070 0.070 mg/kg dry SW-846 7471A 8/29/2013 12:44 JRW
Mercury Digestion SW-846 7471A 8/29/2013 12:02 PJC s
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CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. RI Analytical
8 Jan Sebastian Dr Unit 12 M RI 015
PWS: Project Name: Page, Patrick Sandwich, MA 02563 Address 41 Illinois Avenue
(508)888-6460 Warwick, RI 02888
Sampler: R. Saari 1-800-339-6460 Phone# 401-737-8500
FAX(508)888-6446 Fax# 401-738-1970
Lab ID# Date Time Comp Grab IStation location DEP ID Container Pres. Sample type Analysis requested
WW-132032 08/27/13 1215 X 11780 Main St.W Barnstable Plastic soil PCB 608
Plastic soil Petroleum Scan
Plastic ' soil Hg
Call Lab wsth any,
Exceeded:MCL_
_� •�
Relinquished: j ffDatd/Tim
Receive Reliauished: DateMme Received:
Relin uis `2d: Received: Relinquished: DateTme Received:
_ r-
CHAIN OF CUSTODY FORM ENVIROTECH LABS, INC. Client: Patrick Page
8 Jan Sebastian Dr., Unit 12
Proj. No. Project Name: 1780 Main St W Barnstable Sandwich, MA 02563 Address: 1780 Main St
(508)888-6460/1-800-339-646 �� W. barnstable,MA 02668
Sampler: FAX(508)888-6446 Phone#: 508 280 7243
Fax#:
Lab ID# Date Time Compyg4b Sample location container Pres. Analysis Requested
0u1<3 h3Z-- 08/27/13 Lc f_ Old Cranberry bog exit soil PCB
Petroleum Scan
RECRA 8 metals
i
Relinquishe Date/T' e IK(/"/ Receive Reliquished: Daterrime Received:
Relin ished Da(./rime/ Received: Relinquished: Daterrime Received:
-----Original Message-
From: Brezinski,Brezinski, Paul
Sent:Thursday, October 19, 2017 6:31 AM
To:Woods, Bruce<Woods.Bruce@epa.gov>
Subject: FW: Emailing:Trench 9-22 &9-28-17,8-29-17 outfall bact,8-7-17 ditch,8-13-17 discharge pipe,8-1-13 outfall
Bruce,
The attached are related to a complaint we have in MA. There is an outflow pipe that discharges onto a residential
property. The property owner had tests done and the tests are attached. The matter will be referred to the Agency. I
am not well versed in what exactly these results are showing. Not sure if you would be able to add anything to the
results attached to this email but any input would be appreciated.
Thanks.
Paul
Paul A. Brezinski
Resident Agent in Charge
New York Post of Duty
United States Environmental Protection Agency Office of Inspector General Office of Investigations
290 Broadway,Suite 1S20
New York, NY 10007
212-637-3033 (Office)
917-359-2535.(Mobile)
To report fraud,waste or abuse impacting EPA, please contact the EPA OIG Hotline via telephone numbers 202-566-
2476 or 888-546-8740,fax 202-566-2599,or email at oig_hotline@epa.gov
To report threats directed against EPA employees,contractors,facilities and assets,please
emailreport.EPA.threats@epa.gov
-----Original Message-----
From: Ron Saari [mailto:rsenviro@comcast.net]
Sent: Wednesday, October 18, 2017 11:43 AM
To: Brezinski, Paul<Brezinski.Paul@epa.gov>
Cc: pagecarpentry66@gmail.com
Subject: Emailing:Trench 9-22&9-28-17,8-29-17 outfall bact, 8-7-17 ditch,8-13-17 discharge pipe,8-1-13 outfall
Your message is ready to be sent with the following file or link
attachments:
Trench 9-22&9-28-17
8-29-17 outfall bact
8-7-17 ditch
8-13-17 discharge pipe
8-1-13 outfall
2
Note:To protect against computer viruses, e-mail programs may prevent sending or receiving certain types of file
attachments. Check your e-mail security settings to determine how attachments are handled.-
3
a uptp�&�6 Barnstable
TOWN OF BARNSTABf
U-MMca NY
BARMSTABU. • OFFICE OF TOWN ATTORNEY I
MASS. a
9° 2639• , 367 MAIN STREET
°ArEDM�a HYANNIS, MASSACHUSETTS 02601-3907 2007
RUTH J.WEIL,Town Attorney ruth.weil@town.barnstable.ma.us
T. DAVID HOUGHTON, 1st Assistant Town Attorney david.houghton @town.barnstable.ma.us
CHARLES S. McLAUGHLIN,JR.,Assistant Town Attorney Charles.mclaughIin@town.barnstable.ma.us
CLAIRE R. GRIFFEN, Paralegal/Legal Assistant April 13, 2009 claire.griffen@town.barnstable.ma.us
PAMELA D.GORDON, Legal Clerk TEL.508-862-4620 •FAX.508-862-4724
Ms.Jane Saunders
Mr. Patrick F. Page
1780 Main Street, Route 6A
West Barnstable, MA 02668-1137
Re: 1780 Route 6A and 21 Buttonwood Lane
Our File Ref: #2006-0223 -
Dear Jane and Patrick:
Following several telephone conferences March 30 and April 8'and 9, I left it with
Patrick that his suggestion that Jane would apply for an additional lot at 1780 before
going ahead with 21 Buttonwood was a good idea. I was speaking with Tom Geller
about another matter and he didn't think that was a bad idea either. I did tell Patrick that
we would keep the offer open on 21 Buttonwood while 1780 went forward. Since Jane is
not under.any prohibitions, she can contact the folks at 200 Main if she has questions
about the process for 1780.
To recap, when I spoke with you both on March 30 we talked about setting up a meeting
with staff about 21 Buttonwood. Since I didn't hear back right away after I called on
April 3, 1 did discuss 21 Buttonwood with Tom McKean and Rob Gatewood on April 7.
The consensus was that 21 Buttonwood had a good chance of getting standard wetlands
conditions with growback mitigation, a perc test in the C2 layer in test pit number 7 and
engineered plans. I even expressed a willingness to contact BSC.
The idea was that this would end the war between you and the Town. When I spoke to
Patrick on April 8 he said in addition he wanted either compensation or an additional
buildable lot at 1780. I said I wouldn't recommend compensation nor linking dividing
1780 to permitting 21. He called back on the 9th and that when he mentioned dividing
1780 first.
20060223 pageletter15
This changes the previous standing offer(see letter dated Feburary 5, 2009) to meet with
Rob, but I agree that it makes sense. There aren't any legal issues with 1780 so you can
proceed without my involvement. In fact, I can't and won't be involved, so calls to our
office should cease and Jane can deal directly with the folks at 200 Main.
Best wishes for success.
Sincerely,
/tdh T. DAVID HOUGHTON
cc: Tom Geiler
Rob Gatewood
Tom McKean
20060223 pageletter15
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TOWN OF BAR14STABLE
LOCATICN SEWAGE # 3a
-.�PILLAGE � •A S SSOMAPR'S MP F� LOT
�. KENNEDY TRUCKING
INSTALLER'S NAME & PHONE NO. 575 WILLOW STREET
WEST LARNSTAKl N,ASS, 02668.:._,
SEPTIC TANK CAPACITY +` TEL. 362.30m
LEACHING FACILITTY:(twe) — (size)
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NO. OF BEDROOMS PRIVATE WELL OR nUBLIC WATER
BUILDER OR OWNER '
DATE PERMIT ISSUED: —14
DATE COtiPLIANCE ISSUED-
VARIANCE GRANTED: Yes r No �`
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THE COMMONWEALTH OF MASSACHUSETTS
BOARD OF HEALTH
Application is hereby made for a Permit to Construct or Repair an Individual Sewage Disposal
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System at:
Location Address or Lot No. �
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Own
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Other—Type of Building ._-_---.............. No. of persons............................ Showers ( ) -- Cafeteria ( )
� Other fixtures
Deu6ro Flum------.------_'----_.gallons per person per day. Total daily flow---x�~049�'A���----.gallons.
Septic Tank—Liquid ..gallons Length................ Width................ Diameter................ Depth................
Disposal Trench--No .................... Width.................... Total .................... Total area....................ug fc
Seepage Pit No..................... Diameter.................... Depth below inlet.................... Total leaching area..................sq. ft.
Z Other Distribution box ( ) Dosing tank ( ) '
~~ Percolation Test Reao8u Ierf000edhy----.-.-------- - --------- Dutc------------------'
�Tes Pit No. l-----_minutes per inch Depth of Test Pit.................... Depth to ur000dwatcr-------_
44 Test Pb No. 2................minutes per inch Depth of Test Pit--------- Depth ro ground water------------------------
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0 Description of
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� U Nutoreof Repairs or Alterations—Answer when, licable
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The undersigned agrees to install the aforedescribed Individual Sewage Disposal System in accordance with
the provisions of'ITlE 5 ofdeStateSanitaryCode— I} e undersigned further agrees not m place the system in
operation until u Certificate of Compliance ha be issued by the bo�rd of health.
� Signed ~_
� - -------'-- -'----.�atApplication Approved �--'.__'
By.................. ................................ ----'.�-�-K��-
= � ~ Date
Application Disapproved for the following reasons:..............................................................................................................
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.........................................................................................................................................................................................................
Permit
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THE COMMONWEALTH OF MASSACHUSETTS
BOARD OF HEALTH
...................... ...................OF......................
.........._....
Appliration for Uiapu.ial Works Tnmuurtinn Famit
Application is hereby made for a Permit to Construct ( ) or Repair ( ) an Individual Sewage Disposal
System at:
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Location-Address or Lot No.
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Installer Address
gype of Building Size Lot...............:------------Sq. feet
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WOther—Type of Building ............................ No. of persons............................ Showers ( ) — Cafeteria ( )
P4Other fixtures -----------------------------------------------------------•-•-•••......--------------- -------------------•--•••---�..._.
W Design Flow................v..........................gallons per person per day. Total daily flow......... ._____..gallons.
WSeptic Tank—Liquid capacity�'':(*----gallons Length---------------- Width................ Diameter................ Depth................
x Disposal Trench—No..................... Width.................... Total Length.........._......... Total leaching area....................sq. ft.
Seepage Pit No--------------------- Diameter................_--- Depth below inlet.................... Total leaching area..................sq. ft.
Z Other Distribution box ( ) Dosing tank ( )
1.4 Percolation Test Results Performed by.......................................................................... Date........................................
Test Pit No. 1................minutes per inch Depth of Test Pit.................... Depth to ground water........................
(� Test Pit No. 2................minutes per inch Depth of Test Pit-_-_____-__.__------ Depth to ground water-------:................
119----------
Description of Soil........... . . .................... .. . f
x -------------------------•-----------------------------------------------------•.----
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UNature of Repairs or Alterations,—Answer when a• icable... ...........................................................................................
•-------- ----------------------•-----•••••••------•---•--•••-••-••......•••--•......._....._....
Agreement:
The undersigned agrees to install the aforedescribed Individual Sewage Disposal System in accordance with
the provisions of l yT .,.
p }of the State Sanitary Code—The undersigned further agrees not to place the system in
operation until a Certificate of Compliance has be issued by the board of health.
14
Signed _..........., --------------------------.-.--.•.-.-................•----- .. .. ... %
Application Approved BY Dat
. V.- ��Z�-
Date
Application Disapproved for the following reasons---------------------------------------------------------------------------------------------------------------_
........----•---••-••---•••--•-•....•---•...............••••-•----------------••-------••••-•------••••-------•--••-••--•-••-••-•••-------------------•-•-•---•----------•--•••-•------•••-....._---•--
Date
PermitNo.----- ------------------------ Issued.......................................................
THE COMMONWEALTH OF MASSACHUSETTS
BOARD OF HEALTH
.............O F............... ? � ry...... ................................
TrrtifirFatr of TiantpliFanrr
THIS IS T,CERTIFY That the Individual Sewage Disposal System constructed ( ) or Repaired ( }
by -- •--------------------- ............. ._�...................................................................................................................................
Installer
at-•-•---•--••-•••••47--ir.0.........At......... .-n............ram /'.1." ................................................
has been installed in accordance with the provisions of TITIZ 5 of The State Sanitary Code as described in the
application for Disposal Works Construction Permit No........Fl_.:....L_11,1:2...... dated-------------------------------------------•---.
THE ISSUANCE OF THIS CERTIFICATE SHALL NOT BE CONSTRUED AS A GUARANTEE THAT THE
SYSTEM WILL FUNCTION SAT SFACTPPY
DATE...................... ..:..T•..................... Inspector_...__.... ...........................................
THE COMMONWEALTH OF MASSACHUSETTS
'BOARD OF HEALTH
,\ ...... all�t-�............OF.......... ���?��Y1+.........................................
No.....V,r /..�£�-- FEE.....��?.....
Disposal Iforks 0,41ntrnrtion rrntit
Permission is hereby granted........... ...........ice^'""`"1 --------------------------------------------------------••--...................--•--
to Construct ( ) or Repair >1 an Individual Sewage Disposal System
atNo........... --? -..r'------ .. ------ ,!�-------kn.,f --------------------•------------------------------------------.----------.--
Street
as shown on the application for Disposal Works Construction Permit No.4,1:_l3Q.._ Dated..........................................
................................
......................................................
Board of Health
DATE--- !�-------------�-------�- .-17
....................................
.FORM 1255 HOBBS & WARREN. INC.. PUBLISHERS