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HomeMy WebLinkAbout0590 IYANNOUGH ROAD - HAZMAT ,.' � �ru� ,. �� (� ;,� r _ ---------- - ---- - - -- - -- - - f i �� �' �� 1 \�, �� op THE Tp� Town of Barnstable Office:508-862-4644 Public Health Division Fax:508-790-6304 B"RMMk%` � 200 Main Street• Hyannis, MA 02601 t6S9 TOXIC AND HAZARDOUS MATERIALS INSPECTION REPORT fED MPy << Business Name: JGA C, Date: Location/Mailing Address: MO 2qCAfft(A Contact Name/Phone: Jn$-SM Inventory Total Amount: <6_60 MSDS: wk-non — License#: Tier.11 : Labeling: _ Spill Plan: Oil/WaterSeparator: Floor Drains: Emergency Numbers: J Storage Areas/Tanks: S ' ,-A, i ni Emergency/Containment Equipment: aCX Waste Generator ID: � 71 7cX�SS Waste Product: co ° Date&Amount of Last Shi ment/Fre uenc Licensed Waste Hauler&Destination: Vke Other Waste Disposal Methods: LIST OF TOXIC AND HAZARDOUS MATERIALS f10 Gttern NOTE: Under the provisions of Ch. 111, Section 31, of the %l Laws of"MAhar ous material use, storage and disposal of 111 gallons or more requires a license from the Public Health Division. Antifreeze Dry cleaning fluids Automatic transmission fluid Other cleaning solvents&spot removers Engine and radiator flushes Bug and tar removers Hydraulic fluid (including brake fluid) Windshield wash r Motor oils Miscell eous Corrosives Gasoline,jet fuel, aviation gas Ce ool cleaners Diesel fuel, kerosene, #2 heating oil disinfectants Miscellaneous petroleum products: Road salts grease, lubricants, gear oil Refrigerants Degreasers for engines&garages Pesticides: Caulk/Grout insecticides, herbicides, rodenticides Battery acid (electrolyte)/batteries Photochemicals(Fixers) Rustproofers Photochemicals(Developer) Car wash detergents Printing ink Car waxes and polishes Wood preservatives(creosote) Asphalt&roofing tar Swimming pool chlorine Paints, varnishes, stains, dyes Lye or caustic soda Lacquer thinners Miscellaneous Combustible Paint&varnish removers, deglossers Leather dyes Miscellaneous Flammables Fertilizers Floor&furniture strippers PCB's Metal polishes Other chlorinated hydrocarbons Laundry soil &stain removers (including carbon tetrachloride) (including bleach) Any other products with "poison labels" (including chloroform, formaldehyde, hydrochloric acid, other acids) VIOLATIONS: ORDERS: INFORMATION/RECOMMENDATIONS: V J Inspector: Facility Representative: WHITE COPY-HEALTH DEPARTMENT/CANARY COPY- BUSINESS �` V SOVEPEIGN CONSULTING April 21,2008 DHL#26935641655 Town of Hyannis Town Engineer 367 Main Street Hyannis,MA 02601 Re: Groundwater Sampling Results,March 2008 Former Shell'Branded Gasoline Station#137772 590 Iyannough Road Hyannis,MA Dear Town Engineer: Pursuant to your authorization Sovereign Consulting Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for .laboratory analysis of volatile petroleum hydrocarbons_ (VPH), ethylene- dibromide (EDB),and ethanol. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVEREIGN CONSULTING,INC. Sylvia M. Kirsch Project Manager Attachments: Laboratory Data Reports cc: with attachment 711' Mr.David Weeks,Motiva c 3 MassDEP- SERO Sovereign File-EQ872 -� f+± 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 t I y ' a NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan BWSC 123 This Notice is Related to Release Tracking Number 4� 17651 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 590 lyannough Rd. City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Hyannis,Town Engineer 2. Street Address: 367 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked,the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 590 lyannough Rd. City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Sylvia Kirsch Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: skirsch@sovcon.com f NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment .at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass..qov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. e-Hardcopy 2.0 Automated Report New England ACCUTEST. { t.a b o fat on e 5 Di .. ... .. ..... .. _:: .. _ ... _...... . ... .., , .,, 5/08 ........... __... ._.......... _.. _............. Technlical Reoxt 1'ar y Shell Oil SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA 4 Accutest Job Number: M72046 Sampling Date: 03/28/08 Report to: Sovereign Consulting blaughlin@sovcon.com ATTN: Barbara Laughlin Total number of pages in report: 67 \N ACCpR in TIMUa ., s Test results contained within this data package meet the requirements eZa and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(250204) RI(00071) ME(MA136) FL(E87579) Mff Y,. E A R $ NY(23346) NJ(MA926) NAVY USACE _ This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England 495 Tech Center West • Building 1 • Marlborough,MA 01752 tel:508-481-6200 fax:508-481-7753 http://www.acculest.com ®B 1 of 67 9AC U7FST M72046 Sections: Table of Contents -1- Section1: Sample Summary ................................................................................................... 3 Section2: Case Narrative/Conformance Summary .............................................................. 4 Section3: Sample Results ........................................................................................................ 5 3.1.: M72046-1: MW-101 ..................................................................................................... 6 3.2: M72046-2: GT-3 ........................................................................................................... 9 3.3: M72046-3: GT-7 ........................................................................................................... 12 3.4: M72046-4: MW-102 ..................................................................................................... 15 3.5: M72046-5: GT-4 ........................................................................................................... 18 3.6: M72046-6: GT-1 3.7: M72046-7: MW-202D .................................................................................................. 24 3.8: M72046-8: MW-202 ..................................................................................................... 27 3.9: M72046-9: MT-3/MT-1 ....................................................................I........................... 30 3.10: M72046-10: GT-5 ....................................................................................................... 33 Section4: Misc. Forms ............................................................................................................ 36 4.1: Chain of Custody ........................................................................................................... 37 4.2: MCP Form ..................................................................................................................... 38 4:3: VPH Form ...................................................................................................................... 39 4.4: Sample Tracking Chronicle ........................................................................................... 49 Section 5: GUMS Volatiles - QC Data Summaries .............................................................. 51 5.1.: Method Blank Summary ................................................................................................ 52 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 53 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 54 5.4: Surrogate Recovery Summaries ..................................................................................... 55 Section6: GC Volatiles- QC:Data Summaries ..................................................................... 56 6.1.: Method Blank Summary ................................................................................................ 57 6.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 61 6.3. Blank Spike Summary ................................................................................................... 64 6.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 65 6.5: Surrogate Recovery Summaries ..................................................................................... 66 2 of 67 MACCU TEST. M72046 iai>„=_•n.,ee 1 � 7 Accutest Laboratories �. Sample Summary Shell Oil SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA Job No: M72046 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID 1172,046 1 03/28/08 13:50 RD 04/01/08 AQ Ground.Water MWOi M720 6,2 03/28/08 13:25 RD 04/01/08 AQ Ground Water GT 3 M72046 3 03/28/08 14:00 RD 04/01/08 AQ Ground Water GT 7 M720.46 4 03/28/08 13:00 RD 04/01/08 AQ Ground Water MW 1U2 M720'4fi,5 .` 03/28/08 09:30 RD 04/01/08 AQ Ground Water M7204S 6 .03/28/08 10:10 RD 04/01/08 AQ Ground Water GT 1 M7Q46 7. 03/28/08 12:10 RD 04/01/08 AQ Ground Water �Vt,720;4,6 $ 03/28/08 11:20 RD 04/01/08 AQ Ground Water Mx7ir04i 9' ...03/28/08 10:40 RD 04/01/08 AQ Ground Water MT-3/NI 1. M7r2041a 10:....03/28/08 12:50 RD 04/01/08 AQ Ground Water GT 5 3of67 12AC'7CUTE'ST. M72046 a- - - - Awcclu La. bora. tories SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M72046 Site: SCMAW:97451486(REIMBMA)590 Iyannough Road Hyannis MA Report Date 4/15/2008 2:26:23 PM 10 Sample(s)were collected on 03/28/2008 and were received at Accutest on 04/01/2008 properly preserved,at 2.1 Deg.C and intact. These Samples received an Accutest job number of M7204.6.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GCMS By Method SW846 8260B Matrix AQ Batch ID: MSN968 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Sample(s) M72091-1MS,M72091-1MSD were used as the QC samples indicated. e Only Ethanol requested. Volatiles by GC By Method EPA 504 Matrix AQ Batch ID: OP15528 All samples were extracted within the recommended method holding time. o All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. ■ Sample(s) M72297-5MS,M722971-5MSD were used as the QC samples indicated. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GBD804 All samples were analyzed within the recommended method holding time. i All method blanks for this batch meet method speck criteria. Matrix AQ Batch ID: GBD805 n All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GWX1906 c All method blanks for this batch meet method specific criteria. ® M72046-1:Sample re-analyzed past recommended hold time. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirery.The Accutest Laboratories of NE,Laboratory Director or assignee as verged by the signature on the cover page has authorized the release of this report(M72046). Tuesday,April 15,2008 Page 1 of 1 E 4 of 67 13ACS M72"6 -n Fora c-;¢. New England L.aborator,t, Section 3 Sample Resulfs Report of Analysis 5 of 67 12ACCUTEBT Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-202D Lab Sample ID: M72046-7 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26288.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 ` CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND 200 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane lOzb/o' 79-130% 2037-26-5 Toluene-D8 100p1o..' 80120% 460-00-4 4-Bromofluorobenzene 104% 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 24 of 67 NACCUTENT. M72046 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-202D Lab Sample ID: M72046-7 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17087.D 1 04/10/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene <NA 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether Nl7 i; 2.0 ug/I 91-20-3 Naphthalene lD 3.0 ug/1 108-88-3 Toluene 2.0 ug/1 m,p Xylene .NIA 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj ) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5-C8 Aliphatics [ 50 ug/I C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59 8 2,5-Dibromotoluene '9 Y 70-130% 615 59 8 2,5 Dibromotoluene 92% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 25 of 67 c .rr�sT. M72oas Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-202D Lab Sample ID: M72046-7 Date Sampled: 03/28/08 Matrix: AQ- Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent-Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46434.D 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 33.0 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.016 ug/1 CAS No. Surrogate Recov--ries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 88% 26 158% 460-00-4 Bromofluorobenzene (S) 1:08Q/o 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 26 of 67 1ACCLr.rEWC M72046 ..,. .........._ Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-202 Lab Sample ID: M72046-8 Date Sampled: 03/28/08 Matrix: AQ-Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26289.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND 200 ug/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 1.03% 79-130% 2037-26-5 Toluene-D8 100% 80-120% 460-00-4 4-Bromofluorobenzene 103% 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 27 of 67 A©CUT"EST W2046 ..a. ,,... ...... Accutest Laboratories Report of Analysis Page 1 of 1 CO Client Sample 1D: MW-202 Lab Sample ID: M72046-8 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17088.D 1 04/10/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene Nk. 2.0 ug/1 100-41-4 Ethylbenzene ND: 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND I2.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene =ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) 41) 50 ug/1 C9- C12 Aliphatics (Unadj.) NI)` 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 90°h 70-130% 615-59-8 2,5-Dibromotoluene 91% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 28 of 67 QACCU—TEST. Accutest Laboratories Report of Analysis Page 1 of 1 CO Client Sample ID: MW-202 Lab Sample ID: M72046-8 Date Sampled: 03/28/08 Matrix: AQ-Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46435.D 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 33.8 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane NO 0.016 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 26 158% 460-00-4 Bromofluorobenzene (S) 124% 26-158% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 29 of 67 A J 'E3T M72048 t.AF .,......e5 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MT-3/MT-1 Lab Sample ID: M72046-9 Date Sampled: 03/28/08 Matrix: AQ -Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26290.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol Nb 200 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane I03% 79-130% 2037-26-5 Toluene-D8 80-120% 460-00-4 4-Bromofluorobenzene 1044/0 : ' 84-115% I M ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 30 of 67 12AC CUTrEBT M72046 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MT-3/MT-1 Lab Sample ID: M72046-9 Date Sampled: . 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17089.D 1 04/11/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND : 2.0 ug/1 m,p-Xylene ND .; 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) IN 50 ug/I C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND': 50 ug/1 CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene 91% 70130% 615-59-8 2,5-Dibromotoluene, RO% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 31 of 67 12ACCtJTE M72046 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MT-3/MT-1 Lab Sample ID: M72046-9 Date Sampled: 03/28/08 Matrix: AQ -Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46436.D 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 34.2 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/t CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 107% . 26-158% 460-00-4 Bromofluorobenzene (S) 119%:: 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound B 32 of 67 j2QCCUTEST. M72046 New England MACCuIEsT r'e- Section 4 _. Disc Forms, Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle 36 of 67 AOCUTES_T. M72046 LAB(LOCATION) Q Shell Oi I Products Chain Of Custody Record -7 >.... ' :❑.ENv SDri10E5 : ❑RIDAIIVA RkTNi Y9 q>; .. .. rte;.. .:::.... ....... BiT6oNa :: - .. , . .. ):❑oda nNomceN Rs ....... .. ...... pwmAstAEN 7ox+wlT.Nr l7waEs .._.. .._._-- ':::PO f! .'::S . ........ PAGE- ___1 ❑SMLLPIEEIurE ❑OTIIDI —_— «��Or""'� r aoar¢ss nx«�,ces'..a ar.ac Sovereign Consulting annou h Road Hyannis,MA 905 B South Main Street sur.,,.eeownro ann ra Mansfield,MA 0204e smx..surPxm Iwa uSE dAa.Y 509J79-3200 TURNAROUND TiMe IatanoaR DAvs:0sT REQUESTED ANALYSIS .zawnu.wYl ❑sDArs ❑soars OzDATs ❑zsNams � D[1lVEMBlES: E'Eoroa OC — Q+N ❑RCP 0DD9l(sn—, TeNPERaTURE ON RECFNTC coda er iewwn jeodaq SPECIAL INSTRUCTIONS OR NOTES saraPEmc � >ue Field Sample Identification soma Moor > DATE TORE o Q Z p Cmmon M Readings ;:PY4v Np xupa MSOa NONE 4rxeR eoNr W W dr Ub-d.q N.I. IRO GW k KXX G7 I3Yf } G - 02 1 ao Gam-� i010 Me✓-Z02P 210 M�-2oz ilw MY= 3 p1r-1 tnye :s (y7 Y2S0 w. h 1a T, R.a mnr i oa. `ter Y l l�f J , xm.-_mn rua�w r nee. 13 fao�y F�w.w ev( rxan . (�� l c,7-- /C,3 M72046: Chain of Custody Page 1 of 1 37 of 67 ACC TE.B7: M72046 -ab::ra-.r:,,. Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 i Bureau of Waste Site Cleanup Final Page 10 of 32 ' IJ Title: MADEP MCP Response Action Analytical Report Certification Form Laboratory Name: Accutest Laboratories of New England Project#: M72046 Project Location: SCMAW:97451486(REIMBMA)590 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M72046-1,M72046-10,M72046-2,M72046-3,M72046-4,M72046-5,M72046-6,M72046-7,M72046-8 M72046-9 Test method:EPA 504,and below Sample Matrices: Groundwater X Soil/Sediment () Drinking Water () Other: () () 3 46 X. 82606 X 8151 A__U 8330 0 6010E 7470A/1 A act `__ 8270C 8081A ) VPH(X 6020 9014M z ) r 8082 8021 B ( EPH 7000 S 3 7196A ) fig u rY An affirmative response to questions A, B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with Yes ❑ No ' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and El Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty',as described in Section 2.0(a),(b),(c)and El Yes ❑No (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without El Yes ❑No significant modifications,as specified in Section 11.3? A response to questions E and Fbe/ow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the El Yes El No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified ❑ Yes No ' method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 04/15/2008 38 of 67 AC CLff EST. MADEP VPH FORM ON Aciueous Soil F , Sediment i1 Other F', oYtallrters Satisfactor �i Broken 1 Leaking toaieservatve N/A I H <=2 96 H >2 r , Rec'd at 2.1 de Received on Ice Received at 4 Deg. C �I Other �� 9 C N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-202D Lab ID: M72046-7 Ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 4/10/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 10041-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-Cl 2 ug/I ND 2 m,p-Xylene C9-Cl 2 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WiYes '. No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? C'Yes 1 I No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? L No 'E; Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 45 of 67 12AC=AJTEST M72046 MADEP VPH FORM Aqueous W Soil - Sediment f Other i UN atOWN, Satisfactor Broken F Leaking i O eIPME es N/A PH<=2 �I H 2 ;-- a:. .rate Received on Ice F1 Received at 4 Deg. C Other ik Rec'd at 2.1 deg C ao N/A �. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-202 Lab ID: M72046-8 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene WA 4/10/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND A 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-Cl 2 ug/t ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND 8 50 C9-C12 Aliphatics N/A ug/I ND o 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 90 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-08 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. MC12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes 0 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? OYes E No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WIND ] Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 ®a 46 of 67 12ACCUTEBT. M72046 '-a" pries MADEP VPH FORM �Aa r�x Aqueous ;vF Soil Fi Sediment Other F Otl tkeCs : Satisfactory�� Broken F.. Leaking ueotts�Pr :serraues. N/A I' H <=2 Woi H>2 - Terr� "rae �r�r . = Received on Ice Pi Received at 4 Deg. C i Other �I Rec'd at 2.1 deg C Rif N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MT-3/MT-1 Lab ID: M72046-9 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 4/11/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-Cl 2 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9_C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 90 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? v:Yes i_._. No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WIYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo '._.. Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 ® 47 of 67 M72046 _ - Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M72046 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample Number Method Analyzed By Prepped By Test Codes M72046-1 EPA 504 09-APR-08 0 1:10 CZ 08-APR-08 FG V504EDB M72046-1 SW846 8260B 11-APR-08 03:43 AA V8260ETHL M72046-1 MADEP VPH REV 1.111-APR-08 16:58 AF VMAVPH M72046-1 MADEP VPH REV 1.1 12-APR-08 12:15 AF VMAVPH ���0 M72046-2 EPA 504 09-APR-08 01:40 CZ 08-APR-08 FG V504EDB M72046-2 MADEP VPH REV 1.1 10-APR-08 19:41 AF VMAVPH M72046-2 SW846 8260B 11-APR-08 04:11 AA V8260ETHL kaeT✓�,�7,,..�.�i'�i^���...�e"„�. ,��.fs�M r3f='. ,,u..r a� �,�^fi ,�.�a� "'�_�.F �'� j:�`�� .�..3�.rCzs '3���, �,.����,,w....,,w'3'."��, M72046-3 EPA 504 09-APR-08 02:24 CZ 08-APR-08 FG V504EDB M72046-3 MADEP VPH REV 1.110-APR-08 20:22 AF VMAVPH M72046-3 SW846 8260B 11-APR-08 04:38 AA V8260ETHL M72046-4 EPA 504 09-APR-08 02:54 CZ 08-APR-08 FG V504EDB M72046-4 MADEP VPH REV 1.110-APR-08 21:03 AF VMAVPH M72046-4 SW846 8260B 11-APR-08 05:06 AA V8260ETHL M72046-5 EPA 504 09-APR-08 03:23 CZ 08-APR-08 FG V504EDB M72046-5 MADEP VPH REV 1.110-APR-08 21:45 AF VMAVPH M72046-5 SW846 8260B 11-APR-08 05:34 AA V8260ETHL &'10- M72046-6 EPA 504 09-APR-08 04:37 CZ 08-APR-08 FG V504EDB Page 1 of 2 49 of 67 1ACCUTIEW. M72046 -a-..._......c. Accutest Laboratories Internal Sample Tracking Chronicle P. Shell Oil Job No: M72046 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample Number Method Analyzed By Prepped By Test Codes M72046-6 MADEP VPH REV 1.110=APR-08 22:25 AF VMAVPH M72046-6 SW846 8260B 11-APR-08 06:02 AA V8260ETHL 011,11,01- M72046-7 EPA 504 09-APR-08 05:22 CZ 08-APR-08 FG V504EDB M72046-7 MADEP VPH REV 1.1 10-APR-08 23:07 AF VMAVPH M72046-7 SW846 8260B 11-APR-08 06:29 AA V8260ETHL M72046-8 EPA 504 09-APR-08 05:51 CZ 08-APR-08 FG V504EDB M72046-8 MADEP VPH REV 1.110-APR-08 23:48 AF VMAVPH M72046-8 SW846 8260B 11-APR-08 06:57 AA V8260ETHL ,�"W11,11-01 M72046-9 EPA 504 09-APR-08 06:21 CZ 08-APR-08 FG V504EDB M72046-9 MADEP VPH REV 1.111-APR-08 00:29 AF VMAVPH M72046-9 SW846 8260B 11-APR-08 07:25 AA V8260ETHL M72046-10 EPA 504 09-APR-08 07:05 CZ 08-APR-08 FG V504EDB M72046-10 MADEP VPH REV 1.111-APR-08 03:55 AF VMAVPH M72046-10 SW846 8260B It-APR-08 07:52 AA V8260ETHL I Page 2 of 2 50 of 67 ACCUTEST M72046 �® New England .12ACCU I>Esr. I. ..bor.rlar _ • Section 5 > 1 t ................ GGIMS Volatiles. QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ®( 51 of 67 19AC XJTE�: Method Blank Summary Page I of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSN968-MB N26274.1) 1 04/11/08 AA n/a n/a MSN968 NONE mom The QC reported here applies to the following samples: Method: SW846 8260B M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND_ 200 ug/l CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 104% 79-130% 2037-26-5 Toluene-D8 99"/0 80-120% 460-00-4 4-Bromofluorobenzene 103% 84-115% 52 of 67 12ACCUTEB7: Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSN968-BS N26271.1) 1 04/10/08 AA n/a n/a MSN968 MSN968-BSD N26272.1) 1 04/10/08 AA n/a n/a MSN968 iv The QC reported here applies to the following samples: Method: SW846 8260B M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/I % ug/l % RPD Rec/RPD 64-17-5 Ethanol 5000 4690 94 '. 5250 105 f 25 183/30 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluorome have 105%q.; 165% 79-130% 2037-26-5 Toluene-D8 80120% 460-00-4 4-Bromofluorobenzene 101% iQx1%< 84-115% 53 of 67 9ACCMJTEST M72046 Labarn tnriee Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M72091-1MS N26292.1) 5 04/11/08 AA n/a n/a MSN968 M72091-1MSD N26293.1) 5 04/11/08 AA n/a n/a MSN968 M72091-1 N26275.1) 1 04/11/08 AA n/a n/a MSN968 The QC reported here applies to the following samples: Method: SW846 8260B M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 M72091-1 Spike MS MS MSD MSD Limits CAS No. Compound ug/l Q ug/I ug/I % ug/l % RPD Rec/RPD 64-17-5 Ethanol ND 25000 24300 67 23800 95 2 20 190/30 CAS No. Surrogate Recoveries MS MSD M72091-1 Limits 1868-53-7 Dibromofluoromethane 1U5%' 10 % d0 °10 79-130% 2037 26-5 Toluene-D8 Ifit '100%:>. 80 120% 460-00-4 4-Bromofluorobenzene 10MR 1029'n 103%.: 84115% ® 54 of 67 IRACCUTEST M72046 a^., ....... z Volatile Surrogate Recovery Summary Page I of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: SW846 8260B Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID Sl S2 S3 M72046-1 N26282.1) 100 0;:;' : 99.0 101 0 M72046-2 N26283.1) 99 0 99.0 101 0 M72046-3 N26284.1) <00 0 100.0 M72046-4 N26285.1) 401*0 100.0 1010 M72046-5 N26286.1) 1030 99.0 M72046-6 N26287.1) 103 0 ':99.0 102 0 M72046-7 N26288.1) a0 U 100.0 1104 0. M72046-8 N26289.1) <103`0 100.0 1'Q3 0 M72046-9 N26290.1) 103 0 100.0 104 0 M72046-10 N26291.D i0&0 .;', 99.0 1 4 0 M72091-1MS N26292.1) 105 0 101.0 M72091-1MSD N26293.1) 104 0 101.0 162 0 MSN968-BS N26271.1) i05 0 101.0 "Mr-I MSN968 BSD N26272.D 105:U - 99.0 MSN968-MB N26274.1) 1;04 0 99.0 i# 0 Surrogate Recovery Compounds Limits S 1 = Dibromofluoromethane 79 130 fo S2 = Toluene-D8 S3 = 4-Bromofluorobenzene 55 of 67 QACCUTEST. M72046 .. ............ ®� New England OAccu-r-lEST. L.aborator:e,; a Section Cl ................ ...:.. ...:..._ ..:_. A.._ ___...__. ._. .__._.... - GC `lolat�les:: QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries 56 of 67 12ACCUTEST. M72046 Method Blank Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD804-MB BD17067.1) 1 04/10/08 AF n/a n/a GBD804 as The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9 • CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene N" 2.0 ug/l 1634-04-4 Methyl Ter(Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene NO, 3.0 ug/l 108-88-3 Toluene IUD 2.0 ug/1 m,p-Xylene N€D 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj ) ND 50 ug/l C9-C12 Aliphatics (Unadj.) ND' :. 50 ug/1 . C9- C10 Aromatics (Unadj.) N . , 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Limits s 615-59-8 2,5-Dibromotoluene 93%0 70-130% 615-59-8 2,5-Dibromotoluene 94% . 70-130% 57 of 67 ;jQA JTFST. Method Blank Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD805-MB BD17091.1) 1 04/11/08 AF n/a n/a GBD805 as The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M72046-1, M72046-10 CAS No. Compound Result RL Units Q 71 43 2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene 1Vb 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND, 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj ) ND 50 ug/1 C9-C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unad3) W :. 50 ug/l C5- C8 Aliphatics Nb 50 ug/l C9- C12 Aliphatics Np 50 ug/l CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 94%. 70-130% 615-59-8 2,5-Dibromotoluene 93°1a 70-130% 58 of 67 GAIT: M72046 -a-^ s Method Blank Summary Page I of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GWX1906-MB WX40145.1) 1 04/12/08 AF n/a n/a GWX1906 a> The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 =+ M72046-1 CAS No. Compound Result RL Units Q C9- C12 Aliphatics (Unadj.) NA 50 ug/1 C9- C10 Aromat=cs (Unadj.) ND 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits . 615-59-8 2,5-Dibromotoluene 92%_ _;' 70-130% 615-59-8 2,5-Dibromotolufne 89% 70-130% ® 59 of 67 QAG'CUTEST. M72046 ..,-..._....... Method Blank Summary Page 1 of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15528-MB YZ46422.1) 1 04/08/08 CZ 04/08/08 OP15528 G.YZ1988 os The QC reported here applies to the following samples: Method: EPA 504 :+ M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 • . CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/1 CAS No. Surrogate Recoveries Limits 460-00-4 Bromofluorobenzene (S) fr)1% 26-158% 460-00-4 Bromofluorobenzene (S) I.11%; 26-158% ® 60 of 67 MACCU*TEN 7: M72046 _a Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch GBD804-BSP BD17068.1) 1 04/10/08 AF n/a n/a GBD804 GBD804-BSD BD17069.D 1 04/10/08 AF n/a n/a GBD804 os The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 K) M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/I % ug/l % RPD Rec/RPD 71-43-2 Benzene 50 45.0 90 . - 45.2 90 !.: 0 70-130/25 100-41-4 Ethylbenzene 50 45.7 91` 46.4 93.; 2 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 45.6 04 46.6 93: 2 70-130/25 91-20-3 Naphthalene 50 46.9 94: 48.9 98 4: 70-130/25 108-88-3 Toluene 50. 45.5 9:1 45.8 9,2:`' k;. 70-130/25 m,p-Xylene 100 89.8 9.0 91.5 92 2 70-130/25 95-47-6 o-Xylene 50 43.8 8. 44.6 89 2.:' 70-130/25 C5- C8 Aliphatics (Unadj.) 150 121 81;:.. 132 88 9 70-130/25 C9- C12 Aliphatics (Unadj.) 150 125 83 129 k 3, 70-130/25 C9- C10 Aromatics (Unadj.) 50 46 93 48 95 3` 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 92% 970/6 70-130% 615-59-8 2,5-Dibromotoluene 92% 97% 70-130% ®� 61 of 67 UACCUTEET M72046 I Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD805-BSP BD17092.1) 1 04/11/08 AF n/a n/a GBD805 GBD805-BSD BD17093.1) 1 04/11/08 AF n/a n/a GBD805 os The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 iN) M72046-1, M72046-10 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/I % ug/I % RPD Rec/RPD 71-43-2 Benzene 50 43.5 87 44.9 90 3 70-130/25 100-41-4 Ethylbenzene 50 45.1 90 46.6 93 3 1. 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 44.9 90 46.4 93- 3 70-130/25 91-20-3 Naphthalene 50 46.9 94 49.1 98 5, 70-130/25 108-88-3 Toluene 50 43.9 88 45.6 9=�. : 4 70-130/25 m,p-Xylene 100 88.6 89.' 91.6 92 3 70-130/25 95-47-6 o-Xylene 50 43.3 87 44.7 8,9 3; 70 130/25 C5- C8 Aliphatics (Unadj.) 150 118 79 120 80 2 -:: 70-130/25 C9-C12 Aliphatics (Unadj.) 150 123 82. 130 87 6 70-130/25 C9- C10 Aromatics (Unadj.) 50 47 93 48 96' 3 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 12% 97%° 70-130% 615-59-8 2,5-Dibromotoluene 70-130% ® 62 of 67 WACCUTEST. Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GWX1906-BSP WX40146.1) 1 04/12/08 AF n/a n/a GWX1906 GWX1906-BSD WX40147.1) 1 04/12/08 AF n/a n/a GWX1906 a> The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 i-J M72046-1 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/I % ug/I % RPD Rec/RPD C9- C12 Aliphatics (Unadj.) 150 152 101, 156 104: 3.;.; 70-130/25 C9- C10 Aromatics (Unadj.) 50 51.0 1Q2 52.4 1U5 3' 70 130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 91% 889/6 70-130% 615-59-8 2,5-Dibromotoluene 94% 95% 70-130% ®� 63 of 67 12ACCUTEST. M72046 i Blank Spike Summary Page I of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15528-BS YZ46423.1) 1 04/08/08 CZ 04/08/08 OP15528 GYZ1988 The QC reported here applies to the following samples: Method: EPA 504 wis M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 • Spike BSP BSP CAS No. Compound ug/I ug/l % Limits 106-93-4 1,2-Dibromoethane 0.071 0.070 99 70-130 CAS No. Surrogate Recoveries BSP Limits 460-00-4 Bromofluorobenzene (S) 97% 26-158% 460-00-4 Bromofluorobenzene (S) :113% 26-158% I IQ 64 of 67 ACcLn'WBT M72046 .. . Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15528-MS YZ46424.D 1 04/08/08 CZ 04/08/08 OP15528 GYZ1988 OP15528-MSD YZ46425.1) 1 04/08/08 CZ 04/08/08 OP15528 GYZ1988 M72297-5 YZ46426.D 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 as The QC reported here applies to the following samples: Method: EPA 504 a. M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 • M72297-5 Spike MS MS MSD MSD Limits CAS No. Compound ug/l Q ug/I ug/l % ug/I % RPD Rec/RPD 106-93-4 1,2-Dibromoethane ND 0.071 0.063 89 0.073 103 15 65-135/30 CAS No. Surrogate Recoveries MS MSD M72297-5 Limits 460-00-4 Bromofluorobenzene (S) 100% 117%: 106% " 26-158% 460-00-4 Bromofluorobenzene (S) 119%. 26-158% 65 of 67 AC.CLffEST M12046 '-abareteriec f r Volatile Surrogate Recovery Summary Page I of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b in M72046-1 WX40149.1) 92 0':;.: 90.0 M72046-1 BD17113.D 90.0 M72046-2 BD17082.D 89. ..<.` 88.0 M72046-3 BD17083.D 87©„- 88.0 M72046-4 BD17084.D 89 0 89.0 M72046-5 BD17085.D 89 0 89.0 M72046 6 BD17086.D 90 0 90.0 M72046-7 BD17087.D 91,0 92.0 M72046-8 BD17088.D 90 0 91.0 M72046-9 BD17089.D 910 s 90.0 M72046-10 BD17094.D 95 0 95.0 GBD804-BSD BD17069.D 97.0. 97.0 GBD804-BSP BD17068.D -944 92.0 GBD804-MB BD17067.D 93 0 94.0 GBD805-BSD BD17093.D 97 0 ':: 98.0 GBD805-BSP BD17092.D 92:'-0,r 92.0 GBD805-MB BD1709l.D 94 0 93.0 GWX1906-BSD WX40147.D 88U>. : . 95.0 GWX1906 BSP WX40146.1) 91 94.0 GWX1906-MB WX40145.1) 92:0 89.0 Surrogate Recovery Compounds Limits S l = 2,5-Dibromotoluene 70 1310 (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 B 66 of 67 ACGUTE;gT' I , Volatile Surrogate Recovery Summary Page 1 of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: EPA 504 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b M72046-1 YZ46427.1) 115:0;:, 116.0 M72046-2 YZ46428.1) 8t2 U 97.0 M72046-3 YZ46429.1) 124 119.0 M72046-4 YZ46430.1) 1,080 120.0 M72046-5 YZ46431.D 114.0 ..._....._.. . . M72046-6 YZ46433.1) l0I 0 :.: 108.0 M72046-7 YZ46434.1) $8 Q 108.0 M72046-8 YZ46435.1) 104 0 124.0 M72046-9 YZ46436.1) 107:0= 119.0 .._........... M72046-10 YZ46437.1) 115 0? 109.0 OP15528-BS YZ46423.1) 97 0 113.0 OP15528-MB YZ46422.1) 0 ' : 111.0 OP15528-MS YZ46424.1) f 0 105.0 OP15528-MSD YZ46425.1) :1:1:7:.0< ; 118.0 Surrogate Recovery Compounds Limits S1 = Bromofluorobenzene (S) 26-1-58°l0 (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 ® 67 of 67 12ACC1.TEST M72046 _"-" -- SOVEREIGNf- • April 21,2008 DHL#26936026250 Ms. Donna Miorandi Town of Barnstable,Health Inspector 200 Main Street Hyannis,MA 02601 Re: Groundwater Sampling Results,March 2008 Former Shell Branded Gasoline Station#137772 590 Iyannough Road Hyannis, MA Dear Ms. Miorandi: Pursuant to your authorization Sovereign Consulting Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH), ethylene- dibromide (EDB),and ethanol. A copy of the laboratory analytical is attached. As always,we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVEREIGN CONSULTING,INC. c I �AA Sylvia M. Kirsch Project Manager Attachments: Laboratory Data Reports cc: with attachment Mr.David Weeks,Motiva MassDEP- SERO Sovereign File-EQM 905B S. Main Street, Unit 202 Mansfield„MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING T As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan r f BWSC 123 I I This Notice is Related to I Release Tracking Number ® 17651 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 590 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Health Inspec. Donna Miorandi 2. Street Address: 200 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ✓❑ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 590 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring ❑ Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater) to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Sylvia Kirsch Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508) 339-3200 Email: skirsch@sovcon.com i NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. • e-Hardcopy 2.0 Automated Report New England -lop .. 1 r t r ta` r ...g s: �,t s';e r3 04/15/0.8 Technical, Report for Shell Oil SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Accutest Job Number: M72046 lm-211 Tls-"' Sampling Date: 03/28/08 Report to: Sovereign Consulting blaughlin@sovcon.com ATTN: Barbara Laughlin Total number of pages in report: 67 1N AC CpR 0 041 Test results contained within this data package meet the requirements eZa and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 kYE RCertifications:MA(M-MA136) CT(PH-0109) NH(250204) RI(00071) ME(MA136) FL(E87579) R 5 NY(23346) NJ(MA926) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England 495 Tech Center West Building 1 Marlborough,MA 01752 tel:508-481-6200 fax:508-481-7753 http://www.accutest.com 1 of 67 12ACCUTE.ST c 7r Table of Contents Sections: -1- Section1: Sample Summary ................................................................................................... 3 Section2: Case Narrative/Conformance Summary .............................................................. 4 Section 3: Sample Results .............. 3.1.: M72046-1: MW-101 ..................................................................................................... 6 3.2: M72046-2: GT-3 .........................................................................................:................. 9 3.3: M72046-3: GT-7 ........................................................................................................... 12 3.4: M72046-4: MW-102 ..................................................................................................... 15 3.5: M72046-5: GT-4 ........................................................................................................... 18 3.6: M72046-6: GT-1 ........................................................................................................... 21 3,7: M72046-7: MW-202D .................................................................................................. 24 3.8: M72046-8: MW-202 ..................................................................................................... 27 3.9: M72046-9: MT-3/MT-1 ................................................................................................ 30 3.10: M72046-10: GT-5 .......................................................................................I................ 33 Section4: Misc. Forms ............................................................................................................ 36 4.1: Chain of Custody ........................................................................................................... 37 4.2: MCP Form ..................................................................................................................... 38 4.3: VPH Form ...................................................................................................................... 39 4.4: Sample Tracking Chronicle ........................................................................................... 49 Section 5: GUMS Volatiles - QC Data Summaries ........................................... 5.1.: Method Blank Summary ................................................................................................ 52 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 53 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 54 5.4: Surrogate Recovery Summaries ..................................................................................... 55 :Section 6: GC Volatiles - QC Data Summaries .................................................... .. 56 ............... 6.1.: Method Blank Summary ................................................................................................ 57 6.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 61 6.3: Blank Spike Summary ........:.......................................................................................... 64 6.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 65 6.5: Surrogate Recovery Summaries ..................................................................................... 66 2 of 67 13ACCUTEEM M72046 €. ............. Accutest Laboratories Sample Summary Shell Oil SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA lob No: M72046 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M72046-4 03/28/08 13:50 RD 04/01/08 AQ Ground Water MW-101 M72046-2 <: 03/28/08 13:25 RD 04/01/08 AQ Ground Water GT-3 M72046-3 03/28/08 14:00 RD 04/01/08 AQ Ground Water GT4 472046-4 03/28/08 13:00 RD 04/01/08 AQ Ground Water MW4,02' M72046-5 ; 03/28/08 09:30 RD 04/01/08 AQ Ground Water GT-4' I M72046,=6 03/28/08 10:10 RD 04/01/08 AQ Ground Water GT-1 M720:46-7 03/28/08 12:10 RD 04/01/08 AQ Ground Water MW-202D M72046-8 03/28/08 11:20 RD 04/01/08 AQ Ground Water MW-202 M72046 9: 03/28/08 10:40 RD 04/01/08 AQ Ground Water MT 37M P 1 M72046710 03/28/08 12:50 RD 04/01/08 AQ Ground Water GT-5 �B 3 of 67 12A►CCL TEBT. M72046 vo h t_. a. b o r a. E11 o r i e SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M72046 Site: SCMAW:97451486(REIMBMA)590 Iyannough Road Hyannis MA Report Date 4/15/2008 2:26:23 PM 10 Sample(s)were collected on 03/28/2008 and were received at Accutest on 04/01/2008 properly preserved,at 2.1 Deg.C and intact. These Samples received an Accutest job number of M72046.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Swmmary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GCMS By Method SW846 8260B Matrix AQ Batch ID: MSN968 ■ All samples were analyzed within the recommended method holding tome. " All method blanks for this batch meet method specific criteria. " Sample(s) M72091-1MS,M72091-1MSD were used as the QC samples indicated. m Only Ethanol requested. Volatiles by GC By Method EPA 504 Matrix AQ Batch ID: OP15528 All samples were extracted within the recommended method holding time. " All samples were analyzed within the recommended method holding time. _ All method blanks for this batch meet method specific criteria. Sample(s) M72297-5MS,M72297-5MSD were used as the QC samples indicated. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GBD804 ■ All samples were analyzed within the recommended method holding time. ® All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GBD805 ffi All method blanks for this batch meet me thod specific criteria. Matrix AQ Batch ID: GWX1906 " All method blanks for this batch meet method specific criteria. M72046-1:Sample re-analyzed past recommended hold time. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M72046). i Tuesday,April 15,2008 Page 1 of I 4 of 67 DACCUTEST M72046 New England ACCUTEST �, f Section fi s .i x-rai- ra .t' t Sample Results Report of Analysis �B 5 of 67 12ACCUTEE T M72046 _a. ....,.... -y Accutest Laboratories Report of Analysis Page 1 of 1 a Client Sample ID: MW-101 Lab Sample ID: M72046-1 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26282.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND 200 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 1868-53-7 Dibromofluoromethane l00% 79-130% 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene 101% 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Ea n 6 of 67 12ACCUTE T. M72046 -.. .. ......... Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-101 Lab Sample ID: M72046-1 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17113.1) 1 04/11/08 AF n/a n/a GBD805 Run#2 a WX40149.1) 1 04/12/08 AF n/a n/a GWX1906 Purge Volume Run#1 5.0 ml Run#2 5.0 ml MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND :: 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND > 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND b 50 ug/1 C9- C10 Aromatics (Unadj.) ND b 50 ug/1 C5- C8 Aliphatics ;ND 50 ug/1 C9- C12 Aliphatics ND b 50 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene >90% 92% 70-130% 615-59-8 2,5-Dibromotoluene 90%' 90% 70-130% (a) Sample re-analyzed past recommended hold time. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 67 A M72046 - -- - Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-101 Lab Sample ID: M72046-1 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46427.1) 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 33.7 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane NlY 0.016 ug/1 CAS No. Surrogate Recoveries Run# I Run#2 Limits 460-00-4 Bromofluorobenzene (S) 1.15% 26-158% 460-00-4 Bromofluorobenzene (S) 1'16.%. , 26 158% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound J ® 8 of 67 12ACC JTEST. M72046 ......... ..... Accutest Laboratories Report of Analysis Page 1 of 1 p y Client Sample ID: GT-3 Lab Sample ID: M72046-2 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26283.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND 200 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 99% .. 79-130% 2037-26-5 Toluene-138 99 0 80-120% 460-00-4 4-Bromofluorobenzene 101% 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ©B 9 of 67 QACCUTEST M72046 = - • Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-3 Lab Sample ID: M72046-2 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17082.D 1 04/10/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/t m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ;ND''. 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/t C9- C12 Aliphatics (Unadj.) l) 50 ug/1 C9- CIO Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 89% 70-130% 615-59-8 2,5-Dibromotoluene 88% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �B 10 of 67 13ACCUTEEM M72046 _ . ....... Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-3 Lab Sample ID: M72046-2 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46428.D 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 32.3 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.016 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 82% 26 158% 460-00-4 Bromofluorobenzene (S) 97% 26 158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound QB 11 of 67 13ACCU TEST, M72046 `-a Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample 1D: GT-7 Lab Sample ID: M72046-3 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26284.13 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND 200 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 100% 79-130% 2037-26-5 Toluene-138 :1;00% 80-120% 460-00-4 4-Bromofluorobenzene 102% 84-115% ND = Not detected J = Indicates an estimated value RL_= Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �B 12 of 67 JOACCU TEST. M72046 = ^s Accutest Laboratories Report of Analysis Page 1 of I w Client Sample ID: GT-7 Lab Sample ID: M72046-3 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17083.D 1 04/10/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND. 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) NDI 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics NO 50 ug/1 CAS No. Surrogate Recoveries Run# I Rung 2 Limits 615-59-8 2,5-Dibromotoluene 879/61 70-130% 615-59-8 2,5-Dibromotoluene 88% 70-130% _ ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 67 12ACCUTEST M72046 e � Accutest Laboratories Report of Analysis Page I of I w Client Sample ID: GT-7 Lab Sample 1D: M72046-3 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46429.1) 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 34.6 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 120 26-158% 460-00-4 Bromofluorobenzene (S) 119%: 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound QB 14 of 67 12ACCUTEST. M72046 a � Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample 1D: MW-102 Lab Sample ID: M72046-4 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAVV:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26285.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND . 200 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 101% 79-130% 2037-26-5 Toluene-D8 100% 80-120% 460-00-4 4-Bromofluorobenzene 101% 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q� 15 of 67 12ACCLr .EE3T M72046 r. Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample 1D: MW-102 Lab Sample 1D: M72046-4 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17084.D 1 04/10/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) W 50 ug/I C9- C10 Aromatics (Unadj.) ND:: 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 89%0. > 70-130% 615-59-8 2,5-Dibromotoluene 89% 70-130% ND = Not detected J = Indicates an estimated.value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ® 16 of 67 12ACCI ITEM?; M72046 .a._... _..__ c Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-102 Lab Sample ID: M72046-4 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46430.1) 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 34.1 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 460-00-4 Bromofluorobenzene (S) fog%o 26-158% 460-00-4 Bromofluorobenzene (S) 1,20% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME] 17 of 67 ACCUTEST, M72046 ..,._.... ......_ Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-4 Lab Sample ID: M72046-5 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26286.D 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND 200 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 79-130% 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene 1030/6 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 67 �ACCIJiF.ST. M72046 - a r Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-4 Lab Sample ID: M72046-5 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17085.1) 1 04/10/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND.: 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND;' 50 ug/1 C5- C8 Aliphatics ND ` 50 ug/1 C9- C12 Aliphatics ND: 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene :89%0 70-130% 615-59-8 2,5-Dibromotoluene O% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Elffl 19 of 67 JOACGUTEST M72046 a- -,.....t Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-4 Lab Sample ID: M72046-5 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46431.1) 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 34.3 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane NDl. 0.015 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 98% 26-158% 460-00-4 Bromofluorobenzene (S) 1149/c 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q 20 of 67 OACC JTEST. M72046 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample 1D: GT-1 Lab Sample ID: M72046-6 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26287.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol NI) 200 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 1030/0 79-130% 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene 102% ' 84-115% ND = Not detected J Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 of 67 IOACCA JTEST, M72046 ► w Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-1 Lab Sample ID: M72046-6 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA II File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17086.D 1 04/10/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene NI) 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND. 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND' 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) 11 ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 90% 70-130% 615-59-8 2,5-Dibromotoluene 900/6 _ 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound fB 22 of 67 12ACCVTEST M72046 ' - Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-1 Lab Sample ID: M72046-6 Date Sampled: 03/28/08 Matrix: AQ -Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date. Prep Batch Analytical Batch Run#1 YZ46433.D 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 33.4 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-DibromoethFne ND 0.016 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits .............. .... . 460-00-4 Bromofluorobenzene (S) 101% 26-158% 460-00-4 Bromofluorobenzene (S) 1080/11 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 23 of 67 IMACCLITEST. M72046 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample 1D: MW-202D Lab Sample ID: M72046-7 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26288.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND 200 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 102% 79130% 2037-26-5 Toluene-D8 1009/6 80-120% 460-00-4 4-Bromofluorobenzene 104% 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 24 of 67 12AST, M72046 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-202D Lab Sample ID: M72046-7 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17087.D 1 04/10/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene N.P. 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) NO - 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene >91/0 70-130% 615-59-8 2,5-Dibromotoluene 929/6 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®l] 25 of 67 12ACC rrEST. M72046 _r_.,--�r 7 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-202D Lab Sample ID: M72046-7 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46434.1) 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 33.0 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 I,2-Dibromoethane ND 0.016 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 88% 26-158% 460-00-4 Bromofluorobenzene (S) 108% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 26 of 67 12ACCIJTEST. M72046 Accutest Laboratories Report of Analysis Page 1 of 1 00 Client Sample ID: MW-202 , Lab Sample ID: M72046-8 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26289.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. , Compound Result RL Units Q 64-17-5 Ethanol ND 200 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 79-130% 2037-26-5 Toluene-D8 100% 80-120% 460-00-4 4-Bromofluorobenzene 103% 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Mffl 27 of 67 MACCUTEST. M72046 :_,_ .......... � n Accutest Laboratories Report of Analysis Page 1 of 1 00 Client Sample ID: MW-202 Lab Sample ID: M72046-8 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17088.D 1 04/10/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether NDI 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) IyD. 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 90% 70-130% 615-59-8 2,5-Dibromotoluene 9:1%0 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®EJ 28 of 67 12ACCUTEST, M72046 a Accutest Laboratories Report of Analysis Page 1 of 1 CO Client Sample ID: MW-202 Lab Sample ID: M72046-8 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46435.1) 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 33.8 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.016 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 104% 26-158% 460-00-4 Bromofluorobenzene (S) 124% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 29 of 67 12ACC,JTEST. M72046 i.abor +cries Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MT-3/MT-1 Lab Sample ID: M72046-9 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26290.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol N61 200 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 103% 79-130% 2037-26-5 Toluene-D8 100% 80-120% 460-00-4 4-Bromofluorobenzene 104% 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 30 of 67 12ACClJTE3T. M72046 Accutest Laboratories Report of Analysis Page 1 of 1 e Client Sample ID: MT-3/MT-1 Lab Sample ID: M72046-9 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEF VPH REV 1.1 Percent Solids: n/a Project: SCMAVI:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17089.D 1 04/11/08 AF n/a n/a GBD804 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics NO.. - 50 ug/1 C9- C12 Aliphatics NO. 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-DibromotoluEne 91%0 70-130% 615-59-8 2,5-DibromotoluEne 90% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M® 31 of 67 12ACPVT T. ........._.........................._._...._. M72046 iI Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MT-3/MT-1 Lab Sample ID: M72046-9 Date Sampled: 03/28/08 Matrix: AQ -Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46436.1) 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 34.2 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 107%0 26-158% 460-00-4 Bromofluorobenzene (S) ;119% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ® 32 of 67 13ACCLJTEST. M72046 `- II Accutest Laboratories sa Report of Analysis Page 1 of 1 Client Sample ID: GT-5 Lab Sample ID: M72046-10 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 N26291.1) 1 04/11/08 AA n/a n/a MSN968 Run#2 Purge Volume Run#1 5.0 ml Run#2 CAS No. Compound Result RL Units Q 64-17-5 Ethanol NO 200 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 106% ' 79-130% 2037-26-5 Toluene-D8 99.%0 80-120% 460-00-4 4-Bromofluorobenzene 1049/6 84-115% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ® 33 of 67 12ACCUTEST. M72046 a-• - Accutest Laboratories W Report of Analysis Page I of I Client Sample ID: GT-5 Lab Sample ID: M72046-10 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD17094.D 1 04/11/08 AF n/a n/a GBD805 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-X lene ND 2.0 u /l Y g C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND: 50 ug/l C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 95% 70-130% 615-59-8 2,5-Dibromotoluene 95% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®ffl 34 of 67 12ACCUTEST, Accutest Laboratories t� Report of Analysis Page 1 of 1 Client Sample ID: GT-5 Lab Sample ID: M72046-10 Date Sampled: 03/28/08 Matrix: AQ - Ground Water Date Received: 04/01/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 YZ46437.D 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 Run#2 Initial Volume Final Volume Run#1 34.9 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane NO 0.015 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 115% 26-158% 460-00-4 Bromofluorobenzene (S) 1.09% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 35 of 67 12ACCUTEST. M72046 ® New England ACCUI'EST 7 r 1 I y % a Section 4 Mist-Forms,, Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle ® 36 of 67 12ACCIJPEST. M72046 - I e � Massachusetts Department BWSC-CAM Exhibit VII A-1 (� of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 N Title: MADEP MCP Response Action Analytical Report Certification Form � M�A13�EPtiIGP Anlyttt at Metfto Rp�rertlfltttan ntrt Laboratory Name: Accutest Laboratories of New England Project#: M72046 Project Location: SCMAW:97451486(REIMBMA)590 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M72046-1,M72046-10,M72046-2,M72046-3,M72046-4,M72046-5,M72046-6,M72046-7,M72046-8 M72046-9 Test method:EPA 504,and below i Sample Matrices: Groundwater X Soil/Sediment () Drinking Water () Other: () () MCPS84o6 82606 X 8151A 8330_U 6010E 7470A/1A �MethodsJs��d,� ,; 8270C O 8081A O VPH(X 6020 O 9014M z ) As�pecitiemn AD P � 8082 8021 B ) y h ( ) EPH O 7000 S ( 7196A Co p UrtS 0 s �1SLtSt ele MAIL!g 1 IujberlR�T tftil F, # � � r✓ � � r r a'sr r , �. t, e lyticat Methods 2SW846ad9914 csr� Af3 �P y olog tally f+vaitabie Cyanid (P, G�}Metho � CI ck ill fha. I � s �46 th d ooa S$�rt Inoiiui ual me a`r d artatyt , r h�.q _ � , An affirmative response to questions A, B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with 0 Yes ❑ No ' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed, including the requirement to note and Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty', as described in Section 2.0(a),(b), (c)and O Yes ❑No ' (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only: Was the VPH or EPH method run without Yes ❑No ' significant modifications,as specified in Section 11.3? A response to questions E and Fbelow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the ❑ Yes 0 No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified ❑ Yes LI No ' method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. l the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 04/15/2008 38 of 67 ............._........................_ M72046 i .. ........... MADEP VPH FORM Aqueous Soil Sediment F Other Contatirers . „ _ ' Satisfactory we. Broken F1 Leaking A ueous'P�eseryatiues N/A PH <=2 ✓� pH >2 Tern. efatur� �< v Received on Ice ! Received at 4 De . C iii Other i Reed at 2.1 deg C Methanol y N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-101 Lab ID: M72046-1 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 4/11/2008 04/12/08 FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 ii Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-Cl 2 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 90 70-130% FID:2,5-Dibromotoluene % 90 70-130% PID:2,5-Dibromotoluene % 90 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 'Yes I No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? i_✓.iYes . No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? I- No Yes Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 ff] 39 of 67 OAC PVTWI; M72046 -- -1- - MADEP VPH FORM Ague us Soil Sediment R Other F Cat,3taters .,. _< Sa t i sf acto ry Fv Broken Leakin i 1 A ueous Preservatl�es N/A F1 PH <=2 P-�! PH >2 h Tem er-a#.tare, Received on Ice Received at 4 Deg. C I_J Other �I Reed at 2.1 deg C fiitethan5F4y. r % N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-3 Lab ID: M72046-2 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 4/10/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 �I Naphthalene 91-20-3 N/A ugh ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND e 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 89 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? L'Yes '_.' No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W'Yes L.. No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.37 WIND Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 ME3 40 of 67 12ACCA TEBT. M72046 t � MADEP VPH FORM Matnx < Aqueous ICI Soil 1 Sediment F1! Other 3Conta"iners Sat isf act or V Broken 1 Leaking ueot s Preseryatlw'es': N/A D, PH —2 PH >2 Received on Ice Received at 4 Deg. C `� Other ✓_1 Rer•d at 2.1 deg C tll N/A p Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-7 Lab ID: M72046-3 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 4/10/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 87 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 141Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? EVIYes i_I No-Details Attatched significant modifications made to the VPH method,as specified in Sect. 11.3? l✓_1No ' _9 p .; Were any si Yes-Details Attatched I attest under the pains and penalties-of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 Mm 41 of 67 GACCIREW.. M72046 - MADEP VPH FORM Matrix`,:`', Aqueous Soil Sediment Other j i Co.ntairiers,4x " Satisfactor 'ice; Broken Leaking uleois Preservatives? N/A PH <=2 ✓! PH>2 T�eme�aturc ,> Received on Ice Received at 4 Deg. C F J Other Rec'd at 2.1 deg C Iletta alr Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-102 Lab ID: M720464 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 4/10/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units. Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND° 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 89 70-130% PID:2,5-Dibromotoluene % 89 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of ary surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes 0! No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes I_ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ICI No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 ®ff 1 42 of 67 12ACCUT'EST. M72046 =— - MADEP VPH FORM Mta#rlx f y f� Aqueous �i Soil L., Sediment I Other Contai're�s,...; j Satisfactory W-1 Broken Leaking ueot`s Preswatives N/A � H <=2 k PH >2 i fern e�atur� s Received on Ice Received at 4 Deg. C i. Other Rec'd at 2.1 deg C M0 haroC d: N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-4 Lab ID: M72046-5 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 4/10/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/1 ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 89 70-130% PID:2,5-Dibromotoluene % 89 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? V''•Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ';Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? V!No Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 43 of 67 ®ACp4TE 3T M72046 -- MADEP VPH FORM Matrtx' Aqueous i�i Soil Sediment 7 Other �1 Cont=ainers Satjsfactor Imo! Broken I Leakin yea"irks Preseruatives N/A H <=2 ✓I pH >2 r Received on Ice Received at 4 De . C _ Other Rec'd at 2.1 deg C Methandl` ' " ` N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-1 Lab ID: M72046-6 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 4/10/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-Cl 2 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 90 70-130% PID:2,5-Dibromotoluene % 90 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? l�'Yes :..- No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes _. No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? iIA No Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 Q 44 of 67 12ACCL ES'T. M72046 - MADEP VPH FORM Matrtx A ueous Pei Soil I , Sediment Other (i Contair ers i - Satisfactor �; Broken ! ': Leaking F ueous Pre'servatives N/A PH <=2 W1 PH >2 i= Received on Ice Received at 4 Deg. C Other f�1, Rec'd at 2.1 deg C Melhaniol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-202D Lab ID: M72046-7 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 4/10/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Ranqe Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND A 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-Cl 2 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Li Yes LA No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ��i No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 ®� 45 of 67 12ACC JTEST. M72046 '- - MADEP VPH FORM Matrtx ,,:.« r Aqueous I�i Soil - Sediment f Other Catitalners ,% Satisfactory 14i Broken i Leaking ueous�Preservat.Iues N/A 1, PH <=2 L PH >2 I Received on Ice D Received at 4 Deg. C Other Rec'd at 2.1 deg C N1etha_n.ols . :._ NIA Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-202 Lab ID: M72046-8 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 4/10/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/1 ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND e 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 90 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards efuting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes E No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WJYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? UNo iri Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 EMn 46 of 67 12ACCI,1 rEET M72046 MADEP VPH FORM �tvlatr[x ` ' Aclueous �t l Soil i-i Sediment i7 Other 1 1 Cantaiers ,y R Sati sf actc,ry W, Broken i Leakin ueous�Pres_ervatives N/A PH <=2 F, H >2 Tern ei�tufe ,. Received on Ice Received at 4 Deg. C ! Other ,I Rec'd at 2.1 deg C Mtha ►o( ,- e � N/A A Method for Ranges: m MADEP VPH REV 1.1 Client ID: MT-3/MT-1 Lab ID: M72046-9 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibrom otoluene N/A 4/11/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND A 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/1 ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A u9/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/i ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 90 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons, Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? L1Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? - I,elYes I_' No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? [,it No '_-_' Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 4/15/2008 MIN 47 of 67 ®A=UTEST. M72046 MADEP VPH FORM Matrix Aclueous Soil Sediment j Other Co.ntal-Hers Sat isfactor 14 Broken I—I Leaking ueaus Pres:eruatlues N/A - H <=2 PH >2 Teemrature � :, Received on Ice Received at 4 De . C 1 Other Rec'd at 2.1 deg C M N/A4. Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-5 Lab ID: M72046-10 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 3/28/2008 Date Received: 4/1/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5 Dibromotoluene N/A 4/11/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadi.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/1 ND- 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/1 ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 95 70-130% PID:2,5-Dibromotoluene % 95 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? L.Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ue No Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tan Date 4/15/2008 ®® 48 of 67 �ACCd.ITEST. M72046 Accutest Laboratories Internal Sample Tracking Chronicle P. Shell Oil Job No: M72046 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample Number Method Analyzed By Prepped By Test Codes M7�2046 1 Collected:`28 MAR 08�x 13�50 By` ��F Recelved�'0�1,�APR 08`�B �SfIP E ��� �� "' � ;` �� ;MWr`101 � - ��� s Sri ' �°� �✓: � � �� ���i' `� �� � �'�'�'� M72046-1 EPA 504 09-APR-08 01:10 CZ 08-APR-08 FG V504EDB M72046-1 SW846 8260B 11-APR-08 03:43 AA V8260ETHL M72046-1 MADEP VPH REV 1.1 11-APR-08 16:58 AF VMAVPH M72046-1 MADEP VPH REV 1.1 12-APR-08 12:15 AF VMAVPH M72U46 2 Collected; 2$ MAR 08 13 25Received_,:01-APR 08 �B SA$P� - ., N - _ " 7 h ; k,. _ _ ., M72046-2 EPA 504 09-APR-08 01:40 CZ 08-APR-08 FG V504EDB M72046-2 MADEP VPH REV 1.1 10-APR-08 19:41 AF VMAVPH M72046-2 SW846 8260B 11-APR-08 04:11 AA V8260ETHL M72046 3 f Gollected 28 MAR 08 1�#00 By �R=D Received 01APR�°O8�By� SAPS �"` �� ��``� '� � "�� ,, M72046-3 EPA 504 09-APR-08 02:24 CZ 08-APR-08 FG V504EDB M72046-3 MADEP VPH REV 1.1 10-APR-08 20:22 AF VMAVPH M72046-3 SW846 8260B 11-APR-08 04:38 AA V8260ETHL M72�46 4� Collected�Z8 MAR 08�13 ©O��By�R'F) y��:�eceived OI�APR�,08�By�5 �$� � �� M72046-4 EPA 504 09-APR-08 02:54 CZ 08-APR-08 FG V504EDB M72046-4 MADEP VPH REV 1.1 10-APR-08 21:03 AF VMAVPH M72046-4 SW846 8260B 11-APR-08 05:06 AA V8260ETHL M72046 5 .Collected 28 MAR 08 09�3D By RDA REcciv�dOlAPR08 BySA�P � 4i M72046-5 EPA 504 09-APR-08 03:23 CZ 08-APR-08 FG V504EDB M72046-5 MADEP VPH REV 1.1 10-APR-08 21:45 AF VMAVPH M72046-5 SW846 8260B 11-APR-08 05:34 AA V8260ETHL GT2046Ft6 Collected 28�MAR 081q 1 ByRD �Rec edO1 APR QffB�SAP ' M72046-6 EPA 504 09-APR-08 04:37 CZ 08-APR-08 FG V504EDB Page 1 of 2 Min 49 of 67 12ACCUTEST. I� M72046 Accutest Laboratories Internal Sample Tracking Chronicle Al Shell Oil Job No: M72046 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample Number Method Analyzed By Prepped By Test Codes M72046-6 MADEP VPH REV 1.1 10-APR-08 22:25 AF VMAVPH M72046-6 SW846 8260B 11-APR-08 06:02 AA V8260ETHL M720r46 7�C�ollected 28 N°lAR�08 12 10� RDReceiyed�OI�APR U8B�ySt�P �� ,��,� �� M72046-7 EPA 504 09-APR-08 05:22 CZ 08-APR-08 FG V504EDB M72046-7 MADEP VPH REV 1.1 10-APR-08 23:07 AF VMAVPH M72046-7 SW846 8260B 11-APR-08 06:29 AA V8260ETHL M72046 8 Collected 28 MAR 08 Z0 By *¢ Rece ved O1 APR 08 By SAiP MAW 202 k F M72046-8 EPA 504 09-APR-08 05:51 CZ 08-APR-08 FG V504EDB M72046-8 MADEP VPH REV 1.1 10-APR-08 23:48 AF VMAVPH M72046-8 SW846 8260B 11-APR-08 06:57 AA V8260ETHL M742046 9 Collected 28MAR{3810 40 ByRD RecevedO1APRk08By SAP MT�3 M72046-9 EPA 504 09-APR-08 06:21 CZ 08-APR-08 FG V504EDB M72046-9 MADEP VPH REV 1.1 11-APR-08 00:29 AF VMAVPH M72046-9 SW846 8260B 11-APR-08 07:25 AA V8260ETHL M7Z046 10 Collected�28 MAR08 125QaBy Rb � Received OA R 08�y�SF1Pj " r J M72046-10 EPA 504 09-APR-08 07:05 CZ 08-APR-08 FG V504EDB M72046-10 MADEP VPH REV 1.111-APR-08 03:55 AF VMAVPH M72046-10 SW846 8260B 11-APR-08 07:52 AA V8260ETHL Page 2 of 2 ®Q 50 of 67 12ACPVTEST. M72046 €. ._..... ...... I MIN New England 12AccuTEST 10 Section -GC/MS Volati`les. QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries 51 of 67 12AC PVTWT, ......_:...._.............__._..._. M72046 -......... Method Blank Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File lD DF Analyzed By Prep Date Prep Batch Analytical Batch MSN968-MB N26274.1) 1 04/11/08 AA n/a n/a MSN968 The QC reported here applies to the following samples: Method: SW846 8260B M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 CAS No. Compound Result RL Units Q 64-17-5 Ethanol ND:: 200 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 130/o 1 4°/0 o 0 79 2037-26-5 Toluene-138 90%: 80-120% 460-00-4 4-Bromofluorobenzene 103% 84-115% 52 of 67 MACCt1TEST. M72046 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSN968-BS N26271.D 1 04/10/08 AA n/a n/a MSN968 MSN968-BSD N26272.1) 1 04/10/08 AA n/a n/a MSN968 N The QC reported here applies to the following samples: Method: SW846 8260B M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/l % ug/I % RPD Rec/RPD 64-17-5 Ethanol 5000 4690 94 5250 105 11 25 183/30 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 105% 105% 79-130% 2037-26-5 Toluene-D8 1'Oi% 99%0 80-120% 460-00-4 4-Bromofluorobenzene 1.01% 101% 84-115% � II 53 of 67 12ACC JTEST. M72046 -akor.-1°' ^, Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M72091-1MS N26292.1) 5 04/11/08 AA n/a n/a MSN968 M72091-1MSD N26293.1) 5 04/11/08 AA n/a n/a MSN968 M72091-1 N26275.1) 1 04/11/08 AA n/a n/a MSN968 The QC reported here applies to the following samples: Method: SW846 8260B p M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 M72091-1 Spike MS MS MSD MSD Limits CAS No. Compound ug/l Q ug/I ug/l % ug/l % RPD Rec/RPD 64-17-5 Ethanol ND 25000 24300 97 23800 95; 2 20-190/30 CAS No. Surrogate Recoveries MS MSD M72091-1 Limits 1868-53-7 Dibromofluoromethane 105% 104% 105% 79-130% 2037-26-5 Toluene-D8 101% 101.:% 100%` 80-120% 460-00-4 4-Bromofluorobenzene 100% 102% 103%. 84-115% 54 of 67 12A©PVTPPT. M72046 4 a b',- I r r.; Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: SW846 8260B Matrix: AQ Samples and QC shown here apply to the above method t� Lab Lab Sample ID File 1D Sl S2 S3 M72046-1 N26282.1) 100.0 :: 99.0 MIA: M72046-2 N26283.1) 99.0 99.0 101.0 M72046-3 N26284.1) 100.0 100.0 102:0 M72046-4 N26285.1) <1010 100.0 101.0:< M72046-5 N26286.D 4,03.0 99.0 103.0 M72046-6 N26287.1) 03 0'. 99.0 102.0 M72046-7 N26288.1) 102.0 100.0 1A'41:0 M72046-8 N26289.1) 103 0 '': ' 100.0 103.0 M72046-9 N26290.1) 101.9 - 100.0 104.0'- M72046-10 N26291.D 10,6:0 99.0 104.0 M72091-1MS N26292.1) 1050 101.0 100:0 M72091-1MSD N26293.1) 104 0 101.0 10.2.0 MSN968-BS N26271.1) 105:0 101.0 101.0 MSN968-BSD N26272.1) 105.0 99.0 10 .0 MSN968-MB N26274.1) 104.0 % : 99.0 103.0 Surrogate Recovery Compounds Limits S1 = Dibromofluoromethane 79-13,0% S2 = Toluene-D8 80420%, S3 = 4-Bromofluorobenzene as 55 of 67 JJACCUTEST. M72046 New England ACCI.JTEST ,. Section 6 GC V'latiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries 56 of 67 12AC JTEST M72046 ^. . ...t_..... Method Blank Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD804-MB BD17067.1) 1 04/10/08 AF n/a n/a GBD804 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND,' 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene NO 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/t C5- C8 Aliphatics (Unadj.) ND. 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 93% 70-130% 615-59-8 2,5-Dibromotoluene 94% 70-130% I I 57 of 67 ACCUTEST M72046 Method Blank Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch GBD805-MB BD17091.D 1 04/11/08 AF n/a n/a GBD805 as The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M72046-1, M72046-10 m CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND' 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND' 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) NO 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 946/o 70-130% 615-59-8 2,5-Dibromotoluene 936/6 70-130% ® 58 of 67 12ACC JTEST. M72046 Method Blank Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GWX1906-MB WX40145.D 1 04/12/08 AF n/a n/a GWX1906 css The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M72046-1 CAS No. Compound Result RL Units Q C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9- C10 Aromatics (Unadj.) ND 50 ugA C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 92% 70-130% 615-59-8 2,5-Dibromotoluene .89% 70-130% MIN 59 of 67 �A�fTEST. M72046 - = ' r Method Blank Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15528-MB YZ46422.1) 1 04/08/08 CZ 04/08/08 OP15528 GYZ1988 The QC reported here applies to the following samples: Method: EPA 504 M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/l CAS No. Surrogate Recoveries Limits 460-00-4 Bromofluorobenzene (S) 101% 26-158% 460-00-4 Bromofluorobenzene (S) 26 158% ©� 60 of 67 12ACClJTEST. Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 .lob Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD804-BSP BD17068.1) 1 04/10/08 AF n/a n/a GBD804 GBD804-BSD BD17069.D 1 04/10/08 AF n/a n/a GBD804 os The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 N M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/I % ug/I % RPD Rec/RPD 71-43-2 Benzene 50 45.0 90 45.2 90 :< 0 70-130/25 100-41-4 Ethylbenzene 50 45.7 91 46.4 93 2 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 45.6 M 46.6 93 2 70-130/25 91-20-3 Naphthalene 50 46.9 94 48.9 98 4 70-130/25 108-88-3 Toluene 50 45.5 91 45.8 92 U. 70-130/25 m,p-Xylene 100 89.8 90_ 91.5 92 2 70-130/25 95-47-6 o-Xylene 50 43.8 88 44.6 89 2 70-130/25 C5- C8 Aliphatics (Unadj.) 150 121 81 132 88 01 .. 70-130/25 C9- C12 Aliphatics (Unadj.) 150 125 83 129 86 3 70-130/25 C9- C10 Aromatics (Unadj.) 50 46 93. 48 95 3;' 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 92% 97% 70-130% 615-59-8 2,5-Dibromotoluene 92% 97% 70-130% ®B 61 of 67 12ACCVTEST. M72046 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD805-BSP BD17092.D 1 04/11/08 AF n/a n/a GBD805 GBD805-BSD BD17093.D 1 04/11/08 AF n/a n/a GBD805 os The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 iv M72046-1, M72046-10 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/I % ug/l % RPD Rec/RPD 71-43-2 Benzene 50 43.5 87 44.9 90 - 3 70-130/25 100-41-4 Ethylbenzene 50 45.1 90 46.6 93 3 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 44.9 90 46.4 93 3 70-130/25 91-20-3 Naphthalene 50 46.9 94. 49.1 98 5 70-130/25 108-88-3 Toluene 50 43.9 88 45.6 91 ::' 4 70-130/25 m,p-Xylene 100 88.6 89 91.6 92 3 70-130/25 95-47-6 o-Xylene 50 43.3 87 44.7 89 3 70-130/25 C5- C8 Aliphatics (Unadj.) 150 118 79 120 80 2 70-130/25 C9- C12 Aliphatics (Unadj.) 150 123 82 130 87 6 ' 70-130/25 C9- C10 Aromatics (Unadj.) 50 47 93 48 96 3 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 92.% 97% 70-130% 615-59-8 2,5-Dibromotoluene 92%0 980/6 70-130% 62 of 67 13ACCUTEST M72046 P Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GWX1906-BSP WX40146.1) 1 04/12/08 AF n/a n/a GWX1906 GWX1906-BSD WX40147.1) 1 04/12/08 AF n/a n/a GWX1906 cn The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 N M72046-1 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/l % RPD Rec/RPD C9- C12 Aliphatics (Unadj.) 150 152 101 156 104 3 70-130/25 C9- CIO Aromatics (Unadj.) 50 51.0 102 52.4 105 3 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 919/6 88°l0 70-130% 615-59-8 2,5-Dibromotoluene 94% 95% 70-130% Q® 63 of 67 ®ACCUTEST. .................................. M7204s A r Blank Spike Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15528-BS YZ46423.1) 1 04/08/08 CZ 04/08/08 OP15528 GYZ1988 The QC reported here applies to the following samples: Method: EPA 504 w M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 Spike BSP BSP CAS No. Compound ug/l ug/l % Limits 106-93-4 1,2-Dibromoethane 0.071 0.070 99 70-130 CAS No. Surrogate Recoveries BSP Limits 460-00-4 Bromofluorobenzene (S) 97% 26-158% 460-00-4 Bromofluorobenzene (S) 113%a 26-158% 64 of 67 12ACCl TEST. M72046 - - - Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15528-MS YZ46424.1) 1 04/08/08 CZ 04/08/08 OP15528 GYZ1988 OP15528-MSD YZ46425.1) 1 04/08/08 CZ 04/08/08 OP15528 GYZ1988 M72297-5 YZ46426.1) 1 04/09/08 CZ 04/08/08 OP15528 GYZ1988 rn The QC reported here applies to the following samples: Method: EPA 504 M72046-1, M72046-2, M72046-3, M72046-4, M72046-5, M72046-6, M72046-7, M72046-8, M72046-9, M72046-10 M72297-5 Spike MS MS MSD MSD Limits CAS No. Compound ug/I Q ug/I ug/I % ug/l % RPD Rec/RPD 106-93-4 1,2-Dibromoethane ND 0.071 0.063 89 0.073 103 l;5 65-135/30 CAS No. Surrogate Recoveries MS MSD M72297-5 Limits 460-00-4 Bromofluorobenzene (S) 100%- 117% 106%. 26-158% 460-00-4 Bromofluorobenzene (S) 105%. 118% 119% 26-158% I Q 65 of 67 12ACCUTEST M72046 Volatile Surrogate Recovery Summary Page 1 of 1 .lob Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID Sl a S1 b a) to M72046-1 WX40149.1) 92:0; 90.0 M72046-1 BD17113.D 90.0 90.0 M72046-2 BD17082.D .80.0, 88.0 M72046-3 BD17083.D 87.0 88.0 M72046-4 BD17084.D 89.0- 89.0 M72046-5 BD17085.D 89.10 89.0 M72046-6 BD17086.D 90 0 90.0 M72046-7 BD17087.D 91.0 92.0 M72046-8 BD17088.D 90:0 91.0 M72046-9 BD17089.D 91.0 90.0 M72046-10 BD17094.D 95.0 95.0 GBD804-BSD BD17069.D 970 97.0 GBD804-BSP BD17068.D 92.0 ;` . 92.0 GBD804-MB BD17067.D 93.0 I' 94.0 GBD805-BSD BD17093.D 97.0` 98.0 GBD805-BSP BD17092.D 920 92.0 GBD805-MB BD1709I.D 94:0: 93.0 GWX1906-BSD WX40147.1) 880 95.0 GWX1906-BSP WX40146.1) 91::0 94.0 GWX1906-MB WX40145.D 92;0 89.0 Surrogate Recovery Compounds Limits S1 = 2,5-Dibromotoluene 707130% (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 Q( 66 of 67 12QC AJTEST. 1� • ? w 'Y Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M72046 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: EPA 504 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b a) M72046-1 YZ46427.D 1;150 116.0 M72046-2 YZ46428.1) 92,..W 97.0 M72046-3 YZ46429.1) 1,211.0 119.0 M72046-4 YZ46430.1) 108.0 120.0 M72046-5 YZ46431.D 98 0 »< 114.0 M72046-6 YZ46433.D 101 0 108.0 M72046-7 YZ46434.D 88 0 108.0 M72046-8 YZ46435.1) 104.0 124.0 M72046-9 YZ46436.D 107:0: 119.0 M72046-10 YZ46437.1) 115.0 109.0 ' OP15528-BS YZ46423.1) 974 113.0 OP15528-MB YZ46422.D .1011.01 111.0 OP15528-MS YZ46424.1) 100.:0. 105.0 OP15528-MSD YZ46425.1) 117.0 i< 118.0 Surrogate Recovery Compounds Limits S 1 = Bromofluorobenzene (S i 26-1586/o (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 Q® 67 of 67 13ACCUTEST. M72046 Y _ t. OVE RE I G N CON t September 8,2008 DHL#28881754451 Town of Hyannis Town Engineer 367 Main Street Hyannis, MA 02601 Re: Groundwater Sampling Results,August 2008 Former Shell Branded Gasoline Station#137772 590 Iyannough Road Hyannis,MA Dear Town Engineer: t, Pursuant to your authorization Sovereign Consulting Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH), gasoline oxygenates, ethylene-dibromide (EDB), and dissolved lead. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVEREIGN CONSULTING,INC. Sylvia M. Kirsch Project Manager -`ten Attachments: Laboratory Data Reports Cn ._ cc: with attachment Mr.David Weeks,Motiva Czs MassDEP- SERO c m Sovereign File-EQ872 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CM 40.1403(10) of the Massachusetts Contingency Plan 71 LL BWSC 123 This Notice is Related to Release Tracking Number 4� 17651 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 590 lyannough Rd. City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Hyannis,Town Engineer 2. Street Address: 367 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. Q✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. Q✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked,the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 590 lyannough Rd. City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase 11 Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, grot.ndwater)to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Sylvia Kirsch Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: skirsch@sovcon.com NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. e-Hardcopy 2.0 Automated Report New England rs Laboratories - .... . 3ecinicalReport fart nr Shell Oil SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA EQ 872 Accutest Job Number: M76251 Sampling Date: 08/14/08 Report to: dcollins@sovcon.com ATTN: Diane Collins Total number of pages in report: 111 Q i""Co"o X..;j • ". Test results contained within this data package meet the requirements eZa�5.1 of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) Y E A. R S NY(11791) N](MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • http://www.accutest.com ®In 1 of 111 12A M76251 laeo'�Ihfi4: Sections: Table of Contents -1- Section1: Sample Summary ................................................................................................... 4: Section2: Case Narrative/Conformance Summary.............................................................. 7 Section3: Sample Results ........................................................................................................ 9 3.1: M76251-1: GT-1 ........................................................................................................... 10 3.2: M76251-1A: GT-1 ........................................................................................................ 13 3.3: M76251-2: GT-3 ........................................................................................................... 14 3.4: M76251-2A: GT-3 ........................................................................................................ 17 3.5: M76251-3: GT-4 ........................................................................................................... 18 3.6: M76251-3A: GT-4 3.7: M76251-4: GT-5 ........................................................................................................... 22 3.8: M76251-4A: GT-5 ........................................................................................................ 25 3.9: M76251-5: GT-7 ........................................................................................................... 26 3.10: M76251-5A: GT-7 ...................................................................................................... 29 3.11: M76251-6: MW-101 ................................................................................................... 30 3.12: M76251-6A: MW-101 ..............................................................:................................. 33 3.13: M76251-7: MW-102 ................................................................................................... 34 3.14: M76251-7A: MW-102 ................................................................................................ 37 3.15: M76251-8: MT-1/1VIT-3 ......................................................................:....................... 38 3.16: M76251-8A: MT-1/MT-3 ........................................................................................... 41 3.17: M76251-9: MW-202 ................................................................................................... 42 3.18: M76251-9A: MW-202 ................................................................................................ 45 3.19: M76251-10: MW-202D .............................................................................................. 46 3.20: M76251-10A: MW-202D ........................................................................................... 49 3.21: M76251-11: MW-301D .............................................................................................. 50 3.22: M76251-11A: MW-301D ........................................................................................... 53 3.23: M76251-12: MW-301 S .............................................................................................. 54 3.24: M76251-12A: MW-301S ............................................................................................ 57 3.25: M76251-13: MW-302D .............................................................................................. 58 3.26: M76251-13A: MW-302D ........................................................................................... 61 3.27: M76251-14: MW-302S ................... 3.28: M76251-14A: MW-302S ............:............................................................................... 65 Section4: Misc. Forms ............................................................................................................ 66 4.1: Chain of Custody ........................................................................................................... 67 4.2: MCP Form ..................................................................................................................... 70 4.3: VPH Form ...................................................................................................................... 71 4.4: Sample Tracking Chronicle ........................................................................................... 85 Section 5: GC/MS Volatiles- QC Data Summaries .............................................................. 90' 5.1: Method Blank Summary ................................................................................................ 91 5.2: Blank Spike/Blank Spike Duplicate Summary ...:.......................................................... 92 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 93 5.4: Surrogate Recovery Summaries ..................................................................................... 94 Section 6: GC Volatiles - QC Data Summaries ..................................................................... 95 ®� 2 of 141` 12AC CUTEST. M76251 fist or a to r:c> Table of Contents Sections: 2 6.1: Method Blank Summary ................................................................................................ 96 6.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 98 6.3: Blank Spike Summary ................................................................................................... 99 6.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 100 6.5: Surrogate Recovery Summaries ..................................................................................... 101 Section 7: Metals Analysis- QC Data Summaries ................................................................ 103 7.1: Prep QC MP12365: Pb .................................................................................................. 104 Mel 3 of 111 gACCUTEST. M76251 -atom-,I ri is Accutest Laboratories Sample Summary Shell Oil Job Nw M76251 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M762a41 08/14/08 09:50 AW 08/15/08 AQ Ground Water G 1 k 76251 1A 08/14/08 09:50 AW 08/15/08 A Groundwater Filtered GT�1 F _ Q _. .... M7671 2 x 08/14/08 08:30 AW 08/15/08 AQ Ground Water GT 3 A xMF625s1; A y 08/14/08 08:30 AW 08/15/08 AQ Groundwater Filtered GT3 M76251 08/14/08 09:15 AW 08/15/08 AQ Ground Water M76251 3A ;08/14/08 09:15 AW 08/15/08 AQ Groundwater Filtered GT 4 M76251 4 08/14/08 10:15 AW 08/15/08 AQ Ground Water M76251 N4A 08/14/08 10:15 AW 08/15/08 AQ Groundwater Filtered GT ` M?625a1 5 08/14/08 09:30 AW 08/15/08 AQ Ground Water GT 7 M7t251 5A '':08/14/08 09:30 AW 08/15/08 AQ Groundwater Filtered GT 7 M762b1 6 08/14/08 12:10 AW 08/15/08 AQ Ground Water MW t01 M7621 6A '08/14/08 12:10 AW 08/15/08 AQ Groundwater Filtered MW l;lll M76251 7 08/14/08 12:35 AW 08/15/08 AQ Ground Water14W02 4 of 111 12ACCLlTEST M76257 L`b c r 3 t.ri .S r Accutest Laboratories Sample Summary (continued) Shell Oil Job No: M76251 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample CollectedZ Matrix Client Number Date Time By Received Code Type Sample ID Ms6217 ,08/14/08 12:35 AW 08/15/08 AQ Groundwater Filtered M7621 8 ' 08/14/08 12:15 AW 08/15/08 AQ Ground Water W/114T 3 M76251 8A 08/14/08 12:15 AW 08/15/08 AQ Groundwater Filtered �IITIx% IT Y Mx76251 9 ' 08/14/08 11:30 AW 08/15/08 AQ Ground Water MW 202 M76251 9A 08/14/08 11:30 AW 08/15/08 AQ Groundwater Filtered MAW2l)2 M762" 10 08/14/08 11 AC AW 08/15/08 AQ Ground Water NIW 2`02D ; M76ti51 l0A 08/14/08 11:40 AW 08/15/08 AQ Groundwater Filtered kMW M7621 11 .'08/14/08 10:30 AW 08/15/08 AQ Ground Water MW 3U11� M76251 x1A 08/14/08 10:30 AW 08/15/08 AQ Groundwater Filtered MW`301D M76251 12.`'08/14/08 10:40 AW 08/15/08 AQ Ground Water MW 30, M76251 1m 08/14/08 10:40 AW 08/15/08 AQ Groundwater Filtered MW;3.O1S M7. 13 08/14/08 11:10:AW 08/15/08 AQ Ground Water MW 30215 M76251 13A` 08/14/08 11:10 AW 08/15/08 AQ Groundwater Filtered M<W 302D ®� 5 of 111 1 Accutest Laboratories �. Sample Summary Shell Oil (continued) SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Job No: M76251 Project No: EQ 872 Sample °Clected Matrix Client Number Date Time By Received Code Type Sample ID M76251 I4.,. 08/14/08 11:10 AW 08/15/08 AQ Ground Water BMWOZ� , , .. 1Y761.l°4Y�,.08/14/08 11:10 AW 08/15/08 AQ Groundwater Filtered 11if142S I ®� 6 of III ®ACCU TEST. M76251L-t'C'—t a 1;?c 'AL U a T L a b o r a t o r i e S SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M76251 Site: SCMAW:97451486(REIMBMA)590 lyannough Road Hyannis MA Report Date 8/28/2008 10:19:08 AM 14 Sample(s)were collected on 08/14/2008 and were received at Accutest on 08/15/2008 properly preserved,at 2 Deg.C and intact. These Samples received an Accutest job number of M76251.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GCMS By Method SW846 8260B Matrix AQ Batch ID: MSG3395 N All samples were analyzed within the recommended method holding time. ® All method blanks for this batch meet method specific criteria. 0 Sample(s) M76251-5MS,M76251-5MSD were used as the QC samples indicated. M Only MTBE,DIPE,TAME,ETBE and TBA requested. Volatiles by GC By Method EPA 504 Matrix AQ Batch ID: OP16540 0 All samples were extracted within the recommended method holding time. d All samples were analyzed within the recommended method holding time. a All method blanks for this batch meet method specific criteria. 0 Sample(s) M76326-3MS,M76326-3MSD were used as the QC samples indicated. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GBD985 All samples were analyzed within the recommended method holding time. m All method blanks for this batch meet method specific criteria. Metals By Method SW846 6010B Matrix AQ Batch ID: MP12365 All samples were digested within the recommended method holding time. All samples were analyzed within the recommended method holding time. ■ All method blanks for this batch meet method specific criteria. m Sample(s) M76251-10ADUP,M76251-10AMS,M76251-10ASDL were used as the QC samples for metals. s RPD(s)for Serial Dilution for Lead are outside control limits for sample MP12365-SDI. Percent difference acceptable due to low initial sample concentration(<50 times IDL). Only Lead requested. Note:Compounds whose QC limits are outside MCP criteria are designated by the lab as"Difficult".QC criteria for a"Difficult" compound may meet Accutest in-house generated QC criteria but exceed MCP criteria(compounds exceeding Accutest QC criteria are flagged on the QC summary).Refer to the QC summary pages. Thursday,August 28,2008 Page 1 of 2 ®n 7 of 111 GACCUrEST. M76251 L=tots e: The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its enti ety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M76251). Thursday,August 28,2008 Page 2 of 2 ®O 8 of I I I QACCUTEST. M76251 tat o rato ries 1 ' New England ACCUT86 Section 3 Sample Results: 3 Report of Analysis ®� 9 0 I IMACCL EST. a } Y Accutest Laboratories w Report of Analysis Page 1 of I tn Client Sample ID: MT-1/MT-3 Lab Sample ID: M76251-8 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84097.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q ........... .. ... .... _ 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether LVD 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND. . _x., 20 ug/1 637-92-3 tert-Butyl Ethyl Ether N,D 2.0 ug/1 CAS No. Surrogate Recoveries Run# I Run#2 Limits 1868-53-7 Dibromofluoromethane 10I% 79-130% 2037-26-5 Toluene-D8 90 80-120% 460-00-4 4-Bromofluorobenzene 94% 80 120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 38 of I I I OAC.0 UTEST. s Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MT-1/MT-3 Lab Sample ID: M76251-8 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20739.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene N3D : 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene I1D 3.0 ug/l 108-88-3 Toluene N'D 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj ) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene $0%. 70-130% 615-59-8 2,5-Dibromotoluene 90°l0. 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 39 of 111 12ACCIJ717EST M76251 L w tc:,;,r:c: Accutest Laboratories w Report of Analysis Page I of I Client Sample ID: MT-1/MT-3 Lab Sample ID: M76251-8 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20737.D 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 37.0 rut 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.014 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 104% 26-158% ...:::......... 460-00-4 Bromofluorobenzene (S) W/ 26 158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 40 of 111 QAC=XrEST. M76251 L-bs:at—;— } Accutest Laboratories Report of Analysis Page 1 of 1 M Client Sample ID: MT-1/MT-3 Lab Sample ID: M76251-8A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead 5 0 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ®� 41 of 111 QACCUTEST. M76251 L=t ratt,, ,.; Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-202 Lab Sample ID: M76251-9 Date Sampled: 08/14/08 Matrix: AQ -Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84098.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/I 1634-04-4 Methyl Tert Butt'1 Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methy] Ether ND 2.0 ug/I 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I CAS No. Surrogate Recoveries Run# 1. Run#2 Limits 1868-53-7 Dibromofluoromethane LO1% 79-130% 2037-26-5 Toluene-D8 96% 80-120% 460-00-4 4-Bromofluorobenzene 91% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IM® 42 of 111 QACCUTEBT. M76251 ito: :o::=: Accutest Laboratories Report of Analysis Page 1 of 1 y Client Sample ID: MW-202 Lab Sample ID: M76251-9 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP'VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20740.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether NO. 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj ) Nl) - 50 ug/I C9- C12 Aliphatics (Unadj) ND 50 ug/l C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 8..2%' 70-130% 615-59-8 2,5-Dibromotoluene 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 43 of I I I QACCU E3T: t Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-202 Lab Sample ID: M76251-9 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20738.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 36.0 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene S 9:1%. o ( ) 26 158/o 460-00-4 Bromofluorobenzene (S) 77%0 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME] 44 of 111 QACCUTEB T. M76251 L-to rut o,l i Accutest Laboratories w Report of Analysis Page 1 of I CO Client Sample ID: MW-202 Lab Sample ID: M76251-9A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead 5 0' 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A Z (1) Instrument QC Batch: MA:9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ®� 45 of I I I MAC M76251 Latoriz.,; u Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-202D Lab Sample ID: M76251-10 Date Sampled: 08/14/08 Matrix: AQ- Ground Water Date Received: 08/15/08 Method: SW846 3260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch An alytical Batch Run#1 G84099.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether Np 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/I 637-92-3 tert-Butyl Ethyl Ether ND.::.:;. 2.0 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluorom�!thane LO1% 79130% 2037-26-5 Toluene-D8 97%. 80-120% 460-00-4 4-Bromofluorobenzene 93% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 131q 46 of 111 MACCUTEST M76251 L-tor3to-:at Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-202D Lab Sample ID: M76251-10 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEF VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20741.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71 43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene YND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene IVD 2.0 ug/1 C5- C8 Aliphatics (Unad3 ) ND 50 ug/I C9- C12 Aliphatics (Unadj ) ND. 50 ug/l C9-C10 Aromatics (Unad3 ) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $2% 70130% 615-59-8 2,5-Dibromotoluene 91% 70130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds cali5ration range N = Indicates presumptive evidence of a compound ®� 47 of I l l 12ACCUTEST. M76251 L-t—:4 c- i-- Accutest Laboratories w Report of Analysis Page I of 1 Client Sample ID: MW-202D Lab Sample ID: M76251-10 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20739.D 1 08/20/08 CZ O8/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 37.1 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane N.D 0.014 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 110% 26-158% 460-00-4 Bromofluorobenzene (S) 88% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®21 48 of 111 M76251 Accutest Laboratories w Report of Analysis Page 1 of I o Client Sample ID: MW-202D Lab Sample ID: M76251-10A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <5 Q 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit 49 of I l l UACCUTEST M76251 -eon-O,',fi_. Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-301D Lab Sample ID: M76251-11 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84100.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether N'D 1.0 ug/I 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND- 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 100% 79-130% 2037-26-5 Toluene-D8 95% 80-120% 460-00-4 4-Bromofluorobenzene 91% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M 50 of 111 ACCUTEST. M76251 L_t Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-301D Lab Sample ID: M76251-11 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20742.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene NO:. 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND: : 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9-C12 Aliphatics (Unadj.) NO 50 ug/l C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics NI 50 ug/I C9- C12 Aliphatics NO 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 820/. 70-130% 615-59-8 2,5-Dibromotoluene 91% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound an 51 of III A ST. M76251 j:<::;,.. Accutest Laboratories w Report of Analysis Page I of I Client Sample ID: MW-301D Lab Sample ID: M76251-11 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20740.D 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 35.3 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND_ 0.015 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 1040/0 26-158% 460-00-4 Bromofluorobenzene (S) 89% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IM® 52 of I I I ACCLrrEST_ M76251 =-t c:�Z"r�ts o Accutest Laboratories w Report of Analysis Page 1 of 1 N Client Sample ID: MW-301D Lab Sample ID: M76251-11A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <5.0 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit M 53 of I I I ACCU'TEST. M76251 L-t:�f;t -ie= Accutest Laboratories w Report of Analysis Page 1 of 1 w Client Sample ID: MW-301S Lab Sample ID: M76251-12 Date Sampled: 08/14/08 Matrix: AQ- Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84101.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q .......... . _. ... 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND. 1.0 ug/I 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND.- 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I r CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 100% 79-130% 2037-26-5 Toluene-D8 98% 80-120% 460-00-4 4-Bromofluorobenzene 90% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Effl 54 of III ACCUTES . M76251 'L=tt:o:—'I Accutest Laboratories w Report of Analysis Page 1 of 1 w Client Sample ID: MW-301S Lab Sample ID: M76251-12 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20743.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND.. 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene :NDI. 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics. (Unadj.) NO 50 ug/1 C9- C12 Aliphatics (Unadj.) NO:: 50 ug/1 C9- C10 Aromatics (Unadj.) NO 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 83%0 70-130% 615-59-8 2,5-Dibromotoluene 916/0 70-130% NO = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Mffl 55 of 111 ACCITTEBT. Accutest Laboratories w Report of Analysis Page 1 of 1 w Client Sample ID: MW-301S Lab Sample ID: M76251-12 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 B1320742.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 37.4 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND . .0.014 ug/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) '103% 26-158% 460-00-4 Bromofluorobenzene (S) 88% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 56 of 111 ACCU'TEST M76251 ; -1L=!3c1,-iec Accutest Laboratories w Report of Analysis Page I of 1 K3 Client Sample ID: MW-301S Lab Sample ID: M76251-12A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <5.0` 5.0 ug/I 1 08/21/08 08/22/08 PY Sw846 6010B SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ® 57 of 111 ACCLJT'ES"T. M76251 Cor :or ez Accutest Laboratories w Report of Analysis Page 1 of 1 Cn Client Sample ID: MW-302D Lab Sample ID: M76251-13 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84102.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 1.7 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ,ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100% 79-130% 2037-26-5 Toluene-D8 95% 80-120% 460-00-4 4-Bromofluorobenzene 90% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6919 58 of 111 A►CCUTEST M76251 'a t o:—- n> Accutest Laboratories w Report of Analysis Page 1 of 1 K) Client Sample ID: MW-302D Lab Sample ID: M76251-13 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20744.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene N1 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND: 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene 89% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME] 59 of 111 ACCU•T'EST. M76251 --t-_tlr �_ Accutest Laboratories w Report of Analysis Page 1 of 1 K) Client Sample ID: MW-302D Lab Sample ID: M76251-13 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20743.D 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 33.0 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.016 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 940/6 26 158% 460-00-4 Bromofluorobenzene (S) 62% 26 158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 60 of I I I ST: Accutest Laboratories w Report of Analysis Page 1 of I Client Sample ID: MW-302D Lab Sample ID: M76251-13A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <5 0 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit 61 of I I I ACCUTEST. M76251 - atorr;o-;— Accutest Laboratories w Report of Analysis Page 1 of 1 y Client Sample ID: MW-302S Lab Sample ID: M76251-14 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84103.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ;ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol NI) 20 ug/I 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane J.04% 79-130% 2037-26-5 Toluene-D8 96% 80-120% 460-00-4 4-Bromofluorobenzene 89% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound E) 62 of 111 ACCLrrEST. Accutest Laboratories w Report of Analysis Page I of I y Client Sample ID: MW-302S Lab Sample ID: M76251-14 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20745.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q .. .... ... . .... .._.. 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene Nl) 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 8I% 70-130% 615-59-8 2,5-Dibromotoluene 89% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 63 of 111 ACCUTEST. M76251 = t r °""- Accutest Laboratories w Report of Analysis Page 1 of 1 y Client Sample ID: MW-302S Lab Sample ID: M76251-14 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20744.D 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 36.6 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane N.p 0.014 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 99% 26-158% 460-00-4 Bromofluorobenzene (S) 779/o 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ® 64 of 111 ACCUTEST. Accutest Laboratories w Report of Analysis Page 1 of 1 K) Client Sample ID: MW-302S Lab Sample ID: M76251-14A Date Sampled: 08/14/08 Matrix: AQ -Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead 15 y0 rv: 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010E 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit Mel 65 of 111 ACC U TEST: M76251 Lzt of atori o; i ®� New England Accu�-�sr a... }t o r i c sSection 4 Mist Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle I �® 66 of 111 12ACM TEST. M76251 LAB(LOCATION) Shell Oil Products Chain Of Custody Record YAI,(. El ::x please Cho ck.A.p.. ptiat0:8OXI::: :::INCID ..*1(EN1V S1ERV1ICES) :0 n IT NO awoug 0 0 .� ❑ : ACaMZS 1 ! 1 1 SirDATE: .... ....... ........ ........ 0 anea I -j 10%IELLKPBIW J I D aniet ............. i-T- PAGE of an 11 sa,I fit/—tool: Sovereign Consulting 590 Iyannough Road.HyannK MA 905 B South Main Street 401- Mansfield,MA 02048 Al T l"LL L4, IM- t,STMDAFLD414 MY) DAYS[15Mn ❑1 mn 0 2 can ONHOM REQUESTED ANAMIS ELVER ALES: 0n [a mp 0 G1 oTl*a(5,-CIM TEMPERATURE ON rECEIPTC fmkr/e 1We.12 ;Cq .3 a SPECIAL INSTRUCTIONS OR NOTES: i-C A PLEASE FILTER DISSOLVED LEAD SAMPLES IN LAB PRIOR TO ANALYSIS. Field Sample Identification Contain-Pm R-Op w O or Labmtoy Notas a- 6-t ID,43- 6v X IXI 1*7 X K,X It k.0-1 to C' 4, CAW I-r 4 L w "K---*"* CA '7 ;nza !A ;rJ e't 16 /,INV 14 1 [-t— Wrl, 14 Iloo v v ,P, also .ts , — Y" rl'..qzAv5, M76251: Chain of Custody Page I of 3 67 of III aAC=rrEErr. M76251 LAD(LOCATION) Shell Oil Products Chain Of Custody Record ........ — :.:!f4C1bEWrX(FNV:MV10ES) XvrEp a C.T. U= a- 1 DATE: .......... PO p of El mm L PAGE: 7 So—reign C—ItIng 590 an Road,Hyannis,MA 905 B South Main SI-4 P, Mansfield,NA 02048 --m— WO-339-3249 TUW"ROU- 0-5N 0 s Na-AD(.4 MI) 13 5 W's OlMrs (12 onus (3 1•.IWM REQUESTED X&YSIS DEWERABLE& ID CDWU C3 Cw" El Na 13 po (2)0n (Spmm TEWERATUREMRECEPTC- Ca 81 SPECIAL INSTRUCTIONS OR NOTES: LL PLEASE FILTER DISSOLVED LEAD SAMPLES IN LAB PRIOR TO ANALYSIS. • SAMPLING Field Sample Identiflcadon GATE T-. C.01..Pw Reafto. Lb..wy Ndp A. /I U ;hf 6x- GU 0 t)L) I I T l'f v -±Hff -TFF -/I;,, 14W M76251: Chain of Custody Page 2 of 3 68 of 111 j2AC=rrEBT. M76251 L,b s-i,1,,i tq c Page I of I Frank D'Agostino From: Collins,Diane[DCollins@sovoon.com) Sent: Wednesday,September 03,2008 10:11 AM To: Frank D'Agostino Cc: Kirsch,Sylvia Subject:Well ID Incorrect-Lab Sample M76251 Hi Frank, Can you please correct sample ID and reissue data package for Lab sample M76251 M76251-7-ID M W-103 Sample ID should be MW-102. Please confirm when it's ready. Thank you di Diane Collins Client Support Administrator Sovereign Consulting,Inc. 905B South Main Street Suite 202 Mansfield,MA 02048 P:508-339-3200 Ext.259 F:508-339-3248 email:DCollinslasovcon.com J N Ch I n A� "►y b � w 0 0 Oh 9/3/2008 o � Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 tV Title: MADEP MCP Response Action Analytical Report Certification Form Laboratory Name: Accutest Laboratories of New Enoland Project#: M76251 Project Location: SCMAW:97451486(REIMBMA)590 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M76251-1 through M76251-14 Test method:EPA 504,and below Sample Matrices: Groundwater X Soil/Sediment () Drinking Water () Other: () () - Su _ g 8260E X 8151A 8330 601013 X 7470A/1A fe 8270C 8081A 2 X 8082 8021 B EPH 7000 S 3 7196A to N�Q L�stuR ?rac �_ `� •� y� " �" ,� -, " An affirmative response to questions A,B,C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with Yes ❑ No ' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards orguidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty",as described in Section 2.0(a),(b),(c)and Yes ❑No ' (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without Yes ❑No ' significant modifications,as specified in Section 11.3? A response to questions E and F below is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the Yes No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified ❑ Yes No ' method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned,attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is,to the best of my knowledge and belief,accurate and complete. Si nature: Position: Laboratory Director Printed Name: Reza Tand Date: 08/28/2008 ®� 70 of 111 QACCU EEM M76251 IGcrco MADEP VPH FORM Clllattx� Aqueous W, Soil n Sediment F' Other -I Jyj� 1 ,Satisfactor � Broken Leaking s ueol s F'resetvattves N/A H <= 2 H > 2 F, oaf Received on Ice Received at 4 Deg. C Other Reed at 2.0 Deg.C et>it� z N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MT-1/MT-3 Lab ID: M76251-8 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: , 9 First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ugA ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ugA ND 2 I i Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ugh ND 2 JAdiusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% I PID:2,5-Dibromotoluene % 90 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the i concentration of Target Analytes eluting in that range. IC Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. IZ A'Yqualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? nYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? [':/]No r_I Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 8/28/2008 Printed Name Reza Tand ®® 78 of III ®ACCUTE3T M76251 Labors ,;es MADEP VPH FORM Mat%tax Aqueous W Soil I-1 Sediment F-1 Other I CoYftaai e"rs _� Satisfactory IP Broken Eli Leaking A ueous Pres6005 TO-s N/A 7, 1 pH <= 2 Wi pH > 2 ettl g ftC1 £„ Received on Ice Received at 4 De . C rl Other .i Rec'd at 2.0 Deg.C x � NIA A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-202 Lab ID: M76251-9 C4 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. c Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ! No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 1JYes !_I No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? C�1No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 8/28/2008 Printed Name Reza Tand M® 79 of 111 FQACCUTEST. M76251 1 -t—. ;o,;" o MADEP VPH FORM Aqueous ✓; Soil Fi Sediment F]. Other 1 COn 81 t W ��� Satisfactor ✓1 Broken I Leakin iieofsP esua esa N/A Tr�ettat Received on Ice Received at 4 Deg. C ' Other Fej Rec'd at 2.0 Deg.C thin# N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-202D Lab ID: M76251-10 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadi.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/l ND" 50 Target AnalAes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ugA ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 IAdiusted Ranges C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ugA ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 'Yes `- No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ✓'Yes '..: No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 1No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 8/28/2008 Printed Name Reza Tand' IMP] 80 of 111 MACCUTEST M76251 t-t:o-3t—r— MADEP VPH FORM Matrfx Aclueous Soil �! Sediment I Other F. ContalneSMa Satisfactor [w 1 Broken 1 i Leaking f7 A='ue®us Preset raltive N/A pH <= 2 [,vl PH > 2 r� TemORMWOMI Received on Ice FI Received at 4 De . C !-1 Other �; Rec'd at 2.0 Deg.C N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301D Lab ID: M76251-11 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A . FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 I o-Xylene 95-47-6 C9-C12 ug/I ND 2 1 m,p-Xylene C9-C12 ug/I ND 2 IAdiusted Ranges C5-C8 Aliphatics N/A ug/I ND 8 50 i I C9-C12 Aliphatics N/A ug/I ND c 50 i Surrogate Recoveries Acceptance Range i FID:2,5-Dibromotoluene % 82 70-130% I PID:2,5-Dibromotoluene % 91 70-130% (Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. c Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude i conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. IZ A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? l�!Yes '_, No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? �jYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? L1No I� Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 019 81 of 111 ACCUTEST. a MADEP VPH FORM Aqueous W Soil 111 Sediment F ! Other 7; Go in Satisfacto ✓) Broken D Leaking I_ A-"u"s Presenrativesl: N/A 17 H <= 2 WJ1 PH > 2 i Teat "eiaf`Lrre � ` Received on Ice M Received at 4 Deg. C F! Other (�ii Reed at 2.0 Deg.C M-'Oth WV1 N/A A Method for Ranges: MADEP VPH REV1.1 Client ID: MW-301S Lab ID: M76251-12 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 ,VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: WA 1 N/A I Unadjusted Ranges CAS# Elution Range Units Result RDL Q i C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Benzene 71-43-2 C5-C8 ug/l ND 2 m,p-Xylene C9-C12 ug/I ND 2 i o-Xylene 95-47-6 C9-C12 ug/I ND 2 I Naphthalene 91-20-3 N/A ug/I ND 3 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND 8 50 ,Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 83 70-130% PID:2,5-Dibromotoluene % 91 70-130% !Footnotes !A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range :B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ;c Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. 1Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes 0 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? !�Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? LV ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 8/28/2008 Printed Name Reza Tand O® 82 of 111 M76251 to-3:o la: MADEP VPH FORM A ci ueous I✓i Soil ill Sediment 17 Other F, Corttarnecs � ti.: Satisfactor ✓1 Broken P Leaking ueolasPrese%vattves N/A f I H <= 2 �I H > 2 f Tem erature Received on Ice Received at 4 De a. C Other ✓1 Rec'd at 2.0 Deg.C Mthan_o;f Y N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-302D Lab ID: M76251-13 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL 4 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analvtes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 i I Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 i iAdjusted Ranges C9-C12 Aliphatics N/A ug/I ND c 50 C5-C8 Aliphatics N/A ug/I ND' 50 (Surrogate Recoveries Acceptance Range I PID:2,5-Dibromotoluene % 89 70-130% FID:2,5-Dibromotoluene % 79 70-130 Footnotes 1A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range i6 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. IC Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. jZ A'Yqualifier indicates an estimated value i Were all QA/QC procedures REQUIRED by the VPH Method followed? WIYes 'I No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WiYes 0 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? F--'!No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 83 of 111 ACCUTEST. M76251 -::a---I a<1:;e, MADEP VPH FORM Matrix 3ku ::. ..r Ague ous I✓� Soil F Sediment F-1, Other i Conk Hers ' Satisfactor I✓! Broken - LeakingI A�uetius:Preservattu,s N/A �-; H <- 2 ✓I H > 2 r Them erature x `r'' Received on Ice Received at 4 Deg. C Other I✓ Rec'd at 2.0 Deg.C Nlehao[ N/A +� Method for Ranges: MADEP VPH.REV 1.1 Client ID: MW-302S Lab ID: M76251-14 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 jo-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 i Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 1,Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 ;Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 89 70-130% FID:2,5-Dibromotoluene % 81 70-130% Footnotes ;A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range IB Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. IC Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? V Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? . !Yes {_ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? �No _ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 84 of 111 Accutest Laboratories Internal Sample Tracking ChronicleP. Shell 0i1 Job No- M76251 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes Raw 09�B�A�W� Recele�1 AtJOSBy '� M76251-1 SW846 8260B 19-AUG-08 00:40 EL V8260OXY5 M76251-1 EPA 504 20-AUG-08 07:46 CZ 19-AUG-08 FG V504EDB M76251-1 MADEP VPH REV 1.123-AUG-08 10:12 AF VMAVPH .�.���«:a� �.. z�:z '.9�...�"�..,p�� t'.���.,.:,�..:-<:F...,.....�,..✓r �a`,�„s�:.,,r,. P...y� £-'�v-.�? �: .. .:� k::� .;f��.-�".��z.��. �.as�,�..e'.' � M76251-2 SW846 8260B 19-AUG-08 01:12 EL V8260OXY5 M76251-2 EPA 504 20-AUG-08 08:46 CZ 19-AUG-08 FG V504EDB M76251-2 MADEP VPH REV 1.123-AUG-08 10:53 AF VMAVPH M76251-3 SW846 8260B 19-AUG-08 01:43 EL V8260OXY5 M76251-3 EPA 504 20-AUG-08 09:16 CZ 19-AUG-08 FG V504EDB M76251-3 MADEP VPH REV 1.123-AUG-08 11:34 AF VMAVPH M76251-4 SW846 8260B 19-AUG-08 02:14 EL V8260OXY5 M76251-4 EPA 504 20-AUG-08 09:46 CZ 19-AUG-08 FG V504EDB M76251-4 MADEP VPH REV 1.123-AUG-08 12:15 AF VMAVPH M76251� C�alle�ed.�4�AUG�08 09 30 B,�y A�W„ Received 1�AUG 0`8 B�� 3AJ' ��� �� � �� � �� M76251-5 SW846 8260B 19-AUG-08 02:45 EL V8260OXY5 M76251-5 EPA 504 20-AUG-08 10:16 CZ 19-AUG-08 FG V504EDB M76251-5 MADEP VPH REV 1.123-AUG-08 12:56 AF VMAVPH M76251 6Collec'e 1�4 t3Gfl81Z 1fl� yA Received 15 AtG 08ySAP �s M76251-6 SW846 8260B 19-AUG-08 04:20 EL V8260OXY5 M76251-6 EPA 504 20-AUG-08 10:46 CZ 19-AUG-08 FG V504EDB Page 1 of 5 85 of 111 ®A '�� • r Accutest Laboratories Internal Sample Tracking Chronicle A Shell Oil Job No: M76251 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes M76251-6 MADEP VPH REV 1.123-AUG-08 13:37 AF VMAVPH M76251-7 SW846 8260B 19-AUG-08 04:52 EL V82600XY5 M76251-7 EPA 504 20-AUG-08 11:15 CZ 19-AUG-08 FG V504EDB M76251-7 MADEP VPH REV 1.123-AUG-08 14:18 AF VMAVPH MT 0-111'ram M76251-8 SW846 8260B 19-AUG-08 05:23 EL V82600XY5 M76251-8 EPA 504 20-AUG-08 11:44 CZ 19-AUG-08 FG V504EDB M76251-8 MADEP VPH REV 1.123-AUG-08 14:59 AF VMAVPH M76251-9 SW846 8260B 19-AUG-08 05:55 EL V82600XY5 M76251-9 EPA 504 20-AUG-08 12:14 CZ 19-AUG-08 FG V504EDB M76251-9 MADEP VPH REV 1.123-AUG-08 15:40 AF VMAVPH 1VI7�L�,�1��g10Clleeied��4��1L7C��08�1�1 40�B�y".<,�A�Y]if��' �ecevel�' 98�" �ZSAP�`�� �'� ' M76251-10 SW846 8260B 19-AUG-08 06:27 EL V82600XY5 M76251-10 EPA 504 20-AUG-08 12:44 CZ 19-AUG-08 FG V504EDB M76251-10 MADEP VPH REV 1.123-AUG-08 16:21 AF VMAVPH M7625�1�1��Co,,li M76251-11 SW846 8260B 19-AUG-08 06:58 EL V82600XY5 M76251-11 EPA 504 20-AUG-08 13:13 CZ 19-AUG-08 FG V504EDB M76251-11 MADEP VPH REV 1.123-AUG-08 17:02 AF VMAVPH M7�62`51��2��Collectedl4�A"t�G 08 10 40 By��W�� Received75�A�LIG,�18�B�i��S�Al� ��`� �` -� � Page 2 of 5 ®E1 86 of 111 12ACCU TEST M76251 '-`tsr't""-- y Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M76251 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes M76251-12 SW846 8260B 19-AUG-08 07:30 EL V8260OXY5 M76251-12 EPA 504 20-AUG-08 14:12 CZ 19-AUG-08 FG V504EDB M76251-12 MADEP VPH REV 1.123-AUG-08 17:43 AF VMAVPH �1 ►�21 'Go eeted��U(��81AL;�L��B��k AW� � R ���'�t�8�By�S ►���' � � �� 1W��21� . � ,✓'✓�� , d.� � .���an<w„�,,,,� �.�a�c�r.�".$'��.�.:� ...� ���ky;,-r..���,,. „S s�,.2�_ ..� ,, M76251-13 SW846 8260B 19-AUG-08 08:01 EL V8260OXY5 M76251-13 EPA 504 20-AUG-08 14:42 CZ 19-AUG-08 FG V504EDB M76251-13 MADEP VPH REV 1.123-AUG-08 18:24 AF VMAVPH M76251-14 SW846 8260B 19-AUG-08 08:33 EL V8260OXY5 M76251-14 EPA 504 20-AUG-08 15:12 CZ 19-AUG-08 FG V504EDB M76251-14 MADEP VPH REV 1.123-AUG-08 19:06 AF VMAVPH M76251-1A SW846 6010B 22-AUG-08 12:04 PY 21-AUG-08 PY PB `�6`t6l 2A�o 1�c�d��A e�� 08'�3# �����,��e��� L = �8 �,�y�S'�' � °�✓ �����- ��,.�.�'`��" �.�y��:��� ��,?✓-"- ..... ��ex.<,w«, �.,.�r..v�-,�-rkz�:,:z, .cam,'a n,. .. ..,,;:�,,...��Sy�;k;�.��' M76251-2A SW846 6010B 22-AUG-08 12:08 PY 21-AUG-08 PY PB M76251-3A SW846 6010B 22-AUG-08 12:12 PY 21-AUG-08 PY PB Y .� a+, -r �',z, =`r�, Y r a E '�,�T kr �'""Ls ✓. 2 x ,nr°�*° r �,. c 7625�1� ��'olle�t�d �1 k,iJG 1)8 Lt)�1�$ ��11W Recetsds L#5�Ai008 B���SAP x �� � a � x M76251-4A SW846 6010B 22-AUG-08 12:25 PY 21-AUG-08 PY PB Page 3of5 IM® 87 of I I I 12ACCLl7EST. M76251 '-_cor Accutest Laboratories Internal Sample Tracking ChroniclePlb Shell Oil Job No: M76251 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes N 21 M76251-5A SW846 6010B 22-AUG-08 12:30 PY 21-AUG-08 PY PB M76256 allected h14 AUGEl8�I2 1Q By SAWR£ecevedl§r3A� DBySAP M76251-6A SW846 6010B 22-AUG-08 12:34 PY 21-AUG-08 PY PB M76251-7A SW846 6010B 22-AUG-08 12:39 PY 21-AUG-08 PY PB M7�6�51�SAkCollected�14 A�JG�08 1�2�15�sBy SAW ,��Rece�v�ed�'bAUSG 08 By��SAP '`�� � � � � ,� M76251-8A SW846 6010B 22-AUG-08 12:43 PY 21-AUG-08 PY PB M7C251=9AColieed14AifGDB 11 3DaARCe 1�51U�0$ $y SA�, M76251-9A SW846 6010B 22-AUG-08 12:48 PY 21-AUG-08 PY PB .,d.>�v+rvvsvvs.�$e'r� 3a�z,✓: t��i.,,.�._m .... F .�,.,,.��,�, �x s. ... t_ a..-,� �° t :,zx M76251-10ASW846 6010B 22-AUG-08 11:11 PY 21-AUG-08 PY PB Mf76251� Y M76251-11PSW846 6010B 22-AUG-08 11:46 PY 21-AUG-08 PY PB M76251-12ASW846 6010B 22-AUG-08 11:50 PY 21-AUG-08 PY PB Page 4of5 �® 88 of 111 UACCUMST. M76251 Leto �t,17e'- Accutest Laboratories Internal Sample Tracking Chronicle A Shell Oil Job No: M76251 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes W625=1 M76251-13PSW846 6010B 22-AUG-08 11:55 PY 21-AUG-08 PY PB 1�6251�14��Go11ec#ed1�4��A�1�G�0 �1Y1 14B� W����Receiucf��k5 At1G08��By�S�iP � �� M76251-14ASW846 6010B 22-AUG-08 11:59 PY 21-AUG-08 PY PB Page 5 of 5 �® 89 of I I I M76251 L_t-.''t it, ®® New England A - - rr - - Section 5 GC4MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ®M 90 of 111 11ACCUTEST M76251 tetorator:=c r Method Blank Summary Page I of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3395-MB G84087.1) 1 08/19/08 EL n/a n/a MSG3395 cn The QC reported here applies to the following samples: Method: SW846 8260B P PP g M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, M76251-11, M76251-12, M76251-13, M76251-14 CAS No. Compound Result RL Units Q ......... . .... ... 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol N-D 20 ug/l 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/l CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 99%_ 79-130% 2037-26-5 Toluene-D8 96% 80-120% 460-00-4 4-Bromofluorobenzene 93%' 80-120% I �© 91 of 111 MACCUT .. M76251 -tt !r z c' _: Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3395-BS G84084.1) 1 08/18/08 EL n/a n/a MSG3395 MSG3395-BSD G84085.1) 1 08/18/08 EL n/a n/a MSG3395 N The QC reported here applies to the following samples: Method: SW846 8260B PP g M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, M76251-11, M76251-12, M76251-13, M76251-14 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/1 % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 51.0 "102 51.3 103 1 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 47.4 95 47.8 96 1 70 130/25 994-05 8 tert Amyl Methyl Ether 50 51.2 102 51.2 102 0 51-138/25 75-65-0 Tert Butyl Alcohol 500 493 99 503 2 60 146/25 637-92-3 tert-Butyl Ethyl Ether 50 52.8 106 53.3 107 : 1 46 147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 99% 1M%o- 79-130% 2037-26-5 Toluene-D8 98% 97%' 80-120% 460-00-4 4-Bromofluorobenzene 92% 939/6 80-120% ®® 92 of 111 QACCUTEST: M76251 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M76251-5MS G84093.1) 5 08/19/08 EL n/a n/a MSG3395 M76251-5MSD G84094.1) 5 08/19/08 EL n/a n/a MSG3395 N M76251-5 G84092.1) 1 08/19/08 EL n/a n/a MSG3395 w The QC reported here applies to the following samples: Method: SW846 8260B M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, M76251-11, M76251-12, M76251-13, M76251-14 M76251-5 Spike MS MS MSD MSD Limits CAS No. Compound ug/l Q ug/l ug/l % ug/l % RPD Rec/RPD 108-20-3 Di-Isopropyl ether ND 250 259 104 '` 257 103 1 54 155/30 1634-04-4 Methyl Tert Butyl Ether ND 250 239 96 237 95 1 54-144/30 994-05-8 tert-Amyl Methyl Ether ND 250 246 98 249 100 1 47 142/30 75-65-0 Tert Butyl Alcohol ND 2500 2410 96 2410 ;96.. 0 60-148/30 637-92-3 tert-Butyl Ethyl Ether ND 250 261 104 " 260 104 0 46-151/30 CAS No. Surrogate Recoveries. MS MSD M76251-5 Limits 1868-53-7 Dibromofluoromethane 1:011% 10.0% 100W 79-130% 2037-26-5 Toluene-D8 95% 96%0 95%a 80-120% 460-00-4 4-Bromofluorobenzene 90% 93% 93% 80-120% ®� 93 of 111 12A T.TEB ` Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: SW846 8260B Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 S2 S3 M76251-1 G84088.1) 1'Ofl fl 97.0 92:0 M76251-2 G84089.1) I00 0 "' 91.0 91,0 M76251-3 G84090.1) 10(10 97.0 91,E M76251-4 G84091.1) 97.0 91 M76251-5 G84092.1) 1fl0 0 95.0 93 0 M76251-6 G84095.1) 99 0 9 7.0 920 M76251-7 G84096.1) 102 fl 98.0 92 0 M76251-8 G84097.1) lOf 0 =98.0. 94'0 M76251-9 G84098.1) 1t 1 fl 96.0 91 0 M76251-10 G84099.1) 101 0 97.0 93� M76251-11 G84100.1) 100 0 95.0 91 9 M76251-12 G84101.1) 100 0 98.0 90<0 M76251-13 G84102.1) 100,0 95.0 90.0 M76251-14 G84103.1) I04 0 96.0 89.:11 M76251-5MS G84093.1) 101?0 95.0 90.Q M76251-5MSD G84094.1) I°00.0 .';:96.0 93;0 MSG3395-BS G84084.1) 98.0 98.0 92;0 MSG3395-BSD G84085.1) 100 0 ' 97.0 93 0 MSG3395-MB G84087.1) 99.0 '. 96.0 Surrogate Recovery Compounds Limits S1 = Dibromofluoromethane 7.9..13fl°/ti S2 = Toluene-D8 $0 12fl% S3 = 4-Bromofluorobenzene 80:1,Zfl%.. ®� 94 of I l l 12ACCLrrEST M76251 LA toffs sic: �® New England U b o f i e Section 6 _. ___-_.._ _ _. _ _.__.___.-__.____•v ___-__ sf 3T 5 RLiN .1#6 CkMT5113K G.0 Volatles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries 95 of I l l 12ACCUTEEST. M76251 -;c-"I Method Blank Summary Page I of 1 Job Number: M76251 Account: SHELLWIC'ShellOil Project: SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA Sample File ID DF Analyzed. By Prep Date Prep Batch Analytical Batch GBD985-MB BD20729.D 1 08/23/08 AF n/a n/a GBD985 rn The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, M76251-11, M76251-12, M76251-13, M76251-14 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene Nb 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene NDz, 2.0 ug/1 m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics:(Unadj.) NI)v 50 ug/I C9- C12 Aliphatics (Unadj ) ND 50 ug/1 C9- CIO Aromatics (Unadj.) ND. 50 ug/1 C5- C8 Aliphatics NO. 50 ug/1 C9- C12 Aliphatics ND': 50 ug/l CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluen2 80%;. 70-130% 615-59-8 2,5-Dibromotoluene 89% 70-130% ®® 96 of I I I QACCLffEST. M76251 i::t:o, :o- .., Method Blank Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16540-MB BB20724.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 m The QC reported here applies to the following samples: Method: EPA 504 M76251-1, M76251-2, M762:51-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-101 • M76251-11, M76251-12, M76251-13, M76251-14 CAS No. Compound Result RL Units P Q ..._..... . . .. . 106 93-4 1,2-Dibromoethane ND 0.015 ug/l CAS No. Surrogate Recoveries Limits 460-00-4 Bromofluorobenzene (S) 121%0 26-158% 460-00-4 Bromofluorobenzene (S) 1:20%. 26-158% 97 of III M76251 Lab0r�Z,^-- 4 � Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD985-BSP BD20730.D 1 08/23/08 AF n/a n/a GBD985 GBD985-BSD BD20731.1) 1 08/23/08 AF n/a n/a GBD985 rn The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, • M76251-11, M76251-12, M76251-13, M76251-14 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/1 % RPD Rec/RPD 71-43-2 Benzene 50 53.7 107 54.0 108 1 70-130/25 100-41-4 Ethylbenzene 50 54.6 109 54.8 110 0 70 130/25 1634-04-4 Methyl Tert Butyl Ether 50 53.0 1,06 52.8 1s©6 0 70-130/25 91-20-3 Naphthalene 50 47.3 95s 48.5 J7 3 . !, 70-130/25 108-88-3 Toluene 50 54.4 109 54.7 109;': 1 70-130/25 m,p-Xylene 100 109 109 109 1.09 0 70 130/25 95-47-6 o-Xylene 50 51.0 102 51.2 102': 0.`:.. 70130/25 C5- C8 Aliphatics (Unadj.) 150 146 97 144 9.6 1 70-130/25 C9- C12 Aliphatics (Unadj.) 150 144 96 142 95 1 70-130/25 C9- CIO Aromatics (Unadj.) 50 51.3 103 51.0 102 1 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 79% . 81°/0 70-130% 615-59-8 2,5-Dibromotoluene 88% . 89% 70-130% 98 of 111 QACCUTEST. M76251 L-t c: z—,es Blank Spike Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16540-BS BB20725.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 rn The QC reported here applies to the following samples: Method: EPA 504 w M76251-1, M76251-2, M762S1-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, • M76251-11, M76251-12, M76251-13, M76251-14 Spike BSP BSP CAS No. Compound ug/l ug/l % Limits ._....._....... . 106-93-4 1,2-Dibromoethane 0.071 0.072 101 70-130 CAS No. Surrogate Recoveries BSP Limits 460-00-4 Bromofluorobenzene (S) 125% 26-158% 460-00-4 Bromofluorobenzene (S) 1220/o 26-158% I 99 of 111 12ACCUTEST. M76251 I eLe-s:'—a. ♦ V Matrix Spike/Matrix Spike Duplicate Summary Page I of I Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16540-MS BB20726.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 OP16540-MSD BB20727.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 M76326-3 BB20728.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 rn The QC reported here applies to the following samples: Method: EPA 504 a M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, • M76251-11, M76251-12, M76251-13, M76251-14 M76326-3 Spike MS MS MSD MSD Limits CAS No. Compound ug/l Q ug/l ug/l % ug/l % RPD Rec/RPD 106-93-4 1,2-Dibromoethane ND 0.071 0.070 99 0.065 92 7 65-135/30 _ . CAS No. Surrogate Recoveries MS MSD M76326-3 Limits 460-00-4 Bromofluorobenzene (S) 123% 106% 10500. 26-158% 460-00-4 Bromofluorobenzene (S) 122%0 1066W 108% 26-158% 100 of 111 ®ACC UTEST. M76251 --trr:--i"= i Volatile Surrogate Recovery Summary Page 1 of 1 .Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b in M76251-1 BD20732.D S1. 90.0 M76251-2 BD20733.D 79 0 88.0 M76251-3 BD20734.D ,819 90.0 M76251-4 BD20735.D 83 0 91.0 M76251-5 BD20736.D 80 0 89.0 M76251-6 BD20737.D <82 0 91.0 M76251-7 BD20738.D 77.0..:_'.; 85.0 M76251-8 BD20739.D 80 0 90.0 M76251-9 BD20740.D 82 0 91.0 M76251-10 BD20741.D 82 A 91.0 M76251-11 BD20742.D 82:0. 91.0 M76251-12 BD20743.D 83:0 91.0 M76251-13 BD20744.D 7RAW 89.0 M76251-14 BD20745.E, 81.4 89.0 GBD985-BSD BD20731.G 810 89.0 GBD985-BSP BD20730.G 79:0 88.0 GBD985-MB BD20729.D 80 0 89.0 Surrogate Recovery Compounds Limits S1 = 2,5-Dibromotoluene 70-130% (a) Recovery from GC signal#1 (b) Recovery from GC signal 4f2 101 of 111 NAMES'. M76251 =a LO!�tu,l es f � C Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: EPA 504 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b it M76251 1 BB20729.D 92 0 75.0 M76251-2 BB20731.D 96 0 86.0 M76251-3 BB20732.D 11.2.0 103.0 M76251-4 BB20733.D 104 0 91.0 M76251-5 BB20734.D U 0 90.0 M76251-6 BB20735.D 1-06 0 89.0 M76251-7 BB20736.D -1t}3 0 84.0 M76251-8 BB20737.D 104 0 r.>"84.0 M76251-9 BB20738.D 97 0 77.0 M76251-10 BB20739.D '110 88.0 M76251-11 BB20740.D 1#4:0 89.0 M76251-12 BB20742.D 103 0 88.0 M76251-13 BB20743.D 944 62.0 M76251-14 BB20744.D 9.9:.0,::.-: 77.0 OP16540-BS BB20725.D 125._:0:- 122.0 OP16540-MB BB20724.D 121.0 _ 120.0 OP16540-MS BB20726.D 123.0 122.0 OP16540-MSD BB20727.D 106.0 106.0 Surrogate Recovery Compounds Limits S1 = Bromofluorobenzene (S) 26 158%. (a) Recovery from GC signal#11 (b) Recovery from GC signal#2 102 of 111 ®ACCUTEST M76251 --t o rno 6 e. New England __ ra Section 7 Meg als Analysis QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Matrix Spike and Duplicate Summaries • Blank Spike and Lab Control Sample Summaries • Serial Dilution Summaries ®® 103 of 111 JOACCUTEST. M76251 -to-':o-ie- " 4 BLANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/1 Prep Date: 98/21/08 08/21/-08 MB MB Metal RL IDL raw final raw final . .............. Aluminum 200 18 Antimony 6.0 1.2 Arsenic 10 .83 am V Barium 200 3.7 am Beryllium 4.0 .15 Boron 100 .22 Cadmium 4.0 .15 am Calcium 5000 6.3 Chromium 10 .4 am Cobalt 50 .12 Copper 25 1.7 am Gold 50 .91 Iron 100 4.8 Lead 5.0 2 0.30 <5.0 1.1 <5.0 Magnesium 5000 34 Manganese 15 .36 ._ Molybdenum 100 .28 Nickel 40 .15 am Palladium 50 2 Potassium 5000 48 Selenium 10 1.7 am Silicon 100 5.2 Silver 5.0 53 am Sodium 5000 24 Strontium 10 .18 Thallium 10 .82 Tin 100 .35 Titanium 50 .65 Tungsten 100 5.3 Vanadium 30 .44 Zinc 20 .22 am Associated samples MP12365: M76251-1A, M76251-2A, M76251-3A, M76251-4A, M76251-5A, M76251-6A, M76251-7A, M76251-8A, M76251-9A, M76251-10A, M76251-11A, M76251-12A, M76251-13A, M76251-14A Results < IDL are shown as zero for calculation purposes Page 1 im ®E] 104 of 111 ®ACCITEST. M76251 =_Gcr ito- c: N BLANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 601OB Matrix Type: AQUEOUS Units: ug/1 Prep Date: Metal (') Outside of QC limits (anr) Analyte not requested y :A Page 2 ®� 105 0f 111 QACCUTEST M76251 -=r= • r i MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: M16251 Account: SHELLWIC - Shell Oil Project: SCMAW:97951986 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6O1OB Matrix Type: AQUEOUS Units: ug/1 Prep Date: OS%21/O;8 08/.2:1/`08 M76251-10A Spikelot QC M76251-10A QC Metal Original MS MPICP % Rec Limits Original DUP RPD Limits Aluminum Antimony ,..: Arsenic am V Barium am Beryllium ty Boron r, r Cadmium am r Calcium Chromium am Cobalt Copper am Gold Iron Lead 4.5 989 1000 98.5 75-125 4.5 5.0 10.5 0-20 Magnesium Manganese Molybdenum Nickel am Palladium Potassium Selenium am Silicon Silver am Sodium Strontium Thallium Tin Titanium Tungsten Vanadium Zinc am Associated samples MP12365: M76251-1A, M76251-2A, M76251-3A, M76251-4A, M76251-5A, M76251-6A, M76251-7A, M76251-8A, M76251-9A, M76251-10A, M76251-11A, M76251-12A, M76251-13A, M76251-14A Results < IDL are shown as zero for calculation purposes Page 1 ®21 1060111 0ACCUrEST. M76251 -=6orn;orl-- MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6010B Matrix Type: AQUEOUS - Units: ug/l Prep Date: Metal (*) Outside of QC limits (N) Matrix Spike Rec. outside of QC limits (anr) Analyte not requested v N Page 2 ®® 107 of 111 QACCUTEST M76251 i SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/l Prep Date: 0812JJDQ8 08/21/08 BSP Spikelot QC BSD Spikelot BSD QC Metal Result MPIC'P % Rec Limits Result MPICP % Rec RPD Limit Aluminum Antimony Arsenic am y Barium am a W Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper am Gold Iron - Lead 974 1000 97A 80-120 999 1000 99.9 2-5 20 Magnesium Manganese Molybdenum Nickel am Palladium Potassium Selenium am Silicon Silver am Sodium Strontium Thallium Tin Titanium Tungsten Vanadium Zinc am Associated samples MP12365: M7E251-1A, M76251-2A, M76251-3A, M76251-4A, M76251-5A, M76251-6A, M76251-7A, M76251-8A, M76251-9A, M76251-1CA, M76251-11A, M76251-12A, M76251-13A, M76251-14A Results < IDL are shown as zero for calculation purposes Page 1 ®® 108 of 111 ®ACCUTEST. M76251 t SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Projec_: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 601OB Matrix Type: AQUEOUS Units: ug/1 Prep Date: Metal (*) Outside of QC limits (anr) Analyte not requested V W Q Page 2 �® 109 Of 111 12ACCUTEST. M76251 SERIAL DILUTION RESULTS SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SC14AW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/l Prep Date: 0,8/21/08 M76251-10A QC Metal Original SDL 1:5 RPD Limits . .. ._.. Aluminum Antimony Arsenic am V Barium am A Beryllium y Boron ®. i Cadmium am Calcium Chromium am Cobalt Copper am Gold Iron Lead 4.50 0.00 100.0(a) 0-10 Magnesium Manganese Molybdenum Nickel am Palladium Potassium Selenium am Silicon Silver am Sodium Strontium Thallium Tin Titanium Tungsten Vanadium Zinc am Associated samples MP12365: M76251-1A, M76251-2A, M76251-3A, M76251-4A, M76251-5A, M76251-6A, M76251-7A, M76251-8A, M76251-9A, M76251-10A, M76251-11A, M76251-12A, M76251-13A, M76251-14A Results < IDL are shoran as zero for calculation purposes Page 1 ®TJ 110 of 111 QACC UTEST. M76251 t_bcrat—ie> SERIAL DILUTION RESULTS SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/l Prep Date: Metal (') Outside of QC limits (anr) Analyte not requested (a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL). A Page 2 III of III gACCUTEST. M76251 L=t=-vr t- SOVEREIGN CONSULTING t October 8,2008 p D14L#29277962556 Ms. Donna Miorandi QJ Town of Barnstable,Health Inspector � 200 Main Street Hyannis, MA 02601 Re: Groundwater Sampling Results,September 2008 r C T Former Shell Branded Gasoline St t on#137772 b .;4, 590 Iyannough Road .., Hyannis,MA Dear Ms: Miorandi: Pursuant to your authorization Sovereign Consulting-Inc. personnel collected a groundwater sample from a monitoring well installed at the above referenced/property. The sample was submitted for laboratory analysis of dissolved lead.`�A copy4f the laboratory analytical is attached. ; As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVEREIGN CONSULTING,INC. Sylvia M. Kirsch Project Managerr,,P.,, r Attachments: {` Laboraf dryOata Reports cc: with attachment '1] " Mr. David Weeks,Motiva MassDEP-,SERO U SovereignjFile-EQ872 I` of v 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 Il NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan BWSC 123 r+� , This Notice is Related to , Release Tracking Number "^� 4 17651 � y A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): Roadannou h 1. Street Address: 590 I Y 9 ,., City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Health Inspec. Donna Miorandi 4 1 2. Street Address: 200 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ✓❑ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. Q✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. FV 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 590 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ✓❑ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ✓❑commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater) to the extent known at the time of this notice. Groundwater from monitoring well E. Contact information related to the party providing this notice: Contact Name: Sylvia Kirsch Street Address: 905B South Main Street, Suite 202 City/Town. Mansfield Zip Code: 02048 Telephone: (508) 339-3200 Email: skirsch@sovcon.com r t NOTICE OF/ENVIRONMENTAL SAMPLING As requirfed by 310 CMR�40.1403(,10) of the Massachusetts Contingency Plan f" Ik MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. /) THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the'area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. V-nurucupy Z.v Automated Report New England 4 ......... ........_. _...._. ......._. ... :' ._ ..... .._ .r y.. _.._.. ;_ t r= a L L. ;s r rr e rs. r�`t ;tt r , _ 09/23/08 r � . _ Technical Report for Shell Oil SCMAW:97451486 (REIMBMA) 590 IyannoughRoad Hyannis MA r EQ 872 Accutest Job Number: M77010 ~; Sampling Date: 09/12/08 Report to: Sovereign Consulting skirsch@sovcon.com ATTN: Sylvia Kirsch Total number of pages in report: 23 D�N acca40 14-1 u p Test results contained within this data package meet the requirements Zeza and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) kYE 977j NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE I �° t This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England • 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • http://www.accutest.com 1 of 23 A UTEST. I Sections: � f { Table of Contents ! -1- Section1: Sample Summary- ............................................................................................... 3 Section 2: Case Narrative/Conformance Summary .............................................................. 4 Section3: Sample Results ........................................................................................................ 5 1 3.1: M77010-1: GT-5 ........................................ .........................!'" ......................................................................... 6 Section4: Misc. Forms :.............. ........ 7:............... 5............................................................. 4.1: Chain of Custody ............... ... ....................................................................... 8 4.2: MCP Form ! ...................................................................... 13 4.3: Sample Tracking Chronicle ........................................................................................... 14 ti Section 5: Metals Analysis - QC Data Summaries ................................................................ 15 5.1: Prep QC MP 12467: Pb ... ............................................................................................. 16 � 1 { 2of23 GACCUT............................_......_ T. _......... M77010 ¢s I Accutest Laboratories Sample Summary Shell Oil Job No: M77010 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA,, Project No: EQ 872 t Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M77010-1 09/12/08 13:30 AC 09/12/08 AQ Groundwater Filtered GT-S 3 of 23 IZACCUTEST. M77010 .. ...., a e o ..•: �r MF EN f L i b o r-,,i h c) r i e s i SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M77010 Site: SCMAW:97451486(REIMBMA)590 lyannough Road Hyannis MA Report Date 9/23/2008 3:08:48 PM r � 1 Sample was collected on 09/12/2008 andtw ere received at Accutest on 09/12/2008 properly preserved,at 2.1 Deg.C and intact. These Samples received an Accutest job number of M77;010.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Metals By Method SW846 6010B Matrix AQ Batch ID: MP12467 M All samples were digested within the recommended method holding time. IP All samples were analyzed within the recommended method holding time. 0 All method blanks for this batch meet method specific criteria. 0 Sample(s) M77026-8AMS,M77026-8ASDL,M77026-8ADUP were used as the QC samples for metals. M RPD(s)for Duplicate for Lead are outsidecontrol limits for sample MP12467-DI. RPD acceptable due to low duplicate and sample concentrations. RPD(s)for Serial Dilution for Lead are outside control limits for sample MP 12467-SDI. Percent difference acceptable due to low initial sample concentration(<50 times IDL). Only Lead requested. The Accutest Laboratories of New England certifies that all analysis were performed within method specification. It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M77010). Tuesday,September 23,2008 Page 1 of 1 Q 4 of 23 12ACCUTEST. M77010 ......., New England Section 3 __ _.. . ... ..... Sample Results Report of Analysis . 5of23 CIACCUTEST. M77010 Accutest Laboratories s� Report of Analysis Page I of I Client Sample ID: GT-5 Lab Sample ID: M770101-1 Date Sampled: 09/12/08 Matrix: AQ - Groundwater Filtered Date Received: 09/12/08 Percent Solids: n/a Project: SCMAW:97451486(REIMBMA) 590 lyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead < 'S 0 5.0 ug/1 1 09/16/08 09/16/08 PY SW846 6010B I SW846 3010A 2 (1)Instrument QC Batch: MA9692 (2)Prep QC Batch: MP 12467 5 RL= Reporting Limit 6 of 23 ll__ .:. .. ....................... M77010 New England Section 4 `Y ...__...... ............ t.. ... -s R L,L I N t HE . C.r€E ns.._1 5 1 R,�... Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • Sample Tracking Chronicle . 7of23 _- M77010 ........a t o LAB(LOCATION) 4 Shell Oil Products Chain Of Custody Record 77&6 Please Check Appropriate Boa: Print Bill To Contact Name: INCIDENT 11(ENV SERVICES) CHECK IF NO I CIDEM a ARPLIES ❑ENV.SERVICES I ❑MUnVA RETAIL ❑SHELL RETAIL Q ACCLTEST 9 1 4 5 8 6 DATE: t ❑nonva spec pcoNsuuaxr Owecs PO k SAP p 1 _ - PAGE. ❑OTHER .xRr r.curun SnE aooaess lsr�N,cxy end surel: Sovereign Consulting amss t 5901 annou h Road Hyannis.MA 905 B South Main Street Manslleld,MA 02048 LAe usp oNtr T 508.339-3200 508339.3248 skirscma�sovcon.com w }� ,( G r G(� U ARW ND TIME(CALEfIDAR D O'STANDARD(19 DAY) ❑5 DAoars 01Dars ❑zDAYS ❑za Houns REQUESTED ANALYSIS DELIVERABLES-. 21 MMMA ❑COMnB El WF ❑RC. I]OTHER(S-rY) TEMPS ATVREON RECEIPT C" ('rMl6l b1 ;0WW.2 CJplel a3 Please havD lab toter SPECIAL INSTRUCTIONS OR NOTES: Sample prior to analysis PLEASE FILTER DISSOLVED LEAD SAMPLLS IN LAB PRIOR TO ANALYSIS. v N '7 7,710 J d SAMPLING > L'a Field Sample Identification ATE MATRI% ��Rr w Container PID Readings usa U TIME N or Laboratory Note, oNtr O GT-s /AW 1.10 60 X uirq Obr ls rlW.l .uc�N Iry iseaercl Time: 9e-lam-a e )747 RaAnP+�Mu oy.IBynelurs) R...Ey;l6ienaw.I Del.: e. M77010: Chain of Custody Page i of 5 8 of 23 gJACCUTEST. MT7010 ........I a t I COMMONWEALTH OF MASSACHUSETFS DEPARTMENT OF ENVIRONMENTAL PROTECTION Certified Parameter List as of. 01 SUL 2008 M-:MA136 ACCUTEST LABORATORIES OF NEW ENGLAND MARLBOROUGH MA NON POTABLE WATER(CHEMISTRY) Effective 01 JUL 2008 Expiration 30 JUN 2009 Date Date Anal es MetLods ALUMINUM EPA 200.7 ANTIMONY EPA 200.7 ARSENIC EPA 200.7 BERYLLIUM EPA 200.7 CADMIUM EPA 200.7 CHROMIUM EPA 200.7 COBALT EPA 20D.7 COPPER EPA 200.7 FRON EPA 200.7 LEAD EPA NHl 7 MANGANISE EPA 200.7 MERCURY EPA 245.1 MOLYBDENUM _ EPA 200.7 NICKEL EPA 200.7 SBEINI M EPA 200.7 SILVER EPA 200.7 STRONTIUM EPA 200.7 THALLIUM EPA 200.7 VANADIUM O'A 200.7 Z M EPA 200.7 PH SM 4500-H-B SPECIFIC CONDUCTIJ ITY EPA 120.1 . TOTAL DISSOLVED SOLIDS SM 2540C HARDNESS(CA CO3).TOTAL SM 2340B HARDNESS(CACO3),TOTAL SM 2340C• CALCIUM EPA 200J MAGNESIUM EPA 200.7 SODIUM - EA 200.7 POTASSIUM EPA 200.7 ALKALNIUY,TOTAL _ SM 23208 CHLORINE SM 4500-CL-C FLUORIDE SM450D-F-B,C SULFATE ASTMD616 J SVAB-B.C-NM O AMMONIA-N NITRATE-N EPA 353.2 O KJELDAHL-N EPA 351.2 [� ORTHOPHOSPHATE EPA 365.3. .7 ORTHOPU-IOSPHATE SM 4500-RE �. PHOSPHORUS,TOTAL -EPA 365.4 . CHE]MI AL OXYGEN DEMAND SM 5220C 4 BIOCHEMICAL OXYGEN DEMAND SM5210B oft 3 TOTAL ORGANIC CARBON SM 5310E 0 CYANCE TOTAL EPA 335.4 O O June 25,2008 "=Provisional Certification Page 1 of 3 �-h �O O COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Certified Parameter List as of- 01 JUL 2008 M-MA136 ACCUTEST LABORATORIES OF NEW ENGLAND MARLBOROUGH MA NON POTABLE WATER(CHEMISTRY) Effective Ol JUL 2008 Expiration 30 JUN 2009 Date Date Analytes Methods 1 NON-FLTERABLERESDUE SM 2540D' CHLORIDE,TOTAL RESOLIAL SM 45DO-CL-F OIL AND GREASE EPA 1664 FFrNOLI S,TOTAL EPA 420.1 . VOLATILE.HALOCARSONS EFA 624 VOLATILE AROMATICS EPA 602 VOLATILEAROMATCS EPA 624 CHLORDANE EPA 608 . ALDRIV EPA 608 DIELDRIN EPA 608 DDD - EPA 608 DOE - EPA 608 . DOT EPA.608 HEPTACHLOR EPA 608 HEPTACHLOR EPDXIDE - EPA 608 POLYCFLORNATID BIPHFNYLS(WATER) EPA 608 POLYCHLORNATED BIFFIEW LS(OL) EPA 60014-BI-045 POTABLE RATER(CME1%USTRY) Effective Ol JUL 2008 Expiration 30 JUN 2009 Date Date Anal Methods BARIUM EPA 200.7 _ BERYLLLId EPA 200.7 CADMIUM EPA 200.7 CHROMIUM EPA 200.7 COFFER. EPA 200.7 WERC1RY _ EPA 245.1 NICKEL EPA 200.7 NITRATE N EPA 3532 Nr RITE-N - EPA 3512 FLUOROE SM 450aF-C SODIUM EPA 200.7 J SULFATE "SM-0500-SO4•C CYAMF,TOTAL _ EPA 335.4 Q Ti R60ffY ERA 180,1 ^� CFLORNF-RESmUAL FREE SM 4500.CL-F ` 1 CALCIUM EPA 200.7 � ALKALINITY,TOTAL SM 2320E TOTAL MSOLVEDSOLIDS SM2540C b C PH EPA 150.1 PH►rtp SM4500-KB 3 (1Q 24_D EPA 515.1 o �p c W 2,4,5-TP EPA 515.1 O O June 25,2008 *=Provisional Certification Page 2 of 3 CD COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Certified Parameter List as of: 01 JUL 2008 M-MAIM ACCUTEST LABORATORIES OF NEW ENGLAND MARLBOROUGH MA POTABLE WATER(CHEMISTRY) Effective 01 JUL 2008 Expiration 30 JUN 2009 Date Date Analytes '.Methods TRpIALOMETHANS EPA 524-2 VOLATLE ORGANIC ooLmUNDS S3 A 524.2 1,2•DBROWETHANE EFA 504.1 ' 1.2-DBROMO.3-CHLOROFROPANE EPA 504.1 a J J O O n b C o � p' June 25,2008 `=Provisional Certification Page 3 of. 3 0 COMMONWEALTH OF MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Certified Parameter List as of: 01 JUL 2008 Ai-MA136 ACCUTEST LABORATORIES OF NEW ENGLAND MARLBOROUGH MA POTABLE WATER(MICROBIOLOGY) Effective 01 JUL 2008 Expiration 30 JUN 2009 Date Date Anal es Methods TOTAL COLIFORM WATER TREATMENT AND DkSTR13Ur10N(A'A) ENZ.SUB.SM223 E COLI WATER TREATMENT AND DisTRIBunoN(m) EM.SUB.SM9223 J J O O n O A� O F'C O 3 > � n 0 f° c O O June 25,2008 '=Provisional Certification Page 1 of 1 -0 Wr Massachusetts Department BWSC-CAM Exhibit VI I A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 Title: MADEP MCP Response Action Analytical Report Certification Form M & V P,' NT= -M 4 If rMWORIV INERIU,E-HIVIA L-I A,n a lyt-Jea falyrelff6OReport tue rRITI cau p n, 6--W ,O Laboratory Name: Accutest Laboratories of New England Project#: M7701 0 Project Location: SCMAW:97451486(REIMBMA)590 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M7701 0-1 Sample Matrices: Groundwater X Soil/Sediment Drinking Water Other: 'S 82606 8151A 8330 60106 (X) 7470A/1 A 8270C 8081 A VPH 6020 9014M 2 spec}fredrnMADEF' 8082 d 8021 B EPH 7000S 3 7196A leasi A An affirmative response to questions A,13,C, and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with L'I Yes El No that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and Yes ❑ No discuss in a narrative QC data that did not meet appropriate performance ,standards or guidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty",as described in Section 2.0(a),(b),(c)and 2 Yes [I No (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without FA Yes [I No significant modifications,as specified in Section 11.3? A response to questions E and F below is required for"Presumptive Certainty" status E Were all QC performance standards and recommendations for the FA Yes LJ No specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified El Yes Ld No method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned,attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is,to the best of my knowledge and belief,accurate and complete. Signature: � Position: Laboratory Director Printed Name: Reza Tand Date: 09/23/2008 I 13 of 23 13ACCUTEST M77010 Accutest Laboratories i Internal Sample Tracking Chronicle PI Shell Oil - Job No: M77010 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes � ~ M770 0 �;Collected 12 S�EF 081�3�30\By SAC � -�Reeerved 12�SEF-a8 � 5�� �`: .� M77010-1 SW846 6010B 16-SEP-08 15:42 PY 16-SEP-08 PY PB Page 1 of 1 14 of 23 rjA=__U i; New England w. Section 5 Metals Analysis QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Matrix Spike and Duplicate Summaries • Blank Spike and Lab Control Sample Summaries • Serial Dilution Summaries 15 of 23 UACCUTEST. M77010 l BLANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: M77010 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12467 Methods: SW846 6010E Matrix Type: AQUEOUS Units: ug/l Prep Date: ' 09/16/:O8 09/16168 U1 MB MB ..a Metal RL IDL raw final raw final ma Aluminum 200 18 Antimony 6.0 1.2 Arsenic 10 .83 Barium 200 3.7 Beryllium 4.0 .15 i Boron 100 .22 Cadmium 4.0 .15 am Calcium 5000 6.3 Chromium 10 .4 am Cobalt 50 .12 Copper 25 1.7 am Gold 50 .91 Iron 100 4.8 am Lead 5.0 2 0.50 <5.0 0.10 <5.0 Magnesium 5000 34 Manganese 15 .36 Molybdenum 100 .28 Nickel 40 .15 am Palladium 50 2 Platinum 50 5.7 Potassium 5000 48 Selenium 10 1.7 Silicon 100 5.2 Silver 5.0 .53 am Sodium 5000 24 Strontium 10 .18 Thallium 10 .82 Tin 100 .35 Titanium 50 .65 Tungsten 100 5.3 Vanadium 30 .44 Zinc 20 .22 am Associated samples MP12467: M77010-1 Page 1 16 of 23 A U_......_ST M77010 BLANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: M77010 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12467 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/1 Prep Date: VI Metal Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (anr) Analyte not requested Page 2 17of23 GJACCUTEST. M77010 ,:,:o:;; o,;:,; MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: M77010 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: M212467 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/1 Prep Date: 09/16/08 09/16/081 M77026-8A Spikelot QC M77026-8A QC A Metal Original MS MPICP % Rec Limits Original DUP RPD Limits }V Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper am Gold Iron am Lead 6.8 1000 1000 99.3 75-125 6.8 8.9 26.8 (a): 0-20 Magnesium Manganese Molybdenum Nickel am Palladium Platinum Potassium Selenium - Silicon Silver am Sodium Strontium Thallium Tin ... Titanium Tungsten Vanadium Zinc am Associated samples MP12467: M77010-1 Page 1 18 of 23 GJAC.._._...._ _. ..__..... M77010 MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: M77010 Account: SHELLWIC - Shell Oil Project: SCNAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12467 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/i Prep Date: 0 .a, Metal hi Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (N) Matrix Spike Rec. outside of QC limits (anr) Analyte not requested (a) RPD acceptable due to low duplicate and sample concentrations. Page 2 19 of 23 ACLU M77010 9 SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: M77010 Account: SHELLWIC - Shell Oil Project: SCMAW:97451986 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12467 Methods: SW846 6010E Matrix Type: AQUEOUS Units: ug/1 Prep Date: 09/16/08 09/16/08 L)t BSP Spikelot QC BSD Spikelot BSD QC Metal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit Aluminum Antimony Arsenic Barium Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper am Gold Iron am Lead 995 1000 99.5 80-120 1010 1000 101.0 1.5 20 Magnesium Manganese Molybdenum Nickel am Palladium - - Platinum Potassium Selenium Silicon Silver am Sodium Strontium Thallium Tin Titanium Tungsten Vanadium Zinc am Associated samples MP12467: M77010-1 Page 1 20 of 23 rJACCU . ..., M77010 SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: M77010 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12467 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/l Prep Date: L71 ..a Metal Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (anr) Analyte not requested Page 2 21 of 23 y_UACCUTEST. M77010 ;rc.. SERIAL DILUTION RESULTS SUMMARY Login Number: M77010 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12467 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/1 _..................__.... Prep Date: O'9/16A8 M77026-BA QC Metal Original SDL 1:5 RPD Limits Aluminum Antimony Arsenic Barium - -` Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper am Gold Iron am Lead 6.80 12.0 76.5 (a) 0-10 Magnesium Manganese Molybdenum Nickel am Palladium Platinum Potassium Selenium Silicon Silver am Sodium - Strontium Thallium Tin Titanium Tungsten Vanadium Zinc am . Associated samples MP12467: M77010-1 Page 1 gF= . 22 of 23 . M77010 > e � � s SERIAL DILUTION RESULTS SUMMARY Login Number: M77010 Account: SHELLWIC - Shell Oil Project: SC:•lAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12467 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/1 Prep Date: U7 .a Metal Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (anr) Analyte not requested (a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL). Page 2 23 of 23 MACCUTEST ]•tia t��7� A��� III t Or SOVEkEIGN CONSULTING INC . September 8,2008 DHL#28881876354 Ms. Donna Miorandi Town of Barnstable,Health Inspector 200 Main Street Hyannis,MA 02601 Re: Groundwater Sampling Results,August 2008 Former Shell Branded Gasoline Station#137772 590 Iyannough Road s. Hyannis,MA Dear Ms. Miorandi: Pursuant to your authorization Sovereign Consulting Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH), gasoline oxygenates, ethylene-dibromide (EDB), and dissolved lead. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, a SOVEREIGN CONSULTING,INC. Sylvia M. Kirsch a Project Manager Attachments: Laboratory Data Reports cc: with attachment t; Mr.David Weeks,Motiva MassDEP- SERO Sovereign File-EQ872 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan BWSC 123 L� This Notice is Related to Release Tracking Number ® 17651 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 590 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Health Inspec. Donna Miorandi 2. Street Address: 200 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked,the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 590 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Sylvia Kirsch Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: skirsch@sovcon.com i NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. C e-Hardcopy 2.0 t f Automated Report New England ' All UTEST. a _._: _. . �_. .._. � T t t r t, w 3 t ra �a t •r t# 09/03/08. Technical Report for Shell Oil tc� yr SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA EQ 872 Accutest Job Number: M76251 Sampling Date: 08/14/08 Report to: dcollins@sovcon.com ATTN: Diane Collins Total number of pages in report: 111 ��O`��Q�N accoRo4�c� ® • < Test results contained within this data package meet the requirements /,�a and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) Y E :A R S, NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England • 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 http://www.accutest.com IME2 1 of 111 12ACCUTEST. M76251 La t 0']t4f t 1 � Table of Contents Sections: Section1: Sample Summary .............................1.. . Section 2: Case Narrative/Conformance Summary .............................................................. 7 Section3: Sample Results ........................................................................................................ 9 3.1: M76251-1: GT-1 ........................................................................................................... 10 3.2: M76251-1A: GT-1 ........................................................................................................ 13 3.3: M76251-2: GT-3 ........................................................................................................... 14 3.4: M76251-2A: GT-3 ......................................................................................................... 17 3.5: M76251-3: GT-4 ........................................................................................................... 18 3.6: M76251-3A: GT-4 3.7: M76251-4: GT-5 ........................................................................................................... 22 3.8: M76251-4A: GT-5 ........................................................................................................ 25 3.9: M76251-5: GT-7 ........................................................................................................... 26 3.10: M76251-5A: GT-7 ...................................................................................................... 29 3.11: M76251-6: MW-101 ................................................................................................... 30 3.12: M76251-6A: MW-101 ............................... 33 ................................................................ 3.13: M76251-7: MW-102 3.14: M76251-7A: MW-102 ................................................................................................ 37 3.15: M76251-8: MT-l/MT-3 .............................................................................................. 38 3.16: M76251-8A: MT-1/MT-3 ........................................................................................... 41 3.17: M76251-9: MW-202 ................................................................................................... 42 3.18: M76251-9A: MW-202 ................................................................................................ 45 3.19: M76251-10: MW-202D .............................................................................................. 46 3.20: M76251-10A: MW-202D ........................................................................................... 49 3.21: M76251-11: MW-301D .............................................................................................. 50 3.22: M76251-11A: MW-301D ........................................................................................... 53 3.23: M76251-12: MW-301S .............................................................................................. 54 3.24: M76251-12A: MW-301 S ............................................................................................ 57 3.25: M76251-13: MW-302D .............................................................................................. 58 3.26: M76251-13A: MW-302D ........................................................................................... 61 3.27: M76251-1.4: MW-302S ............................................................................................... 62 3.28: M76251-14A: NM-302S ............................................................................................ 65 Section4: Misc. Forms ............................................................................................................ 66 4.1: Chain of Custody ........................................................................................................... 67 4.2: MCP Form ..................................................................................................................... 70 4.3: VPH Form ...................................................................................................................... 71 4.4: Sample Tracking Chronicle ........................................................................................... 85 Section 5: GUMS Volatiles- QC Data Summaries .............................................................. 90 5.1: Method Blank Summary ................................................................................................ 91 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 92 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 93 5.4: Surrogate Recovery Summaries ...................................................................................... 94 Section6: GC Volatiles - QC Data Summaries ..................................................................... 95 2 of 111 1JACCUTEST. M76251 -corn co l Table of Contents Sections: -2- 6.1: Method Blank Summary .......................... .................................................................... 96 6.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 98 6.3: Blank Spike Summary ................................................................................................... 99 6.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 100 6.5: Surrogate Recovery Summaries ..................................................................................... 101 Section 7: Metals Analysis- QC Data Summaries ................................................................ 103 7.1: Prep QC MP12365: Pb .................................................................................................. 104 ®� 3 of 111 UACZXJTEST M76251 -:torjt—io, t 3 Accutest Laboratories Sample Summary Shell Oil SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Job No: M76251 Project No: EQ 872 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M76251 1 , 08/14/08 09:50 AW 08/15/08 AQ Ground Water GT l M76251 lA 08/14/08 09:50 AW 08/15/08 AQ Groundwater Filtered <GT 1 K M7621 2 08/14/08 08:30 AW 08/15/08 AQ Ground Water GT 3 M7651 2A 08/14/08 08:30 AW 08/15/08 AQ Groundwater Filtered GT-3 M76251 3 08/14/08 09:15 AW 08/15/08 AQ Ground Water GT 4 ............_....._.......................... M76251 3A I 08/14/08 09:15 AW 08/15/08 AQ Groundwater Filtered M76251 4 08/14/08 10:15 AW 08/15/08 AQ Ground Water GT 5 M76251 4A 08/14/08 10:15 AW 08/15/08 AQ Groundwater Filtered GT 5 , M76251 5 08/14/08 09:30 AW 08/15/08 AQ Ground Water GT 7 M7ti251 5A '08/14/08 09:30 AW 08/15/08 AQ Groundwater Filtered `G-,T M76251-.6 08/14/08 12:10 AW 08/15/08 AQ Ground Water §MW 101 TAX. 08/14/08 12:10 AW 08/15/08 AQ Groundwater Filtered MW 101 .......................____.............. M76251 7 08/14/08 12:35 AW 08/15/08 AQ Ground Water MW 1.02 4 of 111 12ACCU TEST. M76251 LIt^ra t—it t 7 Accutest Laboratories Sample Summary (continued) Shell Oil SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Job No: M76251 Project No: EQ 872 SampleCbllected Matrix Client Number Date Time By Received Code Type Sample ID M7621 7A ;08/14/08 12:35 AW 08/15/08 AQ Groundwater Filtered MW 10Z M762518 08/14/08 12:15 AW 08/15/08 AQ Ground Water MT 1/NIT 3 M76251�8A 08/14/08 12:15 AW 08/15/08 AQ Groundwater Filtered MT-1/1VIT,3 M76251 9 08/14/08 11:30 AW 08/15/08 AQ Ground Water MW-262 M76251 9A 08/14/08 11:30 AW 08/15/08 AQ Groundwater Filtered MW 202 M76251 10 08/14/08 11:40 AW 08/15/08 AQ Ground Water MW 2021) M76251 l0A 08/14/08 11:40 AW 08/15/08 AQ Groundwater Filtered MW 202D M76251 11 08/14/OS 10:30 AW 08/15/08 AQ Ground Water MW 301D ................................................ M76251 IlAI 08/14/08 10:30 AW 08/15/08 AQ Groundwater Filtered MW-3p1D M76251 12 x 08/14/08 10:40 AW 08/15/08 AQ Ground Water MW 3015 M762:51 12Ai 08/14/08 10:40 AW 08/15/08 AQ Groundwater Filtered MW=3.01S M76251 _ 08/14/08 11:10 AW 08/15/08 AQ Ground Water IVIW-302D M76251 ON. 08/14/08 11:10 AW 08/15/08 AQ Groundwater Filtered M1N 302D ®� 5 of 111 QAC CUTEST. M76251 cat oraio-ie= t 7; Accutest Laboratories Sample Summary Shell Oil (continued) SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Job No: M76251 Project No: EQ 872 Sample `:Collected Matrix Client Number Date Time By Received Code Type Sample ID M76251 14 08/14/08 11:10 AW 08/15/08 AQ Ground Water ,MW 3025 M7,6251 14A 08/14/08 11:10 AW 08/15/08 AQ Groundwater Filtered MW 3025 �® 6ofIII ®ACCUTEST. M76251 ==Gort e= 0" L d b o r a t: O r i P_ s SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M76251 Site: SCMAW:97451486(REIMBMA)590 Iyannough Road Hyannis MA Report Date 8/28/2008 10:19:08 AM 14 Sample(s)were collected on 08/14/2008 and were received at Accutest on 08/15/2008 properly preserved,at 2 Deg.C and intact. These Samples received an Accutest job number of M76251.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified cahbrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GCMS By Method SW846 8260B Matrix AQ Batch ID: MSG3395 All samples were analyzed within the recommended method holding time. ® All method blanks for this batch meet method specific criteria. ® Sample(s) M76251-5MS,M76251-5MSD were used as the QC samples indicated. Only MTBE,DIPE,TAME,ETBE and TBA requested. Volatiles by GC By Method EPA 504 Matrix AQ Batch ID: OP16540 = All samples were extracted within the reconunended method holding time. e All samples were analyzed within the recommended method holding time. m All method blanks for this batch meet method specific criteria. v Sample(s) M76326-3MS,M76326-3MSD were used as the QC samples indicated. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GBD985 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Metals By Method SW846 6010B Matrix AQ Batch ID: MP12365 a All samples were digested within the recommended method holding time. a All samples were analyzed within the recommended method holding time. m All method blanks for this batch meet method specific criteria. 0 Sample(s) M76251-10ADUP,M76251-10AMS,M76251-10ASDL were used as the QC samples for metals. RPD(s)for Serial Dilution for Lead are outside control limits for sample MP 12365-SDI. Percent difference acceptable due to low initial sample concentration(<50 times IDL). is Only Lead requested. Note:Compounds whose QC limits are outside MCP criteria are designated by the lab as"Difficult".QC criteria for a"Difficult' compound may meet Accutest in-house generated QC criteria but exceed MCP criteria(compounds exceeding Accutest QC criteria are flagged on the QC summary).Refer to the QC summary pages. Thursday,August 28,2008 Page 1 of 2 (Mn 7 of 111 12ACCUTEST M76251 L=tsr 1,r­, � T The Accutest Laboratories of New England certifies that all analysis were performed witain method specification.It is further recommended that this report to be used in its enticety.The Accutest Laboratories of NE.Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M76251). � I Thursday,August 28,2008 Page 2 of 2 ®E2 8 of 111 12ACCUTES'T. M76251 Lator--- r T New England L b is f r.t()f i Section i Sample Results' Report of Analysis ®® 9 of 111 QACCUTEST. M76251 to Gar�tu Pic: � a Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: GT-1 Lab Sample ID: M76251-1 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84088.D 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634 04 4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/I 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100% 79-130% 2037-26-5 Toluene-D8 97% 80-120% 460-00-4 4-Bromofluorobenzene 92% 80120% I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound lull 10 of 111 gACCUTES T. M76251 9 1 ? Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: GT-1 Lab Sample ID: M76251-1 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20732.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND« 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene NO. 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/I C9- C10 Aromatizs (Unadj ) Ni 50 ug/1 C5- C8 Aliphatic: ND 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 90% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IMB 11 of 111 ®ACCUTEEM M76251 L=t 1; L Accutest Laboratories Report of Analysis Page 1 of 1 j Client Sample ID: GT-1 Lab Sample ID: M76251-1 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20729.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 35.3 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 92.% 26-158% 460-00-4 Bromofluorobenzene (S) 75% 26 158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 12 of 111 QACCJTEST: M76251 Lc t cra:orles r r Accutest Laboratories Report of Analysis Page 1 of 1 N Client Sample ID: GT-1 Lab Sample ID: M76251-1A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead ug/1 1 08/21/08 08/22/08 Pr swags 6010s 1 SW896 3010A Z (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ®� 13 of 111 JOACCUTES T; M76251 �=Gory;or ei 1 M Accutest Laboratories Report of Analysis Page 1 of 1 w Client Sample ID: GT-3 Lab Sample ID: M76251-2 Date Sampled: 08/14/08 Matrix: AQ- Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84089.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 100% 79-130% 2037-26-5 Toluene-D8 91% 80120% 460-00-4 4-Bromofluorobenzene 91% 80 120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 14 of 111 QACCUTES'T. M76251 i t o: ;, r Accutest Laboratories Report of Analysis Page 1 of 1 w Client Sample ID: GT-3 Lab Sample ID: M76251-2 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20733.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 2.0 ug/1 100-41-4 Ethylbenzene ND2.0-1-1 ug/1 1634-04-4 Methyl Tert Butyl Ether .NiD 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene NOD 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadj) °ND 50 ug/l C9- C10 Aromatics (Unadj ) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 796 70-130% 615-59-8 2,5-Dibromotoluene 88% 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 15 of 111 12ACCUTEST M76251 Lc bo,,t iec Accutest Laboratories Report of Analysis Page 1 of 1 w Client Sample ID: GT-3 Lab Sample ID: M76251-2 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20731.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 36.2 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 26-158% 460-00-4 Bromofluorobenzene (S) 86%, 26 158% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 16 of 111 12ACCUTEET. M76251 L-L--�' if 5 Accutest Laboratories Report of Analysis Page 1 of 1 A Client Sample ID: GT-3 Lab Sample ID: M76251-2A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead 5 0 5.0 ug/l 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ®21 17 of 111 EACCLR'EST M76251 y Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-4 Lab Sample ID: M76251-3 Date Sampled: 08/14/08 Matrix: AQ- Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84090.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q ......._._.....__......... _.. 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol 1VD 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ... .........._ . .....___.__...__....._ 1868-53-7 Dibromofluoromethane 100% 79130% 2037-26-5 Toluene-D8 97% 80120% 460-00-4 4-Bromofluorobenzene 91% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value-exceeds calibration range N = Indicates presumptive evidence of a compound ® 18 of 111 ®ACCUTEST. M76251 _:to_,t,-;es r Accutest Laboratories Report of Analysis Page I of I Client Sample ID: GT-4 Lab Sample ID: M76251-3 Date Sampled: 08/14/08 Matrix: A - Ground Water Date Re ceived: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20734.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether :NO 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene NO. 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9-C10 Aromatics (Unadj.) ND.. 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics JND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 81% 70 130% 615-59-8 2,5-Dibromotoluene `90% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®11 19 of 111 12ACCUTE3T M76251 L,act nc ,rit r Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-4 Lab Sample ID: M76251-3 Date Sampled: 08/14/08 Matrix: AQ- Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20732.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 38.6 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.014 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 142..% _ 26 158% 460-00-4 Bromofluorobenzene (S) 103% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �® 20 of I l l 12ACCU TEST. M76251 Tztor-Oli-. M Accutest Laboratories Report of Analysis Page 1 of 1 CD Client Sample ID: GT-4 Lab Sample ID: M76251-3A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead 5:0 5.0 ug/I 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A Z (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ®� 21 of 111 QACCUTEST. M76251 M Accutest Laboratories Report of Analysis Page 1 of 1 y. Client Sample ID: GT-5 Lab Sample ID: M76251-4 Date Sampled: 08/14/08 Matrix: AQ -Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84091.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q ..._........_................. .._ 108-20-3 Di-Isopropyl ether ug/1 1634-04 4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether `ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ..................._. 1868-53-7 Dibromofluoromethane 100% 79130% 2037-26-5 Toluene-D8 97% 80-120% 460-00-4 4-Bromofluorobenzene 91% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IM® 22 of 111 ®QCCUTEST. M76251 L-to:,co-ie. Accutest Laboratories Report of Analysis Page 1 of 1 y Client Sample ID: GT-5 Lab Sample ID: M76251-4 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20735.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene sND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene MR 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadi ) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ;NI) 50 ug/I C9- C12 Aliphatics N'D 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 83% 70130% 615-59-8 2,5-Dibromotoluene 91% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound [Mffi 23 of 111 ®ACCL EBT. M76251 =t^°'a',orie, Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-5 Lab Sample ID: M76251-4 Date Sampled: 08/14/08 Matrix: AQ -Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20733.D 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 36.8 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.014 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 104% 26 158% 460-00-4 Bromofluorobenzene (S) 9,1% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 24 of 111 OQ� Accutest Laboratories Report of Analysis Page 1 of 1 00 Client Sample ID: GT-5 Lab Sample ID: M76251-4A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method. Lead 12 5ra `5.0 ug/I 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit �® 25 of 111 QACC L ITEST. M76251 �.torj—,r:c> t Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-7 Lab Sample ID: M76251-5 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84092.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q ....._...._... .......... .. . 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/l 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ............ .. 1868-53-7 Dibromofluoromethane 100% 79-130% 2037-26-5 Toluene-D8 959 80 120% 460-00-4 4-Bromofluorobenzene 93% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IM® 26 of 111 11ACC LITEST, M76251 t:or I;o-Ee Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: GT-7 Lab Sample ID: M76251-5 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20736.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene :ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/1 C9- C10 Aromatics (Unadj ) ND 50 ug/1 C5- C8 Aliphatics N,.D 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 80% 70130% 615-59-8 2,5-Dibromotoluene 89% 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 27 of I l l ®ACCUTEST. M76251 lat�r�;r ;.: i s Accutest Laboratories Report of Analysis Page I of I Client Sample ID: GT-7 Lab Sample ID: M76251-5 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20734.D 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 36.8 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.014 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 1b7% . 26-158% 460-00-4 Bromofluorobenzene (S) 90% 26 158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 28 of 111 12ACCUTEST. M76257 r Accutest Laboratories w Report of Analysis Page 1 of 1 0 Client Sample ID: GT-7 Lab Sample ID: M76251-5A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method _..............__ _... Lead 5 A '5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ®� 29 of 111 12ACCLrrEST: M76257 Accutest Laboratories w Report of Analysis Page I of 1 Client Sample ID: MW-101 Lab Sample ID: M76251-6 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84095.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/I 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ... ..... ... ... 1868-53-7 Dibromofluoromethane 99% 79-130% 2037-26-5 Toluene-D8 97% 80-120% 460-00-4 4-Bromofluorobenzene 92% 80-120% I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �® 30 of 111 ®ACCUTEST. M76251 r Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-101 Lab Sample ID: M76251-6 Date Sampled: 08/14/08 Matrix: AQ-Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20737.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100 41 4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether NTY 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene IVD 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/l C9- C10 Aromatics (Unadj ) ND 50 ug/I C5-C8 Aliphatics ND 50 ug/1 C9-C12 Aliphatics ND . 50 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 82% 70130% 615-59-8 2,5-Dibromotoluene 91% 70 130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IM® 31 of 111 ®ACCLrMST. M76251 -=t=' M Accutest Laboratories w Report of Analysis Page I of I Client Sample ID: MW-101 Lab Sample ID: M76251-6 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20735.D 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 36.2 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND % 0.015 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ...... . ._ ..... . 460-00-4 Bromofluorobenzene (S) 106%' 26 158% 460-00-4 Bromofluorobenzene (S) 89% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 32 of 111 12ACCUTEST M76251 -bo-a:o :ec i r Accutest Laboratories Report of Analysis Page 1 of 1 N Client Sample ID: MW-101 Lab Sample ID: M76251-6A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead 5.0 ug/1 1 08/21/08 08/22/08 PY Sw846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA:9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit F] 33 of 111 QACClJ'1'tEST. M16251 lzbor�;o:;s: Accutest Laboratories J Report of Analysis Page 1 of 1 w Client Sample ID: MW-102 Lab Sample ID: M76251-7 Date Sampled: 08/14/08 Matrix: AQ.- Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84096.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 1'02% 79-130% 2037-26-5 Toluene-D8 9$% 80120% 460-00-4 4-Bromofluorobenzene 92% 80120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 34 of I l l 12ACCLffEST. M76251 Accutest Laboratories Report of Analysis Page 1 of 1 w Client Sample ID: MW-102 Lab Sample ID: M76251-7 Date Sampled: 08/14/08 Matrix: AQ -Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590.Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20738.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ,ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj ) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene $5% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 35 of 111 ®ACCU'TEBT. M76251 -=to:at , ic; • y Accutest Laboratories w Report of Analysis Page 1 of 1 G, Client Sample ID: MW-102 Lab Sample ID: M76251-7 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20736.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 35.3 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 103%: 26-158% 460-00-4 Bromofluorobenzene (S) 84% 26 158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �® 36 of 111 ®ACCLrrEST. M76251 .a t:or,to,its r Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-102 Lab Sample ID: M76251-7A Date Sampled: 08/14/08 Matrix: AQ- Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead c 5 0 5.0 ug/1 1 08/21/08 08/22/08 PY Sw846 6010B 1 Sw846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ®� 37 of 111 ��a►ccu�sr. ' M76251 L=t=recur. Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MT-1/MT-3 Lab Sample ID: M76251-8 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84097.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q _........ ...._. .. 108 20-3 Di Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND7 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/l 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 101% 79130% 2037-26-5 Toluene-D8 98% 80-120% 460-00-4 4-Bromofluorobenzene 94% 80120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �® 38 of 111 QACgL T —sT M76251 L,L r v Accutest Laboratories Report of Analysis Page 1 of 1 N Client Sample ID: MT-1/MT-3 Lab Sample ID: M76251-8 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20739.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND I2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/1 C9- C10 Aromatics (Unadj ) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics .ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 70-130% 615-59-8 2,5-Dibromotoluene "gi 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IME] 39 of I l l QACCLJTEST. M76251 Accutest Laboratories w Report of Analysis Page 1 of 1 L, Client Sample ID: MT-1/MT-3 Lab Sample ID: M76251-8 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20737.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 37.0 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.014 ug/t CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 104%. 26-158% 460-00-4 Bromofluorobenzene (S) 84% ._ 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 40 of 111 QACCLrrES'T. M76251 to-a;u le: Accutest Laboratories Report of Analysis Page 1 of 1 CD Client Sample ID: MT-1/MT-3 Lab Sample ID: M76251-8A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ......_...._......._...__...... Lead 5 0 : 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 f RL = Reporting Limit 41 of 111 IRA►CCUTEST: M76251 =Gc-�;ur e: • M Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-202 Lab Sample ID: M76251-9 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84098.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-But 1 Ethyl Ether Y Y ND 2.0 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 101% 79-130% 2037-26-5 Toluene-D8 96% 80120% 460-00-4 4-Bromofluorobenzene .g 80120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IMP] 42 of I I I 12ACCUTEST. MT6251 L� r Accutest Laboratories Report of Analysis Page I of 1 y Client Sample ID: MW-202 Lab Sample ID: M76251-9 Date Sampled: 08/14/08 is Matrix: AQ -Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20740.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q .............. . . 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 826%.. 70-130% 615-59-8 2,5-Dibromotoluene 91% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 43 of 111 12ACCUTEST. M76251 Accutest Laboratories Report of Analysis Page 1 of 1 y Client Sample ID: MW-202 Lab Sample ID: M76251-9 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20738.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 36.0 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 97% 26-158% 460-00-4 Bromofluoro benzene (S) 77% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �® 44 of 111 12ACCLrMBT. M76251 -ebnrto .. r Accutest Laboratories w Report of Analysis Page 1 of 1 00 Client Sample ID: MW-202 Lab Sample ID: M76251-9A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ... .__._.._.._....... .. Lead <5.0 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A Z (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ® 45 of I l l MAC CU EST. M76251 I� f � Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-202D Lab Sample ID: M76251-10 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84099.D 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether N)J 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 101'% 79130% 2037-26-5 Toluene-D8 % 80120% 460-00-4 4-Bromofluorobenzene 93% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 131 46 of I I I CQCCUTEST. M76251 .at=!'3tc"i- Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-202D Lab Sample ID: M76251-10 Date Sampled: 08/14/08 Matrix: AQ -Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20741.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND ... 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj ) N 50 ug/l C9- C12 Aliphatics (Unadj.) N'D 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/l C5-C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene kwo 70130% 615-59-8 2,5-Dibromotoluene 91% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IME] 47 of 111 12ACCUTEST. M76251 =a c -- Accutest Laboratories w Report of Analysis Page 1 of I Client Sample ID: MW-202D Lab Sample ID: M76251-10 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20739.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 37.1 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q ....._........ ...... ..... 106-93-4 1,2-Dibromoethane ND 0.014 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 110% 26 158% 460-00-4 Bromofluorobenzene (S) 88% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 48 of 111 12ACCU7ES . M76257 Gors;o-le: Accutest Laboratories w Report of Analysis Page 1 of 1 0 Client Sample ID: MW-202D Lab Sample ID: M76251-IOA Date Sampled: 08/14/08 Matrix: AQ- Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL. Units DF Prep Analyzed By Method Prep Method Lead <S.Q 5.0 ug/I 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 M RL = Reporting Limit IMP] 49 of 111 12ACC UTEST. M76251 _ztcra;,. e: Accutest Laboratories Report of Analysis Page 1 of i Client Sample ID: MW-301D Lab Sample ID: M76251-11 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84100.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/I 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 1002/0 79-130% 2037-26-5 Toluene-D8 95% 80-120% 460-00-4 4-Bromofluorobenzene 91% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound JME3 50 of 111 12ACCLJTEST. M76251 i Ito i tr, `"• _ _ i r Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-301D Lab Sample ID: M76251-11 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20742.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) NE). 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 82% 70130% 615-59 8 2,5-Dibromotoluene 91 70 130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 51 of 111 QACCIJTEST. M76251 L_t f'j -:e: r Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-301D Lab Sample ID: M76251-11 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20740.D 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 35.3 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.015 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenz.ene (S) 104% 26-158% 460-00-4 Bromofluorobenzene (S) 89%` 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IM® 52 of 111 12ACCUTEST. M76251 L-tc"atori-- c r Accutest Laboratories w Report of Analysis Page 1 of 1 N Client Sample ID: MW-301D Lab Sample ID: M76251-IIA Date Sampled: 08/14/08 Matrix: AQ- Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF -Prep Analyzed By Method Prep Method Lead <5.0; 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit 53 of i l l 12QCCLrrE3T. M76251 =born cuNes r Accutest Laboratories w Report of Analysis Page i of 1 w Client Sample ID: MW-301S Lab Sample ID: M76251-12 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84101.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q ............. .. . ...... 108-20-3 Di-Isopropyl ether ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 100%.`. 79 130% 2037-26-5 Toluene-D8 98% 80-120% 460-00-4 4-Bromofluorobenzene 90% 80120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 54 of 111 QAC=.0 TEST. M76251 L=G='3 '""- Accutest Laboratories w Report of Analysis Page 1 of 1 w Client Sample ID: MW-301S Lab Sample ID: M76251-12 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20743.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) NI).—.: 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 83% 70-130% 615-59-8 2,5-Dibromotoluene 91% 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M® 55 of I l l ®ACCUTEST. M76251 Accutest Laboratories w Report of Analysis Page 1 of 1 w Client Sample ID: MW-301S Lab Sample ID: M76251-12 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20742.D 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 37.4 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.014 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 03% ' 26-158% 460-00-4 Bromofluorobenzene (S) 889/. 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 56 of I I I ®ACC_ UTE'sT: M76251 =t'J--,r;.., 1 Accutest Laboratories w Report of Analysis Page 1 of i A Client Sample ID: MW-301S Lab Sample ID: M76251-12A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead G 5 0. 5.0 ug/1 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ®� 57 of 111 12ACCU EST: M76251 L t—a1—ieL t Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-302D Lab Sample ID: M76251-13 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84102.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND - 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 7 ` 1.0 ug/l 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100% 79-130% 2037-26-5 Toluene-D8 95% 80-120% 460-00-4 4-Bromofluorobenzene 90% 80120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 58 of I l l QACCInf . M76251 G^^ to rle: v Y Accutest Laboratories w Report of Analysis Page 1 of 1 N Client Sample ID: MW-302D Lab Sample ID: M76251-13 Date Sampled: 08/14/08 Matrix: AQ -Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20744.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene NI), 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND ` 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj ) N3D 50 ug/1 C9- C10 Aromatics (Unadj ) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene $9.% 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound QQ 59 of 111 CACCUTE3T Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-302D Lab Sample ID: M76251-13 Date Sampled: 08/14/08 Matrix: AQ -Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20743.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 33.0 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.016 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 94% 26-158% 460-00-4 Bromofluorobenzene (S) 62% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 60 of 111 ®ACCLJTE T. M76251 L=6crat.,; Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-302D Lab Sample ID: M76251-13A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08. Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <5 0' 5.0 ug/l 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit ®p 61 of 111 QACC UTEST. M76251 L Ito rn to rice Accutest Laboratories w Report of Analysis Page 1 of 1 v Client Sample ID: MW-302S Lab Sample ID: M76251-14 Date Sampled: 08/14/08 Matrix: AQ-Ground Water Date Received: 08/15/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G84103.1) 1 08/19/08 EL n/a n/a MSG3395 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/l 637-9213 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane .104% 79-130% 2037-26-5 Toluene-D8 96% 80-120% 460-00-4 4-Bromofluorobenzene 89% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®19 62 of 111 QACCUrEST M76251 1 7 Accutest Laboratories w Report of Analysis Page I of 1 y Client Sample ID: MW-302S Lab Sample ID: M76251-14 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20745.D 1 08/23/08 AF n/a n/a GBD985 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND I2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND ; 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9-C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND < 50 ug/1 C5- C8 Aliphatics NO, 50 ug/1 C9-C12 Aliphatics ND.... 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 895'6 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IM11 63 of I l i ®ACCUTEST. M76251 ._t�ago':ec Accutest Laboratories w Report of Analysis Page 1 of 1 K) Client Sample ID: MW-302S Lab Sample ID: M76251-14 Date Sampled: 08/14/08 Matrix: AQ - Ground Water Date Received: 08/15/08 Method: EPA 504 EPA 504 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20744.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 Run#2 Initial Volume Final Volume Run#1 36.6 ml 2.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND. 0.014 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 9.9% 26-158% 460-00-4 Bromofluorobenzene (S) 77% 26-158% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �® 64 of 111 ®ACCUTEST. M76251 L-'tsra ,ri Accutest Laboratories w Report of Analysis Page i of I K) Client Sample ID: MW-302S Lab Sample ID: M76251-14A Date Sampled: 08/14/08 Matrix: AQ - Groundwater Filtered Date Received: 08/15/08 Percent Solids: n/a Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method . ....._.......... Lead <5.0 5.0 ug/I 1 08/21/08 08/22/08 PY SW846 6010B 1 SW846 3010A 2 (1) Instrument QC Batch: MA9620 (2) Prep QC Batch: MP12365 RL = Reporting Limit 65 of 111 12ACCUTEST. M76251 Lat Ora to rl es New England -01 AC'.ACUTEST _ Section 4 tr`s jai W. xatr rWEf,4a SIT fty Mike. Forms. Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle ®® 66 of 111 QACCUTEST M76251 L=G^_a a,,,i er 0 LAB(LOCATION) Shell Oil Products Chain Of Custody Record YAP. D-51 :::::::pjeaSe C TV 0�---a5 D�A arruL ❑sir�M� 1.............—— X ' a 6 DATE:F 111171 PES jouim 11 1 .... ...'i i i I PAGE: • of Sovereign Consulting 590 —.gh Road.Wannis.MA 905 B South Main Street L Mansfield,FAA 02o4a 508-339-3248 skir.hZ-20.mn TURNAROUNDAlc u.Lmo" E,-*.t Cr..A*12� TURNAROUND THE(C�N]Wt[)Ant: . . . . ... 9 (L4 MY) 05DAYs 0 IDAYS wws REQUESTED ANAWsis DEMMULES: [a COPM 0 OD0018 0 MCP 0 (SPKLn TEMPEPATUREONIMM[" f 1— jC W 12 SPECIAL INSTRUCTIONS OR NOTES: 1-6 PLEASE FILTER DISSOLVED LEAD SAMPLES IN LAB PRIOR TO ANALYSIS. > :# Field Sample Identifi"flon af Caasa�rPtDlk dIngs HQ.J-140J-1 a- 6-t 44wv X 1 1'7 X K X IXI I I I I I I I 6r 4, &Air 64 vk� & j qN51 M76251: Chain of Custody Page 1 of 3 of 111 JUACCUTEST. M76251 L-,t o:,t,r:t-, LAB(LOCATION) Q Shell Oil Products Chain Of Custody Record V-SERVICES) 0 aE .01, Ippm 13 NDfIVA RETAIL 11 11 8 1 6 DATE 31#tfar TO MIR[I L I...... PAGE:--,�—of cay a.—4: Sovereign Consulting 690 Ivan Road.Hnnnis,MA 905 8 South Main Street L MA 020M ............. u.sr.0m9r. ....... 14 U0 ....... -03mys 02mys 0 x.NplRe REQUESTED)eALYSIS OEUVERABLES: 13 Comm 0 M B 0 N 0 Acp El 0r (Swm v) TEMPEWUAEONRECELWIC C­1 j icoob SPECIAL INSTRUCTIONS OR NOTES: LL PLEASE KILTER DISSOLVED LEAD SAMPLES IN LAB PRIOR TO ANALYSIS. e. • SAMPLING PRESERVATIVE Field Sample Identificalon Contb.,F4D R-dinp DATE TIME wry Nate 0 0 O uja GU X--)� "A 1"7 tj - _,uvo mi nzuae Lj - V A,& L/ v i=-b,i'_—) \4\ij M76251: Chain of Custody Page 2 of 3 68 of III 12ACCUTEST. M76251 L.t�-:-a-,,r i e E Page 1 of 1 Frank D'Agostino From: Collins,Diane[DCollins@sovcon.com] Sent: Wednesday,September 03,2008 10:11 AM To: Frank D'Agostino Cc: Kirsch,Sylvia Subject:Well ID Incorrect-Lab Sample M76251 Hi Frank, Can you please correct sample ID and reissue data package for Lab sample M76251 M76251-7-ID MW-103 Sample ID should be MW-102. Please confirm when it's ready. Thank you di Diane Collins Client Support Administrator Sovereign Consulting,Inc. 905B South Main Street Suite 202 Mansfield,MA 02048 P:508-339-3200 Ext.259 F:508-339-3248 email:DCollins(a)sovcon.com F� J N t11 n kS' A� b O N �® C� � w � l"f• O ^O W p 9/3/2008 u � Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 N Title: MADEP MCP Response Action Analytical Report Certification Form .` �' � v1 , ��'a.,z'�' '' .. � `�•� � -tt as ice' Laboratory Name: Accutest Laboratories of New England Project#: M76251 Project Location: SCMAW:97451486(REIMBMA)590 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M76251-1 through M76251-14 Test method:EPA 504,and below Sample Matrices: Groundwater X Soil/Sediment () Drinking Water () Other: () () 0P ICE ' 8260B X 8151 A 8330_U 60106 X 7470A/1 A ethotlslsed 8270C 8081A VPH LXJ 6020 9014M Z 8082 8021 B EPH 7000 S 3 7196A Compen�w" of � elease rack to zNFtTtJ ,:' wh N( i ^` Hor od �s An affirmative response to questions A,B,C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with Yes ❑ No that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and 0 Yes ❑ No discuss in a narrative QC data that did not meet appropriate performance standards orguidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty", as described in Section 2.0(a),(b),(c)and Yes ❑No (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without 0 Yes ❑No significant modifications,as specified in Section 11.3? A response to questions E and F below is required for"Presumptive Certainty'status E Were all QC performance standards and recommendations for the Yes El No specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified ❑ Yes El No method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is,to the best of my knowledge and belief,accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 08/28/2008 ®� 70 of 111 12ACCUTIEE MADEP VPH FORM 1VlNO k A ueous Soil Sediment Other F1 C"®ntalriers - Satisfactor Broken Leaking ' A ueo4Pre ervattues N/A H <= 2 H > 2 Teri.., ratti Received on Ice Received at 4 De . C Other ✓ Rec'd at 2.0 Deg.C RAIN h;MON s�a"�i`.g�'d" .�-., :,hY Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-1 Lab ID: M76251-1 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target AnalAes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 90 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. c Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'Y qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ClYes L_J No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? C✓JNo I Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 IM® 71 of 111 M76251 '-t 0r l to rlev MADEP VPH FORM affix .- Aqueous W Soil F.. Sediment Other I Containers Satisfactory Broken El Leaking A-ueous�Presetrative-- N/A pH <= 2 ✓ H >2 11 R a e tU e Received on Ice -1 Received at 4 Deg. C Other ✓ Rec'd at 2.0 Deg.C Meth N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-3 Lab ID: M76251-2 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. IZ A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes No Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? !'Yes __' No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? INo Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 ®P] 72 of 111 MACCUTEST. M76251 L=ocr3--it: MADEP VPH FORM Matrtx A ueous Soil L Sediment F Other F iffwla ffi - 4,, Satisfactor ✓ Broken — Leakin A ueotf Preservatives' N/A pH <= 2 .L H > 2 iT e-rature X Received on Ice ; Received at 4 Deg. C Other ✓ Rec'd at 2.0 Deg.C Mth� of mm N/A as Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-4 Lab ID: M76251-3 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Ranoe Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 90 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C70 Aromatic Hydrocarbons. - Z A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? OYes Ul No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? We Yes 0 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ONo D. Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 IBLJ M' 73 of I I I QAC NJTF3T. M76251 Le t or�t o r l es i e MADEP VPH FORM A ueous W, Soil F-1 Sediment 7 Other C' t�ttlrs Satisfactor Broken Leakin r A ueo: PceervaCtues- N/A H <= 2 Imo, H >2 i tt f Received on Ice Received at 4 Deg. C 1— Other Rec'd at 2.0 Deg.C Nletanot £: F N/A a Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-5 Lab ID: M76251-4 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/1 ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 83 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. (c Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude i conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. i IZ A'Y qualifier indicates an estimated value i Were all QA/QC procedures REQUIRED by the VPH Method followed? R]Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? LJYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? DV No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 8/28/2008 Printed Name Reza Tand ME] 74 of I I I �ACCIJ'i'EST M76251 =torsto.i s MADEP VPH FORM: OWN—�i �� Aqueous n Soil Sediment Other (I Corta>nsr Satisfactor Broken ( Leaking t A ueousrPre ervattvkl N/A H <= 2 �' pH > 2 1-1 1�'e�t eratu e � , Received on Ice Received at 4 Deg. C Other Rec'd at2.0 Deg.C ethanEt N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: GT-7 Lab ID: M76251=5 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target AnalAes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 NIA ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 89 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 6 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C1Z aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Y qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑Yes EI No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes CJ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? WNo LI Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 IM® 75 of 111 MACCUTEST. M76257 MADEP VPH FORM fVlatrtx,,_ � A ueous ✓ Soil I 1 Sediment Other Gontalners Satisfactory✓IBroken Leakin A:ueous Preservatives N/A F1 pH <= 2 PH > 2 rn erature Received on Ice D Received at 4 Deg. C Lj Other ✓ Rec'd at 2.0 Deg.C fVle�hartgl _ -�� = N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-101 Lab ID: M76251-6 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 25-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C70 Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ✓-!Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ✓_!Yes I.I No Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No I...' Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 M® 76 of 111 JOACCUTEST M76251 L_tc-na­ie + r MADEP VPH FORM } A ueous I,,l Soil -1 Sediment lI Other I I Corftalners . Satisfactor `v) Broken F1 Leakinci D 'a ueous Preservatives: N/A — H <_ 2 W,I pH > 2 `-J T t11 eratt�re Received on Ice i-I Received at 4 Deg. C 1-1 Other LEI, Rec'd at 2.0 Deg.C i A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-103 Lab ID: M76251-7 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analyzes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 85 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. lZ A'Y qualifier indicates an estimated value I Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 ®® 77 of I I I 12ACa+UTEST. M76251 Lztor�torles MADEP VPH FORM lSlfaW MA IMA Aqueous n Soil Sediment F-1 Other !-1 *uo Satisfactor ✓ Broken n Leaking A=ueousPreservative N/A PH <= 2 ✓ pH > 2 f Tftteaitire Received on Ice Received at 4 Deg. C Other ✓ Read at 2.0 Deg.C fllle--_ no'_ ', N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MT-1/MT-3 Lab ID: M76251-8 Method for Target Analyzes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/1 ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analyzes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/1 ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/1 ND 2 I j Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 (Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 90 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the i concentration of Target Analytes eluting in that range. IC Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. IZ A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes 0 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo r 1 Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 ®® 78 of I l l ®ACCLTEST. M76251 La t crS t,ri MADEP VPH FORM Matrtx A ueous �, Soil ] Sediment F 1 Other F I fpr�ttlilets Satisfactor Broken El Leakin AB u�Qos,Preseatfuesz N/A H <= 2 �: DH > 2 Tt� eratur=e Received on Ice F Received at 4 Deg. C Other :o', Rec'd at 2.0 Deg.C eth�a Q�� r N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-202 Lab ID: M76251-9 Method for Target Analytes: MADEP VPH REV 1 A Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? CND D Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 f® 79 of I I I MACCUTEST M76251 MADEP VPH FORM A ueous ✓ Soil 1 Sediment 7 Other I Co�it Ifaem Satisfactory✓ Broken U1 Leaking Aue`ousPresfuattveSH N/A F, pH <= 2 ✓ H > 2 Tem` etutut Received on Ice Received at 4 Deg. C Other ✓ Rec'd at 2.0 Deg.C WWI rod�.fl NM N/A a Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-202D Lab ID: M76251-10 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Ter(Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C70 Aromatic Hydrocarbons. Z A'Y qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 'Yes _. No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? !Yes _ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? INo Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 80 of I I I MA CCUTEBT. M76251 MADEP VPH FORM IVlatnx w. A ueous Fv-1 Soil n Sediment F, Other f 1 Contai.n, rs r. r, Satisfactory ky� Broken F Leaking A;te°ous Prt'servatives N/A ! H <= 2 pH > 2 Tent e atur %, s Received on Ice Received at 4 Deg. C Other Rec'd at 2.0 Deg.C ethari5 ry N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301D Lab ID: M76251-11 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target AnalAes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range- C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value I Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes LJ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑Yes Ll No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 8/28/2008 Printed Name Reza Tand IME1 81 of 111 QAC.C.0 EST. M76257 tzbo"scum^ MADEP VPH FORM MaiTt f ,x �4 A ueous W, Soil M Sediment ,"-I Other Conanls' Satisfactor Broken F Leaking -i Aqueous Prest? rattyes N/A pH <= 2 W,i pH > 2 i Tem eratifrd % Received on Ice F-1 Received at 4 De . C F-I Other Rec'd at 2.0 Deg.C Methanol � � N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301S Lab ID: M76251-12 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Benzene 7143-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 • o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 i Miusted Ranges i C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND° 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 83 70-130% PID:2,5-Dibromotoluene % 91 70-130 (Footnotes IA Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. IC Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude i conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'Y qualifier indicates an estimated value i Were all QA/QC procedures REQUIRED by the VPH Method followed? R]Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 ®® 82 of Ill 1JACCU TEST M76251 tat=-jt—;es MADEP VPH FORM Hatrlx� � Aqueous ICI Soil R Sediment I-11 Other I—! Ciintat atisfactoryWl Broken n Leaking i AxuasPree vatrvesa N/A H <= 2 Dy pH > 2 Tem ertur� ,; Received on Ice �) Received at 4 Deg. C Other Rec'd at 2.0 Deg.C et# anvluWs N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-302D Lab ID: M76251-13 � Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1. N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/1 ND' 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 89 70-130% FID:2,5-Dibromotoluene % 79 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cons of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'Y qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WlYes r i No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes I 1 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 91No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 �® 83 of 111 ®ACCUTEBT. M76251 t-,-,.o rf e: MADEP VPH FORM Matrtx z ` A ueous Soil F Sediment ( l Other —I Coritalners s Satisfactory Broken 0 Leakin AW ueousIPYeservtfue N/A H <= 2 W I* > 2 Li Tem erasure Received on Ice F1 Received at 4 Deg. C Fl Other l� Rec'd at 2.0 Deg.C N/A ja Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-302S Lab ID: M76251-14 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/14/2008 Date Received: 8/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/23/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 I I o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 I Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 i m,p-Xylene C9-C12 ug/I ND 2 jAdiusted Ranges iC5-C8 Aliphatics N/A ug/I ND° 50 C9-C12 Aliphatics N/A ug/I ND° 50 (Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 89 70-130% I FID:2,5-Dibromotoluene % 81 70-130 Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range IB Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.. C5-C8 Aliphatic Hydrocarbons exclude the j concentration of Target Analytes eluting in that range. IC Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. iZ A'Yqualifier indicates an estimated value I Were all QA/QC procedures REQUIRED b the VPH Method followed? �i P Y Yes No Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes .__' No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? !�!No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 8/28/2008 E® 84 of 111 12ACCUTEST. M76251 Accutest Laboratories Internal Sample Tracking Chronicle P, Shell Oil Job No- M76251 , SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes IG MT76251�C�llected�l�4 1UG�08 09�5BBy A� �Recerved'�1�5 �� i18 By�� �p ��� M76251-1 SW846 8260B 19-AUG-08 00:40 EL V8260OXY5 M76251-1 EPA 504 20-AUG-08 07:46 CZ 19-AUG-08 FG V504EDB M76251-1 MADEP VPH REV 1.123-AUG-08 10:12 AF VMAVPH IU�76251�2Collected 14 AUG 0808:30�By'�AW� �Rece�ved' 31��ttG 0$ �� 5� � �` ��� M76251-2 SW846 8260B 19-AUG-08 01:12 EL V8260OXY5 M76251-2 EPA 504 20-AUG-08 08:46 CZ 19-AUG-08 FG V504EDB M76251-2 MADEP VPH REV 1.123-AUG-08 10:53 AF VMAVPH GAT 41 3��Colleci d14 AUG 08�09,��15�tBy�AWR �� 1� ��08 � � s s ,w,,,... M76251-3 SW846 8260B 19-AUG-08 01:43 EL V8260OXY5 M76251-3 EPA 504 20-AUG-08 09:16 CZ 19-AUG-08 FG V504EDB M76251-3 MADEP VPH REV 1.123-AUG-08 11:34 AF VMAVPH �7625�1 4 "Collected n1 �A�JG 08 10�L5�By, A�W ��'�Rece�ued�1�F�1JGr•08�B��S��� y � �,-� M76251-4 SW846 8260B 19-AUG-08 02:14 EL V8260OXY5 M76251-4 EPA 504 20-AUG-08 09:46 CZ 19-AUG-08 FG V504EDB M76251-4 MADEP VPH REV 1.123-AUG-08 12:15 AF VMAVPH M762�6� 5 Collected 14�AL#�G�08�09 30 �By AW �Rec��ued1� AUG 08�B �5���� �� � M76251-5 SW846 8260B 19-AUG-08 02:45 EL V8260OXY5 M76251-5 EPA 504 20-AUG-08 10:16 CZ 19-AUG-08 FG V504EDB M76251-5 MADEP VPH REV 1.123-AUG-08 12:56 AF VMAVPH {'yam r s h�`"1 v� t` "� a *�^a'°r-' ' 4 °�^ � �`✓zi�c-. '°�'° �" %� y�.� �762'5�6 Collected i4 ALiG�08 12 1(# B AW Received iS=AtC�tl8 By � M76251-6 SW846 8260B 19-AUG-08 04:20 EL V8260OXY5 M76251-6 EPA 504 20-AUG-08 10:46 CZ 19-AUG-08 FG V504EDB Page 1 of 5 ®E] 85 of 111 12ACCUTEST. M76251 Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil , SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Job No: M76251 Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes M76251-6 MADEP VPH REV 1.123-AUG-08 13:37 AF VMAVPH �M-76251 �CaIIecledi4 Att1 08 12SB W Receec1 [408By�S ' � M76251-7 SW846 8260B 19-AUG-08 04:52 EL V8260OXY5 M76251-7 EPA 504 20-AUG-08 11:15 CZ 19-AUG-08 FG V504EDB M76251-7 MADEP VPH REV 1.123-AUG-08 14:18 AF VMAVPH M762 8�ollected 4 AIJ�082°'x15�'By�AW� Rye �ve�d 1�5�;A �0�8�y'�S�P� � �u'� fT 1�'MT 3 s a M76251-8 SW846 8260B 19-AUG-08 05:23 EL V8260OXY5 M76251-8 EPA 504 20-AUG-08 11:44 CZ 19-AUG-08 FG V504EDB M76251-8 MADEP VPH REV 1.123-AUG-08 14:59 AF VMAVPH MW,2251`9 Collected�1AUG11 30BAUU� �ece$d�1 G6BySAP g x 114W 02 M76251-9 SW846 8260B 19-AUG-08 05:55 EL V8260OXY5 M76251-9 EPA 504 20-AUG-08 12:14 CZ 19-AUG-08 FG V504EDB M76251-9 MADEP VPH REV 1.123-AUG-08 15:40 AF VMAVPH '17625-110CoIIec ed 14� Gfl81i 4ByAW �cved 15 AEG 08y S c M76251-10 SW846 8260B 19-AUG-08 06:27 EL V8260OXY5 M76251-10 EPA 504 20-AUG-08 12:44 CZ 19-AUG-08 FG V504EDB M76251-10 MADEP VPH REV 1.123-AUG-08 16:21 AF VMAVPH ,.w,,.,.... .s^l ....,...�, _.rx„ .. ._�.,..m° �. �'' a,': ..,,,°xe<s✓'.. *R.. �,`..u ,a-,,,."'_> '-.,, ..,.,�,' .,rr M76251-11 SW846 8260B 19-AUG-08 06:58 EL V8260OXY5 M76251-11 EPA 504 20-AUG-08 13:13 CZ 19-AUG-08 FG V504EDB M76251-11 MADEP VPH REV 1.123-AUG-08 17:02 AF VMAVPH Page 2 of 5 E] 86 of III 12ACCL EST. M76251 -=t ori,o ie: r Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil , SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Job No: M76251 Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes M76251-12 SW846 8260B 19-AUG-08 07:30 EL V8260OXY5 M76251-12 EPA 504 20-AUG-08 14:12 CZ 19-AUG-08 FG V504EDB M76251-12 MADEP VPH REV 1.123-AUG-08 17:43 AF VMAVPH M76251-13 SW846 8260B 19-AUG-08 08:01 EL V8260OXY5 M76251-13 EPA 504 20-AUG-08 14:42 CZ 19-AUG-08 FG V504EDB M76251-13 MADEP VPH REV 1.123-AUG-08 18:24 AF VMAVPH VI76251r 1�4 Call ed14AUiG t)8r11By AW Receved�lSUG $�By ASS y � } C a e �• - a" r M,W M76251-14 SW846 8260B 19-AUG-08 08:33 EL V8260OXY5 M76251-14 EPA 504 20-AUG-08 15:12 CZ 19-AUG-08 FG V504EDB M76251-14 MADEP VPH REV 1.123-AUG-08 19:06 AF VMAVPH 1��I7625�1,1ACailec fin.,,✓,,,R_ M76251-1A SW846 6010B 22-AUG-08 12:04 PY 21-AUG-08 PY PB �'T��5�1�2 4xt,..,Czn..0 M76251-2A SW846 6010B 22-AUG-08 12:08 PY 21-AUG-08 PY PB iv1762513A`C llecfed"l4AtTGO916ByAW �4tocird15:AG OSB SAP h s n M76251-3A SW846 6010B 22-AUG-08 12:12 PY 21-AUG-08 PY PB 1�765,1- �ACx:�ollec#edAUG 0$�1= e15�B A�WY �Rer�t?d15 AUG D$�BAP � �� �• �to � '��� ��` � � r � M762514A SW846 6010B 22-AUG-08 12:25 PY 21-AUG-08 PY PB Page 3 of 5 �® 87 of I l l 12ACCUTES'T. M76251 ==Gcr co r Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M76251 SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes 1U176251'�5A`C�llected al4.AUG 08�09 3'�O�B ��� �ece�1�d1.5� L�1C,�08By�SA�P-�� � ����� M76251-5A SW846 6010B 22-AUG-08 12:30 PY 21-AUG-08 PY PB M7625�1 6�ACollected �14E13G flfl8 �10 B�A�U Receivedl5 AUG 08 �B SA1' ,��� MW �... .. n.. . M76251-6A SW846 6010B 22-AUG-08 12:34 PY 21-AUG-08 PY PB M76251 TACollect d 14 A�IJGfi08 12 35 By A Received lS AUG 8 By SAP g MW Lr02 ..� .�,.,.m. M76251-7A SW846 6010B 22-AUG-08 12:39 PY 21-AUG-08 PY PB M762 1 8A Collected l4 AUG 08 L2 1�B AW 4' eceived LS,A�Ut 08 B AP y = � � � MT 11MT 3k "� y xy ;. �£ M76251-8A SW846 6010B 22-AUG-08 12:43 PY 21-AUG-08 PY PB 14�AL`I'G'081���30v�By�AW,,� `�Recei�ed�1�5°AUG08"By SAP� fi sg � ���`� RIM_ az:�Xs���..._..�.�w� M76251-9A SW846 6010B 22-AUG-08 12:48 PY 21-AUG-08 PY PB M765a110ollected14 }G 08 11 4I BAWRece�+ed1 �AU ti8BySAP€ M76251-10ASW846 6010B 22-AUG-08 11:11 PY 21-AUG-08 PY PB M762��11 collected 14 A1�1G,08�10 30�By�A�W� ��Receiued 15�AUG�08 B� &�SAP���� � �� MW 30Lr3� � ^�tr``✓r` �s �s��� r� tY'> 3�,�, �X aa§` � ' 2r -, �G � � c"' M76251-11ASW846 6010B 22-AUG-08.11:46 PY 21-AUG-08 PY PB .,.�aA,�,r .. !,,,,, �u«✓,rc-`� , .. ._�, ,...s�.2,-'� ��_ ,..,,,,�F �, .;. ..,��z,..,,. ,.ct�r.�. .� � r'',.._u,,.,..�..� _.:��'�"°.„z. .,,A... M76251-12ASW846 6010B 22-AUG-08 11:50 PY 21-AUG-08 PY PB Page 4 of 5 �® 88 of 111 ®ACC UTEST M76251 L z E o 3--i e. � P Accutest Laboratories Internal Sample Tracking Chronicle A Shell Oil Job No: M76251 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes M�'76251`1�3PGollected 14�AUG'�,�8 11�10„By�AW eiued�15�AUG�0$ i S�AP� � � �� M76251-13ASW846 6010B 22-AUG-08 11:55 PY 21-AUG-08 PY PB x M76251-14ASW846 6010B 22-AUG-08 11:59 PY 21-AUG-08 PY PB Page 5 of 5 �® 89 of I I I QAGGUTEST. M76251 L-tora;—ic: y W% New England All� TAT Section 5 �r� t rya rFEfS14°thr GC/MS Volat h. QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ®� 90 of 111 GJAC.0 TEST. M76251 L a t ora:o ri s Method Blank Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3395-MB G84087.1) 1 08/19/08 EL n/a n/a MSG3395 The QC reported here applies to the following samples: Method: SW846 8260B M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, M76251-11, M76251-12, M76251-13, M76251-14 CAS No. Compound Result RL Units Q ................ ......... ...... 108-20-3 Di-Isopropyl ether ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether Np 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether -ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 999/0 79-130% 2037-26-5 Toluene-D8 9.6% 80-120% 460-00-4 4-Bromofluorobenzene 93% 80-120% ®® 91 of 111 ®ACCLffEST. M76251 t q Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3395-BS G84084.1) 1 08/18/08 EL n/a n/a MSG3395 MSG3395-BSD G84085.1) 1 08/18/08 EL n/a n/a MSG3395 0A IJ The QC reported here applies to the following samples: Method: SW846 8260B M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, M76251-11, M76251-12, M76251-13, M76251-14 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 51.0 51.3 103 1 56 145/25 1634-04-4 Methyl Tert Butyl Ether 50 47.4 95 47.8 96 1 70-130/25 994-05-8 tert-Amyl Methyl Ether 50 51.2 102 _ 51.2 102 0 51 138/25 75-65-0 Tert Butyl Alcohol 500 493 99 503 101 2 60-146/25 637-92-3 tert-Butyl Ethyl Ether 50 52.8 106 53.3 107 1 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 98% 100% 79-130% 2037-26-5 Toluene-D8 98% 97% 80-120% 460-00-4 4-Bromofluorobenzene 92% 93,% 80-120% ®® 92 of Ill ®ACCUTEST M76251 r Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M76251-5MS G84093.1) 5 08/19/08 EL n/a n/a MSG3395 M76251-5MSD G84094.1) 5 08/19/08 EL n/a n/a MSG3395 M76251-5 G84092.1) 1 08/19/08 EL n/a n/a MSG3395 is The QC reported here applies to the following samples: Method: SW846 8260B M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, M76251-11, M76251-12, M76251-13, M76251-14 M76251-5 Spike MS MS MSD MSD Limits CAS No. Compound ug/l Q ug/l ug/I % ug/l % RPD Rec/RPD 108-20-3 Di-Isopropyl ether ND 250 259 1Q4 257 031 54-155/30 1634-04-4 Methyl Tert Butyl Ether ND 250 239 9G 237 95 , i 54-144/30 994-05-8 tert-Amyl Methyl Ether ND 250 246 9$ 249 =100 ' 1 47-142/30 75-65-0 Tert Butyl Alcohol ND 2500 2410 96 2410 96 0 60 148/30 637-92-3 tert-Butyl Ethyl Ether ND 250 261 104 260 104 0 46 151/30 CAS No. Surrogate Recoveries MS MSD M76251-5 Limits 1868-53-7 Dibromofluoromethane 101% 100%. 100% 79-130% 2037-26-5 Toluene-D8 950/6 96% 95% 80-120% 460-00-4 4-Bromofluorobenzene 90% 93%0 93% 80-120% ®� 93 of 111 12ACC UTEST: M76251 L=torn to ties o y Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: SW846 8260B Matrix: AQ Samples and QC shown here apply to the above method cri Lab Lab Sample ID File ID S1 S2 S3 M76251-1 G84088.1) 1fl0.0 97.0 .920 M76251-2 G84089.1) 100..0 91.0 M76251-3 G84090.D 100 0 97.0 91:0 M76251-4 G84091.1) 100.0 ,` 97.0 91'0 M76251-5 G84092.1) 100 0 95.0 93,0 . M76251-6 G84095.D 99 0 97.0 92.0 M76251-7 G84096.1) 102 0 98.0 92:0 M76251-8 G84097.1) 1010 98.0 :9.4;0 M76251-9 G84098.1) 101-.0 96.0 91.;0 M76251-10 G84099.1) I01 0 97.0 93:0 M76251-11 G84100.D 100 0 95.0 91.b M76251-12 G84101.1) 100 0 1 98.0 90:0 M16251-13 G84102.1) 100 0 95.0 90:0 M76251-14 G84103.1) 104.0 96.0 89.0 M76251-5MS G84093.1) 101. 95.0 9OA M76251-5MSD G84094.1) 100.0 96.0 93.0 MSG3395-BS G84084.1) 98 0 98.0 92::0 MSG3395-BSD G84085.1) 100 0 97.0 93:0 MSG3395-MB G84087.1) 99.0 96.0 Surrogate Recovery Compounds Limits S1 = Dibromofluoromethane 79430% S2 = Toluene-D8 80 120% S3 = 4-Bromofluorobenzene 80 L20% ............................... 94 of 111 QAC CUMST. M76251 Lab=rjt i o r ®® New England JZACCUTEST Section 6 GC Volatles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ®® 95 of I l l ®ACCLITEST. M76251 t_to Method Blank Summary Page I of 1 Job Number: M76251 Account: SHELLWIC Shell Oil, Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD985-MB BD20729.D 1 08/23/08 AF n/a n/a GBD985 rn The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, • M76251-11, M76251-12, M76251-13, M76251-14 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND " 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj ) ND 50 ug/1 C9- C10 Aromatics (Unadj ) N.D 50 ug/l C5- C8 Aliphatics NO 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 899% 70-130% �® 96 of 111 12ACCUTEST. M76251 L=t or�Z,.ies Method Blank Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16540-MB BB20724.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 rn The QC reported here applies to the following samples: Method: EPA 504 M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, M76251-11, M76251-12, M76251-13, M76251-14 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane NW. 1-0.015 ug/l CAS No. Surrogate Recoveries Limits 460-00-4 Bromofluorobenzene (S) 121% 26-158% 460-00-4 Bromofluoro benzene (S) 1209/o 26-158% 9 �® 97 of 111 QACCLrrE3T. M76251 Sabo-ac—it, Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD985-BSP BD20730.D 1 08/23/08 AF n/a n/a GBD985 GBD985-BSD BD20731.D 1 08/23/08 AF n/a n/a GBD985 rn The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, M76251-11, M76251-12, M76251-13, M76251-14 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/1 % RPD. Rec/RPD 71-43-2 Benzene 50 53.7 10,7. 54.0 108 I;, 70-130/25 100-41-4 Ethylbenzene 50 54.6 109 54.8 110 0 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 53.0 106 52.8 4,06 : 0 70-130/25 91-20-3 Naphthalene 50 47.3 95 48.5 97 3 70130/25 108-88-3 Toluene 50 54.4 109 54.7 109. 1 70-130/25 m,p-Xylene 100 109 109 109 109 0 70-130/25 95-47-6 o-Xylene 50 51.0 102 51.2 102 0 70-130/25 C5- C8 Aliphatics (Unadj.) 150 146 97 ... 144 981. 1 70-130/25 C9- C12 Aliphatics (Unadj.) 150 144 96 142 95 1 70-130/25 C9-C10 Aromatics (Unadj.) 50 51.3 103 51.0 102 1 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 79% 81% 70130% 615-59-8 2,5-Dibromotoluene 88% 89% 70-130% Ian 98ofIll QACCMEST. Blank Spike Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample. File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16540-BS BB20725.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 rn The QC reported here applies to the following samples: Method: EPA 504 w M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, o M76251-11, M76251-12, M76251-13, M76251-14 Spike BSP BSP CAS No. Compound ug/l ug/l % Limits 106-93-4 1,2-Dibromoethane 0.071 0.072 101 _' 70-130 CAS No. Surrogate Recoveries BSP Limits 460-00-4 Bromofluorobenzene (S) 1251NO 26-158% 460-00-4 Bromofluorobenzene (S) 122% 26 158% 99 of 111 ®ACCUTE.BT. M76251 Lat=' Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16540-MS BB20726.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 OP16540-MSD BB20727.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 M76326-3 BB20728.1) 1 08/20/08 CZ 08/19/08 OP16540 GBB846 rn The QC reported here applies to the following samples: Method: EPA 504 ja M76251-1, M76251-2, M76251-3, M76251-4, M76251-5, M76251-6, M76251-7, M76251-8, M76251-9, M76251-10, • M76251-11, M76251-12, M76251-13, M76251-14 M76326-3 Spike MS MS MSD MSD Limits CAS No. Compound ug/I Q ug/1 ug/l % ug/1 % RPD Rec/RPD 106-93-4 1,2-Dibromoethane ND 0.071 0.070 99 0.065 92 7 65-135/30 CAS No. Surrogate Recoveries MS MSD M76326-3 Limits 460-00-4 Bromofluorobenzene (S) 1230/6 106°l0 105% 26-158% 460-00-4 Bromofluorobenzene (S) 122% 106% 108% 26-158% 100 of 111 ®ACCUTEST. M76251 —t ro ;o1;e, Volatile Surrogate Recovery Summary Page 1 of 1 .Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b 0 M76251-1 BD20732.D 81.0 ', 90.0 M76251-2 BD20733.D 79 0 88.0 M76251-3 BD20734.D 810 90.0 M76251-4 BD20735.D 83..0:._.__._ 9 1.0 M76251-5 BD20736.1) 80 0 89.0 M76251-6 BD20737.D 82 0 91.0 ............._........_..... . ....__.............._.... M76251-7 BD20738.D 77 0 " 85.0 M76251-8 BD20739.D 80.0 90.0 .............._.._........... M76251-9 BD20740.D 82 0 91.0 ............. .. . ......._.. ....... M76251-10 BD20741.D 82 0. 91.0 M76251-11 BD20742.D M76251-12 BD20743.D 83,0 - 91.0 M76251-13 BD20744.D 74.1107, 89.0 M76251-14 BD20745.D 810 89.0 GBD985-BSD BD20731.D 810 .89.0 GBD985-BSP BD20730.D 79.0 88.0 GBD985-MB BD20729.D '800 89.0 Surrogate Recovery Compounds Limits S1 = 2,5-Dibromotoluene 70-130% (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 ®® 101 of 111 12ACC U EST M76251 Lat'^'atofje- Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M76251 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA [��ethod: EPA 504 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b rn CA M76251-1 BB20729.D 92 0 75.0 M76251-2 BB20731.D 96.01 86.0 M76251-3 BB20732.D .I- 0 103.0 M76251-4 BB20733.D M76251-5 BB20734.D 1.0, 0 �90.0 M76251-6 BB20735.D 106.0 . 89.0 M76251-7 BB20736.D 103 fl 84.0 M76251-8 BB20737.D 104.0. ._ : 84.0 M76251-9 BB20738.D 97 0 , !` 77.0 M76251-10 BB20739.D 410.0 88.0 .................. .. ._......................_ ........................... M76251-11 BB20740.D 104A 89.0 M76251-12 BB20742.D 103.0 88.0 ............._...... ... M76251-13 BB20743.D 9.44 62.0 M76251-14 BB20744.D 99.0 77.0 .............. ... .... OP16540-BS BB20725.D 125.0 122.0 OP16540-MB BB20724.D 121.0 120.0 OP16540-MS BB20726.D 123.0 .`: 122.0 OP16540-MSD BB20727.D 106.0 106.0 Surrogate Recovery Compounds Limits S1 = Bromofluorobenzene (S) 26 158%0. (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 102 of 111 ®ACCUTEST. M76251 =t='' i•r c: ® New England b ACCUTEST b c(a to r 1 F Section 7 — g .......... ......,a_.�...._ f _ lUletals Analysis QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Matrix Spike and Duplicate Summaries • Blank Spike and Lab Control Sample Summaries • Serial Dilution Summaries �® 103 of 111 ®ACLU MBT. M76251 BLANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6O10B Matrix Type: AQUEOUS Units: ug/1 Prep Date: 08'%21/08 0$/21/O9. MB MB Metal RL IDL raw final raw final Aluminum 200 18 Antimony 6.0 1.2 Arsenic 10 .83 am y Barium 200 3.7 am .a Beryllium 4.0 .15 £ Boron 100 .22 Cadmium 4.0 .15 am Calcium 5000 6.3 Chromium 10 .4 am Cobalt 50 .12 Copper 25 1.7 am Gold 50 .91 Iron 100 4.8 Lead 5.0 2 0.30 <5.0 1.1 <5.0 Magnesium 5000 34 Manganese 15 .36 Molybdenum 100 .28 Nickel 40 .15 am Palladium 50 2 Potassium 5000 48 Selenium 10 1.7 am Silicon 100 5.2 Silver 5.0 .53 am Sodium 5000 24 Strontium 10 .18 Thallium 10 .82 Tin 100 .35 Titanium 50 .65 Tungsten 100 5.3 Vanadium 30 .44 Zinc 20 .22 am Associated samples MP12365: M76251-1A, M76251-2A, M76251-3A, M76251-4A, M76251-5A, M76251-6A, M76251-7A, M76251-8A, M76251-9A, M76251-10A, M76251-11A, M76251-12A, M76251-13A, M76251-14A Results < IDL are shown as zero for calculation purposes Page 1 104 of 111 QACCUTEST. M76251 t- K BLANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6010E Matrix Type: AQUEOUS Units: ug/l Prep Date: [Mel (*) Outside of QC limits (anr) Analyte not requested v Page 2 105 of 111 QACCUTEST M76251 MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6O10B Matrix Type: AQUEOUS Units: ug/l Prep Date: 08/21/0,8 08/2.1L08 M76251-10A Spikelot QC M76251-10A QC Metal Original MS MPICP o Rec Limits Original DUP RPD Limits . Aluminum Antimony Arsenic am y Barium am N Beryllium Boron c Cadmium am Calcium Chromium am Cobalt Copper am Gold Iron Lead 4.5 989 1000 98.5 75-125 4.5 5.0 0-20 Magnesium Manganese Molybdenum Nickel am Palladium Potassium Selenium am Silicon Silver am Sodium Strontium -- - Thallium Tin Titanium Tungsten Vanadium Zinc am Associated samples MP12365: M76251-1A, M76251-2A, M76251-3A, M76251-4A, M76251-5A, M76251-6A, M76251-7A, M76251-8A, M76251-9A, M76251-1OA, M76251-11A, M76251-12A, M76251-13A, M76251-14A Results < IDL are shown as zero for calculation purposes Page 1 ®21 106 of 111 QACCLff IEST. M76251 '-=t=rato rlcz . MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6O1OB Matrix Type: AQUEOUS Units: ug/1 Prep Date: - Metal (*) Outside of QC limits (N) Matrix Spike Rec. outside of QC limits (anr) Analyte not requested V IN Page 2 ® 107 of 111 12ACCUTEST. M76251 L_to-sc a � SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/1 Prep Date: 08/121/08 O8/21/08 BSP Spikelot QC BSD Spikelot BSD QC Metal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit Aluminum Antimony Arsenic am V Barium am -► Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper am Gold Iron Lead 974 1000 97...4- '. 80-120 999 1000 99.9 2.5 20 Magnesium Manganese Molybdenum Nickel am Palladium Potassium Selenium am Silicon Silver am Sodium Strontium Thallium Tin Titanium Tungsten Vanadium zinc am Associated samples MP12365: M76251-1A, M76251-2A, M76251-3A, M76251-4A, M76251-SA, M76251-6A, M76251-7A, M76251-8A, M76251-9A, M76251-10A, M76251-11A, M76251-12A, M76251-13A, M76251-14A Results < IDL are shown as zero for calculation purposes Page 1 ®® 108 0f 111 ®ATTEST M76251 t:or .o inc SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97951486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6O10B Matrix Type: AQUEOUS Units: ug/1 Prep Date: Metal (') Outside of QC limits (anr) Analyte not requested W Page 2 �® 109 0f 111 12ACCUTEST. M76251 I a b— --- SERIAL DILUTION RESULTS SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/l Prep Date: 08/.21/08 M76251-10A QC Metal Original SOL 1:5 RPD Limits Aluminum Antimony Arsenic am V Barium am .a Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper am Gold Iron Lead 4.50 O.00 100,0(a) 0-10 Magnesium Manganese Molybdenum Nickel am Palladium Potassium Selenium am Silicon Silver am Sodium Strontium Thallium Tin Titanium Tungsten Vanadium Zinc am Associated samples MP12365: M76251-1A, M76251-2A, M76251-3A, M76251-4A, M76251-5A, M76251-6A, M76251-7A, M76251-8A, M76251-9A, M76251-10A, M76251-11A, M76251-12A, M76251-13A, M76251-14A Results < IDL are shown as zero for calculation purposes Page 1 ME] 110 of 111 ACC U TES7: M76251 I \ `i. 40 SERIAL DILUTION RESULTS SUMMARY Login Number: M76251 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12365 Methods: SW846 6010B Matrix Type: AQUEOUS Units: ug/1 Prep Date: FM, al (*) Outside of QC limits (anr) Analyte not requested (a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL). V A Page 2 / ®Li 111 of 111 ACCU MST. ,r a � SOVEPEIGN CONSULTING August 20,2008 DHL#28656197054 Town of Barnstable Mr. Robert Burgman Town Engineer 230 South Street,4th Fl Hyannis,MA 02601 Re: Soil Sampling Results,July 2008 In Vicinity of: _ Former Shell Branded Gasoline Station#137772 590 Iyannough Road Hyannis,MA Dear Town Engineer: Pursuant to your authorization Sovereign Consulting Inc. personnel collected soil samples from monitoring wells installed in the Iyannough Road Right of Way (R.O.W.), in vicinity of the Former Shell Branded Gasoline Station at 590 Iyannough Road. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH), ethylene-dibromide (EDB), and lead. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVEREIGN CONSULTING,INC. ' cm lvia M. Kirsch Project Manager ' cn Attachments: Laboratory Data Reports Cn _r cc: with attachment Mr.David Weeks,Motiva MassDEP- SERO Sovereign File—EQ872 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan i BWSC 123 This Notice is Related to Release Tracking Number ® 17651 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 590 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Mr. Robert Burgman,Town Engineer 2. Street Address: 230 South Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ✓❑ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. [2]2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. Z 3. Check to indicate if the analytical results are attached. (If item 2. above is checked,the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 590 lyannough Road, Right of Way City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other 3. Description of property where sampling will be/has been conducted: (specify) ❑residential ❑✓ commerical C]industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. Soil from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Sylvia Kirsch Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)399-3200 Email: skirsch@sovcon.com L _ s NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass. oq v/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. e Hardcopy Z 0 Autornated Report i t ®� New England 0.ArcurEssr. o Laboratories ^� ... .... rti: rnv O8/18/()8 i i I t f echn�cal Report for i t Shell Oil SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA j EQ 872 Accutest Job Number: M75286 i i r Sampling Dates: 07/10/08 - 07/14/08 l _ I i i Report to: i Sovereign Consulting skirsch@sovereign.com i i ATTN: Sylvia Kirsch Total number of pages in report: 52 ♦��O iN ACCpROQN a i '. ' L 'o:• Test results contained within this data package meet the requirements Reza Znd of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 i Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) Y...E..A.. R..$ NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE :. r �., ,• This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. I New England 495 Tech Center West Building 1 Marlborough,MA 01752 tel:508-48I-6200 fax:508-481-7753 hap://wmv.acculest.com Q® 1 of 52 13ACCU M= M75286 i i Sections: Table of Contents Section1: Sample Summary .......................................................... Section 2: Case Narrative/Conformance Summary............................... 4 Section 3: Sample Results ....................................................... 11: M75286-1: MW-301D 10-12' 3.2: M75286-2: MW-301D 30-32 O 3.3: M75286-3: MW-302D 10-12' ....... ; .........................................................................•-.... 12 M75286-4: MW-302D 30-32' FAA 3.4 3.5: M75286-5: MW-301S 10-12� ....................................................................................... 15 ............................................................................... 18 j 3.6: M75286-6: MW-301S 30-32' 3.7: M75286-7: MW-302S 30-32' ! Section 4: Misc. Forms ...................... .................................................................................... 24 ...................................................................................... 27 4.1: Chain of Custody ..................................................................................................... . 28 4.2: MCP Form 4.3: VPH Form ....................................... ....................... 30 4.4: Sample Tracking Chronicle 37 ' Section 5: GC `'olatiles QC Data Summaries ............................................................ 5.1: Method Blank Summary .................. ...................................... ............................... 40 5.2: Blank Spike/Blank Spike Duplicate Summary .............................. 5.3: Blank Spike Summary .................................................. 43 5.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 44 5.5: Surrogate Recovery Summaries ......................................................... .. 45 Section 6: Metals Analysis- QC Data Summaries .............................................. . 6.1.: Prep QC MP 12227: Pb ................................. ................................................................ 48 i I ! I � f � EP(Q 2 of 52 taACCUTEST. M75286 -•�- -. Accutest LabLin[c@86833 14:52 18-Aug-2008 j Sample Summary shell oil Job No: M75286 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA l Project No: EQ 872 i Sample Co:J#ected Matrix Client Number Date Time By Received Code Type Sample ID M:732$6 1 : : 07/10/08 10:20SB 07/15/08 SO Soil MW 3111D { 7528fi•L ; 07/10/08 10:45 SB 07/15/08 SO Soil MW 301"D 30 32` l ivI?528fi 3:,' 07/11/08 08:45 SB 07/15/08 SO Soil MW 302D 1fl i2' M75286'`4 07/11/08 09:20 SB 07/15/08 SO Soil MW 302n 30-3V N175286 5 07/14/08 08:50 SB 07/15/08 SO Soil MW-308 10 12'` MM218.6--.6 07/14/08 09:15 SB 07/15/08 SO Soil MW 3015 30 32` IVI75286.7. 07/14/08 10:35 SB 07/15/08 SO Soil MVV-302S 30 3'2' i Soil samples reported on a dry weight basis unless otherwise indicated on result page. I �® 3 of 52 M75286 -a^'a•� �^-s 5 / BUSY , L a b o - a t o r i e s ; SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M75286 Site: SCMAW:97451436(REIMBMA)590 Iyannough Road Hyannis MA Report Date 7/28/2008 2:04:45 PM 7 Sample(s)were collected on between 07/10/2008 and 07/14/2008 and were received at Accutest on 07/15/2008 properly preserved, i at 2.1 Deg.C and intact. These Samples received an Accutest job number of M75286.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. E Except as noted below,all method specified calibrations and quality control performance criteria were met for this job-For more information,please refer to QC summary pages. I Volatiles by GC By Met-iod MADEP VPH REV 1.1 Matrix SO Batch ID: GAB2469 All samples were analyzed within the recommended method holding time. i All method blanks for this batch meet method specific criteria. i e M75286-7:Soil to methanol ratio greater than 1.25 to 1. i Volatiles by GC By Method SW846 8011 Matrix SO Batch ID: OP16319 ® All samples were extracted within the recommended method holding time. m All samples were analyzed within the recommended method holding time- - All method blanks for this batch meet method specific criteria. a Sample(s) M75286-1MS,M75286-IMSD were used as the QC samples indicated. Metals By Method SW846 6010B Matrix SO Batch ID: MP12227 All samples were digested withir the recommended method holding time. i o All samples were analyzed withir.the recommended method holding time. e All method blanks for this batch.meet method specific criteria. i Sample(s) N475333-IDUP,M75333-IMS,M75333-1SDL were used as the QC samples for metals. Only Lead requested. i Wet Chemistry By Method SM21 2540 B MOD. Matrix SO Batch ID: GN26414 I Sample(s) M75299-5DUP were used as the QC samples for Solids,Percent. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this reporgM75286). i Monday,July 28,2008 Page I of 1 ®® 4 of 52 OACCUTEST 1 M75286 ........ ...:.. I I ®® New England 13ACCUTEBT. Fab,,.,toric. Section 3 1 S�tnple results i Report of Analysis i I i i i i i i I I i ®® 5 of 52 ®28�d-rTE3T o r Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page I of ICA Client Sample ID: MW-301D 10-12' Lab Sample ID: M75286-1 Date Sampled: 07/10/08 Matrix: SO-Soil Date Received: 07/15/08 1 Method: MADEP VPH REV 1.1 Percent Solids: 97.4 Project: SCMAW:97451486(REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB44008.1) 1 07/18/08 AP n/a n/a GAB2469 j Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 15.0 g 16.0 ml 100 uI I Run#2 i MA-VPH List t CAS No. Compound Result RL Units Q 71-43-2 Benzene ND .0.28 mg/kg 100-41-4 Eth ]benzene Y 'N`D 0.28 mg/kg 1634-04-4 Methyl Ter(Butyl Ether ND 0.11 mg/kg 91-20-3 Naphthalene ND 0.28 mg/kg 108-88-3 Toluene Np . 0.28 mg/kg m,p-Xylene ND 0.28 mg/kg 95-47-6 o-Xylene ND. 0.28 mg/kg C5-C8 Aliphatics (Unadj.) ND 5.6 mg/kg C9-C12 Aliphatics (Unadj.) ND. 5.6 mg/kg i C9-C10 Aromatics (Unadj.) ND 5.6 mg/kg C5-C8 Aliphatics ND 5.6 mg/kg C9-C12 Aliphatics NE) 5.6 mg/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 108% 70-130% 615-59-8 2,5-Dibromotoluene 1:11'% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 6 of 52 J1A I M75286 '-aFor_•.e•ixs i e a i i Accutest LabLink@86833 14:52 18-Aug-2008 i i Report of Analysis Page I of I i Client Sample ID: MW-301D 10-12' Lab Sample ID: M75286-1 Date Sampled: 07/10/08 Matrix: SO-Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 97.4 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA i File ID DF Analyzed By Prep Date Prep Batch Analytical Batch i Run#1 131320072.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 i Run#2 ' i I Initial Weight Final Volume ! Run#1 30.6 g 50.0 ml Run#2 CAS No. Compound Result RL Units Q i 106-93-4 1,2-Dibromoethane 1V°I3.: 0.0025 mg/kg CAS No. Surrogate Recoveries � Run# 1 Run#2 Limits 460-00-4 Bromolluorobenzene (S) 1;Q7°Lo 61-167% 460-00-4 Bromofluorobenzene(S) 108%0 61-167% i i ND = Not detected J = Indicates an estimated value RL = Reporting Limit B —_ Indicates �analY to found in associated n ethod blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 7 of 52 OACGl.17EST M75286 "ac odes i Accutest LabLink@86833 14:52 18-Aug-2008 i Report of Analysis Page I of 1 Client Sample ID: MW-301D 10-12' Lab Sample ID: M75286-1 Date Sampled: 07/10/08 Matrix: SO-Soil Date Received: 07/15/08 Percent Solids: 97.4 j Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead 2 0 1.9 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B t 5W846 3050E 2 (1)Instrument QC Batch: MA9525 (2) Prep QC Batch:W 12227 I II ' ICI i RL = Reporting Limit �® 8 of 52 13ACCUTEST. M75286 ^? E f f 1 t f i i i Accutest LabLink@8683 14:52 18-Aug-2008 I i Report of Analysis Page I of 1 N Client Sample ID: MW-301D 30-32' Lab Sample ID: M75286-2 Date Sampled: 07/10/08 Matrix: SO-'Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 84.8 Project: SCM_AW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB44009.1) 1 07/18/08 AP n/a n/a GAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 15.6 g 16.0 ml 100 ul Run#2 MA-VPFI List CAS No. Compound Result RL Units Q 71-43-2 Benzene 0.35 mg/kg 100-41-4 Ethylbenzene N'D ''0.35 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.14 mg/kg 91-20-3 Naphthalene N 0.35 mg/kg 108-88-3 Toluene ND 0.35 mg/kg m,p-Xylene 'N?D 0.35 mg/kg 95-47-6 o-Xylene ND 0.35 mg/kg C5-C8 Aliphatics (Unadj.) N^.D:.. 6.9 mg/kg C9-C12 Aliphatics (Unadj.) ND 6.9 mg/kg C9-CIO Aromatics (Unadj.) :ND 6.9 mg/kg C5-C8 Aliphatics ND 6.9 mg/kg C9-C12 Aliphatics ND 6.9 mg/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene :$'1%. 70-130% 615-59-8 2,5-Dibromotoluene 80% 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound i �© 9 of 52 ®ACCIJTEST Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of I N Client Sample ID: MW-301D 3032` I Lab Sample 1D: M75286-2 Date Sampled: 07/10/08 Matrix: SO-Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 84.8 Project: SCMAW:97451486(REIMBMA) 590 Iyannough Road Hyannis MA i File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20073.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight. Final Volume Run#1 30.4 g 50.0 ml Run#2 I CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND. 0.0029 mg/kg CAS No. Surrogate Recoveries Run# I Run#2 Limits i 460-00-4 Bromofluorobenzene (S) 1076/6 61-167% 460-00-4 Brqmofluorobenzene (S) 9.9°l0 61 167% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound i Elul 10 of 52 12AC:Cl TEBT. M7s2ae _ , Y_ ► I I 1 Accutest LabLinkC&86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 v I Client Sample ID: MW-301D 30-32' Lab Sample ID: M75286-2 Date Sampled: 07/10/08 Matrix: SO Soil Date Received: 07/15/08 Percent Solids: 84.8 j Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA j Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <c2`:3:' 2.3 mg/kg 1 07/22/08 07/25/08 EAL SW846 smog t SW846 3050E z (I I (1) Instrument QC Batch: MA9525 (2) Prep QC Batch:MP12227 j i i i I t { i I RL = Reporting Limit ®® 11 of 52 MACCUTE.ST. M75286 i i Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 I Client Sample ID: MW-302D 10-12' ; Lab Sample ID: M75286-3 Date Sampled: 07/11/08 Matrix: SO-Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 97.2 i Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA ; File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB44010.D 1 07/18/08 AP n/a n/a GAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 15.5 g 16.0 ml 100 ui ! Run#2 i MA-VPH List i CAS No. Compound Result RL Units Q 71-43-2 Benzene 0.27 mg/kg 100-41-4 Ethylbenzene IUD :; 0.27 mg/kg j 1634-04-4 Methyl Tert Butyl Ether h1D:: .0.11 mg/kg 91-20-3 Naphthalene 0.521 0.27 mg/kg 108-88-3 Toluene ND 0.27 mg/kg i m,p-Xylene NI) 0.27 m /k g g 95-47-6 o-Xylene -ND. 0.27 mg/kg C5- C8 Aliphatics (Unadj.) NI) 5.5 mg/kg C9-C12 Aliphatics (Unadj.) 5.5 mg/kg C9- C10 Aromatics (Unadj.) 5.5 mg/kg C5-C8 Aliphatics ND 5.5 mg/kg C9-Ci2 Aliphatics 769: 5.5 mg/kg CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene 70-130% 615-59-8 2,5-Dibromotoluene `23°fo 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B Indicates cafes anatyte found in associated method blank. E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 12 of 52 1 UAL Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 w Client Sample ID: MW-302D 10-12' Lab Sample ID: M75286-3 Date Sampled: 07/11/08 ; Matrix: SO-Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 97.2 Project: SCMAW:97451486(REIMBMA) 590 Iyannough Road Hyannis MA i File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20074.D 1 07/23/O8 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume I Run#1 30.5 g 50.0 ml I Run#2 i i CAS No. Compound Result RL Units Q j 106-93-4 1,2-Dibromoethane ND 0.0025 mg/kg CAS No. Surrogate Recoveries Run# I Run#2 Limits 460-00-4 Bromofluorobenzene (S) 115°'0'.: 61-167% 460-00-4 Bromofluorobenzene (S) 119°la :: 61-167% i ND Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound B® 13 of 52 ®ACCUTCr'gT. Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 w Client Sample ID: MW-302D 10-12' Lab Sample ID: M75286-3 Date Sampled: 07/11/08 Matrix: SO-Soil Date Received: 07/15/08 Percent Solids: 97.2 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <2:0 2.0 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B 1 SW846 3050B 2 (1) Instrument QC Batch: IAA9525 (2) Prep QC Batch:MP12227 f i i I i i RL = Reporting Limit Ell 14 of 52 INACC_UTEBT; i M75286 i Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page I of ICA I Client Sample ID: MW-302D 30-32' Lab Sample ID: M75286-4 Date Sampled: 07/11/08 Matrix: SO-Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 88.3 I Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB44011.1) 1 07/18/08 AP n/a n/a GAB2469 Run#2 I Initial Weight Final Volume Methanol Aliquot 1 Run#1 18.2 g 16.0 ml 100 ul j Run#2 I I MA-VPH List CAS No. Compound Result RL Units Q I 71-43-2 Benzene ND 0.28 mg/kg 100-41-4 Ethylbenzene N-D 0.28 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.11 mg/kg 91-20-3 Naphthalene NO 0.28 mg/kg 108-89-3 Toluene N'D . .: 0.28 mg/kg m,p-Xylene ND 0.28 mg/kg 95-47-6 o-Xylene ND 0.28 mg/kg C5- C8 Aliphatics (Unadj.) ND 5.6 mg/kg C9-C12 Aliphatics (Unadj.) '1. 5.6 mg/kg I C9-CIO Aromatics (Unadj.) 46 5.6 mg/kg C5-C8 Aliphatics N>) 5.6 mg/kg C9-C12 Aliphatics ND 5.6 mg/kg CAS No. Surrogate Recoveries Run# I Run#2 Limits I 615-59-8 2,5-Dibromotoluene 85:%0. 70-130% 615-59-8 2,5-Dibromotoluene 87% 70-130% i i i ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound I ®B 15 of 52 ®A e Y Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of I Client Sample ID: MW-302D 30-32' Lab Sample ID: M75286-4 Date Sampled: 07/11/08 Matrix: SO-Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 88.3 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA I I File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 131320075.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 ! Run#2 Initial Weight Final Volume Run#1 30.3 g 50.0 MI. Run#2 I CAS No. Compound Result RL Units Q j i 106-93-4 1,2-Dibromoethane ND 0.0028 mg/kg CAS No. Surrogate Recoveries Run# I Run#2 Limits 460-00-4 Bromofluorobenzene (S) 109% 61-167% 460-00-4 Bromofluorobenzene (S) LOB% 61-167% i i t I i ND = Not detected I J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 16 of 52 13AC r-UTES_ .. M75286 - . .... .... i i I i Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-302D 30-32' I Lab Sample ID: M75286-4 Date Sampled: 07/11/08 Matrix: SO-Soil Date Received: 07/15/08 } Percent Solids: 88.3 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <::Z:2.: 2.2 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B t SW846 3050B z (1) Instrument QC Batch: MA9525 (2) Prep QC Batch: MP12227 I I i I i i I I ; RL = Reporting Limit 17 of 52 ®ACCUITEST Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of I Ln Client Sample ID: MW-301S 10-12' Lab Sample ID: M75286-5 Date Sampled: 07/14/08 Matrix: SO-Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 96.6 Project: SCMAW:97451486 (REIMBMA)590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 A1344012.D 1 07/18/08 AP n/a n/a CAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 16.0 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 0.27 mg/kg 100-41-4 Ethylbenzene NO 0.27 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.11 mg/kg 91-20-3 Naphthalene NO, 0.27 mg/kg 108-88-3 Toluene ND 0.27 mg/kg m,p-Xylene NIi 0.27 mg/kg 95-47-6 o-Xylene ND 0.27 mg/kg CS-C8 Aliphatics (Unadj.) N,Q.. 5.4 mg/kg C9-C12 Aliphatics (Unadj) ND. 5.4 mg/kg C9-CIO Aromatics (Unadj.) ND SA mg/kg C5-C8 Aliphatics ND 5.4 mg/kg C9-C12 Aliphatics ND 5.4 mg/kg '• i i CAS No. Surrogate Recoveries Run# I Run#2 Limits i i 615-59-8 2,5-Dibromotoluene 7.6% 70-130% 615-59-8 2,5-Dibromotoluene 78% 70-130% i I i ND = Not detected J = Indicates an estimated value I RL = Reporting Limit B = Indicates analyle found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 18 of 52 13ACCUTEST. i I Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page I of 1 i Client Sample ID: MW-301S 10-12' Lab Sample ID: M75286-5 Date Sampled: 07/14/08 Matrix: SO-Sod Date Received: 07/15/08 ` Method: SW946 8011 SW846 3550B Percent Solids: 96.6 Project: SCMAW:97451486(REIMBMA) 590 Iyannough Road Hyannis MA I i File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20076.D 1 07/23/08 CZ 07/23/08 OP16319 CBB824 Run#2 Initial Weight Final Volume Run#1 30.6 g 50.0 roll Run#2 ! CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.0025 mg/kg I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 Bromofluorobenzene (S) 11:1% 61-167% 460-00-4 BromoEluorobenzene(S) 119% 61-167% i i ND Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 19 of 52 QAW"MBT. M75266 Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 w g Client Sample ID: MW-301S 10-12' I Lab Sample ID: M75286-5 Date Sampled: 07/14/08 Matrix: SO-Soil Date Received: 07/15/08 Percent Solids: 96.6 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method IIII Lead <Z;0 2.0 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B 1 SW846 3050B Z f (1)Instrument QC Batch:fdA9525 ,Ik (2)Prep QC Batch:MP12227 j i i I I RL = Reporting Limit ffl® 20 of 52 ®ACCU_TEST. Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of I Client Sample ID: MW-301S 30-32' Lab Sample ID: M75286-6 Date Sampled: 07/14/08 Matrix: SO-Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 82.7 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA i File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB44013.1) 1 07/18/08 AP n/a n/a GAB2469 Run#2 i Initial Weight Final Volume Methanol Aliquot i Run#1 18.0 g 16.0 ml 100 ul Run#2 i MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene IU:D 0.32 mg/kg 100-41-4 Ethylbenzene ND' 0.32 mg/kg 1634-04-4 Methyl Ter(Butyl Ether :ND. 0.13 mg/kg 91-20-3 Naphthalene ND; 0.32 mg/kg 108-88-3 Toluene NO. 0.32 mg/kg m,p-Xylene ND. 0.32 mg/kg 95-47-6 o-Xylene ND 0.32 mg/kg C5-C8 Aliphatics (Unadj.) ND 6.4 mg/kg C9-C12 Aliphatics (Unadj.) NI) 6.4 mg/kg C9-C10 Aromatics(Unadj.) N17- 6.4 mg/kg C5-C8 Aliphatics ND 6.4 mg/kg C9-C12 Aliphatics NO 6.4 mg/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 93°l0 70130% 615-59-8 2,5-Dibromotoluene 9:4%0. 70 130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 21 of 52 ®/4CCUTE3T Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of I rn Client Sample ID: MW-301S 30-32' Lab Sample ID: M75286-6 Date Sampled: 07/14/08 Matrix: SO -Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 82.7 Project: SCMAW:97451486 (REIMBMA) 590 Iyannougb Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20078.D 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume j Run#1 30.3 g 50.0 ml Run#2 ' i CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromcethane, ND 0.0030 mg/kg CAS No. Surrogate Recoveries Run# I Run#2 Limits i 460-00-4 Bromofluoro)enzene (S) 102%q 61-167% 460-00-4 BromofluorOenzene (S) 111% 61-167% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound i ®® 22 of 52 �ACCUTE3T. M75286 ••.o._...rios i Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page I of 1 Client Sample ID: MW-301S 30-32' Lab Sample ID: M75286-6 Date Sampled: 07/14/08 j Matrix: SO-Soil Date Received: 07/15/08 Percent Solids: 82.7 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <2 2:::. 2.2 mg/kg 1 07/22/08 07/25/08 EA[. SW846 6010B t SW846 3050B 2 (1) Instrument QC Batch:MA9525 (2) Prep QC Batch: MP12227 i RL = Reporting Limit ®® 23 of 52 M75286 •^'"' ^ ' I Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-302S 30-32' Lab Sample ID: M75286-7 Date Sampled: 07/14/08 Matrix: SO-Soil Date Received: 07/15/08 Method: MADEP VPH REV Li Percent Solids: 85.9 Project: SCMAW:97451486(REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB44014.D 1 07/18/08 AP n/a n/a GAB2469 Run#2 i Initial Weight Final Volume Methanol Aliquot i Run#1 19.4 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND. 0.28 mg/kg 100-41-4 Ethylbenzene ND 0.28 mg/kg 1634-04-4 Methyl Tert Butyl Ether NO 0.11 mg/kg 91-20-3 Naphthalene ND 0.28 mg/kg 108-88-3 Toluene NO 0.28 mg/kg m,p-Xylene NO 0.28 mg/kg 95-47-6 o-Xylene ND 0.28 mg/kg C5-C8 Aliphatics (Unadj.) NO 5.6 mg/kg C9-C12 Aliphatics (Unadj.) NO 5.6 mg/kg C9-C10 Aromatics (Unadj.) NO 5.6 mg/kg C5-C8 Aliphatics NO 5.6 mg/kg C9-C12 Aliphatics ND. 5.6 mg/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 72% 70-130% 615-59-8 2,5-Dibromotoluene ':72%0 70-130% (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound E �® 24 of 52 M75286 1 i i Accutest LabLink@86833 14:52 18-Aug-2008 1 i Report of Analysis Page 1 of 1 i Client Sample ID: MW-302S 30-32' Lab Sample ID: M75286-7 Date Sampled: 07/14/08 Matrix: SO-Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 85.9 Project: SCMAW:97451486(REIMBMA) 590 Iyannough Road Hyannis MA i File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 131320079.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume Run#1 30.6 g 50.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibronioethane NO: 0.0029 mg/kg CAS No. Surrogate Recoveries Run# I Run#2 Limits 460-00-4 Bromofluorobenzene(S) 100% 61-167% 460-00-4 Bromofluorobenzene (S) ION. 61-167% I i ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 25 of 52 UAL M75286 '-4`"�'�- Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of I y Client Sample ID: MW-302S 30-32' Lab Sample ID: M75286-7 Date Sampled: 07/14/08 Matrix: So-SoiI Date Received: 07/15/08 Percent Solids: 85.9 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method i Lead 2.1 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B t SW846 3050E 2 (1) Instrument QC Batch: MA9525 (2)Prep QC Batch:MP12227 RL = Reporting Limit �® 26 of 52 � r ' New England ��* 12Accur>rs: Section 4 T " n...: :€t{. Y'tt6 t :ettzs t.iv . ;1Vhsc Forms:...: ; i Custody Documents and Other Forms i Includes the following where applicable: • Chain of Custody r MCP Form r VPH Form • Sample Tracking Chronicle I i i I �® 27 of 52 UAC CUMST. M75286 LAB(LOCATIoN) Shell Oil Products Chain Of Custody Record Please Check A ro date Box- Print Bill To Contact Name: INCIDENT#(ENV SERVICES) ❑oaac IF to woes 0 uvtn5 Q FN'/.58lNQi ❑NDTNA REfA0. ❑AIflLRETALL o IgiIVA meat _9_FgK 11 b DATE: - l QmISATNn QNsa PO III SAP# O orRel c ❑s+al PtvaRr� {7 anle( PAGE: , a J 1HE ali6 aDn4 fay..l dq rMwW: SU MAn A R 97bg %--1j ue uaEDNLr DAYsx c S tA,�. L�t m A D(110Ah ❑SDAYS ❑)OAvS 0=114M OHM" REQUESTED ANALYSIS IEAW9UTURE ON RECEIPT Ctebfl ?Caola'It i •Ctdern SPECIAL INSTRUCTIONS OR NOTES: SAMP RG rvaer.ATln Field Sample Identification DATE TIME WiWt cropf. 7 n ' aPII p C.W-,P(D R-dRpt Aa w.o ea�c oT.cn a Ltbol tary Nate ' f I IL(w •L A = 0 3o t It I 1 I Y � a 1 4P ✓IS:pn.uM l 0.` .RMw•OMIAw•I-.I e lam( 7 f,S�cJ ��D E-7 N-lo ck M75286: Chain of Custody Page I of 1 I I i i ®® 28 of 52 j ��CLJ7'ES_T. Nf75286 Massachusetts Department BWSC-CAM Exhibit V11 A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 A IV Title: MADEP MCP Response Action Analytical Report Certification Form i i Laboratory Name: Accutest Laboratories of New England Project#: M75286 , Project Location: SCMAW:97451486(REIMBMA)590 lyannough Road MADEP RTN [None Hyannis MA This form provides certifications for the following data set: M75286-1,M75286-2,M75286-3,M75286-4,M75286-5,M75286-6,M75286-7 Test method:SW846 8011,SM21 2540 B MOD,and below Sample Matrices: Groundwater SoillSediment X Drinking Water () Other: () {) 82606 8151A 8330 6010B X 7470A/1A a• 8270C ( 8081A VPH(X) 6020 9014M 2 A 8082 8021E (} EPH 7000 S s {) 7196A An affirmative response to questions A,B,C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with 2 Yes ❑ No' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and Yes ❑No' discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty',as described in Section 2.0(a),(b),(c)and R Yes []No ' (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without 0 Yes ❑No ' significant modifications,as specified in Section 11.3? A response to questions E and Fbelow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the El Yes ❑ No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified ❑ Yes ' No ` method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. 1 the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is, to the best of my knowledge and belief,accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 07/28/2008 ®© 29 of 52 A® CCll'TEST • r MADEP VPH FORM Soil lla�rlx Aqueous F Sediment F 1 Other ' Satisfactor hip Broken Leaking es:T :at :0s N/A v H< 2 ;_i PH>2 - '==may,: Received on Ice Received at 4 De .C FI Other ✓ Reed at 2.1 deg C ��� Methanol Coverin 'Soil. mL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301D 10-12' Lab ID: M75286-1 t,W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/1 012 0 0 8 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene NIA 7/18/2008 N/A FID: 2.5-Dibromotoluene %Solids: Low Dilution: High Dilution: 97.4 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q I CS-C8 Aliphatics(Unadj.) N/A mg/kg ND x 5.6 i C9-C10 Aromatics(Unadj.) NIA mg/kg ND' 5.6 C9-C12 Aliphatics(Unadj.) N/A mg/kg ND" 5.6 i Target Analytes Ethylbenzene 100-01-4 C9-C12 mg/kg ND 0.28 Toluene 108-88-3 C5-C8 mg/kg ND 0.28 Methyl Tert Butyl Ether 1634-04A C5-08 mg/kg ND 0.11 Benzene 71.43-2 C5-C8 mg/kg ND 0.28 Naphthalene 91-20-3 N/A mg/kg ND 0.28 o-Xylene 9547-6 C9-C12 mg/kg NO 0.28 m,p-Xylene C9-C12 mg/kg ND 0.28 Adjusted Ranges C5-C8 Aliphatics N/A mg/kg ND' 5.6 C9-C12 Aliphatics NIA mg/kg ND` 5.6 _. .. __ . Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene °/, 108 70-130% PID:2,5-Dibromotoluene % 111 70-130 Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude:he concentration of Target Analytes eluting in that fangs. c Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude cons of Target Analyzes eluting in that range AND concentration of C9-ClO Aromatic Hydrocarbons, Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? �!=Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? !;Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 ®® 30 of 52 i GACCUMST_. M75288 • P MADEP VPH FORM Mali0. ",--Aqueous Soil lv Sediment F': Other Satisfactor W Broken Leaking i 0100 a,arN N/A W PH<=2 DH>2 �l Received on Ice l Received at 4 De a.C - Other ;✓i Rec'd at2.1 deg C Methanol Coverin Soil. mL Methanol/ soil: 1:1 +/-25% A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301D 30-32' Lab ID: M75286-2 W Method for Target Analyles: MADEP VPH REV 1.1 Date Collected: 7/10/2008 Date Received: 7/1 512 0 0 8 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 84.8 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) WA mglkg ND x 6.9 C9-C10 Aromatics(Unadj.) N/A mg/kg NO' 6.9 C9-C12 Aliphatics(Unadj.) N/A mg/kg ND x 6.9 Target Analyles Ethylbenzene 10041-4 C9-C12 mg/kg NO 0.35 Toluene 108-88-3 C5-C8 mg/kg NO 0.35 Methyl Tert Butyl Ether 1634-044 G5-C8 mg/kg NO 0.14 Benzene 7143-2 C5-C8 mg/kg NO 0.35 Naphthalene 91-20-3 N/A mg/kg NO 0.35 o-Xylene 95-47-6 C9-C12 mg/kg NO 0.35 m,p-Xylene C9-C12 mg/kg NO 0.35 Adiusted Ranges C5-C8 Aliphatics N/A mg/kg NO' 6.9 C9-C12 Aliphatics NIA mg/kg NO' 6.9 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID.2,5-Dibromotoluene % 80 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)andrar internal standards eluting in that range B 'Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analyles efuling in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analyles eluting in that range AND concentration of C9-Cl0 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? CYes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes f`! No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 141No U Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 Egli 31 of 52 ®Act_ BT. . 1 M75286 - _ MADEP VPH FORM A ueous r Soil Sediment I i Other Satisfactory Broken i7Leaking r se N/A PH<=2 1 PH>2 r if Received on Ice 11 Received at 4 Deg.C F1 Other WI Rec'd at 2.1 deg C w' .. '�._. := Methanol Coverin Soil. mL Methanol! soil: 1:1 +/-25% p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-302D 10-12' Lab ID: M75286-3 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/11/2008 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 NIA FID: 2,5-Dibromotoluene %Solids: Low Dilution: Nigh Dilution: 97.2 1 NIA Unadiusted Ranges CAS# Elution Range Units Result RDL Q I C5-C8 Aliphatics(Unadj.) N/A mglkg ND' 5.5 C9-C10 Aromatics(Unadj.) NIA mg/kg 10.6" 5.5 C9-C12 Aliphatics(Unadj.) N/A mg/kg 18.2" 5.5 Target Analytes Ethylbenzene 10041-4 C9-C12 mg/kg NO 0.27 Toluene 108-88-3 C5-C8 mg/kg NO 0.27 Methyl Tert Butyl Ether 1634-04-4 C5-C8 mg/kg NO 0.11 Benzene 71-43-2 C5-C8 mg/kg ND 0.27 Naphthalene 91-20-3 NIA mglkg 0.521 0.27 o-Xylene 95-47-6 C9-C12 mg/kg NO 0.27 m,p-Xylene C9-C12 mg/kg ND 0.27 Adjusted Ranges CS-C8 Aliphatics N/A mg/kg ND' 5.5 C9-C12 Aliphatics N/A mg/kg 7.69` 5.5 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 119 70-130 PID:2,5-Dibromotoluene % 123 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogale(s)and/of internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogale(s)andlor internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations w any surrogale(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons_ Z A V'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? CiYes El No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? LYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? f 1No I_! Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature —� Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 �® 32 of 52 ��catr>Es-r. MADEP VPH FORM Mirl�c r t A ueous Fi Soil Sediment Other '] `cfatoeFs - Satisfactory W! Broken i i Leaking ai P eserar e."s': NIA ✓ PH—2 i > - �.:-,_ . Received on Ice F., Received at 4 Deg.C + Other �i Rec'd at 2.1 deg C Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% 4%, Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-302D 30-32' Lab ID: M752864 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/11/2008 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 WA i FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 88.3 1 WA Unadjusted Ranges CAS# Elution Range Units &RUa RDL Q C5 CB Aliphatics(Unadj.) N/A mg/kg ND" 5.6 C9-C10 Aromatics(Unadj.) N/A mg/kg ND" 5.6 i C9-C12 Aliphatics(Unadj.) N/A mglkg ND' 5.6 r i Target Analytes Ethylbenzene 100-41-4 C9-C12 mg/kg ND 0.28 Toluene 108-88-3 C5-C8 mg/kg ND 028 Methyl Tert Butyl Ether 1634-044 C5-C8 mg/kg ND 0.11 i Benzene 71-43-2 C5-C8 m91kg ND 0,28 Naphthalene 91-20-3 NIA mg/kg ND 0.28 j o-Xylene 9547-6 C9-C12 mg/kg ND 0.28 i m,p-Xylene C9-C12 mg/kg ND 0.28 Adjusted Ranges C5-C8 Aliphatics NIA mg/kg ND' 5.6 C9-C12 Aliphatics NIA mg/kg ND` 5.6 i - -. Surrogate Recoveries Acceptance Range FID2,5-Dibromotoluene % 85 70-130% PID:2,5-Dibromotoluene % 87 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogates)andlor internal standards eluting in that range e Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards elating in that range. CSC8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)arid/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclutle cone of Target Analytes eluting in that range AND concentration of C9-ClO Aromatic Hydrocarbons, Z A'Squalifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? F Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? i No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete- Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 �® 33 of 52 ®AC:CdJ7'-- M752ss MADEP VP H FORM Aqueous Soil ii Sediment n Other Satisfactor W Broken Leaking r- s f N/A W nH<_2 H>2 f - Te '" Received on Icei Received at 4 De a. C Other W., Rec'd at 2.1 deg C Methanol Coverin_q Soil. mL Methanol/ soil: 1:1 +/_25% A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301S 10-12' Lab ID: M75286-5 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/14/2008 Date Received: 7/15/2008 i VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-0ibromotoluene N/A 7/18/2006 N/A I FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 96.6 1 N/A l i Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A mg/kg ND* 5.4 C9-C10 Aromatics(Unadj.) N/A mg/kg ND' 5.4 _ i C9-C12 Aliphatics(Unadj.) WA mg/kg 9 9 ND' 5.4 Target Analytes ; I Ethylbenzene 100-41A C9-C12 mg/kg ND 0.27 Toluene 108-88-3 C5-C8 mg/kg ND 0.27 i Methyl Tert Butyl Ether 1634-04A C5-C8 mg/kg ND 0.11 Benzene 71-43-2 C5-C8 mg/kg ND 0.27 i Naphthalene 91-20-3 NIA mg/kg ND 0.27 o-Xylene 95-47-6 C9-C12 mg/kg ND 0.27 m,p-Xyiene C9-C12 mg/kg ND 0.27 Adjusted Ranges C5-C8 Aliphatics NIA mg/kg ND" 5.4 C9-C12 Aliphatics N/A mg/kg ND' 5.4 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 76 70 130 PID:2,5-Dibromotoluene % 78 70-130 Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range j 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concenhation of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C 12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons, Z A'Squalifier indicates an estimated value I Were all QA/QC procedures REQUIRED by the VPH Method followed? ✓..Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 'V'Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? V No Yes-Details Attatched 1 attest under the pains and penalties of perpury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature ���- Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 ®® 34 of 52 13ACCUTEST i MADEP VPH FORM ueous F, Soil I✓! Sediment I; Other tar >°ry� :. Satisfactor f�, Broken Leaking o l; ieserr_. fS N/A �I H<=2 PH>2 t1Ce Received on Ice Received at 4 Deg.C iii Other Rec'd a12.1 deg C v= `> Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% j Method for Ranges: MADEP VPH REV 1A Client ID: MW-3015 30-32' Lab ID: M75286-6 w j Method for Target Analytes: MADEP\,PH REV 1.1 Date Collected: 7/14/2008 Date Received: 7/15/2008 VPH Surrogate Standards 9 Date Extracted: First Date Run: Last Date Run: i PID: 2,5-Dibromotoluene WA 7/1812008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: j 82.7 1 NIA i Unadiusted Ranges CAS# Elution Range Units Result RDL (3 j C5-C8 Aliphatics(Unadj.) N/A mg/kg ND' 6.4 C9-C10 Aromatics(Unadj.) NIA mg/kg ND" 6.4 C9-C12 Aliphatics(Unadi.) NIA mg/kg ND" 6.4 Target Analytes i Ethylbenzene 100-41-4 C9-C12 mg/kg ND 0.32 Toluene 108-88-3 C5-C8 mglkg ND 0.32 { Methyl Tert Butyl Ether 1634-04-4 C5-C8 mglkg ND 0.13 Benzene 71-43-2 C5-C8 mg/kg ND 0.32 Naphthalene 91-20-3 NIA mg/kg ND 0.32 o-Xylene 95-47-6 C9-C12 mg/kg ND 0.32 m,p-Xylene C9-C12 mg/kg ND 0.32 Adiusted Ranges C5-C8 Aliphatics NIA mg/kg ND' 6.4 C9-C12 Aliphatics N/A mg/kg ND' 6.4 Surrogate Recoveries Acceptance Range FID2,5-Dibromotoluene %, 93 70-130 PID:2,5-Dibromotoluene '/ 94 70-130 Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards eluting In that range e Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards etuting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analyles eluting in that range. C Hydrocarbon Range data exclude concentrations of.any surrogate(s)andior internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Anatyies eluting in that range AND cor.centration of C9-C10 Aromatic Hydrocarbons. 2 A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? RlYes r i No-Details Attatched Were all performance/acceptance standards for required QAlQC procedures achieved? W Yes 0 No-Details Attatched Were any significant modifications made to tie VPH method,as specified in Sect.11.39 i./jNo F.l: Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 ®® 35 of 52 eAMUMEST l MADEP VPH FORM WIWI r���?�=� Aqueous ;l Soil io Sediment Other Q a Satisfactory w Broken i Leakin j -i N/A PH—2 ' _i PH>2 Received on Ice r Received at 4 De .C I Other Rec'd at 2.1 deg C 7. 9-W. ——.,- Methanol Covering Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. P. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-302S 30-32' Lab ID: W5286-7 ca Method for Target Analytes: MADEP VPH REV 1-1 Date Collected: 711412008 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene WA 7/18/2008 N/A F1D: 2,5-Dibromotoluene %Solids: Law Dilution: High Dilution: i 85.9 1 N/A I Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) WA mg/kg ND' 5.6 I i C9-C10 Aromatics(Unadj.) N/A mg/kg ND' 5.6 C9-C12 Aliphatics(Unadj.) N/A mg/kg ND' 5.6 j Target Analytes i Ethylbenzene 100-41-4 C9-C12 mg/kg ND 0.28 Toluene 108-88-3 C5-C8 mg/kg ND 0.28 Methyl Tert Butyl Ether 1634-04A C5-C8 mglkg ND 0.11 Benzene 71A3-2 C5-C8 mg/kg ND 0.28 Naphthalene 91-20-3 N/A mglkg ND 0.28 o-Xyiene 95-47-6 C9-C12 mg/kg ND 0.28 m,p-Xylene C9-C12 mg/kg ND 0.28 Adjusted Ranges C5-C8 Aliphatics N/A mg/kg ND' 5.6 C9-C12 Aliphatics N/A mg/kg ND' 5.6 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene e/ 72 70-130% PiD:2,5-Dibromotoluene % 72 70-130 Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range- C Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C 10 Aromatic Hydrocarbons, Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes I-.. No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? CYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? L0 No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 ®® 36 of 52 �A�CU7E3T M75286 •a- r P' r' i Accutest Laboratories i i Internal Sample Tracking Chronicle A Shell Oil Job No: M75286 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 ? Sample Number Method Analyzed By Prepped By Test Codes NOR 11 i a -.r._. a ........�- ..r....a •,...3e-''Ta ... "'l. a�3�_ �` ems;,:.:• a',�i'-� 3 _ z x n' �'' M75286-1 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-1 MADEP VPH REV 1.118-JUL-08 18:21 AP VMAVPH M75286-1 SW846 8011 23-JUL-08 16:25 CZ 23-JUL-08 FG V8011EDB M75286-1 SW846 6010B 25-JUL-08 18:51 EAL 22-JUL-08 EAL PB i .•.o.�e _.:..,_. -.r...... ....r.... .sEr.: -*- 'der;ate S ex t 4r = GzFk��t.� .. :- -..r- .� , M75286-2 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-2 MADEP VPH REV 1.1 18-JUL-08 19:04 AP VMAVPH M75286-2 SW846 8011 23-JUL-08 16:54 CZ 23-JUL-08 FG V8011EDB M75286-2 SW846 6010E 25-JUL-08 18:57 EAL 22-JUL-08 EAL PB - M75286-3 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-3 MADEP VPH REV 1.118-JUL-08 19:46 AP VMAVPH M75286-3 SW846 8011 23-JUL-08 17:24 CZ 23-JUL-08 FG V8011EDB M75286-3 SW846 6010B 25-JUL-08 19:03 EAL 22-JUL-08 EAL PB "Ful, M75286-4 SM21 2540 B MOD. . 16-JUL-08 WC %SOL M75286-4 MADEP VPH REV 1.118-JUL-08 20:29 AP VMAVPH M75286-4 SW846 8011 23-JUL-08 17:53 CZ 23-JUL-08 FG V8011EDB M75286-4 SW846 6010B 25-JUL-08 19:08 EAL 22-JUL-08 EAL PB iS cc-:•. rye["-@t-,7' n �a,"u�.. �a-,�-- �,�"�,�•-�'� h ± � �.�.Vetl ��""`t70 ys„ ��A1' � M75286-5 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-5 MADEP VPH REV 1.118-JUL-08 21:11 AP VMAVPH M75286-5 SW846 8011 23-JUL-08 18:22 CZ 23-JUL-08 FG V8011EDB M75286-5 SW846 6010B 25-JUL-08 19:14 EAL 22-JUL-08 EAL PB Page 1 of 2 ®® 37 of 52 12ACCLlTEST. a75286 Accutest Laboratories Internal Sample Tracking Chronicle A Shell Oil Job No: M75286 ; SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes I M75286-6 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-6 MADEP VPH REV I.1 18-JUL-08 21:54 AP VMAVPH M75286-6 SW846 8011 23-JUL-08 19:21 CZ 23-JUL-08 FG V8011EDB j M75286-6 SW846 6010B 25-JUL-08 19:19 EAL 22-JUL-08 EAL PB M75286-7 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-7 MADEP VPH REV 1.1 18-JUL-08 22:37 AP VMAVPH M75286-7 SW846 8011 23-JUL-08 19:50 CZ 23-JUL-08 FG V8011EDB M75286-7 SW846 6010B 25-JUL-08 19:25 EAL 22-JUL-08 EAL PB i i i i Page 2 of 2 t ®� 38 of 52 ®ACGUT_JSST. M75286 _+" loll New England 12ACCU-rlEs�: Section 5 .... ..._.. I-44 T.IS-E ti f{-E M L 8:r h v.. GC V61atiles i QC Data Summaries i i Includes the following where applicable: I • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries I i i ®B 39 of 52 MACCUTEST. M75286 • 9 Method Blank Summary Page I of I Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2469-MB AB44005.D 1 07/18/08 AP n/a n/a GAB2469 rr The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 CAS No. Compound Result RL Units Q 71-43-2 Benzene sNI) 250 ug/kg 100-41-4 Ethylbenzene ND 250 ug/kg 1634-04-4 Methyl Ter(Butyl Ether ND 100 ug/kg 91-20-3 Naphthalene N..D 250 ug/kg 108-88-3 Toluene NJp 250 ug/kg m,p-Xylene ND 250 ug/kg 95-47-6 o-Xylene ND 250 ug/kg C5-C8 Aliphatics (Unadj.) NO 5000 ug/kg C9-C12 Aliphatics (Unadj.) Nl) 5000 ug/kg C9-C10 Aromatics (Unadj.) ND 5000 ug/kg C5-C8 Aliphatics ND 5000 ug/kg C9- C12 Aliphatics ND 5000 ug/kg CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene .ot% 70-130% 615-59-8 2,5-Dibromotoluene 100.% 70-130% i E® 40 of 52 13ACCLII EB 1. M75286 L 411^= 1� .-+ l Method Blank Summary Page 1 of I Job Number: M75286 Account. SHELLIAW Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16319-MB BB20067.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 The QC reported here applies to the following samples: Method: SW846 8011 M75286-1, M75286-2, M75286-3, M75286-4, M75286-5,M75286-6, M75286-7 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane -N;ID 2.5 ug/kg CAS No. Surrogate Recoveries Limits 460-00-4 Bromofluorobenzene(S) 11.0% 61-167% 460-00-4 Bromofluorobenzene(S) 129% 61-167% �® 41 of 52 ®A Blank Spike/Blank Spike Duplicate Summary Page 1 of i Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 lyannough Road Hyannis MA Sample Fife ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2469-BSP AB44006.D 1 07/18/08 AP n/a n/a GAB2469 GAB2469-BSD AB44007.1) 1 07/18/08 AP n/a n/a GAB2469 CA N The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 Spike BSP BSP BSD BSD Limits CAS No_ Compound ug/kg ug/kg % ug/kg % RPD Rec/RPD 71-43-2 Benzene 2500 2570 103 2580 103 0:. 70-130/25 100-41-4 Ethylbenzene 2500 2630 P6 2640 1306 0 70-130/25 1634-04-4 Methyl Tert Butyl Ether 2500 2670 107 2640 =1106 1 70-130/25 91-20-3 Naphthalene 2500 2650 106 2670 107 t 70-130/25 108-88-3 Toluene 2500 2580 193 2570 103 0 70-130/25 m,p-Xylene 5000 5310 10,6 5340 107 1 70-130/25 95-47-6 o-Xylene 2500 2590 1.04 2600 104 0 70-130/25 C5- C8 Aliphatics (Unadj.) 7500 7440 99 7490 100 1 70-130/25 C9- C12 Aliphatics (Unadj.) 7500 7180 96 7270 97 1 70-130/25 C9-C10 Aromatics(Unadj.) 2500 2600 103 2600 104 0 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 10.0% 101% 70-130% 615-59-8 2,5-Dibromotoluene 99% 100% 70-I30% F 42 of 52 13AC CUT'ESI: Blank Spike Summary Page I of I .fob Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch i OP16319-BS BB20069.D 1 07/23/08 CZ O7/23108 OP16319 GBB824 i i N i W i The QC reported here applies to the following samples: Method: SW846 8011 i M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 Spike BSP BSP CAS No. Compound ug/kg ug/kg % Limits 106-93-4 1,2-Dibromoethane 32.9 37.7 11:5:. 56-140 CAS No. Surrogate Recoveries BSP Limits ' I I 460-00-4 Bromofluorobenzene (S) 11.8% 61-167% 460-00-4 Bromofluorobenzene (S) I37%o 61-167% i i� i 43 of 52 t3AC i7: M75286 - A Matrix Spike/Matrix Spike Duplicate Summary Page I of I Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16319-MS BB20070.D 1 07/23/08 CZ 07/23/08 OP16319 GBB824 OP16319-MSD BB20071.D 1 07/23/08 CZ 07/23/08 OP16319 GBB824 M75286-1 BB20072.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 �p i The QC reported here applies to the following samples: Method: SW846 8011 i M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 M75286-1 Spike MS MS MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD I 106-93-4 1,2-Dibromoethane ND 33.5 36.2 10:8" 33.3 99 8 48-141/27 CAS No. Surrogate Recoveries MS MSD M75286-1 Limits 460-00-4 Bromofluorobenzene (S) 114%0 109% 107% 61-167% 460-00-4 Bromofluorobenzene (S) 136% 11.9%... 108%ti 61-167% II ®� 44 of 52 13AC IITEST. W 5286 I Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: SO Samples and QC shown here apply to the above method vti Lab Lab Sample ID File ID S1 a S1 b M75286-1 AB44008.D 1.:0&4. 111.0 M75286-2 AB44009.D 81<0 ::80.0 M75286-3 A1344010.1) 1-190` 123.0 M75286-4 AB4401.1.D 87.0 M75286-5 AB44012.13 7&D:;`- 78.0 M75286-6 AB44013.D 94.0 M75286-7 AB44014.D T.2 - 72.0 GAB2469-BSD AB44007.D ;101 0 100.0 GAB2469-BSP AB44006.1) I00':U': . 99.0 GAB2469-MB AB44005.D 10:1::0`: 100.0 i Surrogate Recovery Compounds Limits SI = 2,5-Dibromotoluene 70-130% (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 I i ®® 45 of 52 Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: SW846 8011 Matrix: SO Samples and QC shown here apply to the above method Lab Lab to Sample ID File ID Sl a S1 b M75286-1 BB20072.1) '107.0 . 108.0 M75286-2 BB20073.D 1670 99.0 M75286-3 BB20074.D 115.() 119.0 M75286-4 BB20075.D 104.0 .. 106.0 M75286-5 BB20076.D 1 .1.0 . 119.0 M75286-6 BB20078.D 3Q20; 111.0 M75286-7 BB20079.D 1`00 0: 107.0 OP16319-BS BB20069.D 137.0 OP16319-MB BB20067.1) 40::0 129.0 OP16319-MS BB20070.1) 114;0 136.0 OP16319-MSD BB20071.1) Io90 119.0 Surrogate Recovery Compounds Limits I S 1 = Bromofluorobenzene (S) 0 167%0 (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 46 of 52 � Qa►C.CLJ7'ES_T_. M75286 =+•� - 'tec I a � n i ®® New England ' ®ACt �dTEST 10 - Sect.loti 6 _...__. __ ......_.. `:7 S`T.`5 Af:.t IN. TNE" ¢NrT1.2'$"P 3tY i 1 i i Metals Analysis QC Data Summaries i Includes the following where applicable: • Method Blank Summaries • Matrix Spike and Duplicate Summaries • Blank Spike and Lab Control Sample Summaries • Serial Dilution Summaries i i Egli 47 of 52 QACGt.J'tE8"r M75286 _�_or•tc•ie: 0LANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: M75286 Account: SHELLWIC - Shell Gil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12227 Methods: SW846 6010E Matrix Type: SOLID Units: mg/kg Prep Date: 07/22/68 MB Metal R1 IDL raw final Aluminum 20 1.9 Antimony 2.0 .14 �► Arsenic 2.0 .074 am • Barium 20 .086 am Beryllium 0.40 .025 I Boron 10 .17 Cadmium 0.40 .022 am " Calcium 500 .66 Chromium 1.0 .03 am Cobalt 5.0 .061 I Copper 2.5 .081 Iron 10 .63 Lead 2.0 .092 -0.080 <2.0. Magnesium 500 ,66 Manganese 1.5 .024 Molybdenum 10 .022 Nickel 4.0 .047 Potassium 500 .55 _. Selenium 2.0 .1 am Silver 0.50 .031 am - Sodium 500 8 Strontium 1.0 .017 Thallium 2.0 _27 - Tin 10 .13 Titanium 5.0 .031 Tungsten 10 .093 vanadium 3.0 .035 Zinc 2.0 .036 Associated samples MP12227: -475266-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 Results < IDL are shown as zero for calculation purposes (') Outside of QC limits (anr) Analyte not requested I Page 1 ®® 48 of 52 2AC__CLJTEST MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY - - Login Number: M75286 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBt4A) 590 Iyannough Road Hyannis MA ) QC Batch ID: MP12227 Methods: SW846 6O10B j Matrix Type: SOLID Units: mg/kg j Prep Date: 07/22/08 07/22/02 i I M75333-1 S ikelot QC P� QC M75333-1 � Metal Original MS MPTCP g Rec Limits Original DUP RPD Limits Aluminum Antimony a Arsenic am l Barium am - ) Beryllium Boron Cadmium am Calcium Chromium am - i Cobalt i Copper Iron i Lead 2.6 88.2 104 82.1 75-125 2.8 2.7 3.6 0-20 Magnesium Manganese Molybdenum Nickel i Potassium Selenium am } Silver am Sodium Strontium Thallium Tin Titanium Tungsten _ Vanadium " Zinc Associated samples MP12227: M75286-1, M75286-2, M75266-3, M75286-4, M75286-5, M75286-6, 1175286-7 Results < IDL are shown as zero for calculation purposes (') Outside of QC limits (N) Matrix Spike Rec. outside of QC limits (anr) Analyte not requested i Page 1 ®® 49 of 52 ®ACcArrEsT_ . M7 :5286 -" . n r i+ SPIKE BLANK AND LAB CONTROL SAMPLE SUI-24ARY i Login Number: M75286 j Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA I QC Batch ID: MP12221 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg Prep Date: 0.7/22/08 07/22/OB i BSP Spikelot QC BSD Spikelot BSD QC i Metal Result MPICP % Rec Limits Result MPICP 8 Rec RPD Limit ! Aluminum t Antimony .a i W ) Arsenic am ! i Barium am Beryllium Boron E Cadmium am j - j Calcium Chromium am Cobalt .. i i Cooper Iron Lead 92.4 I00 92.4 80-120 90.3 LOO 90.3 2.3 20 Magnesium Manganese Molybdenum Nickel Potassium i ! Selenium am Silver am Sodium Strontium Thallium i Tin Titanium Tungsten Vanadium Zinc Associated samples MP12227: M75286-1, M75286-2, M75286-3, M75286-4, M752R6-5, M75286-6, M75286-7 Results < IDL are shown as zero for calculation purposes 1') Outside of OC limits (anr) Analyte not requested - Page 1 ©® 50 of 52 M75286 1 y ,:o SPIKE BLANK AND LAB CONTROL SA14PLS SUMMARY Login Number: M752B6 Account: SHELLWIC - Shell Oil Pro_ect: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12227 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg Prep Date: 07/22/08 i LCS Spikelot QC i Metal Result MPLCS60 % Rec Limits i Aluminum a7 Antimony W i Arsenic ant Elm Barium am • 12 Beryllium - Boron Cadmium am Calcium 1 Chromium am Cobalt i I Copper Iron i Lead 167 163 99.4 82-118 1. Magnesium Manganese Molybdenum Nickel i Potassium 1 i Selenium am i Silver am Sodium i Strontium I Thallium Tin Titanium Tungsten Vanadium I Zinc Associated samples MP12227: 1475286-1, M75286-2, M75286-3, M75296-4, M75286-5, 1475286-6, M75286-7 Results < IDL are shown as zero for calculation purposes (') Outside of QC limits i (anr) Analyte not requested i Page 2 ®Q 51 of 52 UACC_ UTEST. SERIAL DILUTION RESULTS SUMMARY i Login Number: M75286 Account: SHELLWIC —Shell oil j Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12227 methods: SW896 6010E ! Matrix Type: SOLID Units: ug/l Prep Date: 07122/08. M75333-1 QC Metal Original SDL 1:5 RPD Limits Aluminum - . 61 � Antimony .a i ,p Arsenic am Barium am o i Beryllium .... I' Boron Cadmium am Calcium i Chromium am Cobalt i Copper - Iron Lead 27.4 29.5 7,7 0-10 Magnesium Manganese i Molybdenum - Nickel Potassium Selenium am Silver am Sodium Strontium Thallium Tin Titanium Tungsten Vanadium Zinc Associated samples MP12227:. M75286-1, M75286-2, 1175286-3, M75286-4, M75286-5, 1475286-6, 1-75286-7 Results < IDL are shoran as zero for calculation purposes (') Outside of QC limits (anr) Analyte not requested Page 1 Egli 52 of 52 �a M75286 SOVEREIGN CONSULTING August 20,2008 DHL#28656624651 Ms. Donna Miorandi Town of Barnstable,Health Inspector 200 Main Street Hyannis,MA 02601 Re: Soil Sampling Results,July 2008 In Vicinity of: Former Shell Branded Gasoline Station#137772 590 Iyannough Road Hyannis,MA Dear Ms. Miorandi: Pursuant to your authorization Sovereign Consulting Inc. personnel collected soil samples from monitoring wells installed in the Iyannough Road Right of Way (R.O.W.), in vicinity of the Former Shell Branded Gasoline Station at 590 Iyannough%Road. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH), ethylene-dibromide (EDB), and lead. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVEREIGN CONSULTING,INC. . Sylvia M. Kirsch Project Manager Attachments: Laboratory Data Reports cc: with attachment Mr.David Weeks,Motiva r MassDEP- SERO Sovereign File-EQ872 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan ' BWSC 123 r' i This Notice is Related to Release Tracking Number ® 17651 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 590 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Health Inspec. Donna Miorandi 2. Street Address: 200 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): Q✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. Q✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 590 lyannough Road, Right of Way(R.O.W) City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater)to the extent known at the time of this notice. Soil from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Sylvia Kirsch Street Address: 905E South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: skirsch@sovcon.com i x NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http:Hmass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. e-Hardcopy 2.0 Automated Report New England Laborntori es '. _. .. IS ,t 'a t €a r s r�r 08/18/08 ...... ._ ... ....... 3 m .. .......::. Technical Report for Shell Oil SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA �r. EQ 872 Accutest Job Number: M75286 Sampling Dates: 07/10/08 - 07/14/08 Report to: Sovereign Consulting skirsch@sovereign.com ATTN: Sylvia Kirsch Total number of pages in report: 52 �O\H ACCoRO o • j, /.• Test results contained within this data package meet the requirements Zeza Z of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) Y....E_A R 'S NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE l; I. This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England 495 Tech Center West Building I Marlborough,MA 01752 tel:508-481-6200 fax:508-481-7753 http://www.acculest.com Ell 1 of 52 ®AGClJTEST. M75288 ..a � x Sections: Table of Contents -1- Section1: Sample Summary ................................................................................................... 3 Section2: Case Narrative/Conformance Summary .............................................................. 4 Section3: Sample Results .......<......<...............<.......................<...............<................................. 5 3.1: M75286-1: MW-301D 10-12. ....................................................................................... 6 3.2: M75286-2: MW-301D 30-32. ....................................................................................... 9 3.3: M75286-3: MW-302D 10-12. ....................................................................................... 12 3.4: M75286-4: MW-302D 30-32. ....................................................................................... 15 3.5: M75286-5: MW-301S 10-12. ....................................................................................... 18 3.6: M75286-6: MW-301 S 30-32. ....................................................................................... 21 3.7: M75286-7: MW-302S 30-32. ....................................................................................... 24 Section4: Misc. Forms ............................................................................................................ 27 4.1: Chain of Custody ........................................................................................................... 28 4.2: MCP Form ..................................................................................................................... 29 4.3: VPH Form ...................................................................................................................... 30 4.4: Sample Tracking Chronicle ........................................................................................... 37 Section 5: GC Volatiles - QC Data Summaries .................<................................................... 39 5.1.: Method Blank Summary ................................................................................................ 40 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 42 5.3: Blank Spike Summary ................................................................................................... 43 5.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 44 5.5: Surrogate Recovery Summaries ..................................................................................... 45 Section 6: Metals Analysis -QC Data Summaries ................ 6.1.: Prep QC MP 12227: Pb .................................................................................................. 48 Egli 2 of 52 13ACCL�T. M75286 x Accutest LabLink@86833 14:52 18-Aug-2008 Sample Summary Shell Oil SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Job No: M75286 Project No: EQ 872 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M75286 1 07/10/08 10:20 SB 07/15/08 SO Soil MW'301D 10=;312 M75286 2, 07/10/08 10:45 SB 07/15/08 SO Soil MW 301D 3032' M752;86 3 07/11/08 08:45 SB 07/15/08 SO Soil MUV 302D 1`0 12' M75,86 4 07/11/08 09:20 SB 07/15/08 SO Soil MW 3021) 30-32'. IvI75286 5'; 07/14/08 08:5,0 SB 07/15/08 SO Soil MW 301S'1.0 12'" M75$6=6 07/14/08 09:15 SB 07/15/08 SO Soil MW.30IS30=& M75286-7 07/14/08 10:35 SB 07/15/08 SO Soil MW302S 30 32' Soil samples reported on a dry weight basis unless otherwise indicated on result page. B 3 of 52 12ACCUTEST M75288 1 x O MAwCOUTOSOT Labai- a. tor• ies SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M75286 Site: SCMAW:97451486(REIMBMA)590 Iyannough Road Hyannis MA Report Date 7/28/2008 2:04:45 PM 7 Sample(s)were collected on between 07/10/2008 and 07/14/2008 and were received at Accutest on 07/15/2008 properly preserved, at 2.1 Deg.C and intact. These Samples received an Accutestjob number of M75286.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix SO Batch ID: GAB2469 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. W M75286-7:Soil to methanol ratio greater than 1.25 to 1. Volatiles by GC By Method SW846 8011 Matrix SO Batch ID: OP16319 ® All samples were extracted within the recommended method holding time. c All samples were analyzed within the recommmended method holding time. a All method blanks for this batch meet method specific criteria. ® Sample(s) M75286-1MS,M75286-1MSD were used as the QC samples indicated. Metals By Method SW846 6010B Matrix SO Batch ID: MP12227 ® All samples were digested within the recommended method holding time. All samples were analyzed within the recommended method holding tune. a All method blanks for this batch meet method speck criteria. ® Sample(s) M75333-1DUP,M75333-1MS,M75333-1SDL were used as the QC samples for metals. ® Only Lead requested. Wet Chemistry By Method SM21 2540 B MOD. Matrix SO Batch ID: GN26414 Sample(s) M75299-5DUP were used as the QC samples for Solids,Percent. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.Its further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M75286). Monday,J my 28,2008 Page 1 of 1 M® 4 of 52 ®A M75286 New England 12ACCUTIEST 1. abor9for i e s - -� Section ion 3 _......... _. _.. ...... __ . _. __-----_ ._.... . . . 3 5 A Lt., Yf I H E C,O,t kS:.f a Y Sample Results Report of Analysis Q® 5 of 52 ®ACCUTEET M75286 =a r Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of I Client Sample ID: MW-301D 10-12' Lab Sample ID: M75286-1 Date Sampled: 07/10/08 Matrix: SO- Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 97.4 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB44008.1) 1 07/18/08 AP n/a n/a GAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 15.0 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 0.28 mg/kg 100-41-4 Ethylbenzene N.D.. 0.28 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.11 mg/kg 91-20-3 Naphthalene ND .. 0.28 mg/kg 108-88-3 Toluene ND 0.28 mg/kg m,p-Xylene ND 0.28 mg/kg 95-47-6 o-Xylene ND 0.28 mg/kg C5- C8 Aliphatics (Unadj.) Nb. 5.6 mg/kg C9- C12 Aliphatics (Unadj.) ND. 5.6 mg/kg C9- C10 Aromatics (Unadj.) ND'. 5.6 mg/kg C5- C8 Aliphatics N.D 5.6 mg/kg C9- C12 Aliphatics ND 5.6 mg/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 108% 70-130% 615-59-8 2,5-Dibromotoluene 111% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 6 of 52 MACcUTEST. Ar, Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page I of 1 Client Sample ID: MW-301D 10-12' Lab Sample ID: M75286-1 Date Sampled: 07/10/08 Matrix: SO - Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 97.4 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 131320072.13 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume Run#1 30.6 g 50.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.0025 mg/kg CAS No. Surrogate Recoveries Run# I Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 107% 61-167% 460-00-4 Bromofluorobenzene (S) 108%, 61-167% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 910 7 of 52 13AGCtJTE3T a X Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-301D 10-12' Lab Sample ID: M75286-1 Date Sampled: 07/10/08 Matrix: SO-Soit Date Received: 07/15/08 Percent Solids: 97.4 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead Z 0 1.9 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B 1 SW846 3050B 2 (1) Instrument QC Batch: MA9525 (2) Prep QC Batch: MP12227 RL = Reporting Limit �® 8 of 52 14CCUTEBT. M75286 —..,s Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 ; Client Sample ID: MW-301D 30-32' Lab Sample ID: M75286-2 Date Sampled: 07/10/08 Matrix: SO- Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 84.8 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 A1344009.1) 1 07/18/08 AP n/a n/a GAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 15.6 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 0.35 mg/kg 100-41-4 Ethylbenzene ND 0.35 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND : 0.14 mg/kg 91-20-3 Naphthalene ND 0.35 mg/kg 108-88-3 Toluene N-D 0.35 mg/kg m,p-Xylene NO. 0.35 mg/kg 95-47-6 o-Xylene ND 0.35 mg/kg C5- C8 Aliphatics (Unadj.) ND 6.9 mg/kg C9- C12 Aliphatics (Unadj.) NO 6.9 mg/kg C9- C10 Aromatics (Unadj.) 'ND 6.9 mg/kg C5- C8 Aliphatics ND 6.9 mg/kg C9- C12 Aliphatics NO. 6.9 mg/kg CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81%o 70-130% 615-59-8 2,5-Dibromotoluene 80% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q® 9 of 52 ®ACCUTEST M75286 i.a. ..... ......_ y Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-301D 30-32' Lab Sample ID: M75286-2 Date Sampled: 07/10/08 Matrix: SO-Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 84.8 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 131320073.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume Run#1 30.4 g 50.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.0029 mg/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 107% 61-167% 460-00-4 Bromofluorobenzene (S) :99/0 61-167% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10 of 52 �ACCL nimT. M75286 =a ^'a_r r Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 N Client Sample ID: MW-301D 30-32' Lab Sample ID: M75286-2 Date Sampled: 07/10/08 Matrix: SO- Soil Date Received: 07/15/08 Percent Solids: 84.8 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead . 2 3 2.3 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B 1 SW846 3050B 2 (1) Instrument QC Batch: MA9525 (2) Prep QC Batch: MP12227 RL = Reporting Limit 11 of 52 GACCLffEST. M75286 I Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-302D 10-12' Lab Sample ID: M75286-3 Date Sampled: 07/11/08 Matrix: SO - Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 97.2 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB44010.D 1 07/18/08 AP n/a n/a GAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 15.5 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 0.27 mg/kg 100-41-4 Ethylbenzene ND 0.27 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.11 mg/kg 91-20-3 Naphthalene 0 521 0.27 mg/kg 108-88-3 Toluene ND 0.27 mg/kg m,p-Xylene ND 0.27 mg/kg 95-47-6 o-Xylene ND 0.27 mg/kg C5- C8 Aliphatics (Unadj ) ND 5.5 mg/kg C9- C12 Aliphatics (Unadj ) 18 2 5.5 mg/kg C9- C10 Aromatics (Unadj.) -10.6 5.5 mg/kg C5- C8 Aliphatics ND 5.5 mg/kg C9- C12 Aliphalics 7 69 5.5 mg/kg CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 119w 70-130% 615-59-8 2,5-Dibromotoluene '123% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank. E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound [M® 12 of 52 13ACCUTEST. M75286 14 Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 w Client Sample ID: MW-302D 10-12' Lab Sample ID: M75286-3 Date Sampled: 07/11/08 Matrix: SO - Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 97.2 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 131320074.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume Run#1 30.5 g 50.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.0025 mg/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 115% 61-167% 460-00-4 Bromofluorobenzene (S) 119% 61 167% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound a® 13 of 52 12AC.CUTE ST s Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 w Client Sample ID: MW-302D 10-12' Lab Sample ID: M75286-3 Date Sampled: 07/11/08 Matrix: SO - Soil Date Received: 07/15/08 Percent Solids: 97.2 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <2,,. 2.0 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B 1 SW846 3050B 2 (1) Instrument QC Batch: MA9525 (2) Prep QC Batch: MP12227 RL = Reporting Limit QB 14 of 52 QA©Cl.1TEST. M75286 -a_. Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of I Client Sample ID: MW-302D 30-32' Lab Sample ID: M75286-4 Date Sampled: 07/11/08 Matrix: SO- Soil, Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 88.3 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 A1344011.1) 1 07/18/08 AP n/a n/a GAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 18.2 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 9 0.28 mg/kg 100-41-4 Ethylbenzene ND 0.28 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.11 mg/kg 91-20-3 Naphthalene ND 0.28 mg/kg 108-88-3 Toluene N J "0.28 mg/kg m,p-Xylene ND 0.28 mg/kg 95-47-6 o-Xylene ND 0.28 mg/kg C5- C8 Aliphatics (Unadj.) ND 5.6 mg/kg C9- C12 Aliphatics (Unadj ) ND 5.6 mg/kg C9- C10 Aromatics (Unadj.) ND 5.6 mg/kg C5- C8 Aliphatics ND 5.6 mg/kg C9- C12 Aliphatics NO: 5.6 mg/kg CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 85%; 70-130% 615-59-8 2,5-Dibromotoluene 87% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MIN 15 of 52 ®ACCUTEST. M75286 Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-302D 30-32' Lab Sample ID: M75286-4 Date Sampled: 07/11/08 Matrix: SO - Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 88.3 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20075.D 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume Run#1 30.3 g 50.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.0028 mg/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 404% 61-167% 460-00-4 Bromofluorobenzene (S) 106%. 61-167% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound [MIN 16 of 52 ®ACCUTE3T. M75286 Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-302D 30-32' Lab Sample ID: M75286-4 Date Sampled: 07/11/08 Matrix: SO - Soil Date Received: 07/15/08 Percent Solids: 88.3 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <252 2.2 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B 1 SW846 3050B 2 (1) Instrument QC Batch: MA9525 (2) Prep QC Batch: MP12227 RL = Reporting Limit �® 17 of 52 13ACCUTEST. 1 Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page I of 1 Client Sample 1D: MW-301S 10-12' Lab Sample ID: M75286-5 Date Sampled: 07/14/08 Matrix: SO - Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 96.6 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB44012.D 1 07/18/08 AP n/a n/a GAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 16.0 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene N.D 0.27 mg/kg 100-41-4 Ethylbenzene ND 0.27 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.11 mg/kg 91-20-3 Naphthalene NO: 0.27 mg/kg 108-88-3 Toluene ND 0.27 mg/kg m,p-Xylene NO 0.27 mg/kg 95-47-6 o-Xylene ND 0.27 mg/kg C5- C8 Aliphatics (Unadj.) NO 5.4 mg/kg C9- C12 Aliphatics (Unadj.) ND. 5.4 mg/kg C9- C10 Aromatics (Unadj.) NO 5.4 mg/kg C5- C8 Aliphatics NO 5.4 mg/kg C9- C12 Aliphatics NO 5.4 mg/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 16% 70-130% 615-59-8 2,5-Dibromotoluene 78% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank i E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q 18 of 52 13ACCUTEST. M75286 ^"' Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Ln Client Sample ID: MW-301S 10-12' Lab Sample ID: M75286-5 Date Sampled: 07/14/08 Matrix: SO- Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 96.6 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 131320076.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume Run#1 30.6 g 50.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane NO. 0.0025 mg/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits II 460-00-4 Bromofluorobenzene (S) 111% 61-167% 460-00-4 Bromofluorobenzene (S) :1W/0 61-167% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound QB 19 of 52 MACC_IJTEST. M75286 _a........... s r Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Lq Client Sample 1D: MW-301S 10-12' Lab Sample ID: M75286-5 Date Sampled: 07/14/08 Matrix: SO - Soil Date Received: 07/15/08 Percent Solids: 96.6 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <20 2.0 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B 1 SW846 3050B 2 (1) Instrument QC Batch: MA9525 (2) Prep QC Batch: MP12227 RL = Reporting Limit �® 0 of 52 13ACCUTE3T. M75286 =a i ) Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-301S 30-32' Lab Sample 1D: M75286-6 Date Sampled: 07/14/08 Matrix: SO - Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 82.7 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB44013.D 1 07/18/08 AP n/a n/a GAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 18.0 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 0.32 mg/kg 100-41-4 Ethylbenzene ND 0.32 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.13 mg/kg 91-20-3 Naphthalene ND ..0.32 mg/kg 108-88-3 Toluene ND 0.32 mg/kg m,p-Xylene ND 0.32 mg/kg 95-47-6 o-Xylene ND 0.32 mg/kg C5- C8 Aliphatics (Unadj.) ND 6.4 mg/kg C9- C12 Aliphatics (Unadj.) ND 6.4 mg/kg C9- C10 Aromatics (Unadj.) N'D 6.4 mg/kg C5- C8 Aliphatics ND 6.4 mg/kg C9- C12 Aliphatics ND 6.4 mg/kg CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene .93% 70-130% 615-59-8 2,5-Dibromotoluene 94%. 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M® 21 of 52 ®ACLU TEST. M75286 ..,.....- ....ss Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-301S 30-32' Lab Sample ID: M75286-6 Date Sampled: 07/14/08 Matrix: SO- Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 82.7 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20078.D 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume Run#1 30.3 g 50.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 0.0030 mg/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 102%0 61-167% 460-00-4 Bromofluorobenzene (S) 111% 61-167% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 22 of 52 13ACCIJTEST M75286 b u._..,....... Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-301S 30-32' Lab Sample ID: M75286-6 Date Sampled: 07/14/08 Matrix: SO -Soil Date Received: 07/15/08 Percent Solids: 82.7 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <2:2 2.2 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B 1 SW846 3050B 2 (1) Instrument QC Batch: MA9525 (2) Prep QC Batch: MP12227 RL = Reporting Limit ®� 23 of 52 12AOC.UTEBT M75286 ,1 Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-302S 30-32' Lab Sample ID: M75286-7 Date Sampled: 07/14/08 Matrix: SO - Soil Date Received: 07/15/08 Method: MADEP VPH REV 1.1 Percent Solids: 85.9 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB44014.1) 1 07/18/08 AP n/a n/a GAB2469 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 19.4 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 'ND 0.28 mg/kg 100-41-4 Ethylbenzene ND 0.28 mg/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.11 mg/kg 91-20-3 Naphthalene ND 0.28 mg/kg 108-88-3 Toluene ND 0.28 mg/kg m,p-Xylene ND 0.28 mg/kg 95-47-6 o-Xylene ND 0.28 mg/kg C5- C8 Aliphatics (Unadj.) ND 5.6 mg/kg C9- C12 Aliphatics (Unadj.) ND, 5.6 mg/kg C9- C10 Aromatics (Unadj.) ND 5.6 mg/kg C5- C8 Aliphatics ND 5.6 mg/kg C9- C12 Aliphatics ND 5.6 mg/kg CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 72%._ 70-130% 615-59-8 2,5-Dibromotoluene 72% 70-130% (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 24 of 52 CIACCU T'E5T M75288 -° - Accutest LabLink986833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-302S 30-32' Lab Sample ID: M75286-7 Date Sampled: 07/14/08 Matrix: SO-Soil Date Received: 07/15/08 Method: SW846 8011 SW846 3550B Percent Solids: 85.9 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BB20079.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 Run#2 Initial Weight Final Volume Run#1 30.6 g 50.0 ml Run#2 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane NO: 0.0029 mg/kg CAS No. Surrogate Recoveries Run# I Run# 2 Limits 460-00-4 Bromofluorobenzene (S) 100%0 61-167% 460-00-4 Bromofluorobenzene (S) 107% 61-167% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q® 25 of 52 IRACCUTEST M75286 _ . ,....... Accutest LabLink@86833 14:52 18-Aug-2008 Report of Analysis Page 1 of 1 Client Sample ID: MW-302S 30-32' Lab Sample ID: M75286-7 Date Sampled: 07/14/08 Matrix: SO-Soil Date Received: 07/15/08 Percent Solids: 85.9 Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Lead <2.1 2.1 mg/kg 1 07/22/08 07/25/08 EAL SW846 6010B 1 SW846 3050B 2 (1) Instrument QC Batch: MA9525 (2) Prep QC Batch: MP12227 RL = Reporting Limit �® 26 of 52 ®AC LUTES. M75286 """"" New England ®.AIGCUY—ST. , L.a b o r a t o r i c_ _ . Section 4 _.. .. "_ ........ ...... __ ._......_ Mist Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle �® 27 of 52 12AC AX-rEST. M75286 - •-- LAB(LOCATION) Q Shell Oil Products Chain Of Custody Record Please Check A ro date Box: Print Bill To Contact Name: INCIDENT#(ENV SERVICES) p om u NO IAaOwT°Amm ❑1XV.SERVICES O NGTNA RETML ❑SNE11 MTAR � � t AaurEST 6 DATE: 1- I O MOTIVA SDSCM DONpATMR ❑LI18E5 PO# SAP# ❑OTHER r T ❑sNal Plea2NE Q on1ER 1 17,1 1EFL PAGE: m LAe V%ONLY E Ds 339-3z NSRA IMY()ANDAYS, (2A O S LAYS ❑2 DAYS O:DAYS O 24 NDITAS REQUESTED ANALYSIS DEUVERAMES: ID- OcOHMe pKtP ❑AO Q+OTMER(%MN) SEMPERATUREONRECEIPTC• CwW#, ICe 02 ICookr M] SPECIAL INSTRUCTIONS OR NOTES: SAMPLING PxEAenv.nve4. AAA Field Sample Identification .MTra, "o°f '� , ° DaC DATE TIME o Container PlD Rsadlrpa orA.r mz wro,NZsa NDnE oTrfA < or Laboratory Nolsa V&l Soc\ l -3 - o o - it Z. 'so- 9 1 's (o- T "L M _ t I Ll L:kw --A,0Z S l.aw"cwe W.1' 1. qw..e by 1,ITNlvel D.Is: �1 1 0.ewine by Isw.°asI pale: 'eNn.uW.e K IegruW.l 0.eceMm W 150nepuel Dete: a5I2Aa Rsvwbn �'/per, I M75286: Chain of Custody Page 1 of 1 �® 28 of 52 13ACCUTEST. M75286 .a i•.. ......._s Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 Title: MADEP MCP Response Action Analytical Report Certification Form a,*­q "?, WE I&A 01 ON, K 0 Owl In -WST" Laboratory Name: Accutest Laboratories of New England Project M75286 Hyannis MA None Project Location- SCMAW:97451486(REIMBMA)590 lyannough Road MADEP RTN This form provides certifications for the following data set: M75286-1,M75286-2,M75286-3,M75286-4,M75286-5,M75286-6,M75286-7 Test method:SW846 8011,SM21 2540 B MOD,and below Sample Matrices: Groundwater Soil/Sediment X Drinking Water Other: 82606 8151A_Ll 8330_L 60106 (X) 7470A/1 A 8270C 8081A VPH(X) 6020 9014M 2 gw k 8082 8021B EPH 7000S 7196A ME k6JdWWW& nNy C yge )e,, ateGheckal'Iliat a i ry� sW somas>neth s m s r" a�t,e�� a An affirmative response to questions A, B, C, and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with 0 Yes E] No1 that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and Yes El No I discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty",as described in Section 2.0(a),(b), (c)and Yes El No I (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only: Was the VPH or EPH method run without Yes El No I significant modifications,as specified in Section 11.3? A response to questions E and Fbelow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the Yes No I specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified El Yes El No I method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,accurate and complete. Signature: � Position: Laboratory Director Printed Name: Reza Tan d Date: 07/28/2008 MIN 29 of 52 JJACCVFPPT M75286 MADEP VPH FORM (tilatartx% K � � Aqueous rl Soil rl_0l Sediment i 1 Other I I Con,ta%net's �� Satisfactory ICI Broken i _i Leaking ueous 'reservatlues N/A ✓ H <=2 l H >2 Txem e atl re Received on Ice F1 Received at 4 Deg. C 7 Other 7 Rec'd at 2.1 deg C Methaf of � M Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301D 10-12' Lab ID: M75286-1 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/10/2008 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 97.4 1 N/A Unadjusted Ranges CAS# Elution Ranqe Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A mg/kg ND" 5.6 C9-C10 Aromatics(Unadj.) N/A mg/kg ND' 5.6 C9-C12 Aliphatics(Unadj.) N/A mg/kg ND' 5.6 Target Analytes Ethylbenzene 100-41-4 C9-C12 mg/kg ND 0.28 Toluene 108-88-3 C5-C8 mg/kg ND 0.28 Methyl Tert Butyl Ether 1634-04-4 C5-C8 mg/kg ND 0.11 Benzene 71-43-2 C5-C8 mg/kg ND 0.28 Naphthalene 91-20-3 N/A mg/kg ND 0.28 o-Xylene 95-47-6 C9-C12 mg/kg ND 0.28 m,p-Xylene C9-C12 mg/kg ND 0.28 Adiusted Ranges C5-C8 Aliphatics N/A mg/kg ND a 5.6 C9-C12 Aliphatics N/A mg/kg ND` 5.6 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 108 70-130% PID:2,5-Dibromotoluene % 111 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons, Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? -.Yes ':. . No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ! :Yes t No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? _!e!No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature ��—�� Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 Q11 30 of 52 MACCL11TEST M75286 lab-rzi r,.ries MADEP VPH FORM Matrtz' f'' Aqueous Soil ICI Sediment r Other 11 CoRtal;ners _ Satisfactory Broken r Leaking i 1 eousPreservattves N/A PH <=2 H >2 Tn_;e�afr� Received on Ice Received at 4 De . C ��I Other IWl Read at 2.1 deg C M Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301D 30-32' Lab ID: M75286-2 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/10/2008 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 84.8 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A mg/kg ND" 6.9 C9-C10 Aromatics(Unadj.) N/A mg/kg ND' 6.9 C9-C12 Aliphatics(Unadj.) N/A mg/kg ND" 6.9 Target Analytes Ethylbenzene 100-41-4 C9-C12 mg/kg ND 0.35 Toluene 108-88-3 C5-C8 mg/kg ND 0.35 Methyl Tert Butyl Ether 1634-04-4 C5-C8 mg/kg ND 0.14 Benzene 71-43-2 C5-C8 mg/kg ND 0.35 Naphthalene 91-20-3 N/A mg/kg ND 0.35 o-Xylene 95-47-6 C9-C12 mg/kg ND 0.35 m,p-Xylene C9-C12 mg/kg ND 0.35 Adjusted Ranges C5-C8 Aliphatics N/A mg/kg ND' 6.9 C9-C12 Aliphatics N/A mg/kg ND° 6.9 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 80 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of.any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons, Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? �JYes P No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes E! No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? IV L .! Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 ®19 31 of 52 MAC: M75286 I-a MADEP VPH FORM Matrtx A A ueous r-I Soil Sediment F— Other I-1 SatisfactoryFyi Broken 1 Leaking f I Cantafners����;rNa��;,r, ueous Pres.efvatlu�es� N/A pH <=2 I Tet11 erg#irre � Received on Ice Received at 4 Deg. C F 1 Other ✓; Rec'd at 2.1 deg C Mettianot� Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-302D 10-12' Lab ID: M75286-3 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/11/2008 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 97.2 1 N/A Unadjusted Ranges CAS# Elution Ranqe Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A mg/kg ND" 5.5 C9-C10 Aromatics(Unadj.) N/A mg/kg 10.6" 5.5 C9-C12 Aliphatics(Unadj.) N/A mg/kg 18.2 A 5.5 Target Analytes Ethylbenzene 100-41-4 C9-Cl 2 mg/kg ND 0.27 Toluene 108-88-3 C5-C8 mg/kg ND 0.27 Methyl Tart Butyl Ether 1634-04-4 C5-C8 mg/kg ND 0.11 Benzene 71-43-2 C5-C8 mg/kg ND 0.27 Naphthalene 91-20-3 N/A mg/kg 0.521 0.27 o-Xylene 95-47-6 C9-Cl 2 mg/kg ND 0.27 m,p-Xylene C9-C12 mg/kg ND 0.27 Adjusted Ranges C5-C8 Aliphatics N/A mg/kg ND a 5.5 C9-C12 Aliphatics N/A mg/kg 7.69` 5.5 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 119 70-130% PID:2,5-Dibromotoluene % 123 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes 1.1 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo [l Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 Mr] 32 of 52 13ACCUTEST M75286 _a-.. .......,_ MADEP VPH FORM Ma#rtz k A ueous ri Soil lv Sediment Other i-1 Containers Satisfactory F41 Broken Fi Leaking 1--I A`ueous`P�eservatlueb' N/A W1 PH <=2 i-_' PH >2 Temperature Received on Ice l Received at 4 Deg. C Other % Rec'd at 2.1 des C Met anol � F Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% p, Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-302D 30-32' Lab ID: M75286-4 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/11/2008 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 88.3 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A mg/kg ND" 5.6 C9-C10 Aromatics(Unadj.) NIA mg/kg ND" 5.6 C9-C12 Aliphatics(Unadj.) N/A mg/kg ND' 5.6 Target Analytes Ethylbenzene 100-41-4 C9-C12 mg/kg ND 0.28 Toluene 108-88-3 C5-C8 mg/kg ND 0.28 Methyl Tert Butyl Ether 1634-04-4 C5-C8 mg/kg ND 0.11 Benzene 71-43-2 C5-C8 mg/kg ND 0.28 Naphthalene 91-20-3 N/A mg/kg ND 0.28 o-Xylene 9547-6 C9-C12 mg/kg ND 0.28 m,p-Xylene C9-C12 mg/kg ND 0.28 Adjusted Ranges C5-C8 Aliphatics N/A mg/kg ND' 5.6 C9-C12 Aliphatics N/A mg/kg ND` 5.6 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 85 70-130% PID:2,5-Dibromotoluene % 87 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ' :Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 1_1 No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 G® 33 of 52 ®ACCUTEBT. M75288 i. .. .............:. MADEP VPH FORM Mat�Ix� j � Aqueous F Soil W. Sediment F1 Other f Containers Satisfactory✓i Broken F Leaking - ., w ueaus�Preservattves� N/A ✓ H <=2 H>2 TeriP",er-L222M Received on Ice (7, Received at 4 Deg. CA Other ✓, Rec'd at 2.1 deg C i�et#Sh' " Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301S 10-12' Lab ID: M75286-5 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/14/2008 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 96.6 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A mg/kg ND' 5.4 C9-C10 Aromatics(Unadj.) N/A mg/kg ND' 5.4 C9-C12 Aliphatics(Unadj.) N/A mg/kg ND" 5.4 Target Analytes Ethylbenzene 100-41-4 C9-C12 mg/kg ND 0.27 Toluene 108-88-3 C5-C8 mg/kg ND 0.27 Methyl Tert Butyl Ether 1634-04-4 C5-C8 mg/kg ND 0.11 Benzene 71-43-2 C5-C8 mg/kg ND 0.27 Naphthalene 91-20-3 N/A mg/kg ND 0.27 o-Xylene 95-47-6 C9-C12 mg/kg ND 0.27 m,p-Xylene C9-C12 mg/kg ND 0.27 Adiusted Ranges C5-C8 Aliphatics N/A mg/kg ND a 5.4 C9-C12 Aliphatics N/A mg/kg ND c 5.4 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 76 70-130% PID:2,5-Dibromotoluene % 78 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'T qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? :Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? V'Yes '..' No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? LVi No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 M® 34 of 52 13ACCUTEST. M75286 l MADEP VPH FORM IVlatrtxk' � s A ueous Soil , Sediment I 1 Other on ate ers � Satisfactory%*� Broken Leaking F 1 u(eods Preserva0,44Y N/A H <=2 PH > Tem e ature Received on Ice D Received at 4 Deg. C Other 141 Redd at 2.1 deg C Metianoh _ � Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-301S 30-32' Lab ID: M75286-6 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/14/2008 Date Received: 7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 82.7 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A mg/kg ND" 6.4 C9-C10 Aromatics(Unadj.) N/A mg/kg ND" 6.4 C9-C12 Aliphatics(Unadj.) N/A mg/kg ND" 6.4 Target Analytes Ethylbenzene 100-41-4 C9-Cl 2 mg/kg ND 0.32 Toluene 108-88-3 C5-C8 mg/kg ND 0.32 Methyl Tert Butyl Ether 1634-04-4 C5-C8 mg/kg ND 0.13 Benzene 7143-2 C5-C8 mg/kg ND 0.32 Naphthalene 91-20-3 N/A mg/kg ND 0.32 o-Xylene 95-47-6 C9-C12 mg/kg ND 0.32 m,p-Xylene C9-C12 mg/kg ND 0.32 Adjusted Ranges C5-C8 Aliphatics N/A mg/kg ND a 6.4 C9-C12 Aliphatics N/A mg/kg ND` 6.4 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % 94 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Lk*]Yes El No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ✓,Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 141 No F._I Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 Q® 35 of 52 aACCtJTEST. M75286 MADEP VPH FORM Matrtx r Aqueous f Soil W' Sediment IFF1 Other i 1 Containers Sat isfactoryW Broken i- Leaking n f u ous�Pre`,erlratives N/A H <=2 H>2 � Os Rec'd at 2.1 de Tee er�ture. ., Received on Ice i Received at 4 De . C Other 9 C Metha'na ' F,l Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio > 1.25 to 1. A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-302S 30-32' Lab ID: M75286-7 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 7/14/2008 Date Received: •7/15/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 7/18/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 85.9 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A mg/kg ND" 5.6 C9-C10 Aromatics(Unadj.) N/A mg/kg ND A 5.6 C9-C12 Aliphatics(Unadj.) N/A mg/kg ND A 5.6 Target Analytes Ethylbenzene 100-41-4 C9-C12 mg/kg ND 0.28 Toluene 108-88-3 C5-C8 mg/kg ND 0.28 Methyl Tert Butyl Ether 1634-04-4 C5-C8 mg/kg ND 0.11 Benzene 71-43-2 C5-C8 mg/kg ND 0.28 Naphthalene 91-20-3 N/A mg/kg ND 0.28 o-Xylene 95-47-6 C9-C12 mg/kg ND 0.28 m,p-Xylene C9-C12 mg/kg ND 0.28 Adjusted Ranges C5-C8 Aliphatics N/A mg/kg ND a 5.6 - - -- - - - — N/A- - . . mg/kg _._._ _-.._ND` ....__. -..__ 5.6 C9-C12 Aliphatics Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 72 70-130% PID:2,5-Dibromotoluene % 72 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑J Yes [ ` No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? CYes (__1 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? LNo I Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 7/28/2008 MIN 36 of 52 12ACCUTEST. M75286 l a Accutest Laboratories Internal Sample Tracking Chronicle A Shell 0i1 ' Job No: M75286 SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes I775286 1 Collected i�JUL U8 1�0 20 By ,SBA Received 15 j 7L 08 By SA M75286-1 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-1 MADEP VPH REV 1.118-JUL-08 18:21 AP VMAVPH M75286-1 SW846 8011 23-JUL-08 16:25 CZ 23-JUL-08 FG V8011EDB M75286-1 SW846 6010B 25-JUL-08 18:51 EAL 22-JUL-08 EAL PB M75286-2 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-2 MADEP VPH REV 1.1 18-JUL-08 19:04 AP VMAVPH M75286-2 SW846 8011 23-JUL-08 16:54 CZ 23-JUL-08 FG V8011EDB M75286-2 SW846 6010B 25-JUL-08 18:57 EAL 22-JUL-08 EAL PB M75286-3 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-3 MADEP VPH REV 1.1 18-JUL-08 19:46 AP VMAVPH M75286-3 SW846 8011 23-JUL-08 17:24 CZ 23-JUL-08 FG V8011EDB M75286-3 SW846 6010B 25-JUL-08 19:03 EAL 22-JUL-08 EAL PB III72869 ,Catic#ei1�1U 08�090 $y TSB Rceved1Ld fl8B�SA' Y M75286-4 SM21 2540 B MOD. . 16-JUL-08 WC %SOL M75286-4 MADEP VPH REV 1.118-JUL-08 20:29 AP VMAVPH M75286-4 SW846 8011 23-JUL-08 17:53 CZ 23-JUL-08 FG V8011EDB M75286-4 SW846 6010B 25-JUL-08 19:08 EAL 22-JUL-08 EAL PB - �`I� ©��5�10*1�� M75286-5 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-5 MADEP VPH REV 1.118-JUL-08 21:11 AP VMAVPH M75286-5 SW846 8011 23-JUL-08 18:22 CZ 23-JUL-08 FG V8011EDB M75286-5 SW846 6010B 25-JUL-08 19:14 EAL 22-JUL-08 EAL PB Page 1 of 2 ® 37 of 52 QACC'UTEST. M75286 . .....,..... 4 Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil SCMAW.97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Job No: M75286 Project No: EQ 872 Sample Number Method Analyzed By Prepped By Test Codes �4�7�5286 301530 � N °fix M75286-6 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-6 MADEP VPH REV 1.1 18-JUL-08 21:54 AP VMAVPH M75286-6 SW846 8011 23-JUL-08 19:21 CZ 23-JUL-08 FG V8011EDB M75286-6 SW846 6010B 25-JUL-08 19:19 EAL 22-JUL-08 EAL PB �7528T�Collected�l�4� ��08�10�3y� SB��y ��Recetued �1 JUL 08B'�y�SA�P x ��� � `� '�` M75286-7 SM21 2540 B MOD. 16-JUL-08 WC %SOL M75286-7 MADEP VPH REV 1.118-JUL-08 22:37 AP VMAVPH M75286-7 SW846 8011 23-JUL-08 19:50 CZ 23-JUL-08 FG V8011EDB M75286-7 SW846 6010B 25-JUL-08 19:25 EAL 22-JUL-08 EAL PB i I Page 2 of 2 ME1 38 of 52 ®ACCUTE,ST. M75286 ^"' New England QAMU MST. All t_aborntr�r; a. _ Section 5 Y{, if# .YFA' YiiE iC: {r M$•5Ynv GC>V614tiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ®� 39 of 52 CZAC:Ct,JTE'ST. M75286 =a � s Method Blank Summary Page I of 1 Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2469-MB AB44005.1) 1 07/18/08 AP n/a n/a GAB2469 v, The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 250 ug/kg 100-41-4 Ethylbenzene NO 250 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 100 ug/kg 91-20-3 Naphthalene N'D 250 ug/kg 108-88-3 Toluene ND 250 ug/kg m,p-Xylene ND 250 ug/kg 95-47-6 o-Xylene ND 250 ug/kg C5- C8 Aliphatics (Unadj ) N-D 5000 ug/kg C9- C12 Aliphatics (UnadJ ) ND 5000 ug/kg C9- C10 Aromatics (Unadj.) ND 5000 ug/kg C5- C8 Aliphatics ND 5000 ug/kg C9- C12 Aliphatics ND 5000 ug/kg CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 101%q 70-130% 615-59-8 2,5-Dibromotoluene 1.U0% 70-130% 40 of 52 .13ACCUTE:BT. M75286 s Method Blank Summary Page 1 of 1 Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16319-MB BB20067.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 c� j The QC reported here applies to the following samples: Method: SW846 8011 M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 CAS No. Compound Result RL Units Q 106-93-4 1,2-Dibromoethane ND 2.5 ug/kg CAS No. Surrogate Recoveries Limits 460-00-4 Bromofluorobenzene (S) 11.0%u 61-167% 460-00-4 Bromofluorobenzene (S) 129% 61-167% 41 of 52 ®ACCUTES T. M75286 -' Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2469-BSP AB44006.1) 1 07/18/08 AP n/a n/a GAB2469 GAB2469-BSD A1344007.1) 1 07/18/08 AP n/a n/a GAB2469 w N The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/kg ug/kg % ug/kg % RPD Rec/RPD 71-43-2 Benzene 2500 2570 103 2580 103 0. 70-130/25 100-41-4 Ethylbenzene 2500 2630 105 2640 106 0 70-130/25 1634-04-4 Methyl Tert Butyl Ether 2500 2670 107 2640 106 1 70-130/25 91-20-3 Naphthalene 2500 2650 106 2670 107 1 70-130/25 108-88-3 Toluene 2500 2580 103. 2570 103 0' 70-130/25 m,p-Xylene 5000 5310 A 5340 107 1 70-130/25 95-47-6 o-Xylene 2500 2590 104 2600 104 0. 70-130/25 C5- C8 Aliphatics (Unadj.) 7500 7440 99: 7490 100 1 70-130/25 C9- C12 Aliphatics (Unadj.) 7500 7180 96- 7270 97 1 70-130/25 C9- C10 Aromatics (Unadj.) 2500 2600 103 2600 104 0 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 100% 101% 70-130% 615-59-8 2,5-Dibromotoluene 99% 100% 70-130% ®� 42 of 52 [JACCUTEST M75286 " ^ Blank Spike Summary Page 1 of 1 Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16319-BS BB20069.D 1 07/23/08 CZ 07/23/08 OP16319 GBB824 w The QC reported here applies to the following samples: Method: SW846 8011 M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 Spike BSP BSP CAS No. Compound ug/kg ug/kg % Limits 106-93-4 1,2-Dibromoethane 32.9 37.7 115: 56-140 CAS No. Surrogate Recoveries BSP Limits 460-00-4 Bromofluorobenzene (S) 1>18%.. 61-167% 460-00-4 Bromofluorobenzene (S) 137% 61-167% 43 of 52 ®AC.'CIdTE_ST. M75288 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP16319-MS 131320070.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 OP16319-MSD BB20071.D 1 07/23/08 CZ 07/23/08 OP16319 GBB824 M75286-1 B1320072.1) 1 07/23/08 CZ 07/23/08 OP16319 GBB824 The QC reported here applies to the following samples: Method: SW846 8011 M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 M75286-1 Spike MS MS MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD 106-93-4 1,2-Dibromoethane ND 33.5 36.2 108 33.3 :99'' 8 48-141/27 CAS No. Surrogate Recoveries MS MSD M75286-1 Limits 460-00-4 Bromofluorobenzene (S) :14% 109% 107W 61-167% 460-00-4 Bromofluorobenzene (S) 1369/0: 11:9% 108%. 61-167% it Q� 44 of 52 IJACCCUTE3T. M75286 --- • - -- Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: SO Samples and QC shown here apply to the above method Lab Lab Sample I File ID Sl a S1 b M75286-1 AB44008.D 108.0 111.0 M75286-2 AB44009.D 81.0.:. <I` 80.0 M75286-3 AB44010.D 19 0, 123.0 M75286-4 AB44011.D 85.0 87.0 M75286-5 AB44012.D 76:0 78.0 M75286-6 AB44013,1) 93,0 94.0 M75286-7 AB44014.D 72..0F" 72.0 GAB2469-BSD AB44007.D 10:1:0 100.0 GAB2469-BSP AB44006.D 100.10 99.0 GAB2469-MB AB44005.D 01-0 100.0 Surrogate Recovery Compounds Limits Sl = 2,5-Dibromotoluene 70-130% (a) Recovery from GC signal #1 (b) Recovery from GC signal#2 Q® 45 of 52 M75286 - - Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M75286 Account: SHELLWIC Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA Method: SW846 8011 Matrix: SO Samples and QC shown here apply to the above method w Lab Lab Sample ID File ID S1 a SI b M75286-1 BB20072.D 1070: 108.0 M75286-2 BB20073.1) t07.0 99.0 M75286-3 BB20074.D 115 0_ 119.0 M75286-4 BB20075.1) 104.0 106.0 M75286-5 BB20076.D 111.0 119.0 ................ M75286-6 BB20078.D 1o2.0 111.0 M75286-7 BB20079.D <100:U, 107.0 OP16319-BS BB20069.1) =118 0 137.0 OP16319-MB BB20067.D 110.0 129.0 OP16319-MS 131320070.1) 114.0 136.0 OP16319-MSD BB20071.D 10.1.. 119.0 Surrogate Recovery Compounds Limits SI = Bromofluorobenzene (S) 61-167%0 (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 :B® 46 of 52 13ACCUTEgT M75286 .,-..-_....;', i r ®® New England 12ACCU I i..:h o r,„ o r _ >: Section 6 z ...._........ _ . x€as •e .r; rav Metals Analysis 0 QC Data Summaries Inclu des the following where applicable: • Method Blank Summaries • Matrix Spike and Duplicate Summaries • Blank Spike and Lab Control Sample Summaries • Serial Dilution Summaries ® 47 of 52 UAC XYTEST M75286 '.ab. ...,....es BLANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: M75286 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12227 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg Prep Date: 07/22/08 MB Metal RL IDL raw final Aluminum 20 1.9 .a Antimony 2.0 .14 Arsenic 2.0 .074 am • Barium 20 .086 am Beryllium 0.40 .025 Boron 10 .17 Cadmium 0.40 .022 am Calcium 500 .66 Chromium 1.0 .03 am Cobalt 5.0 .061 Copper 2.5 .081 Iron 10 .63 Lead 2.0 .092 -0.080 .<2..0..': Magnesium 500 .66 - Manganese 1.5 .024 Molybdenum 10 .022 Nickel 4.0 .047 Potassium 500 .55 Selenium 2.0 .1 am Silver 0.50 .031 am Sodium 500 8 Strontium 1.0 .017 Thallium 2.0 .27 Tin 10 .13 Titanium 5.0 .031 Tungsten 10 .093 Vanadium 3.0 .035 Zinc 2.0 .036 Associated samples MP12227: M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (anr) Analyte not requested Page 1 Q® 48 of 52 �ACC�JTEST M75286 :.,....:........ MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: M75286 Account: SHELLWIC - Shell Oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12227 Methods: SW846 6010E Matrix Type: SOLID Units: mg/kg Prep Date: 07/22/08 07/22/.0.8 M75333-1 Spikelot QC M75333-1 QC Metal Original MS MPICP °a Rec Limits Original DUP RPD Limits Aluminum O> Antimony N Arsenic am • Barium am Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper Iron Lead 2.8 88.2 104 82.1 75-125 2.8 2.7 3cfi 0-20 Magnesium Manganese Molybdenum Nickel - Potassium Selenium am Silver am Sodium Strontium Thallium Tin Titanium Tungsten Vanadium Zinc Associated samples MP12227: M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (N) Matrix Spike Rec. outside of QC limits (anr) Analyte not requested Page 1 ffi® 49 of 52 ®ACCUTEST. M75286 9 r ? SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: M75286 Account: SHELLWIC - Shell Oil Project: SCMAW:97951986 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12227 Methods: SW846 6010E Matrix Type: SOLID Units: mg/kg Prep Date: 0.7/22/08 0.7./22/:08 BSP Spikelot QC BSD Spikelot BSD QC [Metal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit Aluminum ai Antimony W Arsenic am Barium am Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper Iron Lead 92.4 100 .92.4 80-120 90.3 100 90.3 2.3 20 Magnesium Manganese Molybdenum Nickel Potassium Selenium am Silver am Sodium Strontium - - Thallium Tin Titanium Tungsten Vanadium Zinc Associated samples MP12227: M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (ant) Analyte not requested Page 1 M® 50 of 52 ®ACCUTEST. M75288 - SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: M75286 Account: SHELLWIC - Shell Oil Project: SCMAW:97951986 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12227 Methods: SW846 6O1OB Matrix Type: SOLID Units: mg/kg Prep Date: '07/22/08 LCS Spikelot QC Metal Result MPLCS6O 8 Rec Limits Aluminum Antimony W Arsenic am • Barium am Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper Iron Lead 167 168 99,9 82-118 Magnesium Manganese Molybdenum Nickel Potassium Selenium am Silver am Sodium Strontium Thallium Tin Titanium - - Tungsten Vanadium Zinc Associated samples MP12227: M75286-1, M75286-2, M75286-3, M75286-9, M75286-5, M75286-6, M75286-7 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (anr) Analyte not requested Page 2 ®B 51 of 52 UAMMEST. M75286 =a SERIAL DILUTION RESULTS SUMMARY Login Number: M75286 Account: SHELLWIC - Shell oil Project: SCMAW:97451486 (REIMBMA) 590 Iyannough Road Hyannis MA QC Batch ID: MP12227 Methods: SW846 6010B Matrix Type: SOLID Units: ug/l Prep Date: 07/.22/.08 M75333-1 QC Metal Original SDL 1:5 RPD Limits Aluminum Antimony Arsenic am + • 1 Barium am Beryllium Boron Cadmium am Calcium Chromium am Cobalt Copper Iron Lead 27.4 29.5 7.7 0-10 Magnesium Manganese Molybdenum Nickel Potassium - Selenium am Silver am Sodium Strontium Thallium Tin Titanium Tungsten Vanadium Zinc Associated samples MP12227: M75286-1, M75286-2, M75286-3, M75286-4, M75286-5, M75286-6, M75286-7 Results < IDL are shown as zero for calculation purposes (*) Outside of QC limits (anr) Analyte not requested Page 1 Ell] 52 of 52 �ACCU7F,ST M75286 = _...-...... 4 ON T 14 November 28,2007 DHL#24644477756 Ms. Donna Miorandi Town of Barnstable,Health Inspector 200 Main Street Hyannis,MA 02601 Re: Groundwater Sampling Results,November 2007 Former Shell Branded Gasoline Station#137772 590 Iyannough Road - Hyannis, MA Dear Ms. Miorandi: Pursuant to your authorization Sovereign Consulting Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH), ethylene-dibromide (EDB), and ethanol. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remedidtion efforts. If you have any'questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVEREIGN CONSULTING,INC. ylvia M. Kirsch Project Manager Attachments: Laboratory Data Reports cc: with attachment Mr. David Weeks,Motiva MassDEP- SERO Sovereign File-EQ872 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 Air '_sue NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan t BWSC 123 This Notice is Related to Release Tracking Number • ® 17651 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 590 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Health Inspec. Donna Miorandi 2. Street Address: 200 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): 7 1.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. Q✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 590 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase 11 Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Sylvia Kirsch Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: skirsch@sovcon.com NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. {, FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts, Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. _ --r• .$'R;i:rw.7�'is• -..- _ „'V,'?dEe.:r:± _ _ � - ... '-;7E�ziRi?"�- 10stA.meri.,Cal THE.-LEADeg.INI Iv11=PdTAL 5 i=fi tNC' 2960 Foster Creighton Road Nashville,TN 37204`800-765-0980•Fax 615-726-3404 November 21,2007 1:38:39PM Client: Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Nbr: SAP 137772/EQ872 Attn: Jason Sherburne P/O Nbr: 97346878 Date Received: 11/07/07 SAMPLE IDENTIFICATION LAB NUMBER COLLECTION DATE AND TIME GT-1 NQK0739-01 11/05/07 11:35 GT4 NQK0739-02 11/05/07 12:30 GT-5 NQK0739-03 11/05/07 12:00 GT-7 NQK0739-04 11/05/07 12:15 M W-101 NQK0739-05 11/05/07 12:45 M W-102 NQK0739-06 11/05/07 13:00 MT-I/MT-3 NQK0739-07 11/05/07 10:30 MW-202 NQK0739-08 11/05/07 11:00 MW-202D NQK0739-09 11/05/07 11:10 An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at 1-800-765-0980. These results relate only to the items tested, and this report may not be reproduced except in full and with the permission of the Laboratory. Any opinions,if expressed,are outside the scope of the Laboratory's accredidation. This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is privileged and confidential. If you are not the intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you have received this material in error,please notify us immediately at 615-726-0177. *HydroCarbon Range data exclude area counts of any surrogate(s)and/or internal standards eluting in that range. *VPH C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. *Adjusted C5-C8 Aliphatic Hydrocarbons range excluded the concentrations fo MTBE,Benzene and toluene. *VPH C9-C 12 Aliphatic Hydrocarbons exclude target analytes eluting in that range AND concentration of C9-C 10 Aromatic Hydrocarbons. *Adjusted C9-C 12 Aliphatic Hydrocarbon range excludes the concentration of Ethylbenzene,m-,p-,and o-Xylene and the C9-C 10 Aromatic Hydrocarbon values. Additional Laboratory Comments: All samples were received in good condition,properly preserved,and properly labeled.All analyses were completed within holding times. All no responses from the attached"MCP Response Action Analytical Report Certification Form"are addressed below. E. The 8011 surrogate recovery in samples NQK0739-03,04&05 was biased high. The data was not impacted, the surrogate was noted with a'72"qualifier,and the data was accepted with no further analysis. F.The full MCP 8260B CAM analyte list was not reported.Only those analytes requested on the chain of custody by the client were reported. The Chain(s)of Custody,2 pages,are included and are an integral part of this report. Page 1 of 36 --------------............ TH15 LF-A13E1 'IN ekVIJk0t41 WTAI_`fESTIkG 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Arm Jason Sherburne Received: 11/07/07 08:00 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. All solids results are reported in wet weight unless specifically stated. Estimated uncertainity is available upon request. This report has been electronically signed. Report Approved By: Ken A.Hayes Senior Project Manager Page 2 of 36 • mert. .. ............ .... ...... ........... . � ���;IN (=1 VI l lu 1�1 J`41_:.°'� b� 1T�1 2960 Foster Creighton Road Nashville,TN 37204'800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Arm Jason Sherburne Received: 11/07/07 08:00 Sample Cooler Information Lab ID Cooler ID Temp Seals Containers Intact Preservation Confirmed On Ice 2213 4.6C Yes Yes Yes Yes I Page 3 of 36 MADEP MCP Response Action Analytical Report Certification Form Laboratory Name: IestAmerica Analytical Testing Corp. Project#: SAP 137772/EQ872 Project Location: SC-590Iyannough Road,Hyanni City: ��Jt MADEP RIN: This Form provides certifications for the following data set: Lab SDG# NQK0739 Sample Matrices: /Groundwater _Soil/Sediment _Drinking Water _Other _✓826013 _8151A 8330 _6010B _74.70A/]A MCP SW-846 Methods Used _8270C _8081A VPH _6020 _9014M 8082 8021 B EPH 7000 S 'Other An affirmative response to questions A,B,and C is r•equir•ed for-"Presumptive Certainty"Status A. Were all samples received by the laboratory in a condition consistent with r that described on the chain-of-custody documentation for the data set? L/Yes ,No B. Were all QA/QC procedures required for the specified analytical method(s) included in this report followed,including the requirement to note and discuss in a narrative QC data that did not meet appropriate performance / standards or guidelines? i� Yes _No C Does the analytical data included in this report meet all the requirements for "Presumptive Certainty",as described in section 2 0 of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? ✓Yes _No D. VPH and EPH methods only:Was the EPH or VPH method run without significant modifications,as specified in section 11 3? ,C Yes _No A response to questions E and F below is required for"Presumptive Certainty" status E Were all QC performance standards and recommendations for the specified methods achieved? Yes ✓No F. Were results for all analyte-list compounds/elements for the specified / method(s)reported? _ Yes ✓No .L All No answers must be addressed in an attached Laboratory Case Narrative I,the undersigned,attest under-the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is,to the best of my knowledge and belief,accurate and complete., Signature: $� y✓" Position: c h 1 tc :.................... #1=1I_ AtJ1=f$ 1I 1_T1ItQ1R1A .-` fo1 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Arm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Datefrime Date/Time Analyst Method Batch Sample ID:NQK0739-01(GT-1-Water)Sampled: 11/05/07 11:35 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112309 m,p-Xylene ND ug/L 4.00 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 CS-C8 Aliphatic Hydrocarbons,Unadjustet 140 ug/L 100 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjust, 212 ug/L 50.0 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons 138 ug/L 100 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons 96.6 ug/L 50.0 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112309 C9-C10 Aromatic Hydrocarbons 116 ug/L 50.0 1 11/05/07 11:35 11/13/07 19:11 KLS MADEP VPH 7112308 Surr:2,5-Dibromotoluene(F1D)(70-130%) 91% Surr:1,5-Dibromotoluene(P1D)(70-13091o) 103% Page 5 of 36 sAL 0 THE MA6.tAAt3 ekVlR'0N'4Ew `AL`Es-Tw , 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date rime Date rime Analyst Method Batch Sample ID:NQK0739-01(GT-1-Water)-cont.Sampled: 11/05/0711:35 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(EDB) 0.0593 ug/L 0.0208 t 11/09/0714:01 11/10/0719:58 BES SW8468011 7111746 Surr:1,3-Dichlorobenzene(44-150%) 138 Page 6 of 36 4. TestAmerica. THIE LEADER-IN C&.VK0NMENTXE,Tt 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980 Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Atm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Datefrime Analyst Method Batch .......... ................... ...... -- -- - ---......- .......... .. Sample ID:NQK0739-01(GT-1-Water)-cont.Sampled: 11/05/07 11:35 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/L 100 1 11/14/0700:00 11/15/0718:29 YAH SW8468260E 7111568 Page 7 of 36 ` �.... � 'LEAl3 Ii ElNV l 6'NM-N AL. Il,(�, 2960 Foster Creighton Road Nashville,TN 37204•800-765-0980•Fax 615-726-3404 _. .. _.. . Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 AM Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dill Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/Time Analyst Method Batch ............... ..... ... ------.-.-—---- ——.- ............................... ...---- - -- --- - - -- Sample ID:NQK0739-02(GT-4-Water)Sampled: 11/05/07 12:30 MADEP VP1I VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 12:30 11/13/07 19:42 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/0712.30 11/13/07 19:42 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 12:30 11/13/07 19:42 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 12:30 11/13/07 19:42 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 12:30 11/13/07 19:42 KLS MADEP VPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/07 12:30 11/13/07 19:42 KLS MADEPVPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 12:30 11/13/0719.42 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons,Unadjuste, ND ug/L 100 1 11/05/07 12:30 11/13/07 19:42 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjust. ND ug/L 100 1 11/05/07 12:30 11/13/07 19:42 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 12:30 11/13/07 19:42 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 12:30 11/13/07 19:42 KLS MADEP VPH 7112308 C9-C10 Aromatic Hydrocarbons ND ug/L 100 1 11/05/07 12:30 11/13/07 19:42 KLS MADEP VPH 7112308 Surr:1,5-Dtbromotoluene(FID)(70-I3091o) 83% Sum 1,5-Dibromotohtene(PID)(70-/30%) 97% Page 8 of 36 s • TO'st.A.4 Ic........................... THE MADEfit j j �1�1VIRONIfv1 NTgt ( � I f�^ 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Dateffime Date/time Analyst Method Batch .. . ................. .......... .- - --.----------.-.. ...------- -- - - - -------- - -. -.--..-...................... Sample ID:NQK0739-02(GT-4-Water)-cont.Sampled: 11/05/07 12:30 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(EDB) ND ug/I, 0.0197 1 11/09/07 14:01 11/10/07 20:17 BES SW846 8011 7111746 Sun:1,9-Dichlorobenzene(44-150%) 141 Page 9 of 36 T e... le ri..c a .............. THE EeAt��Id_�t3 l NVIfiC7hlMEN1`/1L`f�S^�INCa: 2960 Foster Creighton Road Nashville,TN 37204'800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Atm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/Time Analyst Method Batch ............... ......_...... ------------- -- - - --- -- ........-- -- -- - Sample ID:NQK0739-02(GT4-Water)-cont.Sampled: 11/05/07 12:30 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/L too 1 11/14/0700:00 11/15/0718:55 YAH SW8468260B 7111568 Page 10 of 36 ` To. 'stAmen.ca THE LEADER IN E14VIA04MENTAl_TE'STING 2960 Foster Creighton Road Nashville,TN 37204'800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Atm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/rime Analyst Method Batch ..-.-....-. . . .-....I------ - ------------- --------------------------- - --- -------—- --- - ------..-... .-.-...... -.-.-.... Sample ID:NQK0739-03(GT-5-Water)Sampled: 11/05/07 12:00 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether 4.42 ug/L 3.00 1 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/07 12:00 11/13/07 20:12 KLS MADEPVPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons,Unadjustei ND ug/L 100 1 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjust, ND ug/L 100 t 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 t 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 C9-C10 Aromatic Hydrocarbons ND ug/L 100 1 11/05/07 12:00 11/13/07 20:12 KLS MADEP VPH 7112308 Surr:1,5-Dibromoroluene(F1D)(70-130%) 91 Surr:1,5-Dibromotoluene(P1D)(70-13051) 104 Page 11 of 36 T���men,0...A.: THE LICIA It IW 1=HVIRONt�ENtAL•TI:�i ING 2960 Foster Creighton Road Nashville,TN 37204`800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/Time Analyst Method Batch ... . .. . ...... ......................... . ...-.-........- Sample ID: NQK0739-03(GT-5-Water)-cont.Sampled: 11/05/07 12:00 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(ED13) ND ug/L 0.0207 I 11/09/0714:01 11/10/0720:36 BES SW8468011 7111746 Surr:1,3-Dichlorobenzene(44-150%) 161% Z2 Page 12 of 36 F' en.,ca ------------ 'IH 5 LF-Aae ;1a Ef4VIR'ON ENTAL Ta ING 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/rime Analyst Method Batch -------------------- - -- -- --- --- - ........-....-.-_.-.-.... — ............ ....................-.-.-. Sample ID: NQK0739-03(GT-5-Water)-cont.Sampled: 11/05/07 12:00 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/L too 1 11/14/0700:00 11/15/0719:20 YAH SW8468260B 7111568 Page 13 of 36 THE LEADER IN ENVIRONMENTAL 3'CS'i INN' 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980`Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859) Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyse Result Units Flag Limit Factor Date/Time Date/fime Analyst Method Batch - ----- ------------------------------- -- ----— --- ----._.--.-..--....... -- -------- ....._.. - ----- Sample ID:NQK0739-04(GT-7-Water)Sampled: 11/05/07 12:15 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 CS-C8 Aliphatic Hydrocarbons,Unadjuste4 ND ug/L 100 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjust, 102 ug/L 100 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 C9-C12A]iphaticHydrocarbons ND ug/L 100 1 11/05/07 12:15 11/13/07 20:43 KLS MADEP VPH 7112308 C9-CIO Aromatic Hydrocarbons ND ug/L 100 1 11/05/07 12:15 11/13/07 20.43 KLS MADEP VPH 7112308 Surr:2,5-Dibromotoluene(F1D)(70-1309/) 94 Surr:2,5-Dibromotoluene(PID)(70-130%) 107 Page 14 of 36 J , THE LEADER Ahl ENV IA.6 M)=NTAL_TESTING 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905E South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Atm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date rime Datefrime Analyst Method Batch .. Sample ID: NQK0739-04(GT-7-Water)-cont.Sampled: 11/05/07 12:15 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(EDB) ND ug/1. 0.0201 1 11/09/07 14:01 11/10/07 21:15 BES SW84e 8011 7111746 Sum 1.3-DEchlorobenzene(44-I50%) 162% Z2 Page 15 of 36 L j LEAf3E12.1N 514V iONMENTAL TEVIM$ 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859) Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Datefrime DatefFime Analyst Method Batch i _........ .... ...................... -- ----- --- - -_.-......._ ....... ....-.-........_....... ... Sample ID: NQK0739-04(GT-7-Water)-cont.Sampled: 11/05/07 12:15 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ugiL 100 1 11/14/0700:00 11/15/0719:46 YAH SW8469260B 7111568 Page 16 of 36 s . T'OstAmertca THE LF-A080 IN ENVIRONMENTAL TE,9TTN`G 2960 Foster Creighton Road Nashville,TN 37204`800-765-0980•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905E South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/Time Analyst Method Batch ............................. . ............ .._ . ..--------..--......-. .. .-....... ..-........... Sample ID: NQK0739-05(MW-101-Water)Sampled: 11/05/07 12:45 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 12:45 11/13/07 21:13 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/07 12:45 11/13/07 21:13 KLS MADEPVPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 12:45 11/13/07 21:13 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 12:45, 11/13/07 21:13 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/0712.45 11/13/07 21:13 KLS MADEPVPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/07 12:45 11/13/07 21:13 KLS MADEP VPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 12:45 11/13/0721.13 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons,Unadjuste( ND ug/L too 1 11/05/07 12:45 11/13/07 21:13 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjusb ND ug/L too 1 11/05/07 12:45 11/13/07 21:13 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 12:45 11/13/07 21:13 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons ND ug/L 100 t 11/05/07 12:45 11/13/07 21:13 KLS MADEP VPH 7112308 C9-C10 Aromatic Hydrocarbons ND ug/L 100 1 11/05/07 12:45 11/13/07 21:13 KLS MADEP VPH 7112308 Surr:2,5-Dibromoioluene(FID)(70-13091.) 83 Surr:2,5-Dibromololuene(PID)(70-130%) 97 Page 17 of 36 • tAmedica THE l.EADMthl E.NVI lONMEitilTAL ESTI tit : 2960 Foster Creighton Road Nashville,TN 37204`800-765-0980 Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905E South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dill Extracted Analysis Analyte Result Units Flag Limit Factor Dateffime Datefrime Analyst Method Batch ------------ --- - ------------------------ ------ --- -- .-.-.- .- -- --- ---------- _....-.... . . .-...-_..-------- - - -- Sample ID:NQK0739-05(MW-101-Water)-cont.Sampled: 11/05/07 12:45 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(EDB) ND ug/L 0.0203 1 11/09/0714:01 11/10/0721:35 BES SW8468011 7111746 Surr:1.3-Dichlorobenzene(44-150%) I55% Z2 Page 18 of 36 • T�s.t.'Amenca.. ----------------- TESTING2960 Foster Creighton Road Nashville.TN 37204.800-765-0980 Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/Time Analyst Method Batch Sample ID:NQK0739-05(MW-101-Water)-cont.Sampled: 11/05/07 12:45 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/L 100 1 11/14/0700:00 11/15/0720:11 YAH SW8468260B 7111568 Page 19 of 36 i' . T THE.LEAbEI��� EI�fVIf2�1�Eivt�trl fAL.'f�8 f Ii�G' 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859) Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Datetrime Dateffime Analyst Method Batch Sample ID:NQK0739-06(MW-102-Water)Sampled: 11/05/07 13:00 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 13:00 11/13/07 21:43 KLS MADEPVPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons,Unadjuste, ND ug/L 100 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjusb ND ug/L 100 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 C9-C10 Aromatic Hydrocarbons ND ug/L 100 I 11/05/07 13:00 11/13/07 21:43 KLS MADEP VPH 7112308 Surr:1,5-Dibromololuene(FID)(70-130% 90 Surr:1,5-Dibromololuene(PID)(70-13051.) 103 Page 20 of 36 menca., fEI(=LIEADEWIN C VlAONM1=i\1TA1_: 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980`Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859) Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Ann Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date rime Dateffime Analyst Method Batch -------- - - --- - .- ..... .-..-. ..-.-. -.-.--.,..-.-.............. - - —-- -- --- ------------- Sample ID: NQK0739-06(MW-102-Water)-cont.Sampled: 11/05/07 13:00 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(ED13) ND ug/L 0.0200 1 11/09/0714:01 11/10/0721:54 BES SW8468011 7111746 Sum,1,3-Dichlorobenzene(44-150916) 141 Page 21 of 36 ' T��menca THE I_F-Ar1EIt$N ItNVll;t0t`lM NfAL tE$I`IN'"(3 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Atm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyse Result Units Flag Limit Factor Dateffime Datefrime Analyst Method Batch ....... -- -------------------- ......... . _ - ----......- - Sample ID: NQK0739-06(MW-102-Water)-cont.Sampled: 11/05/0713:00 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/L 100 1 11/14/0700:00 11/15/0720:37 YAH SW8468260B 7111568 Page 22 of 36 '�st.Ame, ' . THE LeAom Ili EfikVm NMtNt..AL're,-S f119,,0, 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980`Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/Time Analyst Method Batch ----------- ----------------------- ----------- - --------- - --- ----- ------- -------. ---- - -- . .------- Sample ID:NQK0739-07(MT-1/MT-3-Water)Sampled: 11/05/07 10:30 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEPVPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 10.30 11/13/07 22:14 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons,Unadjuste, ND ug/L 100 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjust, ND ug/L too 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 C9-C10 Aromatic Hydrocarbons ND ug/L 100 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 Surr:2.5-Dibromotoluene(F1D)(70-130916) 86% Surn 2,5-Dibromotoluene(P1D)(70-1309/6) 101% Page 23 of 36 • . TO si �t"A.m—,e- n ` ca .............. .......... ......--------------- THE LEA113MIN CNV1R0NMENTA.L TE$1 IN'C 2960 Foster Creighton Road Nashville,TN 37204'800-765-0980•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Dateffime Datefrime Analyst Method Batch _. ...... .... Sample ID:NQK0739-07(MT-UNIT-3-Water)-cont.Sampled: 11/05/07 10:30 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(EDB) ND ug/L 0.0204 1 11/09/0714:01 11/10/0722:14 BES SW8468011 7111746 Surr:1,3-Dichlorohenzene(44-150%) 147 Page 24 of 36 �J • enca.. THt L1=ADE � l l l F�l 1�CAI 'l� �1 '!1"a` 2960 Foster Creighton Road Nashville,TN 37204'800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attu Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/I'ime Date/Time Analyst Method Batch --- -- - -- - --- ---- ----_..-...-._....... - —- -------..-- --- - .......-......... Sample ID: NQK0739-07(MT-1/MT-3-Water)-cont.Sampled: 11/05/07 10:30 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/L 100 1 11/14/0700:00 11/15/0721.02 YAH SW8468260B 7111568 Page 25 of 36 I s 414r=LF-AbER IN E=4Vlft0141v1ENtA.-:-3°I STING._- 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859) Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Arm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Daterfime Date rime Analyst Method Batch - ---- - --- --- --------------- Sample ID:NQK0739-08(MW-202-Water)Sampled: 11/05/07 11:00 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 I 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEPVPH 7112309 Toluene ND ug/L 3.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 11:00 11/13/07 22.44 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons,Unadjuste( ND ug/L 100 t 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,UnadjusG ND ug/L too 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 CS-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons ND ug/L too 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 C9-C10 Aromatic Hydrocarbons ND ug/L 100 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 Surr:1,5-Dibromotolisene(F1D)(70-130%) 85% Surr:2,5-Dibromotoluene(P1D)(70-130%) 99% Page 26 of 36 i� Tei:si.,,.A. , - -t .... . .......... menca ...... .............. .......... .. .......... TH LEd,MkIN (=.h1V112C7hI#vf1=NTAI-:..TMSTIN'd 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859) Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Atm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/rime Date/rime Analyst Method Batch Sample ID:NQK0739-08(MW-202-Water)-cont.Sampled: 11/05/07 11:00 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(ED13) ND ug/L 0.0198 1 11/09/0714:01 11/10/0722:33 BES SW8468011 7111746 Surr:1,3-Dichlorobenzene(44-150%) 126 Page 27 of 36 r . T ` I'' 1 THiE LEE4M_Wllvi V kVIR0FtME14TAL rrtatiN''.�'_ 2960 Foster Creighton Road Nashville.TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859) Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Ann Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dill Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/Time Analyst Method Batch ......... ...._..-... ......- ...-....... ...... ------- Sample ID: NQK0739-08(MW-202-Water)-cont.Sampled: 11/05/07 11:00 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/L 100 1 11/14/07 00:00 11/15/07 2128 YAH SW8468260B 7111568 Page 28 of 36 • t n '.......... . ............ THE LEAK A" NVIRONMeNT E TEISTI40: 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980`Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Ann Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Datefrime Datefrime Analyst Method Batch ..I.....- .... . ................. .. ...... _.-- .......... ......-......-.... . ..—.. - - -- Sample ID:NQK0739-09(MW-202D-Water)Sampled: 11/05/07 11:10 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/07 11:10 11/13/0723.14 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 11:10 11/13/07 23.14 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 o-Xylene ND ug/L 2-00 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/0711.10 11/13/07 23:14 KLS MADEPVPH 7112309 C5-C8 Aliphatic Hydrocarbons,Unadjustei ND ug/L 100 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjust. ND ug/L 100 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons ND ug/L too 1 11/05/07 11:10 11/13/07 23.14 KLS MADEP VPH 7112308 C9-C10 Aromatic Hydrocarbons ND ug/L too 1 11/05/07 11.10 11/13/07 23:14 KLS MADEP VPH 7112308 Surr 2,5-Dibromotoluene(FID)(70-130%) 91 Surr:2,5-Dibromotoluene(PID)(70-130/) 104 Page 29 of 36 I � • TO�mertoa .... THE LEADER IN ENVIRdkMENTAL` CtTIN_G 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Atm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Dateffime Date/Time Analyst Method Batch .-.. Sample ID: NQK0739-09(MW-202D-Water)-cont.Sampled: 11/05/07 11:10 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(EDB) ND ug/L 0.0199 1 11/09/07 14:01 11/10/07 22:53 BES SW8468011 7111746 Surr:1,3-Dichlorobenzene(44-150%) 135% - Page 30 of 36 1' . Te . .ertca... 'tHE-LtAi>eR Ito �.NV tOnlMENTAL.TIESTI140; 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-5901yannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Datefrime Daterrime Analyst Method Batch ................... .. - - ----— - ----------- -- - -------......--.......- ..-.........-----.... Sample ID: NQK0739-09(MW-202D-Water)-cont.Sampled: 11/05/07 11:10 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/L too 1 11/14/0700:00 11/15/0721:53 YAH SW8468260B 7111568 Page 31 of 36 n-ca" H LAC3f=1`2�IN1V EKtGi�1MEN'1"AE•`�ES �N'�: 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Arm Jason Sherburne Received: 11/07/07 08:00 SAMPLE EXTRACTION DATA WtNol Extraction Parameter Batch Lab Number Extracted Extracted Vol Date Analyst Method EDB and DBCP by EPA Method 8011 SW846 8011 7111746 NQK0739-01 33.70 2.00 11/09/07 14.01 BES EPA 504.1 SW846 8011 7111746 NQK0739-02 35.50 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-03 33.80 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-04 34.90 2.00 11/09/07 14.01 BES EPA 504.1 SW846 8011 7111746 NQK0739-05 34.50 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-06 35.00 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-07 34.30 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-08 35.30 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-09 35.10 2.00 11/09/07 14:01 BES EPA 504.1 MADEP VPH MADEP VPH 7112308 NQK0739-01 5.00 5.00 11/05/07 11:35 KLS MADEP MADEP VPH 7112308 NQK0739-02 5.00 5.00 11/05/07 12:30 KLS MADEP MADEP VPH 7112308 NQK0739-03 5.00 5.00 11/05/07 12:00 KLS MADEP MADEP VPH 7112308 NQK0739-04 5.00 5.00 11/05/07 12:15 KLS MADEP MADEP VPH 7112308 NQK0739-05 5.00 5.00 11/05/07 12:45 KLS MADEP MADEP VPH 7112308 NQK0739-06 5.00 5.00 11/05/07 13:00 KLS MADEP MADEP VPH 7112308 NQK0739-07 5.00 5.00 11/05/07 10:30 KLS MADEP MADEP VPH 7112308 NQK0739-08 5.00 5.00 11/05/07 11:00 KLS MADEP MADEP VPH 7112308 NQK0739-09 5.00 5.00 11/05/07 11:10 KLS MADEP Page 32 of 36 � 1 ` TeistAmertca THE lEADER.'1N 1=Rylk 114l Nt,aL TtST O 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 PROJECT QUALITY CONTROL DATA Blank Analyte Blank Value Q Units Q.C.Batch Lab Number Analyzed Date/Time ----- ----— .. ............ ... ............ MADEP VPH 7112308-BLK1 Methyl tert-Butyl Ether <0.380 ug/L 7112308 7112308-BLKI 11/13/07 18:41 Benzene <0.610 ug/L 7112308 7112308-BLKI 11/13/07 18:41 Toluene <0.600 ug/L 7112308 7112308-BLKI 11/13/07 18:41 Ethylbenzene <0.460 ug/L 7112308 7112308-BLKI 11/13/07 18:41 m,p-Xylene <0.840 ug/L 7112308 7112308-BLKI 11/13/07 18:41 o-Xylene <0.710 ug/L 7112308 7112308-BLKI 11/13/07 18:41 Naphthalene 2.93 ug/L 7112308 7112308-BLKI 11/13/07 18:41 C5-C8 Aliphatic Hydrocarbons,Unadjuste< <50.0 ug/L 7112308 7112308-BLKI 11/13/07 18:41 C9-C 12 Aliphatic Hydrocarbons,Unadjust, <50.0 ug/L 7112308 7112308-BLKI 11/13/07 18:41 C5-C8 Aliphatic Hydrocarbons <50.0 ug/L 7112308 7112308-BLKI 11/13/07 18:41 C9-C 12 Aliphatic Hydrocarbons <50.0 ug/L 7112308 7112308-BLKI 11/13/07 18:41 C9-C10 Aromatic Hydrocarbons <50.0 ug/L 7112308 7112308-BLKI 11/13/07 18:41 Surrogate:2,5-Dibromotoltlene(FID) 81% 7112308 7112308-BLKI 11/13/07 18:41 Surrogate:2,5-Dibromotoluene(PID) 95% 7112308 7112308-BLKI 11/13/07 18:41 EDB and DBCP by EPA Method 8011 7111746-BLKI 1,2-Dibromoethane(EDB) <0.00500 ug/L 7111746 7111746-BLKI 11/10/07 17:41 Surrogate:1,3-Dichlorobenzene 116% 7111746 7111746-BLKI 11/10/07 17:41 Selected Volatile Organic Compounds by EPA Method 8260B 7111568-BLKI Ethanol <74.4 ug/L 7111568 7111568-BLKI 11/15/07 18:04 Surrogate:1,2-Dichloroeihone-d9 102% 7111568 7111568-BLKI 11/15/07 18:04 Surrogate:DibromoJluoromethane 1000/0 7111568 7111568-BLKI 11/15/07 18:04 Surrogate:Toluene-& 101% 7111568 7111568-BLKI 11/15/07 18:04 Surrogate:d-BromoJluorobenzene 101% 7111568 7111568-BLKI 11/15/07 18.04 S Page 33 of 36 L JO�mertca. THE LIE AOtRI i 514VIR01 te11=NTAL`Fl="ST04r 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980 Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: l 1/07/07 08:00 PROJECT QUALITY CONTROL DATA LCS Target Analyzed Analyte Known Val. Analyzed Val Q Units %Rec. Range Batch Date/Time ..... ...................... ....-.-.. - ......-.......-.--.. MADEP VPH 7112308-BS1 Methyl tert-Butyl Ether 50.0 49.1 ug/L 98% 70-130 7112308 11/14/07 08:22 Benzene 50.0 52.5 ug/L 105% 70-130 7112308 11/14/07 08:22 Toluene 50.0 53.9 ug/L 108% 70-130 7112308 11/14/07 08:22 Ethylbenzene 50.0 54.5 ug/L 109% 70-130 7112308 11/14/07 08:22 m,p-Xylene 100 112 ug/L 112% 70-130 7112308 11/14/07 08:22 o-Xylene 50.0 55.0 ug/L 110% 70-130 7112308 11/14/07 08:22 Naphthalene 50.0 50.5 ug/L 101% 70-130 7112308 11/14/07 08:22 C5-C8 Aliphatic Hydrocarbons,Unadjusted 150 152 ug/L 102% 70-130 7112308 11/14/07 08:22 C9-C12 Aliphatic Hydrocarbons,Unadjusted 100 97.5 ug/L 98% 70-130 7112308 11/14/07 08:22 C9-C 10 Aromatic Hydrocarbons 50.0 51.6 ug/L 103% 70-130 7112308 11/14/07 08:22 Surrogate:2,5-Dibromotoluene(FID) 40.0 35.0 87% 70-130 7112309 11/14/07 08:22 Surrogate:2,5-Dibromotoluene(PID) 40.0 40.3 101% 70-130 7112308 11/14/07 08:22 EDB and DBCP by EPA Method 8011 7111746-BSI 1,2-Dibromoethane(EDB) 0.286 0.3429 ug/L 120% 60-141 7111746 11/10/07 18:01 Surrogate:I,3-Dichlorobenzene 5.71 6.91 121% 44-150 7111746 11/10/07 18:01 Selected Volatile Organic Compounds by EPA Method 8260B 7111568-BS1 Ethanol 5000 4630 MNRI ug/L 93% 36-150 7111568 11/15/07 16:22 Surrogate:1,2-Dichloroethane-d4 50.0 4%6 99% 60-140 7111568 11/15/07 16:22 Surrogate:DibromoJluoromethane 50.0 49.5 99% 75-124 7111568 11/15/07 16:22 Surrogate:Toluene-d8 50.0 50.8 102% 78-121 7111568 11/15/07 16:22 Surrogate:a-BromoJluorobenzene 50.0 479 96% 79-124 7111568 11/15/07 16:22 Page 34 of 36 m 'tca.. _.. . .... ............ -------------- THe LEAoeplvd mvmbr4mtw AL 11=enl�'G 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Ann Jason Sherburne Received: 11/07/07 08:00 PROJECT QUALITY CONTROL DATA LCS Dup Spike Target Sample Analyzed Analyte Orig.Val. Duplicate Q Units Conc %Rec. Range RPD Limit Batch Duplicated Date/Time MADEP VPH 7112308-BSD1 Methyl tert-Butyl Ether 49.1 ug/L 50.0 98% 70-130 0.07 25 7112308 11/13/07 17:40 Benzene 52.5 ug/L 50.0 105% 70-130 0.08 25 7112308 11/13/07 17:40 Toluene 53.7 ug/L 50.0 107% 70-130 0.4 25 7112308 11/13/07 17:40 Ethylbenzene 54.7 ug/L 50.0 109% 70-130 0.3 25 7112308 11/13/07 17:40 m,p-Xylene 113 ug/L 100 113% 70-130 0.3 25 7112308 11/13/07 17:40 o-Xylene 55.1 ug/L 50.0 110% 70-130 0.2 25 7112308 11/13/07 17:40 Naphthalene 49.0 ug/L 50.0 98% 70-130 3 25 7112308 11/13/07 17:40 C5-C8 Aliphatic Hydrocarbons,Unadjusted 151 ug/L 150 100% 70-130 1 25 7112308 11/13/07 17:40 C9-C12 Aliphatic Hydrocarbons,Unadjusted 86.9 ug/L 100 87% 70-130 12 25 7112308 11/13/07 I7:40 C9-C10 Aromatic Hydrocarbons 51.2 ug/L 50.0 102% 70-130 0.7 25 7112308 11/13/07 17:40 Surrogate:2,5-Dibromotoluene(F!D) 36.9 ug/L 40.0 92% 70-130 7112308 11/13/07 17:40 Surrogate:2,5-Dibromotoluene(P/D) 41.4 ug/L 40.0 104% 70-130 7112308 11/13/07 17:40 Selected Volatile Organic Compounds by EPA Method 8260B 7111568-BSD1 Ethanol 4910 ug/L 5000 98% 36-150 6 48 7111568 11/15/07 16:48 Surrogate:1,2-Dichloroethane-d4 50.3 ug/L 50.0 101% 60-140 7111568 11/15/07 16:48 Surrogate:DibromoJluoromethane 49.9 ug/L 50.0 100% 75-124 7111568 11/15/07 16:48 Surrogate:Toluene-& 50.7 ug/L 50.0 101% 78-121 7111568 11/15/07 16:48 Surrogate:4-Bromofluorobenzene 48.1 ug/L 50.0 96% 79-124 7111568 11/15/07 16:48 Page 35 of 36 1 Te, A THE L AD TAL`TIE8't 10 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 DATA QUALIFIERS AND DEFINITIONS MNR1 There was no MS/MSD analyzed with this batch due to insufficient sample volume. See Blank Spike. pH<2 pH<2 Z2 Surrogate recovery was above the acceptance limits. Data not impacted. ND Not detected at the reporting limit(or method detection limit if shown) METHOD MODIFICATION NOTES Page 36 of 36 encc Nashville. TN COOLER RECE Cooler Received/Opened On_11/07/07 @ 08:00 NQK0739 1. Tracking#_2Zt_-?,, (last 4 digits,FedEx) Courier: _FED-EX IR Gun ID_A01124 2. Temperature of rep.sample or temp blank when opened.�,&1-_Degrees Celsius 3. If Item#2 temperature is 0°C or less,was the representative sample or temp blank frozen? YE$O..NA 4. Were custody seals on outside of cooler? &...NO...NA If yes,how many and where: ' —(—fj O; 5. Were the seals intact,signed,and dated correctly? L kYES...NNO.. 6. Were custody papers inside cooler? I certify that I opened the cooler and answered questions 1 6(jntiall 7. Were custody seals on containers: YES (NO' and Intact r, Were these signed and dated correctly? 8. Packing mat1 user.-Bubblewrap Plastic bag Peanuts Vermiculite Foam Insert Paper Other None 9. Cooling process: Ic Ice-pack Ice(direct contact) Dry ice Other None 10. Did all containers arrive in good condition(unbroken)? YE ..NO...NA 11. Were all container labels complete(#,date,signed,pres.,etc)? YE ...NO...NA 12. Did all container labels and tags agree with custody papers? ..NO...NA 13a. Were VOA vials received? v CVTSi'NO...NA b. Was there any observable headspace present in any VOA vial? YY 0- �� NA•' 1P�✓� 14. Was there a Trip Blank in this cooler? YES NA If multiple coolers,sequence# l7lo7 I certify that I unloaded the cooler and answered questions 7 14(intiall r 15a. On pres'd bottles,did pH test strips suggest preservation reached the correct pH level? YES..NB4!P b. Did the bottle labels indicate that the correct preservatives were used (P..NO...NA If preservation in-house was needed,record standard ID of preservative used here 16. Was residual chlorine present? YES...NO:<0 I certify that 1 checked for chlorine and PH as per SOP and answered questions 15 16(intial) _ 17. Were custody papers properly filled out(ink,signed,etc)? YES ..NO...NA 18. Did you sign the custody papers in the appropriate place? ES .NO...NA 19. Were correct containers used for the analysis requested? ES .NO...NA 20. Was sufficient amount of sample sent in each container? (9..NO...NA ►_certify that 1 entered this project into LIMS and answered questions 17 20(intial) (ma's 1 certify that 1 attached a label with the unique LIMS number to each container(intial) 21. Were there Non-Conformance issues at login? YES..®O Was a PIPE generated?YES BIN lliokcu in sInpmcni i'uolcr ltcccipl ponn.dor I.F-1 Ilc�iscd:)'6 Ui I.nd ol'Fonn TEST AMERICA 4 Shell Oil Products US Chain Of Custody Record INCIDENT S:(S&E ONLY) 2690 FOSTER CREIGHTON,NASHVILLE,TIN i7204 SOP us Project Manager to be Invoiced: _ PHONE eG0•765.0960 FAXii 616.726 140a ❑SCIENCE&ENGINEERING []CHECh 50x TO VE0.:fr IF NG INCIDENT NUMBER APPLIES 97346878 DATE:J v r-,.y / 24 TAT ONLY ❑TECHNICAL SERVICES NAME OF PERSON TO BILL: SOVEREIGN SAP# PAGE.�_ Of []ID08 W.NINTH AVE,KING OF PRUSSIA,PA 19406 �----- '137772 [[�BILLI CONSULTANT SHELL EE:DAVE WEEKS _ ,e ITF ADDRESS(SNeet entl Cllyl: 'ONSI:I.TANT GWPANv r Sovereign Consulting Inc. 590 I annou h Road,Hyannis,MA PRD,EGT DONrA�T,9<P� e. CONSULTANT PROJECT NO.:.E0872 ADDRESS. 905B South Main Street-Suite 202 S Ivia Kirsch CITV SAMPLER NAMEI'+,,PI�„ -�- Mansfield,MA 02408 / NQK0739 ,ELEn E FAX E.MAa ✓ l<1�Q/:C.If: O r • felc;:�ro (5018) 339-3 000 (508)339-3248 TURNARouND TIME(CALENDAR DAvsJ. 59 REQUESTED ANALYSIS(Please place checkmarks next to desired E 11/2��0� 23: Q STANDARD(10 DAY) ❑S DAYS ❑3 DAYS ❑2 DAYS ❑24 HOURS ❑RESULTS NEEDED ON W EEKFND LBC;Qratdry:-. Deliverables: Copy to SovCon.Copy to Shell EE Notes TEMPERATURE ON RECEIPT C' t0 N SPECIAL INSTRUCTIONS OR NOTE INCLUDE MDL'S 1N THE DATA DELIVERABLES ❑Site is Gwa,please note Detection limit RQ's Go 10 MADEP MCP Response Action Analytical Report Certification Form requires completion;MA DEPVPH/EPH policy Appendix 3 j VPH/EPH Data repOn info needed for VPH/EPH anal III%Report in dry wei ht where needed and according to DEP Methods', C SAMPLING PRESERVATIVE IL C NO.OF 7 M m Field Sample Identification MATRIX CONT. Q « p •:� '.'ea13': P DATE TIME 2 W W ' VSE HCL HNO3 H2SCM NONE OTHER �.'. m< ONLY YI L % -Z Z a e Tune Rocnvea b,(eion-,e) Cu Mody Bed Number RN,n— b,( Ina I� Da:B T,nc uV.dtl . - eoe I,.:et Dme ,mo ne _ Ram4u,snn b:,:KnAluf<1 1�.. I'2005 Fov,son )�•��i�?Goo j f f SOVEPEIGN CONSULTING INC . November 28,2007 DHL#24644167251 Town of Hyannis Town Engineer 367 Main Street Hyannis,MA 02601 Re: Groundwater Sampling Results,November 2007 Former Shell Branded Gasoline Station#137772 590 Iyannough Road Hyannis,MA Dear Town Engineer: Pursuant to your authorization Sovereign Consulting Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH), ethylene-dibromide (EDB), and ethanol. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVEREIGN CONSULTING,INC. 1 y via M.Kirsch Project Manager Attachments: Laboratory Data Reports cc: with attachment Mr. David Weeks,Motiva MassDEP- SERO Sovereign File—EQ872 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan L BWSC 123 This Notice is Related to E Release Tracking Number KI 17651 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 590 lyannough Rd. City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Hyannis,Town Engineer 2. Street Address: 367 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): 01.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. Z 3. Check to indicate if the analytical results are attached. (If item 2.above is checked,the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 590 lyannough Rd. City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase 11 Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types(e.g., soil,groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E.Contact information related to the party providing this notice: Contact Name: Sylvia Kirsch Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: skirsch@sovcon.com i NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.qov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. 1 -..','•- "` tmn ,. "�O0��bJim ......................... 0� ���� 2960 Foster Creighton Road Nashville,TN 37204'600-765 0980'Fax 615-726 3404 November 21,2007 1:38:39PM Client: Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Nbr: SAP 137772/EQ872 Attn: Jason Sherburne P/O Nbr: 97346878 Date Received: 11/07/07 SAMPLE IDENTIFICATION LAB NUMBER COLLECTION DATE AND TIME GT-I NQK0739-01 11/05/07 11:35 GT4 NQK0739-02 11/05/07 12:30 GT-5 NQK0739-03 11/05/07 12:00 GT-7 NQK0739-04 11/05/07 12.15 MW-101 NQK0739-05 11/05/07 12:45 MW-102 NQK0739-06 11/05/07 13:00 MT-1/MT-3 NQK0739-07 11/05/07 10:30 MW-202 NQK0739-08 11/05/07 11:00 MW-202D NQK0739-09 11/05/07 11:10 An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at 1-800-765-0980. These results relate only to the items tested, and this report may not be reproduced except in full and with the permission of the Laboratory. Any opinions,if expressed,are outside the scope of the Laboratory's accredidation. This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is privileged and confidential. If you are not the intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited- If you have received this material in error,please notify us immediately at 615-726-0177. *HydroCarbon Range data exclude area counts of any surrogate(s)and/or internal standards eluting in that range. *VPH C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. *Adjusted C5-C8 Aliphatic Hydrocarbons range excluded the concentrations fo MTBE,Benzene and toluene. *VPH C9-C12 Aliphatic Hydrocarbons exclude target analytes eluting in that range AND concentration of C9-C 10 Aromatic Hydrocarbons. *Adjusted C9-C 12 Aliphatic Hydrocarbon range excludes the concentration of Ethylbenzene,m-,p-,and o-Xylene and the C9-C 10 Aromatic Hydrocarbon values. Additional Laboratory Comments: All samples were received in good condition,properly preserved,and properly labeled.All analyses were completed within holding times. Allno responses from the attached"MCP Response Action Analytical Report Certification Form"are addressed below. E. The 8011 surrogate recovery in samples NQK0739-03,04&05 was biased high. The data was not impacted, the surrogate was noted with a'72"qualifier,and the data was accepted with no further analysis. F.The full MCP 8260B CAM analyte list was not reported.Only those analytes requested on the chain of custody by the client were reported. TheChain(s)of Custody,2 pages,are included and are an integral part of this report. Page 1 of 36 ........ � ': � :T',S 2960 Foster Creighton Road Nashville.TN 37204 800-765.0980•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. All solids results are reported in wet weight unless specifically stated. Estimated uncertainity is available upon request. This report has been electronically signed- Report Approved By: Ken A.Hayes Senior Project Manager Page 2 of 36 ... ....... THE L ; 111fi1 � NI_ 11 �`s. 2960 Foster Creighton Road Nashville,TN 37204.800-765 0980•Fax 6157263404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 Sample Cooler Information Lab ID Cooler ID Tegip Seals Containers Intact Preservation Confirmed On Ice 2213 4.6C Yes Yes Yes Yes Page 3 of 36 I MADEP MCP Response Action Analytical Report Certification Form 1 Laboratory Name: IestAmerica Analytical Testing Corp. Project#: SAP 137772/EQ872 < Project Location: SC-590 Iyannough Road,Hyanni City: ' "S MADEP RTN: This Form provides certifications for the following data set: Lab SDG# NQK0739 Sample Matrices: ✓Groundwater _Soil/Sediment —Drinking Water —Other /8260B _8151A 8330 _6010B _7470AJ1 A MCP SW-846 u Methods Used T 8270C —8081A 2/VPH —6020 _9014M _8082 8021B _EPH `7000 S -,"Other- An affirmative response to questions A,B,and C is r-equirvd for"Presumptive Certainty"Status A.• Were all samples received by the laboratory in a condition consistent with r that described on the chain-of-custody documentation for the data set? ✓Yes —No B. Were all QA/QC procedures required for-the specified analytical method(s) included in this report followed,including the requirement to note and discuss in a narrative QC data that did not meet appropriate performance / standards or guidelines? V Yes _No VI 9f C Does the analytical data included in this report meet all the requirements for "Presumptive Certainty",as described in section 2 0 of the MADEP document CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? Yes —No D. VPH and EPH methods only: Was the EPH or VPH method run without significant modifications,as specified in section 11 3? 2 Yes —No A response to questions E and F below is required for"Presumptive Certainty" status E Were all QC performance standards and recommendations fbr the specified methods achieved? Yes /No F. Were results for all analyte-list compounds/elements for the specified / method(s)reported? — Yes ✓No All No answers must be addressed in an attached Laboratory Case Narrative I,the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for-obtaining the information,the material contained in this analytical report is,to the best of my knowledge and belief,accurate and complete., �./ r � Signature: �� . Zr---� Position: Sc h to r Te ................. � � . - { ��/Il'�� fi1 131 7 2960 Foster Creighton Road Nashville,TN 37204'800-765-MO•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order. NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Ann Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyse Result Units Flag Limit Factor Daterfime Date/Cime Analyst Method Batch ....-. ....... .. ............. .... . .. . .... ......... ........ ........ .. . . ... ... .... . .... ..... ........ ... ..... Sample ID: NQK0739-07(MT-1/MT-3-Water)Sampled: 11/05/07 10:30 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 1 11/05/07 10:30 11/13/01 22:14 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 1030 11/13/07 22:14 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/0710.30 11/13/07 22:14 KLS MADEP VPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons,Unadjuste, ND ug/L 100 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112309 C9-C12 Aliphatic Hydrocarbons,Unadjust. ND ug/L 100 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 C9-C 12 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 C9-C10 Aromatic Hydrocarbons ND ug/L 100 1 11/05/07 10:30 11/13/07 22:14 KLS MADEP VPH 7112308 Surr:2,5-Dibromotoluene(FID)(70-130%) 86% Surr:2,5-Dibromotoluene(PID)(70-130'6) 101% Page 23 of 36 T11111 I e--S" A� --m-en T440 TA!Tr lly` 2960 Foster Creighton Road Nashville,TN 37204.OW-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Ann Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyse Result Units Flag Limit Factor Datelrime Daterrime Analyst Method Batch .. ....... .. ............. ... ... .. - ..... . .... . . ...... . .............. Sample ID: NQK0739-07(MT-1/MT-3-Water)-cont.Sampled: 11/05/07 10:30 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(EDB) ND uglL 0.0204 1 11/09/0714:01 11/10/0722:14 BES SW8468011 7111746 Surr:I,3-Dichlorobenzene(44-150%) 147 Page 24 of 36 I .................. .... ..... THE Le 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980•Fax 615-7263404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Datefrime Date/rime Analyst Method Batch .......................... ............. ....-.-....-..................... .. ... ...-.-.... ....... ....... Sample ID:NQK0739-07(MT-1/MT-3-Water)-cont.Sampled: 11/05/07 10:30 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/L 100 1 11/14/0700:00 11/15/0721:02 YAH SW8469260D 7111568 Page 25 of 36 Tiez, Stx- e 0 ue�1.1 Ewi �N(i EN'Ci41.7t�: 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13359] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/0708:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/Time Analyst Method Batch ....... ............. .... ...... .........-.................... - -- -----.....-. ......- .-..--........... ........... . -. - ........... Sample ID:NQK0739-08(MW-202-Water)Sampled: 11/05/07 11:00 MADEP VPH VPH Preservation pH<2 Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 Benzene ND u91L 1.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 o-Xylene ND u8/L 2.00 ► 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 Naphthalene ND ug/L 5.00 1 11/05/07 11:00 11/13/07 22.44 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons,Unadjuste, ND ug/L 100 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjuso ND ug/1, too 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 11:00 11/13/07 22.44 KLS MADEP VPH 71 t2308 C9-C12 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 C9-C10 Aromatic Hydrocarbons ND ug/L [Go 1 11/05/07 11:00 11/13/07 22:44 KLS MADEP VPH 7112308 Surr.2,5-Dibrommoluene(F1D)(70-130'�0) 85 Surr:1,5-Dibromotoluene(P1D)(70-13091.) 99 Page 26 of 36 Boo .... . _. ' �CAOWIIO ewlk N 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980 Fax 615-7263404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date/Time Analyst Method Batch ... ....... ... ....._. Y Sample ID:NQK0739-08(MW-202-Water)-cont.Sampled: 11/05/07 11:00 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(EDB) ND ugIL 0.0198 1 11/09/0714:01 11/10/072233 BES SW9468011 7111746 Surr:43-Dichlorobenzene(44-/50%) 126 Page 27 of 36 �I ' s 71 'oqi'1 C1 b;; stAz�L � �.` ..... T" 14 Q1 2960 Foster Creighton Road Nashville,TN 37204'800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Date rime Analyst Method Batch .. .......... ........... .... ...... . ..................... . .. . .. ... ................. . . .... .... ............ . .... .. ... . . Sample ID: NQK0739-08(MW-202-Water)-cont.Sampled: 11/05/0711:00 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ug/1. 100 1 11/14/07 00:00 11/15/07 21:28 YAH sW6468260B 7111568 Page 28 of 36 nc. .Q. UK 'r1 /11 +IV(RtjltEfilT�4fT11fG - 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980'Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/fime Date/Time Analyst Method Batch ..... ..... ......... ... ... — ----- .. .. ..._ ... . .... .. .-------- Sample ID:NQK0739-09(MW-202D-Water)Sampled: 11/05/0711:10 MADEP VPH VPH Preservation pHQ Methyl tert-Butyl Ether ND ug/L 3.00 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 Benzene ND ug/L 1.00 t 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 Toluene ND ug/L 3.00 1 11/05/07 11:10 11/13/0723:14 KLS MADEP VPH 7112308 Ethylbenzene ND ug/L 1.00 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 m,p-Xylene ND ug/L 4.00 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 o-Xylene ND ug/L 2.00 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 Naphthalene ND ug[L 5.00 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons,Unadjustet ND ug/L 100 1 11/05/07 11:10 11/13/07 23.14 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons,Unadjuso ND ug/L 100 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 C5-C8 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 C9-C12 Aliphatic Hydrocarbons ND ug/L 100 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 C9-C 10 Aromatic Hydrocarbons ND ug/L too 1 11/05/07 11:10 11/13/07 23:14 KLS MADEP VPH 7112308 Surr:1,5-Dibromoroluene(FID)(70-130%) 91 Surr:1,5-Dibromoroluene(PID)(70-130Y.) 104 Page 29 of 36 en. .. . .. _ ... ..:.. ............... ..... l I if �1lIROTfly/ 1�3 fk .. 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Atm Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Date/Time Daterfime Analyst Method Batch ..... .. ....... . . .- .......... Sample ID:NQK0739-09(MW-202D-Water)-cont.Sampled: 11/05/07 11:10 EDB and DBCP by EPA Method 8011 1,2-Dibromoethane(EDB) ND ug/t. 0.0199 1 11/09/0714:01 11/10/0722:53 BES sw9468011 7111746 Surr. 0-Dichlorobenzene(44-I50%) 135% - ` Page 30 of 36 I I Tet4117 .............. r C LEAb- , V lttt}i� �tr A1_.1"�b"1 INS.' 2960 Foster Creighton Road Nashville,TN 37204'800-765-0980'Fax 615 7263404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 ANALYTICAL REPORT Report Dil Extracted Analysis Analyte Result Units Flag Limit Factor Dateffime Date rime Analyst Method Batch ...... .. ... .... .....................-.. -------- .- -----... . Sample ID: NQK0739-09(MW-202D-Water)-cont.Sampled: 11/05/07 11:10 Selected Volatile Organic Compounds by EPA Method 8260B Ethanol ND ugiL too t 11/14/0700.00 11/15/0721:53 YAH stva4692608 7111568 I Page 31 of 36 � 1.......... i 1 .... Tf L #L[�Ef2l�l � 2960 Foster Creighton Road Nashville,TN 37204'800-765-0980•Fax 615-726-3404,ie Client Sovereign Consulting(Mansfield)/SHELL(13859) Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attlt Jason Sherburne Received: 11/07/07 08:00 SAMPLE EXTRACTION DATA WtNol Extraction Parameter Batch Lab Number Extracted Extracted Vol Date Analyst Method ............... - - ----.... ........ ... EDB and DBCP by EPA Method 8011 _ SW846 8011 7111746 NQK0739-01 33.70 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-02 35.50 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-03 33.80 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-04 34.90 2.00 11/09/07 14:01 BES EPA 504.1 SW846 9011 7111746 NQK0739-05 34.50 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-06 35.00 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-07 34.30 2.00 11/09/07 MOO BES EPA 504.1 SW846 8011 7111746 NQK0739-08 3530 2.00 11/09/07 14:01 BES EPA 504.1 SW846 8011 7111746 NQK0739-09 35.10 2.00 11/09/07 14:01 BES EPA 504.1 MADEP VPH MADEP VPH 7112308 NQK0739-01 5.00 5.00 11/05/07 11:35 KLS MADEP MADEP VPH 7112308 NQK0739-02 5.00 5.00 11/05/07 12:30 KLS MADEP MADEP VPH 7112308 NQK0739-03 5.00 5.00 I1/05/07 12.00 KLS MADEP MADEP VPH 7112309 NQK0739-04 500 5.00 11/05/07 12:15 KLS MADEP MADEP VPH 7112308 NQK0739-05 5.00 5.00 11/05/07 12:45 KLS MADEP MADEP VPH 7112308 NQK0739-06 5.00 5.00 11/05/07 13:00 KLS MADEP MADEP VPH 7112308 NQK0739-07 5.00 5.00 11/05/07 10.30 KLS MADEP MADEP VPH 7112308 NQK0739-08 5.00 5.00 11/05/07 I1:00 KLS MADEP MADEP VPH 7112308 NQK0739-09 5.00 5.00 11/05/07 11:10 KLS MADEP Page 32 of 36 I THE MADE#2:114t .1 2960 Foster Creighton Road Nashville,TN 37204 800-765-0980•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859) Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 PROJECT QUALITY CONTROL DATA Blank Analyte Blank Value Q Units Q.C.Batch Lab Number Analyzed Daterrime ............... .... .......................... ................. . .. ......-........... . MADEP VPH 71l2308-BLKI Methyl tert-Butyl Ether <0.380 ug/L 7I12308 7112308-BLKI 11/13/07 18:41 Benzene <0.610 ug/L 7112308 7112308-BLKI 11/13/07 18:41 Toluene <0.600 ug/L 7112308 7112308-BLKI 11/13/07 18:41 Ethylbenzene <O-460 ug/L 7112308 7112308-BLKI 11/13/07 18:41 m,p-Xylene <0.840 ug/L 7112308 7112308-BLKI 11/13/07 18:41 o-Xylene <0-710 ug/L 7112308 7112308-BLKI 11/13/07 18:41 Naphthalene 2.93 ug/L 7112308 7112308-BLKI 11/13/07 18:41 C5-C8 Aliphatic Hydrocarbons,Unadjuste( <50.0 ug/L 7112308 71 12308-BLK 1 11/13/07 18:41 C9-C12 Aliphatic Hydrocarbons,Unadjuste <50.0 ug/L 7112308 7112308-BLKI 11/13/07 18:41 C5-C8 Aliphatic Hydrocarbons <50.0 ug/L 7112308 7112308-BLKI 11/13/07 18:41 C9-C12 Aliphatic Hydrocarbons <50-0 ug/L 7112308 7112308-BLKI 11/13/07 18:41 C9-CIO Aromatic Hydrocarbons <50.0 ug/L 7112309 7112308-BLKI 11/13/07 18:41 Surrogate:2,5-Dibromotohtene(FID) 81% 7112309 7112308-BLKI 11/13/07 18:41 Surrogate:2,5-Dibromoioluene(PID) 95% 7112308 7112308-BLKI 11/13/07 18:41 EDB and DBCP by EPA Method 8011 7111746-BLKI 1,2-Dibromoethane(EDB) <0.00500 ug/L 7111746 7111746-BLKI 11/10/07 17.41 Surrogate:l,3-Dichlorobenzene 116% 7111746 7111746-BLKI 11/10/07 17:41 Selected Volatile Organic Compounds by EPA Method 8260B 7111568-BLKI Ethanol <74.4 ug/L 7111568 7111568-BLKI 11/15/07 19:04 Surrogate:I,2-Dichloroethane-d4 102% 7111568 7111568-BLKI 11/15/07 18:04 Surrogate:DibromoJluoromethane 100% 7111568 7111568-BLKI 11/15/07 1&04 Surrogate:Toluene-& 101% 7111568 7111568-BLKI 11/15/07 18:04 Surrogate:4-BromoJluorobenzene 101% 7111569 7111568-BLKI 11/15/07 18:04 Page 33 of 36 -Z;St N�U; E, �"M.52 WI iOfjj�"�:.TO STING 2960 Foster Creighton Road Nashville,TN 37204.800-765-0980•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 PROJECT QUALITY CONTROL DATA LCS Target Analyzed Analyze Known Val. Analyzed Val Q Units %Rec. Range Batch Date/Time ... . ........ ............. ......... .. . . ... .......... .. . ..-... . ....... .. ..-...... . MADEP VPH 7112308-BSI Methyl tert-Butyl Ether 50.0 49.1 ug/L 98% 70-130 7112308 11/14/07 08:22 Benzene 50.0 52.5 ug/L 105% 70-130 7112308 11/14/07 08:22 Toluene 50.0 53.9 ug/L 108% 70-130 7112308 11/14/07 08:22 Ethylbenzene 50.0 54.5 ug/L 109% 70-130 7112308 11/14/07 08:22 m,p-Xylene too 112 ug/L 112% 70-130 7112308 11/14/07 0822 o-Xylene 50.0 55.0 ug/L 110% 70-130 7112308 11/14/07 08:22 Naphthalene 50-0 50.5 ug/L 101% 70-130 7112308 11/14/07 08:22 C5-C8 Aliphatic Hydrocarbons,Unadjusted 150 152 ug/L 102% 70-130 7112308 11/14/07 08:22 C9-C12 Aliphatic Hydrocarbons,Unadjusted 100 97.5 ug/L 98% 70-130 7112308 11/14/07 08:22 C9-C 10 Aromatic Hydrocarbons 50.0 51.6 ug/L 103% 70-130 7112308 11/14/07 08:22 Surrogate:2,5-Dibromotoluene(F1D) 40.0 35.0 87% 70-130 7112308 11/14/07 08:22 Surrogate:2,5-Dibromotoluene(P1D) 40.0 40.3 101% 70-130 7112308 11/14/07 08:22 EDB and DBCP by EPA Method 8011 7111746-BSI 1,2-Dibromoethane(EDB) 0.286 0.3429 ug/L 120% 60-141 7111746 11/10/07 18:01 Surrogate:1,3-Dichlorobenzene 5.71 6.91 121% 44-150 7111746 11/10/07 18:01 Selected Volatile Organic Compounds by EPA Method 8260B 7111568-BSI Ethanol 5000 4630 MNRI ug/L 93% 36-150 7111568 11/15/07 16:22 Surrogate:1,2-Dichloroethane-d4 50.0 49-6 99% 60-140 7111568 11/15/07 16:22 Surrogate:Dibromofluoromeihane 50.0 49.5 99% 75-124 7111568 11/15/07 16.22 Surrogate:Toluene-& 50.0 50.8 102% 78-121 7111568 11/15/07 I6:22 Surrogate:a-Bromofluorobenzene 50.0 47-9 961/6 79-124 7111568 11/15/07 16:22 Page 34 of 36 �. .............. TH 19l ;� VIRIfN �lt 'T 11�f 2960 Foster Creighton Road Nashville,TN 37204 800-765.0980•Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(138591 Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 lyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Attn Jason Sherburne Received: 11/07/07 08:00 PROJECT QUALITY CONTROL DATA LCS Dup Spike Target Sample Analyzed Analyte Orig.Val. Duplicate Q Units Conc %Rec. Range RPD Limit Batch Duplicated DatefTime ... ... ... ..... .... ... .... ... ...... . ............ .... ......I ........... ... ...._._. _ MADEP VPH 7112308-BSD1 Methyl tert-Butyl Ether 49.1 ug/L 50.0 98% 70-130 0.07 25 7112308 11/13/07 17:40 Benzene 52.5 ug/L 50.0 105% 70-130 0.09 25 7112308 11/13/07 17:40 Toluene 53.7 u9/L 50.0 107% 70-130 0.4 25 7112308 11/13/07 17:40 Ethylbenzene 54.7 ug/L 50.0 109% 70-130 0.3 25 7112308 11/13/07 17:40 m,p-Xylene 113 ug/L 100 113% 70-130 0.3 25 7112308 11/13/07 17-40 o-Xylene 55.1 ug/L 50.0 110% 70-130 02 25 7112308 11/13/07 17:40 Naphthalene 49.0 ug/L 50.0 98% 70-130 3 25 7112308 11/13/07 17:40 CS-C8 Aliphatic Hydrocarbons,Unadjusted 151 ug/L 150 100% 70-130 1 25 7112308 11/13/07 17:40 C9-C12 Aliphatic Hydrocarbons,Unadjusted 86.9 ug/L 100 87% 70-130 12 25 7112308 11/13/07 17:40 C9-C10 Aromatic Hydrocarbons 51.2 ug/L 50.0 102% 70-130 0.7 25 7112308 11/13/07 17:40 Surrogate:2,5-Dibromotoluene(FID) 36.9 ug/L 40.0 92% 70-130 7112309 11/13/07 17:40 Surrogate:2.5-Dibromotoluene(PID) 41.4 ug/L 40.0 104% 70-130 7112308 11/13/07 17:40 Selected Volatile Organic Compounds by EPA Method 8260B 7111568-BSD1 Ethanol 4910 ug/L 5000 98% 36-150 6 48 7111568 11/15/07 16:48 Surrogate:1,2-Dichloroethane-d4 503 ug/L 50.0 101% 60-140 7111568 I1/15/07 16:48 Surrogate:Dibromofluoromethane 49.9 ug/L soo 100% 75-124 7111568 11/15/07 16:48 Surrogate:Toluene-d8 50.7 ug/L 50.0 101% 78-121 7111568 11/15/07 16:48 Surrogate:4-Bromofluorobenzene 48.1 ug/L 50.0 96% 79-124 7111568 I1/15/07 16:48 Page 35 of 36 ...........�.... ..��� ...... .......... ..................... ............... 29M Foster Creighton Road Nashville.TN 37204 800-765-0980`Fax 615-726-3404 Client Sovereign Consulting(Mansfield)/SHELL(13859] Work Order: NQK0739 905B South Main Street,Suite 202 Project Name: SC-590 Iyannough Road,Hyannis,MA Mansfield,MA 02048 Project Number: SAP 137772/EQ872 Ann Jason Sherburne Received: 11/07/07 08:00 DATA QUALIFIERS AND DEFINITIONS MNRI There was no MS/MSD analyzed with this batch due to insufficient sample volume. See Blank Spike. pH<2 pH<2 Z2 Surrogate recovery was above the acceptance limits. Data not impacted. ND Not detected at the reporting limit(or method detection limit if shown) METHOD MODIFICATION NOTES Page 36 of 36 I , �X4:4%Yr.ni: ;}4; yy�:ry��.�:V..:v`:�f.•�v.:f.;5 Nashville. TN COOLER RECE Cooler Received/Opened On_11/07/07 @ 0&00 NQK0739 1, Tracking# � (last 4 digits,FedEx) Courier: —FED-EX IR Gun ID_A01124 2. Temperature of rep.sample or temp blank when opened.q,.b Degrees Celsius 3. If Item#2 temperature is 0"C or less,was the representative sample or temp blank frozen? YES09,.NA 4. Were custody seals on outside of cooler? Y' ...NO...NA If yes,how many and where: '—'=p, /fir/; 5. Were the seals intact,signed,and dated correctly? Y ...NO...NA 6. Were custody papers inside cooler? ...NA I certify that I opened the cooler and answered questions 1-6(intial) 7. Were custody seals on containers: YESGO ' -,1 andIntact YES...N ..NA. Were these signed and dated correctly? YES...NO.. 8. Packing mat'l us Bubblewrap Plastic bag Peanuts Vermiculite Foam Insert Paper Other None 9. Cooling process: Ic, Ice-pack Ice(direct contact) Dry ice Other None 10. Did all containers arrive in good condition(unbroken)? YE ..NO...NA 11. Were all container labels complete(#,date,signed,Ares.,etc)? YE ...No...NA 12. Did all container labels and tags agree with custody papers? (!!5..NO...NA 13a. Were VOA vials received? C S�.NO...NA b. Was there any observable headspace present in any VOA vial? NA 14. Was there a Trip Blank in this cooler? YES . ..NA If multiple coolers,sequence# P tj171'U7 1 certify that I unloaded the cooler and answered questions 7-14(intial) 44 N./1 15a. On pres'd bottles,did pH test strips suggest preservation reached the correct pH level? YES..NB;V b. Did the bottle labels indicate that the correct preservatives were used 9�_.NO...NA If preservation in-house was needed,record standard ID of preservative used here 16. Was residual chlorine present? YES...NO:(g) I certify that I checked for chlorine and pH as per SOP and answered questions 15 16(intial) 17. Were custody papers properly filled out(ink,signed,etc)? YES ..NO...NA 18. Did you sign the custody papers in the appropriate place? ES .N0...NA 19. Were correct containers used for the analysis requested? ES .NO...NA 20. Was sufficient amount of sample sent in each container? ...NA 1 certify that I entered this project into LIMS and answered questions 17 20(intial) 1 certify that I attached a label with the unique LIMS number to each container(intial) 21. Were there Non-Conformance issues at login? YES..®O Was a PIPE generated?YES BIB HiAvu in shipmcm t'uulcr I(cccipt Punn.dnc LF-1 kcxiscd 9 6:11i Liid of Form I I TEST AMERICA 4 Shell Oil Products US Chain Of Custody Record INCIDENT#:(SSE ONLY) 0 2690 FOSTER CREIGHTON,NASHVILLE,TN 37204 SOP US Project Manager to be Invoiced: -. PHONE 600•765.0980 FAXn 676.12E-1404 ❑SCIENCE&ENGINEERING [�CHECK SOX TO VERJF p'NO INCIDENT NUMBER APPLIES 97346878 DATE:1�=SL,;a=.�� 24 TAT ONLY ❑TECHNICAL SERVICES _ NAME OF PERSON TO BILL: SOVEREIGN SAP PAGE:�_ Of / 1008 W.NINTH AVE,KING OF PRUSSIA,PA 19406 37772 "T l_0 SILL CONSULTAI SHELL EE:DAVE WEEKS t ITF AODRES5151,rr1 end"0' LONSW.TANT 17 -W Sovereign Consulting Inc. 590 I jannough Road H annis,MA FRo�ECT cuNl.ar=•P<• e. CONSULTANT PROJECT NO.: E0872 ADDRESS. 905B South Main Street•Suite 202 S Ivia Kirsch Ap �!r -- SAMPIEP NAME!S,,Prni r Mansfield,MA 02408 (1/1 ��t�r o Nt�K0739 rAz MAIL fELf°NONE E 4 r (508)339-3200 (508)339.3248 11/21/07 23:59 TURNAROUND TIME(CALENDAR oars): REQUESTED ANALYSIS(Please place checkmarks next to desired E 0 STANDARD(10 DAY) ❑S DAYS ❑3 DAYS ❑2 DAYS ❑24 HOURS ❑RESULTS NEEDED ON WEEKEND LStOlatdry. Deliverables: Copy to SOVCon.Copy to Shell EE Notes TEMPERATURE ON RECEIPT C' tD N SPECIAL INSTRUCTIONS OR NOTES INCLUDE MOL'S IN THE DATA DELIVERABLES O Slte Is GWl,please note Detection limit RQ'S O -------------------- !0 ' MADEP MCP Response Action Analytical Report Certification Form requires completion;MA DEPVPH/EPH policy Appendix 3 > VPH/EPH Data re rt info needed for VPH/EPH anal sis;Re rt in dry wei ht where needed and according to DEP Methods; O SAMPLING PRESERVATIVE 0. 0 Field Sample Identification MATRI% coNT. Q w p DATE TIME W W Yam,, HCL HNO3 H250a NONE OTHER .4 3 Lc , o — v 0 Z n e Tune Rp,:rivN b,(9ign Mur el Custody Seat Numbm Rew4— Dare T— c,,INd u Dam � 'Te Rrae.ea yj ' l a — ::,,t::J. e!vlei i :oof Rm—n Number Fee 1073 THE COMMONWEALTH OF MASSACHUSETTS $10o.00 Town of Barnstable Board of Health This is to Certify that Route 132 Sav-On Gas, Inc. 590Iyannough Road, Hyannis,MA 02601 Is Hereby Granted a License FOR: STORING OR HANDLING 111 GALLONS OR MORE OF HAZARDOUS MATERIALS. -------------------------------------------------------------------------------------------------------------------------------------------------------------------- This license is granted in conformity with the Statutes and ordinances relating there to, and and expires 6/30/2010 unless sooner suspended or revoked. ---------------------------------------- WAYNE MILLER,M.D.,CHAIRMAN PAUL J.CANNIFF,D.M.D. 6/30/2009 JUNICHI SAWAYANAGI THOMAS A. MCKEAN,R.S.,CHO Director of Public Health ,.._ Town of Barnstable ;. Barnstable 0 Regulatory' Services Department bc&d • Public Health Division 9r� 1'�: ��� 200 Main Street, Hyannis NIA 02601 A����a 2007 Office: 508-862-4644 Thomas F.Geiler,Director FAX: 508-790-6304 Thomas A.McKean,CHO Application Fee: $100.00 ASSESSORS MAP AND PARCEL NO. r C)"r"7 _DATE lli 4D APPLICATION FOR PE&MIT TO STORE AND/OR UTILIZE MORE THAN 111 GALLONS OF HAZARDOUS MATERIALS FULL NAME OF APPLICANT �Q NA IME OF ESTABLISHMENT S)q-V D (0 4S • ADDRESS OF ESTABLISHMENT n i5 TELEPHONE NUMBER o SOLE OWNER:,,�YES NO IF APPLICANT IS A�} PARTNERSHIP,FULL NAME AND HOME ADDRESS..4 ALL PARTNERS: 1)-411 h4c S-w-6wi 6fi-�- r M_#djR)61 IW2 _;*L IF APPLICANT IS A CORPORATION: FEDERAL IDENTIFICATION NO. ry ral STATE OF INCORPORATION Y FULL NAME AIND HOME ADDRESS OF: PRESIDENT Gl �> c� — 1(� Y1�Q.� -9SL_ - yp�nylo� Imo- O."a— 02(.09Y TREASURER CLERK (/Yl ,/S�!QIATU O P R F APLI1AINT RE,STRICTIONS: ROME ADDRESS %CA(6yv,,6" 0(. *,t( 01}' M""n 5— llOME TELEPHONE QAHazmatlHaz Mat Anplicmion2008.DOC 1 1 • FAX COVER SHEET Sav--Qn Gas Inc Route 132 Sav-On Gas, Inc JayMart, Inc Yarmouthport Getty Office Address: 326 West Main St.- nis, MA 02601 one: 508-778-4124 Fax: 508-771-5733 DATE: AD SENT TO: &fn. IOIe FAX: `— C� — 6J��I • FROM: PAGES: COMMENTS: • Town of Barnstable Barnstable m.r o Regulatory' Services.Department ��abl > idRElsrael,i; t Public Health Division 1 �'A ����' 200 Main Street,Hyannis IVIA 02601 2007 Office; 508-862•4644 Thomas F.Geiler,Director FAX: 508-790-6304 Thomas A.McKean,CHO Application Fee: $100.00 ASSESSORS MAP AND PARCEL NO.. DATE CV 1, - APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE MORE THAN I II GALLONS OF HAZARDOUS MATERIALS FULL NAME OF APPLICANT `� NA1VIE OF ESTABLISHMENT R�z� �. . S�-V ` D (OAS lam. • ADDRESS OF ESTADM21 Iy t T J TELEPHONE NUIVIBER — SOLE OWNER:�YES NO IF APPLICANT IS A PARTNERSHIP,FULL NAI-YU AND HOME ADDRESS OF ALL PARTNERS: A IF APPLICANT IS A CORPORATION: FEDERAL IDENTIFICATION NO. STATE OF INCORPORATION FULL NAIV2 A D HOME ADDRESS OF: PRESIDENT -Vrv�®►.� \(s car-.tia�.cL OC. Y�V►0�1�1�(Jao- v✓�, aZ�o�S TREASURER CLERK • IS 7.GNATUR OF APPLICANT RESTRICTIONS: 1-10ME AD�RESS ( J3!. (YYU>�^ PIOME TELEPRONE () 5- Q:1Hazrriat\hlaz�1V Apphcation2008.DOC „� :53 7054/21�13 R.OUTE.132 = 2 04 8 r; SAV G-ON AS”INC ' q 590IYANOO GHROAD P ' "{ HYAN IS MA 02601 DATE AY TO THE_; t ORDER OF # -77 n DOLLARS t 7 © f Banknorth, N ' Massachuutts{ ♦ a a s� � � yp���NFL g.. t n• squ FOR �QG}'�V �. ' A HORIZED SIGNATURE ! 3. II'.00�20.48iI' �: 2 L L;3�70.5-4 51: -' 8 '24 2"7 78 266�I'` roe," Town of Barnstable Office: 508-862-4644 '1• Fax: 508-790-6304 a .� Regulatory Services Department • B",Nnwar:I� Public Health Division MASS, Thomas A.McKean,CHO 200 Main Street, Hyannis, MA 02601 Payment Receipt ;Hazardous Materials Payment received: $0.00 (Check) on 8/7/2015 ;Check number: 150 Check amount: $0.00 Name on check: Sav-On:George's Garage--DUPLICATE PMT-Check return 1 ,Business: George's Garage Owner: JAY IMAD ENTR IYANNOUGH RD LLC Address: 590 IYANNOUGH ROAD/RTE132, Hyannis Note: 8/13 DUPLICATE PMT-Ann P. returned Check to Vanessa/Mailed Check on 8/17/15 _ —' Town of Barnstable BIKE ram, Regulatory Services ti • Richard V. Scali, Director ' '" MASS. ' Public Health Division iOrFo ' Thomas McKean, Director 200 Main Street, Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 Application Fee: $100.00 ASSESSORS MAP AND PARCEL NO. 3(I V V 1 f7 DATE / APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE MORE THAN 111 GALLONS OF HAZARDOUS MATERIALS 1 FULL NAME OF APPLICANT S NAME OF ESTABLISHMENT � . • ADDRESS OF ESTABLISHMENT ¢ TELEPHONE NUMBER SOLE OWNER: YES NO IF APPLICANT IS A PARTNERSHIP,FULL NAME AND HOME ADDRESS OF ALL PARTNERS: 'IF APPLICANT IS A CORPORATION: FEDERAL IDENTIFICATION NO. �L7 STATE OF INCORPORATION y FULL NAME AND HOME ADDRESS.OF:,r PRESIDENT . ° ,TREASURER ,. - CLERK N E O PPLICANT RESTRICTIONS: HOME ADD SS, J� � HOME TELEPHONE# J:UiAZAPP.D0Q '. % ; 4U h. * Town of Barnstable Office: 508-862-4644 Fax: 508-790-6304 .� Regulatory Services Department • wsrnr ' Public Health Division Mom. Thomas A. McKean,CHO 139— 200 Main Street, Hyannis, MA 02601 Payment Receipt ;Hazardous Materials Payment received: $100.00 (Check) on 8/7/2015� �� i Check number: 150 Check amount: $100.00 Name on check: Sav-On Business: George's Garage Owner: JAY IMAD ENTR IYANNOUGH RD LLC Address: 590 IYANNOUGH ROAD/RTE132, Hyannis i i • • 7� A&J T� -- s Town of Barnstable Aq W'U `Icq 4V a Regulatory Services : B I�' *� A1L'.ASS, L Thomas F. Geiler. Director 1 Public Health Division _ Thomas McKean, Director 200 Main Street Hyannis, MA 02601 G Office: 508-862-4644 Fax: 508-790-6304 (/ To: MOTIVA ENTERPRISES LLC Date Tuesday,February 20, 2007 1100 LOUISIANA AVE HOUSTON TX 77002 RE:Underground Storage Tank at: 590 IYANNOUGH ROAD/ROUTE132 Map Parcel: 311017 Tank NO: 01 Tag NO: 00890 Our records indicate that your underground fuel(or chemical)storage tank is over 20 years old,and has not been removed as required by section 326-3: subsection 2 of the Town of Barnstable Code regarding fuel and chemical storage systems. You are directed to remove this tank within sixty(60)days from the date of this notice. After your tank is removed, please furnish this office evidence in the form of a permit from your local Fire Department within ninety(90) days of the receipt of this notice. You may request a hearing provided a written petition requesting same is received by the Board of Health within ten(10) days after this order is served. Per Order of the Board of Health Thomas A.McKean,RS,CHO Health Agent Town of Barnstable Y� Regulatory Services � � ti AO LL. Thomas F. Geiler. Director Public Health Division Thomas McKean, Director 200 Main Street, Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 To: MOTIVA ENTERPRISES LLC Date Tuesday,February 20,2007 1100 LOUISIANA AVE HOUSTON TX 77002 RE: Underground Storage Tank at: 590 IYANNOUGH ROAD/ROUTE132 Map Parcel: 311017 Tank NO: 02 Tag NO: 00891 Our records indicate that your underground fuel(or chemical)storage tank is over 20 years old,and has not been removed as required by section 326-3: subsection 2 of the Town of Barnstable Code regarding fuel and chemical storage systems. You are directed to remove this tank within sixty(60)days from the date of this notice. After your tank is removed, please furnish this office evidence in the form of a permit from your local Fire Department within ninety(90)days of the receipt of this notice. You may request a hearing provided a written petition requesting same is received by the Board of Health within ten(10) days after this order is served. Per Order of the Board of Health Thomas A.McKean,RS,CHO Health Agent Town of Barnstable Regulatory Services IRA Thomas F. Geiler. Director MASS, Public Health Division rfo Ma's a Thomas McKean, Director 200 Main Street, Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 To: MOTIVA ENTERPRISES LLC Date Tuesday,February 20,2007 1100 LOUISIANA AVE HOUSTON TX 77002 RE: Underground Storage Tank at: 590 IYANNOUGH ROAD/ROUTE132 Map Parcel: 311017 Tank NO: 06 Tag NO: 00000 Our records indicate that your underground fuel(or chemical)storage tank is over 20 years old,and has not been removed as required by section 326-3: subsection 2 of the Town of Barnstable Code regarding fuel and chemical storage systems. You are directed to remove this tank within sixty(60)days from the date of this notice. After your tank is removed, please furnish this office evidence in the form of a permit from your local Fire Department within ninety(90)days of the receipt of this notice. You may request a hearing provided a written petition requesting same is received by the Board of Health within ten(10) days after this order is served. Per Order of the Board of Health Thomas A.McKean,RS,CHO Health Agent Town of Barnstable ►E Regulatory Services k.. A� i''y[( Thomas F. Geiler. Director 4' �tA55, t i `,b,v Public Health Division fFe��a Thomas McKean, Director 200 Main Street, Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 To: MOTIVA ENTERPRISES LLC Date Tuesday,February 20,2007 1100 LOUISIANA AVE HOUSTON TX 77002 RE: Underground Storage Tank at: 590 IYANNOUGH ROAD/ROUTE132 Map Parcel: 311017 Tank NO: 07 Tag NO: 00000 Our records indicate that your underground fuel(or chemical)storage tank is over 20 years old,and has not been removed as required by section 326-3: subsection 2 of the Town of Barnstable Code regarding fuel and chemical storage systems. You are directed to remove this tank within sixty(60)days from the date of this notice. After your tank is removed, please furnish this office evidence in the form of a permit from your local Fire Department within ninety(90)days of the receipt of this notice. You may request a hearing provided a written petition requesting same is received by the Board of Health within ten(10) days after this order is served. Per Order of the Board of Health Thomas A.McKean,RS,CHO Health Agent `op�HE rok Town of Barnstable v Office.508-862-4644 Public Health Division Fax:508-790-6304 a"","SS. 200 Main Street• Hyannis, MA 02601 1639. prEDMn+° TOXIC AND HAZARDOUS MATERIALS INSPECTION REPORT Business Name: Is 0 _ �� _ Date: Location/Mailing Address: 0 an 3 Q U J Contact Name/Phone: O$ Inventory Total Amount: � SDS: 3 CQJI.�J License#: liq 4 Tier II Ab Labeling: Spill Plan: es Oil/WaterSeparator: (, n-J Floor Drains: d Emergency Numbers: e Storage Areas/Tanks: Wmwe o fl Qffirde a fQ-CL ,Sp 0400 Emergency/Containment Equipment: 1 S ' Waste Generator ID: IA L9- 7.71W)s Waste Product: 1 amp k Date&Amount of Last Shipment/Frequency: I AS / /-0 Licensed Waste Hauler&Destination: ( Pw olr orf Other Waste Disposal Methods: LIST OF TOXIC AND HAZARDOUS MATERIALS NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous material use, storage and disposal of 111 gallons or more requires a license from the Public Health Division. Antifreeze Dry cleaning fluids Automatic transmission fluid Other cleaning solvents&spot removers Engine and radiator flushes Bug and tar removers Hydraulic fluid (including brake fluid) Windshield wash otor oils Miscellaneous Corrosives Gasoline,jet fuel, aviation gas Cesspool cleaners Diesel fuel, kerosene, #2 heating oil Disinfectants Miscellaneous petroleum products: Road salts grease, lubricants, gear oil Refrigerants' Degreasers for engines&garages Pesticides: Caulk/Grout insecticides, herbicides, rodenticides Battery acid (electrolyte)/batteries Photochemicals(Fixers) Rustproofers Photochemicals(Developer) Car wash detergents Printing ink Car waxes and polishes Wood preservatives(creosote) Asphalt&roofing tar Swimming pool chlorine Paints, varnishes, stains, dyes Lye or caustic soda Lacquer thinners Miscellaneous Combustible Paint&varnish removers, deglossers Leather dyes Miscellaneous Flammables Fertilizers Floor&furniture strippers PCB's Metal polishes Other chlorinated hydrocarbons Laundry soil &stain removers (including carbon tetrachloride) (including bleach) Any other products with "poison labels" (including chloroform, formaldehyde, hydrochloric acid, other acids) VIOLATIONS: ORDERS: INFORMATION/RECOMMENDATIONS: S A Inspector:, Facility Representative: A J \41�� WHITE COPY- HEALTH DEPARTMENT/CANARY COPY- BUSINESS Number Fee 1244 THE COMMONWEALTH OF MASSACHUSETTS $150.00 Town of Barnstable Board of Health This is to Certify that BA Gas Station #321 .-----------------------------------------------------------------•----.....----------.....-------------------------------------- 590 Iyannough Road, Hyannis, MA ------------------------------------------------------------------------------------------------------------------------------------------------------------------------ Is Hereby Granted a License For: Storing or Handling 500 gallons or more of Hazardous Materials. ------------- ------------------------------------------------------------------------------------------------------------------------------------------------------ Restrictions: This license is granted in conformity with the Statutes and ordinances relating there to, and expires 06/30/2021 unless sooner suspended or revoked. --------------------------------------- JOHN NORMAN DONALD A.GUADAGNOLI,M.D. 07/01/2020 PAUL J.CANNIFF,D.M.D. THOMAS A.MCKEAN,R.S.,CHO Director of Public Health gy, r Town of Barnstable ss S • c Inspectional Services BARN TABLE 0` P NSTnMF•(4A,EMU-tONn•N,ANNIS , `"�, Public Health Division �u�n" .1639-2014°�"014 VNN�°°" { mmsrnsu, Thomas McKean, Director NAM �'ArFo 039. s`� 200 Main Street, Hyannis,MA 02601 r,r Office: 508-862-4644 Fax: 508-790-6304 r- APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE HAZARDOUS MATERIALS IN ACCORDANCE WITH THE TOWN OF BARNSTABLE GENERAL ORDINANCE,CHAPTER 108, HAZARDOUS MATERIALS,ALL BUSINESSES THAT HANDLE OR STORE HAZARDOUS MATERIALS GREATER THAN HOUSEHOLD QUANTITIES ARE REQUIRED TO OBTAIN AN ANNUAL PERMIT(RUNS JULY 1 st—JUNE 30th). APPLICATION FEES CATEGORY 1 PERMIT 26- 110 Gallons: $ 50.00 ❑ - -- . CATEGORY 2 PERMIT 111 -49.9 Gallons:_ -$125.00 _ Vvn --CATEGORY 3 PERMIT 500 or more Gallons: $150.00- d G 1C *A late charge of$10.00 will be assessed if payment is not received by July 1st. Q 1. ASSESSOR'S MAP AND PARCEL NO. 3111017 2. IS THIS A PERMIT RENEWAL? X YES NO. IF YES,SKIP QUESTION 3. • 3. FOR ALL NEW PERMIT APPLICATIONS,INDICATE WHETHER BUSINESS HAS ZONING/BUILDING APPROVAL FOR HAZARDOUS MATERIALS STORAGE/USE OF GREATER THAN HOUSEHOLD QUANTITIES (25 GALLONS)? YES NO. 4. FULL NAME OF APPLICANT:. BJ's Wholesale Club,Inc. 5. NAME OF ESTABLISHMENT: BJ's Gas Station #321 6. ADDRESS OF ESTABLISHMENT: 590 Iyanough Road, Hyannis, MA 02601 7. MAILING ADDRESS(IF DIFFERENT FROM ABOVE: 25 Research Drive, Attn:Licensin est oroug , MA 01581 8. TELEPHONE NUMBER OF ESTABLISHMENT: 508-568-4035 - •__-9.- -EMAIL ADDRESS: gm321@b.7 s.com 10. SOLEOWNER: X YES NO IF NO,NAME OF PARTNER: 11. FULL NAME,HOME ADDRESS,AND TELEPHONE# OF: CORPORATION NAME BJ's Wholesale Club,Inc. PRESIDENT Lee Delaney TREASURER Kristen M. Sugrue CLERK Graham N. Luce • 12. IF PREPARED BY OUTSIDE PARTY: NAME: TELEPHONE#: COMPANY ADDRESS EMAIL: SIGNATURE OF APPLICANT ,�// DATE 6/9/2020 Q:\Application FormsU-Iaz Mat Appli Draft Jan2019.docx TME►ohti Town of Barnstable Office:508-862-4644 Public Health Division Fax:508-790-6304 • BARMs�Le.$ 200 Main Street• Hyannis, MA 02601 t639 moll TOXIC AND HAZARDOUS MATERIALS INSPECTION REPORT rE0 Business Name: �� a Date: �� q Location/Mailing Address: D 1-,60 0 Contact Name/Phone: - — t) Inventory Total Amount: voo SDS: J11tJ License#: y cw Tier II :_ Labeling: d e-5 Spill Plan: Oil/WaterSeparator: O Floor Drains: e Emergency Numbers: - . '� Storage Areas/Tanks: koo Oat MS cldso. gcfiltk} Emergency/Containment Equipment: qAV,fft Waste Generator ID: M J.4R'771 z r')C4 Waste Product: 0111 Date&Amount of Last Shipment/Frequency: Licensed Waste Hauler&Destination: C 11,Z,A S Other Waste Disposal Methods: LIST OF TOXIC AND HAZARDOUS MATERIALS NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous material use, storage and disposal of 111 gallons or more requires a license from the Public Health Division. Antifreeze Dry cleaning fluids Automatic transmission fluid Other cleaning solvents&spot removers Engine and radiator flushes Bug and tar removers Hydraulic fluid (including brake fluid) Windshield wash Motor oils Miscellaneous Corrosives Gasoline,jet fuel, aviation gas Cesspool cleaners Diesel fuel, kerosene, #2 heating oil Disinfectants Miscellaneous petroleum products: Road salts grease, lubricants, gear oil Refrigerants Degreasers for engines&garages Pesticides: Caulk/Grout insecticides, herbicides, rodenticides Battery acid (electrolyte)/batteries Photochemicals(Fixers) Rustproofers Photochemicals(Developer) Car wash detergents Printing ink Car waxes and polishes Wood preservatives(creosote) Asphalt&roofing tar Swimming pool chlorine Paints, varnishes, stains, dyes Lye or caustic soda Lacquer thinners Miscellaneous Combustible Paint&varnish removers, deglossers Leather dyes Miscellaneous Flammables Fertilizers Floor&furniture strippers PCB's Metal polishes Other chlorinated hydrocarbons Laundry soil &stain removers (including carbon tetrachloride) (including bleach) Any other products with "poison labels" (including chloroform,formaldehyde, hydrochloric acid, other acids) VIOLATIONS: ORDERS: INFORMATON/RECOMMENDATIONS: r o m V(Yld Uan , eYf"Ofif- VAR()I Inspect Facility Representative: WHITE COPY- HEALTH DEPARTMENT/CANARY COPY- BUSINESS Number Fee 1244 THE COMMONWEALTH OF MASSACHUSETTS $50.00 Town of Barnstable Board of Health This is to Certify that BJs Gas Station #321 590 Iyannough Road, Hyannis, MA Is Hereby Granted a License For: Storing or Handling 26 - 110 gallons of Hazardous Materials. ---------------------------------------------------------------------------- --------------------- ---------------------------------------------------------- This license is granted in conformity with the Statutes and ordinances relating there to,and and expires 06/30/2020 unless sooner suspended or revoked. -------------------------------------- PAUL J.CANNIFF, D.M.D,CHAIRMAN DONALD A.GUADAGNOLI,M.D. 07/01/2019 JUNICHI SAWAYANAGI THOMAS A. MCKEAN,R.S.,CHO Director of Public Health .y F • � ; CAS Town of Barnstable Inspectional Services BAB TABLE `TNE Tti aaPS�TC'4�SBHtL'S 5'EF'LL' TNa�K'.aE Public Health Division ::39-=01< RARN3CABLE, ' ,� Thomas McKean, Director 'OrEv (a�` 200 Main Street, Hyannis, MA 02601 J Office: 508-862-4644 Fax:508-790-6304 APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE CiD HAZARDOUS MATERIALS IN ACCORDANCE WITH THE TOWN OF BARNSTABLE GENERAL ORDINANCE,CHAPTER 108, HAZARDOUS MATERIALS,ALL BUSINESSES THAT HANDLE OR STORE HAZARDOUS MATERIALS GREATER THAN HOUSEHOLD QUANTITIES ARE REQUIRED TO OBTAIN AN ANNUAL PERMIT(RUNS MY 1 st—JUNE 30th). APPLICATION FEES CATEGORY 1 PERMIT 26— 110 Gallons: $ 50.00 ❑ CATEGORY 2 PERMIT 111—499 Gallons: $125.00 ❑ CATEGORY 3 PERMIT 500 or more Gallons: $150.00 K VSTH � *A late charge of$10.00 will be assessed if payment is not received by Jules 1. ASSESSOR'S MAP AND PARCEL NO. 3111017 2. IS THIS A PERMIT RENEWAL? X YES_NO. IF YES, SKIP QUESTION 3. 3. FOR ALL NEW PERMIT APPLICATIONS,INDICATE WHETHER BUSINESS HAS ZONING/BUILDING APPROVAL FOR HAZARDOUS MATERIALS STORAGE/USE OF GREATER THAN HOUSEHOLD QUANTITIES (25 GALLONS)? YES NO. • 4. FULL NAME OF APPLICANT: BJ's Wholesale Club,Inc. 5. NAME OF ESTABLISHMENT: BJ's Gas Station #321 6. ADDRESS OF ESTABLISHMENT: 590 Iyanough Road, Hyannis, MA 02601 7. MAILING ADDRESS (IF DIFFERENT FROM ABOVE: 25 Research Drive, Attn:Licensing Westborough, MA 01581 8. TELEPHONE NUMBER OF ESTABLISHMENT: 508-568-4035 9. EMAIL ADDRESS: gm321@bjs.com 10. SOLEOWNER:: xx YES NO IF NO,NAME OF PARTNER: f 11. FULL NAME,If ADDRESS,AND TELEPHONE it OF: CORPORATION NAME BJ's Wholesale Club, Inc. PRESIDENT Christopher J. Baldwin 25 Research Drive, Westborough, MA 01581 TREASURER Kristyn M. Sugrue 25 Research Drive, Westborough, MA 01581 CLERK Graham N. Luce 25 Research Drive, Westhorcuugh, MA (11981 12. IF PREPARED BY OUTSIDE PARTY: NAME: TELEPHONE#: COMPANY ADDRESS EMAIL: SIGNATURE OF APPLICANT 144C ell DATE 5/21/2019 6Application Forms\Haz Mat App Revised 09-10-18.docx Number Fee 1244 THE COMMONWEALTH OF MASSACHUSETTS $50.00 Town of Barnstable Board of Health This is to Certify that BJs Gas Station #321 590 Iyannough Road, Hyannis, MA Is Hereby Granted a License For: Storing or Handling 26 - 110 gallons of Hazardous Materials. ---------------------------------------------------------- ----------------------------------------------------------------------------------------------------- ----------------------------------------------------------------- --------------------------------------------------------------------------------------------- This license is granted in conformity with the Statutes and ordinances relating there to, and and expires 06/30/2019 unless sooner suspended or revoked. ---------------------------------------- PAUL J.CANNIFF,D.M.D,CHAIRMAN DONALD A.GUADAGNOLI,M.D. 07/01/2018 JUNICHI SAWAYANAGI THOMAS A.MCKEAN, R.S.,CHO Director of Public Health Vofowr� B nsxable �J S egulatoryYervices Richard V. Scah, Director , mot KNE t�"�. Public Health Division BARNSTABLE BAEN9rABM = Thomas McKean, Director ""�°"S"'pia <� n�� -- - --- -- ArE -200 Main-Street,,Hyannis MA 02601--- --- - ---- 77�- --- -- - -- Office: 508-862-4644 o g Fax: 508-790-6304 APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE HAZARDOUS MATERIALS IN ACCORDANCE WITH THE TOWN OF BARNSTABLE GENERAL ORDINANCE, CHAPTER 108, HAZARDOUS MATERIALS,ALL BUSINESSES THAT HANDLE OR STORE HAZARDOUS MATERIALS GREATER THAN HOUSEHOLD QUANTITIES ARE REQUIRED TO OBTAIN AN ANNUAL PERMIT(RUNS JULY lst-NNE 30th). APPLICATION FEES CATEGORY 1 PERMIT 26- 110 Gallons: $ 50.00 CATEGORY 2 PERMIT 111 -499 Gallons: $125.00 ET CATEGORY 3 PERMIT 500 or more Gallons: $150.00 0 *A late charge of$10.00 will be assessed if payment is not received by July 1st. 1. ASSESSOR'S MAP AND PARCEL NO. 3111017 2. IS THIS A PERMIT RENEWAL? X YES_NO. W YES, SKIP QUESTION 3. 3. FOR ALL NEW PERMIT APPLICATIONS,INDICATE WHETHER BUSINESS HAS ZONING/BUILDING APPROVAL FOR HAZARDOUS MATERIALS STORAGE/USE OF GREATER THAN HOUSEHOLD QUANTITIES (25 GALLONS)? YES NO. 4. FULL NAME OF APPLICANT• BJ's Wholesale C1ub,Inc. 5. NAME OF ESTABLISHMENT: BJ's Gas Station #321 6. ADDRESS OF ESTABLISHMENT: 590 Iyanough Road, Hyannis, MA 02601 7. MAILING ADDRESS(IF DIFFERENT FROM ABOVE: Attn: Licensing 25 Research Drive Westborough, MA 01581 8. TELEPHONE NUMBER OF ESTABLISHMENT: 508-568-4035 9. EMAIL ADDRESS: GM321@bjs.com 10. SOLEOWNER: X YES NO IF NO,NAME OF PARTNER: Office 11. FULL NAME,HOW ADDRESS,AND TELEPHONE#OF: CORPORATION NAME BJ's Wholesale Club,Inc. PRESIDENT Christopher J. Baldwin 25 Research Drive, Westborough, MA 01581 TREASURER Kristyn M. Sugrue 25 Research Drive, Westborough, MA 01581 CLERK Graham N. Luce 25 Research Drive, Westborough, MA 01581 12. IF PREPARED BY OUTSIDE PARTY: NAME: TELEPHONE#: • COMPANY ADDRESS EMAIL: SIGNATURE OF APPLICANT DATE 5/24/2018 Q\Application FormsUiAZMAT APP 2017 REVISED.doc Number Fee 1244 THE COMMONWEALTH OF MASSACHUSETTS $so.00 Town of Barnstable Board of Health This is to Certify that BJs Gas Station #321 590Iyannough Road, Hyannis, MA Is Hereby Granted a License For: Storing or Handling 26 - 110 gallons of Hazardous Materials. -------- - --------------------------------------------------------------------------------------------------- - ------------------------------------------------------------------------------------------------------------------------------------------------------------- This license is granted in conformity with the Statutes and ordinances relating there to, and and expires 06/30/2018 unless sooner suspended or revoked. ---------------------------------------- 6 PAUL J.CANNIFF,D.M.D,CHAIRMAN DONALD A.GUADAGNOLI,M.D. 07/01/2017 JUNICHI SAWAYANAGI THOMAS A.MCKEAN, R.S.,CHO Director of Public Health "A Twn of Barnstable 3 eg story Semces Richard V. Scali, Director Public Health Division BABSTABLE z • � enuxsrne�•a«nanue.cmurt mnvras RAPNSTABLE. Thomas McKean, Director x 's nw51 3'9-2o 4vrsr ea?xsrnwe � , E1 39. 200 Main Street, Hyannis,MA 02601 ��� C>q py��f -� Office: 508-862-4644 0l��� 02 U/V Fax: 508-790-6304 APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE 1 HAZARDOUS MATERIALS IN ACCORDANCE WITH THE TOWN OF BARNSTABLE GENERAL ORDINANCE, CHAPTER 108, HAZARDOUS MATERIALS,ALL BUSINESSES THAT HANDLE OR STORE HAZARDOUS MATERIALS GREATER THAN HOUSEHOLD QUANTITIES ARE REQUIRED TO OBTAIN AN ANNUAL PERMIT(RUNS JULY 1 st-JUNE 3 Oth). APPLICATION FEES CATEGORY 1 PERMIT 26- 110 Gallons: $ 50.00VS CATEGORY 2 PERMIT 111 -499 Gallons: $125.00 ❑ CATEGORY 3 PERMIT 500 or more Gallons: $150.00 ❑ *A late charge of$10.00 will be assessed if payment is not received by July 1st. 1. ASSESSOR'S MAP AND PARCEL NO. 3111017 2. IS THIS A PERMIT RENEWAL? X YES_NO. IF YES,SKIP QUESTION 3. 3. FOR ALL NEW PERMIT APPLICATIONS,INDICATE WHETHER BUSINESS HAS ZONING/BUILDING APPROVAL FOR HAZARDOUS MATERIALS STORAGEIUSE OF • GREATER THAN HOUSEHOLD QUANTITIES (25 GALLONS)? YES NO. 4. FULL NAME OF APPLICANT: BJ's Wholesale Club, Inc. 5. NAME OF ESTABLISHMENT: BJ, s Gas Station #321 6. ADDRESS OF ESTABLISHMENT: 590 Iyanough Road, Hyannis, MA 02601 7. MAILING ADDRESS (IF DIFFERENT FROM ABOVE: Attn: Licensing; 25 Research Drive Westborough, MA 01581 8. TELEPHONE NUMBER OF ESTABLISHMENT: 508-568-4035 9. EMAIL ADDRESS: gm321@bjs.com 10. SOLEOWNER: X YES NO IF NO,NAME OF PARTNER: office 11. FULL NAME,WME ADDRESS,AND TELEPHONE#OF: CORPORATION NAME BJ's Wholesale Club, Inc. PRESIDENT Chris Baldwin 25 Research Drive, Westborough, MA 01581 TREASURER Kri stun on 29 Research Drive, Westborough- MA 01 581 CLERK Graham N. Luce 25 Research Drive, Westborough, MA 01581 12. IF PREPARED BY OUTSIDE PARTY: NAME: TELEPHONE#: • COMPANY ADDRESS EMAIL: SIGNATURE OF APPLICANT DATE 6/8/2017 Q:\Application Forms\HAZMAT APP 2017 REVISED.d c Number Fee 1244 THE COMMONWEALTH OF MASSACHUSETTS $so.00 Town of Barnstable Board of Health This is to Certify that BJs Gas Station #321 590Iyannough Road, Hyannis, MA Is Hereby Granted a License For: Storing or Handling 26 - 100 gallons of Hazardous Materials. -------------------------------------------------------------------------------------------------------------------------------I------------------------------------ This license is granted in conformity with the Statutes and ordinances relating there to, and and expires 06/30/2017 unless sooner suspended or revoked. ---------------------------------------- WAYNE MILLER,M.D.,CHAIRMAN PAUL J.CANNIFF,D.M.D. 07/01/2016 JUNICHI SAWAYANAGI TZ THOMAS A.MCKEAN, R.S.,CHO Director of Public Health t 08/02/2016 15:12 FAX 5085684040 bps 001 • Town, of Barnstable Regulatory Services , r Richard V. $call,Director \a' co q .` �°� _ BARNSTABL MA p Public Health Division �ax�rz.��c..�1 �, a, s6396 MQti' 1+ w Thomasnla6 1�G es3:1,DireCtOX �014* 10 M 200 Main Street,Hyannis,MA 02601 t Office: 508-862-4644 Fax: 508-790-6104 APPLICATION FOR PERMIT TO STORE AND/OR 'I TILIZE HAZARDOUS MATERIALS IN ACCORDANCE.WITH THE TOWN OF BARNSTABLE GENERAL ORDINANCE,CHAPTER 108, HAZARDOUS MATERIALS,ALL BUSINESSES THAT HANDLE OR STORE HAZARDOUS MATERIALS GREATER THAN HOUSEHOLD QUANTITIES ARE REQUIRED TO 013TAIN AN - - ANNUAL PERMIT(RUNS JULY 1st^JUNE 30th). APPLICATION FEES CATEGORY 1 PERMIT 26—110 Gallons: $ 50.00 CAT)EJGORY 2 PERMIT 111 499 Gallons: $125.00 ❑ CATEGORY 3 PERMIT 500 or more Gallons: $150.00 ❑ A late charge of S10 00 will be assessed if nav=nt is not received by July 1st, • ASSESSORS MAP AND PARCEL NO. 311017 DATE 8/2/2016 FULL NAME OF APPLICANT: BJ's Wholesale Club, Inc. NAME OF ESTABLISHMENT: BJ's Gas Station#321 ADDRESS OF ESTABLISHMENT: 590 Iyanough Road, Hyannis, MA 02601 MAILING ADDRESS(IF DIFFERENT): Attn: Licensing; 25 Research Drive, Westborough, MA 01581 TELEPHONE NUMBER OF ESTABLISHMENT: 508-568-4035 EMAIL ADDRESS:_ gm321@b's.com (club) legalnotices@bs.com (licensing) SOLE OWNER: X YES—NO IF NO,NAME OF PARTNER: _ FULL NAME,"i ADDRESS,AND~TE.LEPHONE#OF: CORPORATION NAME BJ's Wholesale Club, Inc.; 25 Research Drive Westborou2 PRESIDENT Chlis Bajdwi2 h MA 0 15 81 - -7400 TREASURER 25 Research Drive Westborough, 01581 77 - -7400 CLERK Graham Luce 25 Research Drive, Westboromg�MA 01581 74-512-7400 IF PREPARED BY OUTSIDE PARTY: SIGNAT '..,&6LICANT Name: fir' Company Address : raha e e retary Telephone#: BJ's Wholesale Club, Inc. Email: C;V1'vt if\i4AZZAPP Rev I6.docx Page 1 of 2 I i t i ( Number Fee 1101 THE COMMONWEALTH OF MASSACHUSETTS 100.00 Town of Barnstable Board of Health This is to Certify that Sav-On Gas Inc, RT 132 590 IYANNO UGH ROAD, HYANNIS, MA Is Hereby Granted a License FOR: STORING OR HANDLING 111 GALLONS OR MORE OF HAZARDOUS MATERIALS. -------------------------------------------------------------------------------------------------------------------------------------------------------------------- ------------------------------------------------------------------------------------------------------------------------------------------------------------------ This license is granted in conformity with the Statutes and ordinances relating there to, and and expires 06/30/2016 unless sooner suspended or revoked. -------------------------------------- WAYNE MILLER,M.D.,CHAIRMAN PAUL J.CANNIFF, D.M.D. 07/01/2015 JUNICHI SAWAYANAGI THOMAS A.MCKEAN,R.S.,CHO a Director of Public Health • I +� UJ Town of Barnstable Regulatory Services ti • °� Richard V. Scali,Director " MkRNSTAELF, Public Health Division �rED N►A'�a Thomas McKean,Director 200 Main Street, Hyannis, MA 02601 "'n Office: 508-862-4644 Fax:='508-790-6304 Application Fee: $100.0.0 / ,/ {�/ o ASSESSORS MAP AND PARCEL NO. �J ' vl DATE APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE MORE THAN III GALLONS OF HAZARDOUS MATERIALS FULL NAME OF APPLICANT V d� NAME OF ESTABLISHMENT �C7 LJ� L V D& 6a . ADDRESS OF ESTABLISHMENT 690 koad , H TELEPHONE NUMBER - SOLE OWNER:XYES NO IF APPLICANT IS A PARTNERSHIP,FULL NAME AND HOME ADDRESS OF ALL PARTNERS: �0,A- I �r WeAf �zoo l IF APPLICANT IS A CORPORATION: FEDERAL IDENTIFICATION NO.)C)-01 STATE OF INCORPORATION ' FULL NAME AND HOME ADDRESS OF: PRESIDENT Dri�L } TREASURER CLERK SIGNATURE OF APPLICANT RESTRICTIONS: HOME ADDRESS I CQ ft �)"I rmouA por HOME TELEPHONE# - � C:\cache\Temporary Intemet Fi1es\0LKD3\HAZAPP ReQ015.DOC I a rq Town of Barnstable office: 508-862-4644 Fax: 508-790-6304 Regulatory Services Department BARN' rASLE, ; Public Health Division Mom. Thomas A.McKean,CHO 200 Main Street, Hyannis, MA 02601 Payment Receipt Hazardous Materials Payment received: $100.00 (Check) on 8/4/2015 Permit number: 1073 Check number: 3498 Check amount: $100.00 Name on check: Route 132 Say-On Gas, Inc Business: Sav-On Gas, Inc. Route 132 f Address: 590 IYANNOUGH ROAD/RTE132, Hyannis I i t i • I Number Fee 1073 THE COMMONWEALTH OF MASSACHUSETTS 1oo.00 Town of Barnstable Board of Health This is to Certify that Sav-On Gas, Inc. Route 132 590Iyannough Road, Hyannis, MA Is Hereby Granted a License FOR: STORING OR HANDLING 111 GALLONS OR MORE OF HAZARDOUS MATERIALS. -------------------------------------------------------------------------------------------------------------------------------------------------------------------- -------------------------------------------------------------------------------------------- ------------------------------------------------------------------- This license is granted in conformity with the Statutes and ordinances relating there to, and and expires 6/30/2015 unless sooner suspended or revoked. ---------------------------------------- WAYNE MILLER,M.D.,CHAIRMAN PAUL J.CANNIFF, D.M.D. 6/30/2014 JUNICHI SAWAYANAGI THOMAS A.MCKEAN,R.S.,CHO Director of Public Health Town of Barnstable Z_wpF114E Regulatory Services Richard V. Scali, Director MUWSTAMAM. ' Public Health Division 9� 13 `fig' �f1 39. A Thomas McKean, Director 200 Main Street, Hyannis, MA 02601 Office: 508-8624644 Fax: 508-790-6304 Application Fee: $100.00 ASSESSORS MAP AND PARCEL NO. DATE APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE MORE THAN 111 GALLONS OF HAZARDOUS MATERIALS FULL NAME OF APPLICANT NAME OF ESTABLISHMENT Aa)LC aU ()n ADDRESS OF ESTABLISHMENT 63C) N n M(- h a,)J ' OoWl TELEPHONE NUMBER508_P_-t71- -3s-�? SOLE OWNER,/YES NO IF APPLICANT IS A PARTNERSHIP,FULL NAME AND HOME ADDRESS OF ALL PARTNERS: Adda!2s C (D 1 ( I C-T IF APPLICANT IS A CORPORATION: FEDERAL IDENTIFICATION NOM STATE OF INCORPORATIJON M a FULL NAME AND HOME ADDRESS OF: PRESIDENT q )Mod,_ )�n1 oronnik ' �r I U�oUarftk"Omd . JJA TREASURER— CLERK IGNATURE OF APPLICANT RESTRICTIONS: HOME ADDRESS yf Y4� HOME TELEPHONE#& _ (p-�7(� Q:1Application FormsUiAZAPP000 4 �s Number Fee 1073 THE COMMONWEALTH OF MASSACHUSETTS $1oo.00 Town of Barnstable Board of Health This is to Certify that Sav-On Gas, Inc. Route 132 590Iyannough Road, Hyannis,MA 02601 Is Hereby Granted a License FOR: STORING OR HANDLING 111 GALLONS OR MORE OF HAZARDOUS MATERIALS. -------------------------------------------------------------------------------------------------------------------------------------------------------------------- ------------------------------------------------------------------------------------------------------------------------------------------------------------------ This license is granted in conformity with the Statutes and ordinances relating there to,and and expires 6/30/2013 unless sooner suspended or revoked. ---------------------------------------- WAYNE MILLER,M.D.,CHAIRMAN PAUL J.CANNIFF,D.M.D. 9/17/2013 JUNICHI SAWAYANAGI THOMAS A.MCKEAN,R.S.,CHO Director of Public Health Town of Barnstable -Y Barnstable Regulatory Services Department ' Public Health Division IAMSTAHLE. MAE& 1,�' 200 Main Street, Hyannis MA 02601 aA 2007 Office: 508-862-4644 Thomas F.Geiler,Director FAX: 508-790-6304 Thomas A.McKean,CHO Application Fee: $100.00 ASSESSORS MAP AND PARCEL NO. DATE��T� APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE MORE THAN III GALLONS OF HAZARDOUS MATERIALS 0 FULL NAME OF APPLICANT NAME OF ESTABLISHMENT 4 ADDRESS OF ESTABLISHMENT . I TELEPHONE NUMBER -- SOLE OWNER: YES �;(O IF APPLICANT IS A PARTNERSHIP,FULL NAME AND HOME ADDRESS OF ALL PARTNERS: IF APPLICANT IS A CORPORATION: FEDERAL IDENTIFICATION NO. STATE OF INCORPORATION FULL NAME HO ADDRESS OT: PRESIDENT TREASURE CLERK TUBE A LPLICANT RESTRICTIONS: HOMEAD SS HOME TELEPHONE# Minspection handouts\Haz Mat Application2008.DOC 5 MAIL-IN REQUESTS Please mail the completed application form to the address below. Also include a copy of your contingency plan (to handle hazardous waste spills, etc.) In addition, please include the required fee of$100. Make check payable to: Town of Barnstable. Allow time for in-house processing. Our mailing address is: Town of Barnstable Public Health Division 200 Main Street Hyannis, MA 02601 FOR FAXED REQUESTS Our fax number is (508) 790-6304. Please fax a completed application form. Also, please fax us a copy of your contingency plan (to handle hazardous waste spills, etc.) In addition, please mail the required fee of$100. Please make the check payable to: Town of Barnstable. The check must be mailed to the address listed above. Allow time for in- house processing. For further assistance on any item above, call (508) 862-4644 Back to Main Public Health Division Page r Dinspection handouts\Haz Mat Application2008.DOC „r ' • I' TOWN OF BARNSTABLE Dater/ ,7/ Z1,� TOXIC AND HAZARDOUS MATERIALS REGISTRATION FORM NAME OF BUSINESS: BUSINESS LOCATION: & INVENTORY MAILING ADDRESS: 14 TOTAL AMOUNT: TELEPHONE NUMBER: P CONTACT PERSON: EMERGENCY CONTA6f TELEPHONE NUMBER: 6 MSDS ON SITE? TYPE OF BUSINESS: /,f 4�0-ij ' INFORMATION / RECOMMEND ONS: Fire District: Waste Transportation: Last shipment of hazardous waste: 0�(� Name of Hauler: Destination: Waste Product: Licensed? Yes No NOTE: Under the provisions of Ch. 111, Section 31, of the General Laws of MA, hazardous material use, storage and disposal of 111 gallons or more a month requires a license from the Public Health Division. LIST OF TOXIC AND HAZARDOUS MATERIALS The Board of Health and the Public Health Division have determined that the following products exhibit toxic or hazardous characteristics and must be registered regardless of volume. Observed / Maximum Observed / Maximum Antifreeze (for gasoline or coolant systems) Miscellaneous Corrosive ❑ NEW 0 USED Cesspool cleaners Automatic transmission fluid Disinfectants Engine and radiator flushes Road salts (Halite) Hydraulic fluid (including brake fluid) Refrigerants Motor Oils Pesticides ❑ NEW ❑ USED (insecticides, herbicides, rodenticides) Gasoline, Jet fuel,Aviation gas Photochemicals (Fixers) Diesel Fuel, kerosene, #2 heating oil ❑ NEW ❑ USED Miscellaneous petroleum products: grease, Photochemicals (Developer) lubricants, gear oil ❑ NEW ❑ USED Degreasers for engines and metal Printing ink Degreasers for driveways&garages Wood preservatives (creosote) Caulk/Grout Swimming pool chlorine Battery acid (electrolyte)/Batteries Lye or caustic soda Rustproofers i Miscellaneous Combustible Car wash detergents Leather dyes Car waxes and polishes Fertilizers Asphalt& roofing tar PCB's Paints, varnishes, stains, dyes Other chlorinated hydrocarbons, Lacquer thinners (including carbon tetrachloride) ❑ NEW ❑ USED Any other products with "poison” labels (including chloroform, formaldehyde, Paint&varnish removers, deglossers hydrochloric acid, other acids) Miscellaneous. Flammables Other products not listed which you feel Floor&furniture strippers may be toxic or hazardous (please list): Metal polishes Laundry soil &stain removers (including bleach) Spot removers&cleaning fluids 1 (dry dbaners) Other cleaning solvents Bug and tar removers Windshield wash WHITE CO Y-HEALTH DEPARTMENT/CANARY COPY-BUSINESS Appli 's Si&uw Staffs Initials 1. YOU WISH TO OPEN A BUSINESS? For Your Information: Business certificates (cost$40.00 for 4 years). A business certificate ONLY REGISTERS YOUR NAME in town [which you must do by M.G.L.-it does not give you permission to operate.) You must first obtain the necessary signatures on this form at 200 Main St., Hyannis. Take the completed form to the Town Clerk's Office, 1 st FI., 367 Main St., Hyannis, MA 02601 (Town Hall) and get the Business Certificate that is required by law. DATE: — ill)n please: APPLICANT'S YOUR NAME/ : S ' e- K, BUSINESS YOUR HOME ADDRESS: C> TELEPHONE # Home Telephone Number NAME OF CORPORATION: 9 ' NAME OF NEW BUSINESS PE O BUSINESS IS THIS A HOME OCCUPATION? YES NO 4 ADDRESS OF BUSINESS �(� MAP/PARCEL NUMBER XU1 (Assessing) When starting a new business there are several things you must do in order to be in compliance with the rules and regulations of the Town of Barnstable. This form is intended to assist you in obtaining the information you may need. You MUST GO TO 200 Main St. - (corner of Yarmouth Rd. & Main Street) to make sure you have the appropriate permits and licenses required to legally operate your business in this town. 1. BUILDING COM IS ION R'S OFF C This individ I ha e irtfor d f na( r it e uirements that pertain to this type of business. Aut orized Signatu e* OMMENTS: S 2. BOARD OF HEALTH This individual has bteenrni#o, r of the permit requirements that pertain to this type of business. COMMENTS: IV P.Q/� u�c�ZfflaFrizedn�rA6,( P l i 3. CONSUMER AFFAIRS (LICENSING AUTHORITY) This individual has been informed of the licensing requirements that pertain to this type of business. Authorized Signature* COMMENTS: a i Number Fee 1073 THE COMMONWEALTH OF MASSACHUSETTS $O.00 Town of Barnstable Board of Health This is to Certify that Sav-On Gas 590 Iyannough Road, MA 02601 Is Hereby Granted a License FOR: STORING OR HANDLING 111 GALLONS OR MORE OF HAZARDOUS MATERIALS. -------------------------------------------------------------------------- ---------------------------------------------------------------------------------- --------------------------------------- ------------------------------------------------------------------------------------- --------------------------- This license is granted in conformity with the Statutes and ordinances relating there to, and and expires June 30, 2008 unless sooner suspended or revoked. ---------------------------------------- WAYNE MILLER,M.D.,CHAIRMAN SUMNER KAUFMAN,M.S.P.H. 7/9/2007 PAUL J. CANNIFF,D.M.D. THOMAS A. MCKEAN,R.S.,CHO Director of Public Health I ` � DATES "4R x'Y `^ aisa 'y v . YP REcavm'FROM :" N G� ?+ ADDRESS- 0 d't � uDOLLARS .t xsx'1 '* uv' Aw ❑FOR RRENT �►�j/�/fj��jJy� u v OFOR� i' 7DUE CASHCHECK MONEYPC ORDER BY 0AIL ,.. I =� Town of Barnstable t0WE r � Regulatory Services Thomas F. Geiler,Director MR AS& Public Health Division �$OreaMv�"�e� Thomas McKean,Director 200 Main Street, Hyannis,MA 02601 Office: 508-8624644 Fax: 508-790-6304 Application Fee: $100.00 ASSESSORS MAP AND PARCEL NO. DATE (v -2 APPLICATION FOR PERMIT TO STORE AND/OR UTILIZE MORE THAN 111 GALLONS OF HAZARDOUS MATERIALS FULL NAME OF APPLICANT — — 1�-mA7 NAME OF ESTABLISHMENT ADDRESS OF ESTABLISHMENT % ,JQd-V4 /f' :I 7 TELEPHONE NUMBER SOLE OWNER: ES NO -; IF APPLICANT IS A PARTNERSHIP,FULL NAME AND HOME ADDRESS OF ALL PARTNERS: r- u> p qT-J .yy` der �n W c-n 1 r- rn r"r IF APPLICANT IS A CORPORATION: FEDERAL IDENTIFICATION NO STATE OF INCORPORATION !'QA:5 S FULL NAME AND HOME ADDRESS OF: PRESIDENT aY�T�J Q� TREASURER CLERK SIGNATURE OF APPLICANT _ RESTRICTIONS: HOME ADDRESS HOME TELEPHONE a „ r Barnstable � BARNSTABLE. Town of Barnstable Regulatory Services Department 2007 Public Health Division 200 Main Street, Hyannis MA 02601 Office: 508-862-4644 Thomas F.Geiler,Director FAX: 508-790-6304 Thomas A.McKean,CHO Date: April 1, 2009 TO: �n JAY IMAD ENTR IYANNOUGH RD, LLC 590 Iyannough Road O v � o Hyannis, MA 02601 c� RE: Underground Storage Tank at: 590 Iyannough Road Hyannis,MA Map Parcel: 311017 Tank NO: 1 Tag NO: 00890 Our records indicate that your underground fuel (or chemical) storage tank is over 20 years old, and has not been removed as required by section 326-3: subsection 2 of the Town of Barnstable Code regarding fuel and chemical storage systems. You are directed to remove this tank within sixty(60) days from the date of this notice. After your tank is removed,please furnish this office evidence in the form of a permit from your local Fire Department within ninety(90) days of the receipt of this notice. You may request a hearing provided a written petition requesting same is received by the Board of Health within ten (10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, RS, CHO Health Agent ti Barnstable 9�A M g Town of Barnstable Regulatory Services Department 2007 Public Health Division 200 Main Street, Hyannis MA 02601 Office: 508-862-4644 Thomas F.Geiler,Director FAX: 508-790-6304 Thomas A.McKean,CHO Date: April 1, 2009 TO: JAY IMAD ENTR IYANNOUGH RD, LLC p 590 Iyannough Road O p � Y o H annis MA 02601 RE: Underground Storage Tank at: 590Iyannough Road Hyannis,MA Map Parcel: 311017 Tank NO: 2 Tag NO: 00891 Our records indicate that your underground fuel (or chemical) storage tank is over 20 years old, and has not been removed as required by section 326-3: subsection 2 of the Town of Barnstable Code regarding fuel and chemical storage systems. You are directed to remove this tank within sixty(60) days from the date of this notice. After your tank is removed, please furnish this office evidence in the form of a permit from your local Fire Department within ninety(90) days of the receipt of this notice. You may request a hearing provided a written petition requesting same is received by the Board of Health within ten(10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, RS, CHO Health Agent of�ram, • * Barnstable 11ARNSMAIBM MASSTown of Barnstable Regulatory Services Department 2007 Public Health Division 200 Main Street, Hyannis MA 02601 Office: 508-862-4644 Thomas F.Geiler,Director FAX: 508-790-6304 Thomas A.McKean,CHO Date: April 1, 2009 TO: TSCOW'JAY IMAD ENTR IYANNOUGH RD, LLC Y g 590 I annou h Road Hyannis, MA 02601 RE: Underground Storage Tank at: 590Iyannough Road Hyannis,MA Map Parcel: 311017 Tank NO: 3 Tag NO: 00892 Our records indicate that your underground fuel (or chemical) storage tank is over 20 years old, and has not been removed as required by section 326-3: subsection 2 of the Town of Barnstable Code regarding fuel and chemical storage systems. You are directed to remove this tank within sixty(60) days from the date of this notice. After your tank is removed,please furnish this office evidence in the form of a permit from your local Fire Department within ninety(90) days of the receipt of this notice. You may request a hearing provided a written petition requesting same is received by the Board of Health within ten(10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, RS, CHO Health Agent �VKGEr s Barnstable 6 SS 9 ,0� Town of Barnstable ATFD MA'S� Regulatory Services Department 2007 Public Health Division 200 Main Street, Hyannis MA 02601 Office: 508-862-4644 Thomas F.Geiler,Director FAX: 508-790-6304 Thomas A.McKean,CHO Date: April 1, 2009 TO: D JAY WAD ENTR IYANNOUGH RD, LLC O p 590 Iyannough Road C Hyannis, MA 02601 RE: Underground Storage Tank at: 590 Iyannough Road Hyannis,MA Map Parcel: 311017 Tank NO: 6 Our records indicate that your underground fuel (or chemical) storage tank is over 20 years old, and has not been removed as required by section 326-3: subsection 2 of the Town of Barnstable Code regarding fuel and chemical storage systems. You are directed to remove this tank within sixty(60) days from the date of this notice. After your tank is removed,please furnish this office evidence in the form of a permit from your local Fire Department within ninety(90) days of the receipt of this notice. You may request a hearing provided a written petition requesting same is received by the Board of Health within ten(10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, RS, CHO Health Agent I� f oti�rA,f, * Barnstable 9$`" & Town of Barnstable Regulatory Services Department 2007 Public Health Division 200 Main Street, Hyannis MA 02601 Office: 508-862-4644 Thomas F.Geiler,Director FAX: 508-790-6304 Thomas A.McKean,CHO Date: April 1, 2009 TO: JAY IMAD ENTR IYANNOUGH RD, LLC 590 I annou h Road y g SCOT Hyannis, MA 02601 RE: Underground Storage Tank at: 590Iyannough Road Hyannis,MA Map Parcel: 311017 Tank NO: 7 Our records indicate that your underground fuel (or chemical) storage tank is over 20 years old, and has not been removed as required by section 326-3: subsection 2 of the Town of Barnstable Code regarding fuel and chemical storage systems. You are directed to remove this tank within sixty(60) days from the date of this notice. After your tank is removed,please furnish this office evidence in the form of a permit from your local Fire Department within ninety(90) days of the receipt of this notice. You may request a hearing provided a written petition requesting same is received by the Board of Health within ten (10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, RS, CHO Health Agent 1' i i 1 CONSULTINGSOVEREIGN ! i i i June 19,2007 DHL#22124363951 Commonwealth of Massachusetts Department of Environmental Protection-SERO 20 Riverside Drive Lakeville,MA 02347 Ph:508-946-2700 ! Re: INSPECTION AND MONITORING REPORT FOR PHASE V REMEDY OPERATING STATUS 590 Iyannough Road Hyannis,Massachusetts 02072 RTN 4-17651 To Whom It May Concern: On behalf of Motiva Enterprises LLC (Motiva), Sovereign Consulting Inc. (Sovereign) is submitting the attached Inspection and Monitoring (I&M) Report for Phase V Remedy Operating Status regarding the above-referenced disposal site. The I&M report was prepared in accordance with the Massachusetts Contingency Plan (MCP) and summarizes response actions conducted between December 19,2006 through June 19,2007. If you have any questions regarding this submittal,please feel free to contact the undersigned. Sincerely, SOVEREIGN CONSULTING INC. 0AAK Erin Foley Eric D.Simpson,P.G.,LSP Field Scientist Operations Manager Attachments: I&M Report Transmittal Form BWSC-108 cc: With Attachments: David Weeks,Motiva Enterprises LLC Hatem Enterprises Iyannough Road,LLC Sovereign File-EQ872 905B S. Main Street, Unit 202 •Mansfield, MA 02048 •Tel: 508-339-3200• Fax: 508-339-3248 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC108 COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM& PHASE I COMPLETION STATEMENT F4 - 17651 Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) A. SITE LOCATION: 1. Site Name:SHELL SERVICE STA 2. Street Address:1590 IYANOUGH RD 3. City/Town: HYANNIS 4. ZIP Code: 02601-0000 5.UTM Coordinates: a.UTM N: 14613259 -1 b. UTM E: 1392621 6. Check here if a Tier Classification Submittal has been provided to DEP for this disposal site. Fla. Tier IA ❑ b. Tier IB ❑ c. Tier IC ❑ d. Tier 11 7. If applicable,provide the Permit Number: { B.THIS FORM IS BEING USED TO: (check all that apply) ❑ 1. Submit a Phase I Completion Statement,pursuant to 310 CMR 40.0484. ❑ 2. Submit a Revised Phase I Completion Statement,pursuant to 310 CMR 40.0484. ❑ 3. Submit a Phase II Scope of Work,pursuant to 310 CMR 40.0834. ❑ 4. Submit an interim Phase II Report. This report does not satisfy the response action deadline requirements in 310 CMR 40.0500. ❑ 5.Submit a final Phase II Report and Completion Statement,pursuant to 310 CMR 40.0836. i ❑ 6.Submit a Revised Phase 11 Report and Completion Statement,pursuant to 310 CMR 40.0836. ❑ 7. Submit a Phase III Remedial Action Plan and Completion Statement,pursuant to 310 CMR 40.0862. l ❑ 8. Submit a Revised Phase III Remedial Action Plan and Completion Statement,pursuant to 310 CMR 40.0862. ❑ 9. Submit a Phase IV Remedy Implementation Plan,pursuant to 310 CMR 40.0874. ❑ 10. Submit a Modified Phase IV Remedy Implementation Plan,pursuant to 310 CMR 40.0874. ❑ 11. Submit an As-Built Construction Report,pursuant to 310 CMR 40.0875. ❑ 12. Submit a Phase IV Status Report,_pursuant to 310 CMR 40.0877. ❑ 13. Submit a Phase IV Completion Statement,pursuant to 310 CMR 40.0878 and 40.0879. Specify the outcome of Phase IV activities:(check one) ❑ a. Phase V Operation,Maintenance or Monitoring of the Comprehensive Remedial Action is necessary to achieve a Response Action Outcome. b. The requirements of a Class A Response Action Outcome have been met. No additional Operation,Maintenance or ❑ Monitoring is necessary to ensure the integrity of the Response Action Outcome. A completed Response Action Outcome Statement and Report(BWSC104)will be submitted to DEP. c. The requirements of a Class C Response Action Outcome have been met. No additional Operation,Maintenance or ❑ Monitoring is necessary to ensure the integrity of the Response Action Outcome. A completed Response Action Outcome Statement and Report(BWSC104)will be submitted to DEP. d. The requirements of a Class C Response Action Outcome have been met. Further Operation,Maintenance or ❑ Monitoring of the remedial action is necessary to ensure that conditions are maintained and that further progress is made toward a Permanent Solution. A completed Response Action Outcome Statement and Report (BWSC104)will be submitted to DEP. (All sections of this transmittal form must be filled out unless otherwise noted above) Revised:2/15/2005 Page 1 of 5 n Massachusetts Department of Environmental Protection BWSC108 Bureau of Waste Site Cleanup COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM& PHASE I COMPLETION STATEMENT Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) B.THIS FORM IS BEING USED TO(cont): (check all that apply) ❑ 14. Submit a Revised Phase IV Completion Statement,pursuant to 310 CMR 40.0878 and 40.0879. [� 15. Submit a Phase V Status Report,pursuant to 310 CMR 40.0892. ❑✓ 16. Submit a Remedial Monitoring Report.(This report can only be submitted through eDEP.) a.Type of Report:(check one) ❑ i. Initial Report Q✓ ii. Interim Report ❑ iii. Final Report b.Frequency of Submittal:(check all that apply) i. A Remedial Monitoring Report(s)submitted monthly to address an Imminent Hazard. ii. A Remedial Monitoring Report(s)submitted monthly to address a Condition of Substantial Release Migration. ❑✓ iii. A Remedial Monitoring Report(s)submitted concurrent with a Status Report. c.Status of Site:(check one) ❑ I. Phase V ✓0 ii. Remedy Operation Status O iii.Class C RAO . I d. Number of Remedial Systems and/or Monitoring Programs: i A separate BWSC108A,CRA Remedial Monitoring Report,must be filled out for each Remedial System and/or Monitoring Program addressed by this transmittal form. 17. Submit a Remedy Operation Status,pursuant to 310 CMR 40.0893. ® 18. Submit a Status Report to maintain a Remedy Operation Status,pursuant to 310 CMR 40.0893(2). 19. Submit a Modification of a Remedy Operation Status,pursuant to 310 CMR 40.0893(5). 20. Submit a Termination of a Remedy Operation Status,pursuant to 310 CMR 40.0893(6). ❑ 21. Submit a Phase V Completion Statement,pursuant to 310 CMR 40.0894. Specify the outcome of Phase V activities: (check one) a. The requirements of a Class A Response Action Outcome have been met. No additional Operation,Maintenance or Monitoring is necessary to ensure the integrity of the Response Action Outcome. A completed Response Action Outcome Statement(BWSC104)will be submitted to DEP. b. The requirements of a Class C Response Action Outcome have been met. No additional Operation,Maintenance or ❑ Monitoring is necessary to ensure the integrity of the Response Action Outcome. A completed Response Action Outcome Statement and Report(BWSC104)will be submitted to DEP. c. The requirements of a Class C Response Action Outcome have been met. Further Operation,Maintenance or Monitoring of the remedial action is necessary to ensure that conditions are maintained and/or that further progress is made toward a Permanent Solution. A completed Response Action Outcome Statement and Report(BWSC104)will be submitted to DEP. 022. Submit a Revised Phase V Completion Statement,pursuant to 310 CMR 40.0894. 23. Submit a Post-Class C Response Action Outcome Status Report,pursuant to 310 CMR 40.0898. (All sections of this transmittal form must be filled out unless otherwise noted above) Revised: 2/15/2005 Page 2 of 5 i Bureau of Waste Site of Environmental Protection Massachusetts De to Cleanup BWSC108 COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM& PHASE I COMPLETION STATEMENTELI - - Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) C. LSP SIGNATURE AND STAMP: I attest under the pains and penalties of perjury that I have personally examined and am familiar with this transmittal form, including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of(i)the standard of care in 309 CMR 4.02(1),(ii)the applicable provisions of 309 CMR 4.02(2)and(3),and 309 CMR 4.03(2),and (iii)the provisions of 309 CMR 4.03(3),to the best of my knowledge,information and belief, > if Section B indicates that a Phase 1,Phase 11,Phase Ill,Phase IV or Phase V Completion Statement is being submitted,the response action(s)that is(are)the subject of this submittal(1)has(have)been developed and implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,and(iii) comply(ies)with the identified provisions of all orders,permits,and approvals identified in this submittal; > if Section B indicates that a Phase H Scope of Work or a Phase IV Remedy Implementation Plan Is being submitted,the response action(s)that is(are)the subject of this submittal(1)has(have)been developed in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,and(iii)comply(ies)with the identified provisions of all orders,permits,and approvals identified in this submittal; > if Section B indicates that an As-Built Construction Report,a Remedy Operation Status,a Phase IV,Phase V or Post-Class C RAO Status Report,a Status Report to Maintain a Remedy Operation Status and/or a Remedial Monitoring Report is being submitted,the response action(s)that is(are)the subject of this submittal(1)is(are)being implemented in accordance with the { applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,and(iii)comply(ies) With the identified provisions of all orders,permits,and approvals identified in this submittal. 1 I am aware that significant penalties may result,including,but not limited to,possible fines and imprisonment,if I submit ` information which I know to be false,inaccurate or materially incomplete. 1. LSP#: 2. First Name: 3. Last Name: .6 .4. Telephone: 5. Ext.. �. : � � 6. FAX 7. Signature: ` � of 8. Date , iL3'lis * 9.LSP Stamp: (mm/dd/yyyy) OF a14s� 1f't1 g ERIC cy� , D. SIMPSON y No.8881 ' �SIIE t�4ts Revised: 2/15/2005 Page 3 of 5 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC108 COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM& PHASE I COMPLETION STATEMENT Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) D. PERSON UNDERTAKING RESPONSE ACTIONS: 1. Check all that apply: Ela.change in contact name ❑ b.change of address ❑ c. change in the person undertaking response actions 2. Name of Organization: MOTIVA ENTERPRISES LLC 3. Contact First Name: DAVID B 4.Last Name: WEEKS 5. Street: PMB 3011830 SOUTH RD UNIT 24 6.Title: OWNER 7. City/Town: WAPPINGERS FALLS 8 State: NY 9. ZIP Code: 12590-4999 10. Telephone: 8454625225 11 Ext: u 12. FAX: I E. RELATIONSHIP TO SITE OF PERSON UNDERTAKING RESPONSE ACTIONS: i ❑✓ 1. RP or PRP ❑ a. Owner ❑ b. Operator ❑ c. Generator ❑ d. Transporter f © e. Other RP or PRP Specify: PRP GENERIC OR NON-SPECIFIED }fi ❑ 2. Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E,s.2) ❑ 3. Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E.s.50)) ❑ 4. Any Other Person Undertaking Response Actions Specify Relationship: F. REQUIRED ATTACHMENT AND SUBMITTALS: 1. Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order(s),permit(s) ❑ and/or approval(s)issued by DEP or EPA. If the box is checked,you MUST attach a statement identifying the applicable provisions thereof. ❑ 2. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the submittal of any Phase Reports to DEP. ❑ 3. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the availability of a Phase III Remedial Action Plan. ❑ 4. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the availability of a Phase IV Remedy Implementation Plan. ❑ 5. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of any field work involving the implementation of a Phase IV Remedial Action. 6. If submitting a Modification of a Remedy Operation Status,check here to certify that a statement detailing the compliance history,as per 310 CMR 40.0893(5),for the person making this submittal is attached. ❑ 7. If submitting a Modification of a Remedy Operation Status,check here to certify that written consent of the person who submitted the Remedy Operation Status submittal,as per 310 CMR 40.0893(5),is attached. ❑ 8. Check here if any non-updatable information provided on this form is incorrect,e.g.Site Name. Send corrections to the DEP Regional Office. ❑✓ 9. Check hereto certify that the LSP Opinion containing the material facts,data,and other information is attached. s Revised: 2/15/2005 Page 4 of 5 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC108 COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM&PHASE I COMPLETION STATEMENT Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) G. CERTIFICATION OF PERSON UNDERTAKING RESPONSE ACTIONS: 1. I,DAVID WEEKS ,attest under the pains and penalties of perjury(i)that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true,accurate and complete,and(iii) that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. I/the person or entity on whose behalf this,submittal is made am/is aware that there are significant penalties,including,but not limited to, possible fines and imprisonment,for willfully submitting false,inaccurate,or incomplete information. 2 By OWNER 3. Title: Signature I 4. For: MOTIVA ENTERPRISES LLC 5. Date: 05/07/2007 I (Name of person or entity recorded in Section D) (mm/dd/yyyy) i I f 6. Check here if the address of the person providing certification is different from address recorded in Section D. 7. Street: I i 8. City/Town: 9. State: 10. ZIP Code: 11. Telephone: 12.Ext.: 13. FAX YOU ARE SUBJECT TO AN ANNUAL COMPLIANCE ASSURANCE FEE OF UP TO$10,000 PER BILLABLE YEAR FOR THIS DISPOSAL SITE YOU MUST LEGIBLY COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR.DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Date Stamp(DEP USE ONLY:) 6/19/2007 4:13:50 PM f Revised: 2/15/2005 Page 5 of 5 r Massachusetts Department of Environmental Protection BWSC108A Bureau of Waste Site Cleanup Release Tracking Number CRA REMEDIAL MONITORING REPORT Pursuant to 310 CMR 40.0800(SUBPART H) 4❑ - 17651 Remedial System or Monitoring Program: 1 � of:0 A DESCRIPTION OF ACTIVE REMEDIAL SYSTEM OR ACTIVE REMEDIAL MONITORING PROGRAM: 1. Type of Active Remedial System or Active Remedial Monitoring Program:(check all that apply) ❑ a. Active Remedial System:(check all that apply) ❑ i.NAPL Recovery ❑ H. Soil Vapor Extraction/Bioventing ❑ iii. Vapor-phase Carbon Adsorption ❑ iv.Groundwater Recovery ❑ v. Dual/Multi-phase Extraction ❑ vi. Aqueous-phase Carbon Adsorption ❑ vii.Air Stripping ❑ viii. Sparging/Biosparging ❑ ix. Cat/Thermal Oxidation ❑ x. Other Describe: ❑ b. Application of Remedial Additives:(check all that apply) ❑ i.To the Subsurface ❑ ii. To Groundwater(Injection) ❑ iii. To the Surface a c. Active Remedial Monitoring Program Without the Application of Remedial Additives:(check all that apply;Sections C,D and E are not required;attach supporting information,data,maps and/or sketches needed by checking Section F5) j i ❑ i.Reactive Wall 0 ii. Natural Attenuation ❑ iii. Other Describe: 2. Mode of Operation:(check one) } ❑ a. Continuous ❑ b. Intermittent ❑ c. Pulsed ❑ d. One-time Event Only ❑ e. Other: 3. System EffluenUDischarge:(check all that apply) ❑ a.Sanitary Sewer/POTW ❑ b.Groundwater Re-infiltration/Re-injection:(check one) ❑ i. Downgradient ❑ ii.Upgradient c. Vapor-phase Discharge to Ambient Air.(check one) ❑ I. Off-gas Controls ❑ ii. No Off-gas Controls ❑ d. Drinking Water Supply ❑ e. Surface Water(including Storm Drains) ❑ f. Other Describe: B. MONITORING FREQUENCY: 1. Reporting period that is the subject of this submittal: From: 6/19/2006 To: 5/7/2007 (mm/dd/yyyy) (mm/dd/YYYY) 2. Number of monitoring events during the reporting period:(check one) ❑ a.System Startup:(if applicable) ❑ i. Days 1,3,6,and then weekly thereafter,for the first month. ❑ it. Other Describe: Qb.Post-system Startup(after first month)or Monitoring Program: ❑ i.Monthly ❑✓ ii.Quarterly ❑ !it. Other Describe: 03. Check here to certify that the number of required monitoring events were conducted during the reporting period. C. EFFLUENT/DISCHARGE REGULATION:(check one to indicate how the effluent/discharge limits were established) ❑ 1.NPDES:(check one) 0 a. Remediation General Permit ❑ b.Individual Permit ❑ c.Emergency Exclusion Effective Date of Permit: ❑ 2. MCP Performance Standard MCP Citatio_ns(s): 3. DEP Approval Letter Date of Letter. mm/dd/ ❑ 4. Other Describe: Revised: 2/9/2005 Page 1 of 3 _.._............. ... ......_--._...._.-..._.._._.._...___... Massachusetts Department of Environmental Protection gWSC108A Bureau of Waste Site Cleanup CRA REMEDIAL MONITORING REPORT Release Tracking Number Pursuant to 310 CMR 40.0800(SUBPART H) �-� 4❑ - 17651 Remedial System or Monitoring Program: 1! of. D. WASTEWATER TREATMENT PLANT OPERATOR:(check one) ❑ 1. Required due to Remedial Wastewater Treatment Plant in place for more than 30 days. a.Name: _ b. Grade: c.License No.: d.License Exp.Datel ❑ 2. Not Required (mm/dd/yyyy) ❑ 3. Not Applicable E. STATUS OF ACTIVE REMEDIAL SYSTEM OR ACTIVE REMEDIAL MONITORING PROGRAM DURING REPORTING PERIOD: (check all that apply) i ❑ 1.The Active Remedial System was functional one or more days during the Reporting Period. j a. Days System was Fully Functional: — b.GW Recovered(gals): c. NAPL Recovered(gals): d.GW Discharged(gals): e.Avg.Soil Gas Recovery Rate(scfm): �— —, I. Avg.Sparging Rate(scfm): ❑ 2.Remedial Additives:(check all that apply) ❑ a.No Remedial Additives applied during the Reporting Period. ❑ b.Enhanced Bioremediation Additives applied:(total quantity applied at the site for the current reporting period) ❑ i.Nitrogen/Phosphorus: ❑ ii.Peroxides: Name of Additive Date Quantity Units Name of Additive Date Quantity Units ❑ ill.Microorganisms: F1 iv.Other. Name of Additive Date Quantity Units Name of Additive Date Quantity Units ❑ c.Chemical oxidation/reduction additives applied:(total quantity applied at the site for the current reporting period) ❑ i.Permanganates: ❑ ii.Peroxides: Name of Additive Date Quantity Units Name of Additive Date Quantity Units ❑ iii.Persulfates: iv.Other: Name of Additive Date Quantity Units Name of Additive Date Quantity Units Revised: 2/9/2005 Page 2 of 3 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC108A CRA REMEDIAL MONITORING REPORT Release Tracking Number Pursuant to 310 CMR 40.0800(SUBPART H)f� 4F - 17651 Remedial System or Monitoring Program: t l of:0 E. STATUS OF ACTIVE REMEDIAL SYSTEM OR ACTIVE REMEDIAL MONITORING PROGRAM DURING REPORTING PERIOD:(cont.) (check all that apply) d.Other additives applied:(total quantity applied at the site for the current reporting period) Name of Additive Date Quantity Units Name of Additive Date Quantity Units e. Check here if any additional Remedial Additives were applied. Attach list of additional additives and include Name of Additive,Date Applied,Quantity Applied and Units(in gals.or lbs.) F. SHUTDOWNS OF ACTIVE REMEDIAL SYSTEM OR ACTIVE REMEDIAL MONITORING PROGRAM:(check all that apply) 1. The Active Remedial System had unscheduled shutdowns on one or more occasions during the Reporting Period. i a.Number of Unscheduled Shutdowns: b.Total Number of Days of Unscheduled Shutdowns: ! } c.Reason(s)for Unscheduled Shutdowns: I I I 2. The Active Remedial System had scheduled shutdowns on one or more occasions during the Reporting Period. a.Number of Scheduled Shutdowns: b.Total Number of Days of Scheduled Shutdowns: I c.Reason(s)for Scheduled Shutdowns: i 3. The Active Remedial System or Active Remedial Monitoring Program was permanently shutdown/discontinued during the Reporting Period. a.Date of Final System or Monitoring Program Shutdown: b. No Further Effluent Discharges. (mm/dd/YYYY) c. No Further Application of Remedial Additives planned;sufficient monitoring completed to demonstrate compliance with 310 CMR 40.0046. d. No Further Submittals Planned. e. Other. Describe: G. SUMMARY STATEMENTS:(check all that apply for the current reporting period) 1. All Active Remedial System checks and effluent analyses required by the approved plan and/or permit were performed when applicable. Q2. There were no significant problems or prolonged(>25%of reporting period)unscheduled shutdowns of the Active Remedial System. 3. The Active Remedial System or Active Remedial Monitoring Program operated i n conformance with the MCP,and all applicable approval conditions and/or permits. 4. Indicate any Operational Problems or Notes: 5. Check here if additional/supporting Information,data,maps,and/or sketches are attached to the form. ,.5 Revised: 2/9/2005 Page 3 of 3 Environniental services executed safe&and romrstentll. PHASE V REMEDY OPERATING STATUS REPORT Former Shell-Branded Service Station 590 Iyannough Road Hyannis, Massachusetts 02601 Incident#97451486 SAP#13772 June 19,2007 MassDEP RTN 4-17651 Prepared for: Motiva Enterprises LLC 1830 South Road Unit 24,PMB 301 Wappingers Falls, New York 12590 Prepared by: Sovereign Consulting Inc. 905B South Main Street Suite 202 Mansfield,MA 02048 Sovereign File: EQ872 Inspection and Monitoring Report for Phase V ROS-RTN 4-17651 June 19,2007 Former Shell-Branded Service Station,590 Iyannough Road,Hyannis,MA TABLE OF CONTENTS 1.0 INTRODUCTION.....................................................................................................1 2.0 SITE DESCRIPTION AND BACKGROUND..........................................................1 2.1 Site Description....................................................................................................1 2.2 Release History ....................................................................................................1 2.2.1 RTN 4-18156.........................................................................................................................2 3.0 INSPECTION AND MONITORING REPORT 3 ....................................................... 3.1 Description of the Type and Frequency of Activities Conducted:310 CMR 40.0892(2)(a) ..........................................................................................................3 3.2 Significant Modifications Since Submittal of Preceding I&M Report:310 CMR 40.0892(2)(b)..........................................................................................................3 3.3 Conditions and/or Problems Affecting Remedial Action Performance:310 CMR 40.0892(2)(d)..........................................................................................................3 3.4 Measure Taken To Correct Conditions and/or Problems:310 CMR 40.0892(2)(d)3 3.5 Analytical Data and Discussion Data:310 CMR 40.0892(2)(c) ............................3 3.6 Summary and Conclusions..................................................................................4 3.7 Schedule...............................................................................................................4 FIGURES Figure 1 Site Locus Map Figure 2 Site Plan TABLES Table 1 Summary of Groundwater Monitoring Data-VPH,EDB,Lead Table 2 Summary of Groundwater Field Parameter Data-MNA ATTACHMENTS Attachment A Copy of Laboratory Analytical Data i Inspection and Monitoring Report for Phase V ROS-RTN 4-17651 June 19,2007 Former Shell-Branded Service Station,590 Iyannough Road,Hyannis,MA 1.0 INTRODUCTION Sovereign Consulting Inc. (Sovereign) prepared this Phase V Remedy Operating Status Inspection and Monitoring (Phase V I&M) Report on behalf of Motiva Enterprises LLC (Motiva). The report presents information related to the operation, maintenance, and/or monitoring of the selected remedial action alternatives(RAAs) for Massachusetts Department of Environmental Protection (MassDEP) Release Tracking Number(RTN)4-17651. In accordance with 310 CMR 40.0892, this report discusses the type, frequency, modifications, conditions, problems, measures, and sampling conducted with regard to the selected RAAs to support the implementation of the Comprehensive Remedial Action (CRA) at the site. This Phase V I&M summarizes environmental activities and response actions conducted from December 19,2006 through June 19,2007. 2.0 SITE DESCRIPTION AND BACKGROUND 2.1 Site Description The subject property is comprised of one parcel of land totaling approximately 20,900 square feet located on the northern side of Iyannough Road and the western side of Hinckley Road in Hyannis, Massachusetts.The subject property was formerly developed as a Shell-branded retail gasoline and automotive repair facility. The property is currently operated as a retail gasoline and automotive repair facility known as "Sav-On". A release of gasoline at the former Shell- branded service station is the subject of RTN 4-17651. According to data obtained from Massachusetts Geographic Information Systems (Mass GIS) maps, groundwater beneath the disposal site is located within a Zone II Wellhead protection district. GW-1 standards apply to groundwater within the disposal site. A private potable well was formerly located at 37 Hinckley Road, New England Tile Company. In September 2006,37 Hinckley Road was connected to the municipal water supply and use of the private drinking water well was discontinued. On November 21, 2006 Sovereign personnel confirmed the connection to municipal water supplies with Mr.Steve Opdyke,the owner of New England Tile and with the town of Barnstable. 2.2 Release History In August 1989 Groundwater Technology Inc., (GTI) prepared a Phase - 1 Limited Site Investigation for Shell Oil Company. The property` was listed with the Massachusetts Department of Environmental Protection (MassDEP) on October 15, 1989 as a Location To Be Investigated (LTBI). On November 4, 1996, Handex submitted a Class B-1 Response Action Outcome (RAO) Statement and Method 1 Risk Characterization identifying a condition of "no significant risk"for RTN 4-0793. As part of a voluntary internal Motiva program designed to evaluate properties located in potentially sensitive areas,soil borings were installed at the site and groundwater samples were collected. Results of analysis on samples collected reported concentrations of volatile organic compounds (VOCs) in excess of the MassDEP GW-1 concentration. A Release Notification Form 1 � Inspection and Monitoring Report for Phase V ROS- RTN 4-17651 June 19 2007 Former Shell-Branded Service Station,590 Iyannough Road,Hyannis,MA (RNF) was submitted to the MassDEP on February 10, 2003, which identified a 120-day notification condition of volatile petroleum hydrocarbons (VPH) fractions detected in groundwater samples at concentrations greater than the Reportable Concentrations (RC) for category GW-1 groundwater. On February 24, 2003, the MassDEP was notified of a 72-hour reporting condition for VPH fraction concentrations detected in excess of the applicable RC for category GW-1 groundwater located within 500 feet of two private water supply wells. In response to the notification, the MassDEP issued RTN 4-17651 to this release condition. A Phase I- Initial Site Investigation Report, Numerical Ranking System (NRS)Score sheet, and Tier Classification was submitted to the MassDEP on December 19, 2003 for RTN 4-17651. Based on exclusionary criteria (the site is within a mapped Zone II) on the NRS Score Sheet the site was classified as Tier 1C and a Tier 1C Permit Application (Permit#W046008)was submitted to the MassDEP. A Phase II Scope of Work (SOW) for RTN 4-17651 was submitted December 19, 2003. A Release Abatement Measure (RAM) Plan was submitted to the MassDEP in September 21, 2004. The RAM Plan was submitted in order to appropriately manage Remediation Waste generated during the scheduled upgrade of underground storage tank (UST) dispensing equipment. A RAM Completion Report was submitted on December 2, 2004 documenting that no Remediation Waste was generated during these activities. A Phase II Comprehensive Site Assessment, Phase III Remedial Action Plan, Phase IV Remedy Implementation Plan, Phase IV Final Inspection Report, and Phase IV Completion Statement were all submitted on December . 13,2005.A Phase V Remedy Operating Status Report was submitted on December 19,2006. 2.2.1 RTN 4-18156 On June 11, 2003 a RAM Plan was submitted to the MassDEP. The RAM Plan was prepared for the appropriate management of petroleum impacted soil and/or groundwater encountered during hydraulic lift removal activities. A RAM Completion Report was submitted to the MassDEP on October 7,2003. Upon review of the in-situ soil sample analytical results, RNF was submitted to the MassDEP on November 21, 2003 for the detection of C11-C12 aromatic hydrocarbons at concentration greater than the RC S-1 soil standards. The MassDEP subsequently issued RTN 4-18156 in response to this condition. On January 15, 2004 a RAM Plan was submitted to the MassDEP for RTN 4-18156. The RAM Plan was prepared for the appropriate management of petroleum impacted soil and/or groundwater encountered during excavation activities. A Class A-1 RAO Statement and RAM Completion Report for RTN 4-18156 was submitted to the MassDEP on March 15,2004. 2 I Inspection and Monitoring Report for Phase V ROS-RTN 4-17651 June 19,2007 Former Shell-Branded Service Station,590 Iyannough Road,Hyannis,MA 3.0 INSPECTION AND MONITORING REPORT 3.1 Description of the Type and Frequency of Activities Conducted: 310 CMR 40.0892(2)(a) On March 1, and May 3, 2007, Sovereign personnel conducted groundwater sampling at the site. During the sampling event, 10 monitoring wells were gauged and sampled. Groundwater samples were submitted to Test America of Nashville, Tennessee in accordance with chain of custody procedures for VPH, dissolved lead, 1,2-Dibromoethane (EDB) analyses. Depth to water (DTW), conductivity, temperature, oxidation/reduction potential (ORP), dissolved oxygen (DO), and pH were measured in each monitoring well. Results from the May 2007 sampling event document that groundwater, sampled from one monitoring well contained COCs above applicable MCP Method 1 Standards. The results of groundwater sampling and field measurements are summarized in Tables 1 and 2. Refer to Attachment A for copies of the laboratory analytical reports. 3.2 Significant Modifications Since Submittal of Preceding I&M Report: 310 CMR 40.0892(2)(b) No significant modifications to the RAAs were conducted during this reporting period. 3.3 Conditions and/or Problems Affecting Remedial Action Performance: 310 CMR 40.0892(2)(d) No significant problems affecting the remedial action performance. 3.4 Measure Taken To Correct Conditions and/or Problems:310 CMR 40.0892(2)(d) No corrective measures were taken during this reporting period. 3.5 Analytical Data and Discussion Data:310 CMR 40.0892(2)(c) Concentrations of dissolved phase COCs in groundwater remain above applicable Method 1 GW-1 and/or GW-3 standards in one site well (GT-5) during this reporting period. Results are summarized in Table 1. Copies of the groundwater laboratory reports are included as Attachment A. Temperature, pH, dissolved oxygen, ORP and conductivity measurements are summarized in Table 2. Quality Assurance/Quality Compliance (QA/QC) data provided in the laboratory reports was within acceptable limits for all samples. 3 Inspection and Monitoring Report for Phase V ROS-RTN 4-17651 June 19,2007 Former Shell-Branded Service Station,590 Iyannough Road,Hyannis,MA 3.6 Summary and Conclusions Overall COC concentrations in groundwater are decreasing. Current data does not suggest any on-going sources or new releases of COCs at the disposal site (i.e. impacts in all wells are consistent with past data). Groundwater sampling will continue on a quarterly basis. 3.7 Schedule Groundwater Sampling August, &November 2007 Inspection and Monitoring Report December 19,2007 r 4 Inspection and Monitoring Report for Phase V ROS-RTN 4-17651 June 19,2007 Former Shell-Branded Service Station,590 Iyannough Road,Hyannis,MA FIGURES 1 p - f 1 w r .i►�' a � , '} q � ? �1 - # 4 Ili ' 'L ` 't �`' ,{f( e ,Z: �.Cravel��its � • _... .. �` `" l ��. �•� _t..� �bl„� ��. rive l 6 'fh Ij F ~�1 .,* 1r ( 5, �" � � 4 � �p• {,_Ey�"'` ��l � 1 + t �� • ! r it heater G �'� I t� fh w 1 [ tiJ n r•••t — , if F ay 1 r I- 4 +1 /16 r • `SS��.. �� Lt�IR '`� r.�� L'y �•`yf \4 1 rA t{.�,.V,-,-` •'j.;�I�3' 'y'.. .. 4� .� �(.•� ;�'?rr��.� U (�'....lit '� i� r 1 • s I`'1/' SITE LOCATION _4j 45 S81 3 _P7 Md. Via: � �• I*+,a.,......../;r,� r �" ram:, r, q i ••,� ,` �. � Y•w/yl7�.� �� � � �llll ��'�r, i kp �\.`, \\ � t�� tA,. •� (Y .. Fire Imam— SOVEREIGN CONSULTING INC. Reference.- Hyannis, MA Quadrangle- USGS 1988 FIGURE 1 Contour Interval = 3 meters SITE LOCATION MAP Former Shell Branded Service Station UTM 19 392621E 4613259N 5901yannough Road, Hyannis, MA Sovereign Scale(approx.) Job No. 1"= 1000' EQ872 LOCATION OF FORMER POTABLE WELL B MONITORING WELL ® SOIL BORING `"- B DEEP MONITORING WELL PIZZERIA A DESTROYED PUMPING WELL NEW ENGLAND UN� LE APPROXIMATE LOCATION OF 37 T HINCKLEY AVENUE PRIVATE WELL ® MANHOLE GT-102 �` ® CATCH BASIN PROPERTY BOUNDARY X- FENCE LINE ® ./BGT-101 x USED ,� W WATER LINE GRASS OIL UST tj OSS-203 1 '1 -G -GAS LINE ® C r g -OHW-OVERHEAD WIRES , ----X -- ` UST UNDERGROUND STORAGE TANK FUEL f1 GASOLINE ` OIL US jl BUILDING I "I f I UST AREA SB-204 1 11 MT-3/MT•-1& i`41. VACANT ' l_ L� �, ASPHALT ram' ,���®B- OS DISPENSER ASPHALT GT-1 ` ISLANDS GTV GT—$ 4 L__ SBJ2026 SB 20 PW-1 —C —G --G —G —G —G —G —G —G E IYANNOUGH ROAD 2 nG CAPE `L OPTICIANS O O MW-202 B MW-2020 FIGURE 2 _ Sovereign ConsultingInc. SITE PLAN 1600 Boston-Providence Hwy Walpole,MA 02081 SHELL SERVICE STATION#137772 (508)404 1866 Fax(508)404 1867;zim-o Iff 590 IYANNOUGH ROAD APPROXIMATE SCALE IN FEET NOTE ORIGINAL MAP FROM GSC FIELD RECONNAISSANCE. I Pmj-aNa Filc P0IMMAP0YANNUSSPAwg Dm 11m106 HYANNIS,MASSACHUSETTS i Inspection and Monitoring Report for Phase V ROS-RTN 4-17651 June 19,2007 Former Shell-Branded Service Station,590 Iyannough Road,Hyannis,MA TABLES TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH,EDB AND LEAD Former Shell Service Station#137772 590lyannough Road Hyannis,MA Ethyl- Total Naphtha- C-1 CS C9-C12 C9-CI0 Ethylene Dissolved Method 1 Benzene Toluene benzene Xylenes BTEX MTBE lene Aliphatics Aliphatics Aromatics Dibromide Lead Standards (P&'L) (AS/I) (PPS) (AYE) (PPS) (Ag/I) (PPS) (ABA) (AS/►�) (AYE) (uSn) (mP4) GW-1 5 1,000_ 700 10,000 N/A 70 140 _ 400 4,000 200 0.02 15 GW-2 2,000 8,000 _ 30,000 9,000 N/A 50,000 1,000 _ 1,000 1,000 5,000__ 2 NE GW-3 10,0)0 4,000 4,000 500 N/A - 50,000 20,000 4,000 20,000 4,000 50,000 10 Well ID Sample Date Depth to Corrected - '' ""% t% TOC Bev. Water Water Elev. 37 HINKLEY 4/22/2003 - - <0.5 <0.5 <0.5 <0.5 ND 2.5 <0.5 <50 <50 <50 <0.5 - 5/28/2003 - - <0.5 <0.5 <0.5 <0.5 ND 2.5 <0.5 <50 <50 <50 <0.5 7/22/2003 - - <0.50 <0.50 <0.50 <0.50 ND 1.7 <0.50 - _ _ <0.50 - 9/16/2004 - <0.53 <0.50 <0.50 <0.50 ND 1.2 <0.50 - - - <0.50 - 5/2/2005 <0.50 <0.50 <0.50 <0.50 ND <0.50 <0.50 <0.50 7/21/2005 - - <0.50 <0.50 <0.50 <0.50 ND 0.52 <0.50 - - - <0.50 - 10/10/2005 - - <0.50 <0.50 <0.50 <0.50 ND 0.79 <0.50 - - <0.50 - 1/16/2006 - - <0.50) <0.500 <0.500 <1.00 ND <0.500 <0.500 - - - <0.500 - 4/17/2006 - _ _ _ - ND <1.00 5/16/2006 - <0.500 <0.500 <0.500 <I.00 ND <0.500 <0.500 - - - <0.500 - Connected to Municipal Water in September 2006 - _ _ _ _ - _ _ _ _ GT-1 5/9/2003 23.85 74.17 <2.0 <2.0 <2.0 <4.0 ND 2.4 <3.0 81.9 <50 85.9 - - (GW-1,GW-3) 7/22/2003 24.11 73.91 <2.0 <2.0 <2.0 <4.0 ND 27.1 <3.0 <50 <50 <50 - - TOC 9/16/2004 26.39 71.63 <2.0 <2.0 <2.0 <4.0 ND 2 <3.0 637 <50 402 - - 98.02 5/2/2005 23.20 74.82 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 73 <50 <50 - - 7/21/2005 23.63 74.39 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 196 <50 97.5 - - 10/10/2005 24.95 73.07 <2.0 <20 <2.0 <4.0 ND <2.0 <3.0 131 <50 142 - - 1/16/2006 23.75 74.27 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 <100 103 <100 - - 4/17/2006 24.18 73.84 <1.00 <1.00 <1.00 <3.00 ND <1.00 <5,00 118 <100 <100 - - 10/25/2006 24.48 73.54 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 581 150 182 - - 3/l/2007 24.75 73.27. <1.00 <3.00 <1.00 <4.00 ND 73.7 <5.00 <100 <100 <100 <0.02023 <0.00500 5/3/2007 22.96 75.06 <1.00 <3.00 <1.00 <4.00 ND 7.06 <5.00 <100 114 <100 - 0.00800 5/3/2007 22.96 75.06 - -- - _ - 5.8• - __ _- - _ -_ GT-2 5/9/2003 24.45 74.06 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 79.8 - - (GW-1,GW-3) 7/22/2003 24.50 74.01 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 66 - - TOC 5/2/2005 23.56 74.95 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 - 98.51 7/21/2005 24.06 74.45 <2.0 <2.0 <2.0 <4.0 ND <2.0 4.0 <50 <50 <50 10/10/2005 25.39 73.12 <20 <2.0 <2.0 <4.0 ND <20 <3.0 <50 <50 <50 - - 1/16/2006 24.16 74.35 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 <100 <100 <100 - - 4/17/2006 24.83 73.68 <1.00 <1.00 <1.00 <3.00 ND <1.00 <5.00 <100 <100 <100 - - GT-3 11/15/2002 29.28 70.41 <2 <2 <2 <4 ND <2 <3 <50 <50 <50 (GW-1,GW-3) 5/9/2003 25.26 74.43 <2.0 <2.0 <2.0 <4.0 ND <20 <3.0 <50 <50 <50 TOC 7/22/2003 25.49 74.20 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 - - 99.69 5/2/2005 24.52 75.17 <2.0 <20 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 7/21/2005 25.00 74.69 <2.0 <20 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 - - 10/10/2005 26.30 73.39 <2.0 <2.0 <2.0 <4.0 ND <20 <3.0 <50 <50 <50 <0.015 - 4/17/2006 25.77 73.92 <1.00 <1.00 <1.00 <3.00 ND <1.00 <5.00 <100 <100 <100 - 10/25/2006 26.05 73.64 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 <100 <100 <100 - - 3/l/2007 26.33 73.36 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 <0.01994 <0.00500 5/3/2007 24.55 75.14 <1.00 <3.00 <1.00 I <4.00 ND <3.00 <5.00 <100 <100 <100 - <0.00500 GT4 11/15/2002 29.25 69.48 <2 <2 4.4 <4 ND <2 10A 1,820 1,300 2,780 - (GW-I,GW-3) 5/9/2003 24.54 74.19 <2.0 <2.0 <2.0 <4.0 ND 46.6 <3.0 750 <50 270 - TOC 7/22/2003 24.78 73.95 <2.0 <2.0 <2.0 <4.0 ND 35.7 <3.0 392 60.9 329 - - 98.73 9/16/2004 27.15 71.58 <2.0 <20 <2.0 <4.0 ND <2.0 <3.0 876 <50 339 - 5/2/2005 23.80 74.93 <20 <2.0 <2.0 <4.0 ND <2.0 <3.0 437 <50 <50 - - 7/21/2005 24.29 74.44 <2.0 <2.0 <20 <4.0 ND 2.1 <3.0 344 <50 83.8 - 10/10/2005 25.63 73.10 <2.0 <2.0 <2.0 <4.0 ND <2,0 <3.0 629 <50 322 <0.015 - 1/16/2006 24.41 74.32 <1.00 <3.00 <1.00 <6.00 ND <3,00 <5.00 449 <100 208 - 4/17/2006 25.03 73.70 1.62 <1.00 <1.00 <3.00 ND 3.25 <5.00 489 245 262 - - 10/25/2006 25.37 73.36 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 118 101 <100 - 3/1/2007 25.61 73.12 <1.00 <3.00 <1.00 <4.00 ND 4.30 <5.00 585 122 281 <0.02023 <0.00500 5/3/2007 28.83 69,90 <1.00 <3.00 <1.00 <4.00 ND 4.30 <5.00 251 <100 <100 - 0.00540 �C i TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH,EDB AND LEAD Former Shell Service Station#137772 590iyannough Road Hyannis,MA Ethyl- Total Naphtha- C5•CS C9C32 C9-C10 Ethylene Dissolved Method 1 Benzene Toluene benzene Xylenes BTEX MTBE lene Aliphatics Aliphatics Aromatics Dibromide Lead Standards I (pg/L) (Ng/L) (pg/L) (ug/L) (NgR-) (Ng(L) (N&,L) WWI.) (V91L) (p9/L) (ug/1) (mgA) GW-1 5 1,000 700 10,000 N/A 70 140 400 4,000 200 0.02 15 GW-2 2,000 8,000 30000 9,000 N/A 50000 1,000 1,000 1000 5,000 2 NE ---t-w-3 W-3 -To,-ow 4,000 4 000 500 N/A 50,000 20,000 4,000 20,000 4,000 50,000 10 Well ID Sample Date Depth to Corrected ' C r� '�, -` ;aa. ' c, - s A � 3 TOC Elev. Water Water Elev a.s ,u�, .,,. n s„F,,,:, <�*s_m<: ., a;, GT-5 11/15/2002 28.52 69.45 <2 <2 ,«a 23.2 23.2 <2 7.6+ �}488 256 946 - - (GW-1,GW-3) 5/9/2003 23.80 74.17 Q:0 <20 <2.0 16.7 16.7 <2.0 4.3 172 <50 577 - - TOC 7/22/2003 24.06 73.91 Q:0 <2.0 <2.0 12.7 12.7 <2.0 <3.0 135 109 638 - - 97.97 9/16/2004 26.33 71.64 <2.0 <2.0 <2.0 8 8 <2.0 <3.0 327 <50 958 - - 5/2/2005 23.07 74.90 <20 <2.0 <2.0 2.8 2.8 <1.0 <3.0 173 172 510 <0.015 <5.0 7/21/2005 23.57 74.40 <2.0 <20 <2.0 <4.0 ND <1.0 <3.0 135 <50 128 <0.015 11.7 10/10/2005 24.88 73.09 <2.0 <2.0 <2.0 2.4 2.4 <2.0 <3.0 201 <50 652 - - 1/16/2006 23.69 74.28 <110 <3.00 <1.00 <6.00 ND <3.00 <5.00 197 152 592 - - 4/17/2006 24.32 73.65 <1.00 <1.00 1.2 <3.00 1.2 <1.00 <5.00 188 440 670 - <5 10/25/2006 24.65 73.32 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 <100 <100 <100 - - 3/l/2007 24.90 73.07 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 153 151 520 <0.02029 <0.00500 5/3/2007 23.14 74.83 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 151 228 478 - <0.00500 GT-7 11/15/2002 28.31 69.47 <2 <2 <2 <4 ND <2 <3 173 74.5 312 - - (GW1,GW-3) 5/9/2003 23.60 74.18 <2.0 <20 <2.0 <4.0 ND <2.0 <3.0 147 <50 474 - - TOC 7/22/2003 23.84 73.94 <2,0 <20 <2.0 2.3 ND <2.0 3.6 155 127 701 - - 97.78 9/16/2004 26.12 71.66 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 155 <50 554 - 5/2/2005 22.84 74.94 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 197 194 558 - - 7/21/2005 23.39 74.39 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 126 <50 173 - - 10/10/2005 24.67 73.11 <2.0 <20 <2.0 <4.0 ND <2.0 <3.0 215 <50 807 - - 1/16/2006 23.47 74.31 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 118 <100 609 - - 4/17/2006 24.12 73.66 1.06 <1.00 <1.00 <3.00 ND <1.00 <5.00 218 950 1,120 <0.0200 <5 10/25/2006 24.43 73.35 <1.00 <9.00 <1.00 <6.00 ND <3.00 <5.00 <100 101 <100 - - 3/l/2007 24.70 73.08 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 205 <0.02000 <0.00500 5/3/2007 22.92 74.86 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 114 171 - <0.00500 MT•l/MF-3 10/28/2004 - - <2 <2 <2 <4 ND <2 <3 <50 <50 <50 - - (GW1,GW-3) 5/2/2005 22.65 74.87 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 - - TOC 7/21/2005 23.14 74.38 <20 <2.0 <2.0 <4.0 ND <2.0 <1.0 <50 <50 <50 - - 97.52 10/10/2005 24.50 73.02 <2.0 <2.0 <2.0 <4.0 ND <20 <3.0 <50 <50 <50 <0.015 - 1/16/2006 23.26 74.26 <I.00 <3.00 <1.00 <6.00 ND 29.8 <5.00 <100 <100 <100 - - 4/17/2006 23.89 73.63 <1.00 <1.00 <1.00 <3.00 ND <1.00 <5.00 <100 <100 <100 - - 10/25/2006 24.22 73.30 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 <100 <100 <100 - - 3/l/2007 24.29 73.23 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 <0.02041 <0.00500 5/3/2007 22.71 74.81 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 - <0.00500 NM-101 5/9/2003 25.12 74.42 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 - - (GW-1,GW-3) 7/22/2003 25.36 74.18 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 - - TOC 5/2/2005 24.35 75.19 <2.0 <2.0 <2.0 <4.0 ND <1.0 <3.0 <50 <50 <50 <0.015 <5.0 99.54 7/21/2005 24.85 74.69 <20 <2.0 <2.0 <4.0 ND <1.0 4.0 <50 <50 <50 <0.015 <5.0 10/10/2005 26.19 73.35 <2.0 <2.0 <2.0 <4.0 ND <20 <3.0 <50 <50 <50 - - 10/25/2006 25.60 73.94 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 <100 <100 <100 - - 3/l/2007 26.17 73.37 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 <0.0155 <0.00500 5/3/2007 24.41 75.13 <.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 - <0.00500 MW-102 5/9/2003 24.44 74.32 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 - - (GW-1,GW-3) 7/22/2003 24.68 74.08 <2.0 <2.0 <2.0 2.5 2.5 <2.0 <i.0 <50 <50 <50 - - TOC 5/2/2005 23.70 75.06 <2.0 <2.0 <2.0 <4.0 ND <1.0 <3.0 <50 <50 <50 0.02 <5.0 98.76 7/21/2005 24.20 74.56 <2.0 <2.0 <2.0 <4.0 ND <1.0 <3.0 <50 <50 <50 <0.015 <5.0 10/10/2005 25.55 73.21 <20 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 <0.015 - 1/16/2006 2222 76.54 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 <100 <100 <100 - - 4/17/2006 24.93 73.83 <1.00 <1.00 <1.00 <3.00 ND <1.00 <5.00 <100 <100 <100 - - 10/25/2006 25.25 73.51 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 <100 <100 <100 - - 3/l/2007 26.53 72.23 <1.00 I <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 <0.01966 <0.005W 5/3/2007 23.73 75.03 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 - <0.00500 TABLE 2 SUMMARY OF GROUNDWATER MONITORING DATA-MNA Former Shell Service Station#137772 590 Iyannough Road Hyannis,MA Conductivity Temp DO ORP Well ID Sample Date pH (PS/cm) VC) (mg(L) (mV) GT-1 10/25/2006 5.24 303 16.26 0.35 211.9 3/1/2007 5.82 442 12.24 5.23 241 5/3/2007 5.32 455 16.07 -* 200.4 GT-3 10/25/2006 5.74 427 15.12 1.03 126.7 3/1/2007 7.48 400 8.33 8.29 83 5/3/2007 5.95 454 15.9 -* 81.8 GT-4 10/25/2006 6.05 483 14.75 3.97 104.5 3/1/2007 6.11 420 12.16 3.64 223 5/3/2007 5.93 6410 15.07 -* 73.7 GT-5 7/21/2005 5.54 421 13.3 1.41 96.8 10/10/2005 5.2 485 13.53 1.84 124.3 1/16/2006 5.51 495 14.6 1.91 115.5 4/17/2006 5.79 367 14.33 2.45 118.7 10/25/2006 5.93 453 15.5 0.96 93.2 3/1/2007 6.15 318 11.96 3.37 220 5/3/2007 5.36 407 15.10 -* 153.4 GT-7 1/16/2006 5.97 461 14.24 0.88 76.8 4/17/2006 5.89 427 14.33 0.5 82.2 10/25/2006 6.02 542 14.6 0.83 101.3 3/1/2007 6.54 365 11.39 2.82 75 5/3/2007 5.77 491 10.11 -* 43.2 MT-3 10/25/2006 5.53 361 13.97 0.22 179.5 3/1/2007 6.24 406 13.04 5.57 187 5/3/2007 5.61 340 14.24 -* 183.1 MW-101 7/21/2005 5.03 449 13.16 5.66 178.1 10/10/2005 5.07 413 13.55 6.32 152.6 10/25/2006 5.42 393 14.29 1.38 148.3 3/1/2007 6.00 356 14.69 3.93 200 5/3/2007 5.35 239 14.80 -* 238.2 Page 1 of 2 TABLE 2 SUMMARY OF GROUNDWATER MONITORING DATA-MNA Former Shell Service Station#137772 590 Iyannough Road Hyannis,MA Conductivity Temp DO ORP Well ID Sample Date pH (µS/cm) VC) (mg/L) (mV) MW-102 7/21/2005 4.88 253 13.43 9.08 161.4 10/10/2005 4.8 317 13.48 9.93 165 1/16/2006 5.08 493 14.06 8.14 244 4/17/2006 5.10 204 11.53 7.05 320 10/25/2006 5.17 236 14.40 2.34 117.8 3/1/2007 6.13 167 13.20 5.18 166 5/3/2007 5.73 239 14.87 -* 192.1 MW-202 7/21/2005 4.96 554 12.94 1.34 197.9 10/10/2005 4.95 562 14.49 5.21 154.3 1/16/2006 4.91 647 14.15 0.48 309.3 4/17/2006 5.0 791 13.83 3.61 389.5 10/25/2006 5.27 851 14.11 0.29 156.6 3/1/2007 6.10 442 11.41 5.41 222 5/3/2007 5.19 690 14.15 -* 230.1 MW-202D 10/25/2006 5.0 741 14.01 0.23 170.4 3/1/2007 5.72 883 10.06 4.65 246 5/3/2007 5.09 767 15.01 -* 220.7 Notes: --is not sampled mg/L is milligrams per Liter (µg/L)is micrograms per Liter mV is millivolts µS/cm is microSiemens per centimeter *-DO readings not taken due to equipment malfunction Page 2 of 2 TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH,EDB AND LEAD Former Shell Service Station#137772 590lyannough Road Hyannis,MA EEthyl- Total Naphtha- CS-C8 C9-C12 C9-C10 Ethylene Dissolved Method 1 Benzene Toluenee Xylenes BTEX MTBE lene Aliphatics Aliphatics Aromatics Dibromide Lead Standards (pg(L) (pP/L) ) (ug(L) (pg1•) (pg/L) (pgM) (pg/L) (pg/L) (pg/L) (ug/1) (mg/1) GW-1 5 1,0W 10,000 N/A 70 140 400 4,000 200 0.02 15 GW-2 2,000 8kW 9,000 N/A 50,000 1,000 1,000 1,000 5,000 2 NE GW-3 10,000 4,000 500 N/A 50,000 20,000 4,000 20,000 4,000 50,000 10 Well ID Sample Date Depth to Corrected ' ] TOC Elev. Water NM-202 5/2/2005 21.60 74.69 r.0.. <2.0 <2.0 <4.0 ND <1.0 <3.0n <50 s. <50 <50 0.082 <5.0 (GW-1,GW-3) 7/21/2005 2211 74.18 <2.0 <2.0 <2.0 <4.0 ND <1.0 <3.0 <50 <1% <50 0.022 <5.0 TOC 10/10/2005 25.55 70.74 <2.0 <2.0 <20 <4.0 ND <20 <3.0 <50 <50 <50 <0.015 - %.29 1/16/2006 22.22 74.07 <1.00 <3.00 <.00 <6.00 ND <3.00 <5.00 <100 <100 <100 - - 4/17/2006 2288 73.41 <1.00 <1.00 <1.00 <3.00 ND <1.00 <5.00 <100 <100 <100 <0.0197 - 10/25/2006 23.17 73.12 <1.00 <3.00 <1.00 <6.00 ND <3.00 <5.00 <100 <100 <100 3/l/2007 24.35 71.94 <.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 <_0.02000 <0.00500 5/3/2007 21.67 74.62 <1.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <700 <00 <100 - <0.00500 MW-202D 5/2/2005 22.29 73.95 <2.0 <2.0 <2.0 <4.0 ND <20 <3.0 <50 <50 <50 - - (GW-1,GW-3) 7/21/2005 22.87 73.37 <2.0 <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 - - TOC 10/10/2005 23.40 72.84 Qp <2.0 <2.0 <4.0 ND <2.0 <3.0 <50 <50 <50 <0.015 - 96.24 1/16/2006 22.87 73.37 <110 <3.00 <1.00 <6.00 ND <3.00 <5.W <100 <100 <100 - - 4/17/2006 23.59 72.65 <1.00 <1,00 <1.00 <3.00 ND <1.00 <5.00 <100 <100 <100 - - 10/25/2006 23.90 72.34 <1.00 <3.00 <1.00 <6.00 ND <3.W <5.00 <100 <100 <100 - - 3/1/2007 28.12 68.12 <.00 <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 <0.02029 <0.W500 5/3/2007 22.30 73.94 <.W <3.00 <1.00 <4.00 ND <3.00 <5.00 <100 <100 <100 - <0.00500 NOTES: ug/L is micrograms per liter(parts per billion) <5.0 is less than the laboratory detection limit of 5.0 ug/L BTEX is total combined benzene,toluene,ethylbenzene,xylenes MTBE is methyl tertiary-butyl ether ND is non-detect NA is not applicable -not sampled Bold is concentration above applicable Method 1 Standards MCP Standards for this table are current as of April 2006 Wave 11 Update MTBE analytical was conducted from two labs to confirm results. Page V 3 �oFT"E, ti Town of Barnstable 0 Regulatory Services Barnstable BARN STABLE, * Thomas F. Geiler, Director Winerica City 163 ��� Public Health Division Thomas McKean,Director 2007 200 Main Street Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 November 23, 2010 Jay Imad Entr Iyannough Rd, LLC 326 West Main Street Hyannis, MA 02601 RE: Underground Storage Tank 590 IYANNOUGH ROAD/RTE132 HYANNIS Map/Parcel: 311017 Tank Number: 2 Tag Number: 00891 Our records indicate that your underground fuel (or chemical) storage tank exceeds twenty (20)years in age, and has not been removed as required by the Town of Barnstable Code Chapter 326, Section 3, Fuel and Chemical Storage Tanks. You are directed to remove this tank within sixty (60) days from the date of this Notice. Upon completion of the tank removal and within ninety(90) days of receipt of this Notice, please submit to this office a copy of the permit for storage tank removal issued by your local Fire Department. This copy of the removal permit serves as documentation that the underground storage tank was properly removed and disposed of. You may request a hearing provided that a written petition requesting same is received by the Board of Health within ten (10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, PS, CHO Health Agent Q:\Hazmat\Underground Tanks\let mail merge Undergrnd tanks 20 yr Nov2010 5nal.doc FTHE tom, Town of Barnstable ti Regulatory Services Barnstable BARN9 BM S& Thomas F. Geiler, Director AFAmerica Cily `b '°39• Public Health Division AtfD MA'S A Thomas McKean,Director 2007 200 Main Street Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 November 23, 2010 Jay Imad Entr Iyannough Rd, LLC 326 West Main Street Hyannis, MA 02601 RE: Underground Storage Tank 590 IYANNOUGH ROAD/RTE132 HYANNIS Map/Parcel: 311017 Tank Number: 3 Tag Number: 00892 Our records indicate that your underground fuel (or chemical) storage tank exceeds twenty (20)years in age, and has not been removed as required by the Town of Barnstable Code Chapter 326, Section 3, Fuel and Chemical Storage Tanks. You are directed to remove this tank within sixty (60) days from the date of this Notice. Upon completion of the tank removal and within ninety(90) days of receipt of this Notice, please submit to this office a copy of the permit for storage tank removal issued by your local Fire Department. This copy of the removal permit serves as documentation that the underground storage tank was properly removed and disposed of. You may request a hearing provided that a written petition requesting same is received by the Board of Health within ten (10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, PS, CHO Health Agent Q:\Hazmat\Underground Tanks\let mail merge Undergmd tanks 20 yr Nov2010 final.doc oFINE 1p Town of Barnstable Regulatory Services Barnstable * BARNSTABLE, ► 9 MASS. Thomas F. Geiler, Director A"mericaCity q, 1639. ,•A Public Health Division I ( I atEo�� Thomas McKean, Director 2007 200 Main Street Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 November 23, 2010 Jay Imad Entr Iyannough Rd, LLC 326 West Main Street Hyannis, MA 02601 RE: Underground Storage Tank 590 IYANNOUGH ROAD/RTE132 HYANNIS Map/Parcel: 311-017 Tank Number: 6 Tag Number: 00000 Our records indicate that your underground fuel (or chemical) storage tank exceeds twenty (20) years in age, and has not been removed as required by the Town of Barnstable Code Chapter 326, Section 3, Fuel and Chemical Storage Tanks. You are directed to remove this tank within sixty(60) days from the date of this Notice. Upon completion of the tank removal and within ninety (90) days of receipt of this Notice, please submit to this office a copy of the permit for storage tank removal issued by your local Fire Department. This copy of the removal permit serves as documentation that the underground storage tank was properly removed and disposed of. You may request a hearing provided that a written petition requesting same is received by the. Board of Health within ten (10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, PS, CHO Health Agent Q:\Hazmat\Underground Tanks\let mail merge Undergmd tanks 20 yr Nov2010 final.doc f IME T Town of Barnstable 0 Regulatory Services Barnstable RARNSTASLE. MASS. Thomas F. Geiler,Director �m 1619. �0� Public Health Division i I I I I., ArFD MA'S A Thomas McKean,Director 2007 200 Main Street Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 November 23, 2010 Jay Imad Entr Iyannough Rd, LLC 326 West Main Street Hyannis, MA 02601 RE: Underground Storage Tank 590 IYANNOUGH ROAD/RTE132 HYANNIS Map/Parcel: 311-017 Tank Number: 7 Tag Number: 00000 Our records indicate that your underground fuel (or chemical) storage tank exceeds twenty (20) years in age, and has not been removed as required by the Town of Barnstable Code Chapter 326, Section 3, Fuel and Chemical Storage Tanks. You are directed to remove this tank within sixty (60) days from the date of this Notice. Upon completion of the tank removal and within ninety(90) days of receipt of this Notice, please submit to this office a copy of the permit for storage tank removal issued by your local Fire Department. This copy of the removal permit serves as documentation that the underground storage tank was properly removed and disposed of. You may request a hearing provided that a written petition requesting same is received by the Board of Health within ten (10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, PS, CHO Health Agent Q:\Hazmat\Underground Tanks\let mail merge Undergrnd tanks 20 yr Nov2010 final.doc y��OFZNE Tp��� Town of Barnstable Regulatory Services Barnstable * B" '„ `E' * Thomas F. G.eiler,Director AFAmerica City 1639. ,.� Public Health Division ATFD��p Thomas McKean;Director 2007 200 Main Street - Hyannis, MA 02601 Office: 508-862-4644 Fax: 508-790-6304 November 23, 2010 Jay Imad Entr Iyannough Rd, LLC 326 West Main Street Hyannis, MA 02601 RE: Underground Storage Tank 590 IYANNOUGH ROAD/RTE132 HYANNIS Map/Parcel: 311017 Tank Number: 1 Tag Number: 00890 Our records indicate that your underground fuel (or chemical) storage tank exceeds twenty (20) years in age, and has not been removed as required by the Town of Barnstable Code Chapter 326, Section 3, Fuel and Chemical Storage Tanks. You are directed to remove this tank within sixty(60) days from the date of this Notice. Upon completion of the tank removal and within ninety(90) days of receipt of this Notice, please submit to this office a copy of the permit for storage tank removal issued by your local Fire Department. This copy of the removal permit serves as documentation that the underground storage tank was properly removed and disposed of. You may request a hearing provided that a written petition requesting same is received by the Board of Health within ten (10) days after this order is served. Per Order of the Board of Health Thomas A. McKean, PS, CHO Health Agent Q:\Hazmat\Underground Tanks\let mail merge Undergmd tanks 20 yr Nov2010 final.doc T OWN OF BARNSTABLE - UNDERGHUUND FUEL AND 1.I�L. S 1 UROGE RE(_j i S-►Rol 1 ION �C MAP NO. 3�/ PARCEL. NU. �� - TAG NO. , 7 (((ADDRESS OF "TANK: Slc�--�y/$�?,�9dri�,[1� ��✓ � VILLAGE: � S --- humb�r mtrw�t .MAILING ADDRESS ( IF DIFFERENT FROM ABOVE ) : O�S,t��$c/�T1Cf�l�i✓� s o7f�l/f�1 • C}/� �' OWNER NAME: /��S /�91C�!/�E(�! PHONE: INSTALLATION DATE: BY: INSTALLER ADDRESS: �lo��/l/� ��� ��r ©�5��( _'CERT .IV0. *TANK LOCATION: ABOVE . /BELOW r/�T ��K71 mcm I nG TANK LOOAT I ON WITH AQmPQCT TO mU I LD I NO) CAPAC I TY TYPE OF TANK � t)' 6AGEYRS. FUEL/CHEMICAL c TESTING CERTIFICATION [ ] PASS [ . I FAIL DATE LEAK DETECTION [ CHECK IF N/A TYPE/BRAND 7o ZONE OF CONTRIBUTION [ ] YES [ ] NO DATE TO BE REMOVED -, FIRE DEPT. PERMIT ISSUED [ j YES [ ] NO DATE CONSERVATION [ ] CHECK IF N/A DATE IjA; 1 s BOARD OF. HEALTH TAG NO. [ 43TrI ] DATE /� ' L�iv,e.112._ * PLEASE PROVIDE A SKETCH SHOWING _THE TANK,,LOCATION,-ON ..THE_:.BA, K.�-OF_..TH T-5-1,r.A.R:n_..- lUWN OF B(43NSTABL� - UNDFR6HUUND FUEL AND S101R06E R[E |SlRorlON ,MAP NO. PARCEL NO. / �A� N0 / '�-�-_�_�- � ADDRESS OF TANK VILLAGE : MAILING ADDRESS ( IF DIFFERENT FROM ABOVE ) : OWNER NAM` `t , PHONE: ����' INSTALLATION DATE: BY: INSTALLER ADDRESS: CERT.NO, *TANK LOCATION: au0vE -ac=^-rx_ - mai CAPACIT� TYPE OF 'TANK AGE RS. FUEL/CHEMlCAL \ TESTING CERTIFICATION [ ] PASS [ ] FAIL DATE LEAK DETECTION CHECK IF N/A TYPE/BRAND ZONE OF CONTRIBUTION [ ] YES [ ] NO DATE TO BE REMOVED / FIRE DEPT. PERMIT ISSUED [ kh YES [ ] NO DATE � CONSERVATION [ ��e CHECK IF N/A DATE � BOARD OF HEALTH TAG NO. [ \ / ] DATE * PLEASE pROVI.DE :,AJS,KETCH.SHOW,ING. THE, 3AN�~�OCAZIQ0~ON���E�g�r�x��m.s=ac� I Ow,N OF BARNSTABLE — UNCLE RGHUUND /FUEL IaND LA I1_!'i i 1,01. S/1 0 �1 7 GE RE( I S TRIG+ i I UN MAP NO. if PARCEL. NU. I / 'I'AG NO. ADDRESS OF TANK: �� .�cf ///1C1(/ '� VILLAGE : S — n+umb�r Ytr��t �., MAILING ADDRESS ( IF DIFFERENT FROM ABOVE ) : 0 i"1I7ny` l/1z f Sf'<�T/l1 PHONE: 7 OWNER NAME: -A`INSTALLATION DATE: BY INSTALLER ADDRESS � 71,e�` Z( Y� rP ,d— (� CERT .140. *TANK LOCATION: ABOVE BELOW /�� i�yL� 6r DCmOW I GG TANK LOCATION WITH ma4maCT TO mu I�/LD I NO) CAPACITY,/ �QO TYPE OF -TANK V AGE �� YRS. FUEL/CHEM I CAL G,4:50('Mr TESTING CERTIFICATION [ ] PASS [ ] FAIL DATE LEAK DETECTION [Sa CHECK IF N/A TYPE/BRAND ZONE OF CONTRIBUTION [ ] YES [ ] NO DATE TO BE REMOVED FIRE DEPT. PERMIT ISSUED [ YES [ ] NO DATE CONSERVATION [ ]/CHECK IF N/A DATE BOARD OF HEALTH TAG NO. [ � 17 ] DATEl . r PLEASE PROVIDE A SKETCH SHOWING. THE TANK._LOCATI.ON ON_v,T_HE_:. BACK..OF:,.THLS.:-CARD...-... | UWN OF BARNSTABLE - UNDERGHUUND FUEL (-)NU LoLn | ' oi 5101-R00E REGiSTRo/ lON ./// �/( - '� MAP NO, - PARCEL NO, TAG NO. Ff^ ` ADDRESS OF TANK: ��n vJL�RGE: MAILING ADDRESS ( IF DIFFERENT FROM ABOVE ) : � OWNER NAME: INSTALLATION DATE: . INSTALLER ADDRESS: -CERT .NO. *TANK LOCATION: ABOVE CAPAClT TYPE OF TANK AGEYRS. FUEL/CHEMlCAL TESTING CERTIFICATION [ ] PASS [ ] FAIL DATE LEAK DETECTION CHECK IF N/A TYPE/BRAND | | ZONE OF CONTRIBUTION [ ] YES [ ] NO DATE TO BE REMOVED FIRE DEPT. PERMIT ISSUED YES [ ] NO ' DATE �� /7-/�� ��. CONSERVATION [/CHECK IF N/A DATE � . BOARD OF HEALTH TAG NO. [ \ -? | ] DATE 1� ' * PLEASE' PROVIDE_A _SkETCH' �HDWlNG�JHE.�AN�� �"~� I OWN OF BARNSTABLE - UNDEPGHUUND FUEL AND l tl!_I`1 : 1,r�l. S I UROUE. RE(-41 S I P!i I I ON n i^�C MAP NO. _v r� FARCE 1_. NU. l - TAG NO. J ' ADDRESS OF TANK: S9U�� /�/7(}Ug/f __ VILLAGE : - MA I L I NG ADDRESS ( IF DIFFERENT FROM ABOVE) : SE ('f-/ OWNER NAME: �-s `V4i/E PHONE: INSTALLATION DATE: By: INSTALLER ADDRESS:-?)f ,d�s%�� d,� 7� A4 &-:5 d 'CER'T.IVO. �114 *TANK LOCATION: ABOVE QmCfV I DG TANK LOCATION W Z TH P�QOPQCT TO mU I LD Z NO) CAPACITY Z(J TYPE OF TANK DW i�l AGE 6✓01JYRS. FUEL/CHEMICALI- i JC%/iM TESTING CERTIFICATION [ ] PASS [A FAIL DATE LEAK DETECTION [�Q CHECK IF N/A TYPE/BRAND e/�"e-1 0711 c. ZONE OF CONTRIBUTION [ ] YES [ . ] NO DATE TO BE REMOV..ED FIRE DEPT. PERMIT ISSUED [ ;J YES [ ] NO DATE � - (' ��� CONSERVATION [ 1/1 CHECK IF N/A DATE -Ab + BOARD OF HEALTH TAG NO. [ J� ] DATE - * PLEASE PROVIDE A SKETCH SHOWING THE TANK yLOCATION. ON �THE__:BACK._ .OF .TF�I.�- r..A 'n 1 OWN OF BARNSTABLE - UNDEP(3HUUND FUEL laNl? t t tl.l`� : t.l�l. 5 I UIInvE RFG L S1 FCC, 1 I UN MAP NO. _? 'ORCEL. NU-.- _ -TAG NO. / ADDRESS OF TANK: �`�C7 ��/I;I rJv�t� � VILLAGE : .MAILING ADDRESS ( IF DIFFERENT FROM ABOVE ) :d /✓_ F. !EE'r-�j�l oK d `rf�.�67(-j, Al OtS ! OWNER NAME: B_�S GJ��i/E +'� �� PHONE: 135(r, INSTALLATION DATE: / BY:/ INSTALLER ADDRESS:. Ef ��if��r�/�fr?% i�? C �'3(tG� tAl ''CERT .IVO.�' lc�/t' *TANK LOCATION: ABOVE DCOOPQ I DG TAN)C LOCATION WITH AQOPQCT TO MU I LD//I NO ) - CAPACITYTr TYPE OF 'TANK / t✓' (9 AGE / �A,) YRS. FUEL/CHEMICAL TESTING CERTIFICATION [ ] PASS [ I LFAIL DATE � .• i — -- -- LEAK DETECTION [� CHECK IF 0A TYPE%BRAND-�'r'�C �y� � )'�.�, 1�dk ZONE OF CONTRIBUTION [ ] YES [ , ] NO DATE TO BE REMOVED ), FIRE DEPT. PERMIT ISSUED [ /J YES [ ] NO DATE �/r '/ /�l/�� _ • ' CONSERVATION [mol"CHECK IF N/A DATE BOARD OF HEALTH TAG No. DATE >k PLEASE. PROV 1 DE,.A, SKETCH .SHOW. ,NG,,,,T,HE, TANK_>LOGA,T'L.p:N..._ONs,THE- .BACK h.OF TH r:5 ..rAR.nW rr f � Q1 i! 'Ae j��Ooo ZQ 660 S 37�. 0�_�>av- S ow aKICS +0 bQ CV—KWVa a, -& 9POSP, 00511 dDo�Z PROCEDURE FOR UNDERGROUND TANK+MDC TRAP FOR MDC TRAP: OIL / WATER SEPARATOR and/or Underground Tank 1) FILL IN THE FORM (5 '/2 x 8 '/2, 3 ply=Underground Fuel and Chemical Storage Registration. 2) SEE Form and have (a) Fire Dept and (b) Conservation sign off 3) Draw a detailed map on back of last page of form to identify where the tank or trap is located with measurements. 4) Return completed card to the Public Health Division and a brass tag (the next numeric tag in sequence) will be issued and is to be attached to the trap on the tank. NOTE TO PUBLIC HEALTH DIVISION: Log in registration information and tag# into the Database for Health Parcels. Additional steps are necessary for UST—Clerks office and Fire Dept. JAN 2011 NOTE - PROCEDURE NECESSARY TO INCREASE THE SIZE OF THE UNDERGROUND FUEL TANK: The process begins with the applicant sending a letter of request addressed to the Town Manager, 367 Main Street, Hyannis. Good to include history and reasons for desired increase. The Town Manager will then review the case and determine whether the applicant can install a larger tank. Q:\Ofce Procedures\HALMAT.-PROCEDURE-UNDERGRND TANK+MDC Trap.doc PNIIIP A.AYOU6 � Registered P.E. } PHILIP A. �, LvY�yay New Hampshire - Connecticut ArouNo s.cx.0 New York - Vermont - Maine 'lb .•��t` PROiESSWIIAL[XGIXE[R �SOnAt r� I _ I AYOUB ENGINEERING, INC. consultants 421 BENEFIT STREET 401-728-5533 PAWTUCKET, R.I. 02861 Ass _ ESSORS N0. TOWN OF BARNSTABLE PARCEL NO PAN I UNDERGROUND FUEL AND CHEMICAL STORAGE S1N ' NAME ! U6 ' �� ��{�G(/ 1 C/W. wzp !/ff ADDRESS /Q � �/�Gdl9�/��/ f VILLAGE LOCATION OF TANKS: CAPACITY: TYPE OF FUEL AGE: TYPE: OR CHEMICAL (Give same information for any additional tanks on reverse side of card) DATE OF PURCHASE OF EACH: 1. 2. 3. 4. DATE OF FIRE DEPARTMENT PERMIT: TESTING CERTIFICATION SUBMITTED: PASSED DID NOT PASS �t:� EJAN' (1'3 ��88I -^ -�� ,,. ! TOWr? Or ARNS 1 TABLE 1 y UND .RGR:' UND FUEL AND- CHEMICAL STORAGE SYSTEMS t NAME F ADDRESS VIL,LAGE 1 LOCATION OF TANKS: CAPACITY: TYPE OF FUEL AGE: TYPE: OR CHEMICAL za/ p (Gii6 uame-information for any additional tanks on reverse side of card) DATE OF PURCHASE OF EACH: 1. _ ���5 2. _3' — 3. � G; 4. S DATE OF FPRE DEPAMTMENT PERMIT: TESTING CERTIFICATION SMAITTED: - PASSED DID NOT PASS 13 S 60 �P - e' ! _ - � - r F .n t t '.L S f ;+ y'y ..J <. ,X rv. '•rM _ r ' August .14 r 1980 f -fir .. �? .t..t r Y•.k r :'w ,�._ {♦ nY� - ,�� f Y C •w. -- _ .. x . w ' • as .5„. . N, Maria r ger tlant c R' ohfield Sery ;ce Station 590 ,Iyanugh=Rd . , Hyannis,,-Ma n` x s 'r ,?'. .a •.€.w •- .gin- Dear Sri The"information;;you'-.returned``toa.usj indicated' the +age of f ive of your Andergio_und, fuel. tanks .'as ,being. fifteen years.",-. Yff You must.,have these tanks •.tested, using :the Kei�t-Moore;Y-Pressure 9'Tby,November..2'4, 19�0. Please, ubm3.'t testing results and', their interpretation to this;offatce-;prio�rto November;20, 198q., For your convenience, w�=have enclosed a list�.ng :of :companies L' .who perform:'thi s testing. Yr�u- maf;also utilize 'any other con-' D" 'cern6 qualified to perfprm this test tng.Y ` very. truly yours f f , , John M4: Kelly: ; Director�,,of Public: Health f Opel* �;'r-, .,+ t , d.tr ,y .. ° J, • r 'r n .. a is ; ,v, _ • °' - .. _ ,.. + - A ARCO Petroleum Products Company 5794 Widewaters Parkway Mailing Address:Box 603 `® Dewitt,New York 13214 Telephone 315 424 1711 March 10, 1982 Mr. John M. Kelly Director of Public Health Town of Barnstable Office of Board of Health 367 Main Street Hyannis, Mass. 02601 RE: Underground Storage Tanks 590 Iyanough Road Hyannis, Mass. Dear Mr. Kelly: Per your request, please find the attached test results for tanks tested at the subject location on January 6, 1981 by Protanic Corporation. Very truly yours, R. ?D. J q Auo* Administrator R. E. & C&M RDJ/nm Attachments CC: V. J. DeLaurentis D. W. Pagel ARCO Petroleum Products Company is a Division of Atlantic Richfield Company - PRO TAN6C PROFESSIONAL. TANK INVESTIGATION ' CORP. P.O. BOX 17591 MILWAUKEE, WISCONSIN 53217 • PHONE WISCONSIN (414)332-9422 332-0494 January 15, 1981 •, k 'n F= Mr. A.J. Sidla k Engineer.. Atlantic Richfield Company Box A « . Providence, R.I. 02901T. v Re: Tank System Test, January 6, `1981 Route 13 2 Hyannis, MA. Dear Mr. Sidla: The tank systems tested at this location are identified as follows . Tank System # 1 North 6, 000, gallon Arco Unleaded gasoline. Tank System. # 2 Middle 5, 000 gallon Arco Regular gasoline. LL . Tank System # 3 South 5, 000 gallon Arco Regular gasoline. (Tank Systems # 2 & 3 are manifolded) The National Fire Protection Association' s criteria for a tight tank system is a system with a rate of leak less than . 050 gal/hr. These are calculated, mathematical tolerances only and are not meant to indicate the permission of any leak. Tank System # 1 showed a rate of leak of -. 005 gal/hr. Tank System : # 1 is tight. Manifolded Tank Systems #. 2 & 3 .showed a. rate of leak of +. 043 gal/hr. Manifolded Tank Systems # 2 & 3 are tight. " MEMBER '9 W - - - m r- z �- ��fUM EQUIPMENT INS\ o y • PROTANIC PROFESSIONAL TANK INVESTIGATION CORP. P.O. BOX 17591 MILWAUKEE, WISCONSIN 53217 PHONE WISCONSIN (414)332-9422 332-0494 January 15, 1981 Mr. A.J. Sidla ; _ r Page 2 All product lines were tested and found to be tight. Prior to testing, the-tank bottoms were checked .for water through -the fill pipes, no- measurable amount was recorded. S ' cerely, William J. P pora WJP/lmw MEMBER IMAW WMW IL ��EUM EQUIPMENT INS�� I Data Chart for Tank 'System Tightness:. 'est.:(J21103364) �r z USING KENT MOORE CORPORATION TANK TIGHTNESS TESTER MODEL 1000 r '"r r .For Packet 4 PLEA E PRINT Copyright 0 Kent-Moore,Corporation 1977 lr f a of 50 Charts ' Ordf:r J 23396-A 1 -OWNER Property P Y - -, ❑ Name, _ Address Representative T'Talephone Tanks) - Name. _ Address _ 'Representative Telephone - 2.- OPERATOR -'. Name AIX_), � �. � Address -' :Telephone 3.1 REASON FOR7777, JEST i (Explain Fully) 4 WHO REQUESTED Na a Title GojnDany or AflfUatlon Dete TEST AND WHEN Y PQc -,ram- R a Z ; p P A dress ... _ . . -;.Telephone I -77-77' S h r4 5.;: WHO IS PAYING FOR THIS TESTZ Company,Agency or individual Person Authoriz(nq Title Telephone s agling.Address ;_� _ &e.- j. I.. 'ay E• J x. _ ty $tat0 ZI r Attention of _ Order Na. o. .•' -'.Other Instructions - - Aa.i ` Identify by Direction Capacity Brand/Supplier.a Grade , Approx Age Steel/Fiberglass ' 6 •TANK(S) INVOLVED � Rr�fa�Gs�Gf 1 . l�iQlil.F. j- cC�tGj f��2cv` 6, LEHnc�?� ao° Sic.. .i < - ,foco�Yl �C/D ,pto-;::. �EAtry .?o sr�-�C, s z �0 r T C D • --.� /P�'6N7'� `.�//1�„STfr1G- �l�t G.�S) r " cationL Cover Ftlls Vents Slphones Pumps'.;:'. ' ..INSTALLATION �M ,` yE5 /Pc/rlorg ti :: DATA D R,sP "Tf-cQES r oith msl" de driveway. Concrete,Black Too .Size,Titaflll make,Drop f- •� Suction.Remote Rear of station,etc. - ' Earth,ate. --tubes,Remote Fills 'Size,Manifolded 'Which tanks]_. Make it known 8. UNDERGROUND the water over the tank? WATER Depth to'the Water table Yes No f •-f' it di.. ' Tanks to be tilled ` hr Date Arranged by 9 .-FILL-UP { Name Telephone ARRANGEMENTS Extra product to top off and run TSTT How and who to provide T F Consider N0 Lead r r ,J �F =r ¢ 'Terming!or other contact r f j L for notice or inquiry Company .r. c .:,f.Name Telephone, 10. CONTRACTOR, - MECHANICS; any other contractor involved i ,1 .11.,' OTHER LE 'T,� '7%F! KiV �/ /Gvt/ . //!f ,AC'Jr ✓E' wins �Ii�lEp INFORMATION lJi�G:,B� tr'i�tp .8 ati>Rwa�ot ct+v S OR REMARKS a J Additional information*on any items above.Officials or others to be advised'when testing is in progress or completed.Visitors or observers present during test etc. Tests were made on the above tank systems in accordance with test procedures prescribed for Kent-Moore Tank Systems Tightness' j 12. TEST RESULTS Tester Model 1000 as detailed on attached test charts with results as follows: tv - F ' Tank identification Tight Leakage Indicated Date Tested T M This Is to certify that these tank systems were tested on t te(s)shown.Those I icat as Tig meet the criteria established by l 13. CERTIFICATION the National Fire Protection Asoclation Pamphlet 329 ' Data mg o tracf t dr Co P y �y�_ Sign s. �Ia N b la,Lt.. // ttIt Serial No.of Thermal Technicians Address rj Sensor t 3, 14 �C/. �E vES ' p-do ''Rl. /32 i�/ ,q v vie. ,. ��S {r ..o/% 4 i Name of Supplier,Owner or Dealer - - Address No.and Streets) - % city•:'i" State,*•' pate of Test 6...V�....1j,I.�.�,,..Ir.,,.,*-.,-..''.II...1,..�.4I-,��;.­..'�.�,!..,-I,.�I..�.�:"i.;.,,I,:,'1,*.1..,1.,.:..,�I,!i..,:,T.��,,�-.-,".,1,..,�,`.,­�-,.­...4:-;-I1,�II-"�-I�;'�,.`,,��,`­",",-I.,I.-7.1-_,­­�%.,.�.�I..1;,(,1 1,',;;;I.�-�_'4,-.�,..,.�..;-�.�;",,I,�;,,..,.,,-..�,�,�.v,,V I"..,,I....-.,..I..-I,�;,',,�'.,,,.,,:,_.�1.;'.1..­"j.,,.I.�.,,.:1,-,"..I..,,,.',...-t­—.:,,-.,.­,.�,,,.."­,,;!,.,��.,�".:_1..,I'..1�-,,1c­;..1!.,,,.,­.�.��:.-I I...',A Z"....�i:��'.',:r_-11,,,-1I�1.,�."I"l.�.1,�;1 I�_,,:�.I-,!�",-.,,,:-;I-,;.-,:I':�,i*-,,.�,,.:!�..1�­.:�,:1�.�,;,..1-..r;..,";.:�'-,....1.,�,1-—�:.,,,;W::-1_�1.I,,'z;�.,,,,.,.,��.1,,.I.�.-.1.­".,.�,,�.._I-�,,-.,',,I..,.,.,.,1 I." 15.: TANK TO TEST 16 CAPACITY k FromY ` } t r ' / t �t Station Chat- . „ : ,, i, By most accurate . ,.< ,`., i; ;,+„i,:: " �✓�`92 T-W Nominal Capacity o, capacity chart available' '� D Tank Manufacturer s Chart - g Idemity by position' Gallons :Gallons r '';' t+. ❑J Company Engineering Data ,`) .+tit ti ..° AAO'' N Is there doubt as to Trua Ca acity 7!. I. r } 7 Y L ❑ Charts suppllad with TSTT •, `i is , � , (/cL: RE�T. �.EY�D 6 Q. i-f' ,! r Brand and Grade x ., See Section"'DE ERMINING�TANK CAPACITY y r '�°, T x u a ❑ Other r F r-t T p d t .{Y: is f t, .:? + i, i •.a '', i r 'Stick Readin S ' r,r,. 1 7: FILL UP FOR TEST g sa, r Total Gallons. q<. a Y t {,, r ? Mu K d�iy ci s t �' to A in ,' Gallons ^. ea.Readin , /� r _ `i ; r! , i 0 \� P � 1 �? i. .w.r y a'. $� g 'it: .;F'.._. i a',. Stick Water Bottom 7 t 0 .' rd r.::, = Y + I ' y�: t sr'�`a' A,. i'• l Mp,:t s 'ram F 3 _ .+- <z: .1, ;� .+,, �'y,.J ,0 .t a before Fill-up O J5/a�iE' '3 c,:rs :.,w:�� Inventory`' ar - �C ��D /Y ;, 1— t to Y.in Gallons. n rt r, i i . , *k-, a + n. P a t,%,` t 1 .y ,e i1 t a.1r s.:S+r w .l,;. n :yt. ,a, _r a G o i.e F e a f;, r :: :1 t ,t _ �.1. , ,;. O �;. x. ..:, , .. r :;r." z., t .i u r ._,,I, g ;.,..:, .. "r.t O Fill up.STICK'.BEFORE AND;AFTER EACH COMPARTMENT DROP OR EACH METERED DELIVERY QUANTITY �„ is '� c i. s {'. a. r. r yF" I t}a..4 t �� SF 'f -:" e; '^ ., VJ�. .,,{. •: ..,t t. .'. ^. ... , a l..t.,4 4 S ,J tJ ;:Sk,: ,yt;.h tJ P. :,.� .., t.,:... .. :. r f , rt W 'a + vp� r, ,r Tank Diameter' i Product in full tank(up to fill pipe) O O R t Z . _ — �A 1—ED`°-`cj•E:" �i�1F 'o�lj`j/UGr- ; i'1 t. ,` 18. : SPECIAL CONDITIONS AND PROCEDURES TO TEST THIS TANK �. _i VAPOR RECOVERY SYSTEM - N. 4;i 4 7 r e-ry ,, t d is .{ s.a r 3 `. p ! ,t rD S l 1 ! a• `,,r :. „ ° : See manual sections a licable.Check slow and record procedure in l0 26) ,t , s: ,, :` o a c Y PP P 9( « t a a i Y d k R s stage I u "A m "! k y- ! ~. nn .+ a Water in flank High water table in tank excavation ?, Line(s)being tested with LVLLT `Stage 11 ,{t .,, , ^. win ,..: : `.:. ��r:r'V J D - URENOLUME FACTOR (a)TO -TEST THIS TANK '$ ,; 21 TEMPERAT . , ;: . "x:'.', i 19. STANK MEASUREMENTS FOR ' , ;' r ° on Truk °F x (-:'' IS Today Warmer. p Colder. ❑_ F 'Product m Tank' __ F FFiI up Product c E pected Change( +or o :TSTT ASSEMBLY { .i ,Zy ... t! ; ! ti , li - O t .! Bottom of tank to Grades ��T n _ r.. (� m r "° 22 Thermal-Sensor reading after circulation. F s m ;a '•t ^Add 30"for 4 L " digts Nearest f� x �+,� ry m Add 24"for 3"L or air seal " 23 �_6 / 2 Digits per°F in range of expected change t digits i. — .•t Total tubing to assemble Approximate It r v A 24 49QA x::. '.t2 �t J'.,d �G �Z gallons i, 20 '. EXTENSION HOSE SETTING t ,✓ a ,, c3 a i — .. _ _ 4 '.. r,_' total quantity in x coefficient of expansion for volume change in this tank'. „ d ' m; v i Tank top to glade• �� x;;-full tank(16 or 17) •` ,° r" ', involved product' ,r per F 4 ,: + :�,}�b L i'.Y T1 45- {.. �;:,4 lei .):• wt &w, ,r,0 1. a:., i.:w:3..•,a. •„ Extend hose on suction tube 6 or more !.c I "1 a SrF = 4' C, O 33, : , (,,, ,�iY , >_C, t _ , -v'_5 t•• i r. ,� S-t.-, {.. 3 .t :,? ; F '+r v .,.... G 7 .r4` �,Jf�, }' ,r/ '•II ,,,: -�/ / 'F q !f rv.,41- /' > ? ,. } j below tank top :;. ...... .?. 54 25 - 0 �(O�� {• } / �.y�/. J J Thlt:i s r s k 4 t' volume change per°F(24) Digits per°F in test `.,`,p Volume change per digit °r- 'test . ' 'If Fill i e extends above rade,use to of fill '�'„ Ran a 23 ":-r Com ute to 4 decimal laces ?'factor a :,: P P g P w„ .: t: :; 9 P HYDROSTATIC 31.. 34. - 38.NET VOLUME 39.' 26 30 PERATURE COMPENSATION ACCUMULATED. ,;= r,:I.1 LOG OF TEST PROCEDURES• ;, PRESSURE:_ VOLUME MEASUREMENTS(Yi K TEM CHANGES . . :,a..,.; ,- .. .'y` , al ,' EACH READING CONTROL:. RECORD TO 001 GAL USE FACTOR( :.CHANGE 1 2] . '.:.' 28. -'t= -• 'a;' ,'- ,'•r 29. Standpipe Level 32:,: tHighL record 35;` 36, 3] ; Temperature A stet t Product m •:+• Product , '' c in Inches Change Computation 4, Adjustment Total End Deflection +' DATES {; Record details of Seltjng Up RmdinQ " " Graduate Replaced(—i)7 Thermal ., Higher+. (c) x'(a)= Volume Minus ;.and running test.(Use full No. Be mnin level to Sensor Lower— Expansion+ At low Level compute a D 0 Expansion(+)or TIME length Of hne if needed.) \ of which " Relore Altor Product Heading (c) Conirachon Contraction(—) Change per Hour t2/dr5. _ '" Heading Restored Reading i Reading flec lusted(+)� 133(V)—iy37(T) (HFPA crHeru) . { i , F i; ,,, 3 .. i, e ,. :. { s 9.-e'.:- ,.:..� .. -.,, -.1 b ^7s, P.".1� 'fit. !''r ....,•A ,.-.:.. Qa,.4 ..>..,':'.,:.. :;3 {' 1 L F v !r7$to- t W,y ,t Y . , t .t�. I ,) N ,.. ,/ '/�/ .TEST /f//_�7��Qc%� . 41' ` . ' //J1 ' . a .- -- y 14 1 ; 'f• )t �f wo- f O'/� .1 7, 41 v , op .v.� ��//)�l1LG .C.DELI s✓ /vS - ' �-b fv/L ,q7-� " 'C o ' �o .r .� ,q G�, ice- t w;„ ST C�7 `o C Si G A pv t�",SlG GG�.. ,v =P�. 1' :• .r...a. -, ... 5 yn. .: -: .. .. �i. }. n+ tR�t. s''. JM'..i 4' 1.,. `> .Ya •..•s r _ .l'. Irk k:,, ..,x t.A mot." .P. 1- ,;'1). J„' we>r. ,,5., .,)::4+,R•. .q.. '+ r' i ..¢J :h,. i. y.' ti•�t.. 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C �. .'r^ .!. w Y:, 1��'," .P' d :v_-..[. .� )f;. 7' .<7" n- r 3 :.F-. i Cai A :..r. ,, 5 ... ;,. . ., , ,t' 1. 14 ��.. /(�CYE�' A � — GC',t /3Z �l%9is�i(//J �J.�S t r ," .t Name of Supplier,Owner or Dealer Address No.and Str et(s), 4 " . Slate Date of Test '�". 15 ;TANK TO TEST J 16. CAPACITY 'r'� r, . From o , 'z y r. c 4 a _ V, k L' t 7 r ( , ..t, t f.. '; v' °a &-i. Chart ; y..ai. :r ,r' �: " t BY most accurate s 'i ,r try �T T :7 Tank Manufacturei s hart +, G o Nominal Capacity �400 ,r j< capacity chart available "'' - 0 G r „ IdantltY by position a 'Gallons Gallon '.::X a h'r F`i c ,' I. r! t •1 X v. L1 '1 Mh / + I'. 1+ a '� ^ Coin an En Lr.! r..v.t3.. r;r P ineeri +s: A r k.r. .J•,:,.flx •e .,;'Mrs !a Y 0 ng Date :��. sj �. S ,. 7gL D ,r a Is there doubt as to True Capacity], sa '�y r x }„ x ,F x,`+ E r ;.:�:; l S,�tf r)7 �d• �t b. /CE �/�/�aQ 4srs,,A I.,.. i a i , ,i Ys ❑ 'Charts supplied with TSTT � a J�-t . t% Brand and Grade - , See Section"DETERMINING TANK CAPACITY, �N zv 4 E k' G ii'+ �w. r 'r ,-'yF•,x� .. t r a ¢ a" , k .i. .a r' � SL s .1;,' ,LJ. vt f.v;R n,-,r + i . , s' o- LS z Othe► t, 5d c , 17 FILL FOR E u ��. Stick Ras in s` 'm T ST r t . ___a i,, XY: . -.a,h ,. ^ -:,t} a y � k, ' 3 ' £�,,T G. {fj< g ;N : 4 c t,Total Gallons 4. "7 �• r �.. :r •.etS .F. :4 ,:t., `? .r T .zCM r;:s.e , ..'di .,,s.', k.. : ..t !,.: ,E r). .,t, ,,,t 3s,,, tee: ;in f ..N<, {4 '.t0 I t :z,i l';• L r. -is " P. } s, aL ,v i:, K n ,� y Gallons . , f..}` , a ,t„ ea.ReadIn so-CD k : t t, a i k, g s,,7 v i tr I b' `i J .r.. .... } Stick Water Bottom nr 4 , «,r ,c, ."., /s , N y: i. . -Y 1 r rl L O k." �'.'u^i,..l-a>. [ y -� t ,r t.,_, :•C frr+ , ! :rj L:,';' '�' before FIIf-u f� /YC/E/Le .,, 7:t TM r + "� 3 ,.f,,; 1 ar-e.' P s.ftc. .,ta�.:,t�.,, r s:. f4. ^. F}s,t}c,: Y .fs AInventory y ` ,.4_, n'^'•�M„ f,,..+r r ,t: -�t�- z,'tt r it .;�:' t to% In. G ?, „' r. W Y to- ,. r a r,,- :; x., -:.,.,.:. ',•^ c' .:,.:; .':o• ?..1. fit '`1 a, T f. Y' J a r,:,s r .,,! s �'.,.A: -d''. J y <. t- ':j xtj ': .r d ,�:l,,., t 'f" i k..:a f' V } '`f +,i. 4I`r d- 0 ...,:''. x'`.r ..: ,w, k••3•x% ra -,7,i. �'?' t Ar, .at K w .i:,.y�;.. 0 .- T YL .. r. ..i.%'�`):.. . 1 a 4 u -Y 1 ',.lk t, .i'b} r _-r .,:n _�$' '' :}!:�''s., . C O FIII up.STICK BEFORE AND`'AFTER EACH COMPARTMENT DROP OR EACH'METERED'DELIVERY QUANTITI! ` ;1 ;',; ,ix' t ,, c , ♦ :, .w,t ... .., S '' a, T' 1 4 M r� .,A. p J L'D d s, ,._ rr v „::r, d +.` "? .I r F': 1. 5. •,#:. �- T � „f n.J t. j h,,, f 11:"r��lA 1�/�:!.. J\ l �:F1 .:..: (n ,,:�,, �:.••, , >: ..., ,:.,, i;. .7 is I :� '� f -/L" •��`%ri, )/.9> 1�,1:..J'. :: ° f�'. r :-':' ''F' ,�: ,.e§u .y. r ,4' ,o ':r t is r .:ar C :.:.. ,. .,,.:r.. :, ..:.• .'.o.. .-.:,.. -" ,; +.., t ay, J'h�u ..r-y�:l f +•.- ,,:.Y i-, x�+b� a.. :, ,} ..:i,- k. 1 r' - ! 5 �,.`.�a ;Y ..�. y �.\ !, �� 3 4"h r, ••lf- Tank Diameter : ,r 4 „rf..,. i E i - ..,. Z " . ` � (up t I PIPE) ;1 , ,` ' %a '< /_y T� O ! ;S�A�FoG -Product In full tank o ill �W „ a °L 4 r , : t:' e 7 r i. 18. SPECIAL CONDITIONS AND PROCEDURES TO TEST : ; , �` -? Y N :1 I THIS TANK h VAPOR x > , ;,rx ,71 "r -` RE a,! i' � COVERY SYSTEM , L •, . v, j. t „,:. m '' See manual'sections applicable.Check below and►ecord procedure in tog(26) - a , ' , a ; - ,'.; �s. ,� ,-..t _:r 7' , r ", F.� -F ,st' r. < stage I , _,.^;. .l. ..,. ,'r' - l �y ah a , — Water in tankHlgh water table in tank excavation �Llne(s)tieing tested with LVLLT Stage II s ^ ' m ; r ti sv r d m , D 21..;.TEMPERATURE/VOLUME FACTOR a1 TO TEST;.THIS.TANK ti " A n -r:y i. �. a.,. • *fir �y1 f 'i, ;; :19. TANK MEASUREMENTS FOR , .,. s oa .; ,' v.:. cn a ,;,, _, Is Today Warmer?O Colder?0 •F Product in Tank_ F Fill up Product on Truck_,F Expected Chan e + or oX '4 .t, TSTT:�ASSEMBLY :; , ( )y �., = d;:,�,' o ° r�. G� Botfom of tank to Grade* /� 'r' m m 22 Thermal-Sensor reading after circulatiop, a 3 7 / 3 i," - Add 30"for 4 L " digits Nearest. ( {{ "r x r r g '��` r ': W m Add 24"for 3"L or air seal .', Digits per•F In range of expected change a ` „ .:.. - digits: t + W 3 Total tubing to assemble Approximate V= i i�� /, ' F f K t: a 24 arcs" X . D,ADd 6 3. 2 3 S/vr" on " 20. EXTENSION HOSE SETTING + 3 T gallons s a j 3tS�"x` ::- w .-a :,total quantity in f • , -.., ^` !coefticlent of expansion for n.� ,volume change In this tank., a ;,- •'.� in Tank top to grade' s t y ;' M t. , „ k(1 7) t ,zs s involved product t e a h:full tan r al< � ..r r. hrr' 'P rr. zc, 6or1 +t•'tfe Extend hose on suction tube 6 or m r a:: ,•.. a .rr .a t� a r 'w a :es d h- i ,e; '• + .(• {�,.,i r9'J Y ,. ..� �e ;.7. � I ,r,,..•. l} t 1'i. '..{e9. ':1' 1 -� .:<r y:,:t f S r a� V,/Y '/�� rf x a�yu:. .. ,.{ ... '•.,. ... ":: ,. -:",�:.,..-., kip. .\l. •9 .: ) rr.', I c ss r. 'below tank to ..-.. ... , .`u ,I,i t .r r x- Sir ciz: r I :, r P 25 3. 23 �,% � �• t r -:=2 D;6//ooi9 l4 , +! + R > ` � •"' !$'.:volume thane er"F 24 2 r b' Di its r"F to`t t .,e_ y This is'f s' . ;. 9 P ( ). „ 9 Pe in s t r, Volume change per diglL :r test p r 4: . 'If Fill pipe extends above grade,use top of fill+ i �o .`, , „.j _-. Range(23) Compute to 4 decimal places factor(a) s 26 ,. .. ,,.: . . 30 ,; HrDI)Dsranc'r, 31.. 34.: 3 .. .. YOWME MEASUREMEIIfS m t TEMPERATURE COMPENSATION $•NET VOLUME 39, t LOG OF TEST PROCEDURES PRESSURE'+ �.::. p CHANGE ACCUMULATED v 3`, :.CONTROL :' L :':', SE FACTOR!A)­ ,, a) h.,. • a RECORD TO ODI GA i r ; U CHANGE , . . ,.,-+ EACH HEADING , ,i .:" 27 ,, 28 ,:,. r; a -• 29. Standpipe Level .?ir ,Temperature,' A 32 Product m '. Product 35 3B 37 At Nigh Laval WWI! 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