Loading...
HomeMy WebLinkAbout0242 MAIN STREET (HYANNIS) - HAZMAT wa main S�rcr�- , N+�n nns fl= �a� 15g la vi2 m Wr 7 N � z �� F.P. 292 d „ Ijc ( olltnuntiv�tt(tIj of �sutljus>:ffs y� Department of Public Safety—Division of Fire Prevention APPLICATION FOR PERMIT FOR REMOVAL AND TRANSPORTATION TO APPROVED TANK YARD �3 . Q . 19 75 fA--- c.ez 1,40 M,G.L. To: HEAD OF FIRE DEPARTMENT Oil DIG SAFE NUMBER Nu an n I;n � I Stort Dote IZ zg $ In accordance with the provisions of Chapter 148, G.L. as provided in Section 38A Application is hereby made by__TnHzDI - ;4 F (_--h Q n Name of Person, irm or orpora ion) Address For permission to remove and transport underground steel storage tank(s) from Street address ci y or town FDID# OI qzz to approved Tank Yard# (,U • P,�)r+ n Il Oo0 State clearly type of inert gas used in df-q C.P 1 Z —steel Str_.rane tank f == �(J� -Ty—e o i�er7.�• y as use„ Name of Person, Firm, Corporation disposing tank___ (o- i n,7s+. Date issued - rejected Iz ZS 191 8" By:4��&,9� - 7 Date of expiration 1 196-0aid/due ignatU _Applicant - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - Vie Commontoeattb of Jmngacbu�ettg DEPARTMENT OF PUBLIC SAFETY—DIVISION OF FIRE PREVENTION P EIR R M IT FOR REMOVAL AND TRANSPORTATION TO APPROVED TANK YARD C.82 S.40 M.G.L. DIG SAFE NUMBER In accordance with the provisions of Chapter 148, G.L. as provided in 9'g39_f� � Section 38A this permit is granted to Start Data z Name: (Q1d I' Can rUc,+->oIn Full name of person, firm or Corporation To transport underground steel storage tank(s) State clearly type of to Approved tank yard# a(--h n -3�lei inert gas used in steel storage tank steel tank: 0eor)e� methodZ�Z F la,n I FDID# O I Name and address of contractor — — — disposing tankP�r{ Fee paid $ 10 — Location to whicCiLank—Will be transported oil pp ove tans yar This permit will expire „p- Prev.en+,o,1 Cit , ignature OTTICI&J granting g permit(TITLE) �, (Head of Fire Dept.) J TOWN ' OF BARNSTABLE COMPLIANCE: CLASS: 1. Marine,Gas Stations,REpair Q satisfactory 2. Printers tTM. R D OF HEALTH 3. panu actu Shops / Q unsatisfactory- 4. Manufacturers �� � � � . (see"Orders") 5. Retail Stores COMPANY 6. Fuel Suppliers d i • ADDRESS /,. M-Ah r FV Class.s 7. Miscellaneous QUANI•ITIES AND STORAGE (IN-Indoors; OUT=outdoor MAJOR MATERIALS- Case - lots Drums AbOveTanks , Undetgrohnd Tanks INOUT -aItons A¢e Ew Fuels: • Gasoline, Jet Fuel (A) Diesel, Kerosene, 02 (D) , Heavy Oils: r' waste motor oil - (C) new motor oil (C) transmission/hydraulic Synthet�.c Organics: degreasers • ~ •Miscellaneous: e r,,j 1,e fA L �JN T SPA Y S Xk U ISPOSAL RECL M T ON REMUS: 1. Sanitary Sewage 2. Water Supply �/ M �- � �� I �� ®Public UA 11 6 1 !5 nS _.?t`�" (�,1�1 0,Town Sewer .,� _ �/. Q On-site Q Private / ,F~�'� ( l,? � 1 �/ �, 3. Indoor Floor Drains: YES NO P —Z _ 0 �— Holding tank: MDC Catch basin/Dry well �ORDER -'""�+'.'~_•_ �..__ s__ ......._....__.__..�__ Q On-site system 1A) /Z 4. Outdoor Surface drains-,YES NO L11 �r .• "' Q HoldinL tank: MDC Z-A ��/ 61n) f Q Catch basin/Dry well Q On-site system r��� G• / � ,� � -_ S. Waste Transporter v ° Licensed? lljjm"f llau1rr_ •,pPstinatlnn taste Product. DES NO ffy ei erson s Int6rviewe - Inspector Date j TOXIC AND HAZARDOUS MATERIALS REGISTRATION FORM NAME OF FIRM: /Jt4 S t- IS MAILING ADDRESS: �""� S f .t�BM��� TELEPHONE NUMBER: 01-f S' 9 9 CONTACT PERSON: Does your firm store any of the toxic or hazardous -materials listed--below-,, either for sale or for your own use, in quantities totalling, at any time, more than 50 gallons liquid volume or 25 pounds dry weight? YES P— NO This form must- be returned to the Board of Health regardless of a YES or NO answer. Use the enclosed envelope for your convenience. If you answered YES above, please indicate if the materials are stored at a site other than your mailing address : ADDRESS: TELEPHONE: LIST OF TOXIC AND HAZARDOUS .MATERIALS The Board of Health has determined that the following products exhibit toxic or hazardous characteristics and must be registered when stored in quantities totalling more than 50 gallons liquid volume or 25 pounds dry weight. Please put a check beside each product that you store: ✓ Antifreeze (for gasline or coolant systems) Refrigerants Automatic transmission fluid Pesticides (insecticides, Engine and Radiator flushes herbicides,rodenticides) Hydraulic fluid (including brake fluid) Photochemicals Motor oils/waste oils Printing Ink Gasoline, Jet fuel Wood preservatives Diesel fuel, Kerosene, #2 heating oil (creosote) Other petroleum products: grease, Swimming Pool chlorine lubricants Lye or caustic soda Degreasers for engines and metal Jewelry cleaners { Degreasers for driveways & garages Leather dyes Battery acid (electrolyte) Fertilizers (if stored Rustproofers outdoors) Car wash detergents PCB' s Car waxes and polishes Other chlorinated hydro- Asphalt & roofing tar carbons, (inc.carbon Paints, varnishes, stains, dyes tetrachloride) Paint and lacquer thinners ' Any other products with Paint & Varnish removers, deglossers "Poison" labels (including Paint brush cleaners chloroform, formaldehyde, Floor & Furniture strippers hydrochloric acid, other Metal polishes acids) Laundry soil & stain removers Other products not listed (including bleach) Spot removers & cleaning fluid � which you feel may be s toxic or hazardous please (dry cleaners) list.: Other cleaning solvents RECEIVE ® . Bug and tar removers HEALTH DEPT. Household cleansers, oven clef(hA&QF BARNSTABLE Drain cleaners Toilet cleaners Cesspool ..cleaners Disinfectants $ 1981 Road Salt (Halite) MAY 1 1 DataMap Technology Corporation 1 1 Environmental FirstSearclim Report 1 TARGET PROPERTY: 1 242 MAIN ST 1 HYANNIS MA 02601 1 Job Number: 5768.00 1 1 PREPARED FOR: 1 Atlantic Environmental Technologies, Inc. 86 Faunce Corner Road, Suite 410 1 North Dartmouth, MA 02747 1 1 07-11-00 ' tnv llUIIirICLl:/ FIRST 1 Tel. (781) 320-3720 Fax: (781) 320-3715 1 Environmrnmi FirstSca ch is a registered trademark of DamMap Technology Corporation.All rights reserved. Environmental Firsdeareh tSearch Summary Report ' Target Site: 242 MAIN ST HYANNIS MA 02601 FirstSearch Summary ' Database Sel Updated Radius Site 1/8 1/4 1/2 1/2> ZIP TOTALS NPL N 01-19-00 1.00 _ CERCLIS N 04-16-00 0.50 RCRATSD N 10-18-99 0.50 RCRA COR N 10-18-99 1.00 RCRA GEN N 10-18-99 0.25 RCRA NLR N 10-I8-99 0.25 ERNS N 01-06-00 0.25 NPDES N 10-18-99 0.25 ' FINDS N 09-21-99 0.25 TRIS N 07-16-98 0.25 State Sites N 05-10-00 1.00 Spills-1990 N 06-09- 1,11 Spills-1980 N 03-10-98 98 0.2525 SWL N 12-07-99 0.50 Permits N NA 0.25 ' Other N NA 0.25 REG UST/AST N 03-29-00 0.25 Leakin¢UST N NA 0.50 - - State Wells Y 12-02-99 0.50 0 1 0 0 _ 0 I Aquifers Y 01-20-99 0.50 2 0 0 1 0 3 ACEC N 01-20-99 0.50 Wetlands N 12-31-99 0.50 Flooditlains N 09-01-96 0.50 Receptors Y 01-01-95 0.50 0 0 0 0 0 0 Nuclear Permits N 04-30-99 0.50 - - _ _ Historic/landmark N 09-01-99 0.50 ' Federal Land Use N 06-17-98 0.50 Federal Wells N NA 0.50 Releases(Air/Water) N NA 0.25 ' TOTALS- 2 1 0 1 0 0 4 Notice of Disclaimer Due to the limitations,constraints,inacc acies and incompleteness of government information and computer mapping data currently available to DataMap Technology Corp.,o"in conventions have been utilized in preparing the locations of all feddal,slate and local agency sites ' residing in DataMap Technology Corp.'s databascs.All EPA NPL and state landfill sites are depicted by a rectangle approximating their location and size.The boundaries of the rectangles represent the eastern and western most longitudes;the northern end southern most latitudes.As such, the mapped areas may exceed the actual Arco and do not represent the actual boundaries of these properties.All other sites Are depicted by a Point representing their Approximate address location and make no attempt to represent the actual arras of the Associated property. Actual ' boundaries and locations of individual properties can be found in the files residing at the agency responsible for such information, Waiver of Liabili Although DataMap Technology Corp.uses its best efforts to research the actual location of each site,DeteMop Technology Corp.don not and an tot warrant the accuracy of dame sites with regard to met location and size.All Authorized users of DataMap Technology Corp.'s services proezcding Are signifying an undastsnding of DaW&p Technology Corp.'o sarching and mapping conventions,and agree to weive any and all liability chains associated with search and map results showing incomplete and or inaccurate site locations. Environmental FirstSearch Sites Summary Report TARGET SITE: 242 MAIN ST JOB: 5768.00 HYANNIS MA 02601 ' TOTAL: 4 GEOCODED: 4 NON GEOCODED: 0 SELECTED: 4 ID DB Type Site Name/ID/Status Address Dist/D1r Map ID 3 AQUIFER GIPECODSSA 0.00- 3 EPA_SSA-81/EPA DESIC SOLESOUR MA 2 AQUIFER CAPECODSSA ,0.00- 2 SSA-371AIED MA I PRS AU ZONE 11 0.12 NE I ' ZONEII-726 AIA AQUIFER GIPECODSS4 0.38 NW EPA_SSA-821EPA DES1G.SOLESOUR MA t Environmental FirstSearch Site Detail Report ' TARGET SITE: 242 MAIN ST JOB: 5768.00 HYANNIS MA 02601 ' AQUIFER SEARCH ID: 3 DIST/DIR: 0.00— MAP ID: 3 NAME: CAPE COD SSA REV: 0120/99 ADDRESS: IDI: EPA_SSA-81 ' MA ID2: STATUS: EPA DESIG.SOLE SOURCE CONTACT: PHONE: ' AREA IN ACRES: 495802282.392579 PERIMETER: 358299.03796435 tSOURCE CODE: GIs ' AQUIFER SEARCH ID: 2 DIST/DIR: 0.00-- MAP ID: 2 NAME: CAPE COD SSA REV: 0120/99 ADDRESS: IDI: SSA-37 MA H)2: ' STATUS: MED CONTACT: PHONE: AREA: 21482335.13298 ' PERIMETER: 183974.12283 SSA NUMBER: 1 ' Selected Site Details Page- 1 Environmental Firsdearch Site Detail Report TARGET SITE: 242 MAIN ST JOB 5768.00 HYANNIS MA 02601 STATE WELLS SITE SEARCH M: 1 DIST/DIR: 0.12 NE MAP ID: 1 NAME: MAZONEII REV: 12/02/99 ADDRESS: IDI: ZONEII-726 MA ID2: ' STATUS: CONTACT: PHONE: ' AREA: 4190164.5 ' PERIMETER: 10210.79 AREA IN ACRES: 1035.4 NUM ZONES: ' AQUIFER ' SEARCH ID: 4 DIST/DIR: 0.38 NW MAP ID: 4 NAME: CAPE COD SSA REV: 0120/99 ADDRESS: IDI: EPA_SSA-82 MA ID2: STATUS: EPA DESIG.SOLE SOURCE CONTACT: PHONE: ' AREA IN ACRES: 525932047.99005 PERIMETER: 380072.769976172 ' SOURCE CODE: GIS ' Selected Site Details Page-1 Environmental SirstSearch Federal Databases and Sources 1. NPL: National Priority List, The EPA's list of confirmed or ' proposed Superfund sites. Source: Environmental Protection Agency. Updated quarterly. ' 2. CERCLIS: Comprehensive Environmental Response Compensation and Liability Information System. The EPA's database of current and potential Superfund sites currently or previously under investigation. Source: Environmental Protection Agency. Updated.quarterly. 3. RCRIS: Resource Conservation and Recovery Information System. The ' EPA's database of registered hazardous waste generators and treatment, storage and disposal facilities. Included are RAATS (RCRA Administrative Action Tracking System) and CMEL (Compliance Monitoring 6 Enforcement List) . Source: Environmental Protection Agency. ' Updated quarterly. ' q. ERNS: Emergency Response Notification System. The EPA's database of emergency response actions. Source: Environmental Protection Agency. Updated quarterly. ' 5. NPDES: National Pollution Discharge Elimination System. The EPA's database of all permitted facilities receiving and ' discharging effluents. Source: Environmental Protection Agency. Updated semi-annually. 6. FINDS: The Facility Index System, The EPA's Index of identification numbers associated with a property or facility which the EPA has investigated or has been made aware of in conjunction with various regulatory programs. Each record indicates the EPA office that may have files on the site or ' facility. Source: Environmental Protection Agency. Updated semi-annually. ' 7. IRIS: Toxic Release Inventory System. The EPA' s database of all facilities that have had or may be prone to toxic material releases. Source: Environmental Protection Agency. . Updated semi-annually. 1 8. ACEC: Areas of Critical Environmental Concern. This database contains contact information for threatened and endangered Services Offices; State GIS Departments. Updated periodically. 9. 8loodplaine - 100 year and 500 year flood zone boundaries for ' select counties in the United States. Source: Federal Emergency Management Agency (FEMA) . ' This database will be updated by us as new data becomes available for purchase. ' 10. Historic Sites- National Register of Historical Places Database. The nation's official list of cultural resources worthy of preservation. Properties listed include districts, sites, buildings, structures, and objects that are significant in American history, architecture, archeology, engineering, and culture. Source: National Park Service. ' Updated yearly. 11. Wetlands - U.S. Fish and Wildlife Service produces information on the characteristics, extent, and status of the Nation's ' wetlands and deepwater habitats. This data is available for select areas of the United States. Source: U.S. Fish and Wildlife Service, National Wetlands Inventory. This database will be updated by us as new data becomes available for purchase. 12. Land Use - Federal Land data includes information from the following government agencies including Bureau of Indian Affairs, Bureau of Reclamation, Bureau of Land Management, Department of Defense, Forest Service, Fish and Wildlife Service, National Park Service, and the Tennessee Valley Authority. This database also contains data regarding wild and scenic rivers. Source: USGS. Updated periodically. r r ri - q. Ir.......r:: ,.... 1 : ...................... .................\...I................'..........................1 ....... :....:. ..:..:.,....................... 49...................,.n. _........'..:.....................t....l 190,10 ......,__ ,. 1......................1:. ..................i ...:........1........................t1...., u.0 M u.... .I p........................u. \O_..u.u. ...... ....up.....uu.......U...a • :,.... ......\. UU...n\.U...U... ....U.. _.,' r. .U\..r.U.1.U.UU...U.UU.....UU...1 ��.... ..U.11._U__._r........:.•...... ....... .. :..l..... \.....H.. ........I..........U\.\..U...\...1.11.\U.1 ..... ..1\... .,.. ._.. U..U.'.....�.._U..\..1.1.._..,.'..111\......U\....U....U.U.U...1 �w..\......I.U.. 1..1....AL .....r...i..0 IUI...1 ./...1..Y. 1.....•...I....U....\.UU..IU...1...\...1.......:.......I..' ._..I.........1.!.... .I 1.. ..................,.............. .........................\.........1 I..UUI....U...... \,r....r..I. ...,U\II.r.U.l........\.'.\\...-....U.I..'1..'..\..U.UU......U...........U.1 1......- •...\..\....r... ......5..I........I a...... .....\.\.......r.......11..1I..._.......U...U.....\.U..\....I IUU....- ...'.UI1.... ...\..UI.U.1.... ..M N.........-• I..`\Ui....'..U............U.U........UUnext ............_ ....1.'� .'..1\.I.....:..-....U.II...........U,..\...,I......Alan .................._\...\II.......1 1../•.`...I I..Y_. •..i..l.• U....\....I.U.1............U....U....11...U..U..\\...U........��\.......\.1 1.... ..........1.1....I/.U..iNUM0....t....'.U........N"mass..U.1.. \.....UU.0 MUN..U1 V A..w_ ...\UU..I..p!.U.....000aUU U.. ...U.UU..U..U.P.r.1..•.....U.......�...............r.....U,l ......\._. nc........ .\....II,U1.............\...\.'JJ....1,...' \..U............\.U......U.U... '••..\.:::: : a...... ..............U.1::::............\ ..'I.. .....'-\......\.......U........ i..,....................r.... ...\...,......�i.f...... ......:....................\.r.........� .\I u..r o mm.....• • aU..c.... r \....i i.um..'.U.......v.U................ u.A......... n MOMM.J:u is:::uU.U.U.U:ilnuu uU.UU...'-UU U..U.0 memo U ii.t..,uuu:ol uuuuur u.0 uuuuuuuuuu•, ii_�,u..,v....mu....u.1 .lu.l..0 uU....UU.. uu .UU.U.U\...Uao.u.n..,•.�_. .........d-,...vU.a..uuU.a O.I....IUU.000.E 1U..J.......U..O...U'uu.uu....�.UI uU.%L:O.9.U....uU.0 • Uu 16. ;.UUU.(( uu LuuUUU.'u.'..L.Ur....•t.0 Uuu I:4.:i.u. .V\O...00...� �...,IU.:i........f ..Iu....,._.. UL.LU. \IUb..0..� ... Y:. .II\......uu Manama vuuul u:n Sp- �uw:iG:u.•.gp.r.uu •.uu u.un RM u.....•........uu -..:..'lama...I...- 1.................L....\..1...�a.........r.::....r.....,1...:.:....... �- -•...L.....i�L.i...............E........d..\..1.......... ....... .....\..0..�:.U.1 •.I..... ..,.. ..............'.....I..................r.......,...............w..7.. .....:1:.. ..:...................1.........1.........I......t.................. �:-\1...1..................... ........1.................'..•_..I...i ............. ..I........r...................................- /O...ul .i' •\..............,...........a...........................• .i::......_"1 •....:...rl........1....../... 1......1..............�..:.1:.....f .. ........................ ....1.1.....I.......... . ......Mi...:.1 ............ .....• ........1.......'........l ...�..•...::::. ......'..r.........MM r ■� ► r � NPL,Solid Waft Landfill 0 APPENDIX B MAtlantic II 1� 1` 1� Appendix B: 1' Laboratory Analytical (August & September 2000) IE 1 1 1 1 1 1 � 1� 1� 1 O 'w,exO ' GI lO, /NDI-AI `!l Groundwater Analytical,Inc. ANALYTICAL �x,200 228 Main Street Buzzards Bay,MA 02532 1 Telephone(508)759-4441 FAX(508)759-4475 October 4, 2000 1 1 Mr. Eric Cardinal Atlantic Environmental 86 Faunce Corner Rd. ' North Dartmouth, MA 02747 Project: Blaine/5786.01 1 Lab ID: 36344 Sampled: 09-29-00 1 Dear Eric: Enclosed is the Volatile Organics Analysis performed for the above referenced project. This project 1 was processed for Rush turnaround. This letter authorizes the release of the analytical results, and should be considered a part of this 1 report. This report contains a project narrative indicating project changes and non-conformances, a brief description of the Quality Assurance/Quality Control procedures employed by our laboratory, and a statement of our state certifications. 1 I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to 1 the best of my knowledge and belief, accurate and complete. Should you have any questions concerning this report, please do not hesitate to contact me. Sincerely, ' Jonathan R. Sanford President ' JRS/ss Enclosures 1� GROUNDWATER ' ANALYTICAL EPA Method 80216 Halogenated Volatile Organics by GC/ELCD ' Field ID: MW-10 Laboratory ID: 36344-01 Project: Blaine/5786.01 QC Batch ID: VG2-1801-W ' Client: Atlantic Environmental Sampled: 09-29-00 Container: 40mL Glass Vial Received: 09-29-00 Preservation: HCI/Cool Analyzed: 10-02-00 Matrix: Aqueous Dilution Factor: 1 ' CAS Number ! Analyte Concentration Units Reporting Limitl ----- - 75-71-8 DichlorodiFluoromethane BRL ug/L 5 74-87-3 Chloromethane BRL ug/L _ 5 .75-01-4 Vinyl Chloride BRL ug/L 2_-.. .--- - - ---- --- - ---- 74 83-9 _ _Bro_m_ome[hane BRL ug/L 75-00-3 _---- Chloroethane BRL ug/L __ 5 _--75-_69-4- _ - -TrichloroFluoromethane BRL ug/L 1_— 75-35-4 1,1-Dichloroethene BRL ug/L _1 _7_5-09-2 __Methylene Chloride BRL ug/L 1 _ 15660-5 trans-1,2-Dichloroethene 8RL ug/L 1 t 75-34-3 1,1-Dichloroethane BRL ug/L 1 156-59-2 cis-1,2-Dichloroethene BRL ug/L 1 67-66-3 Chloroform 2 ug/L 1 ' 107-06-2 11,2-Dichloroethane BRL i ug/L ! 1 71-55-6 1,1,1-Trichloroethane BRL ug/L 1 SCr23-5 Carbon Tetrachloride j BRL ug/L 1 78-87-5 1,2-Dichloropropane BRL ug/L 1 ! 79-01-6 1 Trichloroethene j BRL j ug/L ! 7 75-27-4 Bromodichloromethane BRL ug/L 1 110.75-8 2-Chloroethyl Vinyl Ether BRL 1 ug/L 5 ' j 10061-01-5 i cis-1,3-Dichloropropene BRL ! ug/L I 1 ! 10061-02-6 trans-1,3-Dichloropropene BRL ug/L 11 1 79-00-5 1,1,2-Trichloroethane BRL ug(L j 1 124A8-1 Dibromochloromethane BRL ug/L 1 ' 127-18-4 Tetrachloroethene I 10 ug/L 1 108-90-7 Chlorobenzene BRI ug/L 1 75-25-2 Bromoform I BRI ug/L I1 ' 79-34-5 1,1,2,2-Tetrachloroethane BRL I ug/L I1 ! 541-73-1 4 1,3-Dichlorobenzene BRL ug/L 1 106-46-7 1,4-Dichlorobenzene BRL ug/L 1 95-50-1 1,2-Dichlorobenzene BRL ! ug/L 1 ' QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethane-d, 102 % 70- 130 % ' Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1.996). Analyte list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. ' Reporting limits are adjusted for sample dilution and sample size. ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL Project Narrative Project: Blaine/5786.01 Lab ID: 36344 Client: Atlantic Environmental Received: 09-29-00 1 i A. Physical Condition of Sample(s) This project was received by the laboratory in satisfactory condition. The sample(s) were received undamaged in appropriate containers with the correct preservation. i B. Project Documentation ' This project was accompanied by satisfactory Chain of Custody documentation, with the following amendment(s) or correction(s): 1 1. Project 36344 was changed from Priority (5 business day)to Rush turnaround. The project was given a due date of 10-04-00, as per Eric Cardinal, 10-03-00. 1 C. Analysis of Sample(s) ' No analytical anomalies or non-conformances were noted by the laboratory during the processing of these sample(s). All data contained within this report are released without qualification. 1 1 1 i� 1� Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER Man Street,P.O.Box 1200 Jw Am Buzzards in Bay,MA 02532 CHAIN-OF-CUSTODY RECORD Telephone(508)759 4441 AND WORK ORDER No 43123 ANALYTICAL FAX(508)759-4475 Project Name: Firm: TURNAROUND ANALYSIS REQUEST 13LA Wre, S.—ijudn earvx. -.1. M,l,l, w eenM catho r, G—.cleOWn 00r ❑ NDARD(1D Business Days) m,m Project Number: Address: t3 L S� lG3—� PRIORITY(5 Business Days) @ x 511�( �AdonkA,0j 1 ❑RUSH(RAN- Sampler (Rush requires Rush Authanzati Numbed Name: City/State/Zip: Please FAX ES ❑NO 3 h € LA'S N.b ncl , tlA a2� ao nn FAX Number:fiT)T-99L Project Manager: Telephone: BILLING x - a v E g ? i e Purchase Order No.: GWA Reference No.: � .� � t d1„1 Sid � ( � ) ➢ INSTRUCTIONS:Use separate line for each container(except replicates). e = Sampling Matrix Type Contalre.R.) Preservation foinw A 9AYPLE ° $ $ " a ' n oyy 3 s $ g u 1 3 ee .. a 3 S 5 LABORATORY EMIRCAnON > 3 4 n & a 5 g NUMBER q 5 s 10 e S a s - $ S (Lab Use Only) s ; d 8 f Dg 3 n o 8 i a p [ i 0 3 E S 5 Y i`• .# a e Y f lLe .3 t1W —tp 3 REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF•CUSTODY RECORD r, n Regulalory Program Project Specific OC NOTE:All samples submitted subject to Standard Terms and Conditions on reverse hereof. k ')I L t~ CU L*,) T• ❑Safe Drinking Water Ad Many regulatory programs and EPA methods require project Reli ofshe b pler: ate Time Received by. 1 Tern nature: ❑MA DEP Form specific CC.Project specific OC includes Sample Duplicates, Y Receipt ❑NPDESIClean Water Ad Matrix Spikes,and/or Matrix Spike Duplicates.Laboratory OC is 9�� Specify State: not protect specific unless prearrangetl.Protect specific OC h f� ?S�'ZI ���C,I�Q,/��� 1 ❑RCRA/Haz.Waste Char. samples are charged on a per sample basis.For wafer samples, ehnquished by: Date Time Recived by: ShippinglAirbill 11.l-v5 r,. ❑MA MCP(310 CUR 40) each MS,MSD and Sample Duplicate requires an additional __ .._ . ..._ . ....._._ _ Number: 0-W `xv-v. d ,� l v�y� j Reportable Concentrations sample aliquot. �:x- O RGGW t El RCS-1 Project SWIfic OC Required eeledbn of OC Sample Relinquished by: Data Time _Receved Dv Laboratgryp Custody Seat/ CGW 2❑RCS 2 OSample Dup&ate ❑Seceded or IaDer Numb Serial ❑MA Dredge Disposal -� Number: O NHO RI E)CT❑ME DMavi.Spike ❑Please use sample: Method of Slipment [.I GWA Courier L l Ex ❑Mavix Sp9m Duplicale press Mail I Federal Express Specify Category: _, ❑UPS r'.Hand f GROUNDWATER ANALYTICAL �i Quality Assurance/Quality Control A. Program Overview Groundwater Analytical conducts an active Quality Assurance program to ensure the production of high quality, valid data. This program closely follows the guidance provided by Interim Guidelines and Specifications for Preparing Quality Assurance Project Plans, US EPA QAMS-005/80 (1980), and Test Methods for Evaluating Solid Waste, US EPA, SW-846, Update 111 (1996). Quality Control protocols include written Standard Operating Procedures (SOPs) developed for each analytical method. SOPS are derived from US EPA methodologies and other. established references. Standards are prepared from commercially obtained reference materials of certified purity, and documented for traceability. ' Quality Assessment protocols for most organic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. All samples, standards, blanks, laboratory control samples, matrix spikes and sample duplicates are spiked with internal standards and surrogate compounds. All instrument sequences begin with an initial calibration r verification standard and a blank; and excepting GC/MS sequences, all sequences close with a continuing calibration standard. GUMS systems are tuned to appropriate ion abundance criteria daily, or for each 12 hour operating period, whichever is more frequent. ' Quality Assessment protocols for most inorganic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. Standard curves are derived from one reagent blank and four concentration levels. Curve validity is verified by standard recoveries within plus or minus ten percent of the curve. ' B. Definitions ' Batches are used as the basic unit for Quality Assessment. A Batch is defined as twenty or fewer samples of the same matrix which are prepared together for the same analysis, using the same lots of reagents and the same techniques or manipulations, all within the same continuum of time, up to but not exceeding 24 hours. ' Laboratory Control Samples are used to assess the accuracy of the analytical method. A Laboratory Control Sample consists of reagent water or sodium sulfate spiked with a group of target analytes representative of the method analytes. Accuracy is defined as the degree of agreement of the measured value with the true or ' expected value. Percent Recoveries for the Laboratory Control Samples are calculated to assess accuracy. Method Blanks are used to assess the level of contamination present in the analytical system. Method Blanks consist of reagent water or an aliquot of sodium sulfate. Method Blanks are taken through all the appropriate ' steps of an analytical method. Sample data reported is not corrected for blank contamination. Surrogate Compounds are used to assess the effectiveness of an analytical method in dealing with each sample matrix. Surrogate Compounds are organic compounds which are similar to the target analytes of interest in chemical behavior, but which are not normally found in environmental samples. Percent Recoveries are calculated for each Surrogate Compound. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 ' GROUNDWATER ANALYTICAL ' Quality Control Report Laboratory Control Sample Category: EPA Method 8012E-Halogenated ' QC Batch ID: VG2-1801-W Matrix: Aqueous Units: ug/L Number Analyte _ ! Spiked Measured Recovery QC Limits 75-35-4 1,1-Dichloroethene _ 5 5 102% 70- 130 % -..--- -- ----- ---- - --- -----_ -.--- -- -- - 11)% .------ 79-01 6 Tnchloroethene _ __ _ 5 5 110% 70- 130 °k _ --- — _ _..._ _ ._.. - --_.- 108-90.7 Chlorobenzene 5 6 QC Surrogate Compound Recovery QC Ltmtts 1,2-Dichloroethane-d4 102 % 70-130 % ' Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition, Update III (1996). Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. A I i 1 �j Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 ' GROUNDWATER ANALYTICAL ' Quality Control Report Method Blank Category: EPA Method 8021 B-Halogenated ' QC Batch ID: VG2-1801-W Matrix: Aqueous CAS Number Analyte Concentration a 'f c w• r 75-718 Dichlorodifluoromethane BRL ug/L 5 -- ----- ----- - - - 7487 3 Chforomethane _ _ BRL ug/L 5 - -- -- - - ---- -75-01-4 Vinyl Chloride BRL ug/L- 2 7483 9 Bromomethane BRL ug/L 5 75-00.3 _ Chloroethane BRL ug/L 5 69-4 TnchlorofluoromeIhane_ BRL _______ug/L 1 ' 75-35-4 _ 1_1-Dichloroethene _BRL _ ug/L 1 _-75-09-2 - -Methylere Chloride_ BRL ug/L 1 l56-60-5 trans-1, BR______u -_2-Dichloroethene B ug/L 1 75-34-3 1,1-Dichloroethane BRL' ug/L 1 156-59-2 cis-1,2-Dichloro— ethene-� BRL I ug/L 1 67-66-3 Chloroform BRL ug/L 1 107-06-2 1,2-Dichloroethane _ BRL ug/L i 1 71-55-6 ! 1,1,1-Trichloroethane_ BRL ! ug/L 1 56-23-5 Carbon Tetrachloride BRL ug/L 1 ~; 78-87-5 1,2-Dichloropropane BRL ug/L 1 79-01.6 Trichloroethene BRL __ ! ug/L _ 1 ' L75274 Bromodichloromethane BRL -F ug/L 1 110-75-8 1 2-Chloroethyl Vinyl Ether I BRL j ug/L 5 10061-01-5 cis-1,3-Dichloropropene T_ BRL ug/L 1 10061�-02-6 '; trans-1,3-Dichloropropene BRL ug/L 1 79-00-5 1,1,2-Trichloroethane I _ BRL ug/L 1 —1 j 12448-1 1 Dibromochloromethane 1 BRL ug/L 1 . j 127-18-4 Tetrachloroethene BRL ug/L 1 j ' 108-90-7 Chlorobenzene BRL ug/L 1 75-25-2 1 Bromoform BRL ug/L 1 j 7.9-34-5 1 1,1,2,2-Tetrachloroethane I BRL ug/L 1 ' 11 541-73-1 1,3-Dichlorobenzene ' BRL ug/L 7 j 106-46-7 1 1,4Dichlorobenzene i BRL ug/L 1 j 95-50-1 1 1,2-Dichlorobenzene BRL ug/L 1 QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethaned4 97 % 70- 130% Method Reference: Test Methods for Evaluating Solid Waste,US EPA, 5W-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution and sample size. 1 Groundwater Analytical, Inc., P.O. Box 1200,228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL ' Certifications and Approvals CONNECTICUT, Department of Health Services, PH-0586 Potable Water,Wastewater/Trade Waste,Sewage/Effluent,and Soil pH,Conductivity,Acidity,Alkalinity,Hardness,Chloride,Fluoride,Ammonia,Kjeldahl Nitrogen,Nitrate,Nitrite,Onhophosphate,Total Dissolved Solids.Cyanide,Aluminum,Antimony,Arsenic,Barium,Beryllium,Cadmium,Total Chromium,Hexavalent Chromium,Cobalt,Copper,Iron,Lead, Magnesium,Manganese,Mercury,Molybdenum,Nickel,Potassium,Selenium,Silver,Sodium,Thallium,Tin,Titanium,Vanadium,Zinc,Purgeable Halocadons,Purgeable Aromatics,Pesticides,PCBs,PCBs in Oil,Ethylene Dibromide.Phenols,Oil and Grease. MAINE, Department of Human Services, MA103 Drinking Water Reciprocal certification in accordance with Massachusetts certification for drinking water analytes. Waste Water Reciprocal certification in accordance with Massachusetts certification for waste water analyles. MASSACHUSETTS, Department of Environmental Protection, M-MA-103 Potable Water Antimony,Arsenic,Barium,Beryllium,Cadmium,Chromium,Copper,Lead,Mercury,Nickel,Selenium,Thallium,Nitrate.N,Nitrite-N,Fluoride, Sodium,Sulfate,Cyanide,Turbidity,Residual Free Chlorine,Calcium,Total Alkalinity,Total Dissolved Solids,pH,Trihalomethanes,Volatile Organic ' Compounds,1,2-Dibromcethane, 1,2-Dibromo-3-chloropropane,Total Coliform,Fecal Coliform,Heterotrophic Plate Count,E-Coli Non-Potable Water Aluminum,Antimony,Arsenic,Beryllium,Cadmium,Chromium,Cobalt,Copper,Iron,Lead,Manganese,Mercury,Molybdenum,Nickel,Selenium, ' Silver,Strontium,Thallium,Titanium,Vanadium,Zinc,pH,Specific Conductance,Total Dissolved Solids,Total Hardness,Calcium,Magnesium, Sodium,Poussium,Total Alkalinity,Chloride,Fluoride,Sulfate,Ammonia-N,Nitrate�N,Kjeldahl-N,Orthophosphate,Total Phosphorus,Chemical Oxygen Demand,Biochemical Oxygen Demand,Total Cyanide,Non-Filterable Residue,Total Residual Chlorine,Oil and Grease,Total Phenolics, Volatile Halocarbons,Volatile Aromatics,Chlordane,Aldrin,Dieldrin,DDD,DDE,DDT,Heptachlor,Heptachlor Epoxide,Polychlorinated Biphenyls(water),Polychlorinated Biphenyls(oil). MICHIGAN, Department of Environmental Quality Drinking Water Trihalomethanes,Regulated and Unregulated Volatile Organic Compounds by EPA Method 524.2;1,2-Dibromcethane,1,2-Dibromc-3- chloropropane by EPA Method 504.1 NEW HAMPSHIRE, Department of Environmental Services, 202798 Drinking Water Metals by Graphite Furnace,Metals by ICP,Mercury,NitriteN,Orthophosphate,Residual Free Chlorine,Turbidity,Total Filterable Residue,Calcium ' Hardness,pH,Alkalinity,Sodium,Sulfate,Tout Cyanide,Insecticides,Herbicitles,Base/Neutrals,Trihalomethanes,Volatile Organics,Vinyl Chloride,DBCP,EDB,Nitrate-N. Wastewater ' Metals by Graphite Furnace,Metals by ICP,Mercury,pH,Specific Conductivity,TDS,Tout Hardness,Calcium,Magnesium,Sodium,Potassium, Total Alkalinity,Chloride,Fluoride,Sulfate,Ammonia-N,Nitrate-N,Orthophosphate,TKN,Total Phosphorus,COD,BOD,Non-Filterable Residue, Oil&Grease,Toul Phenolics,Tout Residual Chlorine,PCBs in Water,PCBs in Oil,Pesticides,Volatile Organics,Total Cyanide. RHODE ISLAND, Department of Health, 54 Surface Water,Air,Wastewater, Potable Water,Sewage Chemistry: Organic and Inorganic 'I Groundwater Analytical, Inc., P.O. Box 1200, 22&Main Street, Buzzards Bay,MA 02532 I� 1 Groundwater Analytical,Inc. GROUNDWATER rI /�'1 G P.O.Box 1200 ANALYTICAL Buz Main Street Buzzards Bay,MA 02532 ' Telephone(508)759-4441 FAX(508)759-4475 September 6, 2000 Mr. Eric Cardinal Atlantic Environmental 15 Hamilton St. New Bedford, MA 02740 Project: Blain Hair School/5786.00 Lab ID: 35562 Sampled: 08-28-00 iDear Eric: Enclosed are the Volatile Organics Analyses performed for the above referenced project. This project was processed for Priority One Week turnaround. This letter authorizes the release of the analytical results, and should be considered a part of this report. This report contains a project narrative indicating project changes and non-conformances, a brief description of the Quality Assurance/Quality Control procedures employed by our laboratory, and a statement of our state certifications. I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Should you have any questions concerning this report, please do not hesitate to contact me. Sincerely, ' Jonathan R. Sanford President JRS/myr Enclosures GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: MW-1 Laboratory ID: 35562-01 Project: Blain Hair School/5786.00 QC Batch ID: VG2-1782-W ' Client: Atlantic Environmental Sampled: 08-28-00 Container: 40mL Glass Vial Received: 08-28-00 Preservation: HCI/Cool Analyzed: 08-30-00 Matrix: Aqueous Dilution Factor. 1 CAS Number '"'"`° ;,Anal to s '`I' "`':'Concentration '- ?'Units Reporting Limit - 75_71_8 Dichlorodifluoromethane _ _BRL_ ug/L 5_ ' 74-87-3 Chloromethane BRL ug/L 5 75-01-4 Vinyl Chloride BRL ug/L 2 74-83-9 Bromomethane BRL ug/L 5 75-00-3 Chloroethane BRL ug/L 5 75.69-4 Trichlorofluoromethane BRL ug/L 1 75-35-4 1 1, Dichloroethene BRL ug/L 1 75-09-2 Methylene Chloride EIRL ug/L 1 156-60-5 trans-1,2-Dichloroethene BRL ug/L 1 75-343 1,1-_Dichloroethane BRL ug/L 1 + 156-59-2 cis-1,2-Dichlo— roethe e 6 ug/L 1 67-66-3 Chloroform BRL ug/L 1 ' 107-06-2 1,2-Dichloroethane _ BRL ug/L i 71-55-6 t,l,l-Trichloroethane BRL _ ug/L 1 56-23-5 Carbon Tetrachloride BRL ug/L 1 _ ' 78-87-5 1,2-D_ichloropropane — _ BRL — _ ug/L 1 79-01-6 Trichloroethene _ 10 ug/L 1 _ 75-27-4 Bromodichloromethane —_ BRL ug/L t 11061-0 2-s-1,3- ethyl Vinyl Ether —BRL — ug/L _i- 10061-01-5 cis-1,3-Dichlororopropene BRL ug/L 1 10067-02-6 trans-_7,3-D_ichloropropene _BRL ug/L 1 79-00-5 1,1,2-Trichloroethane BRL ug/L 1 ' 124 48 1 Dibromochloromethane BRL ug/L 1 127 18-4 _ Tetrachloroethene 2t0 _ _ _ _ug/L 1 108 90 7 Chlorobenzene BRL ug/L t i-75 25 2 Bromoform .BRL _ug/L 179 34 5 1 1 2,2 Tetrachloroethane BRL ug/L 1 541 73 1 1 3 Dic_hlorobenz_ene --_ --_- -- -- -BRL - ----ug/L _ - , 106-06-7 1 4-Dichlorobenzene BRL ug/L 1 -- ---- — ---- -- --- ------ 95.50-1- ---.- _- 1,2-Dichlorobenzene BRL ._--.-___.--.-_I-_- ug/L_-__-_ ---__-I QC Surrogate Compound Recovery QC Limits — i 1,2 Dichloroethaned4 �- ---,-._ _ 94 % I 70 130 % - ' Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyse list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration,if any, is below reporting limit for analyte. Reporting limit is the lowest ' concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: MW-2 Laboratory ID: 35562-02 Project: Blain Hair School/5786.00 QC Batch ID: VG2-1782-W Client: Atlantic Environmental Sampled: 08-28-00 Container: 40mL Glass Vial Received: 08-28-00 Preservation: - HCI/Cool Analyzed: 08-30-00 ' Matrix: Aqueous Dilution Factor: 1 CAS Number Anal e i yt Concentration Umts� Reporting Limit 75-71-8 Dichlorodifluoromethane BRL ug/L 5 7487-3 Chloromethane BRL -- _ ug/L 5 75-01-4 Vinyl Chloride BRL_ ug/L 2 74-83-9 Bromomethane BRL ug/L 5 75-00.3 Chloroethane BRL ug/L__ 5 ' 75-69-4 Trichloro8uoromethane _ BRL ug/L 1 _75-354 1,1-Dichloroethene _ _—_- BRL _ ug/L 1 75-09-2 Methylene Chloride _ _ _ BRL _ ug/L 1 �. 156-60-5 trans-1,2-Dichloroethene _BRL ug/L 1 75-34-3 1,1-Dichloroethane BRL ug/L i 15C59-2 cis-1,2-Dichloroethene BRL ug/L 1 67-66-3 Chloroform BRL ug/L 1 107-06-2 1,2-Dichloroethane BRL ug/L 1 71-55-6 1,1,1-Trichloroethane --BRL ug/L 1 56-23-5 Carbon Tetrachloride BRL ug/L 1 _ ' - 78 87 5 1,2-Dichloropropane _ _BRL _ ug/L 1 7901-6 Trichloroethene BRL _ ' ug/L li 75 27-4 Bromodichloromethane BRL ug/L 1 110-75-8 12-Chlor_oethyl Vinyl Ether -- _--- BRL_ _— ug/L 5 10061-01-5 cis-1,3-Dichloropropene BRL _ ug/L 1 10061-02-6 1trans-1,3-Dic_hloro_propene BRL ug/L 1 79-00-5 1 1 2-Trichloroethane BRL T u 1 � ug/L ' -124481 Dlbromochloromethane BRL ug/L 1 J-127-18-4_______ Tetrachloroethene 3 ug/L 1 08 90 7 Chlorobenzene BRLug/L5_25-2 —Bromoform — ----- ------ -BRL ...---- -- -- ug/L_ -�— — —79 345 -1,1 2,2--a mchloroethane BRL ___ ug/L 1 541 73 1 1 3 Dichlorobenzene BRL ug/L 1 -- - 106467 ! 1 4 Dichlorobenzene I BRL ug/L _ 1 j 95 50.1 L 1 2-Dichlorobenzene BRL ug/L 1 QC Surrogate Compound _ _ Recovery QC Limits 1,2 Dichloroethane-d - -- _._- --- a---- - --- — — -- - 94% _ - J _ 70 130 % ' Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyle list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration, it any, is below reporting limit for analyte. Reporting limit is the lowest ' concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution and sample size. Groundwater Analytical, Inc., P.O. Box 12,00, 228 Main Street, Buzzards Bay, MA 02532 i. GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: MW-3 Laboratory ID: 35562-03 Project: Blain Hair School/5786.00 QC Batch ID: VG2-1782-W Client: Atlantic Environmental Sampled: 08-28-00 Container: 40ml.Glass Vial Received: 08-28.00 Preservation: HCI/Cool Analyzed: 08-30-00 ' Matrix: Aqueous Dilution Factor: 1 CAS Number __ Atwlyte _ Concentration ___ Units Reporting Limit 75-71-8 DichlorodiFluoromethane BRL ug/L 5 ---- — ----- -- 7487-3 C nyl—Chl—de BRL ug/L 5 75-01-4 Vinyl Chloride BRL ug/L 2 74-83-9 Bromomethane BRL ug/L 5 75-00-3 Chloroethane BRL ug/L 5 75-69-4 Trichlorofluoromethane BRL ug/L 1 75-35-4 1,1-Dichloro_ethene BRL_ ug/L 1 75-09-2 _ Methylene Chloride BRL ug/L 7 156-60-5 trans-1,2-Dichloroethene BRL ug/L 1 ' 75-34-3 1,1-Dic_hloroethane BRL ug/L 1 15659-2 cis-1,2-Dichloroethene 10 ug/L 1 67-66-3 Chloroform 2 ug/L 1 107-06-2 1,2-Dichloroethane BRL ug/L 1 71-55-6 1,1,1-Tri_chIoroethane BRL _ ��ug/L 1 56-23-5 Carbon Tetrachloride BRL ug/L�-1 78-87-5 ) pane _BRL _ ug/L 1 79-01-6 chloroeth_ene �i-- 5 _ _up�_L 75-27-4 _ -_BRL_ _ ug/L _1 110-75-8 hloroeth I Vinyl Ether _ -..---- — Y Y BRL -- ug/L 1--- 5 10061-01-5 as-1,3-Dichloropropene BRL _ ug/L 1 10061-02-6 I trans-1,3-Dichloropropene BRL ug/L 1..-- -- - --- j— -- ...._ --- ethane -- -- ---- ..------ --- - -- 79-00-5 � 1,1,2-Trichloroe[hane _BRL ug/L 1 - - — — --- 124481 Dibromochlorome --- BRL __u L ne— g� 127 18 4 Telrachloroelhene 56 _ _ ug/L 108 90 7 Chlorobenzene BRL ug/L I ' 75 25 2 I Bromoform BRL ug/L 7 79 34 5 I_1 1 2 2 Tetrachloroethane _BRL _ ug/L t 541 73 1 1 3 Dichlorobenzene I BRL _ _ug/L 706-46-7 7 4 Dichlorobenzene _ BRL j ug/L _� 1 ' 95 50 1 1 2-Dichlorobenzene I _ BRL ug/L 1 .-- -- -- -- --- - -- - _._. i. ---- ---- -QC Surrogate Compound Recovery QC Lrmits 1,2 Dlchloroethane-d, 93 % _ 70 130 % ' Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyze. Reporting limit is the lowest t concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E ' Halogenated Volatile Organics by GC/ELCD Field ID: MW-4 Laboratory ID: 35562-04 Project: Blain Hair School/5786.00 QC Batch ID: VG2-1782-W Client: Atlantic Environmental Sampled: 08-28-00 Container: 40mL Glass Vial Received: 08-28-00 Preservation: HCI/Cool Analyzed: 08-30-00 Matrix: Aqueous Dilution Factor: 1 CAS Number _: : Anal a Concentration Units Reporting Limit 75-71-8 Dichlorodifluoromethane BRL ug/L 5 -74-87-3 Chloromethane BRL ug/L 5 75-01 4 Vinyl Chloride_ BRL ug/L 2 74-83-9 Bromomethane BRL _ ug/L 5 75-00-3 Chloroethane BRL ug/L 5 75-69A Trichlorofluoromethane BRL ug/L 1 75-35-4 1,1-Dichloroethene BRL ug/L 1 75-09-2 Methylene Chloride BRL ug/L 1 ' 156-60-5 trans-1,2-Dichloroethene BRL ug/L 1 75-34-3 1,1-Dichloroethane BRL ug/L 1 156-59-2 cis-1,2-Dich1oroethene _BRL ug/L 1 67-66-3 Chloroform - _BRL ug/L 1 107-06-2 1_2-Dichloroethane BRL_ _- ug/L 1 71-55-6 1 1,1-Trichloroethane BRL_ ug/L 1 56-23-5 Carbon Tetrachloride BRL _ ug/L 1 ' 78-87-5_1 2 Dichloropropane -- ---_____BRL ug/L 1 79-01-6 -Trichloroethene BRL__ ug/L 1 175-27-4 Bromodichloromethane BRL ug/L 1 110 75 8 2 Chloroethyl Vinyl Ether BRL __ ug/L 5 f-- _ --- _ ---- 10061-01-5 c1s 1,3-Dichloropropene BRL ug/L 1 - _ - - _. . . . .._..------._ _..---- --.._ . . --� --- _70061-02-6 trans-1 3 Otchloropropene � _ _BRL -7900-5 11,2-Tnthloroe[hane __ _BRL -_-_I_ ug/L 1 -124-48-1- Dibromochloromethane - I - BRL - u L 1 L-- Y� 12718-0 I Tetrachloroethene 27 ug/L 1 _6 .-- - o --- - -- - - ---- 108 90 7 _l Chlorobenzene ____ __ BRL ' ug/L _ 1 75. 25 2 _ Bromoform I BRL ug/L 1 79 34 5 _--_I_7 1 2,2-Tetrachloroethane _BRL _ _ ug/L 7 541 73 1 1 9 Dichlorobenzene r BRL I 10(r4(r7 14Dichlorobenzene BRL I -- J ' 95 50 1 1,2-Dichlorobenzene BRL ug/L _ QC Surrogate Compound RecoveryQC Limits --- 1 2 Dichloroethane-da — 1 - -a/ -- - -- o - -' 1 � 97 0 70 130 /o ' Method Reference. Test Methods for Evaluating Solid Waste, US EPA, 5W-846,Third Edition, Update III (1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyle. Reporting limit is the lowest ' concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution and sample size. i 1 , , Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: MW-5 Laboratory ID: 35562-05 Project: Blain Hair School/5786.00 QC Batch ID: VG2-1782-W Client: Atlantic Environmental Sampled: 08-28-00 Container: 40mL Glass Vial Received: 08-28-00 Preservation: HCI/Cool Analyzed: 08-30-00 Matrix: Aqueous Dilution Factor: 1 CAS Number IAnal e - Concentration "—_�_ �Units Reporting Limit 75-71-8 Dichlorodifluoromethane BRL____ ug/L 5 74-87.3 Chloromethane _BRL ug/L 5 75-01-4 Vinyl Chloride BRL ug/L 2 74-83-9 _ —BrOmo_m_ethane _ BRL ug/L _ 5_ 75-00.3 Chloroethane BRL ug/L 5 75-694 Trichlorofluoromethane BRL ug/L 1 75-354 1,1-Dichloroethene BRL ug/L_ _t 75-09-2 M rideethylene Chlo BRL ug/L 1 ' 15-34- -- Vans-1,2-D ethaoethene -- — BRL- -- ug/L 1 75-34-3 1,1-Dichloroe[hane BRL ug/L ro 1 156-59-2 cis-1,2-Dichloethene BRL ug/L 1 67-66-3 Chloroform 2 _ ug/L 1 107-06-2 1,2-Dichloroethane _BRL ug/L 1 71-55-6 1,1,1-Trichloroethane BRL ug/L 1 56-23-5 Carbon Tetrachloride _ BRL _ ugtL 1 78-87-5 _ richli roeth propane"--_ -_ —__ — BRL —— ug/L_- 79 01 6 Tnchloroethene 8RL ug/L 1 75274 Bromodichloromethane 6RL _ _ug/L 1 110.75-8 2 Chloroethyl Vinyl Ether BRL ug/L _ 5_ 10061-01-5 cis-1,3-Dichloropropene BRL ug/L 1 70061-02-6 tram- l,3-Dichloropropene BRL ug/L 1 1-. 79-00-5 1,1,2-Trichloroethane BRL ury/L 1 - L-. - _- --""_---_ -_--_�- 124-48 1 I Dlbr_omochloromethane BRL ug/L I 1 127 18 4 ____ Tetrachloroethene 17 _ug/L 1 • 108 9 07 Chlorobenzene _ _ BRL ug/L _ t 75 25 2 Bromoform _ __ BRL ug/L _ t 79 34 5 1 1 2,2 Tetrachloroethane BRL ug/L --- --)_ 73 1 1 3 Dichlorobenzene BRL _ ug/L 1 106-467 1 7 4-Dichlorobenzene BRL ug�L j 95-50.1 � 1 2-Dichlorobenzene BRL 1 ug/L I 1 QSurrogate Compound Recovery QC Limits ! 1,2-Dichloroethanetl -- -- - ----" I- "-- - + 98 /0 70 130 % -' Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyte. Reporting limit is the lowest • concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: MW-7 Laboratory ID: 35562-07 Project: Blain Hair School/5786.00 QC Batch ID: VG2-1782-W Client: Atlantic Environmental Sampled: 08-28410 Container: . 40mL Glass Vial Received: 08-28-00 Preservation: - HCI/Cool Analyzed: 08-30-00 Matrix: Aqueous Dilution Factor 1 CAS Number. a :. k.. 'Analyte „; „,,, . ,.Concentration _ ";:'Umts Reporting_Limit 75-71-8 Dichlorodifluoromethane BRL ug/L 5 ' 74-87-3 Chloromethane BRL ug/L 5 75-01-4 Vinyl Chloride BRL ug/L 2 74-83-9 Bromomethane BRL ug/L 5 75-00-3 Chloroethane BRL ug/L 5 75-694 Trichlorofluoromethane BRL ug/L 1 _75-35-4 1,1-Dichloroethene _ BRL u�L 1 75-09-2 1 Methylene Chloride BRL ug/L 1 156-60-5 trans-1 hl Dichloroethene - BRL — ug/L 1 75-34-3 1 s-1,2--D h-Ioro th BRL ug/L 1 15rr59-2 cis-7rofDichloroethene 74 _ ug/L 1 67-66-3 Chloroform BRL ug/L 1 107-06-2 1,2-Dichloroethane BRL ug/L 1 71-55-6 1,1,1-Trichloroethane BRL ug/L 1 56-23-5 Carbon Tetrachloride BRL ug/L 1 -- - — - 78-87-5 1,2-Dichloropropane BRL ug/L 1 _ 79-01- Trichloroethene 10 ug/L 1 - 6 75-27-:U l - om --- --------- -------------...---- - - -4 Brodichloromethane _ BRL � ug/L -- ---1 - 110-75-8 2-Chloroethyl Vinyl Ether BRL ug/L 5 -01' 10061 -5 cis-1,3-Dichloropropene _ BRL _ _ ug/L 1 3 10061-02-6 _ _trans-1, -Dichloropropene _BRL ug/L 1 79-00-5 1,1,2-Trichloroethane _ BRL ug/L 1_ 124-18-1 Dibromochloromethane BRL ug/L 1 -1 -- ro --._._.. .- -- - ----- --- ----- - - ----- ------- 127-18-4 Tetrachloroethene 180 ug/L -_ 1 108-90-7 Chlorobenzene - BRL _ ug/L __ 1 75 25 2 Brom_oform BRL ug/L 1 -. _ . _chlo. 79 34 5 1 1,2,2 Tetraroethane _ BRL ug/L 1 I 541 73 1 1 3 Dtchlorobenzene _ _BRL _ ug/L_ 1 I_106-06-7 1 4 Dtchlorobenzene BRL ug/L 1 ..-- -- - - - - --- - _- --- -- 95 50.1 1 1 2 Dtchlorobenzene BRL u L 1 QC Surrogate Compound Recovery QC Limits 1 2-Dichloroethane-d4 � -__- 96 % _--� 70 130% Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration,if any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution and sample size. I Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: MW-8 Laboratory ID: 35562-08 Project: Blain Hair School/5786.00 QC Batch ID: VG2-1782-W Client: Atlantic Environmental Sampled: 08-28-00 Container: 40mL Glass Vial Received: 08-28-00 Preservation: HCI/Cool Analyzed: 08-311-00 Matrix: Aqueous Dilution Factor 1 -`CAS,Number ;"+.,.,; ,=' CAnal a `," -�, , ;.,. .„ ;.Concentration,; �:r Reporting-Limit 75-71-8 Dichlorodifluoromethane BRL ug/L 5 74-87-3 Chloromethane BRL ug/L 5 75-01-4 _Vinyl Chloride BRL ug/L 2 74-83-9 Bromomethane BRL W91L 5 75-00-3 Chloroethane BRL ug/L 5 r 75-69-4 Trichlorofluoromethane BRL ug/L 1 75-35-4 1,1-Dichloroethene BRL _ ug/L 1 75-09-2 Methylene Chloride _ BRL _ ugtL 1 156-60-5 trans-1,2-Dichloroethene BRL ug/L 1 75-34-3 1,1-Dichloroethane BRL ug/L 1 156-59-2 cis-1,2-Dichloroeth ne BRL Mitt 1 67-663 Chloroform .BRL ug/L 1 107-06-2— 1,2-Dichloroethane _ — BRL ug/L 1 71-55-6 1,1,1-Trichloroethane BRL — ug/L 1 56-23-5 Carbon Tetrachloride _ BRL ug/L 1 78-87-5 1,2-Dichloropropane BRL ug/L 1 r 79-01-6 Trichloroethene — —_ 3 _ ug/L_ 1 75-27-4 Bromodichloromethane BRL ug/L 1 ------ -- -------- 11C75-8 — 2-Chloroethyl Vinyl Ether - BRL ug/L 5 ' 10061-01-5 cis-1,3-Dichloropropene _BRL — ug/L 1 10061-02-6 trans-1,3-Dichloropropene _ _ BRL _ ug/L 1 79-00-5 1,1,2-Trichloroethane BRL ug/L 1 - -- 124-48-1 Dibromochloromethane BRL Mitt 1 127 18 4 ac Tetrhloroetheue 170 Mitt 1 - ----.. _ ac ---- ------ - - -..._--- - - — -- ----- ---- — 108 90 7 CMorobenzene — BRL _ ug/L 1 75 25 2 _ Bro_m_oform _ BRL ug/L 1 79-34-5 1,3-DicTetrobenzoethane _ BRL ug/L ' �541-73-1 1,3-Dichlorobenzene BRL ug/L 1 l 106-46-7 1 4 Dichlorobenzene BRL ugtL 1 95 50 1 1 2 Dichlorobenzene_ BRL _ug/L 7 11 QC Surrogate Compound _ — Recovery___ QC Limits � 7,2 Dichloroethane-da 94 /0 70 730 k Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition,Update III (1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution and sample size. r r Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 to GROUNDWATER ANALYTICAL Project Narrative Project: Blain Hair School/5786.00 Lab ID: 35562 Client: Atlantic Environmental Received: 08-28-00 A. Physical Condition of Sample(s) This project was received by the laboratory in satisfactory condition. The sample(s) were received undamaged in appropriate containers with the correct preservation. B. Project Documentation �\ This project was accompanied by satisfactory Chain of Custody documentation. The sample container label(s) agreed with the Chain of Custody. C. Analysis of Sample(s) No analytical anomalies or non-conformances were noted by the laboratory during the processing of these sample(s). All data contained within this report are released without qualification. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER 228 Man S PO.Box 1200 Buzzards Bay ,MA02532 CHAIN-OF-CUSTODY RECORD ANALYTICAL Telephone(508)759-4441 AND WORK ORDER N9 42922 FAX(508)759-4475 Project Name: ++ Firm: TURNAROUND ANALYSIS REQUEST 1kAu 55tt4:L ❑ STANDARD If O Business Days) vemn.. srmlaelamn Imedncaa Nem. M1°•'�^ wean. warn penmlraemMry fare,Project Number: Address: �RIORITY(5 Business Days) E o 2S a a -C�/ 13 i(.V 171:i^-1 f ❑ RUSH(RAN- 1 F 2 4 _ £ `a Sampler Name: City/State/tip: (Ruse requires Rush Authorization Number) $q I Please FAX ES ❑ NO a A _ RAG (J k.-; -�n ;llA FAX Number: 3l' e S g5 pp S .eject Manager: Telephone: BILLING o o a o o o o E p p Purchase Order No.: GWA Reference No.: ff $ = S3 $ $ 4 NSTRUCTIONS:Use separate line for each container(except replicates). z 5 v O 4 :amplIng Malrlx Type Contalner(s) Presenatlon h 0 5 0 s 0 s 9 5 c c o o v v c v v ° v SaNPLE i y ",in LABORATORY IDENtIFlCAOON R i $ W d NUMBER $$ �d a a a a a a a _ a5 „ a - g (Lab Use Only) dggx3P ` � ; £ ° g ° 4tlaa 3 3` 03 = � $ gkkes 55(�aS § $ 3 a § � " s' aci € 3 � s9313 `a § 's � a2 v a v v v v o v o o v v v a v v o o B c o - v v v v v v v o = v v nls 3 if U3r w-z a 1"YS �qW, 3 1m h1'r 5 rnr u > nw- I fillg REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program Project Specific OC NOTE:All samples submitted subject to Standard Terms and Conditions on reverse hereof. )yLL LrkN`r G Sale Drinking Water Act Many regulatory programs and EPA methods require project Relinquish tar. Dale Time Received by: Receipt Temperature: 1 ❑Ma DEP Form specific OC.Protect specific OC includes Sample Du 'I' tes, p '^.'�qQ- O NPDES/Clean Water Ad Matrix Spikes,and/or Matrix Spike Duplicates.Laboratory OC is _ Dd'' Speuty Slate: not project specific unless prearranged.Project specific OC �x O CLCn�1):'/L ❑RC Hai.Waste Char. samples are charged on a per sample basis.For water samples, Relinquished by: Date Time Received by: Shippirg/Airbill A MCP(310 CMR 40) each MS,MSD and Sample Duplicate requires an additional Number: Reportable Concentrations sample aliquot. G W I O RCS-1 Project Specific OC Required SeNdbn of OC Sample Relinquished by: Data Time Received by Laboratory: Custody Sear' RCGW 2G RCS-2 ❑Sample Duplicate ❑Seledad by labpratory I' i Copley Serial y� 7'kk�-lull`, L Number: ❑NH Dredge Disposal0ME D Matdx Spike ❑%eau use sample: o ❑NH O Al p CT❑ME Method of Shipment: O GWA Co ❑Express Mail ❑Federal Expra' Specify Category: ❑Malhx spire Duplicate ❑UPS antl 0 GROUNDWATER ANALYTICAL Quality Assurance/Quality Control A. Program Overview Groundwater Analytical conducts an active Quality Assurance program to ensure the production of high quality, valid data. This program closely follows the guidance provided by Interim Guidelines and Specifications for Preparing Quality Assurance Project Plans, US EPA QAMS-005/80 (1980), and Test . Methods for Evaluating Solid Waste, US EPA, SW-846, Update III (1996). Quality Control protocols include written Standard Operating Procedures (SOPs) developed for each analytical method. SOPS are derived from US EPA methodologies and other established references. Standards are prepared from commercially obtained reference materials of certified purity, and documented for traceability. Quality Assessment protocols for most organic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. All samples, standards; blanks, laboratory control samples, matrix spikes and sample duplicates are spiked with internal standards and surrogate compounds. All instrument sequences begin with an initial calibration verification standard and a blank; and excepting GC/MS sequences, all sequences close with a continuing calibration standard. GC/MS systems are tuned to appropriate ion abundance criteria daily, or for each 12 hour operating period, whichever is more frequent. Quality Assessment protocols for most inorganic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. Standard curves are derived from one reagent blank and four concentration levels. Curve validity is verified by standard recoveries within plus or minus ten percent of the curve. ' B. Definitions Batches are used as the basic unit for Quality Assessment. A Batch is defined as twenty or fewer samples of the same matrix which are prepared together for the same analysis, using the same lots of reagents and the same techniques or manipulations, all within the same continuum of time, up to but not exceeding 24 hours: Laboratory Control Samples are used to assess the accuracy of the analytical method. A Laboratory Control Sample consists of reagent water or sodium sulfate spiked with a group of target analytes representative of the method analytes. Accuracy is defined as the degree of agreement of the measured value with the true or expected-value. Percent Recoveries for the Laboratory Control Samples are calculated to assess accuracy. Method Blanks are used to assess the level of contamination present in the analytical system. Method Blanks consist of reagent water or an aliquot of sodium sulfate. Method Blanks are taken through all the appropriate steps of an analytical method. Sample data reported is not corrected for blank contamination. Surrogate Compounds are used to assess the effectiveness of an analytical method in dealing with each sample matrix. Surrogate Compounds are organic compounds which are similar to the target analytes of interest in chemical behavior, but which are not normally found in environmental samples. Percent Recoveries are calculated for each Surrogate Compound. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report M Laboratory Control Sample Category: EPA Method 8012B-Halogenated QC Batch ID: VG2-1782-W Matrix: Aqueous Units: ug/L CAS,NUmber "t Analyte`.: �, ": '' Spiked`2 :_Measured ` Recovery. i:'.'QC Limits 75-35 4 1 1-Dichloroethene 5 5 102 % 70-130 % _79-01-6 Trichloroethene 5 5 105 % 70-130 % 108-90-7 Chlorobenzene 5—_ _ 5 109% 70- 130% QC Surrogate Compound - Recovery -QC Limits'-- 1,2-Dichloroethaned. ___ _ 103 °/ '__ __ 70- 130% Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition, Update 111(1996). Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report �- Method Blank Category: EPA Method 80218- Halogenated QC Batch ID: VG2-1782-W Matrix: Aqueous CAS Number Analyte Concentration Units Reporting limit ' 75-71-8 Dichlorodifluoromethane BRL ug/L 5 74-87-3 Chloromethane BRL ug/L 5 75-01-4 Vinyl Chloride --_ - BRL ug/L 2 - - 74-83-9 Bromo-etKa ne g/L BRL u 5 Chl 75 00-3 oroethane BE— ug/L 5 75 69-4 T r ioromethane _BRL ug/L 1 75-35-4 1,l-Di1-Dich-orloroethene BRL ug/L 1 ' 75-09-2 Methylene Chloride _ BRL ug/L 1 156-60 5 trans 1 2 Dichloroethene BRL _ _ug/L _ 75-34-3 1 1 Dichloroethane _ BRL ug/L____ _7 _. ---- -ich en-o - -- - -- - ----- 156-59-2 as 1 2 Dichloroethene _ _ _ BRL ug/L__ ___7 _ 67-66-3 Chloroform - BRL _ - _ ug/L 1 107-06-2 1,2 Dichloroethane BRL ug/L 1 -- - ------- ---_....----- --- ---- ---�-- --- 71-55-6 1,1boTrichloroethane - -- — BRL - -- L L 1 --- - - ' 56-23-5 Carbon Tetrachloride BRL _ ug/L 1 7--5 ---- - - ------ 78-87-5 1,2-Dichloropropane BRL_ _ ug/L 1 79-01-6 Trichloroethane - - - - BRL --_, ug/L _t 75-27-4 Bromodichlorome[hane- —�__ BRL_- - Jr-- ug/L--- 1 110-75-8 2-ChloroethyI Vinyl Ether BRL ug/L 5 10061-01-5 cis-1,3 Dichloropropene BRL l ug/L 1 10061-0246 trans-1,3-Dichloropropene BRL ug/L 1 79-00-5 *1 1 2 Tnchloroethane _ _ BRL i_ ug/L 1 --- -`- - - -- - ---- - ---124-48-1 Dlbromoch_lorometha_ne _ - _ BpL _ j ug/L 12718-4 1 Teirachloroethene _ BRL ug/L 1 - 108 90-7 Chlorobenzene BRL ug/L 1 75 25-2 I Bromoform - - BRL _ _ ug/L 1 _ 1 1 2 2 Tetrachloroethane _ BRL ug/L I 1 541 73-1 1 3 Dichlorobenzene _ BRL __I_ ug/L 1 106-46-7 1 4 Dichiorobenzene _ BRL ug/L - 1 95 50-1 _.L-1 2 Dichlorobenzene L BRL__- --I-- ug/L - QC Surrogate Compound Recovery QC Limits �� 1 2-Dichloroethaneda 95 % 70- 130°/ Method Reference Test Methods for Evaluating Solid Waste, US EPA, 5W 846,Third Edition Update III (1996t. Analyze list as selected from list formerly specified by EPA Method 8010B. Report Notations: BRL Indicates concentration,if any, is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 1 GROUNDWATER ANALYTICAL Certifications and Approvals CONNECTICUT, Department of Health Services, PH-0586 �.. Potable Water,Wastewater/Trade Waste,Sewage/Effluent,and Soil pH,Conductivity,Acidity,Alkalinity,Hardness,Chloride,Fluoride,Ammonia,Kjeldahl Nitrogen,Nitrate,Nitrite,Orthophosphate,Total Dissolved Solids,Cyanide,Aluminum,Antimony,Arsenic,Barium,Beryllium,Cadmium,Total Chromium,Hexavalent Chromium,Cobalt,Copper,Iron,Lead, Magnesium,Manganese,Mercury,Molybdenum,Nickel,Potassium,Selenium,Silver,Sodium,Thallium,Tin,Titanium,Vanadium,Zinc,Purgeable Halocarbons,Purgeable Aromatics,Pesticides,PCBs,PCBs in Oil,Ethylene Dibromide,Phenols,Oil and Grease. MAINE, Department of Human Services, MA103 rDrinking Water* Reciprocal certification in accordance with Massachusetts certification for drinking water analyzes. Waste Water ' Reciprocal certification in accordance with Massachusetts certification for waste water analytes. MASSACHUSETTS, Department of Environmental Protection, M-MA-10371 �f Potable Water Antimony,Arsenic,Barium,Beryllium,Cadmium,Chromium,Copper,Lead,Mercury,Nickel,Selenium,Thallium,Nitrate-N,Nitrile,N,Fluoride, Sodium,Sulfate,Cyanide,Turbidity,Residual Free Chlorine,Calcium,Total Alkalinity,Total Dissolved Solids,pH,Trihalomezhanes,Volatile Organic Compounds,1,2-Dibromoethane,1,2-Dibromo-3-chloropropane,Total Coliform,Fecal Coliform,Heterotrophic Plate Count,E-Coli Non-Potable Water Aluminum,Antimony,Arsenic,Beryllium,Cadmium,Chromium,Cobalt,Copper,Iron,Lead,Manganese,Mercury,Molybdenum,Nickel,Selenium, Silver,Strontium,Thallium,Titanium,Vanadium,Zinc,pH,Specific Conductance,Total Dissolved Solids,Total Hardness,Calcium,Magnesium, Sodium,Potassium,Total Alkalinity,Chloride,Fluoride,Sulfate,Ammonia-N,Nitrale-N,Kjeldahl-N,Orthophosphate,Total Phosphorus,Chemical �• Oxygen Demand,Biochemical Oxygen Demand,Total Cyanide,Non-Filterable Residue,Total Residual Chlorine,Oil and Grease,Total Phenolics, Volatile Halocarbons,Volatile Aromatics,Chlordane,Aldrin,Dieldrin,DDD,DDE,DDT,Heptachlor,Heptachlor Epoxide,Polychlorinated Biphenyls(water),Polychlorinated Biphenyls(oil). MICHIGAN, Department of Environmental Quality ' Drinking Water Trihalomezhanes,Regulated and Unregulated Volatile Organic Compounds by EPA Method 524.2;1,2-Dibromoezhane,1,2-Dibromo-3- chloropropane by EPA Method 504.1 NEW HAMPSHIRE, Department of Environmental Services, 202798 Drinking Water Metals by Graphite Furnace,Metals by ICP,Mercury,Nitrite-N,Orthophosphate,Residual Free Chlorine,Turbidity,Total Filterable Residue,Calcium ' Hardness,pH,Alkalinity,Sodium,Sulfate,Total Cyanide,Insecticides,Herbicides,Base/Neutrals,Trihalomethanes,Volatile Organics,Vinyl ' Chloride,DBCP,EDE,Nitrate-N. Wastewater Metals by Graphite Furnace,Metals by ICP,Mercury,pH,Specific Conductivity,TDS,Total Hardness,Calcium,Magnesium,Sodium,Potassium, Total Alkalinity,Chloride,Fluoride,Sulfate,Ammonia-N,NitratrN,Orthophosphate,TKN,Total Phosphorus,COD,BOD,Non-Filterable Residue, Oil&Grease,Total Phenolics,Total Residual Chlorine,PCBs in Water,PCBs in Oil,Pesticides,Volatile Organics,Total Cyanide. RHODE ISLAND, Department of Health, 54 Surface Water,Air,Wastewater, Potable Water,Sewage Chemistry: Organic and Inorganic ,.I Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 r, ' Groundwater Analytical, Inc. GROUNDWATERP.O. O Box 1200 ANALYTICAL Buz Main Street Buzzards Bay,MA 02532 t Telephone(508)759-4441 FAX(508)759-4475 September 7, 2000 ' Mr. Eric Cardinal Atlantic Environmental ' 13 Hamilton Street New Bedford, MA 02740 ' Project: Blaine/5786.00 Lab ID: 35636 Sampled: 08-30-00 Dear Eric: Enclosed are the Volatile Organics Analyses performed for the above referenced project. This ' project was processed for Priority One Week turnaround. This letter authorizes the release of the analytical results, and should be considered a part of this report. This report contains a project narrative indicating project changes and non-conformances, a brief description of the Quality Assurance/Quality Control procedures employed by our laboratory, and a statement of our state certifications. I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to ' the best of my knowledge and belief, accurate and complete. Should you have any questions concerning this report, please do not hesitate to contact me. i ' Sincerely, ' Joriathan R. Sanford President ' JRS/jmi Enclosures GROUNDWATER ANALYTICAL EPA Method 8021B ' Halogenated Volatile Organics by GC/ELCD Field ID: AB-1(3) Laboratory ID: 35636-01 Project: Blaine/5786.00 QC Batch ID: VG2-1785-E ' Client: Atlantic Environmental Sampled: 08-30-00 Container: 60mL Glass Received: 08-30-00 Preservation: Methanol/Cool Analyzed: 09-06-00 Matrix: Soil Dilution Factor 4 ' %Moisture 7 CASbNumber f w f_„ Analyte ? k, ."., Conce'ntiatio'hUnrts Reporiirig`Limit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 1,100 ' 74-87-3 Chloromethane BRL ug/Kg 1,100 75-01-4 Vinyl Chloride BRL ug/Kg 430 74-83-9 Bromomethane BRL ug/Kg 1,100 ' 75-00-3 Chloroethane BRL_ ug/Kg 1,100 75-69-4 Trichlorofluoromethane BRL ug(Kg 220 75-35-4 1,1-Dichloroethen_e _ BRL ug/Kg 220 75-09-2 Methylene Chloride BRL ug/Kg 1 220 ' 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 220 75-34-3 1,1-Dichloroethane BRL ug/Kg 220 15659-2 cis-1,2-Dichloroethene BRL j ug/Kg 220 67-66,3 Chloroform _ BRL �_ ug/Kg' _ 220 107-06-2 1,2-Dichloroethane__— BRL__- ugg/Kg_ _220 71-55-6 1,1,1-Trichloroethane BRL _ug/Kg 220 56-23-5 Carbon Tetrachloride BRL — ug/Kg 220 78-87-5 1,2-Dichloropropane BRL i ug(Kg 220 - ----T- 79-01-6 Trichloroethene BRL ' ug/Kg 220 ------- ------ --------------- ------------------ --- 75-27-4 Bromodichloromethane BRL _ug/Kg 220 ' 110-75-8 — 2-Chloroethyl Vinyl Ether _- BRL — ,_ ug/Kg 1,100 10061-01-5 cis-1,3-Dichloropropene _ _ BRL ug/Kg_ 220 10061-02-6 trans-1,3-Dichloropropene_ _' BRL ug/Kg_ _220__ 79-00-5 1,1,2-Trichloroethane -1 BRL ug/Kg _ 220 124-48-1 Dibromochloromethane_ BRL ug/Kg 220 127-18-4 Tetrachloroethene 4,500 ug/Kg 220 10B-9C Chlorobenzene BRL ug/Kg 220 ' 75-25-2 Bromoform BRL ug/Kg 220 — BRL ---- ---- 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 220 -- ------- ----------._--.....------ --- 541-73-1 1,3-Dichlorobenzene BRL I ug/Kg 220 _ 106,4&7 1,4-Dichloro_benzene_ - BRL _ug/Kg 22_0_ 95-50-1 1,2-Dichlorobenzene BRL ug/Kg _ 220 QC Surrogate Compound Recovery QC Limits ' _1,2-Dichloroethane-d, 98 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update 111(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,if any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: AB-1(6) Laboratory ID: 35636-02 Project: Blaine/5786.00 QC Batch ID: VG2-1785-E Client: Atlantic Environmental Sampled: 08-30-00 Container: 60ml.Glass Received: 08-30-00 Preservation: Methanol/Cool Analyzed: 09-06-00 Matrix: Soil Dilution Factor: 1 %Moisture: 4 �MCAS.'NUrhbier1'� 773?—Xni—l—w -':v -'- p6rjIrjtJm-'t 75-71-8 Dichlorodifluoromethane B-RL ug/Kg 260 74-87-3 Chloromethane BRL —u 260— 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 260 75-00-3 Chloroethane BRL 2-60 75-69-4 Trichlorofluoromethane BRL ug/Kg 52 75-354 1,1-Dichloroethene --8RL ug/Kg 5-2 75-09-2 Methylene Chloride BRL ug/Kg— 52 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 52 75-34-3 1,1-Dichloroethane BRL ug/Kg 52 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 5-2 67-66-3 Chloroform BRIL ug/Kg 52 107-06-2 1,2-Dichloroeth _52 71-55-6 1,1,1-Tri ch loraefha—ne BRL ug/Kg 52 56-23-5 Carbon Tetrachloride 52 78-87-5 1,2-Dichloropropane BRL--- ug/K9 52, _ 79-01-6 Trichloroethene BRL---=' ug/Kg 52 75-274 Bromod,ichloromethane---- BRIL ug/Kg 52 110-75-8 2-Chloroethyl Vinyl Ether BRIL ug/Kg 260 ----�0061-01�5 cis ichloropropene BRL ug/Kg— 52 1 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 52 79-00-5 1,1,2-Trichloroethane ug/Kg 5-2- 12448-1 Diloronnochloromethane ug1Kg 52 127-184 Tetrachloroethene 130 ug/Kg --52— 108-90-7 Chlorobenzene BRL ug/Kg 52— 75-25-2 Bromoform BRL —ug/Kg 52 79-34-5 1,1,2,2-Tetrachl-oroethane BRL ug/Kg —52 - -- 11,3-[Dichloro�mzene BRL ug/Kg 52 541-T3-1 106 1 -BR L 52 95-50-1 I--4ki 1,2-Dichlorobenzene__ BRL I ug/Kg 52 _QC Surrogate galeCOmpoo_nl Recovery -QC LimitZR2DichloroQthan:d, q7 % 70 O � Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update 111(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: AB-11(112) Laboratory ID: 35636-03 Project: Blaine/5786.00 QC Batch ID: VG2-1785-E Client: Atlantic Environmental Sampled: 08-30-00 Container: 60mL Glass Received: 08-311-00 Preservation: Methanol/Cool Analyzed: 09-06-00 Matrix Soil Dilution Factor: 1 % Moisture: 2 CAS umuee;; Anal n"i;","-'.""""�� '_ ;::Concentration 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug(Kg 2-60 75-00-3 Chloroethane BRL ug/Kg 260 75-694 Trichlorol'I uomo—methane BRL ug/Kg 51 75-35-4 1,11-Dichloroethene BRL ug/Kg 51 75-09-2 Methylene Chloride BRL ug/Kg 51 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 51 75-34-3 1,1-Dichloroethane BRL ug(Kg 51 156-59-2 cis-1,2-Dichloroethene' BRL 51 67-663 Chloroform— BRL ug/Kg 51 107-0&2 11,2-Dichloloethane BRL -ug/Kg 51 71-556 1,1,1-Tric 110toroeIhane BRL ug/Kg 51 56-21-5 EqCarlon TetrachlorideBRL ug/Kg 51 78-87-5 1,2-D ropropane ---BRL ug/Kg 51 79-01-6 Trichloroethene BRL ug/Kg 51 75-27-4 Bromodichloromethane BRL ug(Kg 51- 110-75-8 2-Chloroethyl Vinyl Ether L --ug/Kg 260 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 51 10061--02-6 trans---1,3-Dichloropropene u K 9 79-M5 YTH61oroethane BRL ug/Kg 51 124-48-1 Dibromochloromethane t--BRL-----I- ug/Kg —51 127-184 Tetrachloroethene 69 ug/Kg 51 108-90-7 Chlorobenzene 1 BRL ug/Kg 5 - 75-25-2 Bromoform M ug/Kg 51 79-34-5 1,1,2,2-fe—trachloroethane BRL ug/Kg 51 541-73-1 11,31-Dich1wodivrizene BRL —"g1ki——511 106-46-7 1,4-Dichlc enzene BRL _ug/Kg_ - 51 95-50-1 1,2-Dichlorobenzene BRL QC Surrogate Compound Recovery QC Limits 1,2-Dichloroelhaned4 96 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update 111(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: AB-2(3) Laboratory ID: 35636-04 Project: Blaine/5786.00 QC Batch ID: VG2-1785-E Client: Atlantic Environmental Sampled: 08-30-00 Container. 60mL Glass Received: 08-30-00 Preservation: Methanol/Cool Analyzed: 09-06-00 Matrix: Soil Dilution Factor: 1 %Moisture: 6 A'CAs c�Cimc-eifitrailiorl: ,,..,Units ;e, Reporting Limit 75-71-11 Dicllorodiluoromethane BRL ug/Kg 270 74-87-3 Chloromethane BRL ug/Kg 270 75-014 Vinyl Chloride BRL ug(Kg 110 74-83-9 Bromomethane BRL ug/Kg 270- 75-00-3 Chloroethane EIRL ug/Kg_ 270 75-694 -tric-k(o-rofl-u-o-ro—m-e—tha—ne-- ---B-R-L---- —ug(Kg -5-3--- 75-354 1,1-Dichloroethene BRL ug/Kg 53 1 75-09-2 Methylene Chloride BRL ug/Kg 53 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 53 75-34-3 1,1-Dichloroethane BRL ug(Kg 53 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 53 67-66-3 Chloroform 56 ug(Kg 53 107-06-2 1,2-Dichloroethane BRL ug/Kg 53 71-55-6 1,1,1-Trichloroethane BRL --- ug/Kg 53 ---- ------- 56-23-5 Carbon Tetrachloride i ug/Kg 53 78-87-5 1,2-Dichloropropane BRL ug/Kg 53 79-01-6 Trichloroethene BRL ugtKg 53 75-27-4 Bromodichloromethane BRL ug(Kg 53 110-75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 270 10061-01-5 cis-1,3-Dichloropropene BRL _ug/Kg 53 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 53 79-00-1 1,1,2-Tnchlorm�tane BRL ug/Kg 53 12448-1 Dibromochloromethane BRL ug/Kg 5-3 127-184 Tetrachloroethene 310 53 Chorobenzene Im-90-7 BRL ug/Kg— 53 75-25-2 Bromoform— BRL ug/Kg 53 1,1,i -- -ne 'jj7 79-34-5 eirachloroetim udkg 53 541-73-1 1,31-Di6lorobenzene BRL ug(Kg 53 106-4&7 1,4�ichlorobenzene BRL ug(Kg _53 � L25-50�1 1,2-Dichlorobenzene BRL ug/Kg 53 QC Surrogate Compound Recovery� QC—Liff—i—ts L_1,2-DichI?methane-d4 100 % 7,D- 130% Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition,Update 111(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021 B ' Halogenated Volatile Organics by GC/ELCD Field ID: AB-2(6) Laboratory ID: 35636.05 Project: Blaine/5786.00 QC Batch ID: VG2-1785-E ' Client: Atlantic Environmental Sampled: 08-30-00 Container: 60mL Glass Received: 08-30.00 Preservation: Methanol/Cool Analyzed: 09-0&00 Matrix Soil Dilution Factor 1 %Moisture: 7 z- CA5`MU' r2 _,:!� 7-:;Arialyte u r. 4�t'-t� ,t s ,`Coriceotratton z '>'�`�'' T Reporiing Limit 75-71-8 Dichlorodifluoromethane BRL 270 74-87-3 Chloromethane BRL 270 75-01-0 Vinyl Chloride BRL 110 74-83-9 Bromomethane BRL 270 75-00-3 Chloroethane BRL 270 75-69-4 Trichlorofluoromethane BRL 54 75-354 1,1-Dichloroethene BRL ug/Kg 54 75-09-2 Methylene Chloride BRL ug/Kg 54 ' 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 54 75-34-3 1,1-Dichloroethane BRL ug/Kg 54 15&59-2 cis-1,2-Dichloroethene BRL ug/Kg 54 ' 67-66.3 Chloroform BRL ug/Kg 54 107-06-2 1,2-Dichloroethane BRL ug/Kg 1 54 71-55-6 1,1,1-Trichloroethane_ BRL ug/Kg 54 56-23-5 Carbon Tetrachloride BRL ug/Kg 54 78-87-5 1,2-Dichloropropane .ug/Kg _ 54 79-01-6 Trichloroethene � BRL ug/Kg 54 75-274 Bromodichloromethane — BRL �ug/Kg 54 ' 110-75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 270 10061-01-5 cis-1,3-Dichloropropene BRIL ug/Kg 54 10061-02-6 trans-1,3-Dichloropropen_e BRL ug/Kg 54 - 79-00-5 1,1,2-Trichloroethane BRL _ug/Kg 54 ' 124-48-1 Dibromochloromethane —BRL ug/Kg 54 127-184 - Tetrachloroethene — _ 1,9.0_0_ '_ug/Kg 54 108-90-7 Chl_oro_b L _enzene _ BR 75-25-2 _ Bromoform _ BRL _ ug/Kg 54 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 54 541-73-1 1,3-Dichlorobenzene BRL ug/Kg 54 106-467_ 1,4-Dichlorobenze_ne__— BRL ug/Kg_ — 54 95-50-1 1,2-Dichlorobenzene BRL ug/Kg 54 QC Surrogate Compound Recovery QC Limits. 1,2-Dichloroethane<14 94 % 70- 130% ' Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update 111(1996). Analyte list as selected from list formerly specified by EPA Method 80108. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. ' Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. 1 ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: AB-2(12) Laboratory ID: 35636-06 ' Project: Blaine/5786.00 QC Batch ID: VG2-1785-E Client: Atlantic Environmental Sampled: 08.30.00 Container: 60ml.Glass Received: 08-30-00 Preservation: Methanol I Cool Analyzed: 09-0&00 Matrix: Soil Dilution Factor: 2 %Moisture: 4 CAS.Number;•;', a Anal e:; ;,. ' . ,yt Concentration #Un1ts ; , Reportinglimit 75-718 Dlchlorodifluoromethane BRL ug/Kg 520 74-87-3 Chloromethane __ BRL _ ug/Kg 520 75-01-4 Vinyl Chloride BRL ug/Kg 210 ' 74-83-9 Bromometh_ane _ - _ BRL_- --- ug/K9 520 75-00-3 Chloroeth_an_e _ BRL _ ug/Kg 520 75-69-4 Trichlorofluoromethane-- - BRL ug/Kg 100 75-35-4 1 1 Dichloroethene._ _ -_ BRL-- - ug/Kg- 100 - 75-09-2 Methylene Chloride_ I BRL_ ug/Kg _ 100 -- 1,2 156-60-5 trans -Dtchbroeth_ene _ BRL_ - 1 ug/Kg 100 75-343 l,l-Dichloroethane BRL ug/Kg_ _ 100 15Cr59-2 cis-7,2-Dichloroethene j BRL -ug/Kg 100 -- 67-663 Chloroform BRL ug/Kg - 100 107-06-2 1,2-Dichloroethane BRL ug/Kg to() ' 71-55-6 1 1,1 Trichloroethane BRL ug/Kg 100 56-23-5 Carbon Tetrachloride BRL ugrKg 100 --- -- - --r ---- -- - - - - ---- ------� 78-87-5 �1 2 Dichloropropane BRL I ug/Kg 100 -- - 79-01 6 Tnchloroethene _ ' BRL ug/Kg 100 i -- -- - -- - 75-27-4 Bromodichloromethane BRL ug/Kg 100 -- '-- -- --- -'-- -- ----"I 110-75-8 _.2-Chloroethyl Vinyl Ether- _-_ i BRL ug/Kg 520 _ 1 ----- ---- -._..-i- _--- 10061-01-5 _ cis-1,3-Dichloropropene BRL ug/Kg 100 _ Iran, P p — -L - --g- ' 70061-02-6 -1,3-Dichloro ro e_n_e_ BRL I ug/Kg 100 1 79-00-5 1,1,2-Trichloroethane - BRL - i_ 1 ugiKg _ 100 -- -- --- 124-48 1 Dlbromochloromethane _ BRL - ug/Kg 100 127-18-4 Tetrachl-roethene _ 2,400 ug/Kg_ _ 100 708-90 7 Chlorobenzene BRL ug/Kg 100 -- -- — — 75-25 2 Bromoform _ I _ BRL_ r ug/Kg 100 I 79-34 51 1 2 2 Tetrachloroethane BRL _ ug/Kg I 100� - - 541-73 1 � 1 3 Dichlorobenzene _ BRL I ug/Kg 100 - _... 106-067 1 4 Dlchlorobenzene BRL .-. ug/Kg 100 { 1,2-Dichlorobenz.- BRL - ug/Kg -_ 100 _ I ----- -- — -- - ---- ' QC Surrogate Compound F Recovery-- QC Limits 1,2_DlchloroethanetJ4 -__ - _ _- 97% _ 1 70 130 % Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. �• r-�..�-1...�.�_ �_J.�f__I __ n� n__. ��nn ern •�_e_ r.___. n..____�_.n_-. ... r.n�nn GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: AB-7(3) Laboratory ID: 35636-07 Project: BlaineI5786.00 QC Batch ID: VG2-1785-E Client: Atlantic Environmental Sampled: 08-30-00 Container: fiOmL Glass Received: 08-30-00 Preservation: Methanol/Cool Analyzed: 09-06-00 Matrix: Soil Dilution Factor: 20 %Moisture: 9 Reporting,Limi It 71,71-8 Dichlorodifluorom-ethane —BRL ug/Kg 5,500 74-87-3 Chloromethane BRL ug/Kg 5,560- 75-01-4 Vinyl Chloride BRL ugil(g-—2,2-00- 74-83-9 Bromometh—ane BRL ug/Kg 5,500 75-00-3 Chloroethane— BRL ---uWK-9 ---5,-500 75-694 Trichlorofluoromethane BRL ug/Kg 1,100 75-354 1,1-Dichloroethene BRL ug/Kg —1,100 75-09-2 Methylene Chloride BRL ug/Kg 1,100 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 1,100 75-34-3 1,1-Dichloroethane —BRL ug/Kg 1,100 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 1,100 67-66-3 Chloroform BRL_____ 1,100 107-06-2 1,2-Dichloroetth—ane BRL 1,100 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 1,100 16-23-1 Carbon Tetrachloride BRL -u-g 1,100 78-87-5 -1,2-Dichloropropane .--BRL 1,100 79-01-6 Trichloroethene -- 1,300 ug/Kg 1,100 - — --hlororne 1,100 75-274 Brornodic tham BRL uwkg -110-6715-0-81 2--C--h1 I,m3- ethyl Vinyl-Ether d - BRL --u- g/Kg 5,500--- - 100 -5 cis Dichloropropene ____BRL 11100 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 1,100 79-00-1 - 1,1,1-Trichlom efha­ne----- BRLug/Kg 1,100 10 12448--1 Dilbrornotchlorome e-than BRL -uglK-9 1,100 1127-18-4 Tetrachloroethene 24,000 ug/Kg 1,1-00 108-90-7 Chlorobenzene BRL ug/Kg 1,100 75-25-2 Bromoform EFRL 9 1100 79-34-5 1,1,2,2 Tetrachloroethane BRL --_�__ug1Kg_ __1,1 00__ 541-73-1 1'3-Dichdorobenzene. BRL ug/Kg 1,100 • :10 9��64(;7 --1,4-Dichlorobenzene BRL ug/Kg 1,100 50 -- h1orob- nz ne- -- - ----- 9�5cl 1,2--Dic e e BRL ug/Kg 1,100 QC Surrogate Compound Recovery QC Limits Ll_,_&_Di,ch I oraaha ne--d, 97 % 70 130% Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update 111(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,it any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ' ANALYTICAL EPA Method 8021B Halogenated Volatile Organics by GC/ELCD ,I Field ID: AB-7(6) Laboratory ID: 35636.08 Project: Blaine/5786.00 QC Batch ID: VG2-1786-E Client: Atlantic Environmental Sampled: 08-30-00 ,i Container: 60mL Glass Received: 08-30-00 Preservation: Methanol/Cool Analyzed: 09-07-00 Matrix Soil Dilution Factor: 20 %Moisture 5 CAS NumbeF. Anal e;?s ', , ,7 3� Concentration ' Yr° i , Units',': Reporting Limit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 5,300 It 74-87-3 Chloromethane BRL ug/Kg 5,300 75-01-4 Vinyl Chloride BRL ug(Kg 2,100 74-83-9 Bromomethane - BRL ug/Kg 5,300 I 75-00-3 Chloroethane - BRL ug/Kg _ 5,300 75-69-4 Trichlorofluoromethane BRL ug/Kg 1,100 75-35-4 1,1-Dichloroethene BRL ug/Kg 1,100 75-09-2 Methylene Chloride BRL ug(Kg 1,100 i 15660.5 trans-1,2-Dichloroethen_e BRL ug/Kg 1,100 1 75-343 1,1Dichloroeth_ane _ _BRL _ ug/Kg_ _ 1,100 156-59-2 cis-1,2-Dichloroethene! ___ BRL_ ug/Kg _ 110, 0_ 67-66-3 Chloroform__ - BRL _ug/Kg 1,100 107-06-2 1,2-Dichloroethane BRL_ ug/Kg 1,100 71-55-6 1,1,1-Trichloroethan_e BRL ug/Kg 1,100 56-23-5 Carbon Tetrachloride _ _ BRL___ ug/Kg _ 1,100 ' 78-87-5 1,2-Dichloropropane_ _ BRL _ ug/Kg ' 1,100 79-01-6 Trichloroethene - BRL ug/Kg 1,100 75-27-4 Bromodichloromethane_ BRL_ ug/Kg 1,100 110-75-8 2-Chloroethyl Vinyl Ether _—_ BRL ug/Kg 5,300 10061-01-5 cis-1,3-Dichloropropene ;_ BRL up/Kg 1,100 10061-02-6 trans-1,3-Dichloropropene _ BRL ug/Kg-- 1,100 - 79_-00.5 1,1,2-Trichloroeth_ane _ _ BRL _ —4_ug/Kg __1,100_ '. 124-48-1 Dibromochloromethane _BRL _ ug/Kg 1,100_ 127-18-4 Tetrachloroethene _ 32,000 _ug/Kg 1,100 ------------- - ----------- 108-90-7 Chlorobenzene_ - 8RL_ _ugft _1,100 75-25-2 _ Bromoform - _ - BRL_ ug/Kg -1,100 79-34-5 1 1 2 2-Tetrachloroethane BRL ug%Kg 1,100 _ 541-73-1 _ 1 3 Dichlorobenzene BRL__ _ __ ug/Kg 1,Too 106-46-7 14Dlchlorobenzene BRL _ ug/Kg_ 1100 _ ,• 95=50.1 1 2 Dichlorobenzene- -_ BRL - —I u K 1,100 -� —� g/ B- QC Surrogate Compound — Recovery �— QC Limits ' 1,2-Dichloroethannr 97 % 70-130 % ---------------- -------- --- ----------------------------- Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. ,I ,I i 'l Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 li GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: AB-702) Laboratory ID: 35636-09 Project: Blaine/5786.00 QC Batch ID: VG2-1785-E Client: Atlantic Environmental Sampled: 08-30-00 Container. 60ml.Glass Received: 08-30-00 Preservation: Methanol/Cool Analyzed: 09-06.00 Matrix: soil Dilution Factor: I %Moisture: 3 CAS�Nili-nbiw,',," '.AFaIyW,, Reporting Limit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 _7487-3 —Ch—loromethane 75-01-4 Vinyl Chloride BRL ug/Kg 260 BRI. ug/Kg 100 74-83-9 —Fro—momethane BRL ug/Kg 260 wme 75-00-3 Chl®r&eth 260 4 fi BRL 75-6� Trichlor rometh,,,e BRLug/Kg 52 , — _�I-Dichlo­roethene BRL —ug/Kg — 75-354 /Kg 52 75-09-2 Methylene Chloride BRL ug/Kg 52 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 52 75-343 1,1-Di6_1oroWhane _ —--------------------------------------------------0� BRL K9 52 u� 156-59-2 cis-I.2-Dichloroethene ug/Kg 52 67-663 Chloroform BRL ug/Kg 52 107-06-2 1,2-Dichloroethane BRL ug/Kg 52 _71—.55-6 1,1,1--Trichloroethane _BRL _. - ug/Kg 52 5&23-5 Carbon Tetrachloride__ __BRL ugAkg_ 78-87-5 1,2-Dichloropropane BRL ug/Kg 52 79-01-6 Trichloroethene BRL _CgtKg 52 75-27-4 Bromodichloromethane BRL ug/Kg - 52 110-75-8_ 2-Chloroethyl Viny-l-Ether __r__Bk_L - ug/Kg 260100 61-01-5 cis-1,3-Dichloropropene BRL ug/K,g 52 10061-02-6 ttan s 1,IDN Lh�Iroppmop e n�e BRL_ ug/Kg 52 79-00-5 1,1,2-Trichloroethane BRL _M101<9 _52 124-48-1 D 1 brornoccWl o�rnWt In a�e BRL ug/Kg 5_2 U7_-184 etrachloroe-thene 670 ug/Kg 52 VMSIC�7 Ohlorobenzene 75-25-2 Bromofor--------- BRL ___52 m BRL 52 79-345----—1,1,2-,2-Tetrachloroethaneug/Kg -52 541-73-1 1,31-Dichlorobenzene- BRL ug/Kg n g 12 _F,_A�chkar�eue ug/Kg W_ 106-4&7 e L u K 1111 1 iKhlorobenzene BRL QC Surrogate Compound Recovery QC Limits 1,2-Dicllo,oethane-d4 98 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,-Update 111(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any,is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ti ANALYTICAL Project Narrative Project: Blaine/5786.00 Lab ID: 35636 Client: Atlantic Environmental Received: 08-30-00 A. Physical Condition of Samplko', This project was received by the laboratory in satisfactory condition. The sample(s) were received undamaged in appropriate containers with the correct preservation. 'I B. Project Documentation'. This project was accompanied by satisfactory Chain of Custody documentation, with the following amendment(s)or correction(s): 1. Samples 35636-01 through —09 were collected on 08-30-00 as indicated on the container labels. i C. Analysis of Sample(s) No analytical anomalies or non-conformances were noted by the laboratory during the processing of these sample(s). All data contained within this report are released without qualification. i r �i '� Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER 228 Main Street.P.O.Box 1200 Buzzards Bay,MA 02532 CHAIN-OF-CUSTODY RECORD ANALYTICAL Telephone(508)759-4441 AND WORK ORDER p FAX(508)759-4475 N- 42925 /Project Name: Firm: TURNAROUND ANALYSIS REQUEST 1�I..4-Ti.1E - ( romlu. a.mHawn.. aulm.meee. rre.k.e xu. Project Number: Address: O SJh176ARD(10 Business Days) £ I Mai same o.anloa,euas olku PRIORITY(5 Business Days) g !g e AA S 6E S'7Plo-O0 l3 Kca irc—�?J �� ❑ RUSH(RAN- S £ a (Rush requires Rush Authorisation Number) o 0 0 o n p Sampler Name: Ciry/State/Zip: gp /�•f `� /t nn A Please FAX WOES ❑NO 8 + l_ 'F W) / tt)?t/ :k(I'r cn7YD FAX Number: 8 && Project Manager: Telephone. BILLING o 0 0 0 0 0 0 § i /1� �� F R e v q q •CJi'd��.n%q[. ff'Z_�,z/��j Purchase Order No.: GWA Relerenrs No.: ° FF INSTRUCTIONS:Use separate line for each container(except replicates). � � @ g$ n F F s p 8 Sampling Matrix T a i $ $ i s { s pp € p{ o E§ gg Yp Container(s) Pmsarvatlon F..e v a v v v o v v v o F' SAMPLE a ° x LABORATORY yyy A, a IDENTIFICAMIN _ 4 a f NUMBER £ F : c rL w W - W > r = - s "s s ` = pp (Labuseonly) Pe F `s eS � d � df R $ 5 4 € 9Zyee 0 1�.§- - ¢ ; Aso D v osill v v v v o 0 o S v o 0 0 o v v a o v v a c v v o c c p sS S- s I Os 2 3 B'SO %IGO _T -3 ,) It — I is, I REMARKS y SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD 3UIU' — Ups fC i� p / Regulatory Program Project Specific OC NOTE:All samples submitted subjeM to Standard Terms aM Conditions on reverse hereof. V Il- y 7nui Yc"S) G Sale Drinking Water Act Many regulatory pro rams aM EPA methods❑MA DEP rm specific OC.Protect require proles Relinquished by Sampler Dale Time Received by: Receipt Temperature: ❑NPDES/Clean Water Act I pacific OC includes Sample Duplicates. Matrix Spikes,and/or Matrix Spike Duplicates.LaboratoryOC is Specify State: not project specific unless prearranged.Pmjeet specific C /a yS gArIPaz.Waste Char, samples are charged on a per sample basis.For water samples, Relinquished by: Date Tim e eecaived by: Shipping/AirbiA (3 t0 CMR 40) each MS,MSD and Sample Duplicatemcluires an additional bar Reportable Concentrations sample aliquot. ❑RCGW t O i PrOlM apednc OL Rpulred SeIMl4n qla sample Relinquished by: QdX$gall_ . 2 al 2 OSample MelkaM Cooler Serial O MA Dredge Disposal ❑Selened M tarn - Number: ❑NH❑RIpCT❑ME CMaM.Spike ❑pleat/use sample: Specity Category' QMdidt Spike DupM1taM Method of Shipment: ❑GWACopr ❑Express Mail❑Federal Express CUPS and O GROUNDWATER ANALYTICAL Quality Assurance/Quality Control A. Program Overview ' Groundwater Analytical conducts an active Quality Assurance program to ensure the production of high quality, valid data. This program closely follows the guidance provided by Interim Guidelines and Specifications for Preparing Quality Assurance Project Plans, US EPA QAMS-005/80 (1980), and Test Methods for Evaluating Solid Waste, US EPA, SW-846, Update III (1996). ' Quality Control protocols include written Standard Operating Procedures (SOPs) developed for each analytical method. SOPs are derived from US EPA methodologies and other established references. Standards are prepared from commercially obtained reference materials of certified purity, and documented for traceability. ' Quality Assessment protocols for most organic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. All samples, standards, blanks, laboratory control samples, matrix spikes and sample duplicates are spiked with internal standards and surrogate compounds. All instrument sequences begin with an initial calibration t verification standard and a blank; and excepting GGMS sequences, all sequences close with a continuing calibration standard. GC/MS systems are tuned to appropriate ion abundance criteria daily, or for each 12 hour operating period, whichever is more frequent. Quality Assessment protocols for most inorganic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. Standard curves are derived from one reagent blank and four concentration levels. Curve validity is verified by standard-recoveries within plus or minus ten percent of the curve. B. Definitions Batches are used as the basic unit for Quality Assessment. A Batch is defined as twenty or fewer samples of the same matrix which are prepared together for the same analysis, using the same lots of reagents and the same techniques or manipulations, all within the same continuum of time, up to but not exceeding 24 hours. Laboratory Control Samples are used to assess the accuracy of the analytical method. A Laboratory Control Sample consists of reagent water or sodium sulfate spiked with a group of target analytes representative of the method analytes. Accuracy is defined as the degree of agreement of the measured value with the true or ' expected value. Percent Recoveries for the Laboratory Control Samples are calculated to assess accuracy. Method Blanks are used to assess the level of contamination present in the analytical system. Method Blanks consist of reagent water or an aliquot of sodium sulfate. Method Blanks are taken through all the appropriate ' steps of an analytical method. Sample data reported is not corrected for blank contamination. Surrogate Compounds are used to assess the effectiveness of an analytical method in dealing with each sample matrix. Surrogate Compounds are organic compounds which are similar to the target analytes of interest in chemical behavior, but which are not normally found in environmental samples. Percent Recoveries are calculated for each Surrogate Compound. 1 ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Laboratory Control Sample Category: EPA Method 8012B-Halogenated QC Batch ID: VG2-1785-E Matrix: Soil Units: ug/Kg 7?"CAS`Number a'_ : 4,'Aria , '_ :Splkedt Measured ' ,Recovery :,QC Limrts 75-35-4 1 1 Dichloroethene 250 270 107% 70- 130% 79-01-6 Trichloroethene 250 270 108% 70- 130% 108-90-7 Chlorobenzene 250 280 112% 70- 130% u a1�=QC'SUROgate COlrlpOUrld,ry ": i� < q;a:',...aF.5 RECOVery„y ,m.._ 1,g, x,� ,. ..�.`�. ..a.'>.QC-limds : 1,2-Dichloroethane-da 102 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition, Update III(1996). Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 n_ GROUNDWATER ANALYTICAL Quality Control Report Method Blank Category: EPA Method 8021B- Halogenated QC Batch ID: VG2-1785-E Matrix: Soil T77�N%' ieporting Limit 75-71-8 Dichlorodifl uoromethane BRL 74-87-3 Chlorome-thane —URL— _ug1Kg 250 ug/Kg 250 75-014 Vinyl Chloride BRL ug/Kg 100 7483-9 Bromomethane EIR-L ug/Kg_ 250_ 75-00-3 Chl&roethwLe BRL ug/Kg 250 75-694 Trichlorofl uoromethane BRL — —ug/Kg 50 75-354 1,1-Dichloroethene BRL ug/Kg __50 75-09-2 Methylene Chloride — —_BRL ug/Kg 50 156-60-5 trans-1,2-Dichloroethene EIRL UIVI<g_­50 _ 75-34-3 1,1-Dichloroethane BRL ug/Kg 5-0 156-59_2_ds--1,2-Dichloroeth-ene BRL ug/Kg 50 67-66-3 Chloroform BRL ug/Kg 50 71-55-6 1,1,1-Trichloroethane BRL — ug/Kg 50 56-23-5 Carbon Tetrachloride BRL ug/Kg 50 107-06-2 1,2-Dichloroethan-e__ BRL ug/Kg 50 79-01-6 Trichlomethene __BRL 149/1<9_ 50 78-87-5 1,2-Dichloropropane BRL ug/Kg 50 75-274 Fro—mod i c h_10 r—om e-t In me BRL ug/Kg --50- 110-75-8 2-Chloroethyl Vinyl Ether __BRL ug/Kg 250 10061--01_5 cis—ij-D_ic_h®ropmp_ene___! EIRL—_ ug/Kg 50 16061-02-6 —trans--1,3--Dich—lor—opropene BRL ug/Kg 50 — 79-00-5 1,1,2-Trichloroethane BRL —_ ug/Kg_ 50 127-184 Tetrachloroethene BRL 12448-1 Dibromochloromethane BRL ug/.-Kg---.--50- 108-96--7 Chlorobenzene B-RL ug/Kg 50 75-25-2 Brornoform BRL —ug/Kg 5-0 79-34-5 1,1—,2,-2-fetra-chloroe—than�--- BRL_ --------- - g_ 50 541-73-1 1,3-Dichlorobenzene EIRL ____ ug/Kg 50 106-46-7 1,4-13ichloroben_i�ne MR-L _ ug/Kg 50 =1�YD 1 6 Lm ene BRL ug/Kg_ 50 QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethane-d4 97 % Method Reference: Test methods for Evaluating Solid Waste, US EPA, SW-846,Third Edition, Update III (1996). Analyle list as selected from list formerly specified by EPA Method 801 OB. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, it any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. if Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Certifications and Approvals CONNECTICUT, Department"of Health Services, PH-0586 Potable Water,Wastewaterfrrade Waste,Sewage(Effluent,and Soil PH,Conductivity,Acidity,Alkalinity,Hardness,Chloride,Fluoride,Ammonia,Kjeldahl Nitrogen,Nitrate,Nitrite,Orthophosphate,Total Dissolved Solids,Cyanide,Aluminum,Antimony Arsenic,Barium,Beryllium,Cadmium,Total Chromium,Hexavatent Chromium,Cobalt,Copper,Iron,Lead, Magnesium,Manganese,Mercury,Molybdenum,Nickel,Potassium,Selenium,Silver,Sodium,Thallium,Tin,Titanium,Vanadium,Zinc,Forgeable Halocarbons,Purgeable Aromatics,Pesticides,PCBs,PCBs in Oil,Ethylene Dibromide,Phenols,Oil and Grease. MAINE, Department of Human Services, MA103 Drinking Water Reciprocal certification in accordance with Massachusetts certification for drinking water analyzes. Waste Water Reciprocal certification in accordance with Massachusetts certification for waste water analyzes. MASSACHUSETTS, Department of Environmental Protection, M-MA-103 Potable Water Antimony,Arsenic,Barium,Beryllium,Cadmium,Chromium,Copper,Lead,Mercury,Nickel,Selenium,Thallium,Nitrate-N,Nitrite-N,Fluoride, Sodium,Sulfate,Cyanide,Turbidity,Residual Free Chlorine,Calcium,Total Alkalinity,Total Dissolved Solids,pH,Trihalomethanes,Volatile Organic Compounds,1,2-Dibromoethane,1,2-Dibromo-3<hloropropane,Total Coliform,Fecal Coliform,Hetemnophic Plate Count,E-Coli Non-Potable Water Aluminum,Antimony,Arsenic,Beryllium,Cadmium,Chromium,Cobalt,Copper,Iron,Lead,Manganese,Mercury,Molybdenum,Nickel,Selenium, Silver,Strontium,Thallium,Titanium,Vanadium,Zinc,pH,Specific Conductance,Total Dissolved Solids,Total Hardness,Calcium,Magnesium, Sodium,Potassium,Total Alkalinity,Chloride,Fluoride,Sulfate,Ammonia-N,Nitrate-N,Kjeldahl-N,Orthophosphate,Total Phosphorus,Chemical Oxygen Demand,Biochemical Oxygen Demand,Total Cyanide,Non-Filterable Residue,Total Residual Chlorine,Oil and Grease,Total Phenolics, Volatile Halocarbons,Volatile Aromatics,Chlordane,Aldrin,Dieldrin,DOD,ODE,DDT,Heptachlor,Heptachlor Epoxide,Polychlorinated Biphenyls(water),Polychlorinated Biphenyls(oil). ' MICHIGAN, Department of Environmental Quality Drinking Water Trihalomethanes,Regulated and Unregulated Volatile Organic Compounds by EPA Method 524.2;1,2-Dibromoethane,1,2-Oibromo-3. chloropropane by EPA Method 504.1 NEW HAMPSHIRE, Department of Environmental Services, 202798 Drinking Water Metals by Graphite Furnace,Metals by ICP,Mercury,Nilrite,N,Orthophosphate,Residual Free Chlorine,Turbidity,Total Filterable Residue,Calcium Hardness,pH,Alkalinity,Sodium,Sulfate,Total Cyanide,Insecticides,Herbicides,Base/Neulmis,Trihalomethanes,Volatile Organics,Vinyl Chloride,DBCP,EDB,Nitrate-N. Wastewater Metals by Graphite Furnace,Metals by ICP,Mercury,pH,Specific Conductivity,TDS,Total Hardness,Calcium,Magnesium,50dium,Potassium, Total Alkalinity,Chloride,Fluoride,Sulfate,Ammonia-N,Nitrate-N,Orthophosphate,TKN,Total Phosphorus,COD,BOD,Non-Filterable Residue, Oil&Grease,Total Phenolics,Total Residual Chlorine,PCBs in Water,PCBs in Oil,Pesticides,Volatile Organics,Total Cyanide. RHODE ISLAND, Department of Health, 54 Surface Water,Air,Wastewater, Potable Water,Sewage Chemistry: Organic and Inorganic Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GRO/ /NDWAT`/T Groundwater Analytical,Inc. 'I `/ 200 228 MaiP.O.Boxo Steel ANALYTICALBuzzards Bay,MA 02532 Telephone(508)759-4441 ,i FAX(508)759-4475 October 2, 2000 i. Mr. Eric Cardinal Atlantic Environmental 86 Faunce Corner Rd. r North Dartmouth, MA 02747 Project: Blaine/5786.01 Lab ID: 36208 Sampled: 09-25-00 Dear Eric: Enclosed are the Volatile Organics Analyses performed for the above referenced project. This project was processed for Priority One Week turnaround. This letter authorizes the release of the analytical results, and should be considered a part of this report. This report contains a project narrative indicating project changes and non-conformances, a brief description of the Quality Assurance/Quality Control procedures employed by our laboratory, and a statement of our state certifications. ' I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Should you have any questions concerning this report, please do not hesitate to contact me. ' Sincerely, Jonathan R. Sanford President I JRS/ss Enclosures I GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GGELCD Field ID: B-1 (4) Laboratory ID: 36208-01 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-27-00 Matrix: Sot, Dilution Factor: 1 +, % Moisture: 5 CAS Number~ ' s + . +»S' ":`i ids Vv£ ..r Concentration , .,; � „r,:Units Reportingiimit 75-71-8 DichlorodiFluoromethane BRL ug1Kg 260 Chloroehane gKg74-87-3 u 260 75-01-4 Vinyl Chloride BRL ug/Kg 110 7483-9 _ Bromomethane BRL ug/Kg 260 754)(5 Chloroethane BRL ug/Kg 260 75-694 _ TrichloroFluoromethane BRL _ ug/Kg 53 75-354 1,1-Dichloro_ethene BRL ug/Kg _ 53 75-09-2 Methylene Chloride BRL _ ug/Kg 5_3___ 156-60-5 trans-1,2-Dichloroethene 75-34 BRL _ ug/Kg 53 3 1,1-Dichloroethane BRL __ ug/Kg 53 156-59-2 —_ _cis-1,2-Dichloroethene 460 ug/Kg_ 53___ �. 67-66-3 __ Chloroform BRL ug/Kg 53 r --- ---�107-06-2 - I-1,2-0ichloroethane _ -BRL _ ug/Kg _53_ 71-55-6 1,1,1-Trichloroethane BRL _ ug/Kg 53 5_6-23-5 Carbon Tetrachloride _ BRL_ _ug/Kg 53 -_ 78-87-5 1,2-Dichloropropane _ BRL ug/K9 53 7941-6 �Trichloroethene__ 130 ug/Kg _ 5_3 --Ir-- - -chloro ---- 75-27-4 Bromodimethane BRL _ u- 9 53 110-75-8 r ------.2-Chloroethyl Vinyl Ether BRL ug/Kg I 260 Y ---- - 10061.OLS cis-1,3-Dichloropropene _-- -BRL -_-._ug/Kg � 53 10061-02-6 trans-1,3-Dichloropropene BRL_ _ ug/Kg 53__ 79-00-5 1,1,2-fHchIoroethane __BRL ug/Kg _53 124-48-1 Dibromochloromethane BRL_ ug/Kg 53 _127-18-44 1 Tetrachloroethene_ 108-90-7 I _Chlorobenzene _ BRL ug/Kg 53___ 75-25-2 Bromoform BRL ug/Kg 53 ' 79-345 -11,1,2,2-Tetrachloroethene BRL ug/Kg 53___ 541-73-1 1,3-Dichlorobenze_ne BRL ug/Kg 53 - 10_6_-06-7 � 1,4-Dichlorobnz eene . --B.RI — _ u K 53 95-50-1 1 1,2_Dichlorobenzene BRL ug/Kg 1 53 L—__ QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethane-d, 91 % _- 70- 130 % Method Reference: Test Methods lot Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update 111(1996). Analyte list as selected from list formerly specified by EPA Method 80108. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyte. Reporting limit is the lowest + concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: B-1 (71 Laboratory ID: 36208-02 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 Matrix Soil Dilution Factor. 2 %Moisture 4 ';.''CAS Number ' °,, z""Anal e+t , -a, �- . '^.y.� -`:.Concentration < ,!?. .=Units,.�i Repgrtinglimit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 520 74-67-3 Chloromethane BRL ug/Kg 520 75-01-4 Vinyl Chloride BRL ug/Kg 210 74-83-9 Bromomethane BRL _ ug/Kg 520 75-00-3 Chloroethane BRL ug/Kg 520 75-69-4 Trichlorofluoromethane -__BRL __ ug/Kg 100 75-35-4 1,1-Dichloroethene BRL ug/Kg 100 75-09-2 Methylene Chloride BRL_ ug/Kg 100 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 100 �I 75-34-3 1,1-Dic_hloroethane BRL ug/Kg _100 156-59-2_ cis-1,2-Dichloroethene _ 16.0 _ _ ug/Kg 100 67-66-3 _ .Chloroform - ----- -BRL _—_ _ ug/Kg 100_ 107-0-6 1,2-Dichloroethane __BRl_ - -_ -�_ ug/Kg 100_ 71-55-6 1,1,1-Trichloroethane ___ BRL -� ug/Kg 100 56-23-5 Carbon Tetrachloride BRL_ _ _ ug/Kg 100 _ jI-78-87-5 7,2-Dichloropropane _BRL____ _ ug/Kg 100 1 79-01-6 -�yJl-Trichloroethene 100 ug/Kg 100 __ _� Bromodichloromethane BRL _ up./Kg 100_ 110-_75-8 -- 2-Chloroethyl Vinyl Ether _-6Rt---_ - - ug/Kg - 520_ 10061-01-5 cis-1,3-D_ichloropropene I BRL ug/Kg 100 10061-02-6 - s-1,3-Dichloropropene BRL ug/Kg 100 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 100 124-48-1 Dibromochloromethane BRL ug/Kg 100 127-18-4 Tetrachloroethene 2,200 ug/Kg 100 _ 108-904 Chlorobenzene ug/Kg 100 75-25_2 — Bromoform BRL_ ug/Kg 100 79-34-5_ 1,1,2,2-Tetrachloroethane BRL_ _ ug/Kg 100 541-73-1 _1_3-Dichlorobenzene BRL_ ug/Kg _1_00 106-4_6-_7 _1,4-Dichlorob_enzene_-- BRL_. g/K_g 100 u 95-50-1 _ 1,&Dichlorobenzene _� BRL I ug/K9 100 QC Surrogate Compound Recovery_ QC limits 1,2-Dichloroethaned4 "/o_ 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III (1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any,is below reporting limit for analyte. Reporting limit is the lowest ' concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: B-6(3) Laboratory ID: 36208-16 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 �4 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 Matrix Soil Dilution Factor. 10 I %Moisture 10 . . „� �r, Concentration ,. �.-_ Repo,�fic7, q ?# Untts R _ifing omit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 2,800 74-87-3 Chloro a BRL ug/Kg 2,800 75-01-4 Vinyl—Chloride BRL ug/Kg 1,100 74-83-9 Bromomethane BRL ug/Kg 2,800 ' 75-00-3 Chloroethane BRL ug/Kg 2,800 75-69-4 Trichlorofluoromethane BRL ug/Kg 550 75-354 1,1-Dichloroethene BRL ug/Kg 550 75-09-2 Methylene Chloride BRL ug/Kg 550 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 550 l 75-34-3 1,1-Dichloroethane BRL ug/Kg 550 156-59-2 cis-1,2-Dichloroeth—en e 1,000 • ug/Kg 550 67-66-3 Chloroform BRL ug/Kg 550 i 107-06.2 1,2-Dichloroethane BRL ug/Kg 550 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 550 56-23-5 Carbon Tetrachloride BRL ug/Kg 550 78-87-5 1,2-Dichloropropane BRL ug/Kg 550 1: 79-01-6 Trichloroethene 1,500 _ ug/Kg 550 75-27-4 Bromodichloromethane BRL ug/Kg 550 110-75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 2,800 10061-01-5 cis-1,3-Dichlo top ropene BRL ug/Kg 550 - 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 550 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 550 12448-1 Dibromochloromethane BRL ug/Kg 550 227-184 T.etrachloroethene 26,000 ug/Kg 550 108-90-7 Chlorobenzene BRL ug/Kg 550 ' 75-25-2 Bromoform BRL ug/Kg 550 79-34-5 1,1,2,2-T_etrach I o roroethane BRL ug/Kg 550 541-73-1 1,3-Dichloro_benzene _ BRL ug/Kg 550 106-46-7 _1,4-D_ichlorobenzene BRL ug/Kg 550 i 95-50-1 i 1,2-Dichlorobenzene BRL ug/Kg 550 QC Surrogate Compound Recovery QC Limits - 1,2_Dichloroethane-d4 95 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. 41'1 �I �� Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 ' GROUNDWATER ANALYTICAL EPA Method 8021E ' Halogenated Volatile Organics by GGELCD Field ID: B-6(6) Laboratory ID: 36208-17 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-27-00 ' Matrix: Soil Dilution Factor 2 %Moisture 11 $t AS.Nymber 110Mts t?r,'_Analyte ZJ'r :; eo- 7EN, >' %.Concentration .' s }) KNI Umtsv;r"Reporfingt mit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 560 74-87-3 Chloromethane BRL ug/Kg 560 75-01-4 Vinyl Chloride BRL ug/Kg 220 74-83-9 Bromomethane BRL ug/Kg 560 ' 75-00-3 Chloroethane BRL ug/Kg 560 75-69-4 Trichlorofluoromethane BRL ug/Kg 110 75-35-4 1,1-Dichloroethene BRL ug/Kg 110 75-09-2 Methylene Chloride BRL ug/Kg 110 156-60-5 trans-1,2-Dichloroethene BRL ug(Kg 110 75-34-3 1,1-Dichloroethane BRL ug/Kg 110 156-59-2 cis-1,2-Dichloroethene 250 ug/Kg 110 ' 67-66-3 Chloroform BRL ug/Kg 110 107-06-2 1,2-Dichloroethane BRL ug/Kg 110 71-55-6 1,1,1-Trichloroethane BRL ulp Kg 110 56-23-5 Carbon Tetrachloride BRL ug/Kg 110 78-87-5 1,2-Dichloropropane BRL ug/Kg 110 79.01-6 Trichloroethene 290 ug/Kg 110 ;�5-2—7-417 Bromodichloromethane BRL ug/Kg 110 � _7g 560- -10-75-8- _ - ---2-Chloroethyi-Vinyl--pro Ether p-- BRL u-/Kg --10061-0--1-5- - cis--1,3--Di-chloropropene BRL ug/- K K — g 11-0 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 110 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 110 124-48-1 —Iibromochloromethane BRL ug/Kg 110 127-18-4 . Tetrachloroethene 4,300 ug/Kg 110 108-90-7 ChIorobenzene BRL ug/Kg 110 75-25_2_ Bromoform _ BRL ug/Kg 110 79-34-5 1,1,22-. TeIrachloroethane BRL ug/Kg 110 541-73-1 1,3-Dichlorobenzene BRL ug/Kg_ 110 -- ro - 106-46-7 1,4-Dichlobenzene BRL ug/Kg_ _710 1,2-13ichlorobenzene _ BRL ug/Kg 110 QC Surrogate Compound - Recovery QC Limits 1,2-Dichloroethaned4 94 % 70- 130% Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SWA46,Third Edition, Update III (1996). Analyte list as selected from list formerly specified by EPA Method 80108. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyze. Reporting limit is the lowest i concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 r� ' GROUNDWATER ' ANALYTICAL EPA Method 8021 B ' Field ID: Halogenated Volatile Organics by GC/ELCD B-6(12) Laboratory ID: 36208-18 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E ' Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-27-00 Matrix: Soil Dilution Factor 1 ' %Moisture 2 (AS'tlUmber rx F,,.n .Aflal C a, L'`„rayn rk't CO11CCntratlOn :%: Relwrtinglimit 75-71-8 DlChlorodlfluOrOmethane BRL ug/Kg 260 ' 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 260 ' 75-00-3 Chloroethane BRL ug/Kg 260 75-69-4 Trichlorofluoromethane BRL ug/Kg 51 75-35-4 M-Dichloroethene BRL ug/Kg 51 75-09-2 Methylene Chloride BRL ug/Kg 51 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 51 75-34-3 7,1-Dichloroethane 8RL ug/Kg 51 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 51 ' 67-66-3 Chloroform BRL ug/Kg 51 107-06-2 1,2-Dichloroethane BRL ug/Kg 51 71-55-6 1,1,1-Trichloroethane —BRL ug/Kg 51 56-23-5 C_arbon_Tetrachloride ___BRL_ ug/Kg 51 ichloropropane BR t 78-87-5 1,2•DL ug/Kg 51 79-01-6 Trichloroethene _ BRL ug/Kg 51 75-27-4 Bromodichloromethane _BRL ug/Kg 51 ' _110-75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 260 -. - - --- -- ---cis-1- ,3-Dich- -- --- -- -------- ---� g - 10061-01.5 loropropene BRL u K 51 10061-02-6 trans•1,3-Dichloropropene _BRL ug/Kg . 51 ' 79-00-5 - 1,1,2-Trichloroethane BRL ug/Kg 51 124-48-1 Di brom_o_chloromethane BRL ug/Kg 51 127-18-4 Tetrachloroethene 160 ugtKg 51 108-90.7 Chlorobenzene BRL ug/Kg 51 ' 75-25-2 Bromoform __ BRL ug/Kg 51 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 51 541-73-1 1,3-Dichlorobenzene BRL ug/K_g 51 ' 106-46,7 1,4_Dichlorobenzene BRL — ug/Kg 51 95-50-1 1,2_Dichlorobenzene BRL ug/Kg 51 QC Surrogate Compound Recovery QC Limits ' 1,2-Dichloroethane d, 101 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. ' Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. 1 1, ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL r EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: B-7(3) Laboratory ID: 36208-19 Project: Blaine/5786.01 QC Batch ID: VG2.1798-E Client: Atlantic Environmental Sampled: 09-25-00 t� Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-27-00 • Matrix: soil Dilution Factor: 2 % Moisture: 7 75-71-8 DichlorodiFluoromethane BRL ug/Kg 540 74-87-3 Chloromethane BRL ug/Kg 540 'i 75-01-4 Vinyl Chloride BRL ug/Kg 220 74-83-9 Bromomethane BRL ug/Kg 540 75-00-3 Chloroethane BRL ug/Kg 540 75-694 Trichlorofluoromethane BRL ug/Kg 110 75-35-4 1,1-Dichloroethene BRL ug/Kg 110 75-09-2 Methylene Chloride BRL ug/Kg 110 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 110 75-34-3 1,1-Dichloroethane BRL ug/Kg 110 156.59-2 cis-1,2-Dichloroethene BRL ug/Kg 110 67-66-3 Chloroform BRL ug/Kg 110 ' 107-06-2 1,2-Dichloroethane BRL ug/Kg 110 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 170 56-23-5 Carbon Tetrachloride BRL ug/Kg 110 78-87-5 1,2-Dichloropropane BRL ug/Kg 110 79-01-6 Trichloroethene BRL ug/Kg 110 75-274 Bromodichloromethane BRL ug/Kg 110 ' 110.75-8 2-Chloroethyl Vinyl Ether _BRL ug/Kg 540 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 110 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 110 - ' 79-00-5 1,1,2Tririchloroethane BRL ug/Kg 110 12448-1 Dibromochloromethane BRL ug/Kg 110 127-184 Tetrachloroethene 2,800 ug/Kg 110 108-9_0.7 � Chlorobenzene BRL ug/Kg 110 ' 75-25-2 Bromoform _ BRL ug/Kg _110 79-34-5 1,1,2,2-Te_trac_hloroethane BRL ug/Kg 110 541-73-1 1,3-Dichlorob_enzene BRL ug/Kg 110 ' 10_64 -_ 1,4-Dichlorobenzene — BRL ug/Kg 110 95-50-11-1 1,2-Dichlorobenzene BRL ug/Kg 110 QC Surrogate Compound Recovery - QC Limits ' -1,2-0ichloroethanedd _ _ 97 % 70- 130% Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,if any, is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. 'I Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 ' GROUNDWATER ' ANALYTICAL EPA Method 8021 B ' Halogenated Volatile Organics by GC/ELCD Field ID: B-7(8) Laboratory ID: 36208.20 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E Client: Atlantic Environmental Sampled: 09-25-00 t Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09.27-00 ' M atrix: Soil Dilution Factor 1 Moisture 4 CAS Number'e fi.?� i ,r1' t :Anal e . 'r 'r'`. a ";' �' u r r'..4 �t.; .._ .. a._ Concentration ..,� f .,, Units +,`:;Reporting Limit ' 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 260 ' 75-00-3 Chloroethane BRL ug/Kg 260 75-69-4 Trichlorofluoromethane BRL ug/Kg 52 75-354 1,1-Dichloroethene BRL ug/Kg 52 ' 75-09-2 Methylene Chloride BRL ug/Kg 52 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 52 75-34-3 1,1-Dichloroethane BRL ug/Kg 1 52 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 52 67-66-3 Chloroform BRL ug/Kg 52 107-06-2 1,2-Dichloroethane BRL ug/Kg 52 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 52 t 56-23-5 Carbon Tetrachloride BRL ug/Kg 52 78-87-5 1,2-Dichloropropane BRL ug/Kg 52 7941-6 Trichloro_ethene _ BRL ug/Kg 52 75-27-4 Bromodichloromethane BRL ug(Kg 52 11WS-8 2{hloroethyl Vinyl Ether BRL up/Kg 260 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 52 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 52 ' 79-0_0-5 1_1,2-Trichloroethane BRL ug/Kg 5_2_ 12448-1 Dibromochloromethane BRL ug/Kg 52 127-184 Tetrachloroethene 52 ug/Kg 52 108-90-7 Chlorobenzene BRL ug/Kg 52 ' 75-25-2 Bromoform BRL ug/Kg 52 79-34-5 1,1,2,2-Tetrachloroethane _ _BRL ug/Kg 52 _541-73-1 1,3-Dichlorobenzene BRL ug/Kg 52 ' 1_06-46-7 1,4-Dic_hlorobenzene BRL ug/Kg _52 95-50-1 1,2-Dichlorobenzene BRL ug/Kg 52 QC Surrogate Compound Recovery QC Limits ' 1,2-Dichloroethaned4 -_ 102 % 70- 130% Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update 111 (1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. ' Report Notations: BRL Indicates concentration, it any,is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. 1 ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL 1) EPA Method 8021B Halogenated Volatile Organics by GC/ELCD Field ID: B-7(12) Laboratory ID: 36208-21 • Project: Blaine/5786.01 QC Batch ID: VG2-1798-E i Client: Atlantic Environmental Sampled: 09-25-00 Container. 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-27-00 Matrix Sod Dilution Factor: 1 %Moisture 5 _-. 9a�, a,, - - - -. ,, =,'r.Concentratton T7 Und; : - Reporting Limit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 7487-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg - 110 74-83-9 Bromomethane BRL ug/Kg 260 75-00-3 Chloroethane BRL ug/Kg 660 75-69-0 Trichlorofluoromethane BRL ug/Kg 53 75-354 1,1-Dichloroethene BRL ug/Kg 53 75-09-2 Methylene Chloride BRL ug/Kg 53 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 53 75-34-3 1,1-Dichloroethane BRL ug/Kg 53 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 53 67-66-3 Chloroform BRL ug/Kg 53 107-06-2 1,2-Dichloroethane _ BRL ug/Kg 53 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 53 56-23-5 Carbon Tetrachloride BRL ug/Kg 53 78-87-5 1,2_Dichloropropane _BRL ug/Kg 53 79-01-6 Trichloroethene BRL ug/Kg 53 75-27-4 Bromodichloromethane BRL ug/Kg 53 ' 110-75-8 2-Chloroethyl Vinyl Ether _BRL ug/Kg 260 10061-01-5 cis-1,3-Dichloropropene BRL ug/K_g 53 10061-02-6 Trans-1,3-Dichloropropene BRL ug/Kg 53 - 79-00.5 1,1,2-Trichloroethane BRL ugfK9 53 ' 12448-1 Dibromochloromethane BRL ug/Kg 53 127-18-4 _Tetrachloroethene — 140 ug/K_g 53 106-90-7 Chlorobenzene _ BRL ug/Kg 53 7525-2 —Bromoform BRL ug/Kg 53 79-34-5 10,2,2-Tetrachloroethane BRL ug/Kg 5_3 541 73-1 1 3 Dichlorobenzene BRL u'Kg 53 10646-7 _ 1 4 Dichlorobenzene BRL _ ug/Kg 53 95-50.1 1 2 Dichlorobenzene _ BRL _ ug/Kg 53 QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethane-d4 103 % 70- 130 0/ ' Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. ' Report Notations: BRL Indicates concentration,if any,is below reporting limit for anaMe. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. 1I 'f '� Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Project Narrative Project: Blaine/5786.01 Lab ID: 36208 Client: Atlantic Environmental Received: 09-25-00 A Physical Condition of Sample(s) 1} This project was received by the laboratory in satisfactory condition. The sample(s) were received undamaged in appropriate containers with the correct preservation. 1! _ B.',Project Documentation 1' This project was accompanied by satisfactory Chain of Custody documentation. The sample container label(s) agreed with the Chain of Custody. C. Analysis of Sample(s) 1� No analytical anomalies or non-conformances were noted by the laboratory during the processing of these sample(s). All data contained within this report are released without qualification. 1. 1 1 1 1) . Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 228 Main Street,P.O.Box 1200 GROUNDWATER Buzzards Bay,MA02532 CHAIN-OF-CUSTODY RECORD Telephone(508)759-4441 AND WORK ORDER N9 '42928 ANALYTICAL FAX(508)759-4475 Project Name: Firm: TURNAROUND• ANALYSIS REQUEST n ` Izic soles sminksou P.a4N.ra Ce. Max. PN^I^^ o Nn' -eenenl Ms.., elver p STjF yDARD(10 Business Days) a wnl. Project Number: AtltlrZc^r.:/, p, FIORITY(5 Business Days) - @ of 1 ✓ /`FZMSI'O.J �� O RUSH(RAN- 1 a' 41, a (Rush requires Rush Authorization Number) o gg o a oo - S� o0 Sampler Name: City/State/Zip: 3 Please FAX ES ❑NO (G:r' Or &0/12 -D /fill" OZ7?po FAX Number: l -2-J'r33 Project Manager: Telephone: ILLING v o 0 o a o o Elk £ �° Sjr$� �AQD SAL �S Z_ G z�.Yj Purchase Order No.: GWA Reference No.. o I 4$ n A a # INSTRUCTIONS:Use separate fine for each container(except replicates). E +° - ' i y Y o 5 ° E n O C O O Sampling Matrix Type Containers) Preservation nnm.a z 0 J 4 J p O O s � SAMPLE - a i d s LABORATORY ,q. $ i 5` a ; e Sa}' $ a a ; E $ IOENRRCATION = : `a' - e e a a s� 9 $ € Ce j F ; II 3 a s m :n c e a a i C Ay (Lab Use Only m i �L z' `� c Y O u x S S a _ a t ! a g v e a s sa = 4 y n > g OB is3 as p = a3 a aid aA a = � `610 0 0 0 0 0 o c o o a a c o 0 0 0 o c 6 0 0 _ c o c o c o a c o D a OtK -1 y 1 oypp u OE t I tMD 6 -- G 2T —2 2 O5D pJ' lostFPfr-- 6 3 Iz v N-1 10 b N I Il N IO REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program Project Specific OC NOTE:All samples submitted subject to Standard Terms and Conditions on reverse hereof. L LL ❑Sale Drinking Water Ad Man regulatory programs and EPA methodsr require project Relinquished Sampler: Date Time Rise d Receipt Temperature: ❑MA DEPForm y ry eq Oi j ^9 y p peralure: specific Spikes, Project specific OC includes udes Sample Laboratory ale". ❑NPDESState: Water Act Matrix Spikes,andlm less p Spike Deprloatise Laboratory DC b Specify Stale: samples protect a e charged specific n a per sample basis. For water OC ❑R az.Waste Char. each MS.MSDa and Sample apersample requires alertionlsamples. Relinquished by: Dale Time eived by: Number: A MCP 13t0 CMq 40) each MS.MSD and Sample Duplicate requires an additional Number: Reportable Concentrations sample aliquot. ❑RCGW-1 ❑RC Project Specific ore Required selection of QC Sample Relinquished by: Date Time Received by Laboratory: Custody Seal/ ❑RCGW-2 OWCS 2 ❑Sample Duplicate O SeNcbd by laboratory Cooler Serial Number: ❑MA Dredge Disposal ❑Matrix Spike O Pleax use sample: ❑NH0 RI 0 CT 0 ME Method of Shipment: ❑GWA Couri Express Mail❑Federal Express Specify Category: OMalex Spike Duplicate 0 UPS and❑ 228 Main Street,P.O.Box 1200 GROUNDWATER Buzzards Bay,MA02532 CHAIN-OF-CUSTODY RECORD Telephone(508)759-4441 ANDWORKORDER N2 42929 ANALYTICAL FAX(508)759-4475 Project Name: Firm: TURNAROUND ANALYSIS REQUEST _� 6Lz}. C' volmta• s.mn•um.• R •e ce• a...y ekwe tie. xar. mwnt cn.mmn en.. rif ❑STANDARD(70 Business Days) ren.el wun Project Number: Address: /' t-FIRIORITY(5 Business Days) J n3'�'CI ,J / ❑ RUSH(RAN- I �g,`^�i-TU fRush requires Rush Authorization Numbed v ° O c .R o O Sampler Name: City I State/Zip: # , Please FAX YES ❑NO C FAX Number Project Manager: Telephone: BILLING o o o o g £ 3 $ 3 Cyo ^ 1 �y2_G�1 Purchase Order No.. GWA Reference No.: o v g - g f 1 = S $ , - 1 1 ° a INSTRUCTIONS:Use separate line for each container(except replicates). $ $ $ s e $ = e E e o +� o g Sampling Matrix Type Contalner(s) Preservation Rana FH ° ° ° ° ° ° o o o v 5 c ds a 4 SA E a a $ a' 'g e' a LABORATORY - g 9a § tln a ; 53' i d� n{ IpEITRCAItON _ a 5 a v m r 5 e = f (Lab Use On z yNUMBER s- s € a a 8 $ a 5ao a 4 = S s 5 g �.3 $ , y g �2Up7(� ° O v o v n ° c o 0 0 'z 12.2 -S mo -5- iS ) 10 (b 3 N g- E Is --) tat n E� REMARKS/SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program Project Specific QC NOTE:All samples submitted subject to Standard Terms and Conditions on reverse hereof. p Sale Drinking Water Act Many regulatory programs and EPA methods require project Relinquishedb Sam Date Time v by: Receipt Temperature: ❑MA DEP Form specific OC.Project specific OC includes Sample Duplicates, / ❑NPDESIClean Water Act Matrix Spikes.andlor Matrix Spike Duplicates.Laboratory OC is �:.` 1 ,0 6- Specify Stale: not project specific unless prearranged.Protect speufic OC •RCRArHaz.Waste Char. samples are charged on a per sample bases.For water samples, Relinquished f Date Tm ecaived by: ShippinglAirblll ❑MA MCP(310 CMR 40) each MS.MSD and Sample Duplicate requires an additional Number: Reponable Concentrations sample aliquot. ❑RCGW I 0 RCS-t Proles Specific OC Required Selection at OC Semple Relinquished by: Date Time Received by Laboratory: Custody Seat/ ❑RCG W 2❑RCS.2 Cooler Senal O Sample Duplicate D selected by bboratory QC�>Ll �, i•, Number: ❑MA Dredge Disposal D Matrix Spike ❑Please use sample: ❑NH❑RI❑CTQ ME Method of Shipment ❑UPS Coyyfa�aer OExpress Mail Federal Express Specify Category: ❑Matrix Spike Oupliale ❑UPS flHantl 0 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD ■i Field ID: B-1 04) Laboratory ID: 36208-03 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 Matrix: Soil Dilution Factor: 1 %Moisture: 13 CAS_Number; . Concentiahon i+ Unitsh RegortingLimit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 290 74-87-3 Chloromethane BRL ug/Kg 990 75-014 Vinyl Chloride BRL ug/Kg 110 74-83-9 Bromomethane BRL ug/Kg 290 75-00-3 Chloroethane BRL ug/Kg 290 75-69-4 Trichlorofluoromethane BRL ug/Kg 57 75-354 1,1-Dichloroethene BRL ug/Kg 57 75-09-2 Methylene Chloride BRL ug/Kg 57 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 57 _ 75-34-3 1,1-Dichloroethane BRL ug/Kg 57 15659-2 cis-1,2-Dichloroethene BRL_ ug/Kg 57 67-66-3 Chloroform BRL ug/Kg 57 t 107-06-2 1,2-Dichloroethane BRL _ ug/Kg 57 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 57 56.23-5 Carbon Tetrachloride _8RL ug/Kg 57 78-87-5 1,2-Dichloropropane_ __BRL _ ug/Kg 57 79-01-6 Trichloroethe_ne_ _ ____BRL_____ ug/Kg _ _ 57 75-27-4 m Broodichloromethane BRL _ ug/Kg 57 110-75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 290 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 57 160 1-0 2-6 trans-1,3-Dichloropropene BRL ug/Kg 57 _79-00-5 1,1,2-Trichloroethane_ BRL ug/Kg 57 ' 124-48-1 Dibromochloromethane WRI. ug/Kg 57 127-184 Tetrachloroethene 2.40 ug/Kg 57 108-90-7 Chlorobenzene _ BRL ug/Kg 57 75-25-2 Bromoform _ BRL ug/Kg 57 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 57 541-73-1 1,3-Dich_lorobenzene BRL ug/Kg 57 106-46-7 _1,4-Dichlorobenzene BRL_ uI Kg_ 57 ' 95-50-1 1,2-Dichloro_benzene _ BRL_ ug/Kg 57 QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethane-d4 99 % 70- 130 % ' Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III (1996). Analyle list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. r Groundwater Analytical, Inc., P.O. Box 1200,228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ' ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: B-2(3) Laboratory ID: 36208-04 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: MethanoUCool Analyzed: 09-26-00 Matrix: Soil Dilution Factor 4 ' %Moisture 7 „CAS.Number ', 75-71-8 Dichlorodifluoromethane BRL ug/Kg 1,100 ' 74-87-3 Chloromethane BRL ug/Kg 1,100 75-01-4 Vinyl Chloride BRL ug/Kg 430 74-83-9 Bromomethane BRL ug/Kg 1,100 75-00.3 Chloroethane BRL ug/Kg 1,100 75-694 Trichlorofluoromethane BRL ug/Kg 210 75-354 1,1-Dichloroethene BRL ug/Kg 210 75-09-2 .Methylene Chloride BRL ug/Kg 210 t 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 210 75-34-3 1,1-Dichloroethane BRL ug/Kg 210 156-59-2 cis-1,2-Dichloroethene WE ug/Kg 210 ' 67-66-3 Chloroform BRL — - ug/Kg 210 107-06-2 1,2-Dichloroethane BRL_ ug/Kg 210 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 210 56-23-5 Carbon Tetrachloride ug/Kg 210 78-87-5 1,2-Dichloropropan_e BRL ug/Kg 210 79-01-6 Trichloroethene_ _ _ BRL ug/Kg 210 75-274 Bromodichloromethane BRL ug/Kg 210 110-75-8 2-Chloroethyl Vinyl Ether BRL —� ug/Kg 1,100 10061-01-5 cis-1,3-Dichlor_opropene _ BRL ug/Kg 210 10061-02-6 trans-1,3-Dichloropropene BRL F ug/Kg 210 79-00-5 1,1,2-Trichloroethane BRL _ ug/Kg 210 12448-1 Dibrom_ochloromethane BRL ug/Kg 210 127-18-4 Tetrachloroethene 6,700 ug/Kg 210 108-90-7 Chlorobenzene BRL ug/Kg 210 ' 75-25-2 Bromoform _ BRL Ug/Kg 210 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 210 541-73-1 1,3-Dichlorobenzene BRL ug/Kg 210 ----- -- - -------- - ---- 106-46-7 1,4-Dichlorobenzene• BRL ug/Kg _ 210_ 95-50.1 1,2-Dichlorobenzene -_ BRL ug/Kg 210 —QC Surrogate Compound Recovery QC Limits L_1,2_Dichloroethaned4 97 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition,Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any,is below reporting limit for analyse. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 A. t GROUNDWATER ANALYTICAL EPA Method 8021B Halogenated Volatile Organics by GC/ELCD Field ID: B-2(6) Laboratory ID: 36208-05 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 Matrix: Soil Dilution Factor: 10 %Moisture 8 '!,CAS;Numberl„ r:ta"',' rn4;�;`;/Anal e„i r"i!`."? s `'bi.�f. COnCentrdtmn^s `'Fk S:yru �,k . ,.. . .zr.� mts, , F.Reportidg limit ' 75-71-8 Dichlorodifluoromethane BRL ug/Kg 2,700 74-87-3 Chloromethane BRL ug/Kg 2,700 .. 75-014 Vinyl Chloride BRL ug/Kg 1,100 7483-9 Bromomethane BRL ug/Kg 2,700 75-00-3 Chloroethane BRL ug/Kg 2,700 75-694 Trichlorofluoromethane BRL ug/Kg 540 75-354 1,1-Dichloroethene BRL ug/Kg 540 t 75-09-2 Methylene Chloride BRL ug/Kg 540 156-60-5 trans-1,2-bichlOrOethene BRL ug/Kg 540 75-343 1,1-13ichloroethane BRL ug/Kg 540 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 540 ' 67-66-3 Chloroform BRL ug/Kg 540 107-06-2 1,2-Dichloroethane BRL ug/Kg 540 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 540 56-23-5 Carbon Tetrachloride -- BRL ug/Kg 540 2 78-87-5 1, Dichloropropane BRL ug/Kg 540 79-01-6 7rnchIoroethene BRL _ ug/Kg 540 75-274 Bromodichloromethane _B_RL ug/Kg 540 110-75-8 2-Chloroethyl Vinyl Ether _BRL ug/Kg 2,700 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 540 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 540 - 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 540 124-48-1 Dibromochloromethane BRL ug/Kg 540 127-18 4 Tetrachloroethene 9,900 ug/Kg 540 108-90-7�Chlorobenzene BRL ug/Kg 540 _75-25-2 Bromoform BRL ug/Kg 540 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 540 541-73-1 1,3-Dichlorobenzene _BRL ug/Kg 540 ' 106-06-7_— 1,4-Dichorobenzene _BRL _ ug/Kg _540 95-50.1 1,2-Dichlorobenzene BRL I ug/Kg 540 QC Surrogate Compound Recovery QC Limits ' ( 1,2-Drchloroethane-d4 99 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition,Update 111(1996). Analyze list as selected from list formerly specified by EPA Method 80108. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. ' Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 1�. GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GOELCD Field ID: B-4(2) Laboratory ID: 36208-10 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 ' Matrix: Soil Dilution Factor: 1 %Moisture 9 CAS Number Y K,,,„ ;;'Anal e°, : fY - ; ; ," Concentration;w . ,,, . Units.. .:' RepoRing:Llmit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 280 74-87-3 Chloromethane BRL _ ug/Kg 280 75-014 Vinyl Chloride BRL ug/Kg 110 74-83-9 Bromomethane BRL _ ug/Kg 280 75-00-3 ISIoroethane BRL ug/K9 280 75-69-4 TrichIorofluoromethane _ _ B_RIL ug/Kg 55 75-35-4 1,1-Dichloroethene BRL ug/Kg 55 75-09-2 Methylene Chloride BRL ug/Kg 55 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 55 75-34-3 1,1-Dichloroethane BRL ug/Kg 55 156-59-2 cis-1,2-Dichloroethene _BRL ug/Kg _ 55 ' 67-66-3 Chloroform_ BRL ug/Kg 55 107_-06-2 1,2-Dichloroethane ___BRL ug/Kg 55 71-55-6 _ 1,1,1-Trichloroethane BRL___ _ ug/Kg 55 56123-5 _ Carbon_Tetrachloride ____ BRL_____ _ ug/Kg 55 ' 78-87-5 1,2-Dichloropropane - _ BRL _ ug/Kg 55 79-01-6 _ Trichlo_roethen_e _ _BRL _ T ug/Kg _55 - - 75-274 Brom odichlorometh—an e BRL_ ___._J_ug/Kg _ 55 110-75-8 2=Chloroethyl Vinyl Ether BRL ug/Kg 280 10061-01-5 cis-1,3-Dichloropropene BRL I ug/Kg 55 -t---— 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 55 - 79-00-5 1,1,2-Trichloroethane BRL ug/Kg_ 55 124-48-1 DibromochIoromethane BRL ug/Kg 55 127-18-4 Tetrachooroethene BRL ug/Kg 55 108-90-7 C_hlorobenzene _BRL ug/Kg 55 _75-25_2 Bromoform BRL _ ug/Kg 55 79-34-5 1,1,2,2-Tetrachloroethane BRL _ ug/Kg 55 541-73-1 1,3-Dichlorobenzene _BRL ug/Kg 55 ' 106-46-7 1,4-Dichlorobenzene _ BRL — u�Kg 55 95-50-1 1,2-Dichlorobenzene BRL u K 55 QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethane-da � _ 100 % _ _ _�_ 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 80108. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD ■� Field ID: B4(4) Laboratory ID: 36208-11 Project: Blaioe/5786.01 QC Batch ID: VG2-1798-E Client: 'Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 Matrix: Soil Dilution Factor. 1 %Moisture 9 a CASNumbera Anal e. Units,`..> RepoNng-Limit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 270 7487-3 Chloromethane I _ BRL ug/Kg 270 j 75-01-4 Vinyl Chloride BRL ug/Kg 110 7483-9 Bromomethane BRL ug/Kg 270 75-00-3 Chloroethane BRL ug/Kg 270 75-69-4 Trichlo_rofluoromethane BRL ug/Kg 55 75-35A 1,1-Dichloroethene BRL ug/Kg 55 75-09-2 Methylene Chloride _ BRL ug/Kg 55 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 55 75-343 1,1-Dichloroethane BRL ug/Kg _ 55 156-59-2 cis-1,2-Dichloroethene __ _BRL ug/Kg _ 55 67-66 3 Chloroform_ _ BRL ug/Kg 55 107-06-2 1,2-Dichloroethane _ _BRL ug/Kg 55 71-55-6 1,1,1Trichloroethane 6RL _ ug/Kg 55 56-23-5 Carbon Tetrachloride _BRL ug/Kg 55_ 78-87-5 1,2-Dichloropropane _ _ _BRL _ ug/Kg 55 79_-01-6 _Trichloroethene_ _ _ BRL_ ug_/Kg _ 55 75-27-4 Bromodichloromethane BRL ug/Kg 55 ---------- ----- 110-75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 270 10061-01-5 _ds 1,3-Dichlo_ropropene _ BR_L___ _ _ug/Kg _55 10061-02-6 trans-1,3-_Dichloropropene BRL ug/Kg 55 79-00.5 1,1,2-Trichloroethane BRL_ ug/Kg 55 124418-1 Dibromochloromethane BRL ug/Kg 55 127-18-4 _ChlTetrachloroethene _ BRL ug/Kg 55 _70_8-90-7_ orobenzene BRL_ _ ug/Kg 75-25-2 Bromofor_m_ __ BRL _ _ug/Kg _55 79-34-5 1,1,2,2-Tetrachloroethane _BRL _ug/Kg—_ 55 541-73-1 1,3-Dichl_robenzene BRL ug/Kg 55 106-46-7 - _ 1,4-Dich_lorobenze_ne ____ BRL __ u9/K9 55 ben 95-50-1 1,2-Dichlorozene _BRL ug/Kg 55 QC Surrogate Compound J Recovery QC Limits 1,2-Dichloroethane-d,_ __ -__ 1 96 % -__--70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 80108. Results are reported on a dry weight basis. 1 Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any,is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. - fi 1' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 L 1 GROUNDWATER ANALYTICAL EPA Method 80218 Halogenated Volatile Organics by GC/ELCD Field ID: B-4(10) Laboratory ID: 36208-12 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 Matrix Soil Dilution Factor: 1 % Moisture 4 CAS Number`•. rY 3 w ;1ni Anal e r 5 u xi �*x q., �j, ,-.:�. ,. 1«a,��,Concentration,<L, R,eportingLimit ' 75-71-8 DichlorodiFluoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 260 75-00.3 Chloroethane BRL ug/Kg 260 75-69-4 Trichiorofluoromethane BRL ug/Kg 52 75-35-4 1,1-Dichloroethene BRL ug/Kg 52 75-09-2 Methylene Chloride BRL ug/Kg 52 156-60-5 trans-1,2-Dichloroethene BRL u911<9 52 75-34-3 1,1-Dichloroethane BRL ug/Kg 52 1_56-59-2 cis-1,2-Dichloroethene6 _BRL ug/Kg 52 67-66-3 Chloroform _ BRL ug/Kg 52 107-06-2 1,2-Dichloroethane BRL ug/Kg 52 ` 71-55-6 1,1,1-Trichloro_ethane BRL _ ug/Kg 52 56-23-5 Carbon Tetrachloride --BRL ug/Kg 52 78-87-5 1,2-Dichloropropane BRL ug/Kg 52 79-01-6 _Trichloroethene BRL ug/Kg _52 75-274 Bromodichloromethane BRL ug/Kg 52 110-75-8 2-Chloroethyl Vinyl Ether _BRL _ ug/Kg 260 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 52 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 52 7 9-0 0 5_1,1,2-Trichloroethane - BRL ug/Kg 52 1_24-48-1 Dibromochloromethane BRL ug/Kg 52 •127-184 Te[rachloroethene rE: 56 ug/Kg 52 108-90-7 Chioro_benzene _ _BRL ug/Kg 52 75-25-2 Bromoform_ BRL ug/Kg 52 34-5 1,1,2,2-Tetrachloroethane BRL ___ _ ul?/ --52 5_2 loro 541-73-1 1,3-Dichbenzene _ BRL ug/Kg 52 _106-46 7 1_,4_Dithlorobenzene _ L BRL_ _ _ ug/Kg__ 52 _ 95-50-1 1,2-Dichlorobenzene BRL ug/Kg _52 QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethaneda 96 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition,Update III(1996). Analyle list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: B-5(4) Laboratory ID: 36208-13 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mt.Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 Matrix: Soil Dilution Factor: 1 %Moisture: 5 i r..CAS Number? Anal et'a r` ,ra 3.:atia. Concentridion r Units' ,•�ReporOng:Limit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 r 74.87-3 Chloromethane BRL ug/Kg 260 _ 75-01-4 Vinyl Chloride BRL ug/Kg 110 74-83-9 Bromomethane BRL ug/Kg 260 75-00-3 Chloroethane BRL ug/Kg 260 75-69A Trichlorofluoromethane BRL ug/Kg 53 75-35-4 1,1-Dichloroethene BRL ug/Kg 53 75-09-2 Methylene Chloride BRL ugtKg 53 156-60-5 trans-1,2-Dichloroethene BRL ugtKg 53 75-34-3 1,1-Dichloroethane BRL u9tK9 53 156-59-2 cis-1,2-Dichloroethene BRL ugtKg 53 67-66-3 Chloroform _ BRL _ ug/Kg 53 107-06-2 1,2-Dichloroethane ElikL ug/Kg 53 71-55-6 1,1,1-Trichloroethane BRL ugtKg 53 56-23-5 Carbon Tetrachloride BRL _ ug/Kg 53 78-87-5 1,2-Dichloropropane BRL _ ugt-Kg 53 _79-01-6 _ � _Trich_loroethene _ 86_ _ _ ug/Kg 53 75-274 Bromodichloromethane BRL _ ug/Kg 53 ' 110-75-8_ 2-C_hloroethyl Vinyl Ether _ _ BRL _ ug/Kg __260 061 10 -01-5 cis-1,3-Dichloropropene BRL ug/Kg 53 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 53 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 53 12448-1 Dibromochloromethane BRL ug/Kg 53 127-18-4 Tetrachloroethene 1,300 _ ug/Kg 53 108-90-7 Chlorobenzene BRL _ ug/Kg 53 ' _ 93475-25-2-_ _ Bromoform - _ BRL ug/Kg 53 7 - -5 1,1,2,2-Tetrachloroethane BRL ug/Kg 53 541-73-1 1,3-Dichlorobenzene BRL ug/Kg 53 ' 1_06-46-7 ,4-Dich— —1lor_obenzene_ — __— BRL ug/Kg_ —53 1, _ 95-50-1 2-Dichlorobenzene BRL ug/Kg 53 QC Surrogate Compound I Recovery QC Limits:. . 1,2-Dichloroethane-d, _ 1 98 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: ' BRL Indicates concentration, if any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021B Halogenated Volatile Organics by GC/ELCD { Field ID: B•5(8) Laboratory ID: 36208-14 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E I Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 Matrix: Soil Dilution Factor. 1 I %Moisture: 2 i r.. CAS,Number F, z= :'•Anal e` a r" : x ,.Concentration , - a _` ;Units Reporting 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 260 75-00-3 Chloroethane BRL ug/Kg 260 75-69-4 Trichlorofluoromethane BRL ug/Kg 51 75-35-4 1,1-Dichloroethene BRL ug/Kg 51 75-09-2 Methylene Chloride BRL ug/Kg 51 156-6_0-5 trans-1,2-Dichloroethene BRL ug/Kg 51 } 75-34-3 1,1-Dichloroethane BRL ug/Kg 51 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 51 67-66-3 Chloroform _BRL ug/Kg 51 1! 107-06-2-55- 1,2-Dic_hlo_roethane BRL ug/Kg 51 716 1,1,1-Trichloroethane _ BRL ug(Kg 51 56-23-5 Carbon Tetrachloride _BRL_ ug1Kg 51 78-87-5 1.2-Dichloropropane BRL ug/Kg 51 79_-0_1-6 Trichlo_roethene_ _ _BRL ug(Kg 51 75-27-4 Bromodichloromethane BRL ug/Kg _ 51 11_0-75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 260 10061_-01-5 cis-1,3-Dichloropropene BRL ug/Kg 51 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 51 1 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 51 124-48-1 Dibromochloromethane BRL ug/Kg 51 127-18-4 Tetrachloroethene 58 _ ug/Kg 51 168-90-7 Chlorobenzene BRL ug/Kg 51 --- — ------ -- _75-25-2 Bro_moform _BRL ug/Kg 51 — _7_9-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg 51 541-73-1 1,3-15ichlorobenzene _BRL_ ug/Kg _51 ' 106-46-7 _ 1,4-Dichlorobenzene _BRL _ ug/Kg 51 0 1 2-95-5 1, Dichlorobenzene BRL ug/K9 51 QC Surrogate Compound Recovery QC Limits ' 1,2-DichloroethaneA, — 100 % 70- 130 % Method Reference: ' Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,if any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. 1� �1 1� Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: B-5(12) Laboratory ID: 36208-15 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mi.Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 Matrix: soil Dilution Factor: 1 %Moisture: 3 CAS Number:?' t,, ;Concentration f,i -E;, ;Units` K; Reportingi_Limit 75-718 DichlorodiFluoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromoethane a BRL ug/Kg 260 75-00.3 loro Chfl BRL ug/Kg 260 75-694 Trichlororofluoromethane BRL ug(Kg 51 - 75-35-4 1,1-Dichloroethene BRL ug/Kg 51 75-09-2 Methylene Chloride BRL ug/Kg 51 �. 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 51 75-34-3 1,1-Dichloroethane_ BRL ug/Kg 51 156-59-2 cis-1_2-Dichloroethene BRL ug/Kg 51 67-663 Chloroform _BRL ug/Kg 51 107-06-2 1,2-Dichloroethane BRL ug(Kg 51 71-55-6 1,1,1—TrnTetloroethane BRL ug/Kg 51 56-23-5 Carbon Tetrachloride BRL ug/Kg 51 78-87-5 1,2-Dichloropropane BRL _ u K 51_ — — g/ g Trichloroethene BRL _ ug/Kg 51 75-27-4 Bromodichloromethane BRL ug/Kg 51 '. 110.75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 260 10061-01-5 cis-1,3-Dichloropropene BRL Ug/K_g _51 10061-02-6 trans-1,3-Dichloropropene BRL ug(Kg-. 51 I 79-_00-5 1,1,2_Trichloroethane _BRL of Kg_ _51 124-48-1 Dibromochlor_omethane BRL ug/Kg 51 127-18-4 Tetrachloroethene BRL ug/Kg 51 _108-9_0.7 _ Chlorob_enzene BRL _ _ ug/Kg 51 _75-25-2 _BRL___ ug/Kg__51 -79-34-5 1,1,2,2-T_e[rachloroethane _BRL tf J 51 541-73-1 _to-Dichlorobenzene _BRL ug/Kg 51 _106-4&7 _1,4_Dichlorobenzene _ BRL __-__ ug/Kg__51 [95-50_1 - 1,2-Dichlorobenzene BRL ug/Kg 51 QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethane-da _ 100 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. ' Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. ,I Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL t EPA Method 80218 Halogenated Volatile Organics by GC/ELCD ! Field ID: B-9 04) Laboratory ID: 36229-06 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E Client: Atlantic Environmental Sampled: 09-26-00 Container: 60 ml.Glass Received: 09-26-00 t Preservation: Methanol/Cool Analyzed: 09.28-00 Matrix: Soil Dilution Factor: 1 %Moisture: 7 i CAS Number' Analyte Concentration" - i Units", Reporting Limit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 270 74-87-3 Chloromethane BRL ug/Kg 270 �c 75-01-4 Vinyl Chloride BRL ug/Kg 110 74-83-9 Bromomethane BRL ug/Kg 270 75-00-3 Chloroethane BRL ug/Kg 270 75-694 TrichloroBuoromethane BRL ug/Kg 54 75-354 1,1-Dichloroethene BRL ug/Kg 54 75-09-2 Methylene Chloride BRL ug/Kg 54 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 54 75-34-3 1,1-Dichloroethane BRL ug/Kg 54 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 54 67-66-3 Chloroform _BRL ug/Kg 54 107-06-2 1,2-Dichloroethane BRL ug/Kg 54 71-55-6 1,1,1-Trichloroethane BRL _ ug/Kg 54 56-23-5 Carbon Tetrachloride BRL ug/Kg 54 78-87_5 _1,2-Dic_hloropropane BRL__ ug/Kg 54 79-01-6 Trichloro_ethene _ BRL ug/Kg 54 75-27-4 Bromodichloromethane BRL ug/Kg 54 'I 110-75-8 2-Chloro_ethyl Vinyl Ether BRL ug/Kg_ 270 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 54 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 54 - 7900-5 1,1,2-Trichloroethane BRL ug/Kg 54 124-48-1 Dibromochloromethane BRL ug/Kg 54 127-184 Tetrachloroethene 100 ug/Kg 54 _108-90.7 Chlorobenzene BRL ug/Kg 54 75-25-2 Bromoform __ _ BRL ug/Kg 54 79-34-5 1,1,2,2-TetrachIoroethane BRL ug/Kg 54 541-73-1 1,3-Dichlorobenzene BRL ug/Kg 54 106-46-7 1,4-Dichlorobenzene• —"— ug/Kg 54t9_5 _1 Dic BRL ug/Kg 54 QC Surrogate Compound Recovery QC Limits . t-1 2-Dichloroethan 100 %_---__-_"-_1 _ A - 130 0/6—=— a ------e-d-d Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, it any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. ,l Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: B-12(3) Laboratory ID: 36229-07 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E ' Client: Atlantic Environmental Sampled: 09.26-00 Container: 60 mL Glass Received: 09-26.00 Preservation: Methanol/Cool Analyzed: 09-28-00 Matrix: soil Dilution Factor: 2 % Moisture: 10 CAS Number Analyte a y: , _Concentration Units>v Reporting Limit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 550 74-87-3 Chloromethane BRL ug/Kg 550 75-614 Vinyl Chloride BRL ug/Kg 220 74-83-9 Bromomethane BRL ug/Kg 550 75-004 Chloroethane BRL ug/Kg 550 75-69-4 Trichlorofluoromethane BRL ug/Kg 110 75-35-4 1,1-Dichloroe_thene BRL ug/Kg 110 75-09-2 Methylene Chloride BRL ug/Kg 110 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 110 75-34-3 1,1-Dichloroethane BRL - ug/Kg 110 156-59-2 cis-1,2-Dichloroethene 140 ug/Kg 1 00 ' 67-66-3 Chloroform BRL ug/Kg 110 107-06-2 1,2-Dichloroethane BRL ug/Kg 110 71-55-6 1rich 1,1, -Tloroethane BRL up/Kg 110 56-23-5 Carbon Tetrachloride BRL ug/Kg 110 78-87-5 1,2-Dichloropropane BRL ug/Kg 110 79-01-6 Trichloroethene_ 200 ug/Kg 110 75-27-4 Bromodichloromethane BRL ug/Kg 110 1.10-75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 550_ 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 110 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 110 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 110 124-48-1 Dibro_mochloromethane BRL ug/Kg 110 127-18-4 Tetrachloroethene 3,300 _ ug/K_g 110 108-90-7 Chlorobenzen_e_ BRL ug/Kg 110 ' 75-25-2 Broform BRL ug/om Kg 110 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/K9 110 -- 7 - -- -- 541 73-1 1 3 Dichlorobenzene _ BRL LgNg 110 ' 106-46-7 1 4 Dichlorobenzene _ _ ME I ug/Kg 110 -. . __- ---._ - --- --_ . _--------- —..__. ..--- -- t -- --- -- -------- 95-50 1 L 2 Dichlorobenzene BRL ug/K9 110 QC Surrogate Compound Recovery QC Limits ' 1,2-Dichloroethane-d _— 93 %_ 70- 130°/> Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyle list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: B-12(9) Laboratory ID: 36229-08 Project: Blaine/5786.01 QC Batch ID: VG2-1800-E Client: Atlantic Environmental Sampled: 09-26.00 Container: 60 mL Glass Received: 09-26-00 Preservation: Methanol/Cool Analyzed: 09-29-00 Matrix: Soil Dilution Factor: 100 %Moisture: 22 - - CAS Number.- - Analyte i -. Concentration Units Reporting Limit 75-71-8 Dichlorodifluoromethane BRL -- ug/Kg 32,000 74-8.7-3 Chloromethane BRL ug/Kg 32,000 75-01-4 Vinyl Chloride BRL ug/Kg 13,000 74-83-9 Bromomethane BRL _ ug/Kg 32,000 75-00-3 Chloroethane BRL - _- ug/Kg 32,000 75-694 Trichlorofluoromethane BRL ug/Kg 6,400 75-354 1,1-Dichloroethene BRL ug/Kg 6,400 75-09-2 Methylene Chloride BRL -- ug/Kg 6,400 156-60-5 trans-1,2-Dichloroethene 9,500 _ ug/Kg 6,400 75-34-3 1,1-_Dichloroethane _ _ BRL ug/Kg 6,400 156-59-2 cis-1,2-Dichloroethene 210,000' ugXg 6,400 67-66-3 Chloroform B __RL ug/Kg 6,400 107-06-2 1,2-Dichloroethane _ BRL ug/Kg 6,400 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 6,400 ------------- -- ' 5623-5 Carbon Tetrachloride BRL ug/Kg 6,400 _. - ---------- ------ --111--- -- 78-87-5 1,2-Dichloropropane BRL { ug/Kg 6,400 -- - - - - - -- - -- -- 79 Ol 6 Tnchloroethene - 65,000 i ug/Kg 6,400 -- - -- - ---- --r-- -- 75 27-4 Bromodichloromethane BRL ug/K_g 6,400 -- -- -- ur - --- -- - - - 110.75-8 2 Chloroethyl Vinyl Ether BRL �Kg 32,000__ 10061-01 5 _ as 1 3 Dichloropropene _ _ BRL _ _ ug/Kg _ 6,400 10061-02 6 ttrans 1 3-Dichloropropene BRL -�Kg 6,400 - 79-00-5 _t 1 2Trichloroethane _ BRL-- /Kg 6,400 12448-1 Dibromochloromethane BRL ug/Kg 6,400 -_._ 127-18-4 Woir b-enz these 23,000 ug/Kg 6,400 108-90-7 Chlorobenzene _ BRL ug/Kg 6,400.._ .---------- - - ---- --- -- - 75 25-2 Bromoform ' _ BRL -ug/Kg 6,400 79 34-5 _ 1 1 2 2 Tetrachloroethane BRL � ug/Kg 6,400 541 73-1 1 3 Dichlorobenzene f_ BRL 1 ug/Kg 6,400 1 W46-7 -1-4 Dichlorobenzene _ --�_ _ BRL _ug/Kg _ 6,400 ' 9550-1 l 1 2 Dichl_orobenzene_ BRL ug/Kg_- 6,400 -QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethan�, _ 100 % --- ---- Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Results are reposed on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,if any, is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: B-12(14) Laboratory ID: 36229-09 Project: Blaine/5786.01 QC Batch ID: VG2-1800-E Client: Atlantic Environmental Sampled: 09-26-00 Container: 60 ml.Glass Received: 09-26-00 Preservation: Methanol/Cool Analyzed: 09-29-00 Matrix: Soil Dilution Factor: 1 % Moisture: 4 CAS Number- Analyte Concentration �:,rt.lnits Reporting Limit 75-71-8 --6�ichlorocfifluoromethane BRL ug/Kg 260 74-87-3 Chloromdh—ane BRL ug/Kg 260 75-01-4 Vinyl Chloride —BRL ug/Kg 1-00 74-83-9 Bromomethane BRL ug/Kg 260 75-00-3 Ch—loroethane —BRL ug/Kg 260 75-69-4 Trichlorofluorometharte— BRL ug/Kg 52 75-35-4_1,11-Richlotroethene --BRL ug/Kg 52 75-09-2— Methylene Chloride BRL ug/Kg 52 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 52 75-34-3 1,11-Dichlm—oethane — BRL —uglk-9——5-2- 156-59-2 cis-1,2-Dichloroethene 55 —ug/Kg 52 67-66-3 Chloroform BRL — ug/Kg 52 -107-06-2 1,2-Dichloroethane BRL ug/Kg 52 71T- 5-6 TTch-1oroeth­ane---B-R­L ug/Kg 52 56-23-5-- Carbon Tetrachloride ug/Kg '2 1 M-87 5 1-2­5`ic h lo—ro-p r o p—an e BRL ug/Kg '2 -79-01-6 Trichlorciethene ----BRIL— ug/Kg 52 75-474 B romod i c h loromethan—e- BRL ug/Kg 52 110-75-8 - 2-Chloroethyl Vinyl Ether _BRL ug/Kg _J60 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 52 1(661-02--6 trans-1,3-Dichloropropene BRL ug/Kg 52 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 52 — 124 4f-1 Dibromochloromethane BRL — ug/Kg 52 7 - 1 Z7-1-4 T—etrachloroethene 71 ug/Kg 52 -108-90-7 Chlorobenzene BRL ug/Kg 52 75 25 2—­Bromoforrn-1---BR­L ug1Kg -52 7944-5 --------J,-I,-�,i-f-e-tra-ch-l-or-o-e-t-h-a--ne- --ug1K-g—5-2-- 1 -_U 5C-7371 f RicNorobenzene BRL ug/Kg 106-46-7 1,4-Dichlorobenzene B In ugxg—u- 1,2-Dichlorobenzene BRL ug/Kg 52 .... ......9C Surrogate Compound Recovery QC Limits 1,2-Dichloroethane-d, 99 % 71Y-�F301. Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition, Update 111(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, it any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Project Narrative Project: Blaine/5786.01 Lab ID: 36229 Client: Atlantic Environmental Received: 09-26-00 A. Physical Condition of Sample(s) This project was received by the laboratory in satisfactory condition. The sample(s) were received undamaged in appropriate containers with the correct preservation. 1 B. Project Documentation This project was accompanied by satisfactory Chain of Custody documentation. The sample container label(s)agreed with the Chain of Custody. C. Analysis of Sample(s) No analytical anomalies or non-conformances were noted by the laboratory during the processing of these sample(s). All data contained within this report are released without qualification. 1 f 1� f Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 22aMain PO.Box 1200 GROUNDWATER Buz Bay, Buzzards Sae.MA 02532 CHAIN-OF-CUSTODY RECORD ANALYTICAL Telephone(50B)759-4441 AND WORK ORDER N9 42936 FAX(508)759-4475 Propel Name: Firm: TURNAROUND ANALYSIS REQUEST �✓�' / 1.0i IePLBt lifiesm, M1 n Nm General EBembna ❑ ST DARD(10 Business Days) el Blner weds Frolect Number: Address: RIORITV(5 Business Days) ? /, $ = d3C+ UJ J-> //A+'t LfZ:I r �7 RUSH(RAN- 1 = =y 5 v o / (Rush requires Rush Authpnza'is beq o 0 0 Sampler Name: City/Slate i Zip: Please FAX VES ❑ NO e S FA%Number: ff 2.f Project Manager: Telephone: BILLING e c g Purchase Order No.: GWA Reference No.: o g3 c 2 INSTRUCTIONS:Use separate line for each container(except replicates). a o o $ o 0 0 jSampffrg Matrix Type Contalnerlsl Preservation nlNna„ e .. 5 - y LABORATORY W Bi _SAMPLE z ' tl d - NUMBERm 9 „ ? o $ 2 a tl aI EMIFICATION aaa 5 5 a S (Lab Use Onlyl 9 - i " a ya N - Ixs �� 3 b 6' s I 9 PY- I 3 7 to b l 6 Sr pr1Z REMARKS I SPECIAL INSTRUCTIONS DATA QUALITY OBJECTIVES CHAIN-OF-CUSTODY RECORD Regulatory Program Project Specific OC NOTE:All samples submitted subject to Standard Terms and Conditions an reverse hereof. L4 �tCyJ>— ❑Sale Drinking Water Act Man regulatory programs and EPA methods require project Relinquished!b Sam Ier: Date Time Reserve b Receipt Temperature ❑MA OFF Form Y e9 ry ec 9 eq P I q Y Y: P specific OC.Project specificDC includes Sample Duplicates, Iza ❑NPpES/Clean Water Act Matrix Spikes,anNor Many Marix Spike Duplicates.Laboratory OC is ,r-Cc Specify Slate. not project specific unless prearranged.Prajed sped OC e ❑RCRAMaz.Waste Char. samples are charged on a per sample basis.For water samples. Relinquis Date Time eceived by: Numbngrgirbill G MA MCP 1310 CAR 40) each MS,MSD and Sample Duplicate requires an additional Number: Reportable Concentrations Sample aliquot.Cl RCGW-t p FPS7.t Protect Specific OC Required Selection of OC Sample Relinquished by: Date Time Received by Laboratory: Custody Seal/ rJ' Cooler Serial G RCGW-2 RCS 2 osample Dawlwle ❑Setecletl by WporalNry Number: G MA Dredge Disposal C Maley Spike ❑Please use sample: G NHGRI GCTGME Method of Shipment❑GWACo ❑Express Mail❑Federal Express Specify Category' OMamx Spike ouwlrate ❑UPS antl 0 GROUNDWATER ANALYTICAL ' Quality Assurance/Quality Control A. Program Overview Groundwater Analytical conducts an active Quality Assurance program to ensure the production of high quality, valid data. This program closely follows the guidance provided by Interim Guidelines and ' Specifications for Preparing Quality Assurance Project Plans, US EPA QAMS-005/80 (1980), and Test Methods for Evaluating Solid Waste, US EPA, SW-846, Update III (1996). Quality Control protocols include written Standard Operating Procedures (SOPS) developed for each analytical method. SOPS are derived from US EPA methodologies and other established references. Standards are prepared from commercially obtained reference materials of certified purity, and documented for traceability. Quality Assessment protocols for most organic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. All samples, standards, blanks, laboratory control samples, matrix spikes and sample duplicates are spiked with internal standards and surrogate compounds. All instrument sequences begin with an initial calibration verification standard and a blank; and excepting GC/MS sequences, all sequences close with a continuing calibration standard. GCIMS systems are tuned to appropriate ion abundance criteria daily, or for each 12 ' hour operating period,whichever is more frequent. Quality Assessment protocols for most inorganic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation ' batch. Standard curves are derived from one reagent blank and four concentration levels. Curve validity is verified by standard recoveries within plus or minus ten percent of the curve. B. Definitions Batches are used as the basic unit for Quality Assessment. A Batch is defined as twenty or fewer samples of the same matrix which are prepared together for the same analysis, using the same lots of reagents and the same techniques or manipulations, all within the same continuum of time, up to but not exceeding 24 hours. Laboratory Control Samples are used to assess the accuracy of the analytical method. A Laboratory Control Sample consists of reagent water or sodium sulfate spiked with a group of target analytes representative of the method analytes. Accuracy is.defined as the degree of agreement of the measured value with the true or expected value. Percent Recoveries for the Laboratory Control Samples are calculated to assess accuracy. ' Method Blanks are used to assess the level of contamination present in the analytical system. Method Blanks consist of reagent water or an aliquot of sodium sulfate. Method Blanks are taken through all the appropriate ' steps of an analytical method. Sample data reported is not corrected for blank contamination. Surrogate Compounds are used to assess the effectiveness of an analytical method in dealing with each sample matrix. Surrogate Compounds are organic compounds which are similar to the target analytes of interest in chemical behavior, but which are not normally found in environmental samples. Percent Recoveries are calculated for each Surrogate Compound. ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Laboratory Control Sample Category: EPA Method 8012E-Halogenated QC Batch ID: VG2-1799-E Matrix: Soil Units: ugtKg CAS Number; A nak I yt e Spiked;.;,:} Measured, R ec o ve ry 75-35-4 1,1-Dichloroethene 250 260 103 % 70- 130% -- 1- —74:6 6 ichloroethene 1 0 1-90-1 Chlorobenzene 250 180 110% 70- 130% QC Surrogate:Compound Recovery" r 1,2-Dichloroethane-d4 130 % Method Reference: Test Methods for Evaluating Solid Waste,US EPA,SW-846,Third Edition,Update 111(11996). Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Method Blank Category: EPA Method 8021 B-Halogenated ' QC Batch ID: VG2-1799-E Matrix: Soil CAS Number` ' -Analyte _ ;?;.Concentiation ', "F Units %: Reporting Limit ' 75-71-8 Dichlorodifluoromethane BRL ug/Kg 250 74-87-3 Chloromethane BRL ug/Kg 250 75-01-4 Vinyl Chloride _ BRL ug/Kg 100 ' 74-113-9 Bromomethane BRL ug/Kg 250 75-00-3 Chloroethane BRL ug/Kg 250 75-69-4 -_Trichlo_rofluoromethane _ ug/ BRL ug/Kg 50 75-35-4 1,1-Dichloroethene BRL K_g 50 ' 75-09-2 Methylene Chloride - _- BRL_ ug/Kg 50 156-60-5 trans-1,2-Dichlor_oethene __ BR_L_ ug/Kg 50 75-34-3 1,1-Dichloroethane ___BRL ug/Kg 50 t 6766-3 cislorofDichloroethene BRL— ug/Kg 50 67-663 Chloroform_ BRL ug/Kg 50 71-55-6 1,1,1-Trichloroethane EEJ— _BRL ug/Kg 50 56-23-5 Carbon Tetrachloride BRL_ ug/Kg 50 107-06-2 _ 1_2-_Dichloroethane - - _ -BRL ug/Kg 50 79-01-6 Trichloroethene _BRL_ _ ug/Kg 50 78-87-5 _ 1,2-Dichloropropane _ _ BRL_ ug/Kg 50 75-274 - Bromodichloromethane_ --BRL-- - __ ug/Kg 50 110-75-8 2-Chloroethyl Vi nyl Ether BRL ug/Kg _ 250 10061-01-5 _ cis-1,3-Dichloropropene _ _-_ .BRL___ ug/Kg 50_ 10061-02-6 trans-1,3-Dichloropropene BRL_ ug/Kg 50 — - ---------BRL_ - -- 79-00-5 1,1,2-Trichloroethane - -. - ug/Kg 50 127-18-4 _ Tetrachloroethen_e__ __ _ BRL___ ug/Kg 50 124-48-1 Dibromochloromethane _ _ . BRL - �ug/Kg 50 ' 708 5- _ - B-romChlorobenze_ne - - -- BRL -- - ug/Kg 50 � 75 25-2 Bromoform BRL ug/Kg 50 79 34-5 _L1 1 2 2 Tetrachloroethane BRL ug/Kg 50 -- - — -- -- -- 541 73-1 I 1 3 DicNorobenzene-- - BRL ug/Kg 50 106-467 1,4-Dichlorobenzene BRL ug/Kg 50 ---- -----... -c------ -B------ ------ P� g - 95-541 1,2-Dihlorobenzene _BRL - _- - u 5 K _ 0— —QC Surrogate Compound Recovery QC Limits' I 1 2-Dichloroethane<l 100 % 70- 130 % Method Reference Test Methods for Evaluating Solid Waste, US EPA SW-846,Third Edition, Update III(1996). Analyte list 25 selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Laboratory Control Sample Category: EPA Method 8012E-Halogenated QC Batch ID: VG2-1800-E Matrix: Soil Units: ug/Kg CAS Number Analyte Measured Recovery . ., Limits'.i 75-354 1,1-Dichloroethene 250 260 106% 1 70- 130 % 79-01-6 Trichloroethene 2 00 _ 2_80 110% 70-130% 108-90-7 Chlorobenzene 250 _ 280 111 % 70- 130% ' QC Surrogate Compound'=. '''__ 5'" Recovery QC Ltmtts V; 1,2-Dichloroethane-da _102 % 70-130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ' ANALYTICAL ' Quality Control Report Method Blank Category: EPA Method 8021E-Halogenated ' QC Batch ID: VG2-1800-E Matrix: Soil CAS Number - '-s Analyze !t< ;'?.Concentration `-,Units F'.. Reporting Limit ' 75-71-8 Dichlorodifluoromethane BRL ug/Kg 250 74-87-3 Chloromethane BRL ug/Kg 250 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 250 ' 75-00-3 Chloroethane BR_L ug/Kg 250 75-69-4 Trichlorofluoromethane _BRL ug/Kg 50 75-35-4 1,1-Dichloroethene BRL ug/Kg 50 ' 75-09-2 Methylene Chloride 15 BRL ug/Kg 50 6-60-5 transtrans-1,2-Dichloroethene BRL ug/Kg 50 75-34-3 1,1-Dichloroethane BRL ug/Kg 50 ' 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 50 67-663 Chloroform BRL _ ug/Kg 50 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 50 56_- 3-5 Carbon Tetrachloride BRL_ ug/Kg 50 107-06-2 1,2-_Dichloroethane __BRL_ ug/Kg 50 79-01-6 Trichloroethene —_ BRL ug/Kg 50 78-87-5 _1,2-Dichloropropane— _ BRL ug/Kg 50 ' 75-27-4 Bromodichloromethane -- BRL------ ug/Kg 50 110-75-8 2-Chloroethyl Vinyl Ether BRL___ ug/Kg 250 1006101-5 _cis=1,3-Dichlo_r_opropene__ ____BRL_____ _ug/Kg 50 10061-02-6 trans-1,3-_Dichloropropene __ BRL _ Lug/Kgr— _ 50 79-00-5 _ 1,1,2-Trichloroethane _______BRL _____ _ug/Kg_ 50 127-18-4 Tetrachl_oroethene _ _____BRL _ _ug/Kg 50 124-48-1 l Dibrom_ochloromethane BE ug/Kg 50 - ' _.1OV66-_7_ Chlorobenz_ene __ BRL — ug/Kg 50 75-25-2 Bromoform BRL ug/Kg 50 1,1,2,2-Tetrachloroethane �— BRL ug/Kg_ 50 541-73-1 1,3-Dichlorobenzene BRL ____ ug/Kg 50 106-46-7 1,4-Dichlorobenzene _BRL_ ug/Kg 50 95-50-1 1,2-Dichlorobenzene _ _ g- -------�---------- _BRL ug/Kg 50 QC Surrogate Compound Recovery QC Limits -1!I_Dichloroethaned�-__---__ _--_-____- - 99 %_-_ _---_ 70=130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition,Update III(1996). Analyze list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. ' Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Certifications and Approvals CONNECTICUT, Department of.Health Services, PH-0586 ' Potable Water,WastewatedTrade Waste,Sewage/Effluent,and Soil pH,Conductivity,Acidity,Alkalinity,Hardness,Chloride,Fluoride,Ammonia,Kjeldahl Nitrogen,Nitrate,Nitrite,Orthophosphate,Total Dissolved Solids,Cyanide,Aluminum,Antimony,Arsenic,Barium,Beryllium,Cadmium,Total Chromium,Hexavalent Chromium,Cobalt,Copper,Iron,Lead, Magnesium,Manganese,Mercury,Molybdenum,Nickel,Potassium,Selenium,Silver,Sodium,Thallium,Tin,Titanium,Vanadium,Zinc,Purgeable ' Halocarbons,Forgeable Aromatics,Pesticides,PCBs,PCBs in Oil,Ethylene Dibromide,Phenols,Oil and Grease. MAINE, Department of Human Services, MA103 Drinking Water Reciprocal certification in accordance with Massachusetts certification for drinking water analyzes. Waste Water Reciprocal certification in accordance with Massachusetts certification for waste water analyles. MASSACHUSETTS, Department of Environmental Protection, M-MA-103 Potable Water Antimony,Arsenic,Barium,Beryllium,Cadmium,Chromium,Copper,Lead,Mercury,Nickel,Selenium,Thallium,Nitrate-N,Nitrite-N,Fluoride, Sodium,Sulfate,Cyanide,Turbidity,Residual Free Chlorine,Calcium,Total Alkalinity,Total Dissolved Solids,pH,Trihalomethanes,Volatile Organic Compounds,1,2-Dibromoethane,1,2-Dibromo-3-chloropropane,Total Coliform,Fecal Coliform,Heterotrophic Plate Count,E-Coli Non-Potable Water Aluminum,Antimony,Arsenic,Beryllium,Cadmium,Chromium,Cobalt,Copper,Iron,Lead,Manganese,Mercury,Molybdenum,Nickel,Selenium, Silver,Strontium,Thallium,Titanium,Vanadium,Zinc,pH,Specific Conductance,Total Dissolved Solids,Total Hardness,Calcium,Magnesium, ' Sodium,Potassium,Total Alkalinity,Chloride,Fluoride,Sulfate,Ammonia-N,Nitrate-N,Kleldahl-N,Orthophosphate,Total Phosphorus,Chemical Oxygen Demand,Biochemical Oxygen Demand,Total Cyanide,Non-Filterable Residue,Total Residual Chlorine,Oil and Grease,Total Phenolics, Volatile Halocarbons,Volatile Aromatics,Chlordane,Aldrin,Dieldrin,DOD,DDE,DDT,Heptachlor,Heptachlor Epoxide,Polychlorinated Biphenyls(water),Polychlorinated Biphenyls(oil). ' MICHIGAN, Department of Environmental Quality Drinking Water Trihalomethanes,Regulated and Unregulated Volatile Organic Compounds by EPA Method 524.2;1,2-Dibrommthane,1,2-Dibromo-3- chloropropane by EPA Method 504.1 NEW HAMPSHIRE, Department of Environmental Services, 202798 Drinking Water Metals by Graphite Furnace,Metals by ICP,Mercury,Nilrile,N,Orthophosphate,Residual Free Chlorine,Turbidity,Total Filterable Residue,Calcium ' Hardness,pH,Alkalinity,Sodium,Sulfate,Total Cyanide,Insecticides,Herbicides,Base/Neutrals,Trihalomethanes,Volatile Organics,Vinyl Chloride,DBCP,EDB,Nitrate-N. Wastewater Metals by Graphite Furnace,Metals by ICP,Mercury,pH,Specific Conductivity,TOS,Total Hardness,Calcium,Magnesium,Sodium,Potassium, ' Total Alkalinity,Chloride,Fluoride,Sulfate,Ammonia-N,Nltrate-N,Orthophosphate,TKN,Total Phosphorus,COD,BOD,Non-Filterable Residue, Oil&Grease,Total Phenolics,Total Residual Chlorine,PCBs in Water,PCBs in Oil,Pesticides,Volatile Organics,Total Cyanide. ' RHODE ISLAND, Department of Health, 54 Surface Water,Air,Wastewater, Potable Water,Sewage Chemistry: Organic and Inorganic ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL EPA Method 80218 Halogenated Volatile Organics by GCIELCD Field ID: B-9(9) Laboratory ID: 36229-05 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E Client; Atlantic Environmental Sampled: 09-26-00 Container. 60 ml.Glass Received: 09-26-00 Preservation: Methanol/Cool Analyzed: 09-28-00 Matrix: Soil Dilution Factor: I % Moisture: 2 CAS Number. Anal ;,Concentration Units ReportingUmit 75-71-8 Dichlorodifl uoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01 A Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 260 75-00-3 Chloroethane BRL ug/Kg 260 -75-69A Trichlorofluoromethane BRL ug/Kg 51 75-35-4 1,1-Dichloroethene---BRIL- ug/Kg 51 75-09-2— Methylene Chloride BRL ug/Kg 51 156-W5 trans-1,2-DAtchloroetheme— BRL ug/Kg 51 75-34-3 1,1-Dichloroethane BRL ug/Kg 51 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 51 67-66-3 Chloroform BRL ug/Kg 51 107-06-2 1,2-Dichloroethane BRL --ug/Kg 5-1 71-55-6 1,1,1-Trichloroethane BRL ug/Kg 51 56-23-5 Carbon Tetrachloride BRL ug/Kg 51 -67 pane ug/Kg 51 ­ - 76- --5 2-Dk-hlc—ropro--- 79-01-6 Trichlomethene BRL ug/Kg 51 75-2 7-4 Bromodichloromethane BRL 51 110-75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 260 -W061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 51 160-6f4-2-6 trans 4,3-15i�chloropnr—opene --Bk-L— ug/Kg 51 79-00-5 10,2-Trichloroethane BRL ug/Kg 51 -24 -- - I -48-T-- Dibromochloromethane L ug/Kg 51 —127-18-4 Tetrachloroeth ene 110 ug/Kg 51- 1-68-40J C h—10 mbmn n e BRL ug/Kg 51 75 25-2 —Bromoforrn BRL _ug/Kg 51 79-34-5 BRL ug/Kg —5 lmoethane—i- L541-73-1 1,3-Dichlorobenzene BRL ug)rKg51 me BRL ug Kg 51 9 51 me BRL QC Surrogate Compound --Recovery J__QC Limits 1,2 Dichlo- C'74 L 100 % 70- 130 % -Ff-,-;:D'�c-hFo-ro-e�thn—e-d4 Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW4846,Third Edition, Update 111(1996). Analyle list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,if any, is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: B-8(12) Laboratory ID: 36229-03 Project: Blaine/S786.01 QC Batch ID: VG2-1799-E Client: Atlantic Environmental Sampled: 09-26-00 Container: 60 mL Glass Received: 09-26-00 Preservation: Methanol/Cool Analyzed: 09-28-00 ' Matrix: Soil Dilution Factor: 1 %Moisture: 3 CAS Number- AnalyteJ.,Concentrahon 4 Units;-;,Reporting limit ' 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 260 ' 75-00-3 Chloroethane BRL ug/Kg 260 75-694 Trichlorofluoromethane _ BRL ug/Kg 52 75-354 1,1-Dichloroethene BRL ug/Kg 52 ' 75-09-2 Methylene_Chloride BRL ug/Kg 52 156-60-5 —trans-1,2-Dichloroethene BRL ug/Kg 52 _75-34-3 _ 1,1-D_ichloroethane BRL ug/Kg 52 1569-2 5 cis-1,2-Dichloroethene° BRL ug/Kg 52 ' 67-66-3 Chloroform BRL ug/Kg 52 107-06 2 2 1, -Dichloroethane BRL ug/Kg 52 71.55-6 1,1,1-Trichloroethane BRL ug/Kg 52 56-23_5 Carbon Tetrachloride BRL ug/Kg 52 78-87.5 . 1,2-Dichloropropane BRL ug/Kg 52 79-01-6 Trichloroethene BRL ug/Kg 52 75-27-4 Bromodichloromethane BRL ug/Kg 52 ' 110-75-8---- 2-Chloroethyl Vinyl Ether - BRL -_ ug/Kg 260 3 ne 10061-01-5 cis-1,=Dichloroprope BRL ug/Kg 52 - 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 52 ,- 79-00-5 — 1,1,2-Trichloroethane BRL ug/Kg _52 12448-1 Dibromochloromethane _BRL ug/Kg 52 127-18-4 Tetrachloroethene BRL ug/K9 52 --- -- 108-90-7 Chlorobenzene BRL ug/Kg 52 _79-75-2_-5 1,1,2,2-Te 5-2_____ Bromoform _ _ BRL _ ug/Kg ___52__ 34trachloroetInane _ _BRL _ __ ugtK--g 52 541-73-1 - 1,3-Dichlorobenzene BRL ug/Kg 52 ' 106-467 _7 4Dichlorobenzene BRL ug/Kg' 52 95-541 _ 1 2 Dichlorobenzene BRL ( ug/Kg 52 QC Surrogate Compound Recovery QC Limits ' - 1,2-Dichloroethaned4 104 % 70- 730 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. ' Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 1 GROUNDWATER ' ANALYTICAL EPA Method 8021B ' Halogenated Volatile Organics by GC/ELCD Field ID: B-9(3) Laboratory ID: 36229-04 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E ' Client: Atlantic Environmental Sampled: 09-26-00 Container: 60 mL Glass Received: 09-26-00 Preservation: Methanol/Cool Analyzed: 09-28-00 ' Matrix: Soil Dilution Factor: 10 % Moisture: 9 CAS Number Analyte, s-Concentratiod Units Reporting Limit ' 75-71-8 Dichlorodifluoromethane BRL ug/Kg 2,800 74-87-3 Chloromethane BRL ug/Kg 2,800 75-01-4 -Vinyl Chloride _BRL ug/Kg 1,100 74-83-9 Bromomethane BRL ug/Kg 2,800 ' 75-00-3 Chloroethane BRL ug/Kg 2,800 75-69-4 Trichlorofluoromethane BRL ug/Kg 550 75-354 1,1-Dichloroethene BRL ug/Kg 550 ' -75-09-2 — Methylene Chloride — BRL ug/Kg 550 156-60-5 _trans-1,2-Dichloroethene _ BRL ug/Kg _ 550 75-343 1,1-Dichlo_roethane _BRL ug/Kg 550 ' 1_56-59-2 cis-1,2-Dichloroethene __ BRL_ ug/Kg 550 67-66-3 Chloroform BRL ug/Kg 550 107-06-2 1,2-Dichloroethane _ BRL ug/Kg 550 71-55-6 1,1,1-Trichloro_ethane BRL ug/Kg 550 ' pane 56-2_3-5 Carbon Tetrachloride ----_BRL--- ugtKg 550 78-87-5 1,2-Dichloropro BRL ug/Kg 550 79-01-6 Trichloroethene 570 ug/Kg 550 _— --- 110-75- BZh_l dichlorom yfl BRl ug/Kg 550 110.75-8 _ _ 2-Chloroethyl Vmyl,Ether __- BRL ug/Kg 2,800 10061-01 5 cis 1 3-Dichloropropene _ _B_RL ug/Kg_ _ 550 10061-02-6 - trans-1,3-Dichloropropene BRL ug/Kg 550 79-00-5 1,1,2-Trichloroethane BRL_ uglKg 550 12448-1 -�lbrchloro thenethane _ _ _ BR_L_ — -- ug/Kg 550 12718-4 Tetrachloroethene 21,000 ug/Kg 550 -- 108 90.7 Chlorobenzene BRL ug/Kg 550 75 25-2 Bromoform 79-34-5 _ _ --� 1,1,2,2-Tetrachloroethane BRL _ ug/Kg 550 541 73-1 i _7 3 Dlchlorobenzene _ _� BRL ug/Kg 550 1 106-06-7 _1 4 Dichlorobenzene BRL __ _ _ug/Kg I 550 L95 50 1 1 2 Dichlorobenzene BRL u K 550 -- -_ ------ - ---- BRL J_ PJ B --- 550 --- QC Surrogate Compound Recovery QC Limits ' �1,2_Dichloroethanedg- _ - _-- 98 % - _�_70_130 %� Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyze list as selected from list formerly specified by EPA Method 80108. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. ' Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyse. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. 1 1 Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ' ANALYTICAL Quality Assurance/Quality Control A. Program Overview Groundwater Analytical conducts an active Y� Quality Assurance program to ensure the production of high quality, valid data. This program closely follows the guidance provided by Interim Guidelines and Specifications. for Preparing Quality Assurance Project Plans, US EPA QAMS-005/80 (1980), and Test Methods for Evaluating Solid Waste, US EPA, SW-846, Update III (1996). Quality Control protocols include written Standard Operating Procedures (SOPS) developed for each analytical method. SOPS are derived from US EPA methodologies and other established references. Standards are prepared from commercially obtained reference materials of certified purity, and documented for traceability. Quality Assessment protocols for most organic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation batch. All samples, standards, blanks, laboratory control samples, matrix spikes and sample duplicates are spiked ' with internal standards and surrogate compounds. All instrument sequences begin with an initial calibration verification standard and a blank; and excepting GGMS sequences, all sequences close with a continuing calibration standard. GC/MS systems are tuned to appropriate ion abundance criteria daily, or for each 12 ' hour operating period, whichever is more frequent. Quality Assessment protocols for most inorganic analyses include a minimum of one laboratory control sample, one method blank, one matrix spike sample, and one sample duplicate for each sample preparation ' batch. Standard curves are derived from one reagent blank and four concentration levels. Curve validity is verified by standard recoveries within plus or minus ten percent of the curve. ' B. Definitions ' Batches are used as the basic unit for Quality Assessment. A Batch is defined as twenty or fewer samples of the same matrix which are prepared together for the same analysis, using the same lots of reagents and the same techniques or manipulations, all within the same continuum of time, up to but not exceeding 24 hours. Laboratory Control Samples are used to assess the accuracy of the analytical method. A Laboratory Control Sample consists of reagent water or sodium sulfate spiked with a group of target analytes representative of the method analytes. Accuracy is defined as the degree of agreement of the measured value with the true or expected value. Percent Recoveries for the Laboratory Control Samples are calculated to assess accuracy. Method Blanks are used to assess the level of contamination present in the analytical system. Method Blanks consist of reagent water or an aliquot of sodium sulfate. Method Blanks are taken through all the appropriate ' steps of an analytical method. Sample data reported is not corrected for blank contamination. Surrogate Compounds are used to assess the effectiveness of an analytical method in dealing with each sample matrix. Surrogate Compounds are organic compounds which are similar to the target analytes of ' interest in chemical behavior, but which are not normally found in environmental samples. Percent Recoveries are calculated for each Surrogate Compound. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Laboratory Control Sample Category: EPA Method 8012B-Halogenated QC Batch ID: VG2-1798-E Matrix: Soil Units: ug/Kg ' :;:CAS Numbec4_ r Nt ?;''AnalyRer `, Sptkedt sti ,Ups;Measured ` °M"Recoverycn":z ,QG.LimltsFi 75-35-4 1 1 Dichloroetheney 250 250 101 % 70- 130 % 79-01-6 Trichloroethene 550 270 107% 70- 130 % 108-90-7 Chlorobenzene 250 270 107% 1 70 130% �QCSurrogate.Compound n x, - Recove a .,ff ? ±"QC'LrmrtsC .;'G ;m``>' 1,2 Dichloroethane-dd 101 % 70. 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL Quality Control Report Method Blank Category: EPA Method 8021 B-Halogenated QC Batch ID: VG2-1798-E Matrix: Soil Reporting Limit CAS Nurnber]', 75-71-8 Dichlorodifluoromethane BRL ug/Kg 250 74-87-3 Chloromethane BRL — 7 _01 ug/Kg 250 7514 Vinyl Chloride —BRL ug/Kg 1-00 74-83-9 Bromomethane BRIL ug/Kg— 250 75-00-3 Chloroethane BRLug/Kg 250 —75--69-4 Trichlorofluoromethane —BRL ug/Kg 50 75-354 1,1-Dichloroethene BRL ug/Kg 50 75-09-2_ Methylene Chloride BRL ug/Kg 50 156-60-5 trans-11,2-Duichn I oroethene BRL ug/Kg 50 7-5-34-3 1,11-Uichloroethane EIRL 50 156-59-2 'Cis-1,2-Dichloroethene BRL ug/Kg 50 67-66-3 Chloroform BRL ug/Kg so 71-55-6 1,1,1-Trichloroethane --BRL ug/Kg SO 56-23-5 Carbon Tetrachloride BRL ug/Kg 50 1 o F6(;2—--i,-2-6,ch—10 rethane— BRL ug/Kg 50 79-01-6 Trichloroethene BRL ---ug/Kg 50 78-87-5_ 1,2-Dichloropropane BRL ug/Kg 50 75-274— EG-m—od—ich—loromethan e- --------B—RL ug/Kg 50 110-7�5--6----Rhi—oro—eth)�l—V'nY—I Ether — BRL ug/Kg 250 10061-01-5 cis-1,3-D ich I oropropene BRL ug/Kg 50 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 50 79700-5 1,1,2-Trichloroethane BRL ug/Kg 50 127-18-4 Tetrachloroethene —ug/K-g----- - 50 12448-1 Dibromochloromethane 108-90-7 Chlorobemie—ne so — ug/Kg 50 75-25-2 Bronnoform ug/Kg 50 541-73-1 1,3FDiic—N—oro­berv—en—e BRL uglt'lg 5'g 106-46-7 1 4-Dichlorobenzene —5095-50.1 q—:�:: BRL ug/Kg 1.2 b,�hr, be ic oro enzene BRL ug/Kg 50 _g [� —QC Surrogate_ Compound Recovery QC Lim—it —s 2-5,cEl�roethanec, 96� 7CF- 130%E�� � --------IJ Method Reference: Test Methods for Evaluating Solid Waste, US EPA, SW-846,Third Edition, Update 111 (1996). Analyte list as seleclecl from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 1 . GROUNDWATER 1 ANALYTICAL ' Quality Control Report Laboratory Control Sample Category: EPA Method 80128-Halogenated QC Batch ID: VG2-1799-E Matrix: Soil Units: uglKg Spiked '( , Measured - ,."':Recovery .y, .=; QC Limits 75-35-4 1,1 Dichloroethene 250 260 103 % 70 130% 79-01-6 Trichloroethene 250 270 107% 70-130% 108-90.7 Chlorobenzene 250 280 110% 70 130% 1 " QGSurrogate,Compound't7 , n` , .. ,�,:"`'' Recove ,'r'rnr_.j =,: :z QC:Limitsj�te., ZI` ;^ , 't 1 2-Dichloroethane-da 103 % 70- 130% ' Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition,Update III(1996). Report Notations: All calculations performed prior to rounding. Quality Control Limits are defined by the methodology, or alternatively based upon the historical average recovery plus or minus three standard deviation units. 1 i 1 i 1 1 � 1 . 1 1 1 ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 ' GROUNDWATER ' ANALYTICAL Quality Control Report Method Blank Category: EPA Method 8021 B-Halogenated ' QC Batch ID: VG2-1799-E Matrix: Soil CAS-Number, : Analyze }tr:. 3 f Malion,,,v,J� Units'75-71-8 Dichlorodifluoromethaneg/Kg 250 74-87-3 Chloromethane g/Kg 250 75-OIA Vinyl Chloride g/Kg 100 74-83-9 Bromomethaneg/Kg 250 75-00-3 Chloroethane g/Kg. 250 75-69-4TrichloroBuoromethaneg/Kg 50 75-35A 'M-Dichloroethene BRL ug/Kg 50 5-09-2 Methylene Chloride BRL_ -- ug/Kg 50 1 56-60.5 trans-1,2-Dichloroethene BR_L ug/Kg 50 75-34-3 1,1-Dichloroethane BRL_ ug/Kg 50 156-59-2 cis-1,2-Dichloroethene ug/Kg 50 67-66-3 Chloroform BRL ug/Kg 50 BR_L 71-55-6 1,1,1-Tric_ rachloroethane ___ BRL ug/Kg 50 56-2_3-5 Carbon Tethloride B_RL ug/Kg _50 107-06-2 1,2-Dichloroethane _ BRL ug/Kg 50 79-01-6 Trichloroethene _ BRL ug/Kg 50 78-87-5 1,2-Dichloropropane _ BRL _ ug/Kg 50 __ 75-27A Bromodichloromethane _ __BRL ug/Kg 50 ' 110.75-8 2{hloroethyl Vinyl Ether BRL _ ug/Kg _250 10061-01-5 cis-1,3-Dichloropropene _ ____ BRL_ _ ug/Kg - 50 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 50 79-00-5 1,1,2-Trichloroethane__ __BRL --_ ug/Kg _50_ 127-18-4 Tetrachloroethene __BRL_ ug/Kg _5_0 124-08-1 Dibromochloromethane _____ BRL ug/Kg 50, 108-90-7 Chlorobenzene__ BRL ug/Kg 50 75-25-2 Bromoform __BRL__ BRL ug/Kg 50 79-34-5�2-Tetrachloroethane BR_L___ ug/Kg_ 50 ------- - --- — ---- _541-73-1 1,3-Dichlorobenzene -�-- _ _ BRL__ ug/Kg 50 106 46 7 1_4-Dichlorobenzene_ _BRL ___ ug/Kg 50 1,2-Dichlorobenzene _ BRL_ _ ug/Kg 50 QC Surrogate Compound Recovery QC Limits_ 1 2 DichloroethanR-dd ----_ --_-_- 100 % --_.__-_-_ _ 70- 130%_-_ Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 80108. Results are reponed on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL Certifications and Approvals CONNECTICUT, Department of Health Services, PH-0586 . ' Potable Water,Wastewater/Trade Waste,Sewage/Effluent,and Soil pH,Conductivity,Acidity,Alkalinity,Hardness,Chloride,Fluoride,Ammonia,Kjeldahl Nitrogen,Nitrate,Nitrite,Orthophosphate,Total Dissolved Solids,Cyanide,Aluminum,Antimony,Arsenic,Barium,Beryllium,Cadmium,Total Chromium,Hexavalent Chromium,Cobalt,Copper,Iron,Lead, ' Magnesium,Manganese,Mercury,Molybdenum,Nickel,Potassium,Selenium,Silver,Sodium,Thallium,Tin,Titanium,Vanadium,Zinc,Purgeable Halocarbons,Purgeable Aromatics,Pesticides,PCBs,PCBs in Oil,Ethylene Dibromide,Phenols,Oil and Grease. MAINE, Department of Human Services, MA10.3 Drinking Water . Reciprocal certification in accordance with Massachusetts certification for drinking water analyzes. 1 Waste Water Reciprocal certification in accordance with Massachusetts certification for waste water analyles. ' MASSACHUSETTS, Department of Environmental Protection, M-MA-103 Potable Water Antimony,Arsenic,Barium,Beryllium,Cadmium,Chromium,Copper,Lead,Mercury,Nickel,Selenium,Thallium,Nilrate-N,Nltllte-N,Fluoride, Sodium,Sulfate,Cyanide,Turbidity,Residual Free Chlorine,Calcium,Total Alkalinity,Total Dissolved Solids,pH,Trihalomethanes,Volatile Organic Compounds,1,2-Dibromoethane,1,2-Dibromo-3chloropropane,Total Coliform,Fecal Coliform,Helerotrophic Plate Count,E-Coli Non-Potable Water Aluminum,Antimony,Arsenic,Beryllium,Cadmium,Chromium,Cobalt,Copper,Iron,Lead,Manganese,Mercury,Molybdenum,Nickel,Selenium, Silver,Strontium,Thallium,Titanium,Vanadium,Zinc,pH,Specific Conductance,Total Dissolved Solids,Total Hardness,Calcium,Magnesium, Sodium,Potassium,Total Alkalinity,Chloride,Fluoride,Sulfate,Ammonia-N,Nitrate-N,Kjeldahl-N,Orthophosphate,Total Phosphorus,Chemical Oxygen Demand,Biochemical Oxygen Demand,Total Cyanide,Non-Filterable Residue,Total Residual Chlorine,Oil and Grease,Total Phenolics, Volatile Halocarbons,Volatile Aromatics,Chlordane,Aldrin,Dieldrin,DDD,DDE,DDT,Heptachlor,Heptachlor Epoxide,Polychlorinated Biphenyls(water),Polychlorinated Biphenyls(oil). MICHIGAN, Department of Environmental Quality Drinking Water - Trihalomethanes,Regulated and Unregulated Volatile Organic Compounds by EPA Method 524.2;1,2.Dibromoethane,1,2-Dibromo-3- chloropropane by EPA Method 504.1 NEW Hater RE, Department of Environmental Services, 202798 Drinking W Water Metals by Graphite Furnace,Metals by ICP,Mercury,Nitrite-N,Orthophosphate,Residual Free Chlorine,Turbidity,Total Filterable Residue,Calcium Hardness,pH,Alkalinity,Sodium,Sulfate,Total Cyanide,Insecticides,Herbicides,Base/Neutrals,Trihalomethanes,Volatile Organics,Vinyl Chloride,DBCP,EDB,Nitrate-N. Wastewater Metals by Graphite Furnace,Metals by ICP,Mercury,pH,Specific Conductivity,TD5,Total Hardness,Calcium,Magnesium,Sodium,Potassium, ' Total'Alkalinily,Chloride,Fluoride,Sulfate,Ammonia-N,Nitrate-N,Orthophosphate,TKN,Total Phosphorus,COD,BOD,Non-Filterable Residue, Oil&Grease,Total Phenolics,Total Residual Chlorine,PCBs in Water,PCBs in Oil,Pesticides,Volatile Organics,Total Cyanide. RHODE ISLAND, Department of Health, 54 Surface Water,Air,Wastewater, Potable Water,Sewage Chemistry: Organic and Inorganic ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 1 Groundwater Analytical,Inc. GROUNDWATER P.O.Box 1200 ANALYTICAL228 Main Street Buzzards Bay,MA 02532 Telephone(508)759-4441 FAX(508)759-4475 October 3, 2000 1 ' 1 Mr. Eric Cardinal Atlantic Environmental 1 86 Faunce Corner Rd. North Dartmouth, MA 02747 Project: Blaine/5786.01 Lab ID: 36229 Sampled: 09-26-00 Dear Eric: Enclosed are the Volatile Organics Analyses performed for the above referenced project. This project was processed for Priority One Week turnaround. This letter authorizes the release of the analytical results, and should be considered a part of this report. This report contains a project narrative indicating project changes and non-conformances, a brief description of the Quality Assurance/Quality Control procedures employed by our laboratory, and a statement of our state certifications. I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Should you have any questions concerning this report, please do not hesitate to contact me. Sincerely, 1, Jonathan R. Sanford President JRS/ss Enclosures i GROUNDWATER ANALYTICAL EPA Method 8021 B Halogenated Volatile Organics by GC/ELCD Field ID: B-8(3) Laboratory ID: 36229-01 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E Client: Atlantic Environmental Sampled: 09-26-00 ' Container: 60 mL Glass Received: 09-26.00 Preservation: Methanol/Cool Analyzed: 09-27-00 Matrix: soil Dilution Factor: 10 % Moisture: 16 CASNumber. - . Anal a '7Concentration Units Reporting.Limit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 3,000 74-87-3 Chloromethane BRL ug/Kg 3,000 75-014 Vinyl Chloride BRL ug/Kg 1,200 74-83-9 Bromomethane BRL ug/Kg 3,000 75-00.3 Chloroethane• BRL ug/Kg 3,000 ---69-4 Trichloro8uoromethane BRL ug/Kg 000 75-35-4 1,1-Dichloroethene BRL ug/Kg 600 75-09-2 Methylene Chloride BRL ug/Kg 600 156 60.5 trans-1,2-Dichloroethene BRL ug/Kg 600 75-34-3 1,1-Dic_hlor_oethane BRL ug/Kg 600 15659-2 cis-1,2-Dichloroethene° BRL ug/Kg 600 67-66 3 Chloroform BRL ug/Kg 600 107-06-2 1,Z-DE) loroethane BRL ug/Kg _ 600 71-55-6 1,1,1-Trichloroethane RL_ B uWKg _ 6_00 56-23-5 Carbon Tetrachloride — BRL ug/Kg 600 — 78-87-5 1,2DicNoropropane BRL ug/Kg 600 O1-79- 6 Trichloroethe_ne_ BRL ug —_600 75-27-4 Bromodichlorometh g/K ane BRL ug/Kg 60o 110.75-8 2-Chloroethyl Vinyl Ether BRL ug/Kg 3,000 10061-01-5 cis-1,3-Dichloropropene BRL ug/Kg 600 10061-02-6 trans-1,3-Dichloropropene BRL. ug/Kg 600 - 79-00-5 1,1,2Trichloroethane BRL ug/Kg 600 124-48-1 Dibromochloromethane BRL ug/Kg 600 127-18-4 Tetrachloroethene 15,000 •ug/Kg 600 108-90-7 Chlorobenzene BRL--- ug/Kg 600 - ---- - -- --- 75-25-2 Bromoform BRL ug/Kg 600 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg_ 600 541-73-1 1,3-Dichlorobenzene BRL ug/Kg 600 -- --- ---- - -- 106-467 1,4-Dichlorobenzene BRL ug/Kg 600 ' 95-50_7 _ 1,2 Dichlorobenzene _ _BRL _- _ ug/Kg =600__ QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethaned4 98 % • 70- I Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyle list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyle. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GC/ELCD Field ID: B-8(8) Laboratory ID: 36229-02 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E Client: Atlantic Environmental Sampled: 09-26-00 Container: 60 mL Glass Received: 09-26-00 Preservation: Methanol/Cool Analyzed: 09-27-00 1 Matrix: Soil Dilution Factor: 1 %Moisture: 4 "CAS Number, - '' Analyze , ` ;°i�Concentration —Units ": Reporting Limit ' 75-71-8 Dichlorodifluoromethane BRL ug/Kg '260 7487-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 260 75-00-3 Chloroethane BRL ug/Kg 260 75-69 4 Trichl --o_rofluoromethane BRL ug/Kg 52 75-354 1,1-Dichloroethene BRL ug/Kg 52 75-09-2 Methylene Chloride BRL ug/Kg 52 156-60-5 trans-1,2-Dichl_oroethene _BRL ug/Kg 52 75-34-3 1,1-Dichlo roe thane BRL ug/Kg 52 156-59-2 cis-1,2-Oichloroe[hene _ BRL ug/Kg 52 67-66-3 Chloroform BRL ug/Kg 52 107-06-2 1,2-Dic_hloroethane BRL ug/Kg 52 71-23-6 1,1,1-Trichloroethane BRL ug/Kg 52 ' S6-87-5 -- Carbon Tetrachloride -- -- ggl -- ug/Kg 52 78-87-5 1,2-Dichloropropane_ _BRL ug/Kg 52 79-01-6 Trichloroethene _ BRL___ ug/Kg 52 75-274 Bromodichloromethane _ _ BRL — — ug/Kg 52 _ 110. BRL_ ug/Kg 2-Chloroethyl Vinyl Ether /Kg 260 10061-01-5 cis-1,3-Dichloropropene _ B_RL ug/Kg 52 10061-02-6 trans-1_3-Dichloropropene BRL ug/Kg 52-- — ---- 79-00-5 1,1,2-Trichloroethane -- --.... _____BRL _ ______ uP�Kg_ __52__ 124-48-1 Dibromochloromethane_ BRL __ ug/Kg 52 127-18-4 Tetrachloroethene 61 _ _ ug/Kg 52 108-90-7 Chlorobenzene _BRL__ ug/Kg 52 75-25-2 ---- _Bromoform --- _ BRL ug/Kg --52 _79-34-5 1,1,2,2-Tetrac_hloroethane _BRL_ ug/Kg _52 541-73-1 1,3-Dichlorobenzene BRL ug/Kg 52 106-46,-7 1,4-Dichlorobenzene BRL _ ug/Kg _ 52--- -----------� —z--- 95-50.1 _ 1,2-Dichlorob_enzene ug/Kg_ 52 QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethaceda _ gq% 70-130% Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyze list as selected from list formerly specified by EPA Method 80108. Results are reported on a dry weight basis. Analysis pedormed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. ' Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021B Halogenated Volatile Organics by GC/ELCD Field ID: B-2(12) Laboratory ID: 36208-06 Project: Blaine/5786.01 QC Batch ID: VG2-1798-E Client: Atlantic Environmental Sampled: 09-25-00 - Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-26-00 ' Matrix: Soil Dilution Factor: 1 % Moisture: 2 r,`,CAS:Numberi = '�"'js� -`';Anal a f,��� v �, �., , r _ =.txxii _ _�z,�, ,'�.>>concentrah91`6, ',,,��,, �z Units;L`?j Reporting:Umit 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane —BRL ug/Kg 260 75-00-3 Chloroethane BRL ug/Kg 260 75-69-4 Trichlorofluoromethane BRL ug/Kg 51 75-354 1,1-Dichloroethene BRL ug/Kg 51 75-09-2 Methylene Chloride BRL ug/Kg 51 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 51 75-34-3 1,1-Dichloroethane BRL ug/Kg 51 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 51 67-66-3 Chloroform BRL ug/Kg 51 f 107-06-2 1,2-Dichloroethane BRL ug/Kg 51 71-55.6 1,1,1-Trichloroethane BRL ug/Kg 51 56-23-5 Carbon Tetrachloride BRL ug/Kg 51 78-87-5 1,2-Dichloropropane BRL ug/Kg 51 79-01-6 Trichloroeth_ene _ BRL _ ug/Kg - 51 75-27-4 Bromodichloromethane BRL ug/Kg 51 ' 110-75-8 2-Chloroethyl Vinyl Ether _ BRL ug/Kg 260 10061-01-5 cis-1,3-Dichloropropene _BRL ug/Kg 51 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 51 - 79-00-5 1,1,2-Trichloroethane BRL ug/Kg 51 124-481 Dibromochloromethane BRL ug/Kg 51 127-18-4_ T etrachloroetIne n e 800 ug/Kg 51 10_ 8-90-7 Chlo—robe nzene BRL ug/Kg 51 75-25_2 Bromoform hlor_ _ BRL ug/Kg 51 79-345 1,1,2,2-Teac troethane BRL ug/Kg 51 541-73-1 _ 1,3-Dichlorobenzene BRL ug/Kg 51 106-46-7 1,4-Dichlorobenzene _ _BRL ug/Kg 51 95-50_1 1,2-Dichlorobenzene __ BRL ug/Kg 51 QC Surrogate Compound _- Recovery QC Limits 12-Dichloroethane-d,__ _ 92 % __70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III(1996). Analyte list as selected from list formerly specified by EPA Method 6010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration,if any,is below reporting limit for analyte. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021E Halogenated Volatile Organics by GGELCD Field ID: B-3(3) Laboratory ID: 36208-07 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E Client: Atlantic Environmental Sampled: 09-25-00 Container: 60 mt.Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-27-00 ' Matrix: Soil Dilution Factor: 1 % Moisture: 3 ' CAS Numbei Coocentratton Units + R rtin Limit Q'nal e . $. � w w s . 4•. Tp g ' 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 100 74-83-9 Bromomethane BRL ug/Kg 260 75-00-3 Chloroethane BRL ug/Kg 660 75-69A Trichlorofluoromethane BRL ug/Kg 52 75-35A 1,1-Dichloroethene BRL ug/Kg 52 75-09-2 Methylene Chloride BRL ug/Kg 52 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 52 75-34-3 1,1-Dichloroethane BRL ug/Kg 52 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 52 ' 67-66-3 Chloroform BRL _ ug/Kg 52 107-06-2 1,2-Dichloroethane _BRL ug/Kg 52 71-55-6 1,1,1-Trichloroethane BRL ug(Kg 52 56-23-5 Carbon Tetrachloride BRL _— ug/Kg 52 78-87-5 1,2-Dichloropropane BRL ug/Kg 52 79-01-6 Trichloroethene_ BRL ug/Kg 52 75-27-4 Bromodichloromethane BRL ug/Kg 52 110-75-8 _ 2-Chloroethyl Vinyl Ether BRL _ _ ug/Kg 260 10061-01-5 cis-1,3-Dichloropropene BRL __ ug/Kg 52 10061-02-6 trans-1,3-Dichloropropene BRL . ug/Kg 52 • 79-00-5 1,1_2-TTrichloroethane -- BRL — ug/Kg 52 12448-1 Dibromochloromethane BRL ug/Kg 52 127-184 Tetrachloroethene 1,100 _ ug/Kg 52 108-90-7 Chlorobenzene BRL ug/Kg 52 ' 75-25-2 - Bro_moform BRL ug/Kg 52 79-34-5 _ 1,1,2,2-Tetrachloroethane BRL _ ug/Kg 52—___ 541-73-1 1,3-Dichlorobenzene BRL ug/Kg 52 _•_106-4G_7_ 1,4-Dichlorobenzene_ __ _BRL _ ug/Kg _ 52 95-50-1 1,2-Dichlorobenzene BRL _ ug/Kg _ 52 QC Surrogate Compound Recovery QC Limits 1,2-Dichloroethane-d4 97 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update III (1996). Analyze list v as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, if any,is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay,MA 02532 GROUNDWATER ANALYTICAL EPA Method 8021B Halogenated Volatile Organics by GC/ELCD Field ID: B-3(6) Laboratory ID: 36208-08 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E Client: Atlantic Environmental Sampled: 09-25-00 Container. 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-27-00 Matrix: Soil Dilution Factor. 1 %Moisture: 4 CM.Num*t Corkeintratiori Reporting Limit 75-71-8 Dichlorodifl uoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 -75-014 Vinyl Chloride BRL ug/Kg too 74w83-9 Bromornethane BRL ug/Kg 260 75-00-3 Chloroethane BRL ug/Kg 2-60 75-694 Trichlorofluoromethane BRL ug/Kg 52 75-35-4 1,1-Dichloroethene BRL --ug/Kg 5-2 75-09-2 Methylene Chloride BRL ug/Kg 52 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 52 75-34-3 1,1-Dichloroethane 52 156-59-2 cis-1,2-6,`c­hloroeth-en�e BRL —ug/Kg 5-2 67-6fr3 -Chloroform —BRL ug/Kg —52 107-06-2 1,2-Dichloroethane BRL ug/Kg 52 7155 6 1,1,1-Trichloroethane BRL ug/Kg .-52 56-23-5 Carbon Tetrachloride BRL ug/Kg 52 78-87-5 1,2-Dichloropropane BRL ug/Kg 52 _79-01-6 Trichloroethene BRL 52 75-274 Bromodic-hloromethane BRL ugliki52 — 11 2--Chlomet—hylVinyl Ether _BR_L ug/Kg 260 -10061-01-5 cis-T4:bichiformp-rapene BRL uglki——si--- �-� 3 16�orcpropi�ne BRL ug/Kg 52 V 061�-02-6 ra n� -�1 -D- 79-00-5 1,1,2-Trichloroethane ug/Kg 52 124-48-1 Dibromochloromethane-- BRL ug/Kg--- 5-2 12f M4 Tetrachloroethene 120 ug/Kg 52 1 C8-9677 ug/Kg 52 Ch-lo—robenzene —B--RL-- ug/Kg —5-2— 75 25-2 ronno-G-r—m- I i�--i4-5----iliY-Tetr-ach-lo- BRL roet—hane— BRL ug/Kg 52 5-41-7-3-1----1-,3-Dichloro6enzene BRL ug/Kg 52 106-46-7 1,4-Dichlorobenzene BRL ug/Kg 52 95-50-1 1,2-Dichlorobenzene BRL ug/Kg 52 QC Surrogate Compound Recovery Its�c Limits 1,2-Dichloroethane-d4 99 % 70- 130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update 111(1996). Analyle list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. Report Notations: BRL Indicates concentration, it any, is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 ! GROUNDWATER ANALYTICAL ! EPA Method 8021E ! Halogenated Volatile Organics by GC/ELCD Field ID: B-3(12) Laboratory ID: 36208-09 Project: Blaine/5786.01 QC Batch ID: VG2-1799-E Client: Atlantic Environmental Sampled: 09.25-00 Container: 60 mL Glass Received: 09-25-00 Preservation: Methanol/Cool Analyzed: 09-27-00 ! Matrix: Soil Dilution Factor: 1 %Moisture 5 —CAS_MUmber! ru `' r Anal a as} ` 3 b s;KCOnCentratlOn_�3 µc2° „r„p a•.:a-' .N., r_ �.Unrts s-d. Reporting,13 75-71-8 Dichlorodifluoromethane BRL ug/Kg 260 74-87-3 Chloromethane BRL ug/Kg 260 75-01-4 Vinyl Chloride BRL ug/Kg 110 74-83-9 Bromomethane BRL ug/Kg 260 ! 75-00-3 Chloroethane BRL ug/Kg 260 75-694 Trichlorofluoromethane BRL ug/Kg 53 75-35-4 1,1-Dichloroethene BRL ug/Kg 53 75-09-2 Methylene Chloride BRL ug/Kg 53 156-60-5 trans-1,2-Dichloroethene BRL ug/Kg 53 75-34-3 0-15ichloroethane BRL ug/Kg 53 156-59-2 cis-1,2-Dichloroethene BRL ug/Kg 53 ! 67-66-3 Chloroform BRL ug/Kg 53 107-06-2 1,2-Dichloroethane BRL ug1Kg 53 71-55-6 1,1,1-Tric_hloroethane BRL ug/Kg 53 56-23-5 Carbon Tetrachloride BRL ug/Kg 53 78-87-5 1,2-Dichloropropane BRL ug/Kg 53 79-01-6 Trichloroethene BRL ug1kg 53 75-27-4 Bromodichloromethane BRL ug/Kg! _ 53 110-75-8 2-Chloroethyl Vinyl Ether _ _ _ _BRL ug/Kg _260 10061-01-5 cis 1,3-Dic_hloropropene BRL ug/Kg 53 10061-02-6 trans-1,3-Dichloropropene BRL ug/Kg 53 ! _79--00-5 1,1,2TrTrichloroethane BRL ug/Kg S3 124-48-1 Dibromochloromethane BRL ug/Kg 53 127-18-4 Tetrachloroethene 67 ug/Kg 53 ! _108-90-7___ Chlorobenzene _ BRL ug/Kg 53—75_25_2 Bromoform _ _ _ BRL___ ug/Kg 53 I 79-34-5 1,1,2,2-Tetrachloroethane BRL ug/Kg - 541-73-1_ 1,3-Dichlorobenzene _ BRL ug/Kg�53 ! [—l(-- 6-7 1,4Dichlorob8nzene --BRL _ ug/Kg 53 95-50-1 _ 1,2-Dichlorobenzene BRL ug/Kg 1_ 53 QC Surrogate Compound Recovery —QC Limits 11,2-Dichloroethane-d, _ _ 97 % 70-130 % Method Reference: Test Methods for Evaluating Solid Waste, US EPA,SW-846,Third Edition, Update 111(1996). Analyte list as selected from list formerly specified by EPA Method 8010B. Results are reported on a dry weight basis. Analysis performed utilizing methanol extraction technique. �I Report Notations: BRL Indicates concentration, if any, is below reporting limit for analyze. Reporting limit is the lowest concentration that can be reliably quantified under routine laboratory operating conditions. Reporting limits are adjusted for sample dilution,percent moisture and sample size. ! Groundwater Analytical, Inc., P.O. Box 1200, 228 Main Street, Buzzards Bay, MA 02532 APPENDIX C 1 :M,Itianfic® 1 1 1 1 1 1 Appendix C: 1 AET Groundwater Monitoring Well Sampling Logs (August & September 2000) 1 1 1 1 1 1 1 1 i �� .. W An ! Site Name: Bliane Hair School MONITORING WELL SAMPLING LOG L Hm a n L I C nr f Envinnlental Technologies,Inc. Site Address: 18 Center Street, Hyannis MA 86Paunce Coma Read,Suite 410 Project No: 5786 RTY- 4-10971 Dartmouth,MA 02747 (508)997.5422 fax(508)9994060 Sampler: EC/JW Page I of 1 Date: 8/28/00 E E. ^ r D = O n E cE V -0o 1 ,r E 72 t5 hE Sample Analyses Sem le ID zi ¢ V a MW-I TOIC 13.84 19.55 5.72 1.2 5 5 B B n T/O VOC 8010/8020 @ 1115 MW-2 TOIC 14.6 19.9 1 5.3 0.84 4 5 B B n O VOC 8010/8020 Q 1135 MW-3 TOIC 13.9 20 6.1 0.98 5 6 P B n O-C VOC 8010/8020 Q 1315 MW-4 TOIC 14.1 19.95 5.85 0.94 4.5 5 B B n O VOC 8010/8020®1200 MW-5 TOIC 13.83 46.55 32.72 5.2 25 25 P B n O VOC 8010/8020 Q 1300 MW6 TOIC 13.58 46.43 32.85 5.2 25 25 P B n O VOC 8010/8020®1120 i MW-7 TOIC 13.61 45.72 32.92 5.2 25 25 P B n O VOC 8010/8020 Q It 55 MW-8 TOIC 13.06 45.72 32.66 5.2 25 26 P B n T VOC 8010/8020 Q 1355 TOIC Top of Inner Casing B Bailer Clear TOOC Top of Outer Casing P Pump Turbid Opaque bmp Below measuring point mS/cm Millisiemens per centimeter Well Casing Volumes °C Degrees Celcius n/a Not applicable 1.25" 0.06 3" 0.37 ft feet NTU Nephelometric Turbidity Units 1.50" 0.09 4" 0.65 mE/I milligrams per liter su Standard Units 2" 0.16 6" 1.47 No data umhos/cm Micmmhos percentimeter 2.5" 0.26 MONITORING WELL SAMPLING LOG Site Name: Bliane Hair School (Former Emerson's Cleaners) LAI anH is Favilomnental Technologies,Inc. Site Address: 18 Center Street, Hyannis MA 86 Faunce Coma Road,Suite 4 10 Project No: 5786 RTN: 4-10971 Dartmouth,MA ofax fax( (508)997-5422 508)999-0060 Sampler: LAS Page 1 of I Date: 9/29/00 E m 3 m 3 2 o ^ a' $ $ a ; o g ° `° o ^ > m > u H 6 9 61, ' •� g w 5 m E r e n x d U o f Sample Analyses Sam le ID a O — g � 3 aU aQ a h a U � n [— Z. U .. O rn MW-lo TOIC 14.43 21 6.57 0.27 1.3 1.5 B B n T VOC 8010/8020 Q 0935 TOIC Top of Inner Casing B Bailer Clear TOOC Top of Outer Casing P Pump Turbid Opaque bmp Below measuring point mS/cm Millisiemens per centimeter Well Casing Volumes °C Degrees Celcius n/a Not applicable 1,25" 0.06 3" 0.37 It feet NTU Nephelometric Turbidity Units 1.50" 0.09 4" 0.65 mg/1 milligrams par liter su Standard Units 2" 0.16 6" 1.47 No date umhos/cm Micromhos percentimeter 2.5" 0.26 APPENDIX D 1 . XAltlanfic® 1 1 1 1 1 1 Appendix D: 1 AET Soil Boring Logs (August & September 2000) 1 1 1 1 1 1 SOIL BORING LOG AB-1 Drilling Co: TDS Page 1 of 3 Driller: Mark Moran Environmental Technologies,Inc. Boring/ Helper: Date: 8/30/00 86 Faunce Comer Road,Suite 410 Monitoring Site Name: Blaine Hair School (Former Emerson Cleaner a Drilling Location: 1'-south&6'-east Dartmouth,MA02747 Well Site Address: 18 Center Street, Hyannis, MA ofS-1 (508)997-5422 Fax(508)999-4060 Spoon Diameter: 2 in. Sampler: EC Max Screen Depth Recovery PIDIFID Headspace NAPL Water Interval Blow Counts (in.) ( m) (Ppm (/n) Table in. Color Soil Description Sample ID 0.4 36 8 14.2 @ 3' n 12 B-m m-f So with cobbles(ash plat) 8010/8020 18 br m-fSa pebbles fill 0955 @ 3' 6 bk m Sa fill with slag) 4-8 36 10 11.3 @ 6' n 12 bk-br in Sa 8010/8020 8 br in Sa w/pebbles 1000 @ 6' 16 in m-fSa with s Si 8.12 36 4 3 @ IT n 8 br-bk Moist m-f Sa with Pebbles 8010/8020 28 br-m f Sa with s Si Fish Eye Sand 1005 @ IT 12.16 48 2.8 - n 14 24 br-tn Moist m-f sa 24 br-m Wet in Sa with s fines Boring Coal Pathched over 1020 PRIMARY CONSTITUENT:ALL CAPS Smndmd Colors: Soil Abbrevimiom: br Brown gr Grey w While Crr Gravel &mid f fine in inches bk Black r Red y Yellow Sa Sand s Some in medimn a feet bl Blue o Orange si silt I Lime c camse gr Green t Tan Cl Clay t Trace -to SOIL BORING LOG AB-2 Drilling Co: TDS Page 2 of 3 LA!alQnlaIc Driller: Mark Moran Environmental Technologies,Inc. Boring/ Helper: Date: 8/30/00 _ 86 Faunce Comer Road,Suite 410 Monitoring Site Name: Blaine Hair School (Former Emerson Cleaners) Drilling Location: 2'-west&4'-north Dartmouth,MA02747 Well Site Address: 18 Center Street, Hyannis, MA of S-2 (508)997-5422 Fax(508)999-4060 Spoon Diameter: 2 in. Sampler: EC Atax Screen Depth Recovery PIDIFID Ileadspace NAPL Water Interval Blow Counts in (Dom) m 1n Table (inj Color Soil Description Sample ID 04 136 3 5.8 @ 3' n 12 gi-In m-f Sa with cobbles(asphalt) 8010/8020 24 If m-fSa pebbles 11112 1025 @ 3- 4-8 21 3 - n 1 I br-lot Moist m-f Sa with s Si&Pebbles 8010/8020 10 br in Sa w/pebbles 1030 @ 6' 8-12 36 6 1 8.3 @ 12' n 36 br-bk Moist m-f Sa with s Pebbles 8010/8020 1035 @ 12' 12.16 42 0 3.6 @ 16' n 12 bk-br Moist in Sa with s cobbles 14 18 br-tn Very moist f-So with s Si 12 br Wet m-f Sa with s Si Boring Coal Pathched over @ 1055 PRIMARY CONSTITUENT:ALL CAPS Standard Colors: Soil Abbreviations: br Brown gr Gay w White Gr Gravel &and f fine in inches bk Black r Red y Yellow So Sand s Some in medium ft feet bl Blue o orange Si Silt 1 Little c caarse gn Green t Tan Cl Clay t Treae -to SOIL BORING LOG A -� Drilling Co: TDS Page 3 of 3 6LI1a'u" nF��'® Driller: Mark Moran Environmental Techno gies,Inc. Boring/ Helper: Date: 8/30/00 86 Faunce Comer Road,Suite 410 Monitoring Site Name: Blaine Hair School (Former Emerson Cleaners) Drilling Location: 4'-west&4'-south Dartmouth,MA02747 Well Site Address: 18 Center Street, Hyannis, MA ofS-7 (508)997-5422 Fax(508)9994060 Spoon Diameter: 2 in. Sampler: EC Maz Screen Depth Recovery PIDIFID Headspace NAPL Water Interval Blow Counts in. ( m) ( m) (/n) Table in. Color Soil Description Sample ID 0-4 42 7 48 @ 3' n 12 gr-tn ]a Sa with cobbles(asphalt) 8010/8020 18 br Moist m-f Se pebbles fill 1100 @ 3' 12 bk Moist in So with cobbles&Pebbles 4-8 36 3.7 5 @ 6' n 6 bk in Saw/pebbles 8010/8020 12 br Moist m-f Sa with s Si&Pebbles 1105 @ 6' 6 bk in So with s Si&pebbles 12 br Moist m-f Sa 8-12 36 0 0@ IT n 12 br-bk Moist m-f Sa 8010/8020 24 br-tn Moist m-f Sa with a Si 1115 @ IT 12-16 36 0 - n 12 br Moist m Sa with s pebbles 14 12 1 br-tn Very moist fSa 12 br Wet f Sa Boring Coal Pathched over 1130 PRIMARY CONSTITUENT:ALL CAPS Standard Colors Soil Abbreviations: br Brown gr Gray w White Or Gravel &and f fine in inches bk BlarJc r Red y Yellow So Sand s Some m rnedimn it feet bl Blue o Orange Si Silt 1 Little c coarse go Green t Tan Cl Clay t Trece -to man i i SOIL BORING LOG B.� Drilling Co: 'Fechnical Drilling Services Page 1 of 12 �tr1F�C© Driller: Mark Moran Envirortmenta Technologies,Inc. Boring/ Helper: Date: 9/25/00 86 Faunce Comer Road,Suite 410 Monitorin Site Name: Former Emerson Cleaners Drilling Location: 10 feet North Dartmouth,MA 02747 g Well Site Address: 18 Center Street, Hyannis Mass of AB-7 (508)997-5422 Fax(508)9994060 Spoon Diameter: 2 in. Sampler: EC Max Screen Depth Recovery PIDIFID Headspace NAPL Water Interval ( .) Blow Counts (in.) (PPm) (ppm) (v1n) Table (in.) Color Soil Description Sample ID 04 48 130 @ 4' Br [Top Soil Pebbles B.1(4)0855 ' 1 12 a 4' 97 @ 3' 32 @ 2' GTBr M-C Sand Gravel,some Cobbles Moist i 4.8 I 36 5.5 @ 7' 312 @ 6' B-1(7)0900 `. 275 @ 6.5' 12 Br Loamy Fill,M-F Sand 490 @ T 24 Br M-C Sand Moist 270 @ 8' Some Pebbles t I 8-12 I 48 0 @ 9' 55 @ 8.5' 12 Bk/Br Med.Sand,Moist 186 @ 9.5' 36 Br Med.Sand Moist 91 @ 10.5' 23@12' 12.16 ! 48 350@ 12' 36 Br M-F Sand,Moist B-1 (14)0910 1 1 0 Q 14 118 @ 13' 12 Br M-F Sand Saturated 14' 1 i i 0@14' r Standard Colors. Soil Abbmiaricns: In Bmraa g Gmy w White Gr Cre l &and f fine in inches bk Black r Red y Yellow Sa Sand s Some m medium fi feet bl Blue a onow Si Silt I Little c coarse w (hem t Ten Cl say t Tmee -to PRWARY CONSTITUENT:ALL CAPS SOIL BORING LOG Drilling Co: Technical Drilling Services Page 2 of 12 L&IanHc' B"2 Driller Mark Moran Environmental Technologies,Inc. Boring/ Helper' Date: 9/25/00 86 Faunce Comer Road,Suite 410 Monitoring Site Name: Former Emerson Cleaners Drilling Location: 23 feet South Dartmouth,MA 02747 Well Site Address: 18 Center Street, Flyannis Mass of AB-7 (508)997-5422 Fax(508)999-4060 Spoon Diameter: 2 in. Sampler: EC A4as Screen Depth Recovery PIDIFID Headspace NAPL Water Interval Blow Counts (in.) (PAM) (mom) Wn) Table (in.) Color Soil Description 0.4 i 36 0 @ 3' 0 8 Br To Soil Pebbles,Moist B-2(3)0925 j 0 OD 2' 28 1 Br IM-C Sand Pebbles i 0@1, 4 8 36 0 @ 4' 36 BrBk I M-F Sand Moist Till B-2(6)0930 0 @ 5' Pebbles/Glass 0@8' t 8-12 48 0 @ 9' 48 Br IMed.Sand,Moist,Pebbles i 0 @ I I' B-2(12)0935 0@IT 0 i i 12 16 i 48 0 @ IT 36 Br IMed.Sand Moist I 0 @ 14' 12 Br Med.Sand Saturated i 0 @ I B 0945 Driller Lost Drill Setup in B-2 i 6'x 6'French Drain 1045 Driller Retrieved Rig From B-2 r i Standard Culors'. Soil Abbreviations: br Bmsru gr Gray w White Gr Gmwl &and f fine m inches bk Blrk r Red y Ycllow Se Sand a Some m medium a feet bl Blue o O.L. Si Sit[ I Little c wane Greco t Ten CI Clay t Trace -to PRIMARY CONSTITUENT:ALL CAPS a ■� r �■ a r i a ■� r a r a r r r r r r SOIL BORING LOG Drilling Co: Technical Drilling Services Page 3 of 12 ��rIQ�F'C® B'3 Driller: Mark Moran FnvironmentalTee nologies,Inc. Boring/ Helper: Date: 9/25/00 86 Fetince Comer Road,Suite 410 Monitoring Site Name: Former Emerson Cleaners Drilling Location: 20 feet East Dartmouth,MA 02747 Well Site Address: 18 Center Street,Hyannis Mass of AB-7 (508)997-5422 Fax(508)999-4060 Spoon Diameter: 2 in. Sampler: EC Max Screen Depth Recovery PIDIFID Headspace NAPL Water Interval (ft.) low Counts (in.) (ppm) (ppm) (y/n) Table (m.) Color Soil Description Sample ID 04 36 1 0 Q I' 12 Bk-Gr As haWFi0/Concrete 4' B-3(3)1050 0 Q 2. 24 Br Med.Stutd,Moist OQ 3' I 4 g 36 0 Q 4' 24 Br Med.Sand B-3(6)1055 0 Q 6' 12 Br Mod.Send,Moist 0@8. i 6.12 48 D Q 9' 36 Hr M-F San Pebbles Moist B-3(12)1058 O Oa 11' 12 Br IFie S.d,Wel 0 Q 12' t 12 16 36 0 @ 12' 24 Br Fine Send Moist 0 Q 14' 12 Br Fine Sand SeNmted 0(ril 16' i i t t i Standard Colors. Soil Abbresiatio.' br Brown Sr Gay w White Or Grawl &and f fine in inch. bk Bloek r Red . y Yellow Se Sand a Smne on medium a feet bl Blue o Orenyc Si Sift 1 Lithe c oomee Sn Or"n t Ten CI Cloy t Two -to PRIMARY CONSTITUENT:ALL CAPS i i i i i i t i i t i r i i i i i i i SOIL BORING LOG B-4/AW-10 Drilling Co: Technical Drilling Services page 4 of 12 LAI'lonlaic" Driller. Mark Moran Environmental Technologies,Inc. Boring/ Helper: Date: 9/25/00 86 France Comer Road,Suite 410 Monitoring Site Name: Former Emerson Cleaners Drilling Location: 2 feet from Fence Dartmouth,MA 02747 Well Site Address: 18 Center Street,Hyannis Mass Grass near Street (508)997-5422 Faa(508)999.4060 Spoon Diameter: 2 in. Sampler: EC Max Screen Depth Recovery PID/PID Ileadspace NAPL Water Interval ( , Blow Counts (in.) (ppm) (ppm) (F/n) Table (in.) Color Soil Description Sam le ID 0.4 f 24 1 0 Q I' 312 Q 2' 24 1 Bk ILmany Sod with Pebbles B-4(2)1110 128Q2' i 4-8 t 36 537 Q 4' 12 Bk Loam Fill/Coal B-4(4)1120 i 186 a 6' 12 RIBr Brick 4" M-F Sand 306 Q 6' 12 Br Fine Send Moist i 8-12 1 40 6200 8' 0 20 BkBr M-F Sind Moist 1 705 Q 10, 20 Br Fine Sand Moist B4(10)1125 i 630 @ 12, i 12-16 I i 48 97 Q12' 16 Br Mod,Sand Moist Well Installed Q 1200 to 58 Q 14' 20 Br Fine Sand Wet 21'BSG 0 Q 16' 12 Br Fine Send Saturated 6.5'of H2O Q 14.5'BSG i 1 t r t Sianderd Colors. Soil Abbooatians: Its,Brown B trolly w white or Gre`el &and f fins in inches bk black r Red y Yellow Ss Send a Some no medium 'a feet bl Blue o Oran, Si Sib I Linle c coarse yn Green t Ten Cl Clay t Trans -to PRIMARY CONSTITUENT:ALL CAPS SOIL BORING LOG Drilling Co: Technical Drilling Services page 5 of 12 L&IV' nfic' B-S Driller: Mark Moran Environmental Technologies,Inc. Boring/ Helper: Date: 9/25/00 86Faunca Comer Roed,Suhe4l0 Monitoring Site Name: Former Emerson Cleaners Drilling Location: 19 feet South of B-4 Dalu nedt,MA 02747 Well Site Address: 18 Center Street,Hyannis Mass Driveway Enterence (509)997-5422 Fee,(508)999-4a0 Spoon Diameter: 2 in. Sampler: EC 15 feet from Street Max Screen Depth Recovery PID/FID Headspace NAPL Water Interval Blow Counts (in.) (oom) (oom) (v/n) Table (m.) Color Soil Description Sample ID 0-0 48 99 Q 1' 12 Or mplinaft,Tpend 9-5(4)1225 34 n 2' 48 24 Br M-F Send 119@4' 10 Br M-F Sand i 2 Bk Asphalt 1 4.8 136 523 Ca 4' 16 Bk Mod. Mona B-5(8)1232 449 n 6' 0 10 Br Med.Send,Pebbles - 47.1 @ 8' 1 10 Br IM-F Sand with some Pebbles 8.12 42 270 @ 9' 0 12 Br Mod.Sand,some Loan✓Ped B.5(12)1240 j 25 @ 10 40 Br Fine Sand 1 1 32@IT 1246 36 0 n 12' 12 er Fine Siuxl,Moist,Pebbles Soil snnk in MiauC n: I 0 rr 14' 24 Br Fite Sand,Wet sampler due to Inge oobble Oro, 16 I I I i Standard Color. Soil Abbreviations: br Brown sr Gay w Wh4e Gr Orewl 8c end f fine in inchm bk Black r Red y Yellow Se Send a Some no medium 8 feet Ill Blaa .0'.." Si Sift I Lntk a loan. gn Breen t Tan Cl Clay t Tmce -to PRIMARY CONSTITUENT:ALL CAPS SOIL BORING LOG L Drilling Cc: Technical Drilling Services - Page 6 of 12 B-6 Driller.' Mark Moran Environmental Technologies,Inc. Boring/ Helper: Date: 9/25/00 86 Faunce Comer Road,Suite 410 Monitoring Site Name: Formcr Emerson Cleaners Drilling Location: 8 feet from Building Darbnouth,MA 02747 Well Site Address: 18 Center Street. Hyannis Mass 2 feet in from comer (508)997-5422 Fax(508)9994060 Spoon Diameter: 2 in. Sampler: EC of Building Max Screen Depth Recovery PID,'FID Headspace NAPL Water Interval Blow Counts (in.) (pom) (Pont) (vin) Table in.) Color Soil Description Sample ID 04 i 18 0 0 7 Bk As halt B-6(3)1320 IS 0 11 Br M-F Sand 4-8 I 20 0 @ 4' 10 BI Br Med,Send,Saturated,Pebbles B-6(6)1325 i 0 @ 8' 10 Br/Gr M-F Sand with Pebbles r 8-12 i 24 0 @ 8' 6 Br Coarse Send w th Pebbles Saturated B-6(12)1330 0 @ 10' 12 Br Coarse sand with some fines Wet,Pebbles 0 @ IT 6 Br Fine Sand,Wet r t 12.16 I 48 0@ IT 12 Br Mod.Sand Saturated Pebbles Odor of Hair Products/Soap 0 @ 14' 36 Br Fine San Saturated 0 Gil 16' Boring was conducted i between marked sewer& water services. t i Standard(V.ra Sod Abb,..u., br Brawn F Gay w White Gr C"acel &and f fine in inch., bk Black r Red y Yellow S.Sand .Some m m.dium fl fe.t b1 Blue "Orange Si Sib I Lade c Wam area" i Ten Cl Clay t Tnwa -to PRIMARY CONSTITUENT:ALL CAPS SOIL BORING LOG B_7 Drilling Co: Technical Drilling Services Page 7 of 12 ��rla 'C.© ' Driller: Mark Moran Environment Tec ologtes,Inc. Boring/ Helper: Date: 9/25/00 86 Faance Comer Road,sore 410 Monitoring Site Name: Former Emerson Cleaners Drilling Location: 17 feet East of B-3 Dartmouth,MA 02747 Well Site Address: 18 Center Street, Hyannis Mass 6 feet North of Asphalt (508)997-5422 Fast(508)9994060 Spoon Diameter: 2 in. Sampler: EC Located in Shrubs Max Screen Depth Recovery ND/F/D Headspace NAPL Water Interval Blow Counts (in.) (ppm) (ppm) Win) Table (in.) Color Soil Description Sample ID OA r1 28 0 @ I' 12 1 In 17ropoill Loam B-7(3)1405 ! 0 @ 2' 0 16 Bk-Br Fd C-M Sand Glass 0 4 4.8 I 36 0 @ 4.5' 6 Bk Med.Sand,Pebbles B.7(8)1410 0 @ 6' 0 4 R Med.Stand,Pebbles ! 0 @ 8' 26 R/Br M-F Sand Moist,Pebbles 9-12 ! 42 0 @ 8' 1 42 Br IM-F Sand Moist some Pebbles B-7(12)1415 f 0@10- ! 0@ IT 12 16 I i 48 0 @ 12' 16 Br M-F Sand Moist 0 n 14' 28 Br M-F Sand Wet o a 16' 4 Br Fine Sand Sla ueted t ! i ! j Standard Colors a Soil Abbrewtiote: br Brown &Gay w White Gr Grewl Rend f fine in inches Its Black r Red y Yellow Sa Sand a Some m medium fl feet bl Blue o Granae Si sat I Lino c cause Gruen t Tan CI any t Traw -to PRIMARY CONSTITUENT:ALL CAPS �■ WON MMMMMMMM m m m m mww m SOIL BORING LOG B_8 Drilling Co: Technical Drilling Services page g Of 12 LAH,anHc Driller: Mark Moran Environmental Technologies,Inc. Boring/ Helper: Date: 9/26/00 86 Pounce Comer Road,Suite 410 Monitoring Site Name: Former Emerson Cleaners Drilling Location: 14 feet South of Dartmouth,MA 02747 Well Site Address: 18 Center Street. Hyannis Mass Catch Basin (508)997-5422 Fax(508)9994060 Spoon Diameter: 2 in. Sampler: EC Located on Asphalt . btar Screen Depth Recovery PIDIFID Headspace NAPL Water Interval Blow Comas (in.) (Ppm) (Pont) (vin) Table (in.) Color Soil Description Sample ID 04 1 1 36 0 I' 12 Bk As he Med.Send B-8(3)1000 0 Ca 2' 0 24 Br/Bk Med.Sand i 0 @4' 4.8 36 0 @ 4' 12 Bk C-M Sand Pebbles B-8(8)1010 0 @y 6' 0 12 Br Coarse Sand Pebbles i 0 8' 12 Br Med.Sand some Fine Sand 8.12 48 0 Ca 8' 12 1 Br C-M Send Moist some Pebbles B-8(12)1015 0 @ to, 0 36 Br Fine Sand 0 @ 12' I 12-16 ' 1 i 38 0 14 Br Med.Sand Fine Sand Pebbles Liner Stuck in Sampler due I 12 Be Fine Sual Moist to large cobble. 12 Br Fine Send,Saturated - Soil put onto asphalt. i Catch basin located 32'from sidewalk and 3'south of 1 grass. I Stenderd(Wm Sail Abbre.uam: br Brown gr Crrey w White Or Gravel &and f fine in inches bk aback r Red y Yellow Sa Send s Some re medium 0 feet b1 Blue o Orenac Si Sill - I Line c come P Given t Tan cl Clay t Trace -to PRIMARY CONSTITUENT:ALL CAPS M I SOIL BORING LOG B_9 Drilling Co: Technical Drilling Services Page 9 of 12 L&IanFic' Driller: Mark Moran Environmental Technologies,Inc. Boring/ Helper: Date: 9/26/00 86 Fatmce Comer Road,Suite 410 Monitoring Site Name: Former Emerson Cleaners Drilling Location: 8 feet North of C.B. Dennrouat,MA 02747 Well Site Address: 18 Center Street,Hyannis Mass Near Pole with (508)997-5422 Fan(508)999-4060 Spoon Diameter: 2 in. Sampler: EC Underground Line(?) A4=Screen Depth Recovery PID/FID Headspace NAPL Water Interval (R.) Blow Counts (in.) (Dom) (DOM) Nln) Table (irr) Color Soil Description Sample ID 0-4 1 30 0 8 1 Br ITop,61,Loam B-9(3)1035 I 0 8 Or Coarse Shed,Gravel,Pebbles i 0 14 Br Coarse Sand With Pebbles and Brick 4-8 1 24 0 @ 4' 12 Br Loam Soil and Med.Sand,Pebbles 0 7 12 Br M-F Semi,Moist 0 &12 I 42 0 @ 8' 12 Br Mnd.Send,some Fir;Sand,Pebbles &9(9)1045 i 0 r@ 10' I 18 Br lFine Send 0 @ IT 0 4 1 er M-C fishey,San if;Moist 1 8 1 Br Fine Sand,Moist 12-16 148 0©12' 12 Br M-F Sand,Moist,Pebbles B-9(14)1055 0014' 24 Br M-F Sand,We 0 @ 16 12 Br Fine Send,Saturated i Pole is 36 feet them sidewalk. f f Standard Colors: Sod Abbreviations: In Bmwi an Cm w Whne Gr Camel &end t fuK in inches bk Back r Red y Yellow Ss Send s Some m medium a fost bl Blue o Dome St Sift 1 Little c coarse gn them t Ten Cl Cley tT. -to PRIMARY CONSTITUENT:ALL CAPS �■1� m f' = cam MAN SOIL BORING LOG 4 B•10 Drilling Ca: Technical Drilling Services Page 10 of 12 �Flani ie� Driller. Mark Moran Environmental Technologies,Inc. Boring/ Helper: Date: 9/26/00 86 Feunce Comer Road,Suite 410 Monitoring Sile Name: Former Emerson Cleaners Drilling Location: 12 feet North of Dartmouth MA 02747 Well Site Address. IN Center Street. I lvannis Mass _ West Bulkhead (508)997-5422 Fm(508)999A060 Spoon Diameter: 2 in. Sampler: GC ,Flax Screen Depth Recocep PIDJ7T) Headspace NAPE Water Interval ( . Bloat Counts on.) RmnU (roll) (rvn) Table (in.1 Color Soil Description Sample ID 04 24 (1 6 Bk As halt n B Br Coarse Sand 0 4 Gr Contoete/Rubbie 6 Br Med Sand with Pebbles i 4-9 IR Br-Tn Redusid C-M Sand with Cobbles I { I I I l - i I I Standard Colon Soil Abbra,natiom: br Brown yr(bey w t\bile G(Gaol & and f fine in inches bk Black r Red y Yellnw Sa Sand s Some as medium R feet bl Blw n Omni, Si Silt I Lime c course pi Green t Tan Cl Clay t Trace -to PRIMARY CONSTITUENT:ALL CAPS - SOIL BORING LOG Drilling Co: 'Technical Drilling Services Page I of 12 LAManHic B" Driller Encironimntal Technolo ies,Inc. Mark Moran 8 " Boring/ Helper.' Date: 9/26/00 86 taunce Comer Road,Suite 410 Afonitoring Sile Name: Former Emerson Cleaners Drilling Location: 2 feet West of B-10 Dartmouth,MA 02747 Well Site Address: 18 Center Street. I h'annis Mass (508)997-5422 Fax(508)9994060 Spoon Diameter: 2 in. .Sampler.' EC ,1 fro'J'creen Depth Recovery P/1)'P 11) fleudsprice A'APL Hater hilemal h. Blow Limner (m i (Ppm) (pp"') O"'n) Table Color Soil Description Sample ID 0-4 Refusal t i Standard(A... • Soil Abbredatrons- ba Brown P Cnay w N'hac Or Grawl & end f fine Ln inches bk Black r Red Se Sand s Some an medium R feei bl Blue o 0'.a- Si Silt I Link c coarse gn Oreen i'fnn Cl Clay t Trace - to PRIMARY CONS]It LEN'P:ALL CAPS SOIL BOWNG LOG DrilNiNCo. FechnicalDrillitr, Services Page 12 0f 12 L��}Af''/I�nfiC.o B-12 --------- - V Drillar. Mmk Moran — IllvirnnnKutal l'echuolohick. Inc. Borings flelpir. --- __ -- Date: 9/2EKIO Sw l ammo Corre td r Ro ,Suds 4 1p Monitoring Site Name: Former F'."lei sort Cla;aners_ — Drilling Locution: 12 feel.North of — oa,nnowh.b1A a2'7.17 Well .Site;lddres.v: ISCentei, StreQt. IlvannisNlass East Side of 0;;)9v7.< ,2 iatiii8)+xta-un;o Spoon.DianwlC,v --2 ill, —�--- Sarnrder: EC Bulkhead. -- Depth Rccurrri Fill 1i% Hcwhpao? :b IPL li'aler Interval n. 131011.Colollc gtpw; h'rxl 7'uFle (in., Color Soil DDscriplioti SO; I9 04 ±S li --- — -- 4 R1. As llt li'I_r_.IL15_.,v_•. 16 Rr bled.Sand.Pchbles -- — 8 G.-Br Med,Sand Cobhles---�y.____,_ 4 8 ,li— _—t -- --.—__ —__ -- — GrrRr Ided.Sand fco nanv[obli _.--_ — — -- t — -- 10 Rr Med.Sand with Cobbles,Concrete —t: --- --- --- 5 fit Itled.Sand with Pebhles 8.12 34 —f —_—_ _-- _ 4 Bt Med.Sand.Moist _.- - 3 W. Med.Sand milli Silt.YVe((WondtGlass) ._, __— 13 12(9i 11'i1r_.__—_.— 3 GI Cobble,Concrete 24 [it' M-F:land.Moist 12-16 ,16 ,I_�— -- --- 10 Rr bled.Sand,some wncrc4 11-12(14) 1158 _.- -1 IN lit' Fine Sand.Moist — — —_ _ -- 8 Rr Fine Sand.Satumtul Soil Abbreviations — — tv Brmtn (it Grovel &aid f line in -.anon. bk Black r Rd rcllan Sa Sad s Sarre m mediun. fl fc:a bl Blur: o I)u'aw Si Sill I Little e wane @t Cheet I -tan CI CIq I -ae -+u PRIMARY CONS"I'ITUEN'I*ALL.CAPS APPENDIX E �w w■ w w w w w w w w w w w w w w w w w IQAtiantic 1 1 i 1 1 1 Appendix E: 1 MADEP RAO Statement (BWSC 1-4) 1 1 1 1 i 1 1 1