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HomeMy WebLinkAbout1140 IYANNOUGH ROAD/RTE132 - HAZMAT (3) i • i , r � r f + s�. e e4 k"f'. ;g. .rs ��.. u . yds.* i. }A{ 'A' 3 ✓ 6 "�� �'� �id T'%:1 � �5,p ;� a 6.r�.�� `ry :!, �' t,:.r�4 �' N.'ld,� `0.ycr'd[tt ,. .Y 4Ea. . ,. a aI :d t. 1. y [ •M'Y K, K :� �'Y tlf �'µ r•'".A pc r tl •,ti 'F „Jw� ''�+.,Ns...� m F k.. 4-. 1 .9. 1. .f a �., �. ` "� x' e .. ''�,..+w-. ... „ �. R ,�Ri'. ��� p,y � 1 .y c�� r�•t"re � .bry �I.."5't}�y � .'«�+' a,r to ��+ �y� �'u � rye: Ft:. a �, c - t t 7 •.f *.'= .�. .,,:�(. a •��'.' Sut �"`.a �� �n ;� F �t�taf - t s r ....:, � ,r,,. ..d5dr7 .. e .:. .:>.,., „�.,.�...;. :.,... ,< .. ..�. .. �33 ,.a. ,,...,�. . .,.. '>s .. d......_•s �..r':; x L:: `�, `.vr, a d• ..-:. -3.'�.tiS r+ ... .+_ ,.k. ....,.• rt. ..j .y M. ...... .5. `} [� .q •k['.3 �-:f ?jl.; 'dr,:l Y"`. 'r .'k'. -,3j' ^•`z > c.�;, a .,,; ., Is .l e y9}+', r. +`�� F;� e - Y a I. "�� �4w v ,+•: 7� r. 'i' a a', .,: # t w >t- I s+ , <,.:�,r� e4..: �+:- ... t'7+ c=.'.„ •,!.5.� t' 1. ,. .'. i.- ,5 '°*5 Sz�, �3 ,i.e.�,. a..,�. i, ;*:.. +sk..:. �. >3;., ,,, .rt, 'N�: *- 3S �;;ew j=_ ,r sa e'#��` _c" ,�`e-� 1• a b. ,p,: >,✓- e IMMEDIATE RESPONSE ACTION PLAN DESIGN SPECIFICATION TEXACO SERVICE STATION #100083 J140 IYANNOUGH ROAD '1_ HYANNIS,MASSACHUSETTS RTN#4-11301 August 2002 Prepared by: Prepared for: Geologic Services Corporation Equiva Services LLC 15 Bonazzoli Avenue P.M.B. 301 Hudson, MA 01749 1830 South Road,Unit 24 (978)568-8740 Wappingers Falls, NY 12590 (845)462-5225 GSC Project No. 000509C BIBLIOGRAPHY OF REPORTS Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts Date of Report Title of Report Prepared By July 16, 1,991 Bay Drain Closure Letter HETI November 1991 Report on Site Inspection and Records Review HETI December 28, 1994 21E Site Assessment(Cooke's Restaurant) D.C.E. June 6, 1995 Notice of Responsibility MA DEP August 11, 1995 Release Notification Form Motiva October 12, 1995 Phase I-Initial Site Investigation Report GES February 22, 1996 Initial Groundwater Monitoring Report Handex July 23, 1996 Groundwater Monitoring Report GES August 15, 1996 Decision to Grant Permit Letter MA DEP October 9, 1996 Groundwater Monitoring Report GES October 28, 1996 Immediate Response Action Plan GES Immediate Response Action Transmittal Form July 23, 1997 Phase II-Comprehensive Site Assessment GES Scope of Work June 26, 1997 Groundwater Monitoring/IRA Status Report GES March 23, 1998 Groundwater Monitoring/IRA Status Report Sage August 13, 1998 Modification to Phase II-Comprehensive Site Assessment Sage Scope of Work March 1998 IRA Status Report Sage September 30, 1998 IRA Status Report Sage March 4, 1999 IRAP Modification Sage May 1999 Phase 11 Extension Request Sage October 1999 IRA Status Report Sage June 2000 Phase II-Comprehensive Site Investigation and Phase III Sage Remedial Action Plan February 16, 2001 IRA Status Report GSC May 9, 2001 IRA Plan and Status Report GSC June 11,2001 IRA Completion Report(RTN 4-16161)and Modification GSC of IRA Work Plan Activities(RTN 4-11301) September 6,2001 IRA Status Report GSC March 6,2002 IRA Status Report GSC August,2002 IRA Plan Design Specification GSC HETI-Hydro-Environmental Technologies,Inc. D.C.E. -Down Cape Engineering, Inc. MA DEP -Massachusetts Department of Environmental Protection GES - Groundwater.&Environmental Services,Inc. Sage- Sage Environmental,LLC Handex -Handex of New England, Inc. GSC -Geologic Services Corporation Ref.#000509C. IRAPDS LIST OF APPENDICES Appendix A - Figures Figure 1 - Locus Plan Figure 2 - Site Plan Figure 3 - Area Plan Figure 4 - GIS Map and Legend Figure 5 - Groundwater Contour/Hydrocarbon Distribution Plan— 12/4/01 Figure 6 - Groundwater Contour/Hydrocarbon Distribution Plan—5/1/02 Figure 7 - Proposed Well Network Layout and Conceptual Radii of Influence Figure 8 - Proposed Trench Layout Figure 9 - Trench Cross Section and SVE/AS Well Head Construction Details Figure 10 - Process&Instrumentation Diagram Figure 11 - Process&Instrumentation Diagram Legend Appendix B - Tables Table 1 - Monitoring Well Gauging Data Summary Table 2 - Groundwater Sample Analytical Results—Volatile Petroleum Hydrocarbons Table 3 - Groundwater Sample Analytical Results—Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Table 4 - Historical Soil Analytical Results—Volatile Petroleum Hydrocarbons Table 5 - Summary of SVE Step Test Table 6 - Summary of SVE/AS Pilot Testing Data Table 7 - Summary of SVE/AS Pilot Test Data—Monitoring Point Data Table 8 - Summary of SVE/AS PilotTesting Data Table 9 - Summary of SVE/AS Pilot Test Air Sample Analytical Data at SVE-1 Appendix C - Groundwater Analytical Results Appendix D - Well Logs Appendix E - Soil Sample Analytical Results Appendix F - Charts Chart l - Applied Vacuum at SVE-1 vs. Flow Rate Chart 2 - Normalized Vacuum vs. Distance from SVE-1 @ 5"H20 Chart 3 - Normalized Vacuum vs. Distance from SVE-1 @10"H20 Chart 4 - Normalized Vacuum vs. Distance from SVE-1 @1.3"H20 Chart 5 - Influent VOC Concentration vs. Time Chart 6 - Groundwater Mounding vs. Time Chart 7 - Dissolved Oxygen Content vs. Time Appendix G - Air Sample Analytical Data Ref.4000509C. IRAPDS Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts MA DEP RTN 4-11301 I. Person Conducting Immediate Response Action,pursuant to 310 CMR 40.0424(1)(a) On behalf of Motiva Enterprises LLC(Motiva), Equiva Services LLC (Equiva) is conducting the Immediate Response Actions(IRA)referenced herein. Motiva is the owner and operator of the subject site. The Equiva representative overseeing the response actions in connection with this IRA is Mr. David B. Weeks. Equiva has retained Geologic Services Corporation(GSC)and Scott K.Parker(Licensed Site Professional#9969)as their consultant and LSP-of-record. II. Background The subject property was listed by the Massachusetts Department of Environmental Protection(DEP) based on information reported in a December 28, 1994 21 E Site Assessment Report,prepared by Down Cape Engineering, Inc. (DCE)for Cooke's Restaurant located downgradient of the site at 1120 Iyannough Road,Hyannis,Massachusetts. Cooke's Restaurant is the abutter to the east of the subject property. As part of this site assessment,DCE collected groundwater samples from three monitoring wells located on the Cooke's Restaurant property. Laboratory analysis indicated the presence of benzene,toluene, and xylenes in the sample obtained from a well reported to be downgradient of the Texaco Station. Release Tracking Number(RTN)4-11301 was issued by the DEP on April 6, 1995 in response to these findings. Resulting from the 2 1 E Site Assessment of Cooke's Restaurant,the DEP issued a Notice of Responsibility(NOR)to the owner of the Star Enterprise(Star)property located at 1140 Iyannough Road in Hyannis,Massachusetts on August 11, 1995. On October 12, 1995, Star,now Motiva, submitted a Phase I-Initial Site Investigation Report and Tier IC Application to DEP for the subject site. During the Phase I investigation, groundwater sampling results of the on-site monitoring wells revealed dissolved- phase petroleum constituents in excess of the DEP reportable concentrations for GW-I groundwater standards. The DEP approved the Tier IC Permit Application(No. 100556)for the subject property on September 12, 1996. At this time it was determined that a Substantial Release Migration(SRM)condition may exist and the DEP required an IRA Plan to be submitted. Star submitted an assessment-only IRA Plan proposing tri-annual groundwater monitoring for a one-year period to evaluate seasonal changes in groundwater elevation and quality. A Phase 11 Scope of Work(SOW)was submitted by Groundwater&Environmental Services,Inc. (GES) on July 25, 1997 for additional subsurface investigations to be completed. This work included the installation of additional monitoring wells and additional groundwater sampling. On September 18, 1998, SAGE Environmental(SAGE) submitted an IRA Status report summarizing the installation of three monitoring wells and the advancement of five soil borings. Groundwater samples were collected from ten on-site monitoring wells on May 6, 1998 and analyzed for extractable petroleum hydrocarbons(EPH) and volatile petroleum hydrocarbons(VPH). Soil analytical results for this sampling event indicated concentrations of methyl-tert butyl ether(MTBE) above applicable S-I/GW-1 soil standard from MW-9 and SB-11. Dissolved phase petroleum constituents were detected above applicable GW-1 standards for all wells sampled except MW-3. Ref.#000509C. IRAPDS SAGE submitted a Modification to the Phase II SOW on August 13, 1998 for the installation of off-site monitoring wells, well surveying, groundwater sampling,a soil vapor extraction(SVE)pilot test, and a limited pump test. SAGE was unable to secure off-site access for the installation of downgradient monitoring wells. However,the SVE pilot test and groundwater sampling were completed on March 25, 1999 and June 4, 1999,respectively. SAGE indicated that the results of the SVE test were skewed due to recent construction activities that may have caused short-circuiting in the airflow diminishing the effective radius of influence. On March 4, 1999, SAGE submitted a Modification to the IRA Plan in response to extensive excavation activities proposed at the site. The modification addressed excess soil to be generated during the installation of a new pump islands and canopy foundations and the removal and replacement of two leaching catch basins. It included a work scope for the soil testing of excavated soils,confirmatory sampling, and management of excavated soils. Approximately 556.75 tons of soil was removed from the site on March 4 and 5, 1999 for reuse at a landfill. Approximately 188.47 tons of petroleum impacted soils was transported to an off-site disposal facility for recycling on March 24, 1999. On August 22, 2000, SAGE submitted a Phase II—Comprehensive Site Assessment and Phase III— Remedial Action Plan(RAP). Groundwater extraction combined with soil vapor extraction technologies were selected as the remedial action alternative for achieving a permanent solution at the subject property. Following review of the Phase II and III Reports, additional delineation of the dissolved phase petroleum hydrocarbons related to the subject property was viewed to be warranted prior to the selection/implementation of a remedial action. In conjunction with the installation of the groundwater monitoring wells,pilot test air sparge(AS)and SVE wells were installed at the subject property. In March of 2001, GSC and Motiva were able to secure off-site access to abutting properties. Between March 19 and 23,2001, GSC personnel supervised the installation of four 2-inch diameter groundwater monitoring wells MW-11,MW-12,MW-13, and MW-14 at and in the vicinity of the subject property in order to further delineate petroleum impact to soil and groundwater. During groundwater monitoring well gauging and sampling activities performed on April 4, 2001, approximately 0.60 feet of non-aqueous phase liquid(NAPL)(i.e.; weathered gasoline)was detected in monitoring well MW-9. The DEP was verbally notified of the presence of greater than 0.5 inches of NAPL on April 5,2001. The DEP subsequently assigned RTN 4-16161 to this 72-hour release condition and verbally approved passive NAPL bailing activities under an IRA. On April 12, 2001,Tanknology—NDE of Springfield,Massachusetts performed a pressure tank tightness test for the gasoline underground storage tank system at the subject property. All the pressure tests performed on the underground storage tank(UST) system passed on this date. On June 8,2001 Motiva submitted a Tier IC Permit Renewal Application to the DEP in order to allow for the continuation of response actions under RTN 4-11301. In addition,the Tier I Permit application detailed the linking of RTN 4-16161 to lead RTN 4-11301. On September 27,2001 a Decision to Grant a Tier IC Permit Extension was approved by the DEP. An IRA Status Report was submitted to the DEP in March 2002 detailing NAPL recovery and assessment activities during the period of August 2001 through January 2002. Additional information pertaining to previous report submittals and response activities can be found in the reports listed in the"Bibliography of Reports"at the front of this document. Ref. #000509C. IRAPDS III. Description of Site Conditions/Surrounding Receptors,pursuant to 310 CMR 40.0424(1)(b) Local area topography slopes in a southerly direction toward Iyannough Road. The subject property is situated at 1140 Iyannough Road in Hyannis,Massachusetts and is currently an active Texaco branded retail gasoline and automobile repair facility. The subject property has an area of approximately 47,916.19 square feet(I.1 acres). The majority of the site is paved with asphalt or reinforced concrete, except a small area in the southern portion of the lot,which is landscaped. The northern portion of the property is wooded and covered in gravel. The properties in the vicinity of the subject site are primarily used for commercial purposes. The single-story Texaco station houses an office area,restrooms, and three repair service bays and also used as a parking lot for school buses. One 12,000 gallon gasoline UST,two 10,000 gallon gasoline USTs,one 8,000 gallon diesel fuel UST,and one 550 gallon waste oil UST currently exist at the site. The site is serviced by municipal water supply and sewer as well as underground telephone and electric service utilities. The subject site drainage system is connected to an on-site leachfield located immediately east of the service station building. Two detention drainage basins are located approximately 80 feet southeast and 90 feet north of the convenience store,respectively. Please refer to Figures 1,2, 3, and 4(Appendix A) for a depiction of the subject property and surrounding area. - According to the United States Geological Survey(USGS)Hyannis,Massachusetts 15 Minute Topographic Quadrangle, a portion of which is provided as Figure 1,the subject property has an elevation of approximately 78 feet above mean sea level(MSL). IV. Description of Release/Threat of Release,pursuant to 310 CMR 40.0424(1)(b) RTN 4-11301 During the review of the Tier IC Permit Application in September 1996, a Condition of SRM was viewed by DEP to be possible at this site. This was based on the presence of petroleum constituents on the abutting property and Texaco property in excess of the GW-1 groundwater standards and the nature of the groundwater in this area. Another IRA(RTN 4-16161)was linked to this RTN(RTN 4-11301) in 2001 due to NAPL present in groundwater monitoring well MW-9. V. Description of IRA Activities Conducted to date,pursuant to 310 CMR 40.0424(1)(c) IRA activities conducted at this site have included the monitoring of groundwater in the site vicinity, soil removal, and passive NAPL bailing. The lead RTN(4-11301)was related to a potential condition of SRM. During site upgrade activities, soil removal and disposal was added to the IRA plan originally submitted for this site. In April 2001,NAPL was discovered in an on-site monitoring well triggering another IRA condition and RTN 4-16161. Passive NAPL bailing has been ongoing at this site. Gauging data is included in Table 1 (Appendix B). The groundwater analytical results for the site are included on Tables 2 and 3 (Appendix B). Groundwater contours have been prepared for the December 4, 2001 and May 1, 2002 sampling events and are included as Figures 5 and 6(Appendix A)respectively. Complete laboratory analytical results for the past two events are included in Appendix C. VI. Objective,Plan, Schedule for Continued IRA Activities, pursuant to 310 CMR 0.0424(1) (e&g) Additional activities anticipated for completion during the course of this IRA include the completion of additional Phase 11 delineation activities and additional field research and reconnaissance to determine the full extent of this disposal site. Ref. #000509C. IRAPDS \ VII. Summary of SVE/AS Pilot Test Drilling Activities Prior to the SVE/AS pilot test, GSC supervised the installation of one AS well(AS-1), one SVE well (SVE-1), and three triplet monitoring points(MP-1 through MP-3)at the site on March 14, 2001. Drilling was conducted by Geosearch Inc., of Sterling, Massachusetts utilizing a truck-mounted hollow- stem auger drill rig. The AS well was installed to a total depth of approximately 49-feet below grade, constructed of 47-feet of 2-inch diameter Schedule 40 PVC riser with 2-feet of 2-inch diameter Schedule 40 PVC 0.010 slot well screen at the base. The borehole annulus of the well was finished with a sand pack to approximately 2-feet above the top of the well screen, a 2-foot bentonite seal, grout to approximately 4-feet below grade, and back-filled to grade with native material. AS-1 was finished with a flush mounted, 8-inch road box, incased in a 2-foot by 2-foot concrete pad. The location of this well is shown on Figure 2. Soil samples collected during these drilling activities were screened in the field with a photoionization detector(PID)calibrated to read total VOCs in parts per million by volume(ppm,,)as benzene. The PID screening results are depicted along with well construction details on the well logs included in Appendix D. The SVE well was installed to a total depth of approximately 36-feet below grade, constructed of 26-feet of 4-inch diameter Schedule 40 PVC riser with 10-feet of 4-inch diameter Schedule 40 PVC 0.010 slot well screen at the base.The bore hole annulus of the well was finished with sand packs to approximately 2-feet above the top of the well screen,a 2-foot bentonite seal and back-filled to grade with native material. SVE-1 was finished with a flush mounted, 12-inch road box, and incased in a 2-foot by 2-foot concrete pad. The location of this well is shown on Figure 2. Soil samples collected during these drilling activities were screened in the field with PID calibrated to read total VOCs in ppmv as benzene. The PID screening results are depicted along with well construction details on the well logs included in Appendix D. The three triplet monitoring point bore holes were advanced to a total depth of approximately 43-feet below grade, with the points constructed of 25, 37, and 41-feet of 1.5-inch diameter Schedule 40 PVC riser with 10, 2, and 2-feet of 1.5-inch diameter Schedule 40 PVC 0.010 slotted well screen at their bases, respectively. Refer to Appendix D for the well construction details and PID screening results.MP-1 through MP-3 were fmished with flush mounted, 12-inch road boxes, and incased in 2-foot by 2-foot concrete pads. The locations of these wells are shown on Figure 2. Soil samples collected during these drilling activities were screened in the field with a PID calibrated to read total VOCs in ppm,,as benzene. The PID screening results are depicted along with well construction details on the well logs included in Appendix D. During the installation of these wells, GSC personnel collected one soil sample from each boring and submitted them to Accutest, for analysis of target VOCs, and VPH fractions via DEP-Approved Methodologies. As noted in Table 4(Appendix B),no compounds were detected above the method detection limit. Complete analytical results from soil samples collected on March 21 through 22,2001 are included as Appendix E. VIII. Summary of SVE/AS Pilot Testing Activities On May 4, 2001, GSC conducted a combined SVE/AS pilot test on wells SVE-1 and AS-1. The principal purpose of the SVE portion of this pilot test was to determine the feasibility of soil vapor extraction as a potential remedial option for this site. Prior to the initiation of the SVE pilot test, a step test was conducted on SVE-1 to determine the relationship between applied vacuum and soil vapor flow from this well. During the step test,the vacuum at the wellhead was allowed to stabilize, flow rates were recorded, and then the vacuum was increased Ref. #000509C. IRAPDS until a maximum flow rate was established or water was pulled into the system. Refer to Table 5 (Appendix B) for a summary of the step test data,and Chart 1 (Appendix F)for a visual depiction of the vacuum—flow relationship. Once the step test was completed it was determined that the SVE test would be conducted by applying a vacuum of approximately 5 inches of water column(in.we)to the extraction well, which yielded a flow rate of approximately 107 standard cubic feet per minute(scfm)of extracted soil vapor. The pilot test was performed for a total period of three and one half(3.5)hours during which time a Rotron 2-Hp regenerative blower was used to apply vacuums of approximately 5 and 10 in. we to SVE-1. During the course of this test,the 1.5 inch points(which are screened across the water table) in the three triplet wells and MW-9 were monitored at regular intervals for pressures(observed vacuums), depth to water,VOC concentrations as measured with a calibrated PID, and dissolved oxygen concentrations (DO). Other parameters measured at the SVE system consisted of vacuum applied to SVE-1 by the blower, VOC concentration of the soil vapor air stream as measured with a PID at the influent,mid- fluent, and effluent of the off-gas treatment and air flow rate. Extracted soil vapors were treated using two 200-pound vapor phase granular activated carbon units (GACs)prior to discharge to the atmosphere. Throughout the course of the SVE test,VOC concentrations of the soil vapor influent air stream were observed to range from 437 to 766 ppm,,VOCs at an extraction rate ranging from approximately 107 to 176 scfm. Vacuum influence was observed in each of the four monitored wells,ranging from 0.65 to 1.05 in. we in MP-1 (located 8.00 feet from SVE-1), 0.33 to 0.65 in. we in MP-2(located 17.50 feet from SVE-1), 0.22 to 0.35 in. we in MP-3 (located 27.00 feet from SVE-1),and 0.11 to 0.18 in.we in MW-9 (located 45.00 feet from SVE-1). The SVE/AS pilot test results are summarized in Tables 6 and 7 (Appendix B). Based on the vacuum applied to SVE-1 (5 and 10 in. we)and the vacuum observed at the four monitoring wells, an estimated radial influence was calculated by plotting the normalized vacuums versus distance on a semi-logarithmic graph(refer to Charts 2 and 3 in Appendix F). Radial influence was determined to be the distance where 1% of the normalized vacuum was observed or extrapolated by graph. Based on the pilot test data,the effective SVE radial influence for SVE-1 when applying a vacuum of 5 and 10 in. we was calculated to be approximately 37 feet and 38 feet,respectively. Refer to Charts 2 and 3 (Appendix F) for a visual depiction of the effective radii of influence observed during the pilot test. During a short SVE pilot test conducted on May 18, 2001 soil vapors were extracted from SVE-1 by utilizing a 2Hp regenerative blower that applied a vacuum of 1.3 in. we with a corresponding air flow rate of 28.9 scfin.During the course of this test,the two inch points(which are screened across the water table)in the three triplet wells were monitored at regular intervals for pressures(observed vacuums. Other parameters measured at the SVE system consisted of vacuum applied to SVE-1 by the blower, and air flow rate. Extracted soil vapors were treated using two 200-pound vapor phase granular activated carbon units(GACs)prior to discharge to the atmosphere. Throughout the course of the SVE test, an extraction rate of approximately 29 scfm was maintained. Vacuum influence was observed in each of the three monitored wells, from 0.22 in. we in MP-1 (located 8.00 feet from SVE-1),0.11 we in MP-2(located 17.50 feet from SVE-1),to 0.05 in. we in MP-3 (located 27.00 feet from SVE-1). The SVE/AS pilot test results are summarized in Tables 8 (Appendix B). Prior to the completion of the SVE/AS pilot test a summa canister sample was collected from the influent of the SVE blower and sent to Accutest Laboratories of NJ for analysis. The air sample was analyzed for air phase petroleum hydrocarbons(APH). Results of the air sample have been summarized in Table 9 (Appendix B) and the complete analytical results can be found in Appendix G. Ref. #000509C. IRAPDS Based on the vacuum applied to SVE-1 (1.3 in. wc)and the vacuum observed at the four monitoring wells, an estimated radial influence was calculated by plotting the normalized vacuums versus distance on a semi-logarithmic graph(refer to Charts 4 in Appendix F). Radial influence was determined to be the distance where 1%of the normalized vacuum was observed or extrapolated by graph. Based on the pilot test data,the effective SVE radial influence for SVE-1 when applying a vacuum of 1.3 in. we was calculated to be approximately 33 feet. Refer to Charts 2 and 3 for a visual depiction of the effective radii of influence observed during the pilot test. On May 24, 2001,GSC conducted a combined SVE/AS pilot test on wells SVE-1 and AS-1. The principal purpose of the AS portion of this pilot test was to determine the feasibility of AS as a potential remedial option for this site. This test was performed for approximately two hours and(2.2)hours,in concert with the last(2.2)hours of the SVE pilot test. A Craftsman 4-HP oil-less air compressor was used to inject air into AS-1 at pressures ranging from 8 to 9 pounds per square inch psi,resulting in flow rates of 3, and 6 scfm, respectively. The 2-inch wells which intersect the water table were monitored at regular intervals for pressures,depth to water,DO, and VOC concentrations as measured with a PID calibrated to read total VOCs in ppm,,as benzene. The 1.5-inch wells that are set below the water table were monitored for pressure, and Helium. Other parameters measured at the SVE and AS systems consist of pressure applied at the blowers,influent,mid-fluent, and effluent VOC concentrations as measured with a PID calibrated to read VOCs as benzene,and air flow rates. Complete pilot test data results are summarized in Tables 5 through 9,Appendix B. During the first hour of the AS portion of the test a pressure of approximately 8 psi, which yielded a flow rate of approximately 3 scfm,was applied to AS-1. Throughout the course of this portion of the SVE/AS pilot test,VOC concentrations of the soil vapor influent air stream were observed to range from 415 to 508 ppmv VOC's. Groundwater mounding influence was observed in MP-1 through MP-3, and an increase in DO concentration was observed at monitoring points MP-1,MP-2, and MP-3. Visual illustrations of groundwater mounding influence and the DO influence can be seen on Charts 6 and 7, respectively. During the second 45 minutes of the AS portion of the test a pressure of approximately 9 psi,which yielded a flow rate of approximately 6 scfin,was applied to AS-1. Throughout the course of this portion of the SVE/AS pilot test,VOC concentrations of the soil vapor influent air stream were observed to range from 375 to 469 ppmv VOC's. Groundwater mounding influence was observed in MP-1 through MP-3, and an increase in DO concentration was observed at monitoring points MP-I,through MP-3. Visual illustrations of groundwater mounding influence and the DO influence can be seen on Charts 6 and 7, Appendix F respectively. The final half hour of the SVE/AS test consisted of the injection of helium as a tracer gas. During this portion of the test a 300 cubic foot helium tank with a standard regulator was used to inject helium into the sparge well at approximately 9 psi, which corresponded to a flow rate of 6 scfm. The three triplet wells and the influent to the system were monitored for helium content. Complete pilot test data results are summarized in Tables 5 through 9(Appendix B). Based on the air flow injection rate at AS-],helium detection data, geometric relationships between wells monitored,the distance of the monitoring points from AS-1, changes in dissolved oxygen levels, and the change in groundwater elevations observed in the wells monitored, an estimated radial influence was determined to be approximately 22 feet for well AS-1 at the respective flow rate of approximately 6 scfm. Ref. #000509C. IRAPDS During a short SVE/AS pilot test conducted on May 18, 2001 soil vapors were extracted from SVE-1 by utilizing a 2 Hp regenerative blower,that applied a vacuum of 1.3 in. we with a corresponding air flow rate of 28.9 scfm. During the course of this test,the two inch points(which are screened across the water table)in the three triplet wells were monitored at regular intervals for pressures(observed vacuums). Other parameters measured at the SVE system consisted of vacuum applied to SVE-1 by the blower, and air flow rate. Extracted soil vapors were treated using two 200-pound vapor phase granular activated carbon units(GACs)prior to discharge to the atmosphere. Throughout the course of the 30 minute AS portion of this test,a pressure of approximately 10 psi, which yielded a flow rate of approximately 6 scfm,was applied to AS-1. Prior to the completion of the AS portion of this test a summa canister sample was collected from the influent of the SVE blower and sent to Accutest Laboratories of NJ for analysis. The air sample was analyzed for air phase petroleum hydrocarbon(APH). Results of the air sample have been summarized in Table 9(Appendix B)and the complete analytical results can be found in Appendix G. IX. Remediation System Design Based on the assessment activities preformed to date for this site and the results of continued groundwater monitoring activities,the UST and pump dispenser area has been identified for immediate remediation using SVE/AS technology. This target area generally correlates to the areas of petroleum impacted groundwater and soil identified during ongoing Phase H and IRA assessment activities. Installation of Additional SVE/AS Wells Based on the pilot test data for this site, a total of 10 additional SVE wells and 7 additional AS wells are proposed to adequately address the area targeted for active remediation on the Texaco property. Refer to Figure 7 (Appendix A)for the location of SVE and AS wells. The 10 additional SVE wells proposed for installation will be installed at a depth of approximately 36 feet below grade,constructed of 26-feet of 4- inch diameter Schedule 40 PVC riser with 10-feet of 4-inch diameter Schedule 40 PVC 0.010 slot well screen at their bases. The borehole annulus of each SVE will be finished with a sand pack to approximately 2-feet above the top of the well screen,a 2-foot bentonite seal and backfilled to grade with native material. The additional 7 AS wells will be installed to a total depth of approximately 49 feet below grade,constructed of 47-feet of 2-inch diameter Schedule 40 PVC riser with 2-feet of 2-inch diameter Schedule 40 PVC 0.010 slot well screen at their bases. The borehole annulus of each AS well will be finished with a sand pack to approximately 2-feet above the top of the well screen, a 2-foot bentonite seal, grouted from above the bentonite seal to approximately 4 feet below grade and back-filled to grade with native material. Remediation System Piping/Trenches Each SVE and AS well will be connected to an individual PVC conduit(2-inch diameter Schedule 40 PVC pipe for the SVE wells and 1-inch diameter Schedule 80 PVC pipe for the AS wells),placed within trenches that will be excavated to a depth of up to four feet below grade. Please refer to Figure 8 (Appendix A)for the approximate locations of the trenches and the equipment enclosure. All bituminous concrete pavement will be saw cut prior to trenching. The piping will be installed on a bed of pea gravel and covered by approximately 4 inches of pea gravel. The trenches will be backfilled with select native material, free of cobbles and organic material,compacted in six-inch lefts and resurfaced. All piping leading from the wells will lead to and be mamfolded together within a shed and/or fenced equipment enclosure. The SVE and AS wells construction details and trench cross-section/piping details are included on Figure 9(Appendix A). Ref.#000509C.IRAPDS Remedial Equipment SVE Equipment The SVE system equipment will consist of a positive displacement/regenerative blower with a relief valve, moisture separator, air filter,heat exchanger(if necessary), sample ports, and flow and pressure gauges. The blower will be capable of providing a vacuum of approximately 1.5 inches of water column with an expected flow of approximately 28 scfm at each well. The type and specifications of the blower itself will be dependent on the manufacturer. The piping from each well will be independently valved to allow for extraction from any or all of the wells at a given time. Each piping leg will contain a sample collection port to monitor individual well head influent vapor concentrations to the system. The SVE system will be equipped with the following failsafes; a high level switch in the moisture separator,a low vacuum or low flow switch on the intake side of the blower and a high temperature switch/or heat exchanger on the discharge side of the blower. Refer to Figures 10 and 11 (Appendix A)for a process and instrumentation diagram and associated legend. The aforementioned equipment will be housed within either a shed or fence enclosure constructed at the location noted on Figure 9,pending local permitting requirements. The layout of the equipment within the equipment compound will be determined in the field at the time of construction. AS Equipment The AS system equipment will consist of a compressor capable of delivering approximately 6-10 scfm at a pressure of 9 pounds per square inch(psi)at each well, and heat exchanger(if necessary). The type and the specifications of the equipment chosen will be dependent on the manufacturer. Additional controls, a relief valve,pressure gauges and flow meters will be provided. The air sparging system will be equipped with appropriate fail safes to shut down the air sparging system should the SVE system shut down. Refer to Figures 10 and 11 (Appendix A)for a process and instrumentation diagram and associated legend. The layout of the equipment within the equipment compound will be determined in the field at the time of construction. Treatment,Management,and Disposal of Remediation Process Wastes Air removed from the SVE wells will enter a moisture separator where the air will be separated from residual water. The resultant air stream is expected to be treated by a series of appropriately sized vapor phase granular activated carbon vessels(VGAC). If it is determined that the soil vapor stream temperature is greater than 120 deg. Fahrenheit a heat exchanger will be placed prior to the first VGAC in order to ensure 95% destruction efficiency. Sample ports will be fitted at the influent and effluent points of each VGAC, in order to complete monitoring of the vapor stream as outlined in this submittal. X. Remediation System Construction Management Field Monitoring and Management of Excavated Soil During drilling and excavation activities, GSC personnel will perform on-site inspections and field screening of excavated soil. Field screening will be performed using.a PID calibrated to read VOCs in ppmv as benzene. Soil which does not exhibit visual or olfactory evidence of petroleum impact and does not exceed a PID reading of 100 ppmv using standard jar headspace techniques may be considered suitable for on-site reuse. Soil exhibiting visual or olfactory indications of petroleum impact or exhibiting a PID response of greater than 100 ppmv VOCs will be considered potential Remediation Waste, and stockpiled separately pending confirmatory laboratory testing. Ref.#000509C. IRAPDS In so far as the purpose of the trench excavations is to allow the construction and installation of the SVE/AS remedial system piping to occur, and not to perform the actual remediation of this portion of the site, it is not anticipated that petroleum-impacted soil will be excavated from beyond the limits of excavation specifically planned for installation of SVE/AS piping. Soil Stockpiling Protocol Soil removed from the excavation during construction activities will be staged on and covered by polyethylene sheeting in separate stockpiles based upon the results of the visual, olfactory, and PID field screening results. Soil piles will be covered with polyethylene sheeting and secured at the end of each day until the soil is either re-used on site or removed from the site. Characterization of Stockpiled Soils Representative soil samples will be collected from any stockpiled soil which is initially characterized as potential Remediation Waste and submitted to a laboratory for analysis of the parameters specified in the intended receiving facility permit requirements. It is anticipated that samples will be collected on a frequency of approximately one sample per 200 cubic yards(if necessary). Other soil analyses may be performed as necessary,in order to provide characterization in accordance with the license/requirements of the receiving facility. The permit requirements of the anticipated receiving facility will determine the frequency of other analyses. Soil found to contain hydrocarbon concentrations which exceed Reportable Concentrations for reporting category S-1 soil will be considered Remediation Waste and will remain stockpiled pending transport to a recycling/disposal facility. Management of Remediation Waste Soil impacted with petroleum and determined to be Remediation Waste, as previously described, may be transported to a permitted recycling facility using a Massachusetts DEP Bill of Lading in accordance with the provisions of 310 CMR 40.0030. Soil impacted with petroleum and determined not to be Remediation Waste, as previously described,may be transported to a permitted recycling facility with the voluntary use of a DEP Bill of Lading, if the soil is not re-used on site. Excavation Dewatering/Treatment Based on historic,groundwater elevations and the estimated depth of excavations, it is not anticipated that excavation dewatering will be needed. Health and Safety/Site Security Work performed as part of the IRA plan shall be conducted in accordance with the requirements of the Occupational Safety and Health Administration(OSHA)under 29 CFR 1910.120. A site-specific Health and Safety Plan for non-contractor employees has been prepared for this project per 310 CMR 40.0018. This Health and Safety Plan will be on site during all field activities described herein, and will be monitored and updated should observations and/or data encountered deem it necessary. Following a contractor bidding and selection process,the successful general contractor will be required to prepare a site-specific Health and Safety Plan in accordance with the documents and specifications for the construction. Areas where excavations are performed will be properly secured at all time using fencing and/or barricades with applicable signage. Ref. #000509C. IRAPDS XI. Permits Required for this IRA,pursuant to 310 CMR 40.0424(1)(h) and Reporting The following permits and approvals are anticipated to be required to complete the work proposed for at this site: Permits/Approval Issuing Agency -Building Permit Town of Barnstable Building Dept. -Electrical Permit Town of Barnstable Building Dept. No other approvals are anticipated to be required for installation and operation of the remedial activities described herein. XII. System Start Up and Extended Operation and Maintenance Groundwater Monitoring Prior to system activation,groundwater samples from site monitoring wells will be collected and analyzed for,at minimum,BTEX,MTBE, and VPH fractions via DEP-approved Methodology. Additional analyses from up to 10 monitoring wells may include dissolved iron via EPA Method 200.1/6010, alkalinity via EPA Method 310.1, carbon,Nitrite via EPA Method 353.3,Nitrite via EPA Method 354.1, Sulfate via EPA Method 375.4, and sulfide EPA Method 376.1. These analyses,combined with in-situ measurements of DO,pH,and/or oxidation redox potential(ORP), conductivity and temperature may be used to evaluate the baseline from which the potential effectiveness of the monitored natural attenuation (MNA)program can be evaluated in the future. These analyses will also aid in determining what effect the AS system operations are having on groundwater chemistry downgradient of the subject property. The results of the VOC analyses will provide a baseline to monitor the relative effectiveness of the active remediation system on the Texaco property over time. Samples will be collected prior to system start-up,to establish the base line conditions,and two additional sampling events will be conducted during the first year of operation. The sampling frequency after the first year of operation may be reduced to semiannual events,based on remedial system performance. System Startup Following start up of the remedial system, Operation and Maintenance(O&M)visits for the first month will be performed approximately on days one,three, seven, and days 14,21, and 28. During each O&M. visit,the following tasks at minimum will be completed: • Monitoring of the vacuum applied to each active SVE well head and at the manifold; • Monitoring of the pressure applied to each sparge well(at the manifold); • Monitoring of flow rates(or air velocity)of each SVE and sparge well; • Monitoring of vacuums and pressures at the SVE and AS equipment; • Monitoring of VOC concentrations with a PID of the SVE influent air stream prior to treatment and the effluent air stream; Ref.#000509C. IRAPDS • Monitoring of vacuum readings at selected monitoring wells in order to estimate effective vacuum radial influence of the SVE system; and • Monitoring of water levels and DO in selected monitoring wells in order to estimate effective sparging radial influence on groundwater(following activation of the sparge system at a later date); Based on the vacuum and flow rates at each SVE well and the pressure and flow rate at each sparge well, flow valves for each well will be adjusted to provide a flow to or from each well which maximizes efficiency of the system. Extended Operation and Maintenance Extended O&M visits will be performed(at a minimum) once per week for the first month of operation after startup, and two visits per month thereafter. This frequency may be modified in the future,based on performance and operating history of the system. The following activities will be completed during routine O&M visits: • Monitoring of the vacuum applied to each active SVE well head and at the manifold;. • Monitoring of the pressure applied to each sparge well(at the manifold); • Monitoring of flow rates(or air velocity) of each SVE and sparge well; • Monitoring of vacuums and pressures at the SVE and AS equipment; • Monitoring of VOC concentrations with a PID of the SVE influent air stream prior to treatment and the effluent air stream; and • Monitoring of vacuum readings at selected monitoring wells in order to estimate effective vacuum radial influence of the SVE system; The following activity will be completed once per month during the routine O&M visits: • Monitoring of water levels, and DO in selected monitoring wells in order to estimate effective sparging radial influence on groundwater. It is anticipated that operation of this system will ultimately be part of the Phase III/IV Remedial Action Plan for achieving a permanent solution at the site. Continual evaluation of the performance of the system will be conducted and all of or portions of the system may be cycled or shut off based on the concentrations of VOCs in extracted air and other system performance criteria. Reporting In accordance with 310 CMR 40.0425, IRA Status Reports will be submitted every 6 months. It is anticipated that the first report documenting remedial system operation will be submitted in February 2003, after the construction of and first few months of operation of the system have been completed. The actual date of submittal will be dependent on the start date and the length of the construction period. The Status reports will include the requirements set fourth in 310 CMR 40.0425 until further evaluation of the site conditions warrant an IRA Completion Report as set fourth in 310 CMR 40.0427. Ref. #000509C. 1RAPDS Appendix A Figures W 4t' 73 rr ' 9 r•� 0jf .i'. c� r `. " CC d T � `'•,� Lewis..•. a ' 'lsland k F Po4idr aa Pdnd �• •�, TIE SITE �� z-` Gopseberry • `r •.. l� 4� $` ��� aJtJ , � <"#�t3 q .•4�4 -* d[sland f` '&� b •'m Lam' ® ® R L t P A i 132 ` epl •,.4�y .04 rc ,4 ns �a f • J� • � b� �� wnlp : �p-.4t,r3: s �� R.Q �.• � sS e � �, a �a (2�81�� — 'q ' • F fl •ram*�� •A a._ •� f} i Cl 'at��4 �� ••� �1 Grp ��� � 9e j` @' , n 3' •_ � o w 4 w� ���+Y•�T. IM' •R°', ,�i � �G�iP� t � 't3. �.� wr: i Zl � ss Y,;-.� '� N 1000 0 1000 2000 .3000 4000 Feet . W E S QUADRANGLE LOCATION UTM COORDINATES: 4 614 214 N 391 115 E LATITUDE: 4f 40' 27" LONGITUDE: ' 90° 18° 29'° ZONE 19 FIGURE 1 LOCUS PLAN. TEXACO SERVICE STATION#100083 1140 IYANNOUGH ROAD HYANNIS,MASSACHUSETTS GEOLOGIC SERMCES CORPORAMN CSC REF: 000509:10cus Checked By: Hydro geologists and Environmental Scientists Drafted By: RJD Date: 3/25/02 Source: USGS Topographic Quads-Hyannis,MA 15 Bonaaoli Avenue • Hudson, MA 01749 • (978) Quadrangle 15 Minute Series • ti ' MP-120 MW-3A N , o , MW— A IBUILDING MWr-17 1 , MW-1A KEY IVIW 144D TMP-103AW— MW-18S , GROUNDWATER MONITORING WELL , MW- 14 ' TMP-1.02 � 18D 0 AIRSPARGE WELL r ' MW-5 (9 SOIL VAPOR EXTRACTION WELL ' ,,UST MW—GO TEMPORARY MONITORING WELL 6 I MW—g AREA CPT-1I CATCH BASIN ' MW-4 I — PROPERTY BOUNDARY DIESEL • DISPENSER ; / UST UNDERGROUND STORAGE TANK ISLAND MP-2,OAS-1 MW-4 SERVICE ' MP- Mt1 SVE—1 �W- 1 STATION / , MW-10 PT— ®CB-1 TM —101 I M —11 I � , 0 I Y`9� ` GASOLINE I �0 M —12 ,�� ISLAND 0 50 �G�7 ,t� �. 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ARKTNG -, ,` \ , , �r6 ti66. ,. ., v 6 --_.�--.,�,�,. P[7N� , ` "--- __ / 66.5 " /� 6. /\6 EV r♦ 4,9 i`6 ' //6 7R3. 6 ,6_ . . \/ : 5�9 \/ w z ``� 65.4 r\ ss,6 S ,\65.8 f ., / I . f�62 � � / 3.1 ,\'/\46 \ 44.0 \ 6 1 4.7 /b._ 5 SCUR \/ , ,46 8/ / 83 �, / �` /,, ", R c7 GRO N /\42R3 /\42 \/ \6 \64. /440 ,\ 7. , ,� , ;, \//50.6� /y -� � . .1 y163R2 '' / 54.2 _ V. UNP ED PARKI 9 \/3 .4. / 3 ; `,.r,67.3 f :' /\6 / ter j/50.9 \/4 \/63. 5 .S \/ /\ 0.8 \/47.3 '��/\ /\34 / . ? 5 I -. ti /'� v/ 6 .1 64 8 .. .:,: � ✓y 67.1 � v 43, 4 . / `�. \ /� f ,� 5.7 \i4 \/�45.0 r\ ,3 OR { /� r\ �/ 6.8 r /\65.6 /4 .5 0 100 9R2 , - �, %/ . " 1/ ._I,.: 65, \/ 1 \r Scale in feet \6.�,4 ,- v/ d6 - r 65; \/ ._, `` 5.4 / 6.1 /\ - �,_ ,g ; / . ��52: " r FIGURE 3 / 5.8 �/6 ,4 w /`� 42.1 AREA PLAN I r\ 3 t65. \/ , \, TEXACO SERVICE STATI ON lflO083 �,/ - �. / v /\48.9 / \:/ 49.s, ./'�''-------- ; 46.2 i� 57.6 , : , /\ f r / /\ i 140 IYANNOUGH .RAO /\ R4 5. t: ;> 5 MASSA ,:,. 6 r4 R9 , ; HYANNIS CHUSETTS . r49. \/ GSC REF.: CMECKEi] b ,, ,,\40R1 BY: \/ .-.., . 62.9 /\ Y. A r _.._"_ -- SOURCE: G5C Field Reconnaissance, Town of /. ► t GE( LOGIC SEaVIGES CORPORATION .- . .. . -._.___m_ -_ 1. - -- --- -- ----. _ _. -_ Barnstable G.I.S. Unit , - - _ -T - -- - - -- ___--- _ .�_.�,..� -- - __ - ----._ ---- _ -- ----- -- I I i I u i � � I �♦� `pit A____�. i i Town Data 111111111 9 MA Towns \tText Town Names ♦tea: ��,--�' � ���``-.� -- - /v Town Arcs s Water Supplies Ground Water SUN . \ NEW � Surface Water \ \ � - PipelineNon Community Powerline NEW\�\\ \ �, . Pipeline Arbitrary Extension : . . Powerline Arbitrary Extension NONNI OSubstation 111i\011110000 Landing Strip/Airport MHD Roads ,,"Limited Access Highway MEN � �� �. IV.Other IV major Road-connector ON Minor Street or Road \ . �. Trail ���, a. ` ��•. ` � SNI Lakes&Ponds r-71 Water Potential Drinking Water' HIGH YIELD . . RN, ,..�...� e � � EM HIGH YIELD PoolsIt MA Certified Vernal \. y MA Rare Habitat ®flM ACECS Zone Ils � a _ . La \ \ l 11 IWPA 1 1 N1111.I I I I Sole Source Aquifers rn•• `u • Major Basins Rivers&streams eee a eee eee .eee :eee - IM Solid Waste Sites FIGURE 4 GIS MAP AND LEGEND ' TEXACO I SERVICE STATION#100083 • • • � �•� • ` = 1140 IYANNOUGH ROAD 10-TrTMI,Me)RV I. SYMBOL & LEGEND SHEET INSTRUMENTATION & CONTROLS EQUIPMENTr } s>3r"fe!< VAPOR PHASE LINE DESIGNATION: PRIMARY ELEMENT SYMBOLS SYMBOL SPECIFICATION OIL WATER ?f %f: cAReON 2 - VR - 0 t - PV SEPARATOR f•<;: AIR COMPRESSOR _ O LEVEL SWITCH INSTRUMENT TYPE: S2E IN PROCESS UNE MATERIAL + I11EHE5 NUMBER SPECIFICATION LOW LOW LEVEL SWITCH LOW PS PRESSURE SWITCH I PI PRESSURE INDICATOR r-r PROCESS LINE INDICATORS FI FLOW INDICATOR TIi'11 BAG FILTER WITH O FOI FLOW METER (TOTALIZING) L°' LEVEL SWITCH HIGH r PUMP PACKED COLUMN FLOW AIR STRIPPING DIRECTION HIGH HIGH TI TEMPERATURE INDICATOR ® LEVEL SWITCH CI CAPACITIVE SENSOR LIQUID RING LIQUID PHASE ' TOWER PUMP FC PBON MAJOR PROCESS O PRESSURE SWITCH TT TEMPERATURE TRANSDUCER MINOR PROCESS HIGH TS TEMPERATURE SENSOR _ _ WATER/AIR O PRESSURE SNITCH LEL EXPLOSIVITY METER O SKIMMER SL STATUS LAMP CENTRIFUGAL � � PIPING LOW PUMP PUMP °os PRESSURE DIFFERENTIAL AIR O SWITCH PC PRESSURE CONTROL ---- PIPING SP SAMPLE POINT ROTARY VANE O PRESSURE INDICATOR COMPRESSOR INSTRUMENTATION DIAPHRAM CONTROLS FLOW SWITCH INSTRUMENTATION DISPLACEMENT LIOUID PHASE PUMP b41 PNEUMATIC LINE PUMP CARBON (STEEL) TT —L CONNECTING LINE O FLOW METER SYSTEMINSTRU UM NT TYPE SYSTEM POSITION NUMBER SIGNATION PRODUCT PROPORTIONING I +I TEMPERATURE INDICATOR DRUM PUMP LOW PROFILE CROSSOVER LINE AIR TEMPERATURE SWITCH INSTRUMENTS WITH INPUTS OR OUTPUTS CENTRIFUGAL STRIPPER HIGH SENSOR TYPE h NUMBER $BIS(M AT THE SITE CONTROL PANEL INLET BLOWER +n TEMPERATURE SWITCH FILTER PUMP PROCESS LINE ABBREVATIONS Low (SENSOR DESIGNATION) CONDENSER ES - ELECTRIC SUPPLY LEVEL ALARM Low D O 1 8 POSITIVE A-ANALOG I-INPUT NUMBER DISPLACEMENT o-gSCRETE o-ouTPur SENSOR GS - GAS SUPPLY LEVEL ALARM HIGH H.HI SPEED BLOWER UNCEUPA HS - HYDRAULIC SUPPLY SWE MOISTURE Sw'cE LIQUID PRESSURE ALARM LOW° INSTRUMENT IS CONTROLLED SEPARATOR HEATER RING PUMP NS - NITROGEN SUPPLY ® OFFSITE BY SCADA INTERFACE HOLDING TANK SS - STEAM SUPPLY SINGLE PORT BLOWER El PITOT TUBE doom SILENCER W WATER SUPPLY INSTRUMENT WITH INPUTS OR OUTPUTS V - VACUUM © AVERAGING LOCATED AT A LOCAL CONTROL PANEL PITOT TUBE OTHER THAN THE SITE CONTROL PANEL CONTROL VALVE VR - VAPOR REMOVAL ® POSITIVE DISPLACEMENT TF - TOTAL FLUIDS FLOW INDICATOR GENERAL INSTRUMENT OR FUNCTION SYMBOLS �r� BODIES ACTUATORS / REGULATOR S FITTINGS & PIPING PROPELLER OR 1 ! BALL VALVE T GEAR ACTUATOR V FOOT VALVE AP - ACCESS PIPE / CONDUIT ® FLOW TURBINE TYPE ELEMENTLOCATION AUXILIARY —I[�fi--EXPANSION JOINT/SLEEVE RMALLnELO LOCATION ALL DQ GATE VALVE SA - SPARGE AIR ❑p VORTEX SENSOR ACCESSIBLE MOUNTED ACCESSIBLE NORMALLY f PRESSURE RELIEF u VICTAULIC CONNECTOR = HOSE CONNECTION PN - PNEUMATIC SUPPLY OPERATOR DW GLOBE VALVE ��— CROSSOVER _b PLUG a SONIC FLOWMETER DIAPHRAGM ACTUATOR ] PIPE CAP G O e INSTRUMENTS NTS —0—FLANGED CONNECTION MATERIAL SPECIFICATION TARGET TYPE SENSOR I'�J BUTTERFLY VALVE —I SCREWED CONNECTION 17 SLIP UPDRAFT VENT CAP HYDRAULIC ACTUATOR PV - POLYVINYL CHLORIDE (1J SWING CHECK VALVE '-LIL— UNION WEIR SHARED DISPLAY, —H-- COUPLING CHI- ELBOW - TURNED UP GM - GALVANIZED SHARED CONTROL � DIAPHRAGM VALVE (� SOLENOID ACTUATOR _ RC - RIGID COPPER TUBE CONTROL t Y OBI- ELBOW - TURNED DOWN REGULATOR CONTROL INTERLOCK T-too TANK I�I BALL CHECK VALVE IR - IRON p FLOW top Lode P-too PUMP ELBOW — 90' NOZZLE WP-100 WELL PUMP FLOW INDICATOR ABS- ACRYLONITRILE BUTADENE STYRENE B—IUM BLOWER W INSTRUMENTS SHARING H-100 HEATER ►t NEEDLE VALVE 4 MOTOR ACTUATOR }K `/� T' � $ ELBOW - 45' fL - FLEX Hv-too Hmwwc VALVE 3 WAY VALVE LEVEL SWITCH COMMON HOUSING MV_100 MOTOR VALVE RUPTURE DISK FLOATS SV-too SOLENOID VALVE DIGITAL ACTUATOR /� 1 �N INDICATOR�UM 0 REDUCER t �R ELBOW - LONG RADIUS 1 C&J 4 WAY VALVE n WATER ACTUATOR STRAINER TT `1 4� REDUCING ELBOW FLOW N SAMPLE VALVE ® RESTRICTOR TEE REDUCING PRESSURE VALVE ABBREVIATIONS RELIEF VALVE -0+- TEE (OUTLET UP) FIGURE 1 1 PROCESS AND INSTRUMENTATION DIAGRAM LEGEND N.C. - NORMALLY CLOSED `^�` w%C FLEX OHOSE T -+0+- TEE (OUTLET GOWN) TEXACO SERVICE STATION #100083 N.O. - NORMALLY CLOSED 1 140 IYANOUGH ROAD MAN - MANUAL QUICK CONNECT +L}- TEE couPUNc HYANNIS, MASSACHUSETTS PRESURE INDICATOR GSC REF.: 000509.01 LEGEND CHECKED BY: DM- s SAMPLE VALVE DRAFTED BY: SC DATE: 7 22 02 ISOLATION VALVE REVISED BY: DATE: SOURCE: GSC ENGINEERING DEPARTMENT �!� GEOLOGIC SERVICES CORPORATION � k Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue •Hudson,MA 01749 •(978)568-8740 itr h I •• CRITICAL DEVICE INLET AMBIENT AIR FILTER SPARGE ZONE TAM TIMER PANEL 1 <U TSH HE01 HE01 ASC01 HOA Y I AIR COOLED HEAT EXCHANGER (IF NECESSARY) DILUTION yALy1 ROTARY VANE I I EXPECTED EXPECTED ( VAPOR PHASE CARBON OPTION COMPRESSOR POSITION PRESSURE FLOW DISCHARGE TO SVE-SP01 _5.3 IWC 3IS ATMOSPHERE (3) 1 LAM PI I VGAC fl fl fl fl fl fl � SP02 ' ASO1 AS02 AS03 AS06 AS07 AS08 I i LSH SVE-DV PI PI Pl PI PI PI PI FI T1 PSL PAL - �501 A502 AS03 AS06 AS07 AS08 SVE SVE SVE 1 (2 SP01 SP01 SP01 � p� I I I I I _ _ _ ' . SVE SVE TAM 1 I SP03 SP04 SVE SVE TSH r J r' J r J r _ r J r J ( I— SP04 SP04 f _ 1 I MOISTURE I V %E .. I - SEPARATOR MOp AIR COOLED HEAT VAPOR PHASE VAPOR PHASE EXCHANGER GAG SVE (IF NECESSARY) I (500 Ib) (500 Ib) SVE01 VEO SVEIO SVEII SLOWER I 8� PRESSURE w/CARBON ASO1 AS02 AS03 AS06 AS07 AS08 JIB ---JJJ ( POTION ��� EXPECTED NOTE: TYPICAL AIR SPARGE MANIFOLD DIAGRAM. ACTUAL MANIFOLD CONSTRUCTION SVE01 SVE02 SVEIO SVEII vv/ WILL INCLUDE Two ZONES OF♦ LEGS RESPECTIVELY. TREATMENT SYSTEM ENCLOSURE AIR SPARGE WELLS AI MANIFOLD POSITION PRESSURE EXPECTED TOTAL CASING �ETGE DIAMETER WAITE PTHR INTERVAL r— J r— J r— J r J , ASOI -10 PSI 6-10 SCFM -49' 2-inch a-inch -30'-32' -47'-49• A502 -10 PSI 6-10 SCFM -49' 2-inch B-inch -30'-32' -47'-49• AS03 -10 PSI 6-10 SCFM -49' 2-inch 8-inch 30'-32• -47'-49• .: ASO4 -10 PSI 6-10 SCFM -49' 2-inch 8-inch -30'-32• -47'-49' - AS05 -10 PSI 6-10 SCFM -49 2-inch 57.ch -30'-32' -47'-49• AS06 -10 PSI 6-10 SCFM -49' 2-inch S-inch -30'-32' -47'-49• AS07 -10 PSI 6-10 SCFM -•49 2-Inch 8-kIch 30'-32 -47'-49• I AS08 -10 P9 6-10$CFY M9' 2-inch 8-inch 30'-32• -47•-49' - EQ IQ SVEOI SVE02 SVE10 SVE11 mTERLOCK/FAILSAFE SCHEDULE NOTE:EOUIPMENT VENDOR SWILL SIZE THE MR SPARGE I.O. LOCATION FUNCTION COMPRESSOR/BLOWER TO DELIVER 6-10 SCFM TO FOUR OF THE SPARGE WELLS AT ANY TDIE (1) AS/SVE MOTOR INTERLOCK AS MOTOR CANNOT OPERATE WITHOUT THE SVE MOTORRUNNING. SHUTS AS MOTOR DOWN IF SVE MOTOR FAILS (ASSUMES THAT THE AIR SPARGE TIMERS WILL BE _ - VAPOR EXTRACTION WELLS (2) SVE LOW PRESSURE SWITCH DEACTIVATES AS MOTOR IF SWITCH SENSES LOW VACUUM ON THE SVE MANIFOLD PIPING CONFIGURED TO CYCLE THE SPARGE WELLS FOUR-ON. FOUR-OFF). EXPECTED EXPECTED TOTAL CASING BOREHOLE DEPTH TO SCREEN POSITION VACUUM FLOW DEPTH ETE DIAMETER WATER TERV TWO-INCH (3) MOISTURE SEPARATOR HIGH LEVEL SWITCH DEACTIVATES SVE MOTOR 1F A HIGH LIO1110 LEVEL 6 PRESENT IN THE SVE MOISTURE SEPARATOR AIR SPAR-INCH 0.010 SLOT PVC WELL SCREEN. IN SVE01 1.3 I1VC 28 SCFM 36' 4-inch 12 inch -30'-32.26'-36'WELL CONSTRUCTION INCLUDES TWO FEET OF N (4) CATOX GENERAL ALARM OFF GAS HIGH TEMP DEACTIVATES SVE MOTOR IF ALARM IS DETECTED SY CATOX OR HIGH TEMP IS SENSED IN OFF GAS DEPENDS ON OFF GAS TREATMENT METHOD SVE02 1.3 M'C 28 SCFM 36' 4-inch 12-inch -30'-32'26'-36' (5) AS HIGH TEMP DEACTIVATES AS MOTOR IF HIGH TEMP IS SENSED IN AIR FLOW SVE03 1.3 IWC 25 SCFM 36 4-inch 12-inch -30-32'26-3V SVE04 1.3 IWC 2a SCFY 36' 4-inch 12-inch -30•-32'26'-36' AIR SPARGE COMPRESSOR SVE05 1.3 IWC 28 SCFM 36' 4-inch 12-inch -30•-32'26'-36' FIGURE 1 O EXPECTED EXPECTED EXPECTED SVE06 1.3 IWC 2a SCFM 36' 4-inch 12-inch -30'-32'26'-36' POSITION PRESSURE Row TEMP. SVE07 1.3 roc 29 SCFM 36 4-inch 12-inch -30•-32 26'-36 +PROCESS AND INSTRUMENTATION DIAGRAM a-AS1 11 PSI - - SVL06 1.3 IWC 28 SCFM 36' 4-inch 12-inch -30•-32'26'-36 i TEXACO SERVICE STATION #1 00083 FI-ASI SC. - SVE09 1.3 FWC 28 SCFM 36 4--inch 12-inN -30-32'26'-36 n-ASI - - Top SVE10 1.3 IwC 28 SCFM 36' 4EM 12-loth -30-32.26•-36' I 1140 IYANOUGH ROAD SVEII 1.3 NTC 28 SCFM 36 4-inch 12-inch -30'-32'26'-36• HYANNIS, MASSACHUSETTS NOTE:ACTUAL 71-ASI TEMPERATURE IS DEPENDANT ON COMPRESSOR SPECIFIED BY VENDOR GSC REF.: 000509.04PID CHECKED BY: DM DRAFTEDI BY: SC DATE: 7 22 02 REVISED BY: I DATE: SOURCE:, GSC ENGINEERING DEPARTMENT GEOLOGIC SERVICES CORPORATION j Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue •Hudson,MA 01749 •(978)568-8740 'I 24" MIN. 1 TRAFFIC BEARING ROAD BOX { BOLTDOWN TYPE WITH RUBBER 24' p GASKET, 12' DIAMETER EXISTING SURFACE TRAFFIC BEARING ROAD BOX ..1 BOLTDOWN TYPE WITH RUBBER ;I GASKET, 8" DIAMETER EXISTING S',URFACE „ 6" MIN. 6"MIN. 4" DIAMETER SCH. 40 RISER SELECTED NATURAL BACKFILL 3' 2' DIAMETER SCH. 40 THREADED RISER CONCRETE PAD 24" x 24" COMPACTED IN 6" LIFTS CONCRETE PAD 24' x 24' SELECTED NATURAL t34CKFlll 3' COMPACTED IN 6"-LIFTS 4" EXPANDABLE LOCKING GRIPPER CAP ...(MIN:E;MANIFOX W,IN .TOW''.. L� _ (MIN:.S'_.1.OR}. . . 2" PVC THREADED PLUG .AIR SPARGE. -T— BACKFILL WITH NATURAL MATERIAL 2,�POR EXTRACTION 1' MIN T."0 SCH, 80'PVC PIPE' 2 0 SCH. 40 PVC PIPE NATIVE BACKFILL MATERIAL 12- MIT N. V I BENTONITE SEAL 3/8" PEASTONE OR - i i ~ 3/8"PEASTONE OR CLEAN WASHED STONE i i i i CEMENT - BENTONITE GROUTS CLEAN WASHED SAND 10' MIN. (DEPENDENT ON TO APPROXIMATELY 4 BELOW GRADE NATIVE BACKFILL BOTTOM OF TRENCH SUBSURFACE MATERIAL) BOTTOM OF TRENCH 4" DIAMETER SCH. 40 THREADED RISER 2' DIAMETER SCH. 40 TNRJIDEO RISER 24' MII BENTONITE SEAL 12' MIN. BENTONITE SEAL 1• MIN. 0.010' SLOT THREADED SCREEN �24 t2' MIN - 0.010" SLOT THREADED SCREEN SAND FILTER PACK _ - SAND FILTER PACK .. - 10' MAX. _ ___ Q 24" 24" MAX. _ Q 24" _ 2" PVC PLUG a" PVC PLUG TRAFFIC BEARING ROAD BOX TRAFFIC BEARING ROAD BOX BOLTDOWN TYPE WITH RUBBER BOLTDOWN TYPE WITH RUBBER VAPOR EXTRACTION WELLHEAD DETAIL GASKET, 12" DIAMETER AIR SPARGE WELLHEAD DETAIL GASKET, 8" DIAMETER it NOT TO SCALE VAPOR EXTRACTION NOT TO SCALE AIR SPARGE WELL MONUMENT DETAIL WELL MONUMENT DETAIL NOT TO SCALE NOT TO SCALE NOT TAR PATCH AT EDGE OF NEW PAVEMENT HOT TAR PATCH AT EDGE OF NEW PAVEMENT HOT TAR PATCH AT EDGE OF NEW PAVEMENT -• 2" BITUMINOUS CONCRETE EXISTING BITUMINOUS - 2 BITUMINOUS CONCRETE EXISTING BITUMINOUS - 2 BITUMINOUS CONCRETE EXISTING BITUMINOUS 4'BASE 8ITUMINOUS CONCRETE CONCRETE PAVEMENT ••• 4" BASE BITUMINOUS CONCRETE% CONCRETE PAVEMENT 4"BASE BITUMINOUS CONCRETE CONCRETE PAVEMENT �\ ROAD BASE-GRADE GRAVEL = ROAD BASE-GRADE GRAVEL = ROAD BASE-GRADE GRAVEL i COMPACTED IN 6 LIFTS g COMPACTED IN 6 UFTS = COMPACTED IN 6 LIFTS g 0 0 0 - 1 I 1 r M � M SELECTED NATURAL BICKFILL SELECTED NATURAL BACKFILL SELECTED NATURAL BACKFILL COMPACTED IN 6'LIFTS COMPACTED IN 6"LIFTS COMPACTED IN 6•LIFTS i > o c o y Rp I y I y 1 CAUTION TAOPFE YELLOW ".4._... CAUTR OWN TAUPE YELLOW ..4._.. M ZAUTINOWNS 1 E YELLOW 4'_ vw�Xm 8'BED CAUT UU 8" BED 1 BED 2 E 1*0 . 80 PVC 'I SCH 1 1"I SCH.80 PVC t ) t ) AIR SPARGE LINE AIR SPARGE LINE FI GURE I U R BED G E 9 4• BED 'e 4 t 2 2"� SCH. 40 PVC C t t SCH. o PVC 2 TRE NCH N t ) vA�R EXTRACTION LINE E CH CROSS SECTION AND SVE A 1) 2 0 SCH. 40 PVC ii I � VAPOR EXTRACTION LINE t k VAP XT IN ORE RACi1pN LINE 12' BED 2 W ELL H A CONSTRUCTION E D CONS UCTION TAI 8"BED B' BED DE L S TEXACO SERVICE STATION #100083 SCR'ENED SOIL OR SCR€EKED SOIL OR SCRgENED SOIL OR 3/8 PEA STONE 3/8 PEA STONE 3/8 PEA STONE 1140 IYANO U G H ROAD TYPICAL TRENCH DETAIL TYPICAL TRENCH DETAIL TYPICAL TRENCH DETAIL ': HYANNIS, MASSACHUSETTS CROSS-SECTION A-A' CROSS-SECTION B-B' CROSS-SECTION C-C' GSC REF.: 000509.04DETAIL CHECKED BY: NOT TO SCALE NOT TO SCALE NOT TO SCALE DRAFTED BY: SC DATE: 7 22 02 REVISED BY: I DATE: ` S GEOLOGIC SERVICES CORPORATION SOURCE: GSC ENGINEERING DEPARTMENT L Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue •Hudson,MA 01749 •(978)568-8740 1. , I TMP-120 MW-3A N I M W-A BUILDING MW/ 1 7 `�. ' A A MW-1 A MW-14D MW-1 BMW 18DW—- 18S KEY MW— 14 � / M _ TMP-10 , ' W I GROUNDWATER MONITORING WELL Mt-6 / O AIRSPARGE WELL CPT- 1 �O B B .® SOIL VAPOR EXTRACTION WELL/ -, ® PROPOSED SOIL VAPOR EXTRACTION WELL MWW-4 ® PROPOSED AIR SPARGE WELL AS—E1 1 SERVICE ' TEMPORARY MONITORING WELL MP— STATION —AW—1 ® CATCH BASIN MW— 0 v I — - — PROPERTY BOUNDARY CPT-2 .®CB— , P��101 v � M —1 1� T l • 0 50 MW- 1 2 MW-2 / Scale in feet FIGURE 8 PROPOSED TRENCH LAYOUT FSE ACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS 000509.06TREN CHECKED BY: Y: SAC DATE: 8 12 02 Y: DATE: GEOLOGIC SERVICES CORPORATION SC ENGINEERING DEPARTMENT Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue •Hudson,MA 01749 •(978)568-8740 i i ' 1 I TMP-120 1 MW-3A N M W -A BUILDING MW/ 17 MW- 1 A MW 144# MW—18S KEY MW- 14 TMP-102 TMP-103 ;'�'W-18D ' smW-5 I GROUNDWATER MONITORING WELL 41i AIRSPARGE WELL M —9 ® MW— C —1 ® ' ® SOIL VAPOR EXTRACTION WELL PROPOSED SOIL VAPOR EXTRACTION WELL ® MW-4 / ® PROPOSED AIR SPARGE WELL P ®MP �VE1 SERVICE {�} TEMPORARY MONITORING WELL M�_1 —1 TATION / ® CATCH BASIN MW— 0 — PROPERTY BOUNDARY CPT-2 , C -1 TMP 101 ® MW- 1 11 / I ; BMW-12 V o 0 50 MW_2 / Scale in feet �, A$. FIGURE 7 �. FDRAFTED OSED WELL NETWORK LAYOUT AND NCEPTUAL RADII OF INFLUENCE ACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS 000509.07ROl CHECKED BY:Y: SAC GATE: 8 13 02 Y: DATE: ZGEOLOGICSERVICES CORPORATION SC ENGINEERING DEPARTMENT Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue •Hudson,MA 01749 •(978)568-8740 MW-15 N 64.98 <5.0 <5.0 <5.0 - TOYS R US <10.0 MW-1 s 5s <5.0 64.99 MW-16 20 414 64.99 <5.0 <5.0 <5.0 <5.0 <5.0 4,280 <10.0 <5.0 E&B DISCOUNT MARINE TMP-5 ® o TMP-6 LANDSCAPE AREA MW-3A 65.18 JENNY <5.0 CRAIG PARKER'S <5.0 MATTRESS TMP-1 TMP-7 LIQUORS <5.0 GIANT <10.0 MW-24 <5.0 65.16 PARKING MW-14 90 122 LOT 62.27LAIVD MW-14 70 <5.0 W_1 ARE ApEO <5.0 TMP-2 65.41 <5.0 65.74 <5.0 <5.0 <5.0 MW-5 MW-18 25 1 11 <5.0 <10.0 <5.0 65.80 65.13 2,700 TMP-3 <5.0 <5.0 <5.0 1,520 <5.0 <10.0 <10.0 10,400 MW-6 <5.0 MW-t8 70 <5.0 <5.0 2000 65.81 <5.0 65.19 36 51.4 2fi 8 TMP-4 ,0 0 <5.0 � s MW-9 <5.0 <5.0 • JO 65.82 8.3 <5.0 Mw-1 a 25 1,620 18.3 <10.0 65.39 16,800 1_170 <5.0 <5.0 2,950 �`N, TMP- 103 <5.0 17,760 �`� �1 S �` MW-1 A <10.0 6,SSo `:��1 T°�q° � 65.13 _ 1 <5.o MP A� 1 v ; 6' PARKING <5.0 SVE-1 S LOT <5.0 MURPHY Mw-1 MW_4 `` / • �? <10.0 MP-3 65.84 Ng S <5.0 REAL ESTATE Mw_10 ® 14.2 65.84 AMP- 48 , S <5.0 CPT-2 22 61 <5.0 MP-1 01 67.5 <5.0 637 <10.0 1 LAND i MW-11 <5.0 65.95 <5.0 MW-2 CUMBERLAN'D FARMS/ 5.75 65.99 <5.0 GULF SERVICE STAITION <5.0 ��� <5.0 <10.0 <5.0 <5.0 102 <5.0 <5.0 <10.0 <10.0 <5.0 I4� J 20.4 MW-13 0� 65.82 Gf I<5.0 <5.0 O <5.0 �� <10.0 <5.0 _ 0 60 Scale in feet RAMADA KEY INN < BELOW METHOD DETECTION LIMIT � CONE PENETROMETER POINT UST UNDERGROUND STORAGE TANK DATA COLLECTED ON 5/1/02 o. TEMPORARY MONITORING O MANHOLE NOTE: MW-2, MW- 1 1 MW- 14(N- 18(70) WELL POINT -65.80 GROUNDWATER CONTOUR MW-14(90) MW-16(�5),NG AND MONITORING WELL <- APPARENT GROUNDWATER NOT USED IN CONTOURI O AIRSPARGE WELL FLOW DIRECTION FIGURE 6 MW-13 WELL IDENTIFICATION GROUNDWATER CONTOUR/ SOIL VAPOR 65.82 WATER TABLE ELEVATION (ft) HYDROCARBON DISTRIBUTION PLAN ® EXTRACTION WELL TEXACO SERVICE STATION #100083 <5.0 BENZENE (ug/I) 1140 IYANNOUGH ROAD ® CATCH BASIN <5.0 TOLUENE (ug/1) HYANNIS, MASSACHUSETTS -- - PROPERTY BOUNDARY <5.0 ETHYLBENZENE (ug/I) GSC REF.: 000509.01 MAY028 CHECKED BY: <10.0 XYLENES (ug/1) DRAFTED BY: ANG DATE: 9 18 01 NS NOT SAMPLED <5.0 MTBE (ug/1) REVISED BY: ANG DATE: 7 2 02 �GEOLOGIC SERVICES CORPORATION SOURCE: SAGE ENVIROMENTAL PLAN AND GSC � e Hydrogeologists and Environmental Scientists FIELD RECONNAISSANCE 15 Bonazzoli Avenue • Hudson,MA 01749 •(978)568-8740 MW-15 N 64.27 <s.0 <s.0 <s.0 TOYS R US <5.0 MW-16D <5.0 64.25 1,410 <50 <50 <50 11,500 E&B DISCOUNT MARINE TMP-5 0 MW-16 ® 64.23 <5.0 TMP-6 <5.0 MW-3A <5.0 <5.0 LANDSCAPED 6.01 JENNY/ <5.0 AREA TMP-7 <5.0 MATTRESS -1 <5.0 PARKER'S 50.6 PARKING MW-14 LIQUORS LOT MW-17 64.63 65.02 L4Np TMP- <5.0 <<5.0 5.0 MW-5 AReA pep _ , <5.0 <5.0 65.02 64.34 TMP-3 MW-1A <5.0 2,260 �� 10,000 `` 14.1 64.27 <5.0 <5.0 <5.0 <5.0 1,390 MW-6 <5.0 <5.0 \ 7,690 65.55 <5.0 T -40 <5.0 46,900 15.6 214 <5.0 MW-9 <5.0 AS-1 64.96 <5.0 64.93 1.28ft. NA <5.0 , <5.0 <5.0 / <5.0 `��`\ SVE-1 173 <5.0 `��� 64 3 <5.0 `��. 0 <5.0 MW-1 i 65.06 P- <5.0 PARKING 6480 JAMES <5.0 LOT MURPHY REAL ESTATE MP- ® MW-4 <5.0 65.76 MP 1 MW-1 <5.0 <5.0 MW-10 65.04 <5.0 KEY DRY 42.3 <5.0 140 <5.0 TEMPORARY MONITORING WELL POINT LANDSCAPED 74. 15.2 GROUNDWATER MONITORING WELL 768 AREA 2 MW-2 \C RESTAOKE'SURANT \ 0 AIRSPARGE WELL MW-12 ROAD WAY 65.08 RESTAURANT ® SOIL VAPOR EXTRACTION WELL MOTEL PROPERTY 64.92 ® <5.0 ® CATCH BASIN <5.0 `1� <5.0 PROPERTY BOUNDARY <5.0 <5.0 UST UNDERGROUND STORAGE TANK <5.0 lt? <5,0 -64.80 GROUNDWATER CONTOUR <5.0 I APPARENT GROUNDWATER <5.0 `�1`I� is FLOW DIRECTION O MW-13 WELL IDENTIFICATION 64.90 WATER TABLE ELEVATION (ft) MW-13 `11 <5.0 BENZENE (ug/1) 64.90 <5.0 TOLUENE (ug/1) <5.0 �u <5.0 ETHYLBENZENE (ug/1) <5.0 <5.0 XYLENES (ug/1) <5.0 <5.0 MTBE (ug/1) <5.0 < BELOW METHOD DETECTION LIMIT <5.0 - \ NAPL NON-AQUEOUS PHASE LIQUID" "=-- NOTE: WELLS MW-10, AS-1 AND MW-16D RAMADA ARE NOT USED IN CONTOURING INN DATA COLLECTED ON 12/4/01 0 60 Scale in feet FIGURE 5 GROUNDWATER CONTOUR/HYDROCARBON DISTRIBUTION PLAN TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.04DEC01 CHECKED BY: Ii^ DRAFTED BY: ANG DATE: 941 0 REVISED BY: RJD DATE: 3 26 02 GEOLOGIC SERVICES CORPORATION SOURCE: SAGE ENVIROMENTAL PLAN AND GSC `r FIELD RECONNAISSANCE It H dro eolo Isis and Enviro men al Scientists y � y � t Scle Usts 15 Bonazzoli Avenue • Hudson,MA 01749 (978)568-8740 i Appendix B Tables Table 1 Page 1 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation AS-1 4/4/01 98.97 32.42 ND - - 66.55 4/9/01 98.97 32.11 ND - - 66.86 4/19/01 98.97 31.65 ND - - 67.32 4/23/01 98.97 31.50 ND - - 67.47 5/3/01 98.97 31.35 ND - - 67.62 6/27/01 98.97 32.06 ND - - 66.91 8/16/01 98.97 32.29 ND - - 66.68 12/4/01 98.97 34.04 ND - - 64.93 12/12/01 98.97 34.19 ND - - 64.78 1/18/02 98.97 34.22 ND - - 64.75 MP-1 4/9/01 98.77 31.84 ND - - 66.93 4/19/01 98.77 31.36 ND - - 67.41 6/27/01 98.77 31.28 ND - - 67.49 8/16/01 98.77 32.02 ND - - 66.75 12/4/01 98.77 33.80 ND - - 64.97 12/12/01 98.77 33.91 ND - - 64.86 MP-2 4/9/01 99.05 32.09 ND - - 66.96 4/19/01 99.05 31.62 ND - - 67.43 6/27/01 99.05 31.54 ND - - 67.51 8/16/01 99.05 32.28 ND - - 66.77 12/4/01 99.05 34.02 ND - - 65.03 12/12/01 99.05 34.17 ND - - 64.88 MP-3 4/9/01 99.07 32.14 ND - - 66.93 4/19/01 99.07 31.72 ND - - 67.35 6/27/01 99.07 31.65 ND - 67.42 8/16/01 99.07 32.37 ND - 66.70 12/4/01 99.07 34.12 ND - 64.95 12/12/01 99.07 34.27 ND 64.80 Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:25 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 2 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-1 1/13/99 98.66 30.49 ND - - 68.17 3/4/99 98.66 30.63 ND - - 68.03 6/4/99 98.66 30.13 ND - - 68.53 10/12/00 98.62 32.32 ND - - 66.30 4/4/01 98.62 31.93 ND - - 66.69 4/9/01 98.62 31.64 ND - - 66.98 4/19/01 98.62 31.18 ND - - 67.44 4/23/01 98.62 31.03 ND - - 67.59 5/3/01 98.62 31.93 ND - - 66.69 5/18/01 98.62 13.10 ND - - 85.52 6/27/01 98.62 31.11 ND - 67.51 8/16/01 98.62 31.82 ND - - 66.80 12/4/01 98.62 33.58 ND - - 65.04 12/12/01 98.62 33.72 ND - - 64.90 1/3/02 98.62 33.96 ND - - 64.66 1/18/02 98.62 33.75 ND - - 64.87 2/12/02 98.62 34.08 ND - - 64.54 3/8/02 98.62 33.76 ND - - 64.86 5/1/02 98.62 32.78 ND - - 65.84 MW-IA 12/4/01 98.70 34.43 ND - - 64.27 1/3/02 98.70 34.77 ND - - 63.93 5/l/02 98.70 33.57 ND - - 65.13 MW-2 1/13/99 98.39 30.60 ND - - 67.79 3/4/99 98.39 31.50 ND - - 66.89 6/4/99 98.39 29.93 ND - - 68.46 10/12/00 98.39 32.11 ND - - 66.28 4/4/01 98.39 32.55 ND - - 65.84 4/19/01 98.39 30.80 ND - - 67.59 8/16/01 98.39 31.50 ND - - 66.89 12/4/01 98.39 33.31 ND - - 65.08 12/12/01 98.39 33.44 ND - - 64.95 1/3/02 98.39 33.68 ND - - 64.71 1/18/02 98.39 33.45 ND - - 64.94 2/12/02 98.39 33.78 ND - - 64.61 3/8/02 98.39 33.43 ND - - 64.96 5/l/02 1 98.39 32.40 1 ND 65.99 Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:25 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA f Table 1 Page 3 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-2A 4/4/01 99.66 33.64 ND - - 66.02 4/19/01 99.66 32.95 ND - - 66.71 8/16/01 99.66 33.52 ND - - 66.14 12/4/01 99.66 35.32 ND - - 64.34 1/3/02 99.66 35.67 ND - 63.99 5/l/02 99.66 34.50 ND 65.16 MW-3A 4/4/01 98.53 32.48 ND i 66.05 4/19/01 98.53 31.77 ND 66.76 8/16/01 98.53 32.35 ND 66.18 12/4/01 98.53 34.12 ND 64.41 1/3/02 98.53 34.48 ND 64.05 5/l/02 98.53 33.35 ND 65.18 MW-4 1/13/99 98.60 30.52 ND - 68.08 3/4/99 98.60 30.68 ND - 67.92 6/4/99 .98.60 30.11 ND - 68.49 10/12/00 99.37 32.31 ND - 67.06 4/4/01 99.37 31.92 ND - 67.45 4/9/01 99.37 31.60 ND - 67.77 4/19/01 99.37 31.18 ND - 68.19 4/23/01 99.37 31.02 ND - 68.35 5/18/01 99.37 31.12 ND 68.25 6/27/01 99.37 31.12 ND 68.25 8/16/01 99.37 31.82 ND - - 67.55 12/4/01 98.60 33.61 ND - - 64.99 12/12/01 98.60 33.73 ND - - 64.87 1/3/02 98.60 33.97 ND - - 64.63 1/18/02 98.60 - - Well Inaccessible 2/12/02 98.60 34.10 ND 64.50 3/8/02 98.60 33.77 ND 64.83 5/l/02 98.60 Well Inaccessible Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:25 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 4 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-5 1/13/99 98.27 30.12 ND - - 68.15 3/4/99 98.27 30.07 ND - - 68.20 6/4/99 98.27 29.71 ND - 68.56 10/12/00 98.22 31.57 ND - - 66.65 4/4/01 98.22 31.94 ND - - 66.28 4/9/01 98.22 - - Well Inaccessible 4/19/01 98.22 - - - Well Inaccessible 4/23/01 98.22 30.66 ND - 67.56 5/18/01 98.22 30.74 ND - 67.48 6/27/01 98.22 30.74 ND - - 67.48 8/16/01 98.22 31.43 ND - - 66.79 12/4/01 98.22 33.20 ND - - 65.02 12/12/01 98.22 33.34 ND - 64.88 1/3/02 98.22 33.56 ND - - 64.66 1/18/02 98.22 33.34 ND - - 64.88 2/12/02 98.22 33.72 ND - - 64.50 3/8/02 98.22 33.41 ND - - 64.81 5/l/02 98.22 32.42 ND - - 65.80 MW-6 1/13/99 98.52 30.40 ND - - 68.12 3/4/99 98.52 - Well Inaccessible 6/4/99 98.52 30.01 ND - - 68.51 10/12/00 98.51 32.20 ND - - 66.31 4/4/01 99.08 32.83 ND - - 66.25 4/19/01 99.08 31.11 ND - - 67.97 8/16/01 99.08 31.76 ND - - 67.32 12/4/01 98.51 33.53 ND - - 64.98 12/12/01 98.51 33.65 ND - - 64.86 1/3/02 98.51 33.87 ND - - 64.64 1/18/02 98.51 33.63 ND - - 64.88 2/12/02 98.51 34.01 ND - - 64.50 3/8/02 98.51 33.68 ND - - 64.83 5/l/02 98.51 32.70 ND 65.81 Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:26 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 5 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-9 1/13/99 99.56 31.36 ND - 68.20 3/4/99 99.56 31.30 ND - 68.26 6/4/99 99.56 31.04 ND - 68.52 10/12/00 99.52 32.23 ND - 67.29 4/4/01 99.52 33.38 32.78 0.60 4/9/01 99.52 33.03 32.50 0.53 4/19/01 99.52 32.28 32.08 0.20 4/23/01 99.52 31.98 ND - - 67.54 5/3/01 99.52 31.85 ND - - 67.67 5/18/01 99.52 32.04 ND - - 67.48 Sheen 6/27/01 99.52 31.57 ND - - 67.95 8/16/01 99.52 32.69 32.59 0.10 12/4/01 99.52 35.53 34.25 1.28 12/12/01 99.52 34.65 ND - 64.87 1/3/02 99.52 34.96 34.85 0.11 1/18/02 99.52 34.67 ND - - 64.85 2/12/02 99.52 35.00 ND - - 64.52 3/8/02 99.52 34.70 ND - - 64.82 Sheen 5/1/02 99.52 33.70 ND - - 65.82 MW-10 1/13/99 98.92 31.20 ND - - 67.72 3/4/99 98.92 31.22 ND - - 67.70 6/4/99 98.92 30.39 ND - - 68.53 10/12/00 98.88 32.60 ND - - 66.28 4/4/01 98.88 32.19 ND - - 66.69 4/9/01 98.88 31.90 ND - - 66.98 4/19/01 98.88 31.42 ND - - 67.46 4/23/01 98.88 31.28 ND - - 67.60 5/18/01 98.88 31.37 ND - - 67.51 6/27/01 98.88 31.36 ND - - 67.52 8/16/01 98.88 31.08 ND - - 67.80 12/4/01 98.88 - - Well Dry 12/12/01 98.88 33.98 ND 64.90 1/3/02 98.88 - - Well Dry 1/18/02 98.88 34.01 ND 64.87 2/12/02 98.88 Well Dry 3/8/02 98.88 Well Inaccessible 5/1/02 98.88 33.04 ND 65.84 i I Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:26 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 6 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-ll 4/4/01 99.78 32.96 ND - 66.82 4/19/01 99.78 32.24 ND - 67.54 8/16/01 99.78 32.88 ND - 66.90 12/4/01 99.78 34.72 ND - 65.06 1/3/02 99.78 35.07 ND - 64.71 5/l/02 99.78 33.83 ND - 65.95 MW12 4/4/01 99.05 32.43 ND - 66.62 4/9/01 99.05 32.13 ND - 66.92 4/19/01 99.05 31.67 ND - - 67.38 4/23/01 99.05 31.56 ND - - 67.49 5/18/01 99.05 31.68 ND - - 67.37 6/27/01 99.05 31.64 ND - - 67.41 8/16/01 99.05 32.36 ND - - 66.69 12/4/01 99.05 34.13 ND - - 64.92 12/12/01 99.05 34.28 ND - - 64.77 1/3/02 99.05 34.52 ND - - 64.53 1/18/02 99.05 34.29 ND - - 64.76 2/12/02 99.05 34.62 ND - - 64.43 3/8/02 99.05 34.27 ND - - 64.78 5/l/02 99.05 33.30 ND - - 65.75 MW-13 4/4/01 98.32 31.67 ND - - 66.65 4/19/01 98.32 30.88 ND - - 67.44 8/16/01 98.32 31.60 ND - - 66.72 12/4/01 98.32 33.42 ND - - 64.90 1/3/02 98.32 33.80 ND - - 64.52 5/l/02 98.32 32.50 ND - - 65.82 MW-14(25) 4/4/01 99.96 33.74 ND - - 66.22 4/9/01 99.96 33.45 ND - - 66.51 4/19/01 99.96 32.98 ND - - 66.98 4/23/01 99.96 32.71 ND - -- 67.25 5/18/01 99.96 32.80 ND - - 67.16 6/27/01 99.96 32.90 ND - - 67.06 8/16/01 99.96 33.59 ND - - 66.37 12/4/01 99.96 35.33 ND - - 64.63 1/3/02 99.96 35.68 ND - - 64.28 5/l/02 99.96 34.57 ND 65.39 MW-14(70) 5/l/02 99.72 34.31 ND 65.41 MW-14(90) 5/l/02 99.95 37.68 ND 62.27 Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:27 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 7 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well fD Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-15(20) 12/4/01 98.47 34.20 ND - 64.27 1/3/02 98.47 34.55 ND - 63.92 5/l/02 98.47 33.49 ND - 64.98 MW-16(20) 12/4/01 98.35 34.12 ND - - 64.23 1/3/02 98.35 34.45 ND - - 63.90 1/18/02 98.35 34.16 ND - - 64.19 5/1/02 98.35 33.36 ND - - 64.99 MW-16(55) 12/4/01 98.27 34.02 ND - - 64.25 1/3/02 98.27 34.36 ND - - 63.91 1/18/02 98.27 34.08 ND - - 64.19 5/1/02 98.27 33.28 ND - - 64.99 MW-17(20) 12/4/01 100.54 35.52 ND - - 65.02 1/3/02 100.54 35.88 ND - - 64.66 5/l/02 100.54 34.80 ND - - 65.74 MW-18(25) 5/1/02 100.28 35.15 ND - - 65.13 MW-18(70) 5/1/02 100.09 34.90, ND 65.19 SVE-1 4/9/01 99.11 31.88 ND - - 67.23 4/19/01 99.11 31.43 ND - 67.68 6/27/01 99.11 31.34 ND - - 67.77 8/16/01 99.11 32.16 ND - - 66.95 12/4/01 99.11 33.82 ND - - 65.29 12/12/01 99.11 33.96 ND - - 65.15 1/18/02 99.11 33.98 ND 65.13 Notes: NAPL - Non-Aqueous Phase Liquid ND - Not Detected -- - Not Applicable All measurements are in feet. Elevations are relative to a local datum with an assumed elevation,of 100.00 feet. Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 2:04:55 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA f Table 2 Page l of 4 Groundwater Sample Analytical Results-Volatile Petroleum Hydrocarbons Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA June 4, 1999 through May 1,2002 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS Groundwater Benzene Toluene Ethyl- Total MTBE Naphthalene C5-Cg C9-C12 C9 C10 Category (ug/I) (ug/1) benzene Xylenes (ug/l) (ug/1) Ali hatics Aliphatics Aromatics u /I u /I u 1 u /1 u /1 GW-1 5.0 1,000 700 10,000 70 20 400 4,000 200 GW-2 2,000 6,000 30,000 6,000 50,000 6,000 1,000 1,000 5,000 GW-3 7,000 50,000 4,000 50,000 50,000 6,000 4,000 1 20,000 4,000 LABORATORY ANALYTICAL RESULTS Well ID Date Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C8 C9-C12 C9 C10 Comments roundwater (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Aliphatics Aliphatics Aromatics Category) u n u /1 u /1 u /1 u /I AS-1 4/4/01 1 <5 1 25.6 1 <5 1 33.8 1 6.5 1 <5 91.3 <50 94 (GW-1,GW-3) 8/16/01 <5 <5 1 <5 1 <10 1 <5 <5 <50 <50 <50 MW-1 6/4/99 �2U60x 18 2700 435 2747 Mg T 040 <1000 <1000 (GW-1,GW-3) a r r 10/12/00 371109U 485 2243 4/4/01 376 257 1141 8 14.8 <100 407 8/16/Ol � 364 162 810 7-0333} <250 <250 7 12/4/01 42 140 63.8 27418` <10 <100 181 2 5/1/02 14 48 22 67.5 "637 <5 <50 1 <50 90.2 MW-lA 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-2 6/4/99 <5 <5 <5 <10 <5 <5 <100 <100 <100 (Gw-1,GW-3) 10/12/00 <5 <5 <5 <10 <5 <5 <50 <50 <50 4/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 20.4 1 <5 <50 <50 <50 MW-2A 4/4/O1k�� 92 147 250.8 5340 433r <50 142r 38 (GW-1,GW-3) 8/16/01 7 <5 <5 <10 fi4 <5 <50 <50 <50 �µ 12/4/0114 <5 <5 <10 14 <5 <50 <50 <50 5/1/02 22 '`` <5 <5 112Ft0 11.3 <50 <50 82.5 MW-3A 4/4/01 <5 <5 <5 <10 <5 6.1 <50 <50 <50 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 50.6 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-4 6/4/99 <1000 <1000 <1000 <10000 <1000 <20000 <20000 <20000 (GW-1,GW-3) 10/12/00 <5 <5 <5 <10 W11 ,.o£ <5 <50 <50 <50 4/4/01 <5 <5 <5 <10 41.7 <5 <50 <50 <50 8/16/01 <5 <5 <5 <10 12 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 15.2 <5 <50 <50 <50 002 GEOLOGIC SERVICES CORPORATION rpt_ma_vph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson MA Page 2 of 4 Table 2 Groundwater Sample Analytical Results-Volatile Petroleum Hydrocarbons Texaco Service Station#100083 1140Iyanough Road Hyannis,MA June 4, 1999 through May 1,2002 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS roundwater Benzene Toluene Ethyl- Total MTBE Naphthalene C5-Cg C9 C12 CO-CIO Category (ug/1) (ug/1) benzene Xylenes (ug/1) 09/1) Ali hatics Ali hatics Aromatics u u /1 u u /I u /l ff -15.0 1,000 700 10,000 70 20 400 4,000 200 -2 2,000 6,000 30,000 6,000 50,000 6,000 1,000 1,000 5,000 -3 7,000 50,000 4,000 50,000 50,000 6,000 4,000 20,000 4,000 LABORATORY ANALYTICAL RESULTS Well ID Date Benzene Toluene Ethyl- I Total MTBE Naphthalene C5-Cg C9 C12 C9 CIO Comments 'roundwater (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Aliphatic s Aliphatics Aromatics Category) (ug/1) (ug/1) (ug/1) (ug/1) (ug/1) MW-5 6/4/99 22 <5 <5 5.2f <5 <100 <100 <100 (Gw-1,Gw-3) 10/12/00 �20 t1 550 2434 23 ,, -0 <50 2580 $� `. 4/4/O1t#8 20 384 2014 ,26Tf �fl� <100 821 8/16/01 423 f L 0b 343 1938 1 Sflfl <200 <2000 ..... <2000 12/4/01 26Q 1{OQO 1 7690 ,,.. <500 4 2F2(l y 5/1/021520 <2500 <2500 MW-6 6/4/99 <25 <25 <25 <50 'SO <25 <500 <500 <500 (GW-1,GW-3) 10/12/00 <5 <5 <5 <10 <5. <5 <50 <50 <50 4/4/01 6.2 5.5 <10 ,00 .7 <5 <50 <50 97 8/16/01 <5 <5 <5 <10 15.6 <5 <50 <50 <50 12/4/01 $b <5 <5 <10 _7 <5 <50 <50 <50 5/1/02 <5 8.3 18.3 <50 <50 6 MW-9 6/4/99 ' QF 22 x0 �1 (1 7 �" 3 <5000 <5000 � ..�. .Y GW-1,GW-3is ( ) 10/12/00 MAW4311 c1 380 & 0 1 0 A r 5/1/02 1£ (Ibg (... $$0... . i � 8I9Q ., 3230611� MW-10 6/4/99 <5 63.8 8.2 50.1 <5 <5 <100 <100 <100 (GW-1,GW-3) 10/12/00 <5 <5 <5 <10 27.2 "ate ' ` .i.Y 71 �" 98.93 „ .• 4/4/01 <5 <5 <5 <10 <5 9.5 <50 <50 100 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-11 4/4/01 <5 <5 <5 <10 7 <5 <50 <50 <50 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 2,<' <5 <50 <50 <50 MW12 4/4/O1 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 <5, <5 <50 <50 <50 MW-13 4/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 2002 GEOLOGIC SERVICES CORPORATION rpt_ma_vph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Page 3 of 4 Table 2 Groundwater Sample Analytical Results-Volatile Petroleum Hydrocarbons Texaco Service Station#100083 1140Iyanough Road Hyannis,MA June 4, 1999 through May 1,2002 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS roundwater Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C8 C9 C12 C9 C10 Category (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Aliphatics Aliphatics Aromatics (ug/1) (ug/1) (ug/1) (ug/1) u l ff -15.0 1,000 700 10,000 70 20 400 4,000 200 -2 2,000 6,000 30,000 6,000 50,000 6,000 1,000 1,000 5,000 -3 7,000 50,000 1 4,000 1 50,000 1 50,000 6,000 4,000 20,000 4,000 LABORATORY ANALYTICAL RESULTS Well ID Date Benzene Toluene Ethyl- Total MTBE Naphthalene C5-Cg C9 C12 C9 C10 Comments Troundwater (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Aliphatics Aliphatics Aromatics Category) (ug/1) (ug/1) (ug/1) (ug/1) (ug/1) MW-14(25) 4/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-14(70) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) MW-14(90) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) MW-15(20) 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-16(20) 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 I (GW-1,GW-3) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-16(55) 12/4/01 Fr <50 <50 <100 115UU <50w' „ <500 (GW-1,GW-3) 1/3/02 h9€} 19.8 8 24.7 3!"P 0# 3 3 E 454 " 330 �0 5/1/02 # <5 <5 <10 �480 <5 <50 <50 122 MW-17(20) 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 l (GW-1,GW-3) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-18(25) 5/1/02 <5 <5 <5 <10 26.8 <5 <50 <50 <50 (GW-1,GW-3) MW-18(70) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) TMP-1 8/16/01 5 <12 <12 <24 8,68 <12 <120 <120 <120 (GW-1,6W-3) TMP-2 8/16/01 j„x )a3 <25 <25 <50 <25 <250 <250 <250 (GW-1,GW-3) TMP-3 8/16/01 <5 <5 <5 <10 � 158x'K' <5 <50 <50 <50 (GW-1,GW-3) TMP4 8/16/01 <5 <5 <5 <10 21.1 <5 <50 <50 <50 (GW-1,GW-3) TMP-5 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) TMP-6 8/16/O1 <5 <5 <5 <10 14.8 <5 <50 <50 <50 (GW-1,GW-3) TMP-7 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-I,GW-3) 2002 GEOLOGIC SERVICES CORPORATION rpt ma_vph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Page 4 of 4 Table 2 Groundwater Sample Analytical Results-Volatile Petroleum Hydrocarbons Texaco Service Station#100083 1140Iyanough Road Hyannis,MA June 4, 1999 through May 1,2002 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS roundwater Benzene Toluene Ethyl- Total MTBE Naphthalene C5-Cg C9 C12 C9 C10 Category (ug/1) (ug/1) benzene Xylenes (ug/I) (ug/1) Aliphatics Aliphatics Aromatics u l u /1 u l u /1 u GW-1 5.0 1,000 700 10,000 70 20 400 4,000 200 GW-2 2,000 6,000 30,000 6,000 50,000 6,000 1,000 1,000 5,000 GW-3 7,000 1 50,000 1 4,000 1 50,000 50,000 6,000 4,000 1 20,000 4,000 LABORATORY ANALYTICAL RESULTS Well ID Date Benzene Toluene Ethyl- Total MTBE Naphthalene C5-Cg C9 C12 CO-C10 Comments groundwater (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Aliphatics Aliphatics Aromatics Category) u /1 u /1 u /1 u /1 u l x: dCP - Massachusetts Contingency Plan :10 - not detected at or above the method detection limit(method detection limit included) ✓ITBE - methyl tertiary butyl ether ig/l - micrograms per liter(parts per billion) GW-2) - well-specific groundwater category not analyzed/not applicable shading indicates reported concentration exceeds the applicable MCP Method 1 Risk Characterization Groundwater Standard(s). 2002 GEOLOGIC SERVICES CORPORATION rpt_m2_vph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 3 Page 1 of 2 Groundwater Sample Analytical Results-Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA June 4, 1999 through April 4,2001 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS C e N m M f W Ol v O OQ S G�i O _ �O N C m C'p C '� C C S C d C C G N C C S 3 Groundwater Category A A m e y GW-1 20 1 300 12,000 1 1.0 1 0.2 1 1.0 1 300 1 1.0--f 2.OT 0.5 300 1 300 1 0.5 1 10 1 20 1 300 1 200 14,000 15,000 1 200 GW-2 - I - - - I - I - I - - 110,00016,000 1 - - 11,000 50,000 GW-3 5,000 3,000 3,000 3,000 3,000 3,000 3,000 3,000 3,000 3,000 200 3,000 3,000 3,000 6,000 50 3,000 20,000 20,000 30,000 LABORATORY ANALYTICAL RESULTS '9 A _ °i ° .�d .. o Q F n c 'i7 •e 9 m C� , (� S C = C S C� C � C C' C N C C � C m C`< N Q�pp p�qq G OG C a C r{ S Well ID Date Comments y MW-1 6/4/99 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 381 1520 <170 (GW-1,GW-3) 10/12/00 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 EM <5 <5 1120 184 <100 4/4/01 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <100 210 127 MW-2 6/4/99 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <60 <167 <170 (GW-1,GW-3) MW-4 6/4/99 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 96.4 <80 <170 (GW-1,GW-3) 10/12/001 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 1 <5 <100 <100 <100 MW-5 6/4/99 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <60 <80 <170 (GW-I,GW-3) �. "w 10/12/00 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 �%`�=4 4:9; <5 <5 1010 <100 105 4/4/01 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <100 <100 134 MW-9 6/4/99 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 17 16 <5.3 <5.3 1200 <84 � 2 (GW-1,GW-3) 10/12/00 1 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 i $33 <5 <5 3890 <100 277 MW-10 6/4/99 <3.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <61 <82 <170 (GW-1,GW-3) 10/12/00 1 <5 1 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <100 <100 <100 6/18/2002 GEOLOGIC SERVICES CORPORATION Ref.: tpt_ma_eph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 3 Groundwater Sample Analytical Results-Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA June 4, 1999 through April 4,2001 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS d N A 'lot no Groundwater Category GW-1 20 1 300 2,000 1 1.0 1 0.2 1 1.0 1 300 1 1.0 1 2.0 1 0.5 1 300 1 300 1 0.5 1 10 1 20 1 300 1 200 1 4,000 15,000 A... GW-2 — — — 10,000 6,000 — 1,000 GW-3 5,000 3 000 3,000 3,000 3,000 3,000 3,000 3,000 3,000 3,000 200 3,000 3,000 3,000 6,000 50 3,000 20,000 20,000 , LABORATORY ANALYTICAL RESULTS 1Z b7 to tL C7 N fi N W O N O N p "d n f0 O = O p A a = of = m o Q oo m e Z2 S C d C C C N C C S C L1 C`�7 C C G N S O O _ ., OC W OG 'O _ A 1.4 We11ID Date Comments m Notes: MCP Massachusetts Contingency Plan ug/1 - micrograms per liter(parts per billion) (GW-3) - well-specific groundwater category <10 - not detected at or above the method detection limit(method detection limit included) not applicable or not analyzed ,. ,' - shading indicates reported concentration exceeds the applicable MCP Method 1 Risk Characterization Groundwater Standard Ref: 002 GEOLOGIC SERVICES CORPORATION Ref.: :pt_ma_eph_aq\000509\100083 Hydmgeologists and Environmental Scientists IS Bonazzoli Ave.,Hudson,MA Page 1 of 1 Table 4 Historical Soil Analytical Results Volatile Petroleum Hydrocarbons Shell Service Station#100083 1140Iyannough Road Hyannis,Massachusetts Groundwater Benzene Toluene Ethyl- Total MTBE Naphthalene CS-Cs C9-C12 C9_C10 Category (ug/g) (ug/g) benzene Xylenes (ug/g) (ug/g) Aliphatics Aliphatics Aromatics (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) S-11GW-1 10 90 80 500 0.3 4 100 1,000 100 S-1/GW-2 40 500 500 500 100 100 100 1,000 100 S-1/GW-3 40 500 500 500 100 100 100 1,000 100 S-3/GW-I 10 90 80 800 0.3 4 500 5,000 100 S-3/GW-2 100 500 2,500 2,500 200 1,000 500 5,000 500 S-3/GW-3 200 2,500 500 500 200 1,000 500 5,000 500 LABORATORY ANALYTICAL RESULTS Sample Date Depth Benzene Toluene Ethyl- Total MTBE Naphthalene C5-Cs C9-C12 C9-Clo ID (it) (ug/g) (ug/g) benzene Xylenes (ug/g) (ug/g) Aliphatics Aliphatics Aromatics u / u / u / u / u / MW-8 5/6/98 29-31 <65 <65 <65 <65 <65 <65 <325 <325 $$ 65 3 65 947 2? > » (:':` : :> `` (Y ::21?43><»> >>2> t1>z> >zz > ifi) <' MW-9 5/6/98 29 1 ......................... ....... �............ ........,........ ..................... MW-10 5/6/98 30-32 <55 <55 <55 <55 <55 <55 <285 <285 MW-11 3/22/01 25-30 <0.190 <0.190 <0.190 <0.190 <0.190 <0.190 <3.9 <3.9 <3.9 MW-12 3/22/01 25-30 <0.210 <0.210 <0.210 <0.210 <0.210 <0.210 <4.2 <4.2 <4.2 MW-13 3/23/01 25-30 <0.220 <0.220 <0.220 <0.220. <0.220 <0.220 <4.3 <4.3 <4.3 MW-14 3/23/01 25-27 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <3.4 <3.4 <3.4 SB-8 5/6/98 30-32 <60 <60 <60 <60 <60 <60 <315 <315 z SB-9 5/6/98 30-32 <65 <65 <65 <65 <65 <65 <335 <335 #x3 < SB-11 5/6/98 30-32 <65 <65 <65 <65 1,&60 <65 $ ? <330 $ . ASO1 3/21/01 24 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <3.4 <3.4 <3.4 MP01 3120/01 30-31 <0.190 <0.190 <0.190 <0.190 <0.190 <0.190 <3.8 <3.8 <3.8 MP-2 3/22/01 25-30 <0.180 <0.180 <0.180 <0.180 <0.180 <0.180 <3.5 <3.5 <3.5 MP03 3/21/01 28 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <3.3 <3.3 <3.3 SVE01 3/20/01 30-31 <0.240 <0.240 <0.240 <0.240 <0.240 <0.240 <4.7 <4.7 <4.7 Notes: MTBE-methyl tert-butyl ether ug/g-micrograms per gram(parts per million) <0.2-not detected(method detection limit included) E -indicates analyte exceeds applicable MCP Reportable Concentration Ref#: 000509.tble-soil-vph TABLE 5 Summary of SVE Step Test Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts May 4,2001 Time SVE-1 SVE S stem (min) Vac (ft/min)* SCFM ACFM ("HZO) (measured)(calculated (calculated) Static --- --- --- 5 2 3375 74 74 10 4 4700 102 103 15 6 5140 112 112 20 8 5900 129 128 25 10 8010 175 172 30 12 L.8750 191 187 Notes: SVE-1 -soil vapor extraction well "HZO-inches of water column SVE System-soil vapor extraction system SCFM-standard cubic feet per minute ACFM-actual cubic feet per minute *Soil vapor flow rates taken from 2-inch diameter PVC pipe,with an anamometer. Summary of SVE/AS Pilot Testing Data Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts May 4,2001 Date: May 4,2001 Extraction Well ID: SVE-1 GSC Job#: 000509 Well Diameter(in): 4" Site ID: EQ/Hyannis Initial DTP(ft): NA Site Address: 1140 Iyanough Road Initial DTW(ft): 31.12 City,State: Hyannis,MA DTB(ft): 35.89 F-Ti-m-ell g Soil Vapor Extraction Well After SVE System 11 SVE Off-Gas Treatment ASS stem (min) Pressure VOC Flow Rate Flow Rate Temp He Pressure VOC Flow Rate Temp Mid Effluent Pressure Flow ("H2O) (ppm") (ft/min) (scfm) ('F) (%) (��H2O) (ppm.) (ft/min) ('F) (ppmv) (PPmV) (psi) (scfm) 0 --- 4.1 --- --- --- --- --- --- --- --- --- --- --- --- 5 -5.00 765 4900 106.9 66.0 --- 20.30 437 8100 132.0 19.7 0.10 15 -5.00 766 4950 107.9 65.6 --- 19.60 440 8110 133.0 20.1 0.20 --- --- 30 -5.00 659 4900 106.8 65.6 --- 20.58 375 8100 134.0 8.4 0.00 --- --- 45 -5.00 716 4920 107.3 65.2 --- 20.50 409 8100 134.0 191.13 0.00 --- --- 60 -10.20 431 8100 176.6 64.3 --- 19.50 450 7400 131.0 88.5 0.70 --- --- 75 -10.50 437 8100 176.E 65.1 --- 19.50 450 7510 132.0 65.5 0.00 --- --- 80 -5.00 --- --- --- --- --- --- --- --- --- --- --- 8.0 3.0 .85 -5.00 --- --- --- --- --- --- --- --- --- --- --- 8.0 3.0 90 -5.20 415 4831 105.3 64.5 --- 20.40 240 7900 130.6 44.8 1.3 8.0 3.0 105 -5.11 818 4740 103.4 65.2 --- 20.70 464 7910 130.6 64.2 2 8.0 3.0 120 -5.23 496 4810 104.9 65.2 --- 20.30 285 7910 130.6 58.7 1.3 8.0 3.0 135 -5.21 508 4830 105.3 65.2 --- 20.20 294 7890 130.4 59.7 1.4 1 8.0 3.0 140 -5.20 --- --- --- --- --- --- -- --- --- - --- 9.0 6.5 145 -5.10 --- --- --- --- --- --- --- --- --- --- --- 9.0 6.5 150 -5.12 375 4820 105.1 65.2 --- 21.10 218 7845 131.4 46.7 1.1 9.0 6.5 165 -5.11 464 4820 105.1 64.9 --- 22.30 268 7920 131.2 66.6 1.1 9.0 6.5 180 -5.20 469 4810 104.9 65.1 --- 21.00 271 7855 132.1 71.2 1.3 9.0 6.5 185 -5.12 --- --- --- --- --- --- --- --- --- --- --- 9.0 6.0 190 -5.20 --- --- --- --- --- --- --- --- --- --- --- 9.0 6.0 195 -5.22 380 4815 105.0 65.3 --- 20.20 220 7850 131.4 48.7 1.2 9.0 6.0 210 -5.15 372 4910 107.1 65.2 --- 20.40 219 7860 132.1 47.9 1.1 9.0 6.0 Notes: Time-time from beginning of pilot test in minutes(min) ACFM-actual cubic feet per minute SVE-1-soil vapor extraction well Mid-soil vapor sample measured between the two carbon vessels with a PID "1120-inches of water column calibrated to read total VOCs as benzene. Influent-soil vapor samples measured with a photoionization detector(PID)calibrated Effluent-soil vapor sample measured after the last GAC with a PID to read total volatile organic compounds(VOCs)as benzene. calibrated to read total VOCs as benzene. ppm -parts per million per unit volume AS System-air sparge system SVE System-soil vapor extraction system psi-pounds per square inch SUM-standard cubic feet per minute NM-not monitored TABLE 7 Summary of SVE/AS Pilot Testing Data-Monitoring Point Data Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts May 4,2001 Date: May 4,2001 Extraction Well ID: SVE-1 GSC Job#: 000509 Site ID: EQ/Hyannis Site Address: 1140 Iyanough Road City,State: Hyannis,MA Time Monitoring Point ID:MP-1 Monitoring Point ID:MP-2 (min) 10.4 ft to AS-1 8.00 ft to SVE-1 15.21 ft to AS-1 17.50 R to SVE-1 Across Shallow = Deep Across Shallow Dee Pressure VOC DTW DO Pressure He rPressure He Pressure VOC DTW DO Pressure He Pressure He ( HzO) Win,) (ft) (mom) ("HzO) (%) ("HzO) (%) ("HzO) (VOC) (ft) (mg/1) ("H20) (%) ("HzO) (%) 0 0.00 4.0 32.44 1.4 -- --- --- --- 0 57.0 32.69 0.9 --- --- --- - 5 -0.77 0.0 32.41 1.0 --- --- --- -- -0.48 0.0 32.67 1.0 --- --- --- -- 15 -0.77 0.0 32.41 1.0 --- --- --- --- -0.48 0.0 32.67 1.0 --- --- --- -- 30 -0.74 0.0 32.42 1.2 --- --- --- --- -0.42 0.0 32.66 1.0 --- --- --- --- 45 -0.65 0.3 32.4 1.2 --- --- --- --- -0.33 0.0 32.67 1.0 --- -- --- -- 60 -1.16 0.0 32.39 1.4 --- -- --- --- -0.52 1 0.0 32.66 1.0 --- --- --- --- 75 1 -1.05 0.0 32.39 1.4 --- - --- -0.65 0.0 32.66 1.2 --- --- -- 80 -0.75 --- 32.36 --- -0.13 --- 0.00 -- -0.37 --- 32.62 --- 0.00 0.00 85 -0.75 --- 32.36 --- -0.13 --- -0.01 --- -0.39 --- 32.62 --- 0.01 --- 0.00 90 -0.76 0.0 32.35 2.8 -0.13 --- 0.01 --- -0.41 0.0 32.60 1.5 0.00 0.00 105 -0.65 0.0 32.34 1.8 -0.13 --- -0.02 --- -0.42 0.0 32.60 2.0 0.01 - 0.00 --- 120 -0.74 0.0 32.35 1.6 -0.12 --- 0.00 --- -0.39 0.0 32.61 1.3 0.00 --- 0.00 -- --- 32.30 - 0.00 --- -0.42 0.0 32.62 1.3 0.00 -- 0.00 --- 140 -0.78 -- 135 -0.74 32.32 1.6 -0.16 --- -0.03 --- -0.38 --- 32.56 --- 0.00 --- 0.11 -- 145 -0.74 --- 32.29 --- -0.14 --- 0.00 -0.38 --- 32.54 0.00 --- 0.00 -- 150 -0.75 0.0 32.28 2.2 -0.14 --- 0.00 --- -0.38 0.0 32.54 1.6 0.00 --- 0.00 --- 165 -0.75 0.0 32.27 3.4 -0.14 --- 0.00 --- -0.37 0.0 32.52 1.6 0.00 --- 0.00 180 -0.75 0.0 32.27 1.8 -0.17 --- 0.00 --- -0.42 0.0 32.51 1.6 0.00 --- 0.00 --- 185 -0.71 32.27 1.8 -0.14 0.01 0.00 0.03 -0.37 --- 32.51 1.5 0.00 0.00mfl�-0020 190 -0.72 32.27 1.7 -0.17 0.02 0.00 0.02 0.36 - 32.51 1.4 0.00 0.00195 -0.71 0 0 32.27 1.6 -0.16 0.02 0.00 0.02 -0.38 0.0 32.52 1.4 0210 -0.73 0.0 32.28 1.7 0.15 002 000 0.02 -0.38 0.0 32.53 1.3 0.00 0.00 Notes: Time-time from beginning of pilot tests in minutes ppmv-parts per million per unit volume SVE-1-vapor extraction well DTW-depth to water measured in monitoring point using an electronic AS-1-air sparge well interface probe measured in feet(ft) Pressure-observed in monitoring well inches of water column("HQ) DO-dissolved oxygen VOC-soil vapor samples measured with a photoionizadon detector(PID)calibrated mg/l-milligrams per liter to read total volatile organic compounds(VOCs)as benzene. NM-not measured TABLE 7 Continued Summary of SVE/AS Pilot Testing Data-Monitoring Point Data Texaco Service Station#100083 1140Iyannough Road Hyannis,Massachusetts May 4,2001 Date: May 4,2001 Extraction Well ID: SVE-1 GSC Job#: 000509 Site ID: EQ/Hyannis Site Address: 1140 Iyanough Road City,State: Hyannis,MA Time Monitoring Point ID:MP-3 Monitoring Point ID:MW-9 (min) 26.32 ft to AS-1 27.00 ft to SVE-1 43.00 ft to AS-1 45.00 ft to SVE-1 Across Shallow Deep -� Across Pressure VOC DTW DO Pressure He Pressure He Pressure VOC DTW DO ("H2O) (ppm.) (ft) (mg/►) (��H2O) (°/u) C H2O) (%) (��H2O? (VOC (ft) (mg/1) 0 0.00 1.7 32.79 1.0 --- --- --- 0.00 4.00 32.44 1.4 5 -0.33 0.0 32.80 1.0 --- --- --- -0.15 0.00 32.41 1.0 15 -0.33 0.0 32.80 1.0 --- --- -0.15 0.00 32.41 1.0 30 -0.27 0.0 32.80 1.0 --- --- --- -0.12 0.00 32.42 1.2 45 -0.22 0.1 32.79 1.0 --- --- -0.11 0.30 32.40 1.2 75 -0.35 0.0 32.79 1.0 - -0.18 0.00 32.39 1.4 80 -0.26 --- _32.76 --- -0.02 --- -0.10 --- --- --- --- --- 85 -0.24 --- 32.75 --- -0.02 --- -0.09 --- --- --- --- 90 -0.24 0.0 32.74 1.6 -0.03 --- -0.09 --- --- 105 -0.22 0.0 32.73 2.4 -0.03 --- -0.09 --- --- --- --- 120 -0.28 0.0 32.73 1.8 -0.05 --- -0.09 --- --- --- --- 135 -0.23 0.0 32.72 1.8 -0.03 --- -0.07 --- --- --- 0.27 --- -0.05 --- 0.13 --- --- --- --- 140 32.71 145 -0.27 --- 32.69 - -0.04 --- -0.09 --- --- --- --- --- 150 -0.20 0.0 32.68 1.6 -0.03 --- -0.09 --- --- --- --- 165 -0.23 0.0 32.65 1.7 -0.04 --- -0.09 --- --- --- --- 180 0.21 0.0 32.64 1.6 0.04 -0.08 --- _ --- --- 185 -0.24 - 32.64 1.6 -0.03 0.02 -0.08 0.00 --- --- 190 -0.22 --- 32.64 1.5 -0.02 0.01 -0.07 0.00 --- --- 195 0.26 0.0 32.64 1.5 -0.02 0.01 -0.08 0.00 --- --- 210 -0.23 0.0 32.65 1.4 -0.03 0.02 0.08 0.00 --- I --- Notes: Time-time from beginning of pilot tests in minutes ppmv-parts per million per unit volume SVE-1-vapor extraction well DTW-depth to water measured in monitoring point using an AS-1-air sparge well electronic interface probe measured in feet(ft) Pressure-observed in monitoring well inches of water column("H20) DO-dissolved oxygen VOC-soil vapor samples measured with a photoionization detector(PID)calibrated mg/l-milligrams per liter to read total volatile organic compounds(VOCs)as benzene. NM-not measured TABLE 8 Summary of SVE/AS Pilot Testing Data Texaco Service Station#100083 1140Iyannough Road Hyannis,Massachusetts May 18,2001 Time SVE-1 AS-1 MP-1 Pressure("H20) MP-2 Pressure("H20) MP-3 Pressure("H20) (min) Pressure("H20) Flow Rate(ft/min) Pressure(psi) Flow Rate(scfm) I across shallow deep across shallow deep across shallow deep --- '1 --- --- --- 15 -1.3 1 1300 0 0 -0.2 0 0 -0.11 0 0 -0.05 0J 0 30 -1.3 1325 0 0 -0.2 0 0 -0.11 0 0 -0.05 0 0 Summa Can Sample Taken For SVE Test --- --- --- --- 15 -1.3 1310 10 6 019 0 0 0.1 0 0 0.05 0 0 30 -1.3 1310 10 6 0.19 0 0 0.1 0 0 0.05 0 0 Summa Can Sam le Taken For SVE/AS Test Notes: Time-time from beginning of pilot tests in minutes SVE-1-vapor extraction well AS-I-air sparge well Pressure-observed in monitoring well inches of water column("HQ) SUM-standard cubic feet per minute PSI-pounds per square inch Table 9 Summary of SVE/AS Pilot Test Air Sample Analytical Data at SVE-1 Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts May 18,2001 Sample ID: SVE Compound Results Results (ppb,) (µg/m3) Benzene 31,900 102,000 Eth lbenzene 30,700 133,000 Toluene 318,000 1,200,000 X lens(total) 132,000 572,000 MTBE 11 79,300 11 285,000 Sam le ID:SVE+AS Compound Results Results (ppb,,) (µg/m3) Benzene 28,200 90,000 Eth lbenzene 29,700 129,000 Toluene 204,000 768,000 X lens(total) 149,000 646,000 MTBE 72,900 262,000 Notes: ppb,,-part per billion per unit volume µg/m-micrograms per cubic meter ND-not detected MTBE-Methyl Tertiary Butyl Ether Ref#000509.SVE/AS Appendix C Groundwater Analytical Results New England 12/19/01 ®A=L)TEST ep.Tt ........................ ._. _..................................................... Equiva Services GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M22269 Report to: Geologic Services Corp. 15 Bonazzoli Ave Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 50 eza Zd Lab Director Certifications:MA(MA136) CT(PH-0109) NH(250293) RI(A-71) ME(MA136) This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England ■495 Tech Center West■Building 1 0 Marlborough,MA 01752 0 tel:508481-6200 2 fax:508481-7753 0 http://www.accutest.com � R Accutest Laboratories Sample Summary Equiva Services Job No: M22269 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sam le COIetetl ' i Matrix Client P ..................... .............................. Number Date Time By Received Code Type Sample ID M22269 12/04/01 14:50 MLM 12/ 5/01 AQ Ground Water >;MWO1: .....M.. 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Hyannis MA .................... .................................................... Sample Collect;> >< Matrix Client Number Date Time By Received Code Type Sample ID M 12 1 A round Water s` 1: `'_ "< 6< .. ;« > '�,M69 14 12/04/01 09:58 ML /05/0 Q G MW 6 MW 1 ..................................................................... M22269.1$: 12/04/01 09:55 MLM 12/05/01 AQ Ground Water 1 IW16D MW 16U M22269-1f: 12/04/01 13:45 MLM 12/05/01 AQ Ground Water 1VWI71vIW i7 . h+I22269-17 12/04/01 16:05 MLM 12/05/01 AQ Field Blank Water FB 2 A Trip Blank Water ..........., 12/04/Ol 16:06 MLM 1 /OS/Ol T$< <<< >> > ' >< > ' .. ''< < 1I222..:.9::1$. Q P _ ....................................... Filtered =It�IVVtJI=1VIV 1 >< <<i > < ; lv€ f9- A 12/04/Ol 14:50 MLM 12/OS/Ol AQ Groundwater .. ......................................................... Filtered ><> > » > >< M 22 t 12/04/01 11:00 MLM 12/05/01 AQ GroundwaterM tJZA...MVO.:2 ::::::::::::::::. :::::......:::::::::::::..: ..................... .:.............................................. wFiltered ::IvI W . 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Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1254.1) 2 12/08/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene A _ » 10 ug/I ........................... ........................... 100-41-4 Ethylbenzene b 8; 10 ug/I 1634-04-4 Methyl Tert Butyl Ether 7G8i'' 'i 10 ug/I ...........I............... ........................... 91-20-3 Naphthalene D ;> 10 ug/l ....:..................... ........................... ........................... 108-88-3 Toluene 0s <> > << 10 ug/I .........................:. ........................... m,p Xylene 189 >> 10 ug/I ......:.................... ........................... ........................... 95-47-6 o-Xylene $ 10 ug/I .......................... ........................... C5-C8 Aliphatics (Unadj.) 100Q <'' 100 ug/I . ...................... ........................... ........................... C9- C12 Aliphatics (Unadj.) <3 ;9 i .. 100 ug/I ........................... 320>C9-C10 Aromatics(Unadj.) ; IM ug/I C5-C8 Aliphatics i` i 100 ug/I ........................... .........................- C9-C12 Aliphatics YS;i< ; 100 ug/I .......:................... ........................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 73ai 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 74%i< >>< 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MWOl-MW-1 Lab Sample ID: M22269-1 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 1118741.1) 1 12/10/01 ANJ n/a n/a N:GII937 Run#2 CAS No. Compound Result RL Units Q 74-82-8 Methane , ::: 0.10 ug/1 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOI-MW-1 Lab Sample ID: M22269-1 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity, Total 5.0 mg/l 1 12/11/01 BF EPA 310.1 Carbon Dioxide .........:.................... ........ 0 mg/l 1 12/11/01 MA SM18 4500002D ...........; ...... ................................. Nitrogen, Nitrate aQa 0.11 mg/l 1 12/12/01 MA EPA 353.2 Nitrogen, Nitrate + Nitrite 4f.1(#........: 0.10 mg/l 1 12/12/01 MA EPA 353.2 .......................................... .............-.......... .................................. Nitrogen, Nitrite (t 01:(1 <; >>>0.010 mg/l 1 12/05/01 MA EPA 354.1 Sulfate (;$; 5.0 mg/I 1 12/10/01 BF EPA 375.4 Sulfide 2 `< `<i 2.0 mg/1 1 12/07/O1 BF EPA 376.1 (a) Calculated as: (Nitrogen, Nitrate + Nitrite)-(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW02-MW-2 Lab Sample ID: M22269-2 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File El) DF Analyzed By Prep Date Prep Batch Analytical Batch Run#I WX1257.D 1 12/08/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ..*:::::::::::: C A ug/I 7143-2 Benzene ........ :: .................. .......................... ........... ... ....... 100-414 Ethylbenzene .... 5.0 ug/I ...... .... ............. 1634-04-4 Methyl Tert Butyl Ether 5.0 ug/I ....................... -...... . ................................ 91-20-3 Naphthalene .:.ND.*::'.....�'-....:...�::�:�'..:�.:'5.0 ug/I ......................... ............. ... .......................... ........................... . . ..... ... ...................... 108-88-3 Toluene 5.0 ug/I .............. .............. .... ........I........... ........... ...... . ......... . ................. m,p-Xylene :NO:*...........:,:..:.....*..,:.�*..:..*5.0 ug/I ....11..... .............. ......................... .................................................. 9547-6 o-Xylene 51.0 ug/I ... ............ ............... C5-C8 Aliphatics(Unadj.) ....N...........D..... ......... ........................... ......-. 50 ug/I . ....... ... . .............-........ C9- C12 Aliphatics(Unadj.) . - JU ug/I C9- CIO Aromatics(Unadj.) 1llj . . 50 ug/I ........I.... ............. .............. .............. C5-C8 Aliphatics 50 ug/I ................. .......................... .............................. C9-C12 Aliphatics .... .. ug/I... ... ............-............ CAS No. Surrogate Recoveries Run#1 Run#2 Limits .......... 615-59-8 2,5-Dibromotoluene -130% 70 ....................... ......................... 615-59-8 2,5-Dibromotoluene .... 70-130% . ................ ................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M22269-3 Date Sampled: 12/04/01 Matrix: AQ.-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1240.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ................... ........................... 71-43-2 Benzene 1:41 >» 5.0 ug/1 5.0 ug/1 100-41-4 Ethylbenzene 1n> <> ........................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether 21 5.0 ug/1 91-20-3 Naphthalene113 ' 5.0 ug/1 ......................... ........................... .. ...................... 108-88-3 Toluene ND< 5.0 ug/I m,p-Xylene I ><>>':>> > 5.0 ug/1 ....................................... ........................... ........................... 95-47-6 o-Xylene ;ND. >s;i; 5.0 ug/1 C5-C8 Aliphatics(Unadj.) 1$` _ 50 ug/I .. ...........:........ ........................... ........................... C9-C12 Aliphatics(Unadj.) ND`>> > >< 50 ug/1 C9-C10 Aromatics(Unadj.) 50 ug/1 ... . ................. ........................... .......................... N . C5-C8 Aliphatics D; 50 ug11 C9-C12 Aliphatics N1 < ; 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene4 '< ;i<> 70-130% 615-59-8 2,5-Dibromotoluene 7 ` < 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M22269-3 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II18743.D 1 12/10/01 ANJ n/a n/a N:GII937 Run#2 CAS No. Compound Result RL Units Q ........................... ........................... 74-82-8 Methane ; 0.10 ugll ........................... (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M22269-3 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method ............................. .................................. Alkalinity, Total 5 2> 5.0 mg/l 1 12/11/01 BF EPA 310.1 Carbon Dioxide 77 > ;; 5.0 mg/l 1 12/11/01 MA SM18 45000O2D ................................. .................................. ................................. Nitrogen, Nitrate a 19i <>i<»> 0.11 mg/1 1 12/12/01 MA EPA 353.2 Nitrogen, Nitrate + Nitrite i;'9>;> _ ; 0.10 mg/l 1 12/12/01 MA EPA353.2 ..:.............................. ................................. .................................. Nitrogen, Nitrite (li 0.010 mg/l 1 12/05/01 MA EPA 354.1 Sulfate 5.0 mg/l 1 12/10/01 BF EPA 375.4 ................................. .........I........................ ................................. Sulfide 2 Q'< ' ' 2.0 mg/l 1 12/07/01 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOIA-MW-IA Lab Sample ID: M22269-4 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch' Analytical Batch Run#1 WX1241.13 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ................--...... ................ ..... ... 71-43-2 Benzene 1ID; 5.0 ug/1 100-41-4 Ethylbenzene1D 5.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 1ID 5.0 ug/1 91-20-3 Naphthalene N33 << 5.0 ug/1 108-88-3 Toluene lD 5.0 ug/1 m,p-Xylene 1tD 5.0 ug/1 95-47-6 o-Xylene ND 5.0 ug/1 :....................I-- CS-C8 Aliphatics(Unadj.) ;' ' 50 ug/1 ... .........:.......... ........................... C9- C12 Aliphatics(Unadj.) ND'; <>> 50 ug/I C9-C10 Aromatics(Unadj.) >>> 50 ug/I C5-C8 Aliphatics ........................ ) > ;> <;; 50 ug/1 C9-C 12 Aliphatics ND << 50 ug/1 CAS No. Surrogate Recoveries Run#1 Ruh#2 Limits ............. 615-59-8 2,5-Dibromotoluene ; 70-130% ..:...................... ................ . ........ 615-59-8 2,5-Dibromotoluene ?I%<<' 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M22269-5 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1293.1) 1 12/10/01 AF n/a n/a GWX36 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene .......... >><> ; 5.0 ug/1 :.......................... ........................... ........................... 100-41-4 Ethylbenzene N ;> >; 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether S(7 « <<i 5.0 ug/1 91-20-3 Naphthalene III 5.0 ug/1 :::..:..................... ........................... ........................... 108-88-3 Toluene tTI3< 5.0 ug/1 ........................... ........................... m,p-Xylene D `< 5.0 ug/1 ............... ........................... ........................... 95-47-6 o-Xylene ND; 5.0 ug/1 C5- C8 Aliphatics(Unadj.) ND 50 ug/1 .......................... ........................... C9-C12 Aliphatics(Unadj.) I1D 50 ug/1 C9-C10 Aromatics(Unadj.) laiD><` ;; 50 ug/1 C5-C8 Aliphatics NIz> 50 ug/1 ......:.................... ........................... ........................... C9- C 12 Aliphatics ND<; ; 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 8 ; 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 84% > ` > 70-130% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M22269-5 Date.Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 1118744.1) 1 12/10/01 ANJ n/a n/a N:GI1937 Run#2 CAS No. Compound Result RL Units Q ........................... 74-82-8 Methane ND><< 0.10 ug11 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound .r Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M22269-5 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity, Total 5£� ;; 5.0 mg/1 1 12/11/01 BF EPA 310.1 .................................. .............................-- ....................-............ Carbon Dioxide 17 5.0 mg/1 1 12/14/01 MA SM18 45000O2D ................................. .................................. ................................. Nitrogen, Nitrate a 2 s >> 0.11 mg/1 1 12/12/01 MA EPA 353.2 ;:.:..:......;: ;:.;;:.:<.:;.;;: Nitrogen, Nitrate + Nitrite ; 0.10 mg/1 1 12/12/01 MA EPA 353.2 .................................. ................................. .................................. Nitrogen, Nitrite C( flQ; ; '; 0.010 mg/1 1 12/05/01 MA EPA 354.1 .....:............................ ................................. .................................. Sulfate >CS 5.0 mg/l 1 12/10/01 BF EPA 375.4 ................................. .................................. ................................. Sulfide <2 >s 2.0 mg/1 1 12/07/01 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW04-MW-4 Lab Sample ID: M22269-6 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1294.D 1 12/10/01 AF n/a n/a GWX36 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene .ND 5.0 ug/I 100-41-4 Ethylbenzene atiTl >; .. 5.0 ug/I.... 1634-04-4 Methyl Tert Butyl Ether 1 ;2 <`> 5.0 ug/I 91-20-3 Naphthalene >; « 5.0 ug/I ........................... ........................... ........................... 108-88-3 Toluene ND 5.0 ug/I m,p-Xylene ND> 5.0 ug/I 95-47-6 o-Xylene I+TD 5.0 ug/I C5-.C8 Aliphatics(Unadj.) 'hID ? 50 ug/I C9-C12 Aliphatics(Unadj.) `ND ; 50 ug/I C9-C10 Aromatics(Unadj.) < »` 50 ug/I C5-C8 Aliphatics :N > > 50 ug/I C9-C12 Aliphatics <Nl`' < ; 50 ug/I ......................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 40 '<< 70-130% .......--.............. ......................... 615-59-8 2,5-Dibromotoluene 8 <>< ; 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M22269-7 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1255.1) 10 12/08/01 AF n/a n/a GWX35 Run#2 WX1295.15 250 12/10/01 AF n/a n/a GWX36 MA-VPH List CAS No. Compound Result RL Units Q -................... ........................... 71A3-2 Benzene 22G( <;<< 50 ug/1 100-41-4 Ethylbenzene 19Q'> >>>' 50 ug/I ......:..:................. ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether 46a ' 1300 ug/I 91-20-3 Naphthalene 70 < 50 ug/I ........................... ........................... ........................... 108-88-3 Toluene 100( 1 50 ug/I m,p-XyleneQ ; 50 ug/I .....--................. ........................... ........................... 95A7-6 o-Xylene 2,5 1(J ; 50 ug/I C5-C8 Aliphatics(Unadj.) $64 500 ug/I ............... ........................... C9-C12 Aliphatics(Unadj.) 17 (3 1 5W ug/I C9-C10 Aromatics(Unadj.) 500 ug/I .. . ...:................ ........................... C5-C8 Aliphatics 1'II)<>'»> 500 ug/I C9-C12 Aliphatics 440 ;> 500 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... ......................... 615-59-8 2,5-Dibromotoluene 70 %; ; 70-130% ......................... ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 82%[ ;86 '; 70-130% ......................... ......................... (a)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M22269-7 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 1118745.1) 1 12/10/01 ANJ n/a n/a N:GI1937 Run#2 CAS No. Compound Result RL Units Q ................... ........................... 74-82-8 Methane 1;81 < 0.10 ug/I (a) Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M22269-7 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method .................................. Alkalinity, Total is11 ; 5.0 mg/1 1 12/11/01 BF EPA 310.1 Carbon Dioxide $Q<;:;:::; ;:: ;:;:<;: 5.0 nigh 1 12/11/01 MA SM18 45000O2D ..................._._.._..... .................................. ................................. Nitrogen, Nitrate a <4 T2;> >; < 0.11 mg/1 1 12/12/Ol MA EPA 353.2 ..............:.................. .................................. ................................. Nitrogen, Nitrate + Nitrite { ; 2; >` .. 0.10 mg/l 1 12/12/01 MA EPA 353.2 ...................:.............. ...................-............ ................................- Nitrogen, Nitrite «C(31 3 0.010 mg/1 1 12/05/01 MA EPA 354.1 ................ ................................. .................................. Sulfate 5 ? 5.0 mg/1 1 12/10/01 BF EPA 375.4 ................................ .................................. ................................. Sulfide 2: <> 2.0 mg/l 1 12/07/01 BF EPA 376.1 .................................. (a) Calculated as: (Nitrogen, Nitrate + Nitrite)-(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW06-MW-6 Lab Sample ID: M22269-8 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1244.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene 156:; 5.0 ug/I ..:........................ ........................... ........................... ........................... 100-41-4 Ethylbenzene ND; 5.0 ug/I ........................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether ? >;«< . 5.0 ug/I 91-20-3 Naphthalene T1< < ; ' S.0 ug/I I08-88-3 Toluene ND ; 5.0 ug/I ........................... ........................... m,p-Xylene ITD5.0 ug/I ........................ ........................... ........................... 95-47-6 o-Xylene NI?< `<' < 5.0 ug/I C5-C8 Aliphatics (Unadj.) ;;<>`;< 50 ug/I ........................ ........................... ........................... C9-C12 Aliphatics(Unadj.) 1ti1D 50 ug/I C9-C10 Aromatics(Unadj.) II) <> > 50 ug/I .......................... ........................... ........................... C5-C8 Aliphatics N.D >' .' 50 ug/I C9-C12 Aliphatics NIA;;;;::::;:;:;;:;;;:: 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits ..................-..... 615-59-8 2,5-Dibromotoluene 3�10 70-130% .................--.... ......................... ......................... 615-59-8 2,5-Dibromotoluene <73i<;`< 70-130% ..................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MWI I-MW-11 Lab Sample ID: M22269-9 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By� Prep Date Prep Batch Analytical Batch Run#1 WX1245.13 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 1rID< >; ; 5.0 ug/1 100-41-4 Ethylbenzene ND ; 5.0 ug/1 ........................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether IR) ; <> 5.0 ug/1 91-20-3 Naphthalene _<< >; 5.0 ug/I ....:...........:.......... ........................... ........................... 108-88-3 Toluene NID ; ;;>< ; 5.0 ug/I ........................ . ..................-....... ........................... m,p-Xylene :.,ND.::":::,*:::::::::::::::--.:::::::::> 5.0 ug/1 ........................... ........................... 95-47-6 o-Xylene NIA::: 5.0 ug/1 C5-C8 Aliphatics(Unadj.) ND' ; 50 ug/1 ... .................... ........................... ........................... C9-C12 Aliphatics(Unadj.) ND 50 ug/I C9-C10 Aromatics(Unadj.) 1tit » 50 ug/I CS-C8 Aliphatics IT)' <;`>< <;<; 50 ug/I ........................... ........................... ........................... C9-C12 Aliphatics << 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ........................ 615-59-8 2,5-Dibromotoluene 6 ; <' 70-130% 615-59-8 2,5-Dibromotoluene 7 % ii>` i 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW12-MW-12 Lab Sample ID: M22269-10 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1246.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 7143-2 Benzene ND 5.0 ug/1 100-41-4 Ethylbenzene iil 5.0 ug/l ....:...................... .... ........................... 1634-044 Methyl Tert Butyl Ether ND 5.0 ug/1 91-20-3 Naphthalene NI3`> > 5.0 ug/1 .......................... ..............I.......-- ...................—...... 108-88-3 Toluene ND ; ;; ; 5.0 ug/l m,p-Xylene .... >` >< 5.0 ug/1 9547-6 o-Xylene D'> 5.0 ug/1 C5-C8 Aliphatics(Unadj.) hII)''>; 50 ug/l C9-C12 Aliphatics (Unadj.). N . 50 ug/I C9-C10 Aromatics(Unadj.) D ; 50 ug/1 ... ................... ........................... ........................... C5-C8 Aliphatics ND< >>>s 50 ug/1 C9-C12 Aliphatics 1 <; 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene6 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene ?S% <' >i 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW13-MW-13 Lab Sample IUD: M22269-11 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1247.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 714 D3-2 Benzene 5.0 ug/I 100-41-4 Ethylbenzene . .... .....I....... 5.0 ug/I ................. ......:................... .........................1634-044 Methyl Tert Butyl Ether 5.0 ug/I ........................ 91-20-3 Naphthalene 5.0 ug/I ............... .......... 108-88-3 Toluene 5.0 ug/I m,p-Xylene . ................. ::.N J5.0 ug/I ............... ................. 9547-6 o-Xylene ............ 5.0 ug/I...... ........................... C5-C8 Aliphatics(Unadj.) 50 ug/I .............. C9-C12 Aliphatics (Unadj -'V ug/I .......................... 50 ug/l C9-CIO Aromatics(Unadj.) ..................... . . ................. ................ ..... C5-C8 Aliphatics JV ug/I . . . ............ C9-C12 Aliphatics ug/I ...................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene -130%.... 70 ............ ...................................... .............. . ............. 615-59-8 2,5-Dibromotoluene .1 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW13-MW-13 Lab Sample El): M22269-11 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a jProject: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 1118746.13 1 12/10/01 ANJ n/a n/a N:GI1937 Run#2 CAS No. Compound Result RL units Q ......................... 74-82-8 Methane 0.10 ug/I ........... (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M22269-11 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method Alkalinity, Total 0 < > 5.0 mg/l 1 12/11/01 BF EPA 310.1 Carbon Dioxide 21 s 5.0 mg/1 1 12/14/01 MA SM18 45000O2D Nitrogen, Nitrate a 0<< i 0.11 mg/1 1 12/12/01 MA EPA 353.2 Nitrogen, Nitrate + Nitrite b >« ;> 0.10 m /1 1 12/12/01 MA EPA 353.2 g g................................. Nitrogen, Nitrite C?1 s; > 0.010 mg/l 1 12/05/01 MA EPA 354.1 Sulfate27><; ><<<<> 5.0 mg/1 1 12/10/01 BF EPA 375.4 SulfideOa < 2.0 mg/1 1 12/07/01 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M22269-12 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1248.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 5.0 ug/1 D'`100-41-4 Ethylbenzene :.' «< > 5.0 ug/1 ........................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether ND 5.0 ug/1 91-20-3 Naphthalene N ; 5.0 ug/1 ........................... ........I.................. ........................... 108-88-3 Toluene Ili)> ;; 5.0 ug/1 m,p-Xylene itib> >> > 5.0 ug/1 95-47-6 o-Xylene ND > <= 5.0 ug/1 C5- C8 Aliphatics (Unadj.) N> 50 ug/I ..: .................... ........................... ........................... C9-C12 Aliphatics(Unadj.) ND' >; ;; 50 ug/1 C9-C10 Aromatics(Unadj.) 1ti(Yj' 50 ug/I :.. . ................. .......................... CS-C8 Aliphatics ND `>< ` 50 ug/1 C9- C 12 Aliphatics IT3> > _ < 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 70-130% 615-59-8 2,5-Dibromotoluene 76.. . 70-130% ........ ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M22269-12 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II18747.1) 1 12/10/01 ANJ n/a n/a N:GII937 Run#2 CAS No. Compound Result RL Units Q ................I.......... ........................... 74-82-8 Methane 1+TD ; 0.10 ug/1 ........................... (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M22269-12 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity, Total mg/1 1 12/11/01 BF EPA 310.1 Carbon Dioxide >< »> 5.0 mg/1 1 12/14/01 MA SM18 45000O2D Nitrogen, Nitrate a 6<a < '< i 0.51 mg/1 1 12./12/01 MA EPA 353.2 Nitrogen, Nitrate + Nitrite 0.50 m /1 5 12/12/01 MA EPA 353.2 .... ....... g ................................. .................................. Nitrogen, Nitrite C4QIa >; 0.010 mg/1 1 12/05/01 MA EPA 354.1 Sulfate 9>$ ' ;' 5.0 mg/1 1 12/10/Ol BF EPA 375.4 ................................. .................................. ................................. Sulfide 2 0<> >< 2.0 mg/l 1 12/07/01 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) I RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW15=MW-15 Lab Sample ID: M22269-13 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1249.D 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene NI) > >>>> 5.0 ug/1 100 41-4 Ethylbenzene ...... _> 5.0 ug/1 ........................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether TT ;> >> 5.0 ug/1 ........................... .........................- ........................... 91-20-3 Naphthalene t3 ; 5.0 ug/1 ........................... ........................... ........................... 108-88-3 Toluene ND 5.0 ug/1 ........................... ........................... ........................... ........................... m,P-Xylene NID > >>>> <s 5.0 ug/1 ........................... ........................... ........................... ug/I 95-47-6 o-Xylene NI) << ; 5.0 ..............:............. ........................... ........................... ........................... C5- C8 Aliphatics(Unadj.) NI3< ;>> >'»s 50 ug/1 ... ............_...... ...........I............... ........................... C9-C12 Aliphatics(Unadj.) ITD 50 ug/1 ........................ ........................... ........................... C9- C10 Aromatics(Unadj_) 1TD 50 ug/1 ........................... C5-C8 Aliphatics h+ITS ; 50 ug/1 C9- C12 Aliphatics NIA;;:;::;';::;;:::;::;:;: 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 77 70-130% ................:........ ......................... ......................... 615-59-8 2,5-Dibromotoluene .8%i 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW16-MW-16 Lab Sample ID: M22269-14 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1250.D 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene ND< <i`;< >; 5.0 ug/1 ........................... ........................... 100-41-4 Ethylbenzene li)<; ;« 5.0 ug/1 .............-...I........ ........................... ........................... 1634-04 4 Methyl Tert Butyl Ether hTD>`«= 5.0 ug/1 91-20-3 Naphthalene 17 < ;% < 5.0 ug/1 ........................... ........................... ........................... 108-88-3 Toluene ND < <; 5.0 ug/1 ........................... ........................... ........................... m,p-Xylene ItD< > >< » 5.0 ug/1 95-47-6 o-Xylene D <; 5.0 ug/1 CS-C8 Aliphatics(Unadj.) N 50 ug/1 :...:...................... ........................... ........................... C9-C12 Aliphatics (Unadj.) ND> << > 50 ug/1 C9-C10 Aromatics (Unadj.) t 50 ug/1 ... .............. ........................... ........................... CS-C8 Aliphatics ND < < 50 ug/1 C9-C12 Aliphatics NON; 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 7G`o ; 70-130% 615-59-8 2,5-Dibromotoluene 7G "'' ? 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW16D-MW-16D Lab Sample ID: M22269-15 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1256.1) 10 12/08/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ;1 (1>»>< 50 ug/1 100-41-4 Ethylbenzene h >; 50 ug/1 1634-04-4 Methyl Tert Butyl Ether l >> 50 ug/I 91-20-3 Naphthalene h11 <; ; 50 ug/1 108-88-3 Toluene NI); ; 50 ug/I m,p-Xylene ;AID<>` ;> > 50 ug/I 95-47-6 o-Xylene D 50 ug/1 C5- C8 Aliphatics(Unadj.) 1 $( i> 500 ug/1 C9-C12 Aliphatics(Unadj.) 2 < 500 ug/1 C9-C10 Aromatics(Unadj.) wXASS:::::;:;:;> > 500 ug/1 ............. ........................... ........................... C5-C8 Aliphatics 1<8: 11<> 500 ug/I C9- C 12 Aliphatics 1 IIl ; 500 ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene '75% ; « 70-130% 615-59-8 2,5-Dibromotoluene ?(i ': ' 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW17-MW-17 Lab Sample ID: M22269-16 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX125I.D 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ..................... 71-43-2 Benzene 5.0 ug/1 100-414 Ethylbenzene 1titD>' >`>; 5.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 1'I3 5.0 ug/I 91-20-3 Naphthalene N ;; 5.0 ug/I. 108-88-3 Toluene I3 ''; >' 5.0 ug/I m,p-Xylene N '`_ <>><< 5.0 ug/I ........................... 9547-6 o-Xylene 1I13 5.0 ug/I C5-C8 Aliphatics(Unadj.) t1D ; 50 ug/1 --....................... ........................... C9-C12 Aliphatics(Unadj.) N13;> `> 50 ug/I C9-C10 Aromatics (Unadj.) 1D'`' '< 50 ug/I C5-C8 Aliphatics '+ITS:;;:;::::;;;< 50 ug/I C9-C12 Aliphatics TS ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 7$ 0i< 70-130% ..............-......... ......................... 615-59-8 2,5-Dibromotoluene 78 << >`< 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FB Lab Sample ID: M22269-17 Date Sampled: 12/04/01 Matrix: AQ-Field Blank Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run##1 WX1252.1) 1 12/08/01 AF n/a n/a GWX35 Run#f2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene ND5.0 ug/I ........................... ........................... .......................... 100-41-4 Ethylbenzene 5.0 ug/I ......................... ........................... . ........................... 1634-04-4 Methyl Tert Butyl Ether N13;' 5.0 ug/I 91-20-3 Naphthalene 5.0 ug/I :.....................:.... ........................... ........................... 108-88-3 Toluene ND > ;5.0 ug/I ........................... ........................... ........................... m,p-Xylene Nb ;; is 5.0 ug/l .....................:..... ........................... ........................... 95-47-6 o-Xylene N . 5.0 ug/I C5-C8 Aliphatics(Unadj.) N. 50 ug/I C9-C12 Aliphatics(Unadj.) AID:;> ' 50 ug/I .............. ........................... C9-C10 Aromatics(Unadj.) D >> < ;; 50 ug/I ... . ................. ...............%.......... ........................... C5-C8 Aliphatics ND ><> > >> 50 ug/I C9-C 12 Aliphatics 1`I ;` "'< 50 ug/I CAS No. Surrogate Recoveries Run## 1 Run#/2 Limits 615-59-8 2,5-Dibromotoluene7% 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 78%> i 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TB Lab Sample ID: M22269-18 Date Sampled: 12/04/01 Matrix: AQ-Trip Blank Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1253.1) 1 12/08/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene NDi 5.0 ug/1 ........................... ........................... ........................... ........................... 100-414 Ethylbenzene ND >' 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND . 5.0 ug/1 --................ ........................... ........................... 91-20-3 Naphthalene N13` 5.0 ug/1 ........................... ...........I............... 108-88-3 Toluene NDs >> 5.0 ug/1 m,p-Xylene 15ID<<` 5.0 D ug/1 ........................... 95-47-6 o-Xylene 1+T > ;< ' 5.0 ug/1 C5-C8 Aliphatics (Unadj.) ICI ; . 50 ug/1 C9-C12 Aliphatics(Unadj.) NDi> ; 50 ug/1 C9-C10 Aromatics(Unadj.) 1ID ` 50 ug/1 .... ................... ........................... ........................... C5-C8 Aliphatics I�+I17 .* 50 ug/1 C9-C12 Aliphatics l > ><` 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 74a<' i 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene54 ; 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW01-MW-I Lab Sample ID: M22269-1A Date Sampled: 12/04/01 Matrix: AQ- Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Iron 21: p(?;i i ; IN ug/I 1 12/06/01 12/10/01 LMN sw846 6010B Sw846 3010A .............. ........................... RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW02A-MW-2A Lab Sample ID: M22269-3A Date Sampled: 12/04/01 Matrix: AQ-Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Iron 2$2 < i <> 100 ug/l 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3010A ............. . ..... RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M22269-5A Date Sampled: 12/04/01 Matrix: AQ-Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis. Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... Iron l{10 s< 100 ug/I 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3010A ...................-...... ........................... RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M22269-7A Date Sampled: 12/04/01 Matrix: AQ- Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... Iron SCi O' 100 ug/1 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M22269-1 I Date Sampled: 12/04/01 Matrix: AQ- Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:969250281140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method .......................... ........................... Iron �2 ;;` ' 100 ug/l 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3010A ........................... ........................... RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M22269-12A Date Sampled: 12/04/01 Matrix: AQ-Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... Iron C;lf� ; ; ' 100 ug/1 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3010A RL = Reporting Limit SAMPLE INFORMATION Aqueous usoil U Sediment U Other. Ld Satisfactory LJ Broken U Leaking: Aqueous N/A0 WM9s NOT LJpH>2 Leaking: Soil or N/A LiservedinmethanoiGr ml Methanol/g soil Sediment Samples reed in Methanol: LJ covering soil U not covering soil ❑1:1+/-25% Samples reed in air-tight container. ❑Other. REM B Received on Ice Reed at 4 Deg.C Woth reed at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID FB MW01-MW-1 MW01A-MW-1A Method for Target Analytes:MADEP VPH 98-1 Lab ID M22269-17 M22269-1 M22269-4 VPH Surrogate Standards Date Collected 12/4/01 1214/01 1214/01 PID:2,5-Dibromotoluene Date Received 12/5/01 12/5/01 12/5/01 FID:2,5-Dibromotoluene Date Analyzed 1218/01 1218/01 12/7/01 Dilution Factor 1 2 1 %Moisture(soil) Range/Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 50 1000 100 ND 50 Unadjusted C9-C12 Aliphatics(1) N/A ND 50 839 100 ND 50 Benzene C5-C8 ugA ND 5 42.3 10 ND 5 Ethylbenzene C9-C12 ugA ND 5 63.8 10 ND 5 Methyl-tert-butylether C5-C8 ugA ND 5 768 10 ND 5 Naphthalene WA ugA ND 5 ND 10 ND 5 Toluene C5-C8 ugA ND 5 140 10 ND 5 m-&p-Xylenes C9-C12 ugA ND 5 189 10 ND 5 o-Xylene C9-C12 ugA ND 5 85.1 10 ND 5 C5-C8 Aliphatic Hydrocarbons(1,2) N/A ugA ND 50 ND 100 ND 50 i C9-C12 Aliphatic Hydrocarbons(1,3) WA ugA ND 50 181 100 ND 50 C9-C10 Aromatic Hydrocarbons(1) N/A ugA ND 50 320 100 ND 50 PID Surrogate%Recovery 78 74 71 FID Surrogate%Recovery 77 73 71 Surrogate Acceptance Range L 70-130% 70-1 30% 70-130% 1-Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 2-05-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 3-C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CI0 Aromatic Hydrocarbons 4-A'J'qualifier indicates an estimated value CERTIFICATION Were all QA/QC procedures REQUIRED by the VPH Method followed? L4J Yes Li No-Details Attached Were all performance/acceptance standards for required QA/QC procedures achieved? Byes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.3? Q No ❑ Yes-Details Attatched Iattest under the pains and penalties of perjury that based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,a urate and wmplete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 PLE INFORMATION W Aqueous usoil u Sediment U Other. Satisfactory LJ Broken U Leaking: Aqueous LJNZA gs NOT pH>2 u Leaking: Sal or UNIA ed in Methanol or ml-Methanotig soil Sediment LJ Samples reed in Methanol: U covering soil LJ not covering sal ❑1:1+/_25% Samples reed in airtight container. ❑Other. Received on Ice Rec'd at 4 Deg.C o Opr reed at 3 deg C ANALYTICAL RESULTS for Ranges:MADEP VPH 98-1 Client'ID MW02-MW-2 MW02A-MW-2A MW03A-MW-3A for Target Analytes:MADEP VPH 98-1 Lab ID M22269-2 M22269-3 M22269-5 urrogate Standards Date Collected 12/4/01 1214/01 1214/01 D:2,5-Dibromotoluene Date Received 12/5/01 12/5101 12/5/01 D:2,5-Dibromotoluene Date Analyzed 12/8101 1217101 12/10/01 Dilution Factor 1 1 1 %Moisture(soil) e/Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q usted C5-C8 Aliphatics(1) N/A ND 50 218 50 ND 50 usted C9-C12 Aliphatics(1) N/A ND 50 ND 50 ND 50 sne C5-C8 ugA ND 5 14.1 5 ND 5 )enzene C9-C12 ugA ND 5 ND 5 ND 5 ll-tert-butylether C5-C8 ugA ND 5 214 5 50.6 5 thalene N/A ugA ND 5 ND 5 ND 5 ne C5-C8 ugA ND 5 ND 5 ND 5 Xylenes C9-C12 ugA ND 5 ND 5 ND 5 ne C9-C12 ugA ND 5 ND 5 ND 5 Aliphatic Hydrocarbons(1,2) WA ugA ND 50 ND 50 ND 50 2 Aliphatic Hydrocarbons(1,3) N/A ugA ND 50 ND 50 ND 50 0 Aromatic Hydrocarbons(1) N/A ug/I ND 50 ND 50 ND 50 urrogate%Recovery 74 73 84 urrogate%Recovery 73 74 81 ate Acceptance Range 70-130% 70-130% 70-130% rocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons qualifier indicates an estimated value TIFICATION I QA/QC procedures REQUIRED by the VPH Method followed? .r Yes No-Details Attached I perfonnance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attached y significant modifications made to the VPH method,as specified in Sect 11.37 (]No ❑ Yes-Details Attatched under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for rg the information,the material contained in this report is,to the best ofmy knowledge and belief,accurate and te. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 SAMPLE INFORMATION MOM W Aqueous usoil U Sediment LJOther U Satisfactory U Broken LJ Leaking: Aqueous LJ WA gs NOT LJpH>2 Leaking: Sal or NIA LJserved in Methanol or mL MethanoVg soil Sediment 10 Samples reed in Methanol: U covering soil LJ not covering soil ❑1:1+t-25% Samples reed in air-tight container Other Received on Ice Redd at 4 Deg.C .r Oth reed at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID MW04-MW4 MW05-MW-5 MW05-MW-5 Method for Target Analytes:MADEP VPH 98-1 Lab ID M22269-6 M22269-7 M22269-7 VPH Surrogate Standards Date Collected 12/4/01 12/4/01 12/4/01 PID:2,5-Dibromotoluene Date Received 12/5/01 12/5101 12/5/01 FID:2,5-Dibromotoluene Date Analyzed 12/10/01 12/8/01 12/10/01 Dilution Factor 1 10 250 %Moisture(soil) Rangerrarget Analyte Elution Range Units Result RL Q Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 50 56700 500 Unadjusted C9-C12 Aliphatics(1) N/A ND 50 17700 500 Benzene C5-C8 ugA ND 5 2260 50 Ethyibenzene C9-C12 ugA ND 5 1390 50 Methyl-tert-butylether C5-C8 ug/I 15.2 5 46900 1300 Naphthalene WA ugA ND 5 270 50 Toluene C5-C8 ugA ND 5 10000 50 m-&p-Xylenes C9-C12 ugA ND 5 5110 50 o-Xylene C9-C12 ugA ND 5 2580 50 C5-C8 Aliphatic Hydrocarbons(1,2) WA ugA ND 50 ND 500 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ugA ND 50 4400 500 C9-C10 Aromatic Hydrocarbons(1) N/A ugA ND 50 4220 500 PID Surrogate%Recovery 83 82 FID Surrogate%Recovery 80 77 82 Surrogate Acceptance Range 170-130% 70-130% 70-130% 1-Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range - 2-C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in fat range 3-C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons 4-A V qualifier indicates an estimated value CERTIFICATION Were all QAIQC procedures REQUIRED by the VPH Method followed? U4 Yes Li No-Details Attached Were all performance/acceptance standards for required QAIQC procedures achieved? I]Yes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.3? No Yes-Details Attatched I attest under the pains and penalties of per/ury that,based upon my inquiry of those individuals immediately responsible for 'obtaining the information,the material contained in this report is,to the best ofmy knowledge and belief, curate and complete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 u ILE INFORMATION Aqueous usoil Li Sediment U Other. Satisfactory Broken U Leaking: Aqueous NIA &NOT UpH>2 U Leaking: Soil or Ll N/A Userved in Methanol or mL MethanoVg soil Sediment U Samples rec d in Methanol: U covering soil LJ not covering soil ❑1:1+/-25% Lj Samples reed in air-tight container. ❑Other. LA Received on Ice U Rec'd at 4 Deg.C .r Oth reed at 3 deg C ANALYTICAL RESULTS for Ranges:MADEP VPH 98-1 Client ID MW06-MW-6 MW11-MW-11 MW12-MW-12 for Target Analytes:MADEP VPH 98-1 Lab ID M22269-8 M22269-9 M22269-10 nrogate Standards Date Collected 1214/01 1214101 12/4/01 Date Received 12/5/01 1215/01 1215/01 :2,5-Dibromotoluene Date Analyzed 1217/01 1217/01 12/7/01 Dilution Factor 1 1 1 %Moisture(soil) Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q sted C5-C8 Aliphatics(1) N/A 206 50 ND 50 ND 50 sted C9-C12 Aliphatics(1) N/A ND 50 ND 50 ND 50 e C5-C8 ugA 15.6 5 ND 5 ND 5 nzene C9-C12 ugA ND 5 ND 5 ND 5 test-butylether C5-C8 ugA 173 5 ND 5 ND 5 alene N/A ugA ND 5 ND 5 ND 5 C5•C8 ugA ND 5 ND 5 ND 5 Xylenes C9-C12 ug/I ND 5 ND 5 ND 5 le C9-C12 ugA ND 5 ND 5 ND 5 Aliphatic Hydrocarbons(1,2) N/A ugA ND 50 ND 50 ND 50 Aliphatic Hydrocarbons(1,3) N/A ugA ND 50 ND 50 ND 50 r Aromatic Hydrocarbons(1) N/A ugA ND 50 ND 50 ND 50 Togate%Recovery 73 75 75 Togate%Recovery 73 76 76 de Acceptance Range I 1 1 70-130% 170-130% 70-130 carbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range I Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range €2 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons lualifier indicates an estimated value IFICATION WOC procedures REQUIRED by the VPH Method followed? WYes U No-Details Attached )erformance/acceptance standards for required QA/QC procedures achieved? ❑r Yes ❑ No-Details Attached significant modifications made to the VPH method,as specified in Sect 11.37 No ❑ Yes-Details Attatched der the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for the information,the material contained in this report is,to the best of my knowledge and belief,a u2te and SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 SAMPLE INFORMATION W Aqueous Ll Soil U Sediment UOther. Satisfactory U Broken U Leaking: Aqueous U WA &NOT UpH>2 Leaking: Soil or U WA Userved in Methanol or mL Methanolig soil Sediment Samples reed in Methanol: covering soil not covering soil ❑7.1./-25% Samples reed in air-tight container. ❑Other. Received on Ice U Rec'd at 4 Deg.C .r Oth ec'd at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID MW13-MW-13 MW14-MW-14 MW15-MW-15 Method for Target Analytes:MADEP VPH 98-1 Lab ID M22269-11 M22269-12 M22269-13 VPH Surrogate Standards Date Collected 12/4/01 12/4/01 1214/01 PID:2,5-Dibromotoluene Date Received 12/5/01 12/5/01 12/5/01 FID:2,5-Dibromotoluene Date Analyzed 1217101 12/7/01 12/7/01 Dilution Factor 1 1 1 %Moisture(soil) Range/Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 50 ND 50 ND 50 Unadjusted C9-C12 Aliphatics(1) N/A NO 50 NO 50 ND 50 Benzene C5-C8 ugA ND 5 NO 5 ND 5 Ethylbenzene C9-C12 ug/I ND 5 NO 5 NO 5 Methyl-tert-butylether C5-C8 ugA NO 5 ND 5 NO 5 Naphthalene N/A ug/I ND 5 ND 5 NO 5 Toluene C5-C8 ugA ND 5 ND 5 ND 5 m-&p-Xylenes C9-C12 ugA ND 5 ND 5 NO 5 o-Xylene C9-C12 ugA ND 5 ND 5 ND 5 CSC8 Aliphatic Hydrocarbons(1,2) N/A ugA ND 50 ND 50 ND 50 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ugA ND 50 ND 50 NO 50 C9-C10 Aromatic Hydrocarbons(1) N/A ugA ND 50 ND 50 ND 50 PID Surrogate%Recovery 76 76 78 FID Surrogate%Recovery 76 75 77 Surrogate A7 ptance Range 70-130% 70-130% 70-130% 1-Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range 2-CS C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range 3-C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons 4-A V qualifier indicates an estimated value CERTIFICATION Were all QAIQC procedures REQUIRED by the VPH Method followed? W Yes U No-Details Attached Were all performance/acceptance standards for required CWQC procedures achieved? Q Yes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.37 O No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belie7ate and complete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tan DATE: 12/19/01 PLE INFORMATION LJ Aqueous usoil U Sediment U Other. Satisfactory LJ Broken Lj Leaking: Aqueous LJ WA �5 NOT pH>2 Leaking: Sal or WA served in Methanol or mL MethanoVg soil Sediment Samples rec'd in Methanol: covering soil not covering soil ❑1:1-A 25% LJ Samples reed in airtight container. ]Other Received on Ice Rec'd at 4 Deg.C Oth reed at 3 deg C ANALYTICAL RESULTS for Ranges:MADEP VPH 98-1 Client ID MW16-MW-16 MW16D-MW-16D MW17-MW-17 for Target Analytes:MADEP VPH 98-1 Lab ID M22269-14 M22269-15 M22269-16 urrogate Standards Date Collected 12/4/01 12/4/01 1214/01 D:2,5-Dibromotoluene Date Received 12/5/01 12/5/01 12/5/01 D:2,5-Dibromotoluene Date Analyzed 12/7/01 12/8/01 1217/01 Dilution Factor 1 10 1 %Moisture(soil) e/Target Analyte Elution Range Units I Result RL Q Result RL Q Result RL Q usted C5-C8 Aliphatics(1) WA ND 50 14800 500 ND 50 usted C9-C12 Aliphatics(1) WA ND 50 729 500 ND 50 ne C5-C8 ug/I ND 5 1410 50 ND 5 )enzene C9-C12 ugA ND 5 ND 50 ND 5 I-tert-butylether C5-C8 ug/I ND 5 11500 50 ND 5 alene N/A ugA ND 5 ND 50 ND 5 ne C5-C8 ug/I ND 5 ND 50 ND 5 Xylenes C9-C12 ugA ND 5 ND 50 ND 5 ne C9-C12 ug/I ND 5 ND 50 ND 5 Aliphatic Hydrocarbons(1,2) N/A ugA ND 50 1830 500 ND 50 2 Aliphatic Hydrocarbons(1,3) WA ugA ND 50 ND 500 ND 50 O Aromatic Hydrocarbons(1) WA ugA ND 50 555 500 ND 50 urrogate%Recovery 76 76 78 urrogate%Recovery 76 75 78 ate Acceptance Range I 1 1 70-130% 170-130% 170-130 mcarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 12 aliphatic Hydrocarbons exdude conc of Target Analytes eluting in that range AND concentration of C9-Cl0 Aromatic Hydrocarbons qualifier indicates an estimated value IFICATION I QA/QC procedures REQUIRED by the VPH Method followed? .r Yes Li No-Details Attached I peronnancelacceptance standards for required QA/QC procedures achieved? ❑Yes ❑ No-Details Attached y significant modifications made to the VPH method,as specified in Sect 11.3? No ❑ Yes-Details Attatched rider the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for g the information,the material contained in this report is,to the best of my knowledge and belief,accurate and e. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 SAMPLE INFORMATION Aqueous usoil ILI Sediment U Other. d Satisfactory U Broken LJ Leaking: Aqueous NIA &s NOT UpH>2 U Leaking: Soil or WA rved in Methanol or ImL Methanol/9 soil Sediment Samples reed in Methanol: U covering soil U not covering soil ❑1:1+l-25% Samples reed in airtight container. ❑Ogres Received on Ice U Reed at 4 Deg.C Woth reed at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID TB Method for Target Analytes:MADEP VPH 98-1 Lab ID M22269-18 VPH Surrogate Standards Date Collected 12/4/01 PID:2,5-Dibromotoluene Date Received 1215/01 FID:2,5-Dibromotoluene Date Analyzed 12/8/01 Dilution Factor 1 %Moisture(soil) Range/Target Analyte Elution Range Units Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 50 Unadjusted C9-C12 Aliphatics(1) N/A ND 50 Benzene C5-C8 ug/I ND 5 Ethylbenzene C9-C12 ugA ND 5 Methyl-tert-butylether C5-C8 ugA ND 5 Naphthalene N/A u9/1 ND 5 Toluene C5-C8 ugA ND 5 m-&p-Xylenes C9-C12 ugA ND 5 o-Xylene C9-C12 ug/I ND 5 C5-C8 Aliphatic Hydrocarbons(1,2) N/A ugA ND 50 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ugA ND 50 C9-C10 Aromatic Hydrocarbons(1) N/A ugA ND 50 PID Surrogate%Recovery 75 FID Surrogate%Recovery 74 Surrogate Acceptance Range 70-130% 1-Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range 2-C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 3-C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons 4-A'J'qualifier indicates an estimated value CERTIFICATION Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes U No-Details Attached Were all perfonnancelacceptance standards for required QA/QC procedures achieved? eyes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.3? eNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,acc to and complete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 ent By: GEOLOGIC SERVICES CORP; 976 568 9316; Dec-5-01 18:U9; rage i/e O: ACCUTEST MA A;: 15084817753 Geologic, • Tog �. �-L�nd-C r FMM �+ L i0 P6oe wee �Z1S�d j CI Ur9wd kwlew ❑Piw►se comnumt O Please R*W 0 Weease ReC11Cle c, t 000 Services CoryoraiM•15 DWOU l Avenue•t dsm,MA 01749•Phone(978)56BW40•Fax(976)M4M16 a t-cif AMx{RJQ$TJOa1h CHAIN OF CUSTODY 45 TECHnMOiCY CANMWFST• Bus.DWOOXF N AGiRLDOIROL6Ki AAA 0 F752 ACCIRSBT ODUM N. N TEL SAWS 1.SM •FAX:508481.77W .. FACILITY INFORMATION ANALYTICAL INFORMATION YATAIX CeQDES rnam 7.1 CL DW- DRIltKi c,1 p.1: CC1' 'T�SC�'iCCi Sf� �t �OCX�� Wj . NA PROJECT f ^ aw.OR6m Al 2 i 1tG .o war• w t�174 LL-130 �'14ck�rt�� STATE ZIP PROJECT 1 M ! 1,� ?y 8L• BWDGE --plc C-tkq •t. r� l'�•�tC•-m,:i. � -> a- oa < m °� T 7 G h 74 fz to - a uniao PHONE 0 FAx 1r_ c' SOL-OTtlMtR COLLECTION r `ti_ �� 80LJD ACCUTEST FIELD ID/POINT OF COLLECTION SMIPLE a DATE TllUJE sY: �' - v e.. e,J LA8 USE'ONLY c) `: yv% r;'tlj,)c a V., 1' ggL4 'r14m 2 .i co co Ln co !}ti,.._,(•� ilr;1., -S � lti'^'C� IF�.J'r� f -- Vol cr- o y;Y'; :.:.;•w: DATA TURNAROUND INFORMIATION %"` r "ra DATA DELIVERANLE NIFORMATN]N COUMENTSMENARKS ' '� $.. 1. `n �+14 DAYS STANDARD APPROVED BY- STANDARD s' 1, 1�;i1.i YCl b (r5L t Z w <� O 7 DAYS RUSH O OOMMERCIAL'B` SS td Sca*�1 . S 1 j�t�p H ~ "HOUR EMERGENCY O QJSKOEUY6RABLE w C OTHER O STATE FORMS U 14 DAY TURN ROUND HAROCOPY EMERGENCY OR RUSH 19 FAX O OTHER(SPECIFY) DATA UNLESS PFMV10U6LY APPROVED SAMPLE CUSTODY MUST BE DOCUIMNTED BELOW EACH TIME SAMPLES CHANGE POSSEBaON,INCLUDDIO COURIP.R DELI "•:... w �MELMYOUOMODY3"PLM; DAM TM or- aA7SttYa� IN�rtiO>rri , /� 2. C Z. S-ul�`�2U 2. f j, RELINOV6HfO0Y OATLTrAt 1lE wool: RmY1oY m oATf 11Ma0WwRN 3. 3. 4. 4, RELMOL"MM BY: OATS TI AICEIYlDE1h SEAL t /1/mllrm 1EMAE AM1muuMS OK KX 7E1 {MIE No MARLBOROUGH,MA 01752 ACCUTEST QUOTE r TEL:508-481-6200 • FAX 5OS 481-7753 CLIENT INFORMATIONJ — FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODS -so'eVi(P� cQ r-YD re),4rAC0 5+C, 1OY1 1p ��8 DW- WATER DRINKING NAME Ili --� I PROJECT NAME GW- GROUND I�;�li � zn c: 9( Q Z So ZR ww• WATER ADD ES LOCATION �^ WATER 6*1 I I 1/�14 0(7 q 1q C.a � (� -_� �soq---__..__--- -- SO- SOIL CITY, STATE ZIP PROJECT 0. 1 SL- SLUDGE MA OI- OIL SEND REPORT TO C. -p O LIQ- OTHER LIQUID PHONE# �'7�'`.SCoX- o�4h FAX# /7��S�D�- /.��p SOL-OTHER ACCUTEST COLLECTION x PRESERVATION ` SOLID SAMPLE# DATE TIME BY. $FIELD ID/POINT OF COLLECTION SAMPLED ° _125-1111lull I, v LAB USE ONLY --:l - -2 1 1349 rh tm -Z --3 rnWoM - mw-Z mW 010i ✓ ✓ �/ ✓ ✓ - rr - rnL z ✓ _ rn A 1 � � � ✓ - m s - ►mw-� m� ✓ ✓ —g - I'Y� - /yS L Z ✓ ✓ --le, _ 14 Z V ✓ 'mw - 3 &rY, Z DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMME-NhTSIREMA�R1KS O`7 DAYS RUSH 4 DAYS STANDARD APPROVED BY: STANDARD Cl COMMERCIAL"B" �'« �O SC'mlJler' �I4el b.IGS� IZ'y�0� O 48 HOUR EMERGENCY 0 DISK DELIVERABLE O OTHER O STATE FORMS LOc,- 3 C3 ' t3 6� 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX O OTHER(SPECIFY) • DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVE RELINQUISHED BY:SAMPLER: DATE TIM RECEIVED BY: RELINQUISHED BY: DATE TIME: RECEIVED BY: 1. 1 n.. U 1 (Wo 1. 2. _ lgzo 2. RELINO ISMED BY: DAT EIVED BY•TIME: RECEIVED RELINQUISHED BY: DAT Tl . RECEIVED BY. 3. /241 3. 4. 4. RELINQUISHED BY: DATE TIM RECEIVED BY: SEAL 1 PRESERVE YMEDRE APPLICABLE ON ICES TRC 5. 5. (O� Md ft Lv"w " CHAIN OF CUSTODY ACCUTESTJOBM �?a�-a�9 495 TECHNOLOGY CENTER WEST • BUILDING ONE MACCUTEST MARLBOROUGH,MA 01752 ACCUTEST QUOTE C. TEL:508-481-6200 • FAX:508-481-7753 Gc � CLIENT INFORMATION -�• FACILITY INFORMATION � ANALYTICA I ORMATION MATRIX COG E S DW• DRINKING _01OCQ C Ct WATER NAM ,,,,. J �''' PRWECT NAM GW- GROUND C � Lf� #' WATERC ; &C WW- WASTE ADDRESS LOCATION WATER �yn�S 5Y1 mA 6175q �Gl ��d1`1V 5 �a��9 SO- SOIL CITY, STATE ZIP PROJECT NO. an -S (11cf 01_ OILSLUDGE k fir,m 11 Z•a cn�a 1^ �rr�, I SEND REPORT TO: ` UO- OTHER r,1 LIQUIDPHONE# q 79, 4 Cr y - �{7�� FAX# � C S All y' SOL-OTHER COLLECTION Lc U.rA PRESERVATION SOLID ACCUTEST ¢ SAMPLE# FIELD ID/POINT OF COLLECTION SAMPLED ° O c DATE TIME BY: 2 $ s = i a - LAB USE ONLY Maaa6f�J — of N c fAw J J ✓ ✓ J —J W 15 YY1W ! 1 oq ✓ ✓' _J .. m w - I o mW 2 oqc oun --� - - i"7 r34 mW 2 1 ✓ r7 F� t rn!_� � ✓ DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTSIREMA�RKS 14 DAYS STANDARD APPROVED BY: STANDARD O 7 DAYS RUSH 0 COMMERCIAL"B" �- O 48 HOUR .EMERGENCY O DISK DELIVERABLE D OTHER O STATE FORMS l 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX O OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERY RELINQUISHED BY.SAMP .R: DAT TIME: RECEIVED BY. RELINQUISHED BY: DATE TIME: RECEIVED BY: h I�aj I. � F 2. 1 2. REIIN UISHE BY:. DATE E: RECEIVED B REUNQ (SHED BY: 0A ME: RECEIVED BY: 3. /L f 3. 4. 4. RELINQUISHED BY: DA ETIMLf. RECEIVED BY: SEAL# PRESERVE WHERE APPUCABLE ON IC TEMPERATURE / O S 1 n C j: Y2 } NewEng/and OS/17/02 ®ACCU MST echcalepOrt Equiva Services GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Accutest Job Number: M24976 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 76 O`S�Q►M 1lccpq�y - �y cp Test results contained within this data package meet the requirements /eza d of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications:MA(MA136) CT(PH-0109) NH(250293) RI(A-71) ME(MA136) USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 0 495 Tech Center West 0 Building 1 0 Marlborough,MA 01752■tel:508481-6200■ fax:508481-7753■htip://www.accutest.com Accutest Laboratories Sample Summary Equiva Services Job No: M24976 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Sample oeEtetk>>i Matrix Client .::...:..:...:.....::............................ Number Date Time By Received Code Type Sample ID ........................... M2 97G=1 0 1 s/0 /02 lo: H 00 G OS/ 2/0 02 A Ground Water ;.::........:.,.::.::.., :.;:.;;;:.;::.;;;;;;;:.;;>;:.;:.;:.;::.; MWp:1:A_MW::' A::>:; .....:>::>;:><:>`:>:>:>::>::<::>'::>':> Q ...... ........................... 7`: << O5/01/02 1 M" 9 1 .25 HG 4.....6 ... OS/02/ 2 0 A Ground Water M'5�02.'� > :. :>:>:>>:`:: ........................... as 4;; W.4.9 6-3 0:30 HG 05/02/02 AQ Ground Water 1t+I I31 =M1#-:3A:::>::;:>::>::>::»>:<:>:: ::>:: »>::<;>::>::>::>::>:::: : ........................... 4 OS/Ol/ 2 Mtil 9 0 15:3 2..:.:16 0 MLM 05/02/02 A Ground Water - »::::»::>::> ::<:::::<:»>»:....>::::::>::: Q IvZ tll:M t�::::I::;:.;;::.:;.;:.::.;:.>;.::. ........................... 2 0.7&5... 0 /5 Ol/02 13:30 MW os/a2ro2 . A Ground Water ;MW02:::MVO=2::: :>::>::>:>:>:::>:: <: :<::_»:>::::>:::::<: ;::>::::::>::::>:: Q ........................... l`9 05/01/02 14.4 2 .._6 .. O HG OS/02/02 A Ground W :.::><::>:::::>:»:: >::<>:::>:::::::>:: >»<::>::>::>::::>:::>;: Q ater M'Sy4 :11+17 ;: .;;:.;;:.;:.;:.:;.;:.;:.;;:;;.;:.::.;:.;:.; ........................... ........................... M2: _.:<: 5/01/02 16.35 MLM 05/02/02 A Ground Water MW 6:_: - ::>;:.....:....::::<:>:>:>:<<;::::»>; ........................... 9 . - >>'05/01/02 4: .: 2.. 76 8... 1 15 MW OS/02/02 A Ground Water : : :: .: '::« »::<::>:::>>:> ........................... ........................... >M24' 0 /0 13.40 MW 05/02/02 AQ Ground Water MW1It-M :Yfl::>:>::::>::::>><::>:: >::»:<::<:>::::>:<:>::......... ........................... T ...........:.:::::::::::: ::::. 9..6-1t3 O5/01/02 1. 1.40 MW OS/02/02 A Ground Wate ........................... M ..96-.11. O5/01/02 1 05/02/02 AQ Ground Water MW12:=MV :=:......>::>::>:>:>:::<::::>:_:::»:::::<::<: >::>::::>::::::::::::<:> 24 97G 1 OS/O1/02 13:45 MLM OS/02/02 A Ground Water MW1:3>:. W�13;::>:>:::>::>::> .... <:;:»;_::>::;>:<:>;;>::;::»::: - M2- < 976. .OS/ 1 2 0 /0 15:2 AQ Ground Water >MW14.11� ::: :»>::>::::::::>:>:>:::>:>:>:<:><::><:>::>: Accutest Laboratories Sample Summary (continued) Equiva Services Job No: M24976 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Sample ...>... Matrix Client. .. .... .......;. P Number Date Time By Received Code Type Sample ID ........................... 2497 -14 OS/O1/02 14:45 RA 5/ 2 ........ ........ 0 0 /02 A Ground Water MtK14I::' ........................... a1rf24 .7 9 6 15 os/ol/02 14:11 RA 0 /02 A Ground Water MWfI]:=lw1 >4I3:';>:>:«::<::>: Q ......:::::;..... ::::::::::::::::::::.;: ..... ......................................... ........................... M24 N— . 05/011 2 ...........:.::..::..:..: 0 09:35 HG 05/02/02 A Ground Water ::::..:<:>:>:>:>< <:;:<::>:<:::<::::::»::::> Q .;fir ;1.. .:1s ::::::::: :: ::: vI24. T 9 6 1? Os/0 1/02 09:3 0 MW Os/02/02 A Ground Water IWIW:1�i:IufW:>l:.>::>:::::>::>:::::>:>;:<:>::»::>::>:>:::>:::<:>::<::::<; ::«::: ................. Q .... .................::.;:6:::::::::::: .: ........................... _..... ... W64 7 = i 05/01/02 10:05 MW 05/02/02 AQ Ground Water > ........................... ........................... M24 .7 = .9 6 19 05/Ol/02 16:00 RAOS/02/02 A Ground Water MW 7:-: �: : is> >:::' :<::<:::::>««:::::>:: >::>:_:::«>:::«<:<::: Q ..................h W.::17..................:::::.:::::::: :.:::.:::::::: ........................... 6 20OS/O1/02 10:25 MW OS/02/02 A r G ound Water MWI :.::.. isgS:<::;::»:>:<:<:<«<:>:>>:«`: : ....> :,M24`7``'2 6✓ 1 OS/ 1 0 /02 11 1 .:.:...................::.;:::::.;;:; 5 MW OS/02/02 A Ground Water MW__1_SI):::MW=:1::.......:<:>:»<><:::>>: M 4976 22 05/01 02/ 16:4 0 HG OS/02/02 A Field Blank W : <::<:>::>«::>:>:»:> >«:>>: ::..... `2V : ::«::<:><: : :: <:.>::>76-2: 05/01102 16: Q Tn Blank Water TB ;::<< ::M24976=2 05/01/02 11:50 MLM 05/02/02 A Ground Water F' ' .'< '- M24: 762SOS/O1/02 14:00 M 9. LM 05/02/02 A Ground Water 2�i:04:>::::::<:>:>::>::::>::::>::>:::>:<:>::>:<:::>:::<:>::>:::<: 4 :6: 05/01/02 11:25 HG 05/02/02 AQ Groundwater Filtered :1tW02A Accutest Laboratories Sample Summary (continued) Equiva Services Job No: M24976 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Sample flltel< > « > ; ;»> Matrix Client ...................... .................................................... Number Date ltime By Received Code Type Sample ID ;. ....:.::..::.:::::.::::::::: :::: :: :: ivI2 976.3A 05/01/02 10:30 HG 05/02/02 A Groundwater Filtered tered :::MWQ3A::MW: A< > > >>' ;; .......................... Q .::::::.::::::::::.::.._:::::.::::::::::::::::::::::::::::::::::::::::::::: ........................... 9 A 05/01/02 1 5 30 MLM 0 02/02 A r w 5/ G ound ater Filtered M49CZ 05/01/02 14:40 HG 05/02/02 AQ Groundwater Filtered 0, .. 24. 768A 05/O1/02 14:15 MW M.....9.. 05/02/02 A Groundwater Filtered :::MW =. «:::::_»>:<:>::::>:::«<:::>:::::>::::-:: ........................... Q .;;��;: '...I......... ::::.:;::::.:::>:<.>::<:<:::>:::<.................:: :<:: .. ......... ...... . ZI ::: 1 2 M .....t'�-.IP05/0 /0 13:45 MLM 05/02/02 AQ Groundwater Filtered :::M1�V13: :1 :::>...........::>::>::::>::»::>:----...... :::<::::.. avi4:. :: 9 6 3�05/Ol/ 2 1 2 0 5. 0RA 0 / 202 A :...........::.:..:.:...;.......::..;:..:: :.::: i.... 5 0 / Groundwater Filtered :MViW * ::;:<:<_>:::::»::::>;::<::::::<:>::>::>::>::>::>::»>::>:::;>:::>;>:;:> Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MWOlA-MW-IA Lab Sample ID: M24976-1 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13195.1) 1 05/12/02* AMY n/a n/a GMN371 Run#2 MA-VPH List CAS No. Compound Result RL Units Q .................. 5.0 ug/I 71-43-2 Benzene ........................ ..................... ................................................ ........................... 100-414 Ethylbenzene ug/I ..... ................... ...................... . ............. 1634-044 . ....... . ug/I Methyl Tert Butyl Ether ......... .... .............................................. ..................... 91-20-3 Naphthalene ... ........... ug/I ..................... ................I....-- ..................... 108-88-3 Toluene . .........................-....... 5.0 ug/I .......................... m,p-Xylene . .. 5.0 ug/I ................--.-.- ...........I............. ......... ... 9547-6 o-Xylene 5.0 ug/I . ............................... C5-C8 Aliphatics (Unadj.) .... N J5 AV ug/I ...... 50 ug/I C9-C12 Aliphatics (Unadj.) ......................... ................... ......... . ...... 50 , ug/l C9-CIO Aromatics(Unadj.) ..................-............. ........... ........................... ...... .... . .......... . .. .. ...... ..... ...... C5-C8 Aliphatics 50 ug/I ..........- ug/I C9-C12 Aliphatics :.ND:. .. JV ........... ........................... CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene ................ ..... 70-130%...................... .......... 615-59-8 2,5-Dibromotoluene 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of.1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M24976-2 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 lyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13196.1) 1 05/12/02 AMY n/a n/a GMN371 Run#2 MN13214.1) 2 05/13/02 AMY n/a n/a GMN372 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene I ; < 5.0 ug/l 100-41-4 Ethylbenzene 5.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 27flQ 10 ug/l ...........:............... ........................... 91-20-3 Naphthalene if 5.0 ug/l 108-88-3 Toluene ND.<; >': 5.0 ug/l m,p-Xylene 1 (? 5.0 ug/l 95-47-6 o-Xylene NIA <s > < ;; 5.0 ug/l C5-C8 Aliphatics(Unadj.) 7 (<a<< 100 ug/l C9-C12 Aliphatics(Unadj.) IIfi 50 ug/l C9- C10 Aromatics (Unadj.) 8 << ; < > 50 ug/l C5-C8 Aliphatics NIA ;;<`> 50 ug/l C9-C12 Aliphatics N1 >; <;<50 ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluenexoi`i 9 70-130% 615-59-8 2 5-Dibromotoluene $f 's ><>» :, »:><_ > > - > 9'0lfl8.°�0 70 130% (a)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M24976-2 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW946 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II21140.1) 1 05/14/02 ANJ n/a n/a N:GII1034 Run#2 a 1121141.1) 5 05/14/02 ANJ n/a n/a N:GII1034 CAS No. Compound Result RL Units Q 74-82-8 Methane2' " = 0.10 ug/l Carbon Dioxide 620..01. 500 ug/l (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 (b)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M24976-2 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method Alkalinity, Total s8 : _> 5.0 mg/l 1 05/10/02 OP EPA 310.1 ................... ........... Nitrogen, Nitrate a <:< <<< << 0.11 m /l 1 05/07/02 sx EPA 353.2 g g Nitrogen, Nitrate + Nitrite iS "``>> > >_0.10 mg/1 1 05/07/02 sx EPA 353.2 Nitrogen, Nitrite tl 01 0.010 mg/l 1 05/02/02 xBm EPA 354.1 ...........................-..... ................................. .................................. Sulfate 3 2 ; 5.0 mg/l 1 05/03/02 OP EPA 375.4 Sulfide ... 2.0 mg/l 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)-(Nitrogen, Nitrite) . RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M24976-3 Date Sampled: 05/01/02 j Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13197.1) 1 05/12/02 AMY n/a n/a GMN371 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene 1D ` > 5.0 ug/I 100-41-4 Ethylbenzene 1 > >s5.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 1IZ 5.0 ug/I 91-20-3 Naphthalene Nib ; =' 5.0 ug/I 108-88-3 Toluene ND5.0 ug/I m,p-Xylene N « <5.0 ug/I 95-47-6 o-Xylene 1'I 5.0 ug/I C5-C8 Aliphatics(Unadj.) l '` 50 ug/I C9-C12 Aliphatics(Unadj.) N3 50 ug/I C9-C10 Aromatics(Unadj.) li > >`'` 50 ug/I C5-C8 Aliphatics D'> <>>`` 50 ug/I C9-C12 Aliphatics '>. 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene '7 %> .. 70-130% ......................... 615-59-8 2,5-Dibromotoluene }4 '>< 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M24976-3 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a I121142.1) 1 05/14/02 ANJ n/a n/a N:GII1034 Run#2 CAS No. Compound Result RL Units Q <»74-82-8 Methane N?s > <>> 0.10 ug/l Carbon Dioxide 222(; »<;> 100 ug/l (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M24976-3 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. Alkalinity, Total S Q <> 5.0 mg/l 1 05/10/02 OP EPA 310.1 Nitrogen, Nitrate a 0.11 mg/1 1 05/07/02 sK EPA 353.2 Nitrogen, Nitrate + Nitrite 0.10 mg/1 1 05/07/02 SK EPA 353.2 Nitrogen, Nitrite ( OIt `: 0.010 mg/1 1 05/02/02 BBM EPA 354.1 Sulfate 5.0 mg/I 1 05/03/02 op EPA 375.4 ......:.......................... Sulfide G2f1 _ 2.0 mg/1 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MWOI-MW-1 Lab Sample ID: M24976-4 Date Sampled: 05/01/02 Matrix: AQ-Ground Water . Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13210.1) 1 05/13/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 1 <>>> ><5.0 ug/l 100-41-4 Ethylbenzene 2 Q ` 5.0 ug/l ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether .637 5.0 ug/l 91-20-3 Naphthalene IIJi5.0 ug/l ........................... ........................... 108-88-3 Toluene 8 f >i i 5.0 ug/l m,p-Xylene :-6 { 5.0 ug/1 ........................... ........................... 95-47-6 o-Xylene ;22 9< . 5.0 ug/l C5-C8 Aliphatics (Unadj.) 725 50 ug/l .:.. . ................ ........ C9-C12 Aliphatic.(Unadj.) 196' ' <; 50 ug/l C9-C10 Aromatics(Unadj.) 902;>> ' ' 50 ug/l ..... ..--............ ........................... ........................... C5-C8 Aliphatic. ND< '" _ 50 ug/l... C9-C12 Aliphatics `:' 'S0 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $ % 70-130% ........................: ......................... 615-59-8 2,5-Dibromotoluene 9(9 <>> <' « 70-130% .......................- ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOI-MW-1 Lab Sample ID: M24976-4 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II21143.1) 1 05/14/02 ANJ n/a n/a N:GII1034 Run#2 a II21144.1) 5 05/14/02 ANJ n/a n/a N:GII1034 CAS No. Compound Result RL Units Q 74-82-8 Methane Is>52; 0.10 ug/I Carbon Dioxide �42Q b ><< 500 ug/1 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 (b)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOI-MW-1 Lab Sample ID: M24976-4 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method .................................. Alkalinity,Total Q 5.0 mg/l 1 05/10/02 op EPA 310.1 Nitrogen, Nitrate a ...................; 0.11 mg/l 1 05/07/02 Sx EPA 353.2 Nitrogen, Nitrate + Nitrite f 0.10 mg/l 1 05/07/02 Sx EPA 353.2 Nitrogen, Nitrite fl t) ';;> > 0.010 mg/l 1 05/02/02 HBM EPA 354.1 Sulfate I2 <j; < '' " 5.0 mg/1 1 05/03/02 OP EPA 375.4 SulfideX,2(1; 2.0 mg/1 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)-(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02-MW-2 Lab Sample ID: M24976-5 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA I File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13215.1) 1 05/13/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND = 5.0 ug/l 100-41-4 Ethylbenzene I ➢< 5.0 ug/l ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether <4< 5.0 ug/l 91-20-3 Naphthalene << < ..S.0 ug/l .:..:...:.................. 108-88-3 Toluene l il) 5.0 ug/l m,p-Xylene 1 T 5.0 ug/l 95-47-6 o-Xylene NI)<a ;%"5.0 ug/l C5-C8 Aliphatics(Unadj.) Nl 50 ug/l C9-C12 Aliphatics(Unadj.) 50 ug/l C9-C10 Aromatics(Unadj.) 11 ` `_> 50 ug/l C5-C8 Aliphatics T) < >> 50 ug/l C9-C12 Aliphatics `N i <` 50 ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene `1 70-130% .......:................. ................... 615-59-8 2,5-Dibromotoluene It)8° 70-130% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ED: MW05-MW-5 Lab Sample ID: M24976-6 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Ba tch Analytical Batch Run#1 MN13234.1) 50 05/14/02 AMY n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene I52(3250 ug/I 100414 Ethylbenzene 2dt(3' >s> 250 ug/I 1634-04-4 Methyl Tert Butyl Ether, 3 <. ` 250 ug/I 91-20-3 Naphthalene {tT < ; 250 ug/I 108-88-3 Toluene Itl4( > ` 250 ug/I 711 m,p-Xylene 250 ug/I 95-47-6 o-Xylene 383(3 250. ug/I C5-C8 Aliphatics(Unadj.) 4$ 2500 ug/I C9-C12 Aliphatics (Unadj.) ? $ 2500 ug/I C9-C10 Aromatics(Unadj.) 3 <> <` 2500 ug/I X.77C5-C8 Aliphatics NI) >> '' 2500 ug/I C9-C12 Aliphatics I1 <<>' 2500 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 9 70-130% ......................... 615-59-8 2,5-Dibromotoluene 9.9 > <<... 70-130% ..................... . ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M24976-6 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II21145.1) 1 05/14/02 ANJ n/a n/a N:GII1034 Run#2 a I121146.1) 5 05/14/02 ANJ n/a n/a N:GII1034 CAS No. Compound Result RL Units Q 74-82-8 Methane 9r61< < 0.10 ug/1 Carbon Dioxide >38i5( l<� ::'500 ug/1 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 (b)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of'Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M24976-6 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ...................I............. Alkalinity,Total pf#' '>> 5.0 mg/1 1 05/10/02 op EPA 310.1 Nitrogen, Nitrate a 0.11 mg/1 1 05/07/02 SK EPA 353.2 ................................. .................................. ................................ Nitrogen, Nitrate + Nitrite 4 I#? 0.10 mg/l 1 05/07/02 SK EPA 353.2 Nitrogen, Nitrite OIQ `'=`";' 0.010 mg/1 1 05/02/02 HBM EPA 354.1 .................................. ................................. .................................. Sulfate ! 5CA .0 mg/l 1 05/03/02 op EPA 375.4 Sulfide 2 0 ><>`'2.0 mg/l 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite) -(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW06-MW-6 Lab Sample ID: M24976-7 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA I I File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13217.1) 1 05/13/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene # 5.0 ug/1 100-414 Ethylbenzene $3 >>.. S.0 ug/1 1634-044 Methyl Tert Butyl Ether >1 ( `> 5.0 ug/1 91-20-3 Naphthalene _ >` ">` 5.0 ug/1 108-88-3 Toluene NI) < 5.0 ug/1 m,p-Xylene 12> » < > 5.0 ug/1 ........................... ........................... 95-47-6 o-Xylene ��r;l? 5.0 ug/1 ......:.........:.......... ........................... C5-C8 Aliphatics(Unadj.) 11 () ' 50 ug/1 .................... ........................... C9-C12 Aliphatics(Unadj.) 279 50 ug/1 C9-C10 Aromatics(Unadj.) 2'ZG >> 50 ug/1 ..:.. .................. ........................... C5-C8 Aliphatics Nib:;::::::;::::;::::':;::;;:: 50 ug/1 C9-C12 AliphaticsTI` >> <„ 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene fl9%` 70-130% ...:..................... ......................... 615-59-8 2,5-Dibromotoluene I.2. :.: ; 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW09-MW-9 Lab Sample ID: M24976-8 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13235.1) 50 05/14/02 AMY n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene 62Q: ' 250 ug/I ....I...................... ........................... 100-414 Ethylbenzene 2! Q ;> '> 250 ug/1 ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether 68 ' `ii< 250 ug/1 ........................... ........................... 91-20-3 Naphthalene $ 250 ug/1 ........................... ........................... 108-88-3 Toluene I: 84q: < > 250 ug/1 m,p-Xylene 11 p : > >250 ug/l ........................... ........................... 95-47-6 o-Xylene 6fJG(#: < : 250 ug/l C5-C8 Aliphatics(Unadj.) 5 :>>`' 25W ug/1 .. .................... ........................... C9-C12 Aliphatics(Unadj.) 9 Q('' ? 25M ug/1 .. : .................. ........................... C9-C10 Aromatics (Unadj.) 15G4 < <' 2500 ug/l .._.......... ........................... C5-C8-Aliphatics9t1`;<` >>„2500 ug/l ........................... ........................... C9-C12 Aliphatics 23 >;>< ;> 2500 ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 95%:<> 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene )>> 3 70-130% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 01 i Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW09-MW-9 Lab Sample ID: M24976-8 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW946 8015 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a I121147.D 1 05/14/02 ANJ n/a n/a N:GII1034 Run#2 a II21148.1) 5 05/14/02 ANJ n/a n/a N:GII1034 CAS No. Compound Result RL Units Q 74-82-8 Methane '3 <> 0.10 ug/1 .:..:...................... Carbon Dioxide 49 > 500 ug/1 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 (b)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW09-MW-9 Lab Sample ID: M24976-8 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 lyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method Alkalinity, Total Gt1Z 5.0 mg/1 1 05/10/02 op EPA 310.1 Nitrogen, Nitrate o f " 0.11 mg/l 1 05/07/02 Sx EPA 353.2 xx Nitrogen, Nitrate + Nitrite n><> 0.10 mg/1 1 05/07/02 SK EPA 353.2 Nitrogen, Nitrite If 0.010 mg/1 1 05/02/02 HBM EPA 354.1 Sulfate 6 Q i 5.0 mg/l 1 05/03/02 op EPA 375.4 ...... ...... Sulfide` 2.0 mg/1 1 05/07/02 BF EPA 376.1 ......:..................... (a)Calculated as: (Nitrogen, Nitrate + Nitrite) -(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis P PO � age 1 of 1 Client Sample ID: MW10-MW-10 Lab Sample ID: M24976-9 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 11401yannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13219.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND< <« 5.0 ug/I 100414 Ethylbenzene N ; 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 1'+T ? < < 5.0 ug/1 91-20-3 Naphthalene N 5.0 ug/I 108-88-3 Toluene ID ; < <>s 5.0 ug/1 m,p-Xylene lD 5.0 ug/1 9547-6 o-Xylene 1'1D ; ; 5.0 ug/1 C5-C8 Aliphatics(Unadj.) >N1 50 ug/1 C9-C12 Aliphatics(Unadj.) ND 50 ug/1 C9-C10 Aromatics(Unadj.) 1tD 50 ug/1 C5-C8 Aliphatics 1+II3 ;< i< 50 ug/I C9-C12 Aliphatics NIA::....; > 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ..................... 615-59-8 2,5-Dibromotoluene $20 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene IN-... 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWI l-MW-11 Lab Sample ID: M24976-10 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13220.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene ll)>; ;; 5.0 ug/1 100-41-4 Ethylbenzene `>> i> 5.0 ug/1 ........................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether 1Q 5.0 ug/1 91-20-3 Naphthalene13< ' < ' 5.0 ug/1 .....::.................... ........................... ........................... 108-88-3 Toluene NI) 5.0 ug/1 m,p-Xylene ICI)> ` 5.0 ug/1 95-47-6 o-Xylene ND>> 5.0 ug/I C5-C8 Aliphatics(Unadj.) 922 50 ug/1 .:...................... ........................... ........................... C9-C12 Aliphatics(Unadj.) I 50 ug/1 C9-C10 Aromatics(Unadj.) ;> << 50 ug/1 ........... ...: .................... ........................... ........... ..... C5-C8 Aliphatics ND < ; 50 ug/1 C9-C12 Aliphatics NI3 >> `><> 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 10¢% >;>; 70-130% ......:.................: ......................... ......................... 615-59-8 2,5-Dibromotoluene 1t77°j ;; ; 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW12-MW-12 Lab Sample ID: M24976-11 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File E[) DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13221.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units ......................... 71-43-2 Benzene 5.0 ug/I .......... .. ............- ............ ...........- ...................... 100-41-4 Ethylbenzene ug/I .............. ............. .......... .......... - - ---- ........................... . .... ......... 1634-04-4 Methyl Tert Butyl Ether 5.0 ug/I .... ......- ............................................ . .............— 91-20-3 Naphthalene 5.0 ug/I . .............. ........... ...... 108-88-3 Toluene - 5.0 ug/I ...................................... m,p-Xylene ug/I ................... ...... ..... . .................. 95-47-6 o-Xylene -..:ND:-.:.................� 5.0 ug/I. . ................ ............... 50 ug/I C5-C8 Aliphatics(Unadj.) ...... ........ ...........-.1. ........................ ....................-- .............- ............ C9-C12 Aliphatics (Unadj.) 50 ug/I C9-CIO Aromatics(Unadj.) 50.-... ... .......... ug/I 1.. . ................. ............. ......................... ............C5-C8 Aliphatics JV 50 ug/I ............ ................ ............- ............... C9-C12 Aliphatics, ...ND. 50 ug/I .......................... ........................ CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 42 615-59-8 2,5-Dibromotoluene -130% 70 . ........... ................ ............. .......... 615-59-8 2,5-Dibromotoluene :.*.8 70-130% ........... -...... ........... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of i Client Sample ID: MW13-MW-13 Lab Sample ID: M24976-12 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13222.D 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......................... 71-43-2 Benzene ................. ug/I 100-41-4 Ethylbenzene : tD 5.0 ug/I ....:..................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether D. 5.0 ug/I ........:.................. ........................... 91-20-3 Naphthalene 1 5.0 ug/I ........................... ........................... ........................... 108-88-3 Toluene NI); ; 5.0 ug/1 m,p-XylenetitD'>> `> 5.0 ug/1 ........................... ........................... 9547-6 o-Xylene I) 5.0 ug/l CS-C8 Aliphatics(Unadj.) li `>'' 50 ug/1 ......... ................ ........................... ........................... C9- C12 Aliphatics(Unadj.) lID 50 ug/I C9- C10 Aromatics (Unadj.) :-N : :> : 50 ug/I .... . ................. ........................... ........................... C5-C8 Aliphatics ND 50 ug/I C9-C12 Aliphatics 1TD » :50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits ............... 615-59-8 2,5-Dibromotoluene l %a z '':. 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene IbB%4<; 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M24976-12 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 1I21149.1) 1 05/14/02 ANJ n/a n/a N:GI11034 Run#2 CAS No. Compound Result RL Units Q ........................... 74-82-8 Methane NI? 0.10 ug/1 Carbon Dioxide 4$4 >>' `..` `. 100 ug/1 (a) Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M24976-12 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity,Total $ 5.0 mg/l 1 05/10/02 op EPA 310.1 Nitrogen, Nitrate ak9 0.11 mg/1 1 05/07/02 SK EPA 353.2 ................................. .................................. ................................. Nitrogen, Nitrate + Nitrite :9 < >`>>i >> 0.10 mg/1 1 05/07/02 sx EPA 353.2 Nitrogen, Nitrite # #1Q < < 0.010 mg/1 1 05/02/02 HBM EPA 354.1 ..................:............... ................................. Sulfate 59 5.0 mg/1 1 05/03/02 OP EPA 375.4 .................................. ................................. .................................. Sulfide 2 >;' ; <<;2.0 mg/l 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)-(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M24976-13 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch . Run#1 MN13223.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene ND < s5.0 ug/1 100414 Ethylbenzene ND> > 5.0 ug/I ...:....................... 1634-04-4 Methyl Tert Butyl Ether NI? ;< 5.0 ug/1 91-20-3 Naphthalene 5.0 ug/1 108-88-3 Toluene ND' ; 5.0 ug/1 m,p-Xylene ND > > < 5.0 ug/1 ........................... ........................... 9547-6 o-Xylene ND <> ; 5.0 ug/1 CS- C8 Aliphatics (Unadj.) <. 50 ug/1 ........................... C9-C 12 Aliphatics(Unadj.) NI) '' i 50 ug/1 C9-CIO Aromatics(Unadj.) l `...`(' ' 50 ug/1 ........................... C5- C8 Aliphatics N 50 ug/1 C9- C12 Aliphatics NL7[ 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ............... 615-59-8 2,5-Dibromotoluene $ 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene 9E1 ; 70-130% ......................... .......................- ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M24976-13 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II21150.1) 1 05/14/02 ANJ n/a n/a N:GII1034 Run#2 CAS No. Compound Result RL Units Q ........................... 74-82-8 Methane 1t ; 0.10 ug/1 Carbon Dioxide 90I 100 ug/1 (a) Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client.Sample ID: MW14-MW-14 Lab Sample ID: M24976-13 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL units DF Analyzed By Method ................................. .................................. Alkalinity,Total r £ " 5.0 mg/l 1 05/10/02 op EPA 310.1 Nitrogen, Nitrate a ... 0.51 /l 1 05/07/02 Sx EPA 353.2 Nitrogen, Nitrate + Nitrite 5 < 0.50 mg/l 5 05/07/02 Sx EPA 353.2 Nitrogen, Nitrite (`OIQ 0.010 mg/l 1 05/02/02 HBM EPA 354.1 Sulfate i <`>> 5.0 mg/1 1 05/03/02 op EPA 375.4 .................................. Sulfide21<> ``'''' 2.0 mg/1 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)-.(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14I-MW-14I Lab Sample ID: M24976-14 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GAB543.1) 1 05/03/02 AF n/a n/a GAB15 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene )' _>'' 5.0 ug/1 100-41-4 Ethylbenzene 11 5.0 ug/I ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether L> < ' 5.0 ug/1 91-20-3 Naphthalene 1 >> 5.0 ug/l 108-88-3 Toluene N ) > 5.0 ug/1 m,p-Xylene 1 ><>> 5.0 ug/1 ........................... ........................... 95-47-6 o-Xylene NZ <> 5.0 ug/1 C5-C8 Aliphatics(Unadj.) _ 50 ug/1 :.......................... ........................... C9-C12 Aliphatics (Unadj.) ID < »< 50 ug/1 C9-C10 Aromatics (Unadj.) 1 < 50 ug/1 C5-C8 Aliphatics I1>< 50 ug/1 C9-C12 Aliphatics N 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $8 70-130% 615-59-8 2,5-Dibromotoluene 8i 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14D-MW-14D Lab Sample ID: M24976-15 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GAB544.1) 1 05/03/02 AF n/a n/a GAB15 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene I1D <> 5.0 ug/1 100-41-4 Ethylbenzene 1tD5.0 ug/1 ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether N <>_ 5.0 ug/1 91-20-3 Naphthalene > > ' <> < 5.0 ug/1 :.......................... ........................... 108-88-3 Toluene AID':::' '< 5.0 ug/1 m,p-Xylene l'tn >> > 5.0 ug/1 ..................-....... 95-47-6 o-Xylene I+II5.0 ug/1 C5-C8 Aliphatics(Unadj.) IT 50 ug/1 C9-C12 Aliphatics(Unadj.) IrLD> <>;; 50 ug/1 C9-C10 Aromatics(Unadj.) li << 50 ug/1 C5-C8 Aliphatics NZ� > < �<> 50 ugll C9-C 12 Aliphatics NIA '50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 9"aalo : : 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene 9 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW15-MW-15 Lab Sample ID: M24976-16 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis,.MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13224.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... . 7143-2 Benzene IrTD 5.0 ug/l 100-414 Ethylbenzenei => > > 5.0 ug/l .......................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether AID: 5.0 ug/l ........ ......-........ ........................... 91-20-3 Naphthalene Imo':::; ;;; 5.0 ug/l ........................... ........................... 108-88-3 Toluene 1rID5.0 ug/l ........................... ........................... m,p-XyleneIl «>> > 5.0 ug/l 95-47-6 o-Xylene NI ' > 5.0 ug/1 CS-C8 Aliphatics(Unadj.) IIt ; 50 ug/l ........................... C9-C12 Aliphatics(Unadj.) I1Dii 50 ug/1 C9-C10 Aromatics(Unadj.) 50 ug/1 C5-C8 Aliphatics N 50 ug/l C9-C12 Aliphatics "-. 50 ug/1 --...---........... CAS No. Surrogate Recoveries Run#1 Run#2 Limits ........................ 615-59-8 2,5-Dibromotoluene ;7 ; . 70-130% 615-59-8 2,5-Dibromotoluene $3' 70-130% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW16-MW-16 Lab Sample ID: M24976-17 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File EI) DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13225.1) 1 05/14/02 AMY nia n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene ND5.0 ug/I .......... ............. 100-41-4 Ethylbenzene ........ ug/l ................... ................... 1634-04-4 Methyl Tert Butyl Ether 5.0 ug/l .. ....... ....... . ...................... 91-20-3 Naphthalene J.V ug/I .. .................. .......................... .......... ....... .. . ...... 108-88-3 Toluene ........ 5.0 ug/1 ................... m,p-Xylene ND*.*':::*::':":::*::::'::::**::::::*::: 5 A ug/l ..... ..... ............................... ........................... .......... 9547-6 o-Xylene 5.0 ug/I .... ........ C5-C8 Aliphatics(Unadj.) .. 'X ......... 50 ug/l .. ....... ....................... C9-C12 Aliphatics(Unadj.) .. ug/I ......... ........... CA ..........­'...­.'.'... C9-CIO Aromatics (Unadj.) .. ug/I . ....... CA ........................ C5-C8 Aliphatics .N ug/I .......... ------ .......................... C9-C12 Aliphatics 50 ug/l ........... ................... CAS No. Surrogate Recoveries Run#I Run#'2 Limits ......................... .......... 615-59-8 2,5-Dibromotoluene -130% ....................... 70 ............. X 615-59-8 2,5-Dibromotoluene :155% 70-130% .....I.................._...................... ........... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound I Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW16D-MW-16D Lab Sample ID: M24976-18 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13232.D 1 05/14/02 AMY n/a n/a GMN373 Run#2 QR14492.1) 5 05/15/02 AA n/a n/a GQR663 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 4I4 =i; < 5.0 ug/1 100-41-4 Ethylbenzene " 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 4Z8a 25 ug/1 91-20-3 Naphthalene } ;< < 5.0 ug/1 108-88-3 Toluene ug/1 m,p-Xylene I)>> > 5.0 ug/1 ..................I........ ........................... 95-47-6 o-Xylene ND """ »> 5.0 ug/1 C5-C8 Aliphatics(Unadj.) 38 » 250 ug/1 .. ................... C9-C12 Aliphatics(Unadj.) 14: ` = 50 ug/1 C9-C10 Aromatics(Unadj.) 12 ': ; 50 ug/1 C5-C8 Aliphatics N <>> 50 ug/1 C9-C12 Aliphatics Tjj `" »`<«> 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotolueneo < ;[ > 1fl % ><<<>>> 70-130% 615-59-8 2 5-Dibromotoluene $$%>> > > 'I22 `>»>>< 70-130% ....... ..........%a........... (a)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW17-MW-17 Lab Sample ID: M24976-19 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13233.1) 1 05/14/02 AMY n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 5.0 ug/l.. ........... . .........-............ a 100-41-4 Ethylbenzene 5.0 ug/l 1634-044 Methyl Tert Butyl Ether NIA s .5.0 ug/l 91-20-3 Naphthalene .. ..................:.:0.:-- 5*0 ug/l .......... 108-88-3 Toluene 5.0 ug/l ...... ....... ..... ......... m,p-Xylene 5.0 ug/l ............ 9547-6 o-Xylene ug/l ............................................... ... C5-C8 Aliphatics(Unadj.) 4 . ............ -IV ug/l C9-C12 Aliphatics(Unadj.) .. . . ........50 ug/l C9-C 10 Aromatics(Unadj.) 50 ug/l .. ......... . ........... . . ............. C5-C8 Aliphatics ....... 50 ug/l .................. C9-C12 Aliphatics 50 ug/l CAS No. Surrogate Recoveries Run#I Run#2 Limits .................... 615-59-8 2,5-Dibromotoluene :k.......... ........... -130% -9.4 70 ........ 615-59-8 2,5-Dibromotoluene . . 70-130% ......................... ............... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW 18S-MW-18S Lab Sample ID: M24976-20 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN 13229.D 1 05/14/02 AMY n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND << 5.0 ug/l 100-41-4 Ethylbenzene li 5.0 ug/l ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether ? 8 >> > 5.0 ug/1 ........................... ........................... 91-20-3 Naphthalene >< 5.0 ug/l 108-88-3 Toluene ITDi > ; 5.0 ug/l m,p-Xylene ) >` 5.0 ug/l 95-47-6 o-Xylene 1tI}` 5.0 ug/l C5-C8 Aliphatics(Unadj:) 9 50 ug/l C9-C12 Aliphatics(Unadj.) ; ' 50 ug/l C9-C10 Aromatics(Unadj.) 1tT) i >`= 50 ug/l ..........:::::.:::::::::. C5-C8 Aliphatics NIA:;:::::::;::: 50 ug/l C9-C12 Aliphatics NTH::::::::::;:::::..... 50 ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 93%<' 70-130% 615-59-8 2,5-Dibromotoluene 98 >`> ' . 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW18D-MW-18D Lab Sample ID: M24976-21 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GAB542.D 1 05/03/02 AF n/a n/a GAB 15 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene Nt >;> < < ;; 5.0 ug/I 10041-4 Ethylbenzene N < ; 5.0 ug/I ....:......:............... ........................... 1634-04-4 Methyl Tert Butyl Ether ND ;;;' ` 5.0 ug/I 91-20-3 Naphthalene N <><< `" 5.0 ug/I ........................... 108-88-3 Toluene .ND ;; 5.0 ug/I m,p-Xylene <>>' 5.0 ug/I 95-47-6 o-Xylene ND5.0 ug/I C5-C8 Aliphatics(Unadj.) Nl ; '< 50 ug/I C9-C12 Aliphatics(Unadj.) D ; =50 ug/I C9-C10 Aromatics(Unadj.) ht ; 50 ug/I C5-C8 Aliphatics N) ;< 50 ug/I C9-C12 Aliphatics 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 9i ; 70-130% ......................... 615-59-8 2,5-Dibromotoluene .......... 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FB-FB Lab Sample ID: M24976-22 Date Sampled: 05/01/02 Matrix: AQ-Field Blank Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13250.1) 1 05/15/02 AMY 'n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene hills> >> > 5.0 ug11 100-414 Ethylbenzene Iil) '' ; 5.0 ug/1 ..:........................ ........................... 1634-04-4 Methyl Tert Butyl Ether ICID`>>_ ; 5.0 ug/1 91-20-3 Naphthalene >> 5.0 ug/I 108-88-3 Toluene D "' <> > 5.0 ug/1 m,p-Xylene N `<>i;;>>< 5.0 ug/1 95-47-6 o-Xylene ND 5.0 ug/1 C5-C8 Aliphatics(Unadj.) i1 '` "'> 50 ug/1 C9-C12 Aliphatics(Unadj.) ND,......... 50 ug/1 ug/1 C9-C10 Aromatics(Unadj.) `>1 <`; 50 ........................... C5-C8 Aliphatics N?; < 50 ug/1 C9-C12 Aliphatics Nl < >; ' 50 ug/1 ........................ CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $7 70-130% ................-....... ......................... 615-59-8 2,5-Dibromotoluene g9% 70-130% ..............- _....._...... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TB-TB - Lab Sample ID: M24976-23 Date Sampled: 05/01/02 Matrix: AQ-Trip Blank Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GAB684.1) 1 05/10/02 AF n/a n/a GAB20 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ...._...--........_.... ........................... 71-43-2 Benzene lI); >; 5.0 ug/1 ........................... ........................... ........................... 100-41-4 EthylbenzeneT < ' ' S.0 ug/1 1634-04-4 Methyl Tert Butyl Ether NI < 5.0 ug/1 ........................... ........................... ........................... 91-20-3 Naphthalene NTH:; <r<;< 5.0 ug/1 :...:...................... ........................... ........................... 108-88-3 Toluene ND; ; 5.0 ug/1 ........................... ........................... ........................... m,p-Xylene 1tI <s > 5.0 ug/1 95-47-6 o-Xylene ItI 5.0 ug/I CS-C8 Aliphatics(Unadj.) IIT3 ; 50 ug/I C9-C12 Aliphatics(Unadj.) IUD <> 50 ug/1 C9-C10 Aromatics(Unadj.) l� ;``` 50 ug/1 ... ................... _. _........ CS-C8 Aliphatics ND 50 ug/1 C9-C 12 Aliphatics N1 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 9o > 70-130% ......... ......................... ......................... 615-59-8 2,5-Dibromotoluene2%»; 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis. Page 1 of i Client Sample ID: TMP119(78-80') Lab Sample ID: M24976-24 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed.By Method pH ( >; su 1 05/02/02 SAP EPA 150.1 RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TMP119(102-104') Lab Sample ID: M24976-25 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method pH 5 . Su 1 05/02/02 SAP EPA 150.1 RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M24976-2A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... Iron 100 ug/1 1 05/08/02 05/10/02 LMN SW846 6010B SW846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M24976-3A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Iron 1 >> 100 ug/1 1 05/08/02 05/10/02 LMN SW846 6010B SW846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOI-MW-1 Lab Sample ID: M249764A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method .......................... Iron 28Q¢ 100 ug/1 1 05/08/02 05/10/02 LMN SW846 6010B SW846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M24976-6A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Iron Sa50¢ ' < > 100 ug/1 1 05/08/02 05/10/02 LMN sw846 6010B sw846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW09-MW-9 Lab Sample ID: M24976-8A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ............. ........................... Iron 3 SU4 I ug/1 1 05/08/02 05/10/02 LMN SW846 6010B Sw846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M24976-12A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... Iron 1( <„ 100 u9/1 1 05/08/02 05/10/02 LMN SW846 6010B SW846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M24976-13A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Iron If)Fl 100 ug/I 1 05/08/02 05/10/02 LMN SW846 6010B SW846 3010A RL = Reporting Limit MADEP VPH FORM NEA ueous W Soil Sediment n Other Satisfacto Broken Leaking N/A PH<=2 PH>2 Receivedon1ce Received at 4 Deg. C Other W Rec'd at 3 deg C MKIM N/A ethod for Ranges: MADEP VPH 98-1 Client ID: MW01A-MW-1A Lab ID: M24976-1 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A pad usted Ranges CAS Al Elution Ranae Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) NIA ugA ND" 50 r et Anal es Ethylbenzene 100-41-4 C9-1312 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ugA ND 5 usted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND° 50 rro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 85 70-130% PID:2,5-Dibromotoluene % 89 70-130% otnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C5-C9 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9410 Aromatic Hydrocarbons. AV qualifier indicates an estimated value ere all CA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? RIND ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for taining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5117/02 i MADEP VPH FORM A ueous W Soil F1 Sediment n Other SatisfactoryPI Broken n Leakin N/A F1 PH<=2 V PH>2 Received on ice Received at 4 Deg. C F1 Other W Redd at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW02A-MW-2A Lab ID: M24976-2 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1102 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/02 05/13/02 FID: 2,5-Dibromotoluene %.Solids: Low Dilution: High Dilution: N/A 1 2 Unad usted Ranges CAS# Elution Ranae Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I 2770 A 100 C9-C10 Aromatics(Unadj.) N/A ug/I 82.5" 50 C9-C12 Aliphatics(Unadj.) N/A ugA 116 A 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 2700 10 Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ug/1 122 5 Naphthalene 91-20-3 N/A ug/I 11.3 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/l 11 5 Ad'usted Ran es C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ugA ND c 50 Surro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 99 70-130% PID:2,5-Dibromotoluene % 108 70-130% FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 81 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? VNo ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for obtaining the Information,the material contained In this report is,to the best of my knowledge and belief,accurate and. complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 S MADEP VPH FORM Aqueous Soil n Sediment F1 Other SatisfactorvW Broken F1 Leaking- N/A H<=2 W PH>2 Received on Ice F1 Received at 4 Den.C F1 Other WJ Rec'd at 3 deg C N/A lethod for Ranges: MADEP VPH 98-1 Client ID: MW03A-MW-3A Lab ID: M24976-3 lethod for Target Analytes• MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nadiusted Ranaes CAS# Elution Ranae Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 aroet Analvtes Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ugA ND 5 diusted Ranaes C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ugA ND c 50 urroaate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 84 70-130% )otnotes Hydrocarbon Range data exclude concentrations of any sunrogate(s)and/or Internal standards eluting in that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-Ca Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Aralytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. A'J'qual ier Indicates an estimated value re all QA/QC procedures REQUIRED by the VPH Method followed? ❑d Yes ❑ No.Details Attatched re all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No.Details Attatched re any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my Inquiry of those individuals Immediately responsible for taining the information,the material contained In this report Is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director Date 5I17/02 Tinted Name Reza Tand MADEP VPH FORM A ueous W Soil Sediment n Other SatisfactoryV Broken n Leakin N/A_ F1 PH<--2 W PH>2 Received on Ice Received at 4 De a.C F1 Other W Rec'd at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW01-MW-1 Lab ID: M24976-4 Method for Target Analytes• MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: -PID: 2,5-Dibromotoluene N/A 5/13/02 WA FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 WA Unadiusted Ranges CAS# Elution Range Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ugA 725 A 50 C9-C10 Aromatics(Unadj.) N/A ugA 90.2 A 50 C9-C12 Aliphatics(Unadj.) N/A ugA 196 A 50 Tar et Mal es Ethylbenzene 100-41-4 C9-C12 ugA 22 5 Toluene 108-88-3 C5-C8 ugA 48 5 Methyl Tert Butyl Ether 1634404-4 C5-C8 ugA 637 5 Benzene 71-43-2 C5-C8 ugA 14.2 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ugA 22.9 5 m,p-Xylene C9-C12 ugA 44.6 5 Ad lusted Ran es C5-C8 Aliphatics N/A ugA ND 8 50 C9-C12 Aliphatics N/A ug/1 ND` 50 Surrogate Recoveries Acceotance Range FID:2,5-Dibromotoluene % 87 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of arty surrogate(s)andior Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor Internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Annalytes eluting in that range. C Hydrocarbon Range data exclude concentrations of arty surrogate(s)andlor Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target_Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 66Yes ❑ No.Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified In Sect.11.3? ❑d No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report Is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous P1 Soil n Sediment F1 Other SatisfactorvW Broken n Leakin N/A F1 DH <=2 W DH>2 Received on Ice n Received at 4 Den. C F1 Other W Rec'd at 3 deg C N/A ethod for Ranges: MADEP VPH 98-1 Client ID: MW02-MW-2 Lab ID: M24976-5 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution• N/A 1 N/A nad usted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) NIA ugA ND" 50 'arnet Analytes Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 20.4 5 Benzene 71-43-2 C5-C8 ugn ND 5 Naphthalene 91-20-3 N/A ug/l ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ugA ND 5 d usted Ran es C5-C8 Aliphatics N/A ugA ND 8 50 C9-C12 Aliphatics N/A ug/I ND c 50 urro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 101 70-130% PID:2,5-Dibromotoluene % 108 70-130% otnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. CS-CO Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9C10 Aromatic Hydrocarbons. A'J'qualffier indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? ©No El Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for taining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5/17/02 MADEP VPH FORM Aqueous Soil F1 Sediment F1 Other SatisfactorvW Broken F1 Leaking N/A n pH<=2 W PH>2 Received on Ice F1 Received at 4 Den. C Other W Reed at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW05-MW-5 Lab ID: M24976-6 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 50 N/A Unad usted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 48700A 2500 C9-C10 Aromatics(Unadj.) N/A ug/I 7730 A 2500 C9-C12 Aliphatics(Unadj.) N/A ug/I 22800 A 2500 Tar et Analytes Ethylbenzene 100-41-4 C9-C12 ugA 2000 250 Toluene 108-88-3 C5-C8 ugA 10400 250 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 36000 250 Benzene 71-43-2 C5-C8 ug/I 1520 250 Naphthalene 91-20-3 N/A ug/I 540 250 o-Xylene 95-47-6 C9-C12 ugA 3830 250 m,p-Xylene C9-C12 ugA 7710 250 Ad lusted Ran es C5-C8 Aliphatics N/A ug/I ND a 2500 C9-C12 Aliphatics N/A ug/I ND r 2500 Surro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % 99 70-130% Footnote Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Internal standards eluting In that range 9 Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑d Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified In Sect.11.3? ONo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those Individuals Immediately responsible for obtaining the Information,the material contained in this report Is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17102 MADEP VPH FORM A ueous W Soil F1 Sediment Other SatisfactorvW Broken F1 Leakin NIA H<=-2 W PH>2 Received on Ice F1 Received at 4 Deg. C Other WJ Redd at 3 deg C NIA ethod for Ranges: MADEP VPH 98-1 Client ID: MW06-MW-6 Lab ID: M24976-7 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 512102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 25-Dibromotoluene N/A 5/13/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ran a CAS# Elution Ranae Units Result RDL f3 C5-C8 Aliphatics(Unadj.) N/A ug/I 1110" 50 C9-C10 Aromatics(Unadj.) N/A ug/I 226 A 50 C9-C12 Aliphatics(Unadi.) N/A ug/I 279 A 50 ar et Anal es Ethylbenzene 100-41-4 C9-C12 ug/I 8.3 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 1170 5 Benzene 71-43-2 C5-C8 ug/I 51.4 5 Naphthalene 91-20-3 N/A ug/I 33.7 5 o-Xylene 95-47-6 C9-C12 ug/l 6.1 5 L m,p-Xylene C9-C12 ug/1 12.2 5 usted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 urro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 109 70-130% PID:2,5-Dibromotoluene % 112 70-130% ootnotes Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. A'J'qualifier Indicates an estimated value Jere all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? WV Yes ❑ No.Details Attatched /ere any significant modifications made to the VPH method,as specified in Sect.11.3? ONo ❑ Yes-Details Attatched bttest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for taining the information,the material contained in this report Is,to the best of my knowledge and belief,accurate and omplete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous Soil M Sediment F1 Other SatisfactoryW Broken F1 Leakin NIA FI DH<=2 V PH>2 Received on Ice Received at 4 Dog. C Other Rec'd at 3 deg C MEN/A Method for Ranges: MADEP VPH 98-1 Client ID: MW09-MW-9 Lab ID: M24976-8 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 50 N/A Unad usted Ran es CAS# Elution Range Units Resul RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/l 33500" 2500 C9-C10 Aromatics(Unadj.) N/A ug/I 15600" 2500 C9-C12 Aliphatics(Unadj.) N/A ug/I 39500" 2500 Tarnet Analytes Ethylbenzene 100-41-4 C9-C12 ug/I 2950 250 Toluene 108-88-3 C5-C8 ug/l 16800 250 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 6880 250 Benzene 71-43-2 C5-C8 ug/I 1620 250 Naphthalene 91-20-3 N/A ug/I 968 250 o-Xylene 95-47-6 C9-C12 ug/I 6060 250 m X lene .P- Y C9-C12 ug/I 11700 250 Ad lusted Ran es C5-C8 Aliphatics N/A ug/I 81900 2500 C9-C12 Aliphatics N/A ug/I 3230 c 2500 Surro a e Recoveries Acceptance Range FID:2,5-Dibromotoluene % 95 70-130% PID:2,5-Dibromotoluene % 103 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arty surrogates)and/or internal standards eluting in that range. CS-CII Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Anatytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. 1zA V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? OYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous W Soil F1 Sediment F1 Other SatisfactoryW Broken Leakin NIA F1 PH<-_2 PH>2 Received on Ice Received at 4 Deg. C Other W Reed at 3 deg C EN/A ethod for Ranges: MADEP VPH 98-1 Client ID: MW10-MW-10 Lab ID: M24976-9 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 H Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A ID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A ad usted Ran es CAS# Elution Ranae Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) WA ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 r et Anal es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 L m,p-Xylene C9-C12 ugA ND 5 sted Ran es C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ugA ND° 50 rro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 91 70-130% otnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CSC8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9C72 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9470 Aromatic Hydrocarbons. A V qualiner Indicates an estimated value re all QA/QC procedures REQUIRED by the VPH Method followed? PlYes ❑ No-Details Attatched re all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched re any significant modifications made to the VPH method,as specified in Sect.11.3? R1No ❑ Yes-Details Attatched est under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for taining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and plete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous Soil n Sediment F1 Other SatlsfactoryW Broken F1 Leaking MEN NIA F1 PH<=2 W PH>2 Received on Ice F1 Received at 4 Deg. C F1 Other d ReC'd at 3 deg C NIA Method for Ranges: MADEP VPH 98-1 Client ID: MW 11-MW-11 Lab ID: M24976-10 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ran es CAS# Elution Range Units Result RDL 2 C5-C8 Aliphabcs(Unadj.) N/A ug/I 92.2 A 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Taroet Anal es Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 102 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/I ND 5 Ad usted Ranges C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surro ate Recoveries Acceptance Range. FID:2,5-Dibromotoluene % 100 70-130% PID:2,5-Dibromotoluene % 107 70-130% Footnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C5-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. A V qualHler Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No.Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified In Sect.11.3? WIND ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the Information,the material contained In this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5117/02 MADEP VPH FORM Aciueous W Soil F1 Sediment n Other SatisfactorvW Broken F1 Leaking NIA F1 H<=2 W1 PH >2 Received on Ice Received at 4 Den.C Other Rec'd at 3 deg C N/A ethod for Ranges: MADEP VPH 98-1 Client ID: MW 12-MW-12 Lab ID: M24976-11 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PH 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nadlusted Ran es CAS# Elution Ranae Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ug/l ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 r et Analytes Ethylbenzene 100-41-4 C9-C12 ug/l ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/1 ND 5 m,p-Xylene C9-C12 ug/I ND 5 lusted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 A1iphatics N/A ug/I ND` 50 rro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 86 70-130% rAXquallifler arbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range arbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude entration of Target Analytes eluting in that range. arbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Indicates an estimated value re all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No.Details Attatched re all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No.Details Attatched re any significant modifications made to the VPH method,as specified in Sect.11.3? RIND ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my inquiry of those individuals Immediately responsible for taining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and mplete. Signature �'-� ��� Postition Laboratory Director rinted Name Reza Tand Date 5/17/02 MADEP VPH FORM Aqueous Soil Sediment FI Other SatisfactoryFyl Broken F1 Leakin N/A H<=2 V pH>2 Received on Ice Received at 4 Den. C F1 Other W Read at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW 13-MW-13 Lab ID: M24976-12 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %.Solids: Low Dilution: High Dilution: N/A 1 N/A Unad usted Ran es CAS# Elution Range Units Result RDL f3 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Tar et Anal es Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ug/l ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/I ND 5 Ad'usted Ran es C5-C8 Aliphatics N/A ug/l ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 100 70-130% PID:2,5-Dibromotoluene % 108 70-130% Footnotes Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range 6 Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Internal standards eluting In that range. CS-C9 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. A'J'qualifler Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? SaYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified In Sect.11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for obtaining the Information,the material contained In this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17102 MADEP VPH FORM A ueous W Soil F1 Sediment F1 Other SatisfactorvW Broken F1 Leakin N/A F1 1PH <=2 W PH>2 Received on Ice Received at 4 Deg. C n Other W Reed at 3 deg C NIA ethod for Ranges: MADEP VPH 98-1 Client ID: MW14-MW-14 Lab ID: M24976-13 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: 'PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution- N/A 1 N/A nadiusted Ranges CAS# Elution Ranne Units Result RDL 9 C5-C8 Aliphatics(Unadj.) NIA ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 artlet Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ug/I ND 5 lusted Ran es C5-C8 Aliphatics N/A ug/l ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 rro ate Recoveries Acceptance Ranue FID:2,5-Dibromotoluene % 85 70-130% PID:2,5-Dibromotoluene % 90 70-130% FAX rbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range rbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range. CS-CO Aliphatic Hydrocarbons exclude entration of Target Analytes eluting in that range. rbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude Target Analytes eluting In that range AND concentration of MOO Aromatic Hydrocarbons. ll ier Indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No.Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for taining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous Soil n Sediment n Other SatisfactorvW Broken F1 Leakin N/A n PH<=2 W PH>2 Received on Ice n Received at 4 Deg. C FI Other Vj Reed at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW 141-MW-141 Lab ID: M24976-14 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/3/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unad usted Ran es CAS# Elution Ranae Units Resul RDL (3 C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Taraet Analvtes Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634 04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/I ND 5 Ad'usted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ugA ND c 50 Surro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 88 70-130% PID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arty surrogatels)and/or Internal standards eluting in that range. CS-C9 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9410 Aromatic Hydrocarbons. A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? RJYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? VlYes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ONo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the Information,the material contained In this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5117/02 MADEP VPH FORM Aciueous Soil F1 Sediment F1 Other Satisfactory9i Broken Fl Leakin N/A F1 pH<=2 W PH>2 Received on Ice Received at 4 De a.C F1 Other W Read at 3 deg C N/A thod for Ranges: MADEP VPH 98-1 Client ID: MW14D-MW-14D Lab ID: M24976-15 thod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 H Surrogate Standards Date Extracted: First Date Run: Last Date Run: ID: 2,5-Dibromotoluene N/A 5/3/02 N/A ID: 2,5-Dibromotoluene %e Solids: Low Dilution: High Dilution: N/A 1 N/A adlusted Ranges CAS# Elution Ranae Units Res I RDL f� C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/1 ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 stet Anaivtes Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 5 Benzene 71-43-2 C5-C8 ug/1 ND 5 Naphthalene 91-20-3 N/A ug/1 ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ug/I ND 5 iusted Ranaes C5-C8 Aliphatics N/A ug/1 ND B 50 C9-C12 Aliphatics N/A ugA ND c 50 'roseate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene %e 95 70-130% PID:2,5-Dibromotoluene %B 93 70-130% Anotes. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Internal standards eluting In that range. CS-08 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-G10 Aromatic Hydrocarbons. A'J'qualMor Indicates an estimated value re all QA/QC procedures REQUIRED by the VPH Method followed? Dyes ❑ No-Details Attatched re all performance/acceptance standards for required QA/QC procedures achieved? RYes ❑ No-Details Attatched re any significant modifications made to the VPH method,as specified In Sect.11.3? ONo ❑ Yes-Details Attatched test under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for aining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and nplete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous W Soil F1 Sediment F1 Other SatisfactorvW Broken F1 Leakin N/A F1 DH<=2 W DH>2 Received on Ice F1 Received at 4 Deg.C Other W Reed at 3 deg C MIEN/A Method for Ranges: MADEP VPH 98-1 Client ID: MW 15-MW-15 Lab ID: M24976-16 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unad us ed Ran es CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Tarnet Anal es Ethylbenzene 100-414 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ug/1 ND 5 Ad lusted Ran es C5-C8 Aliphatics N/A ug/l ND a 50 C9-C12 Aliphatics N/A ugA ND° 50 Surro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 83 70-130% Footnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? RiYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? RIND ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those Individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM Aqueous W Soil F1 Sediment n Other .SatisfactorvW Broken F1 Leakin NIA F1 PH<=2 NA DH>2 Received on Ice Received at 4 Deg. C F1 Other W Rec'd at 3 deg C N/A ethod for Ranges: MADEP VPH 98-1 Client ID: MW16-MW-16 Lab ID: M24976-17 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ranges CAS# Elution Ranae Units Resui RDL 2 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 ar et Anal es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ug/i ND 5 Lm,p-Xylene C9-C12 ug/I ND 5 usted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 urro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 83 70-130% PID:2,5-Dibromotoluene % 85 70-130% FAX rbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range arbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-CB Aliphatic Hydrocarbons exclude entration of Target Analytes eluting In that range. rbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. lifier Indicates an estimated value Nere all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified In Sect.11.3? WNo ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my Inquiry of those Individuals immediately responsible for btaining the Information,the material contained In this report is,to the best of my knowledge and belief,accurate and omplete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous 91 Soil F1 Sediment F1 Other SatisfactorvW Broken F1 Leakina El N/A n DH <=2 W PH>2 El Received on Ice F1 Received at 4 Den.C Other nv Reed at 3 deg C NIA Method for Ranges: MADEP VPH 98-1 Client ID: MW16D-MW-16D Lab ID: M24976-18 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 05/15/02 FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 5 Unad ust d Rannes CAS# Elution Range Units Resul RDL f� C5-C8 Aliphatics(Unadj.) N/A ugA 4380 A 250 C9-C10 Aromatics(Unadj.) N/A ugA 122 A 50 C9-C12 Aliphatics(Unadj.) N/A ug/l 149 A 50 Taraet Analvtes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 4280 25 Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ug/I 414 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/I ND 5 Ad usted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 107 70-130% PID:2,5-Dibromotoluene % 122 70-130% FID:2,5-Dibromotoluene % 83 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnote A Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9410 Aromatic Hydrocarbons. A'Y qualifier Indicates an estimated value Were all QA(QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? RJNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for obtaining the information,the material contained In this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM Aqueous Soil n Sediment F1 Other SatisfactorvW Broken n Leaking N/A F1 PH<=2 P1 PH>2 Received on Ice Received at 4 De- .C Other W Redd at 3 deg C NIA ethod for Ranges: MADEP VPH 98-1 Client ID: MW17-MW-17 Lab ID: M24976-19 ethod for Target Analytes MADEP VPH 98 1 Date Collected: 5/1/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 NIA FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ran es CAS# Elution Range Units Result RDL l3 C5-C8 Aliphatics(Unadj.) NIA ug/I ND" 50 C9-C10 Aromatics(Unadi.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 aroet Anal es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ug/l ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/I ND 5 dusted Ran es C5-C8 Aliphatics N/A ug/l ND a 50 C9-C12 Aliphatics N/A ugA ND° 50 urro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 94 70-130% PID:2,5-Dibromotoluene % 100 70-130% FAXqualffier arbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range arbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-CS Aliphatic Hydrocarbons exclude entration of Target Analytes eluting In that range. rbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude Target Analytes eluting in that range AND concentration of C9410 Aromatic Hydrocarbons. Indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No.Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for talning the information,the material contained in this report is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17102 MADEP VPH FORM Aqueous Soil F1 Sediment F1 Other SatlsfactoryW Broken n Leakin NIA H<=-2 W PH>2 Received on Ice Received at 4 Den.C F1 Other W Reed at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW18S-MW-18S Lab ID: M24976-20 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A U ad'usted Ranges CAS# Elution Ranae Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 51.9 A 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Tarnet Analytes Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 26.8 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xyiene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ugli ND 5 Ad lusted Ran es C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ugA ND c 50 Surro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % 98 70-130% Footnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range 8 Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. A'X qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? VYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for obtaining the Information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous Soil n Sediment Other Satisfacto Broken Leakin N/A F1 PH<=2 W H>2 Received on Ice n Received at 4 De- . C El Other W Rec'd at 3 deg C i- i- N/A ethod for Ranges: MADEP VPH 98-1 Client ID: MW181)-MW-18D Lab ID: M24976-21 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/3102 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A ad lusted Ran es CAS# Elution Ranae Units Result RDL t3 C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/1 ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/i ND" 50 r et Anal es Ethylbenzene 100-41-4 C9-C12 ug/1 ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugll ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ug/l ND 5 o-Xylene 95-47-6 C9-C12 ug/1 ND 5 m,p-Xylene C9-C12 ugA ND 5 lusted Ran es C5-C8 Aliphatics N/A ug/l - ND a 50 C9-C12 Aliphatics N/A ugA ND' 50 rro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % 92 70-130% otnotes Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9C10 Aromatic Hydrocarbons. A'J'qualifier indicates an estimated value re all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched re all performance/acceptance standards for required QAIQC procedures achieved? DYes ❑ No.Details Attatched re any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for taining the Information,the material contained in this report is,to the best of my knowledge and belief,accurate and mpiete. Signature Postition Laboratory Director "rioted Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous NA Soil Sediment F1 Other SatisfactoryWl Broken F1 Leaking NIA n PH<=2 W PH>2 Received on Ice Received at 4 Den. C Other W Reed at 3 deg C NIA Method for Ranges: MADEP VPH 98-1 Client ID: FB-FB Lab ID: M24976-22 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/15/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Ranae Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Tar et Analytes; Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/l ND 5 m,p-Xylene C9-C12 ug/I ND 5 Adjusted Ranges C5-C8 Aliphatics N/A ug/l ND a 50 C9-C12 Aliphatics N/A ug/l ND c 50 Surro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 89 70-130% Footnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualMler Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? IYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report Is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM Aqueous W Soil F1 Sediment Other SatisfactorvW Broken F1 Leakin N/A H<=-2 W PH>2 Received on Ice F1 Received at 4 Deg.C F1 Other W Reed at 3 deg C N/A ethod for Ranges: MADEP VPH 98-1 Client ID: TB-T13 Lab ID: M24976-23 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene NIA 5/10/02 NIA FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 NIA nad usted Ranges CAS# Elution Ranae Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 ar et Anal es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 L m,p-Xylene C9-C12 ugA ND 5 usted Ran es C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ug/l ND c 50 urro ate Recoveries Acceotance Raring FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 92 70-130% loom es Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. A'J'qualHler indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? Oyes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect 11.3? ©No ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my inquiry of those Individuals immediately responsible for Ibtaining the information,the material contained In this report is,to the best of my knowledge and belief,accurate and omplete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 l,�ill�11r lJl' t/ I 1 'VL I ACCUTE81•JOB 0 / ®ACCUTEST 'M TECHNOLOGY CENTER WEST • BUILDING ONE AZ 9 D MARLBOROUGH,MA 01752 ACCUTEST QUOTE a: TEL:508481-6200 • FAX.-508-481-7753 CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES r� �... �l�• ��X�I.L-i� ��� '� OW- DRINKING NAME PROJECT NAME WATER ,i dW- GROUND 3, caagoU ' ILi0 ..r�.��n e r"I �d Ci i ini - WATER A RESS . L CATION - WW- WASTE 1 Sc>� 01�� _ ay�VOI 4y►/�LS (� Soot G WATER C p STATE ZIP PROJECT NO. SO- SOIL _�c1 char 7hc "r (0 9 9L50 o?$ a- OIL DGE SEND REPORT TO: d LIQ- OTHER PHONE# 9-t.R - Cj{n� O FAX# �,Q,- _ 0 00 - Cl-ISi a LIQUID SOL-OTHER ACCUTEST COLLECTION PRESERVA71O SOLID SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SALi MPLED g 1741 ad _..w S } Q vil LAB USE ONLY Z 97a- _ I loz 1t-Nvo R<57 G w Z Ix -Z Zmw,m _ i IZ5 1-7 X X x Ix x x x• x -3 3 - - �l 4030 �G`1 W X X X xxly KAmWo t - >v\w- 1 630 MCA G YC Y, >C X W ZA x i q'4p taw X - mw-1 14 i S7 12 W -7 x xi th X kW KmW 2- X DATA TURNAROUND INFORMATION FDATA DELIVERABLE INFORMATION COMMENTS/REMARKS ❑ 14 DAYS STANDARD APPROVED BY: ❑ STANDARD ❑ 7 DAYS RUSH O COMMERCIAL"B" O 48 HOUR EMERGENCY ❑ DISK DELIVERABLE O OTHER ❑ STATE FORMS - 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX O OTHER(SPECIFY) 3H 6 DATA UNLESS PREVIOUSLY APPROVED V6cx SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERY RELINQUISHED BY SAMPLER DATE TIME: RECEIVED BY: REU IS ED BY: Y717— DA ME: RECEIV Y: 1. 1910 1, G SC ti,� 2� 2, RELINQUISHED BY: DA E ME: RECEIVED BY: RELINQUISHED BY: DATSTIMI& RECEIV Y 3. 3. 4. 4. RELINQUISHED BY: DATE TIME: RECEIVED BY: SEAL# PRESERVE WHO APPLICABLE ON TEMpER/�{!RE 5. .3 _C © MARLBOROUGH,MA 01752 ACCUTEST QUOTE 1k TEL•508-481-6200 • FAX 508 d81-7753 CLIENT INFORMATION pFACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES DW- DRINKING (� J C �/'L/i G CFS'7_ _ 1-f- .CkCO I � WATER NAME (1 PROJECT NAME W1A GW- GROUND � �l � f; f4 40 n 1 ��dti��5 WATER ADDRESS? LOCATION WW- WAS TE OIT/� WATER [�"O� 'K1 ZC �A C SO- SOIL C� STATE ZIP PROJ,�U NO. SL- SLUDGE c S2 ICJ C b; .�-��o aSoag OI- OIL LIQ- OTHER SEND REPORT TO: LIQUID PHONE II - _�7 /4n FAX -SCo_- -9�?16 SOL-OTHER ACCUTEST COLLECTION LL PRESERVAI. TION o N SOLID O SAMPLE* FIELD ID/POINT OF COLLECTION DATE TIME S BYLED ft 9 $ ? Q 8 LAB USE ONLY Z y? -It 02 13Zo Hcr 16W 2 X -- 2 IZA M 1`3 y mLmh GW '7 X X >C V -I LI tLa k445 4A C-k Z -/.� -MW - 14 I1 I'LA GW Z- - pow e t?a3o 1MW vJ 2 x 100 mvi 5,w Z x I )C -12m w-ri tow -zo (Mint \ .- i�S 1OZ5 fv\w . w Z Ihs mw Gw 2 DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTS/REMARKS ❑ 17 DAYS RUSH STANDARD4 DAYS APPROVED BY: 0 STANDARD O COMM RCIAL"B" m c ;SS FP ajad adalod O 48 HOUR EMERGENCY Cl DISK DELIVERABLE zh,A1 ❑ OTHER ❑ STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) o DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERY RELINQUISHED BY SAMPLER: DATE TIME: RE NW BY: RELIN DISHED BY: D ME RECEIV BY: !Q 1p 1-�C eu, 2 'z 0Z/?� 2. J I l RELINQUISHED BY: DA E TIME: RECEIVED BY: -By. DATE TIME RECEN Y. 3. 3. 4. 4: 67- REUNOUtSHED BY: DATE TIME: RECEIVED BY: SEAL t PRESERVE VFHERE APPLICABLE ON TEMP31i�URC 5. 5. 0 UkIA1N OF CUSTODY ACCUTEST J081: ®A TEST 40 TECHNOLOGY CENTER WEST• BUILDING ONE Z MARLBOROUGH,MA 01752 ACCUTEST QUOTE 11: TEL:508-481-62W • FAX 508-481-7753 CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES yyi I Q c_ Cvy'p _�ACA.C.n I[ 7 3 DW- DRINKING NAME. PROJECT NAME — WATER ))� ` `fM GW- GROUND OUND A RES //�� nn ER LOCATION WW- WASTE Sn,n YYl tit• c 17!,T _I �� a-IA nh'S 073 ps7 o Cf C WATER CITY,�, STATE ZIP PROJECT N p, A SO- SOIL 1•�n K r(C ./ j�y�_ 'A. 1 G l aso a$ SL- SLUDGE SEND REPORT Tq, OI- OIL LIQ- OTHER PHONE# `'/7w- SSCO 9-�7Y() FAX# 4`7�c �Y(pg-q�(�n LIQUID SOL-OTHER COLLECTION i m PRESERVATION ACCUTEST SOLID SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLED Q BY: $ _ LAB USE ONLY -2-3 T — i n i(�So ..z `gym -zs'rMPII 1 1 ti DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTS/REMARKS ❑ 14 DAYS STANDARD APPROVED BY. O STANDARD II ❑ 7 DAYS RUSH 6`1�� O COMMERCIAL"B" -�a O 48 HOUR EMERGENCY O DISK DELIVERABLE O OTHER O STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX O OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHA E POSSESION�INCLUDING COURIER DEL RELINQUISHED BY SAMPLER: MIME: RECEIVED BY: RELI QUI ED BY: p TI RECEIV Y: 1. O Z q1p 1. oZ% 2.RELINQUISHED : DATE TIME: RECEIVED BY: RELINQUISHED BY: ATE TIME: RE V y. 3. 3. 4. 4. 1RELINQUISHED BY: DATE TIME: RECEIVED BY: SEAL# 5. PRESERVE WHERE APPLICABLE ON ICE TEMPERATURE Appendix D Well Logs 5. GEOLOGIC SERVICES CORPORATION DRILLINGLOG Hydrogeologists and Environmental Scientists AS-1 15 Bonazzoli Avenue,Hudson,MA 01749 978 568-8740 Project Texaco Station tl 100093 Client EquivaServices LLC Sketch Map(not to scale) Limon: 1140 bough Road,Hyannis,MA Total DepOe 49 feel Well m: AS-1 S—m Diameter: 2 inch Water Level: 31 feet slot Size: 0.010 inch Screm Lmg&: 2 feet Casing Diameter. 2 inch Type. PVC Type: PVC Casing Leng6: 47 feet Driller. Mike DeAnu— See Site Plan Top Elevation: 99.08 feet Drilling Company Geosc=h,Inc. Method Hollow Stem Auger GSC Inspector: SC/KS Date Start 3/19/2001 Data End 3/212001 Notes:Testing consist of PlDheadspacerespmnse(ppmv) - Sample E Depth Well Key ID Depth Blows/6" Pen/Rex Sample a feet Construction Description 0 Road box Gripper plug S-1 04' Brown,dry,medium to coarse SAND, ND z Concrete some medium to fine gravel,some cobbles a Native Material S-2 4-8' Brown,dry,medium to coarse SAND, ND 6 Casing some medium to fine gravel,some cobbles s 10 rz S-3 12-14' Brown,dry,medium to coarse SAND, ND _14 some fine to medium gravel,some cobbles 16 18 S4 18-20' Brown,dry,coarse SAND,some fine ND z0 gravel,little cobble zz 24 S-5* 24-26' Brown,moist,medium to coarse SAND, 1.5 _26 Grout fine gravel 2s 30 S-6 30-32' Brown,wet,medium to coarse SAND, 89 32 some fine gravel 3a 36 S-7 36-38' Brown,wet,coarse SAND 45 38 a0 a2 S-8 42-44' Brown,wet,coarse SAND - 35 a as Bentonite seal Well screen 48 Filter sand so End of Exploration @ 49' GSC Project Number. 000509 Checked By: �l Page 1 of 1 Notes: *-Sample taken at this depth GEOLOGIC SERVICES CORPORATION DRILLING LOG Hydrogeologists and Environmental Scientists SVE-1 15 Bonazzoli Avenue,Hudson,MA 01749 978-568-8740 _ Project: Texaco Station#100083 Client Equiva Services LLC Sketch Map(not to scale) Location: 11401yannough Road Hyannis,MA Total Depth 36 feet Well ID: SVE-1 Screen Diameter. flinch Water Level: —31 feet Slot Size: 0.010inch Screen Length: 10 fed Casing Diameter. 4 inch Type: PVC Type: PVC Casing Length 26 feet Driller: Mike DeAmicus See Site Plan Top Elevation: 99.11 feet Drilling Company: Geosearch,htc. Method: Hollow Stem Auger GSC Inspector: SCOW Date Start 3/19/01 Date End 3/20/01 Notes:Testing consists of PID headspace response(ppmv) ample Depth Well Key ID Depth Blows/6" Pen/Rec Sample a feet Construction Description o Road box Gripper plug S-1 0-5' Brown,dry,fine SAND,little fine-medium ND _2 Concrete gravel(SP) a 6 Casing S-2 5-10' Brown,dry,fine SAND,little fine gravel ND (SP) _a 10 S-3 10-15' Brown,dry,fine SAND,some fine gravel, ND _12 Native Material cobbles(GM) _14 16 S4 15-20' Brown,dry,fine SAND,little to some ND fine gravel(SP) to _zo S-5 20-25' Brown,dry,fine SAND,little fine gravel ND 22 (SP) Bentonite seal zb Filter sand S-6 25-30' Brown to tan,dry,fine SAND(SM) 0.2 zs 0 Well screen S-7* 30-35' Tan,dry to moist,fine SAND QvIL) 111.7 z 4 6 S-8 35-36' Tan,moist to wet,fine SAND 78 End of Exploration @ 36' (t 40 GSC Project Number: 000509 Checked By: r1�//\ Page 1 of 1 Notes: *-Sample taken at this depth GEOLOGIC SERVICES CORPORATION DRILLING LOG Hydrogeologists and Environmental Scientists MP-1 15 Bonazzoli Avenue,Hudson,MA 01749(978)-568-8740 Project Tezaoo Station k 100083 Client Eviva Services LLC Sketch Map(not to scale) Location: 1140 Iyamough Road,Hyannis,MA Total Depth: 43 feet Well ID: MP-1 Sacm Diameter. 1.5 inch Water Level: —31 feet Slot Size: 0.010 inch Screen Length: 10,2,2 fed Casing Diameter: 1.5 inch Type: PVC Type: PVC Casing Length: 25,37,41 feet Driller. Mike DeAmicus See Site Plan Top Elevation: 98.77 feet Drilling Company: Geosearch,Inc. Method: Hollow Stem Auger GSC Inspector: DW Date Start 3/202001 Date End: 3/202001 Notes: Testing consists of PID headspace response(ppmv) ample Depth Well Key ED Depth Blows/6" Pen/Rec Sample (feet) Construction Description u Road box Gripper plugs S-1 0-5' Brown,dry,fine SAND(SC) ND z Concrete a 6 Casing S-2 5-10' Brown,dry,fine SAND,fine gravel(SW) ND 8 10 S-3 10-15' Brown,dry,fine SAND,fine Pavel(SW) ND 12 14 —16 S-4 15-20' Brown,dry,fine SAND,fine gravel(SW) ND 18 Native Material 20 S-5 20-25' Brown to tan,dry,fine SAND(SC) ND 22 z4 Bentonite seal zb Filter sand S 6 25-30' Tan,dry to moist,fine SAND(SC) ND 28 30 • S-7" 30-35' Brown,dry,fine SAND(SC) 0.5 32 Well screen 34 —36 S-8 35 40' Tan,moist to wet,fine SAND(SC) 1.3 38 Bentonite seal a0 S-9 40-43' Tan,moist to wet,fine SAND(SC) 1.7 az —44 End of Exploration @ 43' GSC Project Number: 000509 Checked By: �`1( :�� Page 1 of 1 Notes: •-Sample taken at this depth GEOLOGIC SERVICES CORPORATION DRILLING LOG Hydrogeologists and Environmental Scientists MP-2 15 Bonazzoli Avenue,Hudson,MA 01749(978)-568-8740 Project: Texaco Station k 100083 Client Equiva Services LLC Sketch Map(not to stele) Location: 1140 lyannough Road,Hyannis,MA Total Depth: 43 fed Well ID: MP-2 Screen Diameter: 1.5 inch Water Level: —31 feet Slot Size: 0.010 inch Screen Length: 10,2,2 feet Casing Diameter: 1.5 inch Type: PVC Type: PVC Casing Length: 25,37,41 feet Driller Mike DCAmicus See Site Plan Top Elevation: 99.05 fed Drilling Company. Geosearch,Inc. Method: Hollow Stan Auger GSC Inspector. SC/MLM Date Start 3/19/2001 Date End: 3/222001 Notes:Testing consists of PID headspace response(ppmv) Sample Depth Well Key ID Depth Blows/6" Pen/Rec Sample a (feet) Construction Description o Road box Gripper plugs S-1 04 Brown,dry,medium to coarse SAND(SP) z Concrete a S-2 4-8' Brown,dry,medium to coarse SAND, _6 Casing some cobble(SW) 8 S-3 8-12' Brown,dry,medium to coarse SAND, _10 mostly cobble(SW) 12 Boulder 14 _16 S-4 15-20' Brown,dry,medium to coarse SAND, some fine gravel(SW) 18 Native Material 20 S-5 20-25' Light brown,dry,medium SAND,some z2 fine gravel(SW) 24 Bentonite seal 26 Filter sand S-6• 25-30' Tan,dry,medium SAND,little gavel(SP) z8 _30 S-7 30-35' Tan,dry,medium SAND,little gravel(SP) 32 Well screen 34 36 S-8 35-40' Tan,dry,medium SAND,little gravel(SP) 38 Bentonite seal 40 S-9 40-43' Light brown,moist,medium SAND,little 42 fine gravel(SP) 4A End of Exploration @ 43' GSC Project Number: 000509 Checked By: �r„r\. Page 1 of 1 Notes: '-Sample taken at this depth GEOLOGIC SERVICES CORPORATION DRILLING LOG Hydrogeologists and Environmental Scientists MP-3 15 Bonazzoli Avenue,Hudson,MA 01749(978)-568-8740 Project Texaco Station tt 100083 Client: Equiva Services LLC Sketch Ma not to scale Location: 1140 Iyannough Road Hyannis,MA Total Depth: 43 feet Well ID: MP-3 Screen Diameter. 1.5 inch Water Level: -31 feet Slot Siu: 0.010 inch Screen Length: 10,2,2 feet Casing Diameter: 1.5 inch Type: PVC Type: PVC Casing Length: 25,37,41 feet Driller. Mike DeAfficas See Site Plan Top Elevation: 99.07 feet Drilling Company: Geosearch,Inc. McthotL Hollow Stem Auger GSC Inspector: SC/KS Date Start 3/21/01 Date End 3/21/01 Notes:Testing consists of PID heads ace response my ample Depth Well Key ID Depth Blows/6" Pen/Rec Sample (feet) Construction Description o Road box Gripper plugs S-1 04 Brown,dry,fine to medium SAND,some ND —2 Concrete coarse sand,some fine to medium gravel, little cobble(GM) 4 _6 Casing s S-2 8-10' Brown,dry,fine to medium SAND,some ND —10 fine gravel,little cobble(GP) 12 —14 S-3 14-16' Brown,dry,medium to coarse SAND, ND —16 some to little fine gravel(SW) la Native Material 20 S4 20-22' Brown,moist,medium to coarse SAND ND —22 (SP) 24 Bentonite seal 26 Filter sand S-Sfi 26-28' Brown,moist,medium to coarse SAND 1.2 —2s (SP) 0 2 Well screen S-6 32-34' Brown,wet,coarse SAND,some medium 6.2 4 sand(SP) 6 38 Bentonite seal S-7 3849 Brown,wet,coarse SAND,some medium 0.7 —40 sand(SP) a2 Endo Exploration @ 43' GSC Project Number. 000509 Checked By: p�l�n�1 Page 1 of 1 Notes: *-Sample taken at this depth ! Appendix E Soil Sample Analytical Results r ® APR 112001 ®ACCUTEST 04/05/01 Techiucal Report for Equiva Services GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M17430 Report to: Geologic Services Corp. 15 Bonazzoli Ave Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 6 Reza Tand Lab Director Certifications: MA(MA136) CT(PH-0109) NH(250293) NJ(59928) RI(A-71) ME(MA136) Results relate only to the items tested. This report shall not be reproduced,except in its entirety, without the written approval of Accutest Laboratories. Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•lel:508 481 6200•fax:508 481 7753•http://www.accutest.com APR 11 200' ®ACCUTEST Sample Summary Equiva Services Job No: M 17430 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID ........................... ........... ............... M174. 30 l:<03/20/01 10:25 DW 03/21/01 SO Soil 1VIP01 (30 31) ........................... M:1743.02 03/20/01 13:20 DW 03/21/01 SO Soil 5VI~Ot (30 3lJ Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508.481-6200•fax:508.481 7753•http://www.accutest.com MAJ ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MPO1 (30-31) Lab Sample ID: M17430-1 Date Sampled: 03/20/01 Matrix: SO-Soil Date Received: 03/21/01 Method: MADEP VPH Percent Solids: 96.9 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR4916.1) 1 04/03/01 JR n/a n/a GQR219 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND> 190 ug/kg 100-41-4 Ethylbenzene ND:...._...... 190 ug/kg 1634-04-4 Methyl Tert Butyl Ether ..ND............ : 190 ug/kg _........._..... .... ........................... 91-20-3 Naphthalene ND.,... » 190 ug/kg 108-88-3 Toluene Nb,,......... : 190 ug/kg m,p-Xylene ND 190 ug/kg 95-47-6 o-Xylene ,IUD;,,_, _ 190 ug/kg CS-C8 Aliphatics (Unadj.) :..ND' 3800 ug/kg C9- C12 Aliphatics (Unadj.) ND' :;:>::;;; ;: 3800 ug/kg C9-CIO Aromatics (Unadj.) ND ; :::>:::::;> 3800 ug/kg C5- C8 Aliphatics N11 3800 ug/kg C9-C12 Aliphatics ND; 3800 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 89i% < ; 70-130% 615-59-8 2,5-Dibromotoluene 96%:;;;::;.:;.:;:>:< 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•let:508 481 6200•tax:508 481 7753•http://www.acculest.com ii,.u'.i.�'�x�. 11 ®ACCUTEST 112001 Report of Analysis Page I of I Client Sample ID: SVE01 (30-31) Lab Sample ID: M17430-2 Date Sampled: 03/20/01 Matrix: SO- Soil Date Received: 03/21/01 Method: MADEP VPH Percent Solids: 96.7 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR4917.1) 1 04/03/01 JR n/a n/a GQR219 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 240 ug/kg 100-41-4 Ethylbenzene 240 ug/kg 1634-04-4 Methyl Tert Butyl Ether ; ;;:;:; <_ 240 ug/kg 91-20-3 Naphthalene ND ::; ;<< 240 ug/kg 108-88-3 Toluene ND 240 ug/kg m,p-Xylene ND 240 ug/kg 95-47-6 o-Xylene ND 240 ug/kg C5-C8 Aliphatics(Unadj.) ND ,.. 4700 ug/kg C9- C12 Aliphatics (Unadj.) ND,,,,,. 4700 ug/kg C9- C10 Aromatics(Unadj.) ND;;; _;>'< ; 4700 ug/kg C5-C8 Aliphatics IUD'::;:::;:;;:::;:; is 4700 ug/kg C9-C12 Aliphatics ND.. 4700 ug/kg g CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 99 ;> '; 70-130% 615-59-8 2,5-Dibromotoluene $;%.... ..... 70-130% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•lel:508 481.6200•lax:508 481 7753•hitp://www.accutest,com 011 A ����! ®ACCUTEST MPLE INFORMATION _,• U Aqueous 'soil U Sediment Other. El Satisfactory U Broken Leaking: -01 Aqueous ' N/A 1-100a,2,NOT UpH>2 U Leaking: - Soil or U N/A served in Methanol or ImL Methanol/g soil fr=Sediment 'Samples reed in Methanol: 'covering soil 0 not covering soil 1:1+/-25% ` - Samples reed in air-tight container. ❑Other ' Received on Ice U Reed at 4 Deg.C v Other reed at 2 deg C H ANALYTICAL RESULTS thod for Ranges:MADEP VPH 98-1 Client ID MP01 (30-31) SVE01(30-31) thod for Target Analytes:MADEP VPH 98-1 Lab ID M17430-1 M17430-2 H Surrogate Standards Date Collected 3/20/01 3/20/01 PID:2,5-Dibromotoluene Date Received 3/21/01 3/21/01 FID:2,5-Dibromotoluene Date Analyzed 4/3/01 4/3/01 Dilution Factor 1 1 %Moisture(soil) 3.1 3.3 ge/Target Analyte Elution Range Units Result RL Q Result RL Q djusted C5-C8 Aliphatics(1) N/A NO 3800 ND 4700 adjusted C9-C12 Aliphatics(1) N/A NO 3800 ND 4700 izene C5-C8 ug/kg NO 190 ND 240 ylbenzene C9-C12 ug/kg NO 190 NO 240 thy[-tent-butylether C5-C8 ug/kg ND 190 NO 240 )hthatene N/A ug/kg NO 190 ND 240 ene C5-C8 ug/kg NO 190 NO 240 p-Xylenes C9-C12 ug/kg NO 190 ND 240 ylene C9-C12 ug/kg NO 190 NO 240 C8 Aliphatic Hydrocarbons(1,2) N/A ug/kg NO 3800 NO 4700 C12 Aliphatic Hydrocarbons(1,3) NIA ug/kg ND 3800 ND 4700 C10 Aromatic Hydrocarbons(1) N/A ug/kg NO 3800 NO 4700 Surrogate%Recovery 96 98 Surrogate%Recovery 89 99 ate Acceptance Range 70-130% 1 70-130 Iydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 9C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons 'J"qualifier indicates an estimated value IRTIFICATION all QA/QC procedures REQUIRED by the VPH Method followed? v Yes U No-Details Attached all perfonnance/acceptance standards for required QA/QC procedures achieved? Q Yes ❑ No-Details Attached any significant modifications made to the VPH method,as specified in Sect 11.37 Q No ❑ Yes-Details Attatched st under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for ping the information,the material contained in this report is,to the best of my knowledge and belief,ax to and Mete. SIGNATURE: _ POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 04/05/01 Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•let:508 481 6200•tax:508 481 7753•hUp://www.accutest.com CHAIN OF CUSTODY ACCUTESTJOBIi: /7 495 Tech Center West,Bldg.I 11ACCUTESTMarlborough,MA 01752 ACCUTEST OUOTE R: � Tel:508-481-6200• Fax:508-481-7753 PQ CLIENT INFORMATION FACILITY INFORMATION a ANALYTICAL INFORMATION Consultants Name j Project Name Addres Site Location City, State ip Project No. �. Project Contact: /-2?, Phone p: `7 Fax"A: > -kiAFFiM Collection c Preservation Field ID/Point of Collection Date Time Sae led =m _ 5 vcz)I ? s/ f t /"Zc? TURNAROUND INFORMATIONM` i DATA DELIVERABLE INFORMATION COMMENTS/REMARKS F IN Now, ;.CStandardTurnaround Approved By: ❑ Commercial "A" ❑ FULL CLP t?Z. ❑ 7 Days EMERGENCY ❑ Commercial "B" ❑ State Forms ❑ 72 hr.EMERGENCY lBL,Full Deliverables ❑ Disk Deliverable Format ❑ 48 hr.EMERGENCY ❑ 24 hr.EMERGENCY Emergency T/A is for FAX or Lablink Data ❑ Other K Saman a Posseslon Including Courier DeliverY le CustodyMust be Do umented Below Each Time Samples C e> € � N Re =Isdampler Da Tiny: Received By: Rellnquiahe �y r) Date s: �5y� Received By: •inquiehed by Sam er• at I a,. Y� Recelved By: R linqulehed By: D eTl e: Received By: - 3. 4, 4. ®ACCUTEST 04/12/01 Techrlcal Report for P Equiva Services GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M17520 Report to: Geologic Services Corp. 15 Bona zzoli Ave Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 6 Reza Tand ab Director Certifications: MA(MA136) CT(PH-0109) NH(250293) NJ(59928) RI(A-71) ME(MA136) Results relate only to the items tested. This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•lei:508 481 6200•tax:508 481 7753•http://www.accutesi.com j ®ACCUTEST Sample Summary Equiva Services Job No: M 17520 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M17520 l ;; 03/21/01 10:45 KS 03/27/01 SO Soil AS01-AS-124' M17520 2 03/21/01 14:00 KS 03/27/01 SO Soil l ll'03 MP 328' _.. Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508.481.6200•tax:508 481 7753•http://www.accutest.com ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: ASOI-AS-1-24' Lab Sample ID: M 17520-1 Date Sampled: 03/21/01 Matrix: SO- Soil Date Received: 03/27/01 Method: MADEP VPH Percent Solids: 98.0 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5066.1) 1 04/11/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 170 ug/kg 100-41-4 Ethylbenzene ND 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether 170 ug/kg 91-20-3 Naphthalene ND 170 ug/kg 108-88-3 Toluene ND < 170 ug/kg m,p-Xylene ND; 170 ug/kg 95-47-6 o-Xylene ND' 170 ug/kg C5-C8 Aliphatics (Unadj.) 3400 ug/kg C9-C12 Aliphatics (Unadj.) ND 3400 ug/kg ...................:.. C9-.C10 Aromatics (Unadj.) hID;_.. 3400 ug/kg C5-C8 Aliphatics ND 3400 ug/kg C9-C12 Aliphatics ND 3400 ug/kg .........:................. CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene ,:.;:.;::.;:; 70-130% % 615-59-8 2,5-Dibromotoluene 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•let:508 481 6200•lax:508 481 7753•http://www.accutest.com i "Yi ia eACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MP03-MP-3-28' i Lab Sample ID: M 17520-2 Date Sampled: 03/21/01 Matrix: SO- Soil Date Received: 03/27/01 Method: MADEP VPH Percent Solids: 90.4 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5067.1) 1 04/12/01 JR n/a n/a GQR223 Run#2 MA-VPH List III CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 170 ug/kg 100-41-4 Ethylbenzene ND 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether NI3 170 ug/kg 91-20-3 Naphthalene ND 170 ug/kg 108-88-3 Toluene ND 170 ug/kg m,p-Xylene NID 170 ug/kg 95-47-6 o-Xylene ND 170 ug/kg C5- C8 Aliphatics (Unadj.) ND 3300 ug/kg C9- C12 Aliphatics (Unadj.) NI3 3300 ug/kg C9- C10 Aromatics (Unadj.) ND 3300 ug/kg C5- C8 Aliphatics ND ! 3300 ug/kg C9- C 12 Aliphatics „ND,.;,,,..;,:..:;.. 3300 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 1Q1:%.;: ;.i 70-130% 615-59-8 2,5-Dibromotoluene 1:02%< >: > 70-130% I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•let:508 481 6200•fax:508 481 7753•hup://www.acculest.com a 05 ®ACCUTEST MPLE INFORMATION Li Aqueous ' soil Lj Sediment LJ Other. KR - Satisfactory U Broken Leaking: Aqueous U N/ALJ O -�s NOT LJ pH>2 U Leaking: Soil or N/A LJserved in Methanol or mL Melhanollg soil vest 1P Sediment U Samples reed in Methanol: U4 covering soil not covering soil 21 1:1+/-25% I Lj Samples reed in air-tight container. ❑Other. Received on Ice Rec'd at 4 Deg.C 4 Other reed at 3 deg C H ANALYTICAL RESULTS od for Ranges:MADEP VPH 98-1 Client ID ASOI-AS-1-24' MP03-MP-3-28' od for Target Analytes:MADEP VPH 98-1 Lab ID M17520-1 M17520-2 Surrogate Standards Date Collected 3/21/01 3/21/01 ID:2,5-Dibromotoluene Date Received 3/27/01 3/27/01 ID:2,5-Dibromotoluene Date Analyzed 4/11/01 4/12/01 Dilution Factor 1 1 %Moisture(soil) 2 9.6 gerrarget Analyte Elution Range Units Result RL Q Result RL Q justed C5-C8 Aliphatics(1) N/A ND 3400 ND 3300 justed C9-C12 Aliphatics(1) N/A NO 3400 NO 3300 zene C5-C8 ug/kg ND 170 ND 170 lbenzene C9-C12 ug/kg ND 170 ND 170 1yl-tent-butylether C5-C8 ug/kg ND 170 ND 170 thalene N/A ug/kg ND 170 ND 170 ne C5-C8 ug/kg ND 170 ND 170 p-Xylenes C9-C12 ug/kg ND 170 ND 170 lene C9-C12 ug/kg ND 170 ND 170 Aliphatic Hydrocarbons(1,2) N/A ug/kg ND 3400 ND 3300 12 Aliphatic Hydrocarbons(1,3) N/A ug/kg ND 3400 ND 3300 10 Aromatic Hydrocarbons(1) N/A ug/kg ND 3460 ND 3300 urrogate%Recovery 88 102 urrogate%Recovery 88 101 gate Acceptance Range 70-130% 70-130% rocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons qualifier indicates an estimated value TIFICATION II QA/QC procedures REQUIRED by the VPH Method followed? �Yes U No-Details Attached 11 performance/acceptance standards for required QAIQC procedures achieved? 2 Yes No-Details Attached ny significant modifications made to the VPH method,as specified in Sect 11.3? Q No ElYes-Details Attatched underthe pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for ng the information,the material contained in this report is,to the best of my knowledge and belief,accu a and 4te. SIGNATURE' POSITION: Laboratory Director PRINTED NAME: Reza Tan DATE: 04/12/01 Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•fax:508 481 7753•htlp://www.accutest.com CHAINOF CUSTODY ACCUTEST JOB#: ®ACCI.(TEST 495 TECHNOLOGY CENTER WEST • BUILDING ONE ,,0,7-6 MARLBOROUGH,MA 01752 ACCUTEST QUOTE!: TEL:508-481-6200 • FAX:508-481-7753 CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES DW- DRINKING NL°Qjsf-.4 Sf�t'1I1C1�S �yS`t1 �G ' t . Ll D tG (xsc�S WATER NAME ^ PROJECT 14AME GW- GROUND 9nk-7 12.k� i- �-969�saa�_` ��\I " � WATER ADDRE LO ATION WW- WASTE . ILIA SO- WOATER CITY, Q STATE ZIPPROSE" T N SLUDGE ( !eft C 000Jet/ 1 OI- OIL SEND REPORT TO:- G- y L ^ `� LIO- OTHER PHONE# FAX# K�]�`, ✓�� .�1� LIQUID SOL-OTHER ACCUTEST COLLECTION x U. w PRESERVATION SOLID SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLED a D c o z BY: 2 m = z = = i LAB USE ONLY 17.00- --�lco s -1 - a 3 �� v,�r so xl m X, xi '; DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTSMEMARKS 14 DAYS STANDARD APPROVED BY: 'St STANDARD ❑ 7 DAYS RUSH O COMMERCIAL"B" ❑ 48 HOUR EMERGENCY ❑ DISK DELIVERABLE ❑ OTHER ❑ STATE FORMS w ` 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER SPECIFY _ 4, DATA UNLESS PREVIOUSLY APPROVED 4� Y . SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERY RELINQUISHED BY SAMPLER DATE TIME: RECEIVED BY: RELINOUISHE°�Y: DATE ME: RECEIVED BY: S«+c., r.�,e•/�' 3 /o f C ;.I 2. 1�U t: la.I'c�l' 2csf��' - ..- RELINQUISHED BY; DATE TIME: /,l;y RECEIVED BY. RELINQUIS D BY: AT TIME: RECEIVED BY: 3. _ 4. 4. RELINOUISHE15 BY: DATE TIME: RECEIVED BY: SEAL# PRESERVE WHERE APPLICABLE ON ICE _ TEMPERATURE ®ACCUTEST 04/12/01 APR 13 ^noj Technical Report for Equiva Services GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M17503 Report to: Geologic Services Corp. 15 Bonazzoli Ave Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 10 Reza Tand Lab Director Certifications: MA(MA136) CT(PH-0109) NH(250293) NJ(59928) RI(A-71) ME(MA136) Results relate only to the items tested. This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Massachusetts•495 Technology Center West•Building One•Marlborough.MA 01752•tel:508 481 6200•fax:508 481 7753•http://www.accutest.com _j ®ACCUTEST Sample Summary Equiva Services Job No: M 17503 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID ........................... M1:7503 1' 03/22/01 09:20 MM 03/2.6/01 SO Soil 1VIW1 i'(25 30') ........................... M1:7503 2` 03/22/01 11:50 MM 03/2.6/01 SO Soil PIiQ5 ........................... .M47503 3:::03/22/01 15:00 MM 03/26/01 SO Soil MW12,.(..5 30°J M17$03 4 xx : 03/23/01 09:25 MM 03/26/01 SO Soil IvtW3(2$ 30':): lull 7503 5 03/23/01 10:55 MM 03/26/01 SO Soil IvIWl4(25 27') Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•fax:508 481 7753•http://www.accutest.com ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MW11 (25-30') Lab Sample ID: M17503-1 Date Sampled: 03/22/01 Matrix: SO- Soil Date Received: 03/26/01 Method: MADEP VPH Percent Solids: 96.0 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5013.1) 1 04/09/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND,: 190 ug/kg 100-41-4 Ethylbenzene ND 190 ug/kg 1634-04-4 Methyl Tert Butyl Ether Nb. 190 ug/kg 91-20-3 Naphthalene ND 190 ug/kg 108-88-3 Toluene ND.... 190 ug/kg ........... _:.. m,p-Xylene NDs 190 ug/kg 95-47-6 o-Xylene ND: 190 ug/kg C5- C8 Aliphatics (Unadj.) ;ND..-- ;::;<; 3900 ug/kg C9- C12 Aliphatics (Unadj.) ,ND;;,,,„....,,;< 3900 ug/kg C9- C10 Aromatics (Unadj.) AID, _ ;I 3900 ug/kg C5- C8 Aliphatics ND; 3900 ug/kg C9- C12 Aliphatics ND 3900 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 102%........: 70-130% ......................... ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene IOQ% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•lei:508 481 6200•fax:508 481 7753•hnp://www.acculesi.com jr. ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MP2(25-30') Lab Sample ID: M17503-2 Date Sampled: 03/22/01 Matrix: SO - Soil Date Received: 03/26/01 Method: MADEP VPH Percent Solids: 93.5 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R5014.D 1 04/09/01 Q JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 180 ug/kg 100-41-4 Ethylbenzene .:..:: 180 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 180 ug/kg 91-20-3 Naphthalene ND 180 ug/kg 108-88-3 Toluene ND 180 ug/kg m,p-Xylene ND 180 ug/kg 95-47-6 o-Xylene ND 180 ug/kg C5-C8 Aliphatics Unadj. hID 3500 ug/kg C9-C 12 Aliphatics (Unadj.) ND 3500 ug/kg C9- C10 Aromatics (Unadj.) ND 3500 ug/kg CS-CS Aliphatics ND 3500 ug/kg C9-C12 Aliphatics ND 3500 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 101% 70-130% 615-59-8 2,5-Dibromotoluene :;93::%;::::::: 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•fax:508 481.7753•http://www.accutest.com ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MW12(25-30') Lab Sample ID: M 17503-3 Date Sampled: 03/22/01 Matrix: SO- Soil Date Received: 03/26/01 Method: MADEP VPH Percent Solids: 94.9 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5015.D 1 04/09/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene N..D :;.;_.;..::::;::> 210 ug/kg 100-41-4 Ethylbenzene IUD .......,,,< 210 ug/kg .:......................:.. ........................... 1634-04-4 Methyl Tert Butyl Ether ND:.;:.;:.;:.;..;:.; > 210 ug/kg 91-20-3 Naphthalene ND. 210 ug/kg 108-88-3 Toluene ND 210 ug/kg m,p-Xylene ND; 210 ug/kg 95-47-6 o-Xylene N...D ::;::;::;::;::; 210 ug/kg C5- C8 Aliphatics (Unadj.) :N.D. ,:.,:: 4200 ug/kg C9- C12 Aliphatics (Unadj.) ND:...............< 4200 ug/kg C9- C10 Aromatics (Unadj.) :,.ND.....:. 4200 ug/kg C5- C8 Aliphatics NDi:::;:: 4200 ug/kg C9- C12 Aliphatics ND 4200 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 95;%,:............ 70-130% 615-59-8 2,5-Dibromotoluene 9:T%:;:; 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough;MA 01752•tel:508 481.6200•fax:508 481 7753•hftp://www.acculest.com ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MW13 (25-30') Lab Sample ID: M17503-4 Date Sampled: 03/23/01 Matrix: SO - Soil Date Received: 03/26/01 Method: MADEP VPH Percent Solids: 96.0 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5016.D 1 04/09/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ............ .... ........................... 71-43-2 Benzene ND._...... 220 ug/kg 100-41-4 Ethylbenzene ND......._..:.;;;' 220 ug/kg ........................... 1634-04-4 Methyl Tert Butyl Ether ND 220 ug/kg 91-20-3 Naphthalene ND_.,. 220 ug/kg 108-88-3 Toluene ND 220 ug/kg m,p-Xylene ...N...D: ::::::;:.;.;:::; 220 ug/kg 95-47-6 o-Xylene ND 220 ug/kg C5- C8 Aliphatics (Unadj.) ;ND ;:;::;::;:; 4300 ug/kg C9-C12 Aliphatics (Unadj.) ND. ........;; '4300 ug/kg C9- C10 Aromatics(Unadj.) ND 4300 ug/kg C5- C8 Aliphatics NI) 4300 ug/kg C9-C12 Aliphatics ND 4300 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 9..6%.... 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 94% ;;;; 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•tax:508.481 7753•http://www.accutest.com eACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MW14 (25-27') Lab Sample ID: M17503-5 Date Sampled: 03/23/01 Matrix: SO- Soil Date Received: 03/26/01 Method: MADEP VPH Percent Solids: 95.8 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5017.D 1 04/09/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q _....... 71-43-2 Benzene ND 170 ug/kg 100-41-4 Ethylbenzene ND;:.;;:.;:.:::.;:...... 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND,..,,, >; 170 ug/kg 91-20-3 Naphthalene ND...: : ,,.: 170 ug/kg 108-88-3 Toluene ND >: 170 ug/kg m,p-Xylene N..D...._.__. 170 ug/kg 9547-6 o-Xylene ND 170 ug/kg C5-C8 Aliphatics (Unadj.) ND 3400 ug/kg C9- C12 Aliphatics(Unadj.) N..D 3400 ug/kg D C9- C 10 Aromatics(Unadj.) N 3400 ug/kg C5- C8 Aliphatics N...I3.. .:.;..;.,;;_:< 3400 ug/kg C9- C12 Aliphatics ND 3400 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 9I% < 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene 98%.....:::: 70-130% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•let:508 481 6200•fax:508 481 7753•hRp://www.acculest.com e ©""' ®ACCUTEST SAMPLE INFORMATION ON .„� Aqueous ' Soil Sediment Other: Satisfactory LJ Broken U Leaking: Aqueous ' N/A LJ Ored2s NOT LJpH>2 U Leaking: Soil or LJ N/A Userved in Methanol or mL ' di Sement 'Samples recd in Methanol: v covedn w� _ P 9 soil 0 not covering soil ❑' Samples rec'd in air-tight container: ❑ Received on Ice Rec'd at 4 De 9.C M4Other reed at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID MP2(25-30') MW11 (25-30') MW12(25-30') Method for Target Analytes:MADEP VPH 98-1 Lab ID M17503-2 M17503-1 M17503-3 VPH Surrogate Standards Date Collected 3/22/01 3/22/01 3/22/01 PID:2,5-Dibromotoluene Date Received 3/26/01 3/26/01 3/26/01 FID:2,5-Dibromotoluene Date Analyzed 4/9/01 4/9/01 4/9/01 Dilution Factor 1 1 1 %Moisture(soil) 6.5 4 5.1 Range/Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 3500 ND 3900 ND 4200 Unadjusted C9-C12 Aliphatics(1) N/A NO 3500 ND 3900 ND 4200 Benzene C5-C8 ug/kg ND 180 ND 190 ND 210 Ethylbenzene C9-C12 ug/kg ND 180 ND 190 ND 210 Methyf-tert-butylether C5-C8 ug/kg ND. 180 ND 190 ND 210 Naphthalene N/A ug/kg ND 180 ND 190 ND 210 Toluene C5-C8 ug/kg ND 180 ND 190 ND 210 m-&p-Xylenes C9-C12 ug/kg ND 180 ND 190 ND 210 o-Xylene C9-C12 ug/kg ND 180 ND 190 ND 210 C5-C8 Aliphatic Hydrocarbons(1,2) N/A ug/kg ND 3500 ND 3900 ND 4200 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ug/kg ND 3500 ND 3900 ND 4200 C9-C10 Aromatic Hydrocarbons(1) N/A ug/kg ND 3500 ND 3900 ND 4200 PID Surrogate%Recovery 93 100 97 FID Surrogate%Recovery 101 102 95 Surrogate Acceptance Range 70-130% 70-130% 70-130% 1-Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 2-C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 3-C -C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons 4-A V qualifier indicates an estimated value CERTIFICATION Were all QA/QC procedures REQUIRED by the VPH Method followed? U4 Yes Li No-Details Attached Were all perfomiancefacceptance standards for required QA/QC procedures achieved? Q Yes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.3? ❑' No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief a to and complete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 04/12/01 i Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508.481 6200•fax.508.481 7753•http://www.accutesl.com : 3 e ACCUTEST SAMPLE INFORMATION _ ' �� _ Aqueous Soil Sediment Other. '' Satisfactory LJ Broken Leaking: Aqueous ' N/A 9 -&NOT pH>2 Leaking: Soil or T7NiA served in Methanol or mL SedimentW Samples reed in Methanol: U4 covering sail not covering soil ❑' Samples rec'd in air-fight container. - ❑ ' Received on Ice U Rec'd at 4 Deg.C L10ther rec'd at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID MW13(25-30') MW14(25-27') Method for Target Analytes:MADEP VPH 98-1 Lab ID M175034 M17503-5 VPH Surrogate Standards Date Collected 3/23/01 3/23/01 PID:2,5-Dibromotoluene Date Received 3/26/01 3/26/01 FID:2,5-Dibromotoluene Date Analyzed 4/9/01 4/9/01 Dilution Factor 1 1 %Moisture(soil) 4 4.2 Range/Target Analyte Elution Range Units Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 4300 NO 3400 Unadjusted C9-C12 Aliphatics(1) N/A ND 4300 ND 3400 Benzene C5-C8 ug/kg ND 220 ND 170 Ethylbenzene C9-C12 ug/kg ND 220 ND 170 Methyl-tert-butylether C5-C8 ug/kg ND 220 ND 170 Naphthalene N/A ug/kg ND 220 ND 170 Toluene C5-C8 ug/kg ND 220 ND 170 m-&p-Xylenes C9-C12 ug/kg ND 220 ND 170 o-Xylene C9-C12 ug/kg ND 220 ND 170 C5-C8 Aliphatic Hydrocarbons(1,2) N/A ug/kg ND 4300 ND 3400 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ug/kg ND 4300 ND 3400 C9-C10 Aromatic Hydrocarbons(1) N/A ug/kg ND 4300 ND 3400 PID Surrogate%Recovery 94 98 FID Surrogate%Recovery 96 91 urrogate Acceptance Range 70-130% 1 70-130% -Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards elufing in that range -C5-08 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range -C9-C12 aliphatic Hydrocarbons exclude oonc of Target Analytes eluting in that range AND concentration of C9L10 Aromatic Hydrocarbons -A V qualifier indicates an estimated value 1,'ERTIFICATION ere alt QA/QC procedures REQUIRED by the VPH Method followed? Yes No-Details Attached ere all peRomrance/acceptance standards.for required QA/QC procedures achieved? Yes ❑ No-Details Attached ere any significant modifications made to the VPH method,as specified in Sect 11.3? E)No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for btaining the information,the material contained in this report is,to the best of my knowledge and belief a yrrate and mplete. (/V/// SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 04/12/01 Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•lel:508 481 6200•tax:508.481 7753•hnp://www.acculest.com ME3 CHAIN OF CUSTODY ACC;;;ST JOB#: ®ACCUTEST 495 TECHNOLOGY CENTER WEST - BUILDING ONE 17 MARLBOROUGH,MA 01752 ACCUTEST OUOTE C TEL:508-481-6200 - FAX-508-481-7753 ' CLIENT INFORMATION FACILITY INFOR`MArrTION ANALYTICAL INFORMATION MATRIX CODES . l� ,c SGrT`V s �C�t.. y c cL��J-I ajv0 V 7S 3 DW- DRINKING NAM rr PROJECT NAME �� WATER ✓1�ZZ1�l� ��d ✓� ,... /LLC. II 'i�l� s GW- GROUND WATER ADD�SO^ Y"I OI �7 LOCATION / ZSO WW- WASTE t� WATER CITY, .A^_/ n ESTATE ZIP PROJECT NO. SO- SOIL SL- SLUDGE !� OI- OIL SEND PHONE REPORT TO: UO• OTHER Q��—���J FAX# ��25 �'- �, LIQUID ` ION SOL-OTHER ACCUTEST COLLECTION x U. PRESERVAT SOLID us oc SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLED � O z 0 g w BY: o = _ _ = f `7 LAB USE ONLY 2-5-301 V"ul Sc o cizC—D X Z S Z?' =-e, 2 oG: �h-Y DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTS/REMARKS 14 DAYS STANDARD APPROVED BY: -STANDARD 7 DAYS RUSH §__,:OMMERCIAL"B" O 48 HOUR EMERGENCY ❑ DISK DELIVERABLE O OTHER ❑ STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES�H OSSESION,INCLUDING COURIER DELIVERY REUtIQUISHE BY DATE TI E: RECEIVED BY: REU (SHED Y: - D E TI E: ?� RECEIVED B 2l � 7 R LINOUISHED BY. DATE TIME: RECEIVED BY: REUNQUISHED BY: DATE ME: RECEIVED BY: 3. /4/10 1J� /,3� 3.�ff.� 4. 4. RELINQUISHED DATE TIME: RECEIVED 8 SEAL PRESERVE WHEREPP C LE ON ICE TEMPERATURE Appendix F Charts s Chart 1 Applied Vacuum at SVE-1 vs Flow Rate Texaco Service Station#100083 1140 Iyanough Road Hyannis, MA 14 12 10 0 2 8 _. v 6 4 2 0 0 20 40 60 80 100 120 140 160 180 200 Flow Rate(SCFM) Chart 2 Normalized Vacuum vs. Distance from SVE-1 @ 5"H20 Texaco Service Station#100083 1140 Iyanough Road Hyannis, MA 1 I� ♦MP-1 c ®MP-2 a 0.1 o MP-3 x MW-9 E � o ea x N 0.01 0 z Radius of Influence of 37 ft 0.001 0 5 10 15 20 25 30 35 40 45 50 Distance (ft) Chart 3 Normalized Vacuum vs. Distance from SVE-1 @ 10"H20 Texaco Service Station#100083 1140 Iyanough Road Hyannis, MA 1 a 0.1 ♦MP-1 ®MP-2 o o MP-3 .a x MW-9 m N x E 0.01 0 z Radius of Influence of 38 ft 0.001 0.0 5.0 10.0 15.0 20.0 25.0 30.0 35.0 40.0 45.0 50.0 Distance (ft) Chart 4 Normalized Vacuum vs. Distance from SVE-1 @ 1.3"H20 Texaco Service Station#100083 1140 Iyanough Road 'Hyannis,MA 1 a 0.1 ea E ♦MP-1 d N 0 0.01 z Radius of Influence of 33 ft 0.001 0 5 10 15 20 25 30 35 40 45 50 Distance (ft) Chart 5 Influent VOC Concentrations vs. Time Texaco Service Station #100083 1140 lyanough Road Hyannis, MA 900 800 700 f\ E n. a c 600 o R 500 d c 0 U 400 - NIJ C V O 300 th 5 "H20 10"H20 5"H20 Vacuum with 2 2 acuum wi Vacuum Vacuum Sparge @ 3 scfm Vacuum Helium Injection 200 with S are 6 scfm @ 6.5 scfm 100 0 0 20 40 60 80 100 120 140 160 180 200 220 Time(min) Chart 6 Groundwater Mounding vs. Time Texaco Service Station #100083 1140 lyanough Road Hyannis, MA 0.2 0.18 0.16 -- 0.14 5 "H20 Vacuum 10 "H20 5"H20 Vacuum with E Vacuum Sparge @ 3 scfm 0.12 c MP-1 0.1 MP-2 ea 0.08 If0 a 0.06 5 "H20 Vacuum with 5"H20 Vacuum with Sparge @ 6.5 scfm Helium Injection 0.04 0.02 -- 0 0 20 40 60 80 100 120 140 160 180 200 220 Time (min) Chart 7 Dissolved Oxygen Content vs. Time Texaco Service Station #100083 1140 lyanough Road Hyannis, MA 4.0 3.5 ---- 3.0 J E 2.5 +MP-1 °� —®--MP-2 2.0 O —6 MP-3 m > N 1.5 N G 1.0 0.5 5 "HZO Vacuum 10 "H2p 5"H20 Vacuum with 5 "H20 Vacuum with vacuum wi Helium Injection @ Vacuum Sparge @ 3 scfm Sparge @ 6.5 scfm 0.0 1 1 1 6 scfm 0 20 40 60 80 100 120 140 160 180 200 220 Time(min) Appendix G Air Sample Analytical results 06/07/01 hnc�.� epc�rt >' Equiva Services GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA Accutest Job Number: E91703 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 9 0 11CCpq y � < s Test results contained within this data package meet the requirements li;nc�ent J. Pugllese of the National Environmental Laboratory Accreditation Conference President and/or state specific certification programs as applicable. Certifications: NJ(12129),NY(10983),CA,CT,DE,FL,MA,MD,NC,PA,RI,SC,VA This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New Jersey 2235 Route 130■Dayton,NJ 08810 0 tel:732-329-0200■ fax:732-329-3499 0 http://www.accutest.com Accutest Laboratories Sample Summary Equiva Services Job No: E91703 GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA Sample COIIec ei3 » .. Matrix Client Number Date Time By Received Code Type Sample ID .................._....... E 5/ 8/01 10:00 DF 05/23/01 AIR Air ....... - OS/18/ 1 70 2 0 09:25 D F OS/�3/Ol AIR Air 1: Accutest-Laboratories Report of Analysis Page 1 of 3 Client Sample ID: AS + SVE Lab Sample ID: E91703-1 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 Q10989.1) 800 05/31/01 WG n/a n/a VQ415 Run#2 Q10997.1) 2000 05/31/01 WG n/a n/a VQ415 CAS No. MW Compound Result RL Units Q Result RL Units 71-43-2 78 Benzene 282ti0 160 ppbv <'>< ' 510 u /m3 ..................:.::... g 160PPby I290 690 u /m3100-41-4 106 Ethylbenzene 297(1Q 1634-044 88 Methyl Tert Butyl Ether 4000 PPby 14000 u /m3&8 p 4091-20-3 128 Naphthalene 160 PPby '><0 ug/m32Q Q 15000 ug/m3108-88-3 92 Toluene 004 :j 4000 ppbv >7 17000_ u /m3106 m, -X lene 109004 a > 4000 PPby 47200fl a ' ' 17000 ug/m3 195-47-6 106 o-X lene 3OU 4000 ppbv 1330-20-7 106 Xylenes(total) 149000: 4000 by f46000 >' : 17000 u /m3 ...........:........... PP ........................... g CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 460-00-4 4-Bromofluorobenzene It %< 88i%< > » 70-130% ......................... ......................... CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q Pentane 5.34 724f3: ;>; ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 5.48 2 ...... ppbv J ........................... ........................... C5-C8 Aliphatic 5.64 1IOQ < :< ppbv J ......................:.... C5-C8 Aliphatic 5.75 3f)ot�> > i>` ppbv J .......::.................. ........................... C5-C8 Aliphatic 6.11 :10(3;':; ' : ppbv J C5-C8 Aliphatic 6.54 41? :ppbv J C5-C8 Aliphatic 6.65 41 >> >< ppbv J .::........................ ........................... C5-C8 Aliphatic 6.85 5O13 ;>;» <::ppbv J ........................... ........................... C5-C8 Aliphatic 7.34 79Q(}: ;; ppbv J ..:...:..............:..... ........................... ........................... C5-C8 Aliphatic 7.48 22Q0:< " ppbv J ...:....::.:............... ........................... C5-C8 Aliphatic 7.82 8000 ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 7.96 #)0(3 >'< =>:' ppbv J ........................... ........................... CS-C8 Aliphatic 8.02 2GQt ; ;< ppbv J :.......................... ........................... ........................... C5-C8 Aliphatic 8.14 :> ppbv J C5-C8 Aliphatic 8.24 1200>s. ppbv J; ........................... ........................... C5-C8 Aliphatic 8.43 2Q0;i< : ppbv J ........................... C5-C8 Aliphatic 8.5730;>;: >>; :: ppbv J C5-C8 Aliphatic 8.68 56(?4< ppbv J C5-C8 Aliphatic 8.75 3;$ti0 ; = ; ppbv J C5-C8 Aliphatic 8.95 €1OQ <> ppbv J ...:....................... ........................... C5-C8 Aliphatic 9.36 1300 ; ppbv J .........:................. ........................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 2 of 3 Client Sample ID: AS + SVE Lab Sample ID: E91703-1 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q ........................... ........................... C5-C8 Aliphatic 9.57 2;i ppbv J C5-C8 Aliphatic 9.67 2504 ppbv J ........................... C5-C8 Aliphatic 9.72 b7Q( ppbv J C5-C8 Aliphatic 9.92 3G044 >>''»ppbv J ....:..:................... ........................... ........................... C5-C8 Aliphatic 10.00 200t '; <; ` ppbv J C5-C8 Aliphatic 10.20 704t <' ppbv J ..........:................ ........................... ........................... C5-C8 Aliphatic 10.28 5300 ppbv J C5-C8 Aliphatic 10.45 950(3 ppbv J ........................... ........................... C5-C8 Aliphatic 10.54 >1a0i >> `ppbv J C5-C8 Aliphatic 10.64 6Qt? <'; ppbv J ......:.................... ........................... C5-C8 Aliphatic 10.88 Slf 'i >> ppbv J C5-C8 Aliphatic 10.95 24 ppbv J ........................... ........................... C5-C8 Aliphatic 11.01 170(6` ppbv J C5-C8 Aliphatic 11.09 (00 ppbv J .........:.:............... ........................... ........................... C5-C8 Aliphatic 11.16 1604 ; ppbv J C5-C8 Aliphatic 11.25 4;W. ppbv J ......:................... ........................... .......................... C5-C8 Aliphatic 11.34 ;<1000(1 ppbv J C5-C8 Aliphatic 11.68 180( < ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 11.74 10(1 ppbv J ........................... ........................... C5-C8 Aliphatic 11.94 120d4< i> ppbv J .......::.................. ........................... ........................... C5-C8 Aliphatic 12.02 190i ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 12.26O(;> ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 12.35 T: 00 ; <; ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 12.46 3 ppbv J ........................... ........................... C5-C8 Aliphatic 12.56 42000< ppbv J C5-C8 Aliphatic 12.88 ..1.....OG..i....;.... > Pv I; ... . ................................ C5-C8 Aliphatic 12.97 I4000<< ppbv J C5-C8 Aliphatic 13.02 10 ppbv J ....................... ........................... .... .............. C5-C8 Aliphatic 13.11 270Q> > ' >ppbv J C5-C8 Aliphatic 13.20 1QOtl> ;> ; ppbv J C5-C8 Aliphatic 13.3917(H)`<' ; ppbv J C5-C8 Aliphatic 13.52 .10.i 0;; ppbv J C5-C8 Aliphatic 13.66 19Q0:: :>`<:i ppbv J C5-C8 Aliphatic 13.72 $ Q € »< ppbv J C5-C8 Aliphatic 13.78 I :D( »;> ppbv J C5-C8 Aliphatic 13.85 1GQ ; > ppbv J ........................... C5-C8 Aliphatic 13.94 11U00; ;> ; ppbv J C5-C8 Aliphatic 14.02 2200 < ; ; ;ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 14.15 4600ii <?> ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 14.28 850 <; » ; ppbv J ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 3 of 3 Client Sample ID: AS + SVE Lab Sample ID: E91703-1 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/O1 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140,Iyanough Road, Hyannis, MA CAS No. Tentatively Identified Compounds R.T. Est. Cone. Units Q ........................... ........................... C5-C8 Aliphatic 14.34 13t)Q ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 14.45 10f1;> ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 14.62 Z0(3< < ::ppbv J C5-C8 Aliphatic 14.78 100 ; >>; ppbv J ........................:.. ........................... ........................... C5-C8 Aliphatic 14.97 49pQ<: '< ppbv J C5-C8 Aliphatic 15.10 $(S() ppbv J .......................... ........................... ........................... C5-C8 Aliphatic 15.19 :1.3i ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 15.34 1f00;_ = ppbv J .:......................... ........................... ........................... C5-C8 Aliphatic 15.91 360Q< _ ppbv J CS-CS Aliphatic 16.13 1 ;; > ppbv J ........................... ........................... ........................... C9-C12 Aliphatic 16.60 :I7(l( ;> ppbv J C9-Cl0 Aromatic 17.09 18 ppbv J C9-C12 Aliphatic 17.26 12Qt)<< < ; ppbv J C9-C 12 Aliphatic 17.50 1 ( ` ppbv J ........................... ........................... ............ C9-C 10 Aromatic 17.82 42Q(1< >< ppbv J ..::....................... ........................... ........................... C9-C 10 Aromatic 17.98 1 ( ;< ppbv J ........................... ........................... ........................... C9-C 10 Aromatic 18.04 6"— ppbv J C9-C10 Aromatic 18.16 7P..0 <; ppbv J C9-C12 Aliphatic 18.23 1_1(f(1 <i ppbv J C9-C10 Aromatic 18.43 470O;; ; ; ppbv J C9-C 10 Aromatic 18.78 1;50t)(li<i ` ppbv J ........................... ........................... C9-C10 Aromatic 19.46 20 ; ; ;ppbv J ........................... ........................... C9-C10 Aromatic 19.77 ls5OQ; ;; ppbv J Total C5=C$ lipliaties 42OW PPbv `fafal:CS > i h�itTCs> < ... >< ; . .. 2fl6000 r> II /m3 v .......................... `';<< C =:C>12*A* l alics<<>> >>><> ................... >><< >>>< 1 `i>>> > »<>u /m3 Olal.. 1:.;;:;;.;:.;:.;:.::.::.::.:::.;:.: .;;.... g T1'oala1 TI > to . . ( i :::....... ppb90 Arb SD :.0 . 3(6af ug/m 3t ...#al> COAritint . .< . ...........................1........................s.............................. .... .. ......................... ...... .....I.... .............. ........: ................... ... .....1.............. .>> 13214 PPbvVIe : ::: 6 .::::.... . ... > ........................... , .....(a)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 3 Client Sample ID: SVE Lab Sample ID: E91703-2 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA i File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 Q10990.1) 4000 05/31/01 WG n/a n/a VQ415 Run#2 Q10998.1) 8000 05/31/01 WG n/a n/a VQ415 CAS No. MW Compound Result RL Units Q Result RL Units ........................... ........................... .................... ........................... 71-43-2 78 Benzene 30' 800 ppbv 1:02()DO ; 2600 ug/m3 3500 u /m3800 >>'100-4 -4 106 Eth Ibenzene '3fl?d PPby 2900 u /m31.634-04-4 88 Methyl Tert Butyl Ether 7 7-50 80 PPby 8 by F1 ... 4200 u /m3 91-20-3 128 Naphthalene Tit) 00 pp .:N..,:::.:::.:::.::.... g ............ ........................... 108-88-3 92 Toluene 3180O0;<a1600 ppbv fC1QOE)Oas ; 6000 ug/m3 106 m -X lene 98( 1 > < > 800 byt30O0 >_ 3500 u /m3 �P Y PP g - 14 >< > 35W u /m3 95 47 6 106 o Xylene 32 0:.. 800 ppbv.. 0000 g 1330 20 7 106 Xylenes(total) 132000; 800 ppb 5.:2(Q(l..,:._:::. g CAS No. Surrogate Recoveries Run#1 Run#2 Limits 460-00-4 4-Bromofluorobenzene 9U 00......... 0° 70-130 CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q 70000 C5-C8 Aliphatic 5.33 ppbv J ......... ........................... ........................... C5-C8 Aliphatic 5.47 170UOi<i ppbv J C5-C8 Aliphatic 5.63 91{)O. ' ppbv J .................:......... ........................... ........................... C5-C8 Aliphatic 5.73 '26M.ii << ppbv J {C5-C8 Aliphatic 5.93 1 ppbv J C5-C8 Aliphatic 6.09 18000i>> > ppbv J ppbv J C5-C8 Aliphatic 6.53 4200 ........................... ........................... C5-C8 Aliphatic 6.59 (30 ppbv J ........................... ........................... C5-C8 Aliphatic 6.63 3U0 ; '> ppbv J C5-C8 Aliphatic 6.83 000 <> < ppbv J .....:............:........ C5-C8 Aliphatic 6.93 120Q0 ppbv J ........................... C5-C8 Aliphatic 7.32 ?bfl <> <ppbv J C5-C8 Aliphatic 7.4600 r>» ppbv J C5-C8 Aliphatic 7.94 1000 >``> ppbv J 23fl00 C5-C8 Aliphatic 8.01 ;>; ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 8.12 1?0OI; ; >< ppbv J C5-C8 Aliphatic 8.22 ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 8.41 190 (1:; i < ppbv J C5-C8 Aliphatic 8.55 560b ;» ppbv J ......:.................... ........................... ........................... C5-C8 Aliphatic 8.66 :5:10(1Q ji :ppbv J C5-C8 Aliphatic 8.73 3:G000; ;<>_ ppbv J ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 2 of 3 Client Sample ID: SVE Lab Sample ID: E91703-2 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q C5-C8 Aliphatic 9.35 180(if : ::< ppbv J C5-C8 Aliphatic 9.55 ;42oQ> ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 9.65 35Qf1 ppbv J C5-C8 Aliphatic 9.71 9GOE1> ; ppbv J ........:..:............... ........................... ........................... C5-C8 Aliphatic 9.89 _5-m::i: ;: ;ppbv J C5-C8 Aliphatic 9.98 310. ppbv J _..:..:............ ........................... C5-C8 Aliphatic 10.18 S90f)fl;:; ;; ;ppbv , J C5-C8 Aliphatic 10.29 69(i .........:..::ppbv J ..:::..::.................. _. C5-C8 Aliphatic 10.43 ppbv J C5-C8 Aliphatic 10.52 1SObQ< ;; <; ppbv J I2flf(If?:>C5-C8 Aliphatic 10.63 ppbv J C5-C8 Aliphatic 10.77 3704>:; >;: :> ppbv J C5-C8 Aliphatic 10.86 73t)a > ppbv J C5-C8 Aliphatic 10.9370p1` ppbv J C5-C8 Aliphatic 10.99 2lOQQ. ppbv J C5-C8 Aliphatic 11.07 S41Q ppbv J C5-C8 Aliphatic 11.14 :2-5, : < <;: ppbv J C5-C8 Aliphatic 11.23 55:0(3>::::<;;';;<ppbv J C5-C8 Aliphatic 11.32 1 «>: ;:ppbv J C5-C8 Aliphatic 11.66 >ti8 : :<« :ppbv J ......................:.... ........................... C5-C8 Aliphatic 11.93 17000; ppbv J C5-C8 Aliphatic 12.00 29000. > i ppbv J ......... ........................... ........................... C5-C8 Aliphatic 12.12OQ[1 ppbv J C5-C8 Aliphatic 12.25 711(3:: ; :i:> ppbv J ...........:............... ........................... ........................... C5-C8 Aliphatic 12.45 42Q4)> ;;: < ;ppbv J C5-C8 Aliphatic 12.53 59000; :< ppbv J ........................... ........................... C5-C8 Aliphatic 12.81 200W :: : ppbv J C5-C8 Aliphatic 12.95 21{3 (1 ;' ;ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 13.01 1200f1 ppbv J C5-C8 Aliphatic 13.10 3S0(`: ;; ;: ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 13.18 2$f100..... >>i ppbv J C5-C8 Aliphatic 13.37 94fl...... ppbv J ................. ......:... ........................... ........................... C5-C8 Aliphatic 13.51 .I6:000 « ppbv J C5-C8 Aliphatic 13.65 ;I;Q » ppbv J C5-C8 Aliphatic 13.84 22{ ;; <ppbv J C5-C8 Aliphatic 13.92 ;1a0t�; >;; ppbv J C5-C8 Aliphatic 14.02 2..2Q0:;.;;:::;::;.; ppbv J C5-C8 Aliphatic 14.14 6 00.......... >: ppbv J C5-C8 Aliphatic 14.33 2000 ppbv J C5-C8 Aliphatic 14.44 27fl(1 ppbv J ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 3 of 3 Client Sample ID: SVE Lab Sample ID: E91703-2 Date Sampled: 05/18/O1 Matrix: AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q C5-C8 Aliphatic 14.61Ot ppbv J C5-C8 Aliphatic 14.77 ppbv J :.......................... ........................... ........................... C5-C8 Aliphatic 14.96 b50Cfi;< ';;:::::ppbv J C5-C8 Aliphatic 15.91 ' $ <>> ppbv J ........................... ........................... ........................... C9-C10 Aromatic 17.08 ppbv J C9-C10 Aromatic 17.81fi> ppbv J ........................... ........................... ........................... C9-C10 Aromatic 17.98 IQt `;< ppbv J C9-C10 Aromatic 18.03 >�4 >c< << ppbv J ........................... ........................... ........................ C9-C10 Aromatic 18.16 : OQ<>< ppbv J ........................... ppbv J C9-C10 Aromatic 18.43 340( ........................... ........................... ........................... C9-C 10 Aromatic 18.78 $OQ ;ppbv J : `''tics » > » <_> by I�................................................. PP Total::CBA13;.>;<> es'<` s> i> > » > 57. u /m3 ;: .... :. g Tot 9'_..1 «Mattes:.:;:::::;:<;;:>:; »>::»>:<::;:::»>::»:<:: (i >» » » > b v P . ..:...........:........._ t< > <>>> » > u /m3 :::::.:::::.:::::::::,...........::::::::::::. g 10 PP by .`e > : :.a9CltAe u /m 3Q ... »'I`> e :«Toa '?y >` '»>>a. : PPby 13179( 3 .... . f:.::: .... ......(a)Result is from Run#2 (b)No peaks found for Total C9-C12 Aliphatics ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ® °7" .� 495 TECHNOLOG NTERINVEST MARLBOROUGH,fA 4 01752 ACCUTFST QUOTE as TEL:508-481-62W • Five 50"81.7753 CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES eO�o�i c S RVi�eS Dw- 0O2Po 12 4Td • 1(„! � AGv ,S�IC�/i .. SLAi?oJ *-}= DATER d WATER NAME ^' o T 04ECT tLkME ^ OW- GROUND WArER go WW- WASTE ZRESS �QCATIONWATER r►'ll4 dl 1 N Y/! /it/iS' JA1�4. :L- say Cl� ,c STATE 21P �,�Q.1��tCT 1i ���� _ O�� OI- OIL OGE �C� ;) LIG. OTHER SEND REPORT TO: LIQUID PHONE 4 o^ yJ FAX IY —S-6 B l q 3 5o/ _T SOL•OTi1HR ACCUTE8T COLLECTION PRESERVATION C SOLID SAMPLE* FIELD ID/POINT OF COLLECTION DATE TIME SA BPY�..ED I LAB USE ONLY ISVE 1Z ( i } r DATA TURNAROUND INFORMATION DATA DELIVERA13U-INFORMATION COMMENT$JREMARKS 14 DAYS STANDARD APPROVED BY: kSTANDARD O 7 DAYS RUSH CT COMMERCIAL"B" O 48 HOUR EMERGENCY C:I DISK DELIVERABLE O OTHER O STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERY REL SHED BY SAMPLER: DATE TIME: RECEIVp BY: RELINO ED Y: DAT TIM i RECEIVED Ir RE OUISHE BY: DATE TIME: RECOXED BY: RELINOUISHID BY. TI L WAUVED or. LAELINQUISHEdW. 3. 4. DATE TI . REC ED BY: SEAL• �IIEBERYELAMER APPLICABLE ON ICE TIMPBRATNRB 5. ❑ ❑ C Tom' umm" Ltinlw ur L U 1'UI) Y ACCUTEBTJOB#: } ®ACCUTEST 495 TECHNOLOGY CENTER WEST • BUILDING ONE MARLSOROUGH,MA 01752 ACCUTEST OUOTE# TEL:508-481-6200 • FAX.,608-481-7753 CLIENT INFORMATION':: FACILITY INFORMATION ANALYTICAL INFORMATIONil MATRIX CODES Oq 1 G p2t/iceS ra a-PC,ARTd„J Dw- DRINKI k', -G Sc�rA� �Se�cylcc_ S�--�:� }�g3 NAME /�� PRO(�ECT AME I' OW• ROUNII ' 15e�lA?? n�l ✓� ! 'lo YnA140j QOIO�� 4ADDRESS O� CATION WW- WAS ATER <!SO- SOIL 'r STATE ZIP JwECT N0. / �j L) c 1IC� r.4.__�v� ,��r7 `� SL- SLUD�iE I'. OI• OIL SEND REPORT TO: G L10- OTHER UOUID..".: PHONE# �- o- qJ FAX# / Q--ST 9 - 7 3/ / So SOL•OTHER. ACCUTEST COLLECTION H PRESERVATION Q• SOLID W SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLED ' LAB USE ONII BY: E -LS-� teoa Ap .a'. va _.. DATA TURNAROUND INFORMATION ,: DATA DELIVERABLE INFORMATION COMMENTS/REMARKS 9� 14 DAYS STANDARD APPROVED BY: IkSTANDARD `: ❑ 7 DAYS RUSH O" COMMERCIAL"B" O 48 HOUR EMERGENCY O DISK DELIVERABLE O OTHER O STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERY m*LP'rt: RELI ISHED BY SAMPLER: DATE TIME: RECEIVED BY: D��i RELINO SHED Y. DAT TIM : RECEIVED BY: 1• S=�Q•d 1. te_ 2. O1 *cc,2. RErTNOUISHED BY: DATE TIME: RECEIVED BY: RELINQUISHED BY; 0n TI E: RECEIVED BY: 3. 3. 4, 4- RELINOUISHEO BY: DATE TIME: RECEIVED BY: SEAL f PRESERVE WHERE APPLICABLE ON ICE TEMpERATURi,." i Jun-07-01 02:25pm From- T-333 P.01/07 F-319 URI ®ACC . 2235 Route 130, Building 8, Dayton, New Jersey 08810 i WWW.A000TEST.COM j FAX TRANSMISSION Date: 6 1 �101 COVER PAGE Number of pages,including:over: T0: FROM: Marie Rutsky _LL4 COMPANY: CAS C MA COMPANY: ACCUTEST LABS Phone: Phone: 1732)329-0200 finl)) Fax: `�'1 _ 5(04-9 3 f Fax: (732)329-349s 13480 Email: marier@accuiest.com URGENT X FOR REVIEW _REPLY ASAF Remarks: Accutest cannot be held accountable for the security of the data once media containing the data has left the possession or control of Accutest. Analytical data transmitted via facsimile should be conside►ad preliminary. I N,-w jer.r •F(CSh Ponds Corporate Village•Bv4ding 0.2235 Route 130•Dayton,NJ 08810•tel:732.329.0200•lax.732.3253499•mrp!/www.accu1es1.0om Jun-07-01 01:25pm From- T-333 P.02/07 F-319 Aecutest Laboratories Report of Analysis Page 1 of 3 Client Sample M- AS + SVE Date Sampled. 05/18/01 Lab Sample ID: E91703-1 bate Received: 05/23/01 Matrian AIR-Air Method: TO-14/TO-I5 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road.Hyannis,MA file ID DF Analyzed By prep Date h'rep Batch Analytical Batch Run N1 Q10989.1) 800 05/31/01 WG a/a Ida VQ415 Run f/2 Q10997.D 2000 05/31/01 WG n/a Ida VQ415 CAS No. MW Compound Result RL Units Q Result RL 17ttits 71-43-2 78 Benzene 28200 160 ppbv 90000 510 ug/m3 100-41- 106 Ethylbenzene 29700 160 ppbv 129000 690 ug/m3 1634 04-4 88 Methyl Ten Butyl Ethdr 729003 4000 ppbv 2620002 14000 ugtm3 9120-3 128 Naphthalene 2800 160 ppbv 14600 840 ug/m3 108-88-3 92 Toluene204000 a 4000 ppbv 768000 a 15000 ug/m3 106 m,p-Xylene 1090002 4000 ppbv 472000 a 17000 ug/m3 95-47-6 106 o-Xylene 39400 a 4000 ppbv 171000 a 17o00 ug/m3 1330-20-7 106 Xylenes(total) 149000 a 4000 ppbv 6460001 17000 u9/m3 CAS No. Surrogate Recoveries Run# 1 Run#2 14mits 460-00-4 4-Bro1nofluoroben7ene 101% 88% 70-130% CAS No. Tentatively Identified Compounds R.T. Est. Conc. 'Units Q pew 5.34 7200 _ppbv J CS-C8 Aliphatic 5.48 2100 ppbv J C5-C8 Aliphatic 5.64 1100 ppbv J C5-C8 Aliphatic 5.75 3000 ppbv J C5-C8 Aliphatic 6.11 2100 ppbv J CS-C8 Aliphatic 6.54 470 ppbv J C5-C8 Aliphatic 6.65 410 ppbv J C5-C8 Aliphatic 6.85 5900 ppbv J CS-C8 Aliphatic 7.34 7900 ppbv J C5-C8 Aliphatic 7.48 2200 ppbv J CS-C8 Aliphatic 7.82 8000 ppbv J CS-CS Aliphatic 7.96 2000 ppbv J C5-C8 Aliphatic 8.02 2600 ppbv J C5-C8 Aliphatic 8.14 2000 ppbv J CS-C8 Aliphatic 8.24 1200 ppbv J C5-C8 Aliphatic 8.43 2200 ppbv J CS-C8 Aliphatic 8.57 630 ppbv J C5-C8 Aliphatic 8.68 5600 ppbv J CS-C8 Aliphatic 8.75 3800 ppbv J C5-C8 Aliphatic 8.95 1000 ppbv J CS-C8 Aliphatic 9.36 13000 ppbv J ND = Not detected J = indicates an e:timated value RL Reporting Limit B = Indicates analyze found in associated method blank E =Indicates value exceeds calibration range N = Indicatea pre;.umptive evidcncc of a compound Jun-07-01 02:26pm From- T-333 P.03/07 F-319 Accuwt Laboratories Report of Analysis Page 2 of 3 Client Sample ID: AS + SVE Lab Sample Im: E91703-1 Date Sampled: 05/18/01 Matri= AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Pement Solids: n/a Project: GSCMAx:96925028 1140 Iyanough Road,Hyanmis.MA CAS No. Tentatively Identified Compounds R.T. Est.Conc. Units Q CS-0 Aliphatic 9.57 2900 ppbv J C5-C8 Aliphatic 9.67 2500 ppbv J C5-C8 Aliphatic 9.72 6700 1>pbv J C5-C8 Aliphatic 9.92 36000 1>pbv J C5-C8 Aliphatic 10.00 20000 ppbv J C5-C8 Aliphatic 10.20 37000 ppbv J C5-C8 Aliphatic 10.28 5300 I)pbv J C5-C8 Aliphatic 10.45 9500 1)pbv J C5-C8 Aliphatic 10.54 11000 ppbv J C5-C8 Aliphatic 10.64 66000 1)pbv J C5-C8 Aliphatic 10.88 5100 ]?pbv J CS-C8 Aliphatic 10.95 28000 ]?pbv J CS-C8 Aliphatic 11.01 17000 ]?pbv J C5-C8 Aliphatic 11.09 4000 !ppbv J C5-C8 Aliphatic 11.16 1600 .ppbv J C5-C8 Aliphatic 11.25 4700 "?pbv J CS-C8 Aliphatic 11.34 10000 ppbv J C5-C8 Aliphatic 11.68 18000 ppbv J C5-C8 Aliphatic 11.74 1200 ppbv J C5-C8 Aliphatic 11.94 12000 ppbv J C5-C8 Aliphatic 12.02 19000 ppbv J C5-C8 Aliphatic 12.26 4700 ppbv J C5-C8 Aliphatic 12.35 1400 ppbv J C5-C8 Aliphatic 12.46 3000 ppbv J C5-C8 Aliphatic 12.56 42000 ppbv J C5-C8 Aliphatic 12.88 1600 ppbv J CS-C8 Aliphatic 12.97 14000 ppbv J C5-C8 Aliphatic 13.02 8100 ppbv J C5-C8 Aliphatic 13.11 2700 ppbv J C5-C8 Aliphatic 13.20 19M ppbv J CS-C8 Aliphatic 13.39 4700 ppbv J C5-C8 Aliphatic 13.52 11000 ppbv J C5-C8 Aliphatic 13.66 1900 ppbv J C5-C8 Aliphatic 13.72 850 ppbv J C5-C8 Aliphatic 13.78 1300 ppbv J C5-C8 Aliphatic 13.85 1600 ppbv J CS-C8 Aliphatic 13.94 11000 ppbv J CS-CS Aliphatic 14.02 2200 ppbv J C5-C8 Aliphatic 14.15 4600 ppbv J C5-C8 Aliphatic 14.29 850 ppbv J ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exccc&calibration range N = Indicates premniptive evidence of a compound Jun-07-01 02:26pmm From- T-333 P.04/07 F-319 Accutest Laboratories Report of Analysils Page 3 of 3 Client Sample ID: AS + SVE Lab Sample ID: E91703-1 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received. 05/23/01 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis,MA CAS No. Tentatively Identified Compounds R.T. Est. Cone. 'Units Q CS-CS Aliphatic 14.34 1300 ppbv J O-CS Aliphatic 14.45 1900 f pbv J C5-C8 Aliphatic 14.62 2700 I-pbv J C5-C8 Aliphatic 14.78 1600 lTbv J C5-C8 Aliphatic 14.97 4900 ppbv J C5-C8 Aliphatic 15.10 800 1►pbv J C5-C8 Aliphatic 15.19 1300 1-pbv J C5-C8 Aliphatic 15.34 1600 1,pbv J C5-CS Aliphatic 15.91 3600 1,pbv J C5-C8 Aliphatic 16.13 1000 ppbv J C9-C12 Aliphatic 16.60 1700 ppbv J C9-CIO Aromatic 17.09 1800 1)pbv J C9-C12 Aliphatic 17.26 1200 ppbv J C9-C12 Aliphatic 17.50 1100 ppbv J C9-CIO Aromatic 17.82 4200 ])pbv J C9-C10 Aromatic 17.99 16000 13pbv J C9-C10 Aromatic 18.04 6000 I?pbv J C9-C10 Aromatic 18.16 7100 1?pbv J C9-C12 Aliphatic 18.23 1100 I?pbv J C9-C10 aromatic 18.43 4700 iapb v J C9-C10 Aromatic. 18.79 15000 ppbv J C9-C 1 O Aromatic 19.46 2700 ppbv J C9-C10 Aromatic 19.77 1500 ppbv J Total C5-C8 Aliphatics 542000 ppbv Total C5-C8 Aliphatics 2060000 ag/m3 Total C9-C12 Aliphatics 5100 ppbv Total C9-C12 Aliphatics 31100 ug/m3 Total C9-C 10 Aromatics 59000 ppbv Total C9-C10 Aromatics 306000 tWm3 Total TIC.Volatile 613210 ppbv (a)Result is from Run#2 ND _ Not detected J =Indicates an essimated value RL = Reporting Limit 13 = Indicates analyte found in associated method blank E = Indicates value exceeds calibration Mgt N = Indicates premniptive Evidence of a compound Jun-07-01 02:21pm From- T-333 P.05/07 F-319 re Accutast Labotorizs Report of Analysis Page 1 of 3 Client Sample ID: SVB Lab Sample ID: E91703-2 Date Sampled 05/18/01 Matrix: AIR-Air Date Received: 05/23/01 Method: TO-141TO-15 Percent Solids: u/a Project; GSCMAH-96925028 1140 Iyanough Road,Hyannis,MA Mile ID DF Analyzed By prep Date prep Batch Analytical Batch Run 1 Q10990.D 4000 05/31/01 WO n/a »/a VQ415 Run g2 Q10998.D 8000 05/31/01 WO n/a »/a VQ415 CAS No. MW Compound Result RL Units Q Result RL Units 71-43-2 78 Benzene 31900 800 ppbv 102000 2600 ug/m3 10041-4 106 Ethy%enzene 30700 80o ppbv 133000 3500 ug/m3 1634-04-4 88 Methyl Ten Butyl Ether 79300 800 ppbv 285000 2900 ug/m3 91-20-3 128 Naphthalene ND 800 ppbv ND 4200 ug/m3 108-88-3 92 Toluene 3180002 1600 ppbv 1200000 a 6000 ug/m3 106 m.p-Xylene 99300 800 ppbv 430000 3500 ug/m3 95-47-6 106 o-Xylene 32200 800 ppbv 140000 3500 ug/m3 1330-20-7 106 Xylenes(total) 132000 800 ppbv I 572000 3500 ug/m3 CAS No. Surrogate Recoveries Run#1 Rtn#2 I:nnits 460-004 4-Bromofluorobenzenz 90% 90% 70-130% I I CAS No. Tentatively Identified Compounds R.T. Est. Cone.; Units Q i C5-C8 Aliphatic 5.33 70000 ! ppbv J CS-C8 Aliphatic 5.47 17000 ppbv J CS-C8 Aliphatic 5.63 9100 ppbv J C5-C8 Aliphatic 5.73 26000 ppbv J C5-C8 Aliphatic 5.93 14000 ppbv J C5-C8 Aliphatic 6.09 18000 ppbv J C5-C8 Aliphatic 6.53 4200 ppbv J CS-C8 Aliphatic 6.59 2200 ppbv J C5-C8 Aliphatic 6.63 3300 ppbv J C5-C8 Aliphatic 6.93 54000 ppbv J C5-C8 Alipbatic 6.93 120000 I ppbv J C5-C8 Aliphatic 7.32 76000 ppbv J C5-C8 Aliphatic 7.46 19000 ' ppbv J C5-C8 Aliphatic 7.94 19000 ppbv J C5-C8 Aliphatic 8.01 23000 ppbv J CS-CS Aliphatic 8.12 17000 ppbv J C5-C8 Aliphatic 8.22 11000 ppbv J C5-C8 Aliphatic 8.41 19000 ppbv J CS-C8 Aliphatic 8.55 5600 ppbv J C5-C8 Aliphatic 8.66 51000 ppbv J CS-C8 Aliphatic 8.73 36000 ppbv J ND = Not detected J = Indicates an evtimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Ideates pre,umptive evidence of a compound Jun-07-01 02:27pm From- T-333 P.o6/U1 r-Jia Accutest Laboratories Report of Analysis Page 2 of 3 Client Sample ID: SVE Lab Sample ID: E91703 2 Date Sampled: OS/18/Ol Matrix: AIR-Air Date Received: 05/23/0 t Method: 'JO.14/T0-15 percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road,Hyannis,MA CAS No. Tentatively Identified Compounds R.T. Est. Cone. Units 0 C5-C8 Aliphatic 9.35 18000 ppbv J C5-C8 Aliphatic 9.55 4200 ppbv J CS-C8 Aliphatic 9.65 3500 hpbv J CS-CS Aliphatic 9.71 9600 ppbv J CS-C8 Aliphatic 9.89 55000 I)pbv J CS-C8 Aliphatic 9.98 31000 Iapbv J CS-C8 Aliphatic 10.18 59000 ppbv J C5-C8 Aliphatic 10.29 6900 hpbv J C5-C8 Aliphatic 10.43 14000 .ppbv J C5-C8 Aliphatic 10.52 18M .hpbv J C5-C8 Aliphatic 10.63 12M .apbv J C5-C8 Aliphatic 10.77 3700 ppbv J C5-C8 Aliphatic 10.86 7300 ppbv J C5-C8 Aliphatic 10.93 31000 ppbv J C5-C8 Aliphatic 10.99 21000 ppbv J C5-C8 Aliphatic 11.07 5400 ppbv J C5-C8 Aliphatic 11.14 2500 ppbv J C5-C8 Aliphatic 11.23 6500 ppbv J C5-C8 Aliphatic 11.32 11000 ppbv J C5-C8 Aliphatic 11.66 28000 ppbv J C5-C8 Aliphatic 11.93 17000 ppbv J C5-C8 Aliphatic 12.00 29000 ppbv J C5-C8 Aliphatic 12.12 3000 ppbv J C5-C8 Aliphatic 12.25 7100 ppbv J C5-C8 Aliphatic 12.45 4200 ppbv J C5-C8 Aliphatic 12.53 59000 ppbv . J C5-C8 Aliphatic 12.81 20000 ppbv J C5-C8 Aliphatic 12.95 21000 ppbv J C5-C8 Aliphatic 13.01 12000 ppbv J C5-C8 Aliphatic 13.10 3500 ppbv J C5-C8 Aliphatic 13.18 28000 ppbv J C5-C8 Aliphatic 13.37 9400 ppbv J C5-C8 Aliphatic 13.51 16000 ppbv J C5-C8 Aliphatic 13.65 4100 ppbv J C5-C8 Aliphatic 13.84 2200 ppbv J C5-C8 Aliphatic 13.92 14000 ppbv J CS-C8 Aliphatic 14.02 2700 ppbv J C5-C8 Aliphatic 14.14 6500 ppbv J CS-C8 Aliphatic 14.33 2000 ppbv J CS-C8 Aliphatic 14.44 2700 ppbv J ND = Not detected J = Indicates an waimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value eucecds calibration rangc N = Indicates pre_:umptive evidence of a compound Jun-07-01 02:17pm From- T-333 P-OT/UT F-319 Accutest Laboratories Report of Analysis Page 3 of 3 Client Sample MD: SVE Date Sampled: 05/18/0t Lab Sample ID: E91703-2 05/23/01 Date Received Matrix: AIR-Air Percent Solids: n/a lfriethod: T0-14/TO-15 Project; GSCMAH:969250M 1140 Iyauough Road,Hyannis,MA CAS No. Tentatively Identified Compounds R.T. Est.Cone. Units Q C5-C-g Aliphatic 14.61 3500 ppbv J CS-C8 Aliphatic 14.17 2000 ppbv J CS-C8 Aliphatic 14.96 6500 13pbv J C5-C8 Aliphatic 15.91 4800 I?pbv J C9-C10 Aromatic 17.08 2" !?pbv J C9-C10 Aromatic 17.91 3500 .>pbv J C9-C10 Aromatic 17.98 13000 ppbv J C9-C10 Aromatic 18.03 5400 ppbv J C9-C10 Aromatic 18.16 5600 ppbv J C9-C10 Aromatic 18.43 3400 ppbv J C9-C10 Aromatic 18.78 9800 ppbv J Total C5-C8 Aliphatics 1360000 ppbv Total C5-C8 Aliphatics 5170000 ug/m3 Total C9-C12 Aliphatics b 0 ppbv Total C9-C12 Aliphatics b 0 ug/m3 Total C9-C10 Aromatics 42700 ppbv Total C9-Cl0 Aromatics 222000 ug/m3 Total TIC,'Volatile 1397900 ppbv (a)Result is from Runl12 (b)No peaks found for Total C9-C12 Aliphatics ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N =Indicates presumptive evidence of a compound IMMEDIATE RESPONSE ACTION PLAN DESIGN SPECIFICATION TEXACO SERVICE STATION#100083 ' 1140 IYANNOUGH ROAD H' 'ANNIS, MASSACHUSETTS RTN#4-11301 August 2002 Prepared by: Prepared for: Geologic Services Corporation Equiva Services LLC 15 Bonazzoli Avenue P.M.B. 301 Hudson,MA 01749 1830 South Road, Unit 24 (978)568-8740 Wappingers Falls, NY 12590 (845)462-5225 GSC Project No. 000509C 1 BIBLIOGRAPHY OF REPORTS Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts Date of Report Title of Report Prepared By July 16, 1991 Bay Drain Closure Letter HETI November 1991 Report on Site Inspection and Records Review HETI December 28, 1994 21E Site Assessment(Cooke's Restaurant) D.C.E. June 6, 1995 Notice of Responsibility MA DEP August 11, 1995 Release Notification Form Motiva October 12, 1995 Phase I-Initial Site Investigation Report GES February 22, 1996 Initial Groundwater Monitoring Report Handex July 23, 1996 Groundwater Monitoring Report GES August 15, 1996 Decision to Grant Permit Letter MA DEP October 9, 1996 Groundwater Monitoring Report GES October 28, 1996 Immediate Response Action Plan GES Immediate Response Action Transmittal Form July 23, 1997 Phase 11-Comprehensive Site Assessment GES Scope of Work June 26, 1997 Groundwater Monitoring/IRA Status Report GES March 23, 1998 Groundwater Monitoring/IRA Status Report Sage August 13, 1998 Modification to Phase II-Comprehensive Site Assessment Sage Scope of Work March 1998 IRA Status Report Sage September 30, 1998 IRA Status Report Sage March 4, 1999 IRAP Modification Sage May 1999 Phase II Extension Request Sage October 1999 IRA Status Report Sage June 2000 Phase II-Comprehensive Site Investigation and Phase III Sage Remedial Action Plan February 16, 2001 IRA Status Report GSC May 9,2001 IRA Plan and Status Report GSC June 11,2001 IRA Completion Report(RTN 4-16161) and Modification GSC of IRA Work Plan Activities(RTN 4-11301) September 6,2001 IRA Status Report GSC March 6,2002 IRA Status Report GSC August,2002 IRA Plan Design Specification GSC HETI-Hydro-Environmental Technologies,Inc. D.C.E. -Down Cape Engineering, Inc. MA DEP-Massachusetts Department of Environmental Protection GES - Groundwater&Environmental Services,Inc. Sage Sage Environmental, LLC Handex -Handex of New England, Inc. GSC -Geologic Services Corporation Ref.#000509C.IRAPDS LIST OF APPENDICES Appendix A - Figures Figure 1 - Locus Plan Figure 2 - Site Plan Figure 3 - Area Plan Figure 4 - GIS Map and Legend Figure 5 - Groundwater Contour/Hydrocarbon Distribution Plan— 12/4/01 Figure 6 - Groundwater Contour/Hydrocarbon Distribution Plan—5/l/02 Figure 7 - Proposed Well Network Layout and Conceptual Radii of Influence Figure 8 - Proposed Trench Layout Figure 9 - Trench Cross Section and SVE/AS Well Head Construction Details Figure 10 - Process&Instrumentation Diagram Figure 11 - Process&Instrumentation Diagram Legend Appendix B - Tables Table 1 - Monitoring Well Gauging Data Summary Table 2 - Groundwater Sample Analytical Results—Volatile Petroleum Hydrocarbons Table 3 - Groundwater Sample Analytical Results—Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Table 4 - Historical Soil Analytical Results—Volatile Petroleum Hydrocarbons Table 5 - Summary of SVE Step Test Table 6 - Summary of SVE/AS Pilot Testing Data Table 7 - Summary of SVE/AS Pilot Test Data—Monitoring Point Data Table 8 - Summary of SVE/AS PilotTesting Data Table 9 - Summary of SVE/AS Pilot Test Air Sample Analytical Data at SVE-1 Appendix C - Groundwater Analytical Results Appendix D - Well Logs Appendix E - Soil Sample Analytical Results Appendix F - Charts Chart 1 - Applied Vacuum at SVE-1 vs. Flow Rate Chart 2 - Normalized Vacuum vs. Distance from SVE-1 @ 5"H20 Chart 3 - Normalized Vacuum vs. Distance from SVE-1 @10"H20 Chart 4 - Normalized Vacuum vs. Distance from SVE-1 @1.3"H20 Chart 5 - Influent VOC Concentration vs. Time Chart 6 - Groundwater Mounding vs. Time Chart 7 - Dissolved Oxygen Content vs. Time Appendix G - Air Sample Analytical Data Ref. 4000509C. IRAPDS I Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts MA DEP RTN 4-11301 I. Person Conducting Immediate Response Action,pursuant to 310 CMR 40.0424(1)(a) On behalf of Motiva Enterprises LLC(Motiva), Equiva Services LLC (Equiva) is conducting the Immediate Response Actions(IRA)referenced herein. Motiva is the owner and operator of the subject site. The Equiva representative overseeing the response actions in connection with this IRA is Mr. David B. Weeks. Equiva has retained Geologic Services Corporation(GSC)and Scott K. Parker(Licensed Site Professional#9969)as their consultant and LSP-of-record. II. Background The subject property was listed by the Massachusetts Department of Environmental Protection(DEP) based on information reported in a December 28, 1994 21 E Site Assessment Report,prepared by Down Cape Engineering, Inc. (DCE) for Cooke's Restaurant located downgradient of the site at 1120 Iyannough Road, Hyannis,Massachusetts. Cooke's Restaurant is the abutter to the east of the subject property. As part of this site assessment,DCE collected groundwater samples from three monitoring wells located on the Cooke's Restaurant property. Laboratory analysis indicated the presence of benzene,toluene,and xylenes in the sample obtained from a well reported to be downgradient of the Texaco Station. Release Tracking Number(RTN)4-11301 was issued by the DEP on April 6, 1995 in response to these findings. Resulting from the 21 E Site Assessment of Cooke's Restaurant,the DEP issued a Notice of Responsibility(NOR)to the owner of the Star Enterprise(Star)property located at 1140 Iyannough Road in Hyannis,Massachusetts on August 11, 1995. On October 12, 1995, Star, now Motiva, submitted a Phase I-Initial Site Investigation Report and Tier IC Application to DEP for the subject site. During the g p PP J g Phase I investigation,groundwater sampling results of the on-site monitoring wells revealed dissolved- phase petroleum constituents in excess of the DEP reportable concentrations for GW-1 groundwater standards. The DEP approved the Tier IC Permit Application(No. 100556) for the subject property on September 12, 1996. At this time it was determined that a Substantial Release Migration(SRM)condition may exist and the DEP required an IRA Plan to be submitted. Star submitted an assessment-only IRA Plan proposing tri-annual groundwater monitoring for a one-year period to evaluate seasonal changes in groundwater elevation and quality. A Phase II Scope of Work(SOW)was submitted by Groundwater&Environmental Services, Inc. (GES) on July 25, 1997 for additional subsurface investigations to be completed. This work included the installation of additional monitoring wells and additional groundwater sampling. On September 18, 1998, SAGE Environmental(SAGE) submitted an IRA Status report summarizing the installation of three monitoring wells and the advancement of five soil borings. Groundwater samples were collected from ten on-site monitoring wells on May 6, 1998 and analyzed for extractable petroleum hydrocarbons(EPH) and volatile petroleum hydrocarbons(VPH). Soil analytical results for this sampling event indicated concentrations of methyl-tert butyl ether(MTBE) above applicable S-1/GW-1 soil standard from MW-9 and SB-11. Dissolved phase petroleum constituents were detected above applicable GW-1 standards for all wells sampled except MW-3. Ref. #000509C. 1RAPDS I r SAGE submitted a Modification to the Phase II SOW on August 13, 1998 for the installation of off-site monitoring wells, well surveying,groundwater sampling, a soil vapor extraction(SVE)pilot test,and a limited pump test. SAGE was unable to secure off-site access for the installation of downgradient monitoring wells. However,the SVE pilot test and groundwater sampling were completed on March 25, 1999 and June 4, 1999,respectively. SAGE indicated that the results of the SVE test were skewed due to recent construction activities that may have caused short-circuiting in the airflow diminishing the effective radius of influence. On March 4, 1999, SAGE submitted a Modification to the IRA Plan in response to extensive excavation activities proposed at the site. The modification addressed excess soil to be generated during the installation of a new pump islands and canopy foundations and the removal and replacement of two leaching catch basins. It included a work scope for the soil testing of excavated soils, confirmatory sampling, and management of excavated soils. Approximately 556.75 tons of soil was removed from the site on March 4 and 5, 1999 for reuse at a landfill. Approximately 188.47 tons of petroleum impacted soils was transported to an off-site disposal facility for recycling on March 24, 1999. On August 22, 2000, SAGE submitted a Phase II—Comprehensive Site Assessment and Phase III— Remedial Action Plan(RAP). Groundwater extraction combined with soil vapor extraction technologies were selected as the remedial action alternative for achieving a permanent solution at the subject property. Following review of the Phase II and III Reports,additional delineation of the dissolved phase petroleum hydrocarbons related to the subject property was viewed to be warranted prior to the selection/implementation of a remedial action. In conjunction with the installation of the groundwater monitoring wells,pilot test air sparge(AS)and SVE wells were installed at the subject property. In March of 2001, GSC and Motiva were able to secure off-site access to abutting properties. Between March 19 and 23,2001,GSC personnel supervised the installation of four 2-inch diameter groundwater monitoring wells MW-11,MW-12,MW-13, and MW-14 at and in the vicinity of the subject property in order to further delineate petroleum impact to soil and groundwater. During groundwater monitoring well gauging and sampling activities performed on April 4, 2001, approximately 0.60 feet of non-aqueous phase liquid(NAPL)(i.e.; weathered gasoline)was detected in monitoring well MW-9. The DEP was verbally notified of the presence of greater than 0.5 inches of NAPL on April 5, 2001. The DEP subsequently assigned RTN 4-16161 to this 72-hour release condition and verbally approved passive NAPL bailing activities under an IRA. On April 12, 2001,Tanknology—NDE of Springfield,Massachusetts performed a pressure tank tightness test for the gasoline underground storage tank system at the subject property. All the pressure tests performed on the underground storage tank(UST) system passed on this date. On June 8,2001 Motiva submitted a Tier IC Permit Renewal Application to the DEP in order to allow for the continuation of response actions under RTN 4-11301. In addition,the Tier I Permit application detailed the linking of RTN 4-16161 to lead RTN 4-11301. On September 27,2001 a Decision to Grant a Tier IC Permit Extension was approved by the DEP. An IRA Status Report was submitted to the DEP in March 2002 detailing NAPL recovery and assessment activities during the period of August 2001 through January 2002. Additional information pertaining to previous report submittals and response activities can be found in the reports listed in the`Bibliography of Reports"at the front of this document. Ref. #000509C. IRAPDS III. Description of Site Conditions/Surrounding Receptors,pursuant to 310 CMR 40.0424(1)(b) Local area topography slopes in a southerly direction toward Iyannough Road. The subject property is situated at 1140 Iyannough Road in Hyannis,Massachusetts and is currently an active Texaco branded retail gasoline and automobile repair facility. The subject property has an area of approximately 47,916.19 square feet(1.1 acres). The majority of the site is paved with asphalt or reinforced concrete, except a small area in the southern portion of the lot,which is landscaped. The northern portion of the property is wooded and covered in gravel. The properties in the vicinity of the subject site are primarily used for commercial purposes. The single-story Texaco station houses an office area,restrooms, and three repair service bays and also used as a parking lot for school buses. One 12,000 gallon gasoline UST,two 10,000 gallon gasoline USTs,one 8,000 gallon diesel fuel UST,and one 550 gallon waste oil UST currently exist at the site. The site is serviced by municipal water supply and sewer as well as underground telephone and electric service utilities. The subject site drainage system is connected to an on-site leachfield located immediately east of the service station building. Two detention drainage basins are located approximately 80 feet southeast and 90 feet north of the convenience store,respectively. Please refer to Figures 1,2, 3,and 4(Appendix A) for a depiction of the subject property and surrounding area. - According to the United States Geological Survey(USGS)Hyannis,Massachusetts 15 Minute Topographic Quadrangle, a portion of which is provided as Figure 1,the subject property has an elevation of approximately 78 feet above mean sea level(MSL). IV. Description of Release/Threat of Release,pursuant to 310 CMR 40.0424(1)(b) RTN 4-11301 During the review of the Tier IC Permit Application in September 1996,a Condition of SRM was viewed by DEP to be possible at this site. This was based on the presence of petroleum constituents on the abutting property and Texaco property in excess of the GW-1 groundwater standards and the nature of the groundwater in this area. Another IRA(RTN 4-16161)was linked to this RTN(RTN 4-11301)in 2001 due to NAPL present in groundwater monitoring well MW-9. V. Description of IRA Activities Conducted to date,pursuant to 310 CMR 40.0424(1)(c) IRA activities conducted at this site have included the monitoring of groundwater in the site vicinity, soil removal,and,passive NAPL bailing. The lead RTN(4-11301)was related to a potential condition of SRM. During site upgrade activities, soil removal and disposal was added to the IRA plan originally submitted for this site. In April 2001,NAPL was discovered in an on-site monitoring well triggering another IRA condition and RTN 4-16161. Passive NAPL bailing has been ongoing at this site. Gauging data is included in Table 1 (Appendix B). The groundwater analytical results for the site are included on Tables 2 and 3 (Appendix B). Groundwater contours have been prepared for the December 4, 2001 and May 1, 2002 sampling events and are included as Figures 5 and 6(Appendix A)respectively. Complete laboratory analytical results for the past two events are included in Appendix C. VI. Objective,Plan, Schedule for Continued IRA Activities, pursuant to 310 CMR 0.0424(1) (e&g) Additional activities anticipated for completion during the course of this IRA include the completion of additional Phase 11 delineation activities and additional field research and reconnaissance to detennine the full extent of this disposal site. Ref.4000509C. IRAPDS VII. Summary of SVE/AS Pilot Test Drilling Activities Prior to the SVE/AS pilot test, GSC supervised the installation of one AS well(AS-1), one SVE well (SVE-1), and three triplet monitoring points(MP-1 through MP-3)at the site on March 14,2001. Drilling was conducted by Geosearch Inc.,of Sterling, Massachusetts utilizing a truck-mounted hollow- stem auger drill rig. The AS well was installed to a total depth of approximately 49-feet below grade, constructed of 47-feet of 2-inch diameter Schedule 40 PVC riser with 2-feet of 2-inch diameter Schedule 40 PVC 0.010 slot well screen at the base. The borehole annulus of the well was finished with a sand pack to approximately 2-feet above the top of the well screen, a 2-foot bentonite seal, grout to approximately 4-feet below grade, and back-filled to grade with native material. AS-1 was finished with a flush mounted, 8-inch road box, incased in a 2-foot by 2-foot concrete pad. The location of this well is shown on Figure 2. Soil samples collected during these drilling activities were screened in the field with a photoionization detector(PID)calibrated to read total VOCs in parts per million by volume(ppm )as benzene. The PID screening results are depicted along with well construction details on the well logs included in Appendix D. The SVE well was installed to a total depth of approximately 36-feet below grade,constructed of 26-feet of 4-inch diameter Schedule 40 PVC riser with 10-feet of 4-inch diameter Schedule 40 PVC 0.010 slot well screen at the base. The bore hole annulus of the well was finished with sand packs to approximately 2-feet above the top of the well screen, a 2-foot bentonite seal and back-filled to grade with native material. SVE-1 was finished with a flush mounted, 12-inch road box, and incased in a 2-foot by 2-foot concrete pad. The location of this well is shown on Figure 2. Soil samples collected during these drilling activities were screened in the field with PID calibrated to read total VOCs in ppm,,as benzene. The PID screening results are depicted along with well construction details on the well logs included in Appendix D. The three triplet monitoring point bore holes were advanced to a total depth of approximately 43-feet below grade, with the points constructed of 25, 37,and 41-feet of 1.5-inch diameter Schedule 40 PVC riser with 10, 2, and 2-feet of 1.5-inch diameter Schedule 40 PVC 0.010 slotted well screen at their bases, respectively. Refer to Appendix D for the well construction details and PID screening results.MP-1 through MP-3 were finished with flush mounted, 12-inch road boxes,and incased in 2-foot by 2-foot concrete pads. The locations of these wells are shown on Figure 2. Soil samples collected during these drilling activities were screened in the field with a PID calibrated to read total VOCs in ppm,,as benzene. The PID screening results are depicted along with well construction details on the well logs included in Appendix D. During the installation of these wells, GSC personnel collected one soil sample from each boring and submitted them to Accutest, for analysis of target VOCs, and VPH fractions via DEP-Approved Methodologies. As noted in Table 4(Appendix B),no compounds were detected above the method detection limit. Complete analytical results from soil samples collected on March 21 through 22,2001 are included as Appendix E. VIII. Summary of SVE/AS Pilot Testing Activities On May 4, 2001, GSC conducted a combined SVE/AS pilot test on wells SVE-1 and AS-1. The principal purpose of the SVE portion of this pilot test was to determine the feasibility of soil vapor extraction as a potential remedial option for this site. Prior to the initiation of the SVE pilot test, a step test was conducted on SVE-1 to determine the relationship between applied vacuum and soil vapor flow from this well. During the step test,the vacuum at the wellhead was allowed to stabilize, flow rates were recorded, and then the vacuum was increased Ref. #000509C. IRAPDS until a maximum flow rate was established or water was pulled into the system. Refer to Table 5 (Appendix B) for a summary of the step test data,and Chart 1 (Appendix F) for a visual depiction of the vacuum—flow relationship. Once the step test was completed it was determined that the SVE test would be conducted by applying a vacuum of approximately 5 inches of water column(in.we)to the extraction well,which yielded a flow rate of approximately 107 standard cubic feet per minute(scfm)of extracted soil vapor. The pilot test was performed for a total period of three and one half(3.5)hours during which time a Rotron 2-Hp regenerative blower was used to apply vacuums of approximately 5 and 10 in. we to SVE-1. During the course of this test,the 1.5 inch points(which are screened across the water table)in the three triplet wells and MW-9 were monitored at regular intervals for pressures(observed vacuums),depth to water, VOC concentrations as measured with a calibrated PID, and dissolved oxygen concentrations (DO). Other parameters measured at the SVE system consisted of vacuum applied to SVE-1 by the blower,VOC concentration of the soil vapor air stream as measured with a PID at the influent,mid- fluent, and effluent of the off-gas treatment and air flow rate. Extracted soil vapors were treated using two 200-pound vapor phase granular activated carbon units (GACs)prior to discharge to the atmosphere. Throughout the course of the SVE test,VOC concentrations of the soil vapor influent air stream were observed to range from 437 to 766 ppmv VOCs at an extraction rate ranging from approximately 107 to 176 scfm. Vacuum influence was observed in each of the four monitored wells,ranging from 0.65 to 1.05 in. we in MP-1 (located 8.00 feet from SVE-1),0.33 to 0.65 in. we in MP-2(located 17.50 feet from SVE-1), 0.22 to 0.35 in. we in MP-3 (located 27.00 feet from SVE-1),and 0.11 to 0.18 in. we in MW-9 (located 45.00 feet from SVE-1). The SVE/AS pilot test results are summarized in Tables 6 and 7 (Appendix B). Based on the vacuum applied to SVE-1 (5 and 10 in.we)and the vacuum observed at the four monitoring wells, an estimated radial influence was calculated by plotting the normalized vacuums versus distance on a semi-logarithmic graph(refer to Charts 2 and 3 in Appendix F). Radial influence was determined to be the distance where 1%of the normalized vacuum was observed or extrapolated by graph. Based on the pilot test data,the effective SVE radial influence for SVE-1 when applying a vacuum of 5 and 10 in. we was calculated to be approximately 37 feet and 38 feet,respectively. Refer to Charts 2 and 3 (Appendix F) for a visual depiction of the effective radii of influence observed during the pilot test. During a short SVE pilot test conducted on May 18, 2001 soil vapors were extracted from SVE-1 by utilizing a 2Hp regenerative blower that applied a vacuum of 1.3 in. we with a corresponding air flow rate of 28.9 scfin. During the course of this test,the two inch points(which are screened across the water table)in the three triplet wells were monitored at regular intervals for pressures(observed vacuums. Other parameters measured at the SVE system consisted of vacuum applied to SVE-1 by the blower, and air flow rate. Extracted soil vapors were treated using two 200-pound vapor phase granular activated carbon units(GACs)prior to discharge to the atmosphere. Throughout the course of the SVE test, an extraction rate of approximately 29 scfm was maintained. Vacuum influence was observed in each of the three monitored wells, from 0.22 in. we in MP-1 (located 8.00 feet from. SVE-1), 0.11 we in MP-2 (located 17.50 feet from SVE-1),to 0.05 in. we in MP-3 (located 27.00 feet from SVE-1). The SVE/AS pilot test results are summarized in Tables 8 (Appendix B). Prior to the completion of the SVE/AS pilot test a summa canister sample was collected from the influent of the SVE blower and sent to Accutest Laboratories of NJ for analysis. The air sample was analyzed for air phase petroleum hydrocarbons (APH). Results of the air sample have been summarized in Table 9 (Appendix B)and the complete analytical results can be found in Appendix G. Ref.4000509C.. IRAPDS Based on the vacuum applied to SVE-1 (1.3 in. wc)and the vacuum observed at the four monitoring wells, an estimated radial influence was calculated by plotting the normalized vacuums versus distance on a semi-logarithmic graph(refer to Charts 4 in Appendix F). Radial influence was determined to be the distance where 1%of the normalized vacuum was observed or extrapolated by graph. Based on the pilot test data,the effective SVE radial influence for SVE-1 when applying a vacuum of 1.3 in. we was calculated to be approximately 33 feet. Refer to Charts 2 and 3 for a visual depiction of the effective radii of influence observed during the pilot test. On May 24, 2001,GSC conducted a combined SVE/AS pilot test on wells SVE-1 and AS-1. The principal purpose of the AS portion of this pilot test was to determine the feasibility of AS as a potential remedial option for this site. This test was performed for approximately two hours and(2.2)hours, in concert with the last(2.2)hours of the SVE pilot test. A Craftsman 4-HP oil-less air compressor was used to inject air into AS-1 at pressures ranging from 8 to 9 pounds per square inch psi, resulting in flow rates of 3, and 6 scfm, respectively. The 2-inch wells which intersect the water table were monitored at regular intervals for pressures,depth to water,DO, and VOC concentrations as measured with a PID calibrated to read total VOCs in ppm,,as benzene. The 1.5-inch wells that are set below the water table were monitored for pressure, and Helium. Other parameters measured at the SVE and AS systems consist of pressure applied at the blowers, influent,mid-fluent, and effluent VOC concentrations as measured with a PID calibrated to read VOCs as benzene, and air flow rates. Complete pilot test data results are summarized in Tables 5 through 9,Appendix B. During the first hour of the AS portion of the test a pressure of approximately 8 psi, which yielded a flow rate of approximately 3 scfm,was applied to AS-1. Throughout the course of this portion of the SVE/AS pilot test,VOC concentrations of the:soil vapor influent air stream were observed to range from 415 to 508 ppmv VOC's. Groundwater mounding influence was observed in MP-1 through MP-3, and an increase in DO concentration was observed at monitoring points MP-I,MP-2, and MP-3. Visual illustrations of groundwater mounding influence and the DO influence can be seen on Charts 6 and 7, respectively. During the second 45 minutes of the AS portion of the test a pressure of approximately 9 psi,which yielded a flow rate of approximately 6 scfin,was applied to AS-1. Throughout the course of this portion of the SVE/AS pilot test,VOC concentrations of the soil vapor influent air stream were observed to range from 375 to 469 ppmv VOC's. Groundwater mounding influence was observed in MP-1 through MP-3, and an increase in DO concentration was observed at monitoring points MP-1,through MP-3. Visual illustrations of groundwater mounding influence and the DO influence can be seen on Charts 6 and 7, Appendix F respectively. The final half hour of the SVE/AS test consisted of the injection of helium as a tracer gas. During this portion of the test a 300 cubic foot helium tank with a standard regulator was used to inject helium into the sparge well at approximately 9 psi, which corresponded to a flow rate of 6 scfin. The three triplet wells and the influent to the system were monitored for helium content. Complete pilot test data results are summarized in Tables 5 through 9(Appendix B). Based on the air flow injection rate at AS-1,helium detection data, geometric relationships between wells monitored,the distance of the monitoring points from AS-1, changes in dissolved oxygen levels, and the change in groundwater elevations observed in the wells monitored, an estimated radial influence was determined to be approximately 22 feet for well AS-1 at the respective flow rate of approximately 6 scfm. Ref.#000509C. IRAPDS During a short SVE/AS pilot test conducted on May 18,2001 soil vapors were extracted from SVE-1 by utilizing a 2 Hp regenerative blower,that applied a vacuum of 1.3 in. we with a corresponding air flow rate of 28.9 scfm. During the course of this test,the two inch points(which are screened across the water table)in the three triplet wells were monitored at regular intervals for pressures(observed vacuums). Other parameters measured at the SVE system consisted of vacuum applied to SVE-I by the blower, and air flow rate. Extracted soil vapors were treated using two 200-pound vapor phase granular activated carbon units(GACs)prior to discharge to the atmosphere. Throughout the course of the 30 minute AS portion of this test, a pressure of approximately 10 psi, which yielded a flow rate of approximately 6 scfm,was applied to AS-1. Prior to the completion of the AS portion of this test a summa canister sample was collected from the influent of the SVE blower and sent to Accutest Laboratories of NJ for analysis. The air sample was analyzed for air phase petroleum hydrocarbon(APH). Results of the air sample have been summarized in Table 9(Appendix B)and the complete analytical results can be found in Appendix G. IX. Remediation System Design Based on the assessment activities preformed to date for this site and the results of continued groundwater monitoring activities,the UST and pump dispenser area has been identified for immediate remediation using SVE/AS technology. This target area generally correlates to the areas of petroleum impacted groundwater and soil identified during ongoing Phase H and IRA assessment activities. Installation of Additional SVE/AS Wells Based on the pilot test data for this site, a total of 10 additional SVE wells and 7 additional AS wells are proposed to adequately address the area targeted for active remediation on the Texaco property. Refer to Figure 7 (Appendix A)for the location of SVE and AS wells. The 10 additional SVE wells proposed for installation will be installed at a depth of approximately 36 feet below grade, constructed of 26-feet of 4- inch diameter Schedule 40 PVC riser with 10-feet of 4-inch diameter Schedule 40 PVC 0.010 slot well screen at their bases. The borehole annulus of each SVE will be finished with a sand pack to approximately 2-feet above the top of the well screen, a 2-foot bentonite seal and backfilled to grade with native material. The additional 7 AS wells will be installed to a total depth of approximately 49 feet below grade,constructed of 47-feet of 2-inch diameter Schedule 40 PVC riser with 2-feet of 2-inch j diameter Schedule 40 PVC 0.010 slot well screen at their bases. The borehole annulus of each AS well will be finished with a sand pack to approximately 2-feet above the top of the well screen, a 2-foot bentonite seal, grouted from above the bentonite seal to approximately 4 feet below grade and back-filled to grade with native material. Remediation System Piping/Trenches Each SVE and AS well will be connected to an individual PVC conduit(2-inch diameter Schedule 40 PVC pipe for the SVE wells and 1-inch diameter Schedule 80 PVC pipe for the AS wells),placed within trenches that will be excavated to a depth of up to four feet below grade. Please refer to Figure 8 (Appendix A)for the approximate locations of the trenches and the equipment enclosure. All bituminous concrete pavement will be saw cut prior to trenching. The piping will be installed on a bed of pea gravel and covered by approximately 4 inches of pea gravel. The trenches will be backfilled with select native material, free of cobbles and organic material,compacted in six-inch lefts and resurfaced. All piping leading from The wells will lead to and be manifolded together within a shed and/or fenced equipment enclosure. The SVE and AS wells construction details and trench cross-section/piping details are included on Figure 9(Appendix A). Ref#000509C. IRAPDS Remedial Equipment SVE Equipment The SVE system equipment will consist of a positive displacement/regenerative blower with a relief valve, moisture separator, air filter,heat exchanger(if necessary), sample ports, and flow and pressure gauges. The blower will be capable of providing a vacuum of approximately 1.5 inches of water column with an expected flow of approximately 28 scfm at each well. The type and specifications of the blower itself will be dependent on the manufacturer. The piping from each well will be independently valved to allow for extraction from any or all of the wells at a given time. Each piping leg will contain a sample collection port to monitor individual well head influent vapor concentrations to the system. The SVE system will be equipped with the following failsafes; a high level switch in the moisture separator, a low vacuum or low flow switch on the intake side of the blower and a high temperature switch/or heat exchanger on the discharge side of the blower. Refer to Figures 10 and 11 (Appendix A)for a process and instrumentation diagram and associated legend. The aforementioned equipment will be housed within either a shed or fence enclosure constructed at the location noted on Figure 9,pending local permitting requirements. The layout of the equipment within the equipment compound will be determined in the field at the time of construction. AS Equipment The AS system equipment will consist of a compressor capable of delivering approximately 6-10 scfm at a pressure of 9 pounds per square inch(psi) at each well,and heat exchanger(if necessary). The type and the specifications of the equipment chosen will be dependent on the manufacturer. Additional controls,a relief valve,pressure gauges and flow meters will be provided. The air sparging system will be equipped with appropriate fail safes to shut down the air sparging system should the SVE system shut down. Refer to Figures 10 and 11 (Appendix A)for a process and instrumentation diagram and associated legend. The layout of the equipment within the equipment compound will be determined in the field at the time of construction. Treatment,Management, and Disposal of Remediation Process Wastes Air removed from the SVE wells will enter a moisture separator where the air will be separated from residual water. The resultant air stream is expected to be treated by a series of appropriately sized vapor phase granular activated carbon vessels(VGAC). If it is determined that the soil vapor stream temperature is greater than 120 deg. Fahrenheit a heat exchanger will be placed prior to the first VGAC in order to ensure 95%destruction efficiency. Sample ports will be fitted at the influent and effluent points of each VGAC, in order to complete monitoring of the vapor stream as outlined in this submittal. X. Remediation System Construction Management Field Monitoring and Management of Excavated Soil During drilling and excavation activities, GSC personnel will perform on-site inspections and field screening of excavated soil. Field screening will be performed using a PID calibrated to read VOCs in ppmv as benzene. Soil which does not exhibit visual or olfactory evidence of petroleum impact and does not exceed a PID reading of 100 ppm,:using standard jar headspace techniques may be considered suitable for on-site reuse. Soil exhibiting visual or olfactory indications of petroleum impact or exhibiting a PID response of greater than 100 ppm,:VOCs will be considered potential Remediation Waste, and stockpiled separately pending confirmatory laboratory testing. Ref. #000509C. IRAPDS In so far as the purpose of the trench excavations is to allow the construction and installation of the SVE/AS remedial system piping to occur, and not to perform the actual remediation of this portion of the site, it is not anticipated that petroleum-impacted soil will be excavated from beyond the limits of excavation specifically planned for installation of SVE/AS piping. Soil Stockpiling Protocol Soil removed from the excavation during construction activities will be staged on and covered by polyethylene sheeting in separate stockpiles based upon the results of the visual, olfactory, and PID field screening results. Soil piles will be covered with polyethylene sheeting and secured at the end of each day until the soil is either re-used on site or removed from the site. Characterization of Stockpiled Soils Representative soil samples will be collected from any stockpiled soil which is initially characterized as potential Remediation Waste and submitted to a laboratory for analysis of the parameters specified in the intended receiving facility permit requirements. It is anticipated that samples will be collected on a frequency of approximately one sample per 200 cubic yards(if necessary). Other soil analyses may be performed as necessary, in order to provide characterization in accordance with the license/requirements of the receiving facility. The permit requirements of the anticipated receiving facility will determine the frequency of other analyses. Soil found to contain hydrocarbon concentrations which exceed Reportable Concentrations for reporting category S-1 soil will be considered Remediation Waste and will remain stockpiled pending transport to a recycling/disposal facility. Management of Remediation Waste Soil impacted with petroleum and determined to be Remediation Waste, as previously described,may be transported to a permitted recycling facility using a Massachusetts DEP Bill of Lading in accordance with the provisions of 310 CMR 40.0030. Soil impacted with petroleum and determined not to be Remediation Waste, as previously described,may be transported to a permitted recycling facility with the voluntary use of a DEP Bill of Lading, if the soil is not re-used on site. Excavation Dewatering/Treatment Based on historic,groundwater elevations and the estimated depth of excavations, it is not anticipated that excavation dewatering will be needed. Health and Safety/Site Security Work performed as part of the IRA plan shall be conducted in accordance with the requirements of the Occupational Safety and Health Administration(OSHA)under 29 CFR 1910.120. A site-specific Health and Safety Plan for non-contractor employees has been prepared for this project per 310 CMR 40.0018. This Health and Safety Plan will be on site during all field activities described herein, and will be monitored and updated should observations and/or data encountered deem it necessary. Following a contractor bidding and selection process,the successful general contractor will be required to prepare a site-specific Health and Safety Plan in accordance with the documents and specifications for the construction. Areas where excavations are performed will be properly secured at all time using fencing and/or barricades with applicable signage. Ref.#000509C.IRAPDS XI. Permits Required for this IRA,pursuant to 310 CMR 40.0424(1)(h) and Reporting The following permits and approvals are anticipated to be required to complete the work proposed for at this site: Permits/Approval Issuing A ency -Building Permit Town of Barnstable Building Dept. -Electrical Permit Town of Barnstable Building Dept. No other approvals are anticipated to be required for installation and operation of the remedial activities described herein. XII. System Start Up and Extended Operation and Maintenance Groundwater Monitoring Prior to system activation,groundwater samples from site monitoring wells will be collected and analyzed for,at minimum,BTEX,MTBE, and VPH fractions via DEP-approved Methodology. Additional analyses from up to 10 monitoring wells may include dissolved iron via EPA Method 200.1/6010, alkalinity via EPA Method 310.1, carbon,Nitrite via EPA Method 353.3,Nitrite via EPA Method 354.1, Sulfate via EPA Method 375.4, and sulfide EPA Method 376.1. These analyses, combined with in-situ measurements of DO,pH,and/or oxidation redox potential(ORP), conductivity and temperature may be used to evaluate the baseline from which the potential effectiveness of the monitored natural attenuation (MNA)program can be evaluated in the future. These analyses will also aid in determining what effect the AS system operations are having on groundwater chemistry downgradient of the subject property. The results of the VOC analyses will provide a baseline to monitor the relative effectiveness of the active remediation system on the Texaco property over time. Samples will be collected prior to system start-up,to establish the base line conditions, and two additional sampling events will be conducted during the first year of operation. The sampling frequency after the first year of operation may be reduced to semiannual events,based on remedial system performance. System Startup Following start up of the remedial system,Operation and Maintenance(O&M)visits for the first month will be performed approximately on days one,three, seven, and days 14,21,and 28. During each O&M visit,the following tasks at minimum will be completed: • Monitoring of the vacuum applied to each active SVE well head and at the manifold; • Monitoring of the pressure applied to each sparge well(at the manifold); • Monitoring of flow rates(or air velocity)of each SVE and sparge well; • Monitoring of vacuums and pressures at the SVE and AS equipment; • Monitoring of VOC concentrations with a PID of the SVE influent air stream prior to treatment and the effluent air stream; Ref. #000509C. IRAPDS • Monitoring of vacuum readings at selected monitoring wells in order to estimate effective vacuum radial influence of the SVE system; and • Monitoringof water levels and DO in selected monitoring wells in order to estimate effective g sparging radial influence on groundwater(following activation of the sparge system at a later date); Based on the vacuum and flow rates at each SVE well and the pressure and flow rate at each sparge well, flow valves for each well will be adjusted to provide a flow to or from each well which maximizes efficiency of the system. Extended Operation and Maintenance Extended O&M visits will be performed(at a minimum)once per week for the first month of operation after startup, and two visits per month thereafter. This frequency may be modified in the future,based on performance and operating history of the system. The following activities will be completed during routine O&M visits: • Monitoring of the vacuum applied to each active SVE well head and at the manifold; • Monitoring of the pressure applied to each sparge well(at the manifold); • Monitoring of flow rates(or air velocity)of each SVE and sparge well; • Monitoring of vacuums and pressures at the SVE and AS equipment; • Monitoring of VOC concentrations with a PID of the SVE influent air stream prior to treatment and the effluent air stream; and • Monitoring of vacuum readings at selected monitoring wells in order to estimate effective vacuum radial influence of the SVE system; The following activity will be completed once per month during the routine O&M visits: • Monitoring of water levels, and DO in selected monitoring wells in order to estimate effective sparging radial influence on groundwater. It is anticipated that operation of this system will ultimately be part of the Phase IIUIV Remedial Action Plan for achieving a permanent solution at the site. Continual evaluation of the performance of the system will be conducted and all of or portions of the system may be cycled or shut off based on the concentrations of VOCs in extracted air and other system performance criteria. Reporting In accordance with 310 CMR 40.0425, IRA Status Reports will be submitted every 6 months. It is anticipated that the first report documenting remedial system operation will be submitted in February 2003, after the construction of and first few months of operation of the system have been completed. The actual date of submittal will be dependent on the start date and the length of the construction period. The Status reports will include the requirements set fourth in 310 CMR 40.0425 until further evaluation of the site conditions warrant an IRA Completion Report as set fourth in 310 CMR 40.0427. Ref. #000509C. IRAPDS Appendix A Figures � �.�•�fl,.t�M r p ���a��'Y >�'�'�(f� � t? •^fir '• , ,1� �n �..� .�w r ..E."'�-k• nF � r � �� 33 �• f � C?7,. Island l ' T11E SITE � .. . • ... r�,�t`/F .�, �, J l Y :,,-. 4'a,x�y dry .e� _ �.. »' �, /" r �86 °'kr a ��•s ° ( ij •b� • 7 $� �eeh�it o • �r;���''` 1,�J� .s t:-r.r" •: • a •-4-- •i F "` Ey, r � �' p i '� Gooseberry � :�r :•�' 3� � . �a ��'r � t e � u.. /� f otsland •lei' tr °•� R t MVP A 1 EFulfer Lon -.PtPt �£�t• idr � �•o to • �, •yq • r 7 a+f . to a I •." •��` _ • ... q ... (�, .:R f e �� n � _ E r- . rij 10 3�1!•• :r «1►�.• i •`t _ .._ a` ¢_..•4s '* - ° .,.x' - n_ @-s' r. N 1000 0 1000 2000 3000 4000 Feet W E S QUADRANGLE LOCATION UTM COORDINATES: 4 614 214 hT 391 115 E LATITUDE: 41° 40'.27" LONGITUDE'.': 700 18' 29" ZONE 19 FIGURE 1 LOCUSPLAN TEXACO SERVICE STATION#100083 1140 IYANNOUGH ROAD I-IYANNIS,MASSACHUSETTS GEOLOGIC SERVICES CORPORATION GscxEF: 000so9aocus I Checked By: �'��: HydrogeoloOts and Environmental Scientists Drafted By: RJD I I Date: 3/25/02 Source: USGS Topographic Quads-Hyannis,MA 15 Bonaaoli Avenue • Hudson, MA 01749 • (978)568-8740 Quadrangle 15 Minute Series MP-120 MW-3A N MW—')A (BUILDING MW-17 MW- 1A KEY MW-141 / TMP-103 ,MW-18S GROUNDWATER MONITORING WELL MW-14� ( ' TMP-1.02 W-18D AIRSPARGE WELL i ' MW-5 SOIL VAPOR EXTRACTION WELL ' ,GUSTO TEMPORARY MONITORING WELL CPT-1� MW-9 AREA ' IB CATCH BASIN ' MW_6 MW-4 PROPERTY BOUNDARY DIESEL DISPENSER / UST UNDERGROUND STORAGE TANK ISLAND MP-2 SVE1 1 SERVICE MW-4 MP— M 1 STATION I W-1 , MW-10 PT— ®CB-1 TM —101 , � M — 111 I 41k ` �, GASOLINE I DISPENSE ItJG,Z, M —12 ` ISLAND / 0 50 �7 MW-2� I Scale in feet 4� FIGURE 2 SITE PLAN TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.08SITE CHECKED BY: L*A RAFTED BY: SAC DATE: 6 4 .17 02 ` REVISED BY: CD DATE: 8 2 02 GEOLOGIC SERVICES CORPORATION SOURCE: GSC Field Reconnaissance Hydrogeologists and Environmental Scientists 15 Sonazzoli Avenue • Hudson, MA 01749 • (978)568-8740 1 r i r\ \ \/5 \/43, \/45. ♦/ 4.4 \/43.1 ,\42. \/ �\ 4.4 \f \r `r 4, b3,b .� .3 r♦ ,\/6? 6 60. ,♦57.7 .6 r\66 r .0 i 49,3 QU RY \f \r QUARRY \f44.3 ;/44.9 \/65.3 0 \b 44,4 b1.0 9,2 i �67,4 / 4 \/ .0 .�\ 38.5 8 ,0 i� \/60.6 Z/6 \f66,3 r44.3 \/ i� .8 /\ i�43.0 ,\../,39,6 �65. \i /59. �` \/ ~ ib /♦ ? r i\48,8 \/46.4 ♦/ \/45.0 /\ ,�67.6 \ .5 6.5 r \f 64.6 \/ r♦ /\/45.0 r\ / 5.7 \/43.3 40.7 f KEY /\48.4 \� i�4S 7 39,9 � 45,E \46,7 /\ \/45,7 ,r 42,6 f\42.6 65,1 1. / ♦f v/ 67.0 70.9 /♦ VAPOR EXTRACTION WELL �/ \/68. \/ .9 \/b / /\ .0 �, ,7 O AIR SPARGE WELL i1 4P4 / -----.____. `` %`� MONITORING WELL \ /♦ \/ 8 \/ 8 CONE PENETROMETER LOCATION \ ,5 i�41.3 �/41 i\ \ '' ' " , , � TEMPORARY MONITORING WELL f4 � ` �4 \r /57.9 \� rb�;.," / 5 �f b. ♦/ \/ ♦f87.7 /. /,. .2 ♦!'. '�'"'''`� ,,, .!,, ,,♦64,6 \ 60 65.1 / °+.' PROPOSE© TEMPORARY MONFFAi WELL ,�♦42,6 r♦7 /♦ / � � ' /� ,--'` ,, 37.9 70.9 O MANHOLE \ w 47.0 .�', 70.5 7Q \/ -- - • \ „� i�5 i ti .a68.8 ': / t � i UTILITY POLE tif70 ,\ 70.1 / - /♦65. 65.3 r 9 �. \/ ,. / ER CATCH BASIN j/70.5 r65.4 ,, 7 1\ /�68,8 $, T n �`66.5 / � /♦ \, nr IRRIGATION WELL , i69.2 -.., •,,/ LOT BOUNDARY :x �ti63 b `'` �`" �, BUILDING LINE 7 70.5 \ 64.5 ® TMP—tps''-- _. CONTOUR ) \ 4.8 6?,4 ,,,• PAVED SURFACE ELEVATION CONTO FEET 66,2 69, /\ `�. o . _. EDGE OF SURFACE WA _.r /♦ b7,7 / \/ FAC TER r - i \ f 62,6 r♦ 6� ' 69.1 / .3 f♦ 6,4 �� :' \b4,4 PARK1Nti`� 3,1 \ ,\ 4.5 \/70.5 /.� \f /\65,4 \/67,1 63 , ♦r \/ ry /v 6 3,5 ,\/66 i/65,7 /\ /\67.4 �6 \r69.$ ,�♦64,1 \/67A TMP-118 /\61.1 69.2 , .5 /\ \67 3 4 \63 8 \/67.0 ` , 0.7 : , r\ P_ _. TM 23 TMP 1fls `6 / r { i 64,7 \ ♦f \r i \r 60, / .�\ :.: 7,1 67. \/ • , _ ..,.. 67.., t 1,0 .6 63, r\ 66,6 .: 66,E CPT-3P, 1 a7 „ , .♦ /"� �, / 2;6 ♦1 - 64, , ., \/ „ 1 \ \f 4 / 0 \/ 8 r \� — s 2fl ss sa .,, k \ - \/ 62,8 t 66.8 .3 / / '~ \69. / / 43 7 .9P-108 `+�/ 116 64, i Mw-15 zfl 659 66,9 . ,. 1\ ., 2 _.. ,.., _ ., 64.3 5 ,3 �°, 61.4 Mw—�s s5 \ : { —16 2fl f \ ® 64,7 / /+ 4, A . 5 9 MW, 1'6 90 C�--` 69,�a > ..... , 64 \/ i \/ P �i ; i ,�j� 3 r V Iw 3A I 67 L'. 6 : t \ , 31,30 r\ T R EV ;,.., r \ Mw ! 2.7 ' � ,,.2a 55 90 64,7 6 ., 63 / POND /♦ � M � za �fb ` /42; Y .` Mw 14 TMP-1a ) W—,1A$ r�6812 bl � TMR 2 \/67,1 f' / 1-5 —6 , ♦ ♦f 7,� 68, —9 i 6 , 47.0 CPT-1 67. Pr .r MIIlIy C8-1 \66,4 , 6 c� Mw-1 01 .S ' 6 /44. \ �t $TMP— 1 \ 68.3 37, O 66,8 \ \/ 38.1 66, , / A-TER ELEV. Mw-� \/ //64.7 04 \/631 ' -- 32,14 .......... ARKTNG \ �6, \/ i66,66. \/ /6 ---- ,._. . ,� POND 4,9 ., \673 q \/6 z / r ; ,. . 5,9 58.6 '4.J / 65.8 44.0 65, 651 \ 4J i`b.,' ,5 lu ,\6 .8 GR® N SCUR A \,�42.3 /\46`8/42 $,9 \ 64 40 \ ,1 /\63.2 4. ,\54.2 0, UNP ED PARKT M. \/67.3 ,\ , / Q \/50.9 ♦/ \ ./ 0.$ �\ \f4 \/34 / /.�47.3 ' \ 6 8 \ r \/4 43, 6 ,1 0.3 Y, 6.8 /\65,. " ..: 0 100 ,f /\49.2 \/65 / Seale in feet �. 4 ! \/65. \/ \ „ k 5,4 ; 4b 1 I 8/\ ,. f52. \ ♦,• r\, r _ ° FIGURE 3 / 63,4 ;., � ' r � ,, � ,. . . ... / / AREA PLAN 65. ... ♦/ 48,9 j ♦/ � : . ,, TEXACO SERVICE STATION 100083 i \f \ /\ ,1 49..E \. 4 r\46,2 i\ r r ,�\57,6 1140 IYANNOUGH ROAD /\ \ �55,6 \4 .` HYANNIS MASSACHUSETTS \/ µ \49, GSC .REF.; CHECKE:O BY: 1 � \f Y: , 64 A.: : i 02 GEOLOGIC SERVICES CORPORATION :F REVISED BY: SOURCE: GSG Field Reconnaissance, Town of BarnstableG.I.S. Unit i , i -- — Large Format Box # Doc # C Image # IMF G E e ---- - i 211,11, LJ MA Towns Text-Town Names ON tv .Town Arcs MEMO IV County Arcs Water Supplies 1 \\ "` Surface �. - \\ � Non Community - Ground Water Tinsmission Lines � .Pipeline Arbitrary Extension �VPowerllne Arbitrary Extension Trains 'IV,Landing Strip/Airport MHD Roads Limited Access Highway SE1101 IV other Numbered Hwy ,. �. Sig Major Road-Connector 1:00 MN Minor Street or Road \ \ . �. Trail . . as ` \�,.�w wee \, ���, Water - INS Potential Drinking Water Sourc SNIN ���- \ • HIGH YIELD =1 MEDIUM YIELD r 00 IS MA Certified Vernal Pools ` 100 ! M MA Rare Habitat S 'sue !, �e sources � � \ �. \ Zone lie 1 Iii , l llll mum Sole Source Aquifers 2 itm Openspace Major Basins Rivers&Streams mow Solid Waste Sites FIGURE 4 GIS MAP AND LEGEND: • ��• ••� GEOLOGIC SERVICES CORPORATION W .....i 1� • .•- • •• • . 1 � SYMBOL & LEGEND SHEET INSTRUMENTATION & CONTROLS EQUIPMENTT g f-% VAPOR PHASE S LINE DESIGNATION: PRIMARY ELEMENT SYMBOLS f SYMBOL SPECIFICATION OIL WATER 's;'f c� 3� CARBON SEPARATOR ��t��.r 1 AIR COMPRESSOR 2 — VR — 0 t — PV ff O LEVEL SWITCH INSTRUMENT TYPE: SIZE IN PROCESS UNE MATERIAL IN <<t CHES NUMBER SPECIFICATION LOW LOW LEVEL SWITCH LOW PS PRESSURE SWITCH PI PRESSURE INDICATOR WELL PROCESS LINE INDICATORS FI LOW INDICATOR BAG FILTER WITH O LEVEL SWITCH HIGH F01 FLOW METER (TOTALIZING) PUMP PACKED COLUMN FLOW AIR STRIPPING DIRECTION ® LEVEL CI CAPACITIVE SENSOR HIGH HIGH TI TEMPERATURE INDICATOR LIQUID PHASE TOWERLIOUID PUMP RING FCARBON MAJOR PROCESS O PRESSURE SWITCH TT TEMPERATURE TRANSDUCER RP MINOR PROCESS HIGH TS TEMPERATURE SENSOR ^� Y CENTRIFUGAL n SKIMMER _ _ WATER/AIR O PRESSURE SWITCH LEL EXPLOSMTY METER PUMP }IJ� PUMP PIPING AIR OLOW ros PRESSURE DIFFERENTIAL SL STATUS LAMP SNITCH PC PRESSURE CONTROL PIPING SP SAMPLE POINT ALL']1 ROTARY VANE ____ O PRESSURE INDICATOR COMPRESSOR INSTRUMENTATION CONTROLS J� LIQUID.PHASE DIAPHRAM '= FLOW SWITCH INSTRUMENTATION 1`1 DISPLACEMENT PUMP CARBON PUMP -af rf` PNEUMATIC LINE (STEEL) TT _� O FLOW METER INSTRUMENT TYPE PI CONNECTING LINE SYSTEM DESIGNATION VEt SYSTEM POSITION NUMBER PRODUCT PROPORTIONING I " TEMPERATURE INDICATOR DRUM PUMP LOW PROFILE — CROSSOVER LINE I ray TEMPERATURE SWITCH TYPE IAHEMSITE CONTROL PANEL OUTPUTS STRIPPER HIGH SENSOR TYPE h NUMBER SLIISat CENTRIFUGAL INLET BLOWER ra TEMPERATURE SWITCH FILTER PUMP PROCESS LINE ABBREVATIONS Low (SENSOR DESIGNATION) 121 ES - ELECTRIC SUPPLY LEVEL ALARM Low D 0 1 8 SENSOR POSITIVE CONDENSER j� A.�TE °INPUT NUMBER DISPLACEMENT GS - GAS SUPPLY 5z;z LEVEL ALARM HIGH H-H1 SPEED BLOWER ,,,' 'p HS - HYDRAULIC SUPPLY MOISTURE satNlcE LIQUID PRESSURE ALARM LOW ® INSTRUMENT IS CONTROLLED SEPARATOR HEATER RING PUMP NS - NITROGEN SUPPLY OFFSITE BY SCADA INTERFACE . @ HOLDING TANK SS - STEAM SUPPLY BLOWER 0 PITOTETUBE T SILENCER W WATER SUPPLY INSTRUMENT WITH INPUTS OR OUTPUTS V - VACUUM © AVERAGING e LOCATED AT A LOCAL CONTROL PANEL PITOT TUBE OTHER THAN THE SITE CONTROL PANEL CONTROL VALVE VR - VAPOR REMOVAL ® POSITIVE DISPLACEMENT 'rF - TOTAL FLUIDS FLOW INDICATOR GENERAL INSTRUMENT OR FUNCTION SYMBOLS �r� BODIES ACTUATORS J REGULATORS FITTINGS & PIPING PROPELLER OR PRIMARYNE TYPE ICJ BALL Va VE T GEAR ACTUATOR V FOOT VALVE AP — ACCESS PIPE / CONDUIT ® FLOWTURBI ELEMENT LOCATION FIELD AUXILIARY �[�F—EXPANSION JOINT/SLEEVE SA - SPARGE AIR NORMALLY MOUNTED NORMALLYACCESSIBLE GATE VALVE r-r TI D❑ VORTEX SENSOR ACCESSIBLE TO ACCESSIBLE TO C'4 " VICTAULIC CONNECTOR —{ HOSE CONNEC ON t PRESSURE RELIEF PN - PNEUMATIC SUPPLY OPERATOR OPERATOR Da GLOBE VALVE 1�- CROSSOVER �d PLUG 4 DIAPHRAGM ACTUATOR a SONIC FLOWMETER INSTRUMENTS e O e f TARGET TYPE SENSOR FLANGED CONNECTION PIPE CAP MATERIAL SPECIFICATON: Q a f'�J BUTTERFLY VALVE -+- SCREWED CONNECTION � SLIP UPDRAFT VENT CAP HYDRAULIC ACTUATOR PV - POLYVINYL CHLORIDE WEIR SHARED Iti SWING CHECK VALVE -+k— UNION O$ ELBOW - TURNED UP GM - GALVANIZED SHARED coNTFAY —I-+— COUPLING � DIAPHRAGM VALVE RC — RIGID COPPER �� VENTURI ❑S SOLENOID ACTUATOR �_ O-I�- ELBOW - TURNED DOWN TUBE O W I BALL CHECK VALVE TT REGULATOR IR - IRON FLOW ROO LOGIC INTERLOCK P_i0000 PUMP ELBOW - 90' NOZZLE wP-100 WELL PUMP FLOW INDICATOR ABS— ACRYLONITRILE BUTADENE STYRENE H_1o00 BLOWER Y� INSTRUMENTS IHARING H HEATER NEEDLE VALVE 4 MOTOR ACTUATOR � � ELBOW - 45' FL - FLEX } LEVEL SWITCH 00 COMMON HOUSING W-,� MOTOR vA��� C�J 3 WAY VALVE 4 DIGITAL ACTUATOR RUPTURE DISK FLOATS y� Sv-IOO SOLENOID VALVE �+ v REDUCER uP ELBOW - LONG RADIUS 1 O PLAT LIGHT°R 1 ALARM INDICATOR 4 WAY VALVE n WATER ACTUATOR fV STRAINER REDUCING ELBOW Lx N FLOW SAMPLE VALVE Y ® RESTRICTOR TEE REDUCING } z PRESSURE VALVE ABBREVIATIONS RELIEF VALVE -+p.F_ TEE (OUTLET UP) FIGURE 1 1 PROCESS AND INSTRUMENTATION DIAGRAM LEGEND OUIN.C. - NORMALLY CLOSED w/CFLEX HOSE -+C>H TEE (OUTLET DOWN) TEXACO SERVICE STATION 100083 N.O. - NORMALLY CLOSED p MAN _ MANUAL 4 QUICK CONNECT T. TEE 1 140 IYANOUGH ROAD COUPLING HYANNIS, MASSACHUSETTS °j PRESURE INDICATOR GSC REF.: 000509.01 LEGEND CHECKED BY: DM SAMPLE VALVE DRAFTED BY: SC DATE: 7 22 02 ISOLATION VALVE REVISED BY: DATE: SOURCE: GSC ENGINEERING DEPARTMENT GEOLOGIC SERVICES CORPORATION Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue •Hudson,MA 01749 •(978)568-8740 J F I } ••CRITICAL DEVICE — INLET AMBIENT AIR FILTER 1 ; SPARGE ZONE TAH TIMER PANEL 1 (U TSH TI FI TI HOA r' ASC01 AIR COOLED HEAT EXCHANGER (IF NECESSARY) DILUTION ROTARY VANE EXPECTED EXPECTED VAPOR PHASE CARBON OPTION COMPRESSOR I I POSITION PRESSURE FLOW I DISCHARGE TO SVE-SPOT -5.3 RVC 308 ATMOSPHERE I (3) t LAH PI I VGACSVE I I FI FI FI FI FI Ft � SP02 ' ASO1 AS02 AS03 AS06 AS07 AS08 LSH SVE-DV PI PI PI PI PI PI SVE — — — — I 1 �SOI AS02 AS03 AS06 AS07 AS08 SVE SPOT S Q PSL PAL (771 I TAH PI PI 1 VE SVE SP03 SP04 FI TI SVE SVE TSH r- J r- J r- --I r- J r- J r- J I I— SP04 SP04 ID&I SEPARATOR FIOA I AIR �LED EXCHANGER VAPOR PHASE VAPOR PHASE Svc (IF NECESSARY) II I (500 C lb (500Ib) SVEOI VEO SVEIO SVEII SOWER _J SACK PRESSURE W/CARBON EDJ ASO1 AS02 AS03 AS06 AS07 ASOS I POSITION PRESSURE EXPEOW SVE01 VEO SVEIO SVE11 (a>� SVE-SP04 -8 IWC -yp8 NOTE: TYPICAL AIR SPARGE MANIFOLD OIAGRAM. ACTUAL MANIFOLO CONSTRUCTION SVE01 SVE02 SVEIO SVEII WILL INCLUDE TWO ZONES OF 4 LEGS RESPECTIVELY. L — TREATMENT SYSTEM ENCLOSURE AIR SPARGE WELLS & MANIFOLD EXPECTED EXPECTEDM2-.h ASING BOREHOLE DEPTH T SCREEN POSITION PRESSURE FLOWE OUWETER WATER INTERVAL r J r J r J r J ASO1 -10 PSI 6-10 SCFM -Inch 8-inch 30'-32' -47'-49' AS02 -10 PSI 6-10 SCFM -inch 8-inch 30'-32' -47'-49' A503 -10 PSI 6-10 SCFM inch 8-inch 30'-32' -47'-49' ASO4 -10 PSI 6-10 SCFM2-inch 8-inch -30'-32' -47'-49' AS05 -10 PSI 6-10 SCFM2-inch 8-inch 30'-32' -47'-49' AS06 -10 PSI 6-10 SCFM2-inch 8-inch 30'-32' -47'-49' ;? AS07 -10 PSI 6-10 SCFM2 inch 8-inch 30'-32 -47'-49' ASOB -10 PSI 6-10 SCFY2-inch 8-inch 30'-32 -47'-49' 1 E3 El SVEOI SVE02 SVEIO SVEI1 WTERLOCK/FAILSAFE SCHEDULE NOTE:EOUIPMEM VENDOR SHALL SIZE ME AIR SPARGE I.D. LOCATION FUNCTION COMPRESSOR/BLOWER TO DELIVER 6-10 SCFM TO TOUR - OF THE SPARGE WELLS AT ANY TIME (1) AS/SVE MOTOR INTERLOCK AS MOTOR CANNOT OPERATE WITHOUT THE SVE MOTOR RUNNING. SHUTS AS MOTOR DOWN IF SVE MOTOR FAILS ((jA�S.�S,�UMES THAT THE AIR SPARGE TIMERS WILL BE VAPOR EXTRACTION WELLS (2) SVE LOW PRESSURE SWITCH DEACTIVATES AS MOTOR IF SWITCH SENSES LOW VACUUM ON THE SVE MANIFOLD PIPING CONFlGUREO TO CYCLE THE SPARGE WELLS FOUR-ON. FOUR-OFF). EXPECTED EXPECTED TOTAL CASING BOREHOLE DEPTH TO SCREEN POSITION � VACUUM ROW DEPTH ETE DIAMETER WATER INTERVAL (3) MOISTURE SEPARATOR NIGH LEVEL SWITCH DEACTIVATES SVE MOTOR IF A HIGH LIOUID LEVEL f5 PRESENT IN THE SVE MOISTURE SEPARATOR AIR SPARGE WELL CONSTRUCTION INCLUDES TWO FEET OF (4) CATOX GENERAL ALARM OFF GAS HIGH TEMP DEACTIVATES SVE MOTOR IF ALARM IS DETECTED BY CATOX OR HIGH TEMP IS SENSED IN OFF GAS DEPENDS ON OFF GAS TREATMENT METHOD TWO-INCH 0.010 SLOT PVC WELL SCREEN. SVEOI 1.3 IWC 28 SCFM 36' 4-1nch 12-inch -30'-32'26'-36' IN SVE02 1.3 RYC 28 SCFM 36' 4-inch 12-inch -30'-32'26'-36' (5) AS MGM TEMP DEACTIVATES AS MOTOR IF HIGH TEMP IS SENSED IN AIR FLOW SVE03 1.3 IWC 28 SCFM 36 4 inch 12-inch -30'-32'26'-36' .. SVE04 1.3 IWC 28 SCFM 36' 4-inch 12-inch -30'-32'26-36' AIR SPARGE COMPRESSOR SVE05 1.3 IWC 28 SCFM 36' 4-inch 12-inch -30'-32'26-36' FIGURE 1 EXPECTED EXPECTED EXPECTED SVEOG 1.3 MC 28 SCFM 36' 4-inch 12-into -30'-32'26'-36' PosR1oN PRESSURE FLOW TEMP. S,E07 1.3 RYC 28 SCFM 36 4_;nc„ ,2_nch -30'_,2 26_36' PROCESS AND INSTRUMENTATION DIAGRAM PI-AS' I PSI - - SVE08 1.3 RIC 28 SCFM 36' _4-imh 12'nch -30'-32'26'-36 TEXACO SERVICE STATION #1 00083 Fl-A51 24-40 SCFM SVE09 1.3 IIV 28 SCFM-- 36 4-inch 12-inch -30'-32 26'-36' TI-ASI --- - - TOO SVEIO 1.3 RFC 28 SCFM 36' 4-inch 12-inch -30'-32'26'-36' 1140 IYANOUGH ROAD svE,t 1.3 IWC 28 SCFM 36 4-inch 12-inch -30'-32'26'-36' HYANNIS, MASSACHUSETTS NOTE:ACTUAL T1-A$1 TEMPERATURE IS DEPENDANT ON co11PRESsoit SPECIFIED BY VENWR GSC REF.: 000509.04PID CHECKED BY: DM DRAFTED BY: SC DATE: 7 22 02 REVISED BY: DATE: SOURCE: GSC ENGINEERING DEPARTMENT (� VEOLOGIC SERVICES CORPORATION ydrogeologists and Environmental Scientists 15 Bonazzoli Avenue • Hudson,MA 01749 •(978)568-8740 24" MIN. TRAFFIC BEARING ROAD BOX 24' BOLTDOWN TYPE WITH RUBBER GASKET, 12" DIAMETER EXISTING SURFACE TRAFFIC NEARING ROAD BOX BOLTDOWN TYPE WITH RUBBER CASKET, 8' OIAMEIER EXISTING SURFACE • .• 6" MIN. 6'MIN. 4" DIAMETER SCH. 40 RISER V. SELECTED NATURAL BACKFILL 3' 2' DIAMETER SCH. 40 THREADED RISER CONCRETE PAD 24' z 24' COMPACTED IN 6" LIFTS CONCRETE PACT 24' z 24' SELECTED NATURAL BACKFILL 3' jL . . . . . PC,MANIF•0LD PIPI TOWARD,W L� COMPACTED IN 6"-LIFTS 4" EXPANDABLE LOCKING GRIPPER CAP (MIN S _.1 OR) . 2' PVC THREADED PLUG .AIR SPARGE . BACKFILL WITH NATURAL MATERIAL VgPOR E%TRACTION 1' MIN .1'. . . . .0 PVC PIPE 2 0 SCH. 40 PVC PIPE NATIVE BACKFILL MATERIAL 12" MIT- BENTONITE SEAL .'. I 3/8" PEASTONE OR _ i i 3/8" PEASTONE OR CLEAN WASHED STONE CEMENT - SENTONITE GROUT S CLEAN WASHED SAND 10' MIN. (DEPENDENT ON , ' , , TO APPROXIMATELY 4' BELOW CRADE NATIVE BACKFILL BOTTOM OF TRENCH SUBSURFACE MATERIAL) BOTTOM OF TRENCH 4" DIAMETER SCH. 40 THREADED RISER 2' DIAMETER SCH. 40 TNitiA0E0 RISER 24' MII BENiONITE SEAL 12' MIN. BENTONITE SEAL 1' MIN. 0.010" SLOT THREADED SCREEN �24 12' MIN 0.010' SLOT THREADED SCREEN �24 -_-_ ............ SAND FILTER PACK - SAND FILTER PACK - 10' MAX. .1. __--_ Q 24 24' MAX. _ Q 24' - _ 2" PVC PLUG 4' PVC PLUG TRAFFIC BEARING ROAD BOX TRAFFIC BEARING ROAD BOX BOLTDOWN TYPE WITH RUBBER BOLTDOWN TYPE WITH RUBBER VAPOR EXTRACTION WELLHEAD DETAIL GASKET, 12" DIAMETER AIR SPARGE WELLHEAD DETAIL. , GASKET, 8" DIAMETER NOT TO SCALE VAPOR EXTRACTION NOT TO SCALEAIR SPARGE WELL MONUMENT DETAIL WELL MONUMENT DETAIL NOT TO SCALE NOT TO SCALE HOT TAR PATCH AT EDGE OF NEW PAVEMENT HOT TAR PATCH AT EDGE OF NEW PAVEMENT HOT TAR PATCH AT EDGE OF NEW PAVEMENT - 2' BITUMINOUS CONCRETE EXISTING BITUMINOUS 2' BITUMINOUS CONCRETE EXISTING BITUMINOUS - 2 BITUMINOUS CONCRETE EXISTING BITUMINOUS .- 4'VASE BITUMINOUS CONCRETE CONCRETE PAVEMENT •- 4'VASE BITUMINOUS CONCRETE CONCRETE PAVEMENT -. 4'80.5E BITUMINOUS CONCRETE CONCRETE PAVEMENT ROAD BASE-GRAQE GRAVEL = `ROAD BASE-CRAQE GRAVEL = ROAD BASE-CRAQE GRAVEL i k COMPACTED IN 6 LIFTS 7 COMPACTED IN 6 LIFTS Z COMPACTED IN 6 LIFTS p p o 1 1 1 M N 41 SELECTED NATURAL BACKFILL SELECTED NATURAL BACKflLL SELECTED NATURAL BACKFILL COMPACTED IN 6"LIFTS COMPACTED IN 6'LIFTS COMPACTED IN 6'LIFTS 7 O O O �� RRpp 1 yy 1 22 1 Ca1Tg1N TAOPFE YELLOW ...4.-... M CaJf�lON TAPE YELLOW _ ♦1 CAU TAPE YELLOW ::.4._:.'. .. .. ..... .. .. ...... .- .. ...... a'BED e" BED 1 2 BED 8 t'. SCH. BO PVC 1 1". SCH. 80 PVC AIR P N SPARGE u a�S E E N SPARGE LIE FIGURE 9 a' BEE) 4- BED z) z'. SCH. 40 PVC TRENCH AN V A R SECTION cosssc o osE s tt 2'e SCH. 40 PVC VAPOR E%TRACTION UNE E ( ) (1 2'. SCH. 40 PVC - / V M N VAPOR EXTRACTION LINE vA� N I OR E O N I BEO xrRACTI L E 2 W I HA CONSTRUCTION N TA WELL R 0 DETAILS e'BED a'BED t HEAD CO S UC E T XA R STATION E CO SERVICE STA 0 #100083 3SCCRREENNEED SOIL R SCREENED SOIL OR SCREENED SOIL OR 3/8 PEA STONE 3/a PEA STONE 1 140 IYANOUGH ROAD TYPICAL TRENCH DETAIL TYPICAL TRENCH DETAIL TYPICAL TRENCH DETAIL HYANNIS, MASSACHUSETTS CROSS—SECTION A—A' CROSS—SECTION 8—B'_ CROSS—SECTION C—C' GSC REF.: 000509.04DETAIL CHLD BY: NOT TO SCALE NOT TO SCALE NOT TO SCALE DRAFTED BY: SC DA 22 02REVISED BY: DA` � GEOLOGIC SERVICES CORPORATION SOURCE: GSC ENGINEERING DEPARTMEN Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue •Hudson,MA 01749 •(978)568-8740 F j 1 f ` Ih I TMP-120 MW-3A N , I M WA � `O BUILDING MW' 17 MW-1A MW-14D I IMW—18S Y KEY MW—141# W— 18D MW— 14 � � M _ TMP- 103 f ' W / GROUNDWATER MONITORING WELL Mf-6 / O AIRSPARGE WELL CPT—1 ® SOIL VAPOR EXTRACTION WELL -_�B B I ® PROPOSED SOIL VAPOR EXTRACTION WELL MW-4 % ® PROPOSED AIR SPARGE WELL AS—1 VE-1 SERVICE TEMPORARY. MONITORING WELL MP— STATION — ® CATCH BASIN 1-'$MW—1 f MW— 0 1 — --- PROPERTY BOUNDARY CPT-2 .®CB— T P�—�l Ow O M —1 1 /f -MW-1 i 0 50 2 `W-2 f Scole in feet �. FIGURE 8 PROPOSED TRENCH LAYOUT TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS [REVISED C REF.: 000509.06TREN CHECKED BY:I'l AFTED BY: SAC DATE. 8 12 02 BY: DATE: �GEOLOGIC SERVICES CORPORATIONURCE: GSC ENGINEERING DEPARTMENT Hydrogeologists and Environmental Scientists 15 Bonaaoli Avenue • Hudson,MA 01749 •(978)568-8740 I i . I ' TMP-120 I MW-3A N ' M W-A BUILDING M ' , 7 MW-1 A MW—'I41# MW1 18S MW- 14 TMP-102 TMP-103 ;""W-18D I _j$MW-5® I GROUNDWATER MONITORING WELL I ® Q ® I 0. AIRSPARGE WELL M —9 ® MW— C — 1 ® ® SOIL VAPOR EXTRACTION WELL I / ® PROPOSED SOIL VAPOR EXTRACTION WELL ® MW-4 ® / ® PROPOSED AIR SPARGE WELL ' OMP �VE1 SERVICE ` 41 TEMPORARY MONITORING WELL P— TATION / M 1 _1 ® CATCH BASIN I MW— 0 — --- PROPERTY BOUNDARY CPT-2 .®C —1 TMP 101 ® M — 11 / 0 50 BMW-12 V I MW-2 / Scale in feet • FIGURE 7 PROPOSED WELL NETWORK LAYOUT AND CONCEPTUAL RADII OF INFLUENCE TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.07ROI CHECKED BY: DRAFTED BY: SAC DATE: 8 13 02 REVISED BY: DATE: GEOLOGIC SERVICES CORPORATION SOURCE: GSC ENGINEERING DEPARTMENT Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue •Hudson,MA 01749 •(978)568-8740 MW-15 N 64.98 <5.0 <5.0 <5.0 TOYS R US <10.o MW-16 55 <5.0 64.99 MW-16 20 414 64.99 <5.0 <5.0 <5.0 <5.0 <10.0 <5.0 4,280 <10.0 <5.0 E&B DISCOUNT MARINE TMP-5 �\ ® O TMP-6 LANDSCAPE AREA MW-3A 65.18 JENNY <5.0 CRAIG PARKER'S <5.0 MATTRESS TMP-1 0-TMP-7 LIQUORS <5.0 GIANT <10.0 MW- A MW-14 90 <5.0 65,16 PARKING 122 LOT 62.27 MW-17 L4/�OS <5.0 MW-14 70 <5.0 65.74 ARE Ap�O <5.0 TMP-2 65.41 <5.0 <5.0 <5.0 <5.0 MW-5 MW-18 25 11 <5.0 <10.0 <5.0 65.80 65.13 2,700 TMP-3 <5.0 <5.0 <5.0 1,520 <5.0 <10.0 <10.0 ' 10,400 MAW-6 <5.0 MW-18 70 <5.0 <5.0 2 000 <5.0 65.81 65.19 51 11 540 <10.0 TMP-4 `6S MW-9 36,000 .4 26.8 <5.0 0 J <5.0 65.82 8.3 <5.0 O MW-14 25 1,620 , 18.3 <10.0 65.39 16,800 1,170 <5.0 <5.0 2,950 �^`�� TMP-103 <5.0 17 760 � S ` MW-1A <10.0 6,880 ` �� TO,Q �' 65.13 <5.0 / A -1 \�•� qcF ` <5.0 MP ; �S PARKING <5.0 SVE-1 ` JAMES � � MW-1 Myy_4 LOT <10.0 REALMUR ESTATE _MP-3 6.84 NS / �S <5.0 MW 10 65.84 MP- 48 22 , �S <5.0 CPT-2 �Q 67.5 <5.0 MP-101 7. <5.0 \ 637 <10.0 I LAND MW-1 1 <5.0 \ 65.95 <5.0 MW-2 CUMBERLAND FARMS/ 65.75 65.99 <5.0 GULF SERVICE STAITION <5.0 <5.0<5.0 10.0< ` <5.0<5.0 <5.0 102 <5.0 <10.0 <10.0 . lI4 20.4 AV MW-13 65.82 <5.0 <5.0 O <5.0 `9, <5.0 0_ 60 Scale in feet RAMADA KEY INN < BELOW METHOD DETECTION LIMIT � CONE PENETROMETER POINT UST UNDERGROUND STORAGE TANK DATA COLLECTED ON 5/1/02 TEMPORARY MONITORING O MANHOLE NOTE: MW-2, MW-1 1 MW-14(N-18(70) WELL POINT -65.80 GROUNDWATER CONTOUR MW-1490) MW-16(�5),NG AND � MONITORING WELL `r APPARENT GROUNDWATER NOT USED IN CONTOURI O AIRSPARGE WELL FLOW DIRECTION FIGURE 6 MW-13 WELL IDENTIFICATION GROUNDWATER CONTOUR/ SOIL VAPOR 65.82 WATER TABLE ELEVATION (ft) HYDROCARBON DISTRIBUTION PLAN ® EXTRACTION WELL TEXACO SERVICE STATION #100083 <5.0 BENZENE (ug/I) 1140 IYANNOUGH ROAD ® CATCH BASIN <5.0 TOLUENE (ug/1) HYANNIS, MASSACHUSETTS - - - PROPERTY BOUNDARY <5.0 ETHYLBENZENE (ug/1) GSC REF.: 000509.01 MAY02B CHECKED BY: M NS NOT SAMPLED <10.0 XYLENES (ug/1) DRAFTED BY: ANG DATE: 9 18 01 <5.0 MTBE (ug/1) REVISED BY: ANG DATE: 7 2 02 ` j C GEOLOGIC SERVICES CORPORATION SOURCE: SAGE ENVIROMENTAL PLAN AND GSC Hydrogeologists and Environmental Scientists FIELD RECONNAISSANCE 15 Bonazzoli Avenue • Hudson,MA 01749 •(978)568-8740 MW-15 N 64.27 <5.0 <5.0 <5.0 TOYS R US <5.0 MW-16D <5.0 64.25 1,410 <50 <50 <50 11,500 E&B DISCOUNT MARINE TMP-5 Q MW-16 ® 64.23 <5.0 TMP-6 <s.0 MW-3A 0. <5.0 64.41 <5.0 LANDSCAPED JENNY <5.0 AREA� <5.0 CRAIG <5.0 MATTRESS ATN TMRESS - 1 OTMP-7 <5.0 PARKER'S 50.6 PARKING LIQUORS LOT MW-14 MW-17 64.63 65.02 L%Ds TMP- <5.0 <5.0 gRfq pf0 MW-5 _ <5.0 <5.0 65.02 64.34 .TMP-3 MW-1A <5.0 2,260 <5.0 �� 10,000 `` 14.1 64.27 <5.0 <5.0 <5.0 1 390 MW-6 <5.0 <5.0 7 690 65.55 <5.0 T _4 <5.0 46,900 15.6 214 <5.0 MW-9 <5.0 AS-1 64.96 <5.0 64.93 1.28ft. NAPL <5.0 <5.0 / SVE-1 173 <5.0 61.30 <5.0 `�N, <5.0 MW-1 1 65.06 ` P- <5.0 PARKING 6.1JAM8 MURPHY <5.0 LOT REAL ESTATE MP-31 ® MW-4 MID 1 65.76 <5.0 <5.0 MW-1 <5.0 MW-10 65.04 <5.0 DRY 42.3 <5.0 KEY 140 <5.0 -0 TEMPORARY MONITORING WELL POINT LANDSCAPED 63.8 15.2 GROUNDWATER MONITORING WELL AREA 274.1 MW-2 COOKE'S 768 RESTAURANT O AIRSPARGE WELL ROAD WAY � 65.08 ® SOIL VAPOR EXTRACTION WELL MOTEL PROPERTY MW-12 64.92 ® <5.0 ® CATCH BASIN <5.0 <S,p PROPERTY BOUNDARY <5.0 <S.0 UST UNDERGROUND STORAGE TANK <5.0 <5.0 -64.80 GROUNDWATER CONTOUR <5.0 J� t- APPARENT GROUNDWATER �94 O FLOW DIRECTION �y MW-13 WELL IDENTIFICATION 64.90 WATER TABLE ELEVATION (ft) MW-13 <5.0 BENZENE (ug/1) 64.90 �� <5.0 TOLUENE (ug/1) <5.0 40 <5.0 ETHYLBENZENE (ug/1) <5.0 <5.0 XYLENES (ug/1) <5.0 <5.0 MTBE (ug/1) <5.0 < BELOW METHOD DETECTION LIMIT - NAPL NON-AQUEOUS PHASE LIQUIDLL NOTE: WELLS MW=10, AS-1 AND MW-16D RAMADA ARE NOT USED IN CONTOURING INN DATA COLLECTED ON 12/4/01 0 60 Scale in feet FIGURE 5 GROUNDWATER CONTOUR/HYDROCARBON DISTRIBUTION PLAN TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.04DEC01 CHECKED BY: VIA DRAFTED BY: ANG DATE: 9 18 0 ` REVISED BY: RJD DATE: 3 26 02 c GEOLOGIC SERVICES CORPORATION SOURCE: SAGE ENVIROMENTAL PLAN AND GSC Hydrogeologists and EnviroVmental Scientists FIELD RECONNAISSANCE 15 Bonazzoli Avenue • Hudson,MA 01749 (978)568-8740 L i Appendix B Tables Table 1 Page 1 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation AS-1 4/4/01 98.97 32.42 ND 66.55 4/9/01 98.97 32.11 ND 66.86 4/19/01 98.97 31.65 ND 67.32 4/23/01 98.97 31.50 ND 67.47 5/3/01 98.97 31.35 ND 67.62 6/27/01 98.97 32.06 ND 66.91 8/16/01 98.97 32.29 ND 66.68 12/4/01 98.97 34.04 ND 64.93 12/12/01 98.97 34.19 ND 64.78 1/18/02 98.97 34.22 ND 64.75 MP-1 4/9/01 98.77 31.84 ND 66.93 4/19/01 98.77 31.36 ND 67.41 6/27/01 98.77 31.28 ND 67.49 8/16/01 98.77 32.02 ND 66.75 12/4/01 98.77 33.80 ND 64.97 12/12/01 1 98.77 33.91 ND 64.86 MP-2 4/9/01 99.05 32.09 ND 66.96 4/19/01 99.05 31.62 ND 67.43 6/27/01 99.05 31.54 ND 67.51 8/16/01 99.05 32.28 ND 66.77 12/4/01 99.05 34.02 ND 65.03 12/12/01 99.05 34.17 ND - - 64.88 MP-3 4/9/01 99.07 32.14 ND - - 66.93 4/19/01 99.07 31.72 ND - - 67.35 6/27/01 99.07 31.65 ND - 67.42 8/16/01 99.07 32.37 ND - - 66.70 1.2/4/01 99.07 34.12 ND - - 64.95 12/12/01 99.07 34.27 ND 64.80 Ref.: tpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:25 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 2 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-1 1/13/99 98.66 30.49 ND - 68.17 3/4/99 98.66 30.63 ND - 68.03 6/4/99- 98.66 30.13 ND - 68.53 10/12/00 98.62 32.32 ND - - 66.30 4/4/01 98.62 31.93 ND - - 66.69 4/9/01 98.62 31.64 ND - - 66.98 4/19/01 98.62 31.18 ND - - 67.44 4/23/01 98.62 31.03 ND - - 67.59 5/3/01 98.62 31.93 ND - - 66.69 5118101 98.62 13.10 ND - - 85.52 6/27/01 98.62 31.11 ND - - 67.51 8/16/01 98.62 31.82 ND - - 66.80 12/4/01 98.62 33.58 ND - - 65.04 12/12/01 98.62 33.72 ND - - 64.90 1/3/02 98.62 33.96 ND - - 64.66 1/18/02 98.62 33.75 ND - - 64.87 2/12/02 98.62 34.08 ND - - 64.54 3/8/02 98.62 33.76 ND - - 64.86 5/l/02 98.62 32.78 ND - - 65.84 MW-IA 12/4/01 98.70 34.43 ND - - 64.27 1/3/02 98.70 34.77 ND - - 63.93 5/l/02 98.70 33.57 ND - - 65.13 MW-2 1/13/99 98.39 30.60 ND - 67.79 3/4/99 98.39 31.50 ND - 66.89 6/4/99 98.39 29.93 ND - 68.46 10/12/00 98.39 32.11 ND - 66.28 4/4/01 98.39 32.55 ND - 65.84 4/19/01 98.39 30.80 ND - 67.59 8/16/01 98.39 31.50 ND - 66.89 12/4/01 98.39 33.31 ND - 65.08 12/12/01 98.39 33.44 ND - 64.95 1/3/02 98.39 33.68 ND - 64.71 1/18/02 98.39 33.45 ND - 64.94 2/12/02 98.39 33.78 ND 64.61 3/8/02 98.39 33.43 ND 64.96 5/l/02 1 98.39 1 32.40 1 ND 65.99 Ref.: tpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:25 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 3 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation _ Elevation MW-2A 4/4/01 99.66 33.64 ND 66.02 4/19/01 99.66 32.95 ND 66.71 8/16/01 99.66 33.52 ND 66.14 12/4/01 99.66 35.32 ND 64.34 1/3/02 99.66 35.67 ND 63.99 5/l/02 99.66 34.50 ND 65.16 MW-3A 4/4/01 98.53 32.48 ND 66.05 4/19/01 98.53 31.77 ND 66.76 8/16/01 98.53 32.35 ND 66.18 12/4/01 98.53 34.12 ND 64.41 1/3/02 98.53 34.48 ND 64.05 5/l/02 98.53 33.35 ND 65.18 MW-4 1/13/99 98.60 30.52 ND 68.08 3/4/99 98.60 30.68 ND 67.92 6/4/99 .98.60 30.11 ND 68.49 10/12/00 99.37 32.31 ND 67.06 4/4/01 99.37 31.92 ND 67.45 4/9/01 99.37 31.60 ND 67.77 4/19/01 99.37 31.18 ND 68.19 4/23/01 99.37 31.02 ND 68.35 5/18/01 99.37 31.12 ND 68.25 6/27/01 99.37 31.12 ND 68.25 8/16/01 99.37 31.82 ND 67.55 12/4/01 98.60 33.61 ND 64.99 12/12/01 98.60 33.73 ND 64.87 1/3/02 98.60 33.97 ND 64.63 1/18/02 98.60 - - Well Inaccessible 2/12/02 98.60 34.10 ND 64.50 3/8/02 98.60 33.77 ND 64.83 5/l/02 98.60 Well Inaccessible 4 Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:25 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 4 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-5 1/13/99 98.27 30.12 ND - - 68.15 3/4/99 98.27 30.07 ND - - 68.20 6/4/99 98.27 29.71 ND - - 68.56 10/12/00 98.22 31.57 ND - 66.65 4/4/01 98.22 31.94 ND - - 66.28 4/9/01 98.22 - - Well Inaccessible 4/19/01 98.22 - - - Well Inaccessible 4/23/01 98.22 30.66 ND - - 67.56 5/18/01 98.22 30.74 ND - - 67.48 6/27/01 98.22 30.74 ND - - 67.48 8/16/01 98.22 31.43 ND - - 66.79 12/4/01 98.22 33.20 ND - - 65.02 12/12/01 98.22 33.34 ND - - 64.88 1/3/02 98.22 33.56 ND - - 64.66 1/18/02 98.22 33.34 ND - - 64.88 2/12/02 98.22 33.72 ND - 64.50 3/8/02 98.22 33.41 ND - - 64.81 5/1/02 1 98.22 32.42 ND - 65.80 MW-6 1/13/99 98.52 30.40 ND - - 68.12 3/4/99 98.52 - - Well Inaccessible 6/4/99 98.52 30.01 ND - - 68.51 10/12/00 98.51 32.20 ND - - 66.31 4/4/01 99.08 32.83 ND - - 66.25 4/19/01 99.08 31.11 ND - - 67.97 8/16/01 99.08 31.76 ND - - 67.32 12/4/01 98.51 33.53 ND - - 64.98 12/12/01 98.51 33.65 ND - - 64.86 1/3/02 98.51 33.87 ND - - 64.64 1/18/02 98.51 33.63 ND - - 64.88 2/12/02 98.51 34.01 ND - - 64.50 3/8 1 98.51 33.68 ND - - 64.83 5/l/02 98.51 32.70 ND - - 65.81 Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:26 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 5 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-9 1/13/99 99.56 31.36 ND - - 68.20 3/4/99 99.56 31.30 ND - - 68.26 6/4/99 99.56 31.04 ND - - 68.52 10/12/00 99.52 32.23 ND - - 67.29 4/4/01 99.52 33.38 32.78 0.60 4/9/01 99.52 33.03 32.50 0.53 4/19/01 99.52 32.28 32.08 0.20 4/23/01 99.52 31.98 ND - - 67.54 5/3/01 99.52 31.85 ND - - 67.67 5/18/01 99.52 32.04 ND - - 67.48 Sheen 6/27/01 99.52 31.57 ND - - 67.95 8/16/01 99.52 32.69 32.59 0.10 12/4/01 99.52 35.53 34.25 1.28 12/12/01 99.52 34.65 ND - - 64.87 1/3/02 99.52 34.96 34.85 0.11 1/18/02 99.52 34.67 ND - - 64.85 2/12/02 99.52 35.00 ND - - 64.52 3/8/02 99.52 34.70 ND - - 64.82 Sheen 5/1/02 99.52 33.70 ND - - 65.82 MW-10 1/13/99 98.92 31.20 ND - - 67.72 3/4/99 98.92 31.22 ND - - 67.70 6/4/99 98.92 30.39 ND - - 68.53 10/12/00 98.88 32.60 ND - - 66.28 4/4/01 98.88 32.19 ND - - 66.69 4/9/01 98.88 31.90 ND - - 66.98 4/19/01 98.88 31.42 ND - - 67.46 4/23/01 98.88 31.28 ND - - 67.60 5/18/01 98.88 31.37 ND - - 67.51 6/27/01 98.88 31.36 ND - - 67.52 8/16/01 98.88 31.08 ND - - 67.80 12/4/01 98.88 - - Well Dry 12/12/01 98.88 33.98 ND 64.90 1/3/02 98.88 - - Well Dry 1/18/02 98.88 34.01 ND 64.87 2/12/02 98.88 - - Well Dry 3/8/02 98.88 - - Well Inaccessible 5/1/02 98.88 1 33.04 ND 65.84 Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:26 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 6 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-11 4/4/01 99.78 32.96 ND - - 66.82 4/19/01 99.78 32.24 ND - - 67.54 8/16/01 99.78 32.88 ND - - 66.90 12/4/01 99.78 34.72 ND - - 65.06 1/3/02 99.78 35.07 ND - - 64.71 5/1/02 1 99.78 33.83 ND - - 65.95 MW12 4/4/01 99.05 32.43 ND - - 66.62 4/9/01 99.05 32.13 ND - - 66.92 4/19/01 99.05 31.67 ND - - 67.38 4/23/01 99.05 31.56 ND - - 67.49 5/18/01 99.05 31.68 ND - - 67.37 6/27/01 99.05 31.64 ND - - 67.41 8/16/01 99.05 32.36 ND - - 66.69 12/4/01 99.05 34.13 ND - - 64.92 12/12/01 99.05 34.28 ND - - 64.77 1/3/02 99.05 34.52 ND - - 64.53 1/18/02 99.05 34.29 ND - - 64.76 2/12/02 99.05 34.62 ND - - 64.43 3/8/02 99.05 34.27 ND - - 64.78 5/l/02 99.05 33.30 ND - - 65.75 MW-13 4/4/01 98.32 31.67 ND - - 66.65 4/19/01 98.32 30.88 ND - - 67.44 8/16/01 98.32 31.60 ND - - 66.72 12/4/01 98.32 33.42 ND - - 64.90 1/3/02 98.32 33.80 ND - - 64.52 .5/l/02 98.32 32.50 ND - - 65.82 MW-14(25) 4/4/01 99.96 33.74 ND - - 66.22 4/9/01 99.96 33.45 ND - - 66.51 4/19/01 99.96 32.98 ND - - 66.98 4/23/01 99.96 32.71 ND - - 67.25 5/18/01 99.96 32.80 ND - - 67.16 6/27/01 99.96 32.90 ND - - 67.06 8/16/01 99.96 33.59 ND - - 66.37 12/4/01 99.96 35.33 ND 64.63 1/3/02 99.96 35.68 ND - 64.28 511/02 99.96 34.57 ND - 65.39 MW-14(70) 5/l/02 99.72 34.31 ND - 65.41 MW-14(90) 5/l/02 99.95 37.68 ND - 62.27 Ref.: rpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 1:47:27 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 1 Page 7 of 7 Monitoring Well Gauging Data Summary Texaco Service Station#100083 1140Iyanough Road Hyannis,MA January 13, 1999 through May 1,2002 Well ID Date Top of Depth to Depth to NAPL Correction Corrected Comments Casing Water NAPL Thickness Factor Water Elevation Elevation MW-15(20) 12/4/01 98.47 34.20 ND - - 64.27 1/3/02 98.47 34.55 ND - - 63.92 5/1/02 1 98.47 33.49 ND - - 64.98 MW-16(20) 12/4/01 98.35 34.12 ND - - 64.23 1/3/02 98.35 34.45 ND - - 63.90 1/18/02 98.35 34.16 ND - - 64.19 5/l/02 98.35 33.36 ND - 64.99 MW-16(55) 12/4/01 98.27 34.02 ND - - 64.25 1/3/02 98.27 34.36 ND - - 63.91 1/18/02 98.27 34.08 ND - - 64.19 5/l/02 98.27 33.28 ND - - 64.99 MW-17(20) 12/4/01 100.54 35.52 ND - - 65.02 1/3/02 100.54 35.88 ND - - 64.66 5/1/02 100.54 34.80 ND - - 65.74 MW-18(25) 5/l/02 100.28 35.15 ND - - 65.13 MW-18(70) 5/l/02 100.09 34.90. ND - - 65.19 SVE-1 4/9/01 99.11 31.88 ND - - 67.23 4/19/01 99.11 31.43 ND - - 67.68 6/27/01 99.11 31.34 ND - - 67.77 8/16/01 99.11 32.16 ND - - 66.95 12/4/01 99.11 33.82 ND - - 65.29 12/12/01 99.11 33.96 ND - - 65.15 1/18/02 1 99.11 33.98 ND - 65.13 Notes: NAPL - Non-Aqueous Phase Liquid ND - Not Detected - Not Applicable All measurements are in feet. Elevations are relative to a local datum with an assumed elevation of 100.00 feet. Ref.: tpt_gauging\000509\100083 GEOLOGIC SERVICES CORPORATION 6/18/2002 2:04:55 PM Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Pagel of 4 Table 2 Groundwater Sample Analytical Results-Volatile Petroleum Hydrocarbons Texaco Service Station#100083 1140Iyanough Road Hyannis,MA June 4, 1999 through May 1,2002 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS roundwater Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C8 C9 C12 CO-C10 Category (ug/I) (ug/1) benzene Xylenes (ug/1) (ug/1) Ali hatics Ali hatics Aromatics u l u /1 u 1 GW-1 5.0 1,000 700 10,000 70 20 400 4,000 200 GW-2 2,000 1 6,000 30,000 6,000 50,000 6,000 1,000 1,000 5,000 GW-3 7,000 1 50,000 4,000 1 50,000 1 50,000 6,000 4,000 20,000 1 4,000 LABORATORY ANALYTICAL RESULTS Well ID Date Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C8 C9 C12 C9 C10 Comments Groundwater (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Aliphatics Aliphatics Aromatics Category) u u /I u u /I u /1 AS-1 4/4/01 <5 25.6 <5 33.8 6.5 <5 91.3 <50 94 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-1 6/4/99 I fi3f1 435 2747 06D 7 }' 4f <1000 <1000 (GW-1,GW-3) 10/12/00 7 0.4- 485 2243 8i{� 4/4/O1 376 257 1141 8 14.8 <100 407 8/16/O1 F l 6 364 162 810 ,. Jt�,, 3 9 <250 <250 s: 7�o 12/4/01 140 63.8 2741 g-stsm <10 <100 181 !1 5/1/02 48 22 67.5 637 <5 <50 <50 90.2 MW-lA 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (Gw-1,Gw-3) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-2 6/4/99 <5 <5 <5 <10 <5 <5 <100 <100 <100 (GW-1,GW-3) 10/12/00 <5 <5 <5 <10 <5 <5 <50 <50 <50 4/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 1 <5 <5 <10 <5 <5 <50 <50 <50 5/l/02 <5 <5 <5 <10 20.4 <5 <50 <50 <50 MW-2A E4/4/O92 147 250 83 <50 142 (GW-1,GW-3) 17 1 <5 <5 <10 36$4 <5 <50 <50 <50 i 1 <5 <5 <10 i4 < <50 <50 <50 xi22„ <5 <5 I1 27 11.3 <50 <50 82.5 MW-3A 4/4/01 <5 <5 <5 <10 <5 6.1 <50 <50 <50 (Gw-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 50.6 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-4 6/4/99 <1000 <1000 <1000 <1000 ) i14 <1000 <20000 <20000 <20000 (GW-1,GW-3) 10/12/00 <5 <5 <5 <10 t <5 <50 -50 <50 4/4/01 <5 <5 <5 <10 41.7 <5 <50 <50 <50 80/16/01 <5 <5 <5 <10 12 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 15.2 <5 <50 <50 <50 /2002 GEOLOGIC SERVICES CORPORATION rpt_ma_vph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 2 Page 2 of 4 Groundwater Sample Analytical Results-Volatile Petroleum Hydrocarbons Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA June 4, 1999 through May 1,2002 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS Groundwater Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C8 C9 C12 C9 C10 Category (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Ali hcs Ali hatics Aromatics u /1 u /1 MR), u /l u /1 GW-1 5.0 1,000 700 10,000 70 20 400 4,000 200 GW-2 2,000 6,000 30,000 6,000 50,000 6,000 1,000 1,000 5,000 GW-3 7,000 50,000 4,000 50,000 50,000 6,000 4,000 1 20,000 4,000 LABORATORY ANALYTICAL RESULTS Well ID Date Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C$ FAliphatics C9 C10 Comments Groundwater (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) AliphaticsAromatics Category) u u 1 u /1u MW-5 6/4/99 FV s>.a <5 <5 52 ��';-�S�I, <5 <100 <100 <100 (Gw-1,Gw-3) 10/12/00 4320� 5I3r 550 2434 300 20 ` <50 2580 1Z i ,MM � .. 4/4/015z08..e 384 2014 -6U00 `6d,..,, <100 821 <,6m 8/16/01 343 1938I251© <200 <2000 <2000 <2000 12/4/01 6 g00©Q 139H1 7690 q0. ,3 . .w <500 04�120� 5/1/02 sd152 �<s1U40t1mm2()0© 115` Q0 4`0 <2500 j <2500 140 7 MW-6 6/4/99 <25 <25 <25 <50 S50 <25 <500 <500 <500 (Gw-1,GW-3) 10/12/00 <5 <5 <5 <10 <5 <5 <50 <50 <50 4/4/01 11� 6.2 5.5 <10 10 0,5` <5 <50 <50 97 8/16/01 <5 <5 <5 <10 15.6 <5 <50 <50 <50 12/4/O15 6y�`" <5 <5 <10 <5 <50 <50 <50 5/1/02 � <5 8.3 18 3 70 N <50 <5036 , MW-9 6/4/99 33$�` 22$ 2U l$Q70Q�400 � r <5000 <5000 10$04 (Gw-1,Gw-3) 10/12/0050k�5$ ¢ � 80 3830 � 0' [2<3�Qpg�`' 74Q( 5/1/02L62�Q �6$Qf1; �25 177i;0 $0 96$ a94 3230Gp 8 6P MW-10 6/4/99 <5 63.8 8.2 50.1 <5 <5 <100 <100 <100 (GW-1,GW-3) 10/12/00 <5 <5 <5 <10 27.2 36#9` 1 98.9 29 4/4/01 <5 <5 <5 <10 <5 9.5 <50 <50 100 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-11 4/4/01 <5 <5 <5 <10 7 <5 <50 <50 <50 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <16 <5 <50 <50 <50 MW12 4/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/l/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-13 4!4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 /2002 GEOLOGIC SERVICES CORPORATION rpt_ma_vph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA r Page 3 of 4 Table 2 Groundwater Sample Analytical Results-Volatile Petroleum Hydrocarbons Texaco Service Station#100083 1140Iyanough Road Hyannis,MA June 4, 1999 through May 1,2002 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS Groundwater Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C8 C9 C12 C9 C10 Category (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Ali hatics Ali hatics Aromatics (ug/1) (ug/1) u /1 ug/1) /1 u l GW-1 5.0 1,000 700 .10,000 70 20 400 4,000 200 GW-2 2,000 6,000 30,000 6,000 509000 6,000 1,000 1,000 5,000 GW-3 7,000 50,000 4,000 50,000 1 50,000 6,000 4,000 20,000 4,000 LABORATORY ANALYTICAL RESULTS Well ED Date Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C8 C9-C12 C9 C10 Comments Groundwater (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Aliphatics Aliphatics Aromatics Category) (ug/1) (ug/1) (ug/1) (ug/1) (ug/1) MW-14(25) 4/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-14(70) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) MW-14(90) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) MW-15(20) 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (Gw-1,GW-3) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 di MW-16(20) 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 I 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-16(55) 12/4/01 llk <50 <50 <100 1�00 <50 �0 <5005 (GW-1,GW-3) 1/3/02490 19.8 8 24 7 6„ 3 35 330 560 ;- „�.. <50 <50 122 5/1/02 4 ..: <5 <5 <10 <5� 42 MW-17(20) 12/4/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (Gw-1,Gw-3) 5/1/02 <5 <5 <5 <10 <5 <5 <50 <50 <50 MW-18(25) 5/1/02 <5 <5 <5 <10 26.8 <5 <50 <50 <50 (GW-1,GW-3) MW-I8(70) 5/1/02 <5 <5 T:E] <10 <5 <5 <50 <50 <50 (GW-1,GW-3) TMP-1 8/16/01 _ <12 <12 <24 868 <12 <120 <120 <120 (GW-1,GW-3) TMP-2 8!16/01 3113 <25 <25 <50 2av' <25 <250 <250 <250 (GW-1,GW-3) TMP-3 8i 16/01 <5 <5 <5 <10 8 <5 <50 <50 <50 (GW-1,GW-3) TMP-4 8/16/01 <5 <5 <5 <10 21.1 <5 <50 <50 <50 (GW-1,GW-3) TMP-5 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) TMP-6 8/16/01 <5 <5 <5 <10 14.8 <5 <50 <50 <50 (GW-1,GW-3) TMP-7 8/16/01 <5 <5 <5 <10 <5 <5 <50 <50 <50 (GW-1,GW-3) /2002 GEOLOGIC SERVICES CORPORATION rpt ma_vph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Page 4 of 4 Table 2 Groundwater Sample Analytical Results-Volatile Petroleum Hydrocarbons Texaco Service Station#100083 1140Iyanough Road Hyannis,MA June 4, 1999 through May 1,2002 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS Groundwater Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C8 C9-C12 C9 C10 Category (ug/1) (ug/1) benzene Xylenes (ug/1) (ug/1) Ali hatics All hatics Aromatics (ug/1) (ug/1) u /1 ug/1) /1 u l GW-1 5.0 1,000 700 10,000 70 20 400 4,000 200 GW-2 2,000 6,000 30,000 6,000 50,000 6,000 1,000 1,000 5,000 GW-3 7,000 50,000 45000 50,000 50,000 6,000 4,000 20,000 4,000 LABORATORY ANALYTICAL RESULTS Well ID Date Benzene Toluene Ethyl- Total MTBE Naphthalene C5-C8 C9 C12 C9 C10 Comments (Groundwater (ug/1) (ug/I) benzene Xylenes (ug/1) (119/1) Aliphatics Aliphatics Aromatics Category) u (ug/1) u l u /I u l tes: MCP Massachusetts Contingency Plan <10 - not detected at or above the method detection limit(method detection limit included) MT 3E methyl tertiary butyl ether ug/I micrograms per liter(parts per billion) (GW-2) - well-specific groundwater category not analyzed/not applicable shading indicates reported concentration exceeds the applicable MCP Method 1 Risk Characterization Groundwater Standard(s). r 112002 GEOLOGIC SERVICES CORPORATION f.: tpt_m4 _vph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 3 Page 1 of 2 Groundwater Sample Analytical Results-Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA June 4, 1999 through April 4, 2001 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS q N � tz W W '>' N o N o N 3 o N F n ° e �z7 .. .� °' m n w n C� y v � S Cv,,,,' C G ° C C � C C d C C N 2. o ee es n -Eri •o >• A m 3 A m A ro =* m ° Groundwater Category o A o y GW-1 20 300 2,000 1.0 0.2 1.0 300 1.0 2.0 0.5 300 300 0.5 10 1 20 300 200 4,000 5,000 200 GW-2 - - - - 10,000 6,000 - - 1,000 - 50,000 GW-3 5,000 3 000 3,000 3,000 3,000 3,000 3,000 3,000 3,000 3,000 200 3,000 3,000 3,000 6,000 50 3,000 20,000 20,000 30,000 LABORATORY ANALYTICAL RESULTS t77 t0 A 1", tz N C G T L d C C C a C N FF Well ID Date A ; 2n y Comments MW-1 6/4/99 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 (GW-1,GW-3) E4/4/01 00 <5 <5 <5 <5 <5 <5 <5 a <5 <5 <5 <5 <5 <5 MW-2 6/4/99 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <60 <167 <170 (GW-1,GW-3) MW-4 6/4/99 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 96.4 <80 <170 (GW-1,GW-3) 110/12/001 <5 1 <5 1 <5 1 <5 1 <5 <5 I <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <100 <100 <100 MW-5 6/4/99 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <60 <80 <170 (GW-1,GW-3) 10/12/00 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 I4 4 <5 <5 1010 <100 105 4/4/01 <5 <5 <5 <5 <5 <5 <5 s, <� M W-9 6/4/99 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 S 17 156 <5.3 <5.3 1200 <84 4 (GW-1,GW-3) 10/12/001 <5 1 <5 1 <5 1 <5 1 <5 <5 1 <5 <5 <5 <5 <5 <5 <5 833S <5 <5 3890 1 <100 277 , MW-10 6/4/99 1 <5.1 1 <5.1 1 <5.1 <5.1 1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <61 <82 <170 (GW-1,GW-3) 110/12/001 <5 1 <5 1 <5 <5 1 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <100 <100 <100 6/18/2002 GEOLOGIC SERVICES CORPORATION Ref.: rpt_ma_eph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Table 3 Page 2 of 2 Groundwater Sample Analytical Results-Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA June 4, 1999 through April 4,2001 MCP METHOD 1 RISK CHARACTERIZATION GROUNDWATER STANDARDS C N � tZ mtZ A (>f = ro N S Groundwater Category GW-1 20 300 2,000 1.0 0.2 1.0 300 1.0 2.0 0.5 300 300 0.5 10 20 300 200 4,000 5,000 200 GW-2 — — - — — — 10,000 6,000 — 1,000 50,000 GW-3 5,000�3,000 3,000 3,000 3,000 3,000 3,000 3,000 3,000 3,000 200 3,000 3,000 3,000 6,000 50 3,000 20,000 20,000 30,000 LABORATORY ANALYTICAL RESULTS tZ m Cr a n n A PYi ry N ryWry b S � ,a',y _ .fl O ? O y 7 W O y C S G = O OC ... � `! .r = rr ; ....� ....to rr R d �.. � .... _ �.. � ...i A G rr S v Well ID Date A A A > > y Comments m ee = A Notes: MCP - Massachusetts Contingency Plan ug/l - micrograms per liter(parts per billion) (GW-3) - well-specific groundwater category <10 - not detected at or above the method detection limit(method detection limit included) not applicable or not analyzed E: - shading indicates reported concentration exceeds the applicable MCP Method 1 Risk Characterization Groundwater Standard 6/18/2002 GEOLOGIC SERVICES CORPORATION Ref.: rpt_ma_eph_aq\000509\100083 Hydrogeologists and Environmental Scientists 15 Bonazzoli Ave.,Hudson,MA Page 1 of 1 Table 4 Historical Soil Analytical Results Volatile Petroleum Hydrocarbons Shell Service Station#100083 1140Iyannough Road ` Hyannis,Massachusetts Groundwater Benzene Toluene Ethyl- Total MTBE Naphthalene C'Cs C9-C12 C9-CIO Category (ug/g) (ug/g) benzene Xylenes (ug/g) (ug/g) Aliphatics Aliphatics Aromatics (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) S-1/GW-1 10 90 80 500 0.3 4 100 1,000 100 S-1/GW-2 40 500 500 500 100 100 100 1,000 100 S-1/GW-3 40 500 500 500 100 100 100 1,000 100 S-3/GW-1 10 90 80 800 0.3 4 500 5,000 100 S-3/GW-2 100 500 2,500 2,500 200 1,000 500 5,000 500 S-3/GW-3 200 2,500 500 500 200 1,000 500 5,000 500 LABORATORY ANALYTICAL RESULTS Sample Date Depth Benzene Toluene Ethyl- Total MTBE Naphthalene CS-Cs C9-C12 Cv-C" ID (ft) (ug/g) (ug/g) benzene Xylenes (ug/g) (ug/g) Aliphatics Aliphatics Aromatics u / u / u / u / u / MW_8 5/6/98 29-31 <65 <65 <65 <65 <65 <65 <325 <325 w <M S 5/6/98 29 31 65 947 ................... MW-10 5/6/98 30-32 <55 <55 <55 <55 <55 <55 <285 <285QR : MW-11 3/22/01 25-30 <0.190 <0.190 <0.190 <0.190 <0.190 <0.190 <3.9 <3.9 <3.9 MW-12 3/22/01 25-30 <0.210 <0.210 <0.210 <0.210 <0.210 <0.210 <4.2 <4.2 <4.2 MW-13 3/23/01 25-30 <0.220 <0.220 <0.220 <0.220. <0.220 <0.220 <4.3 <4.3 <4.3 MW-14 3/23/01 25-27 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <3.4 <3.4 <3.4 S13-8 5/6/98 30-32 <60 <60 <60 <60 <60 <60 <315 <315 4 S13-9 5/6/98 30-32 <65 <65 <65 <65 <65 <65 <335 <335 # � 9i SB-11 5/6/98 30-32 <65 <65 <65 <65 fdEx <65 $?? <330 $ : ASO1 3/21/01 24 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <3.4 <3.4 <3.4 MPO1 3/20/01 30-31 <0.190 <0.190 1 <0.190 <0.190 <0.190 <0.190 <3.8 <3.8 <3.8 MP-2 3/22/01 25-30 <0.180 <0.180 <0.180 <0.180 <0.180 <0.180 <3.5 <3.5 <3.5 MP03 3/21/01 28 <0.170 <0.170 <0.170 <0.170 <0.170 <0.170 <3.3 <3.3 <3.3 SVE01 3/20/O1 30-31 <0.240 <0.240 <0.240 <0.240 <0.240 <0.240 <4.7 <4.7 <4.7 Notes: MTBE-methyl tert-butyl ether ug/g-micrograms per gram(parts per million) <0.2-not detected(method detection limit included) indicates analyte exceeds applicable MCP Reportable Concentration Ref#: 000509.ttle-soil-vph TABLE 5 Summary of SVE Step Test Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts May 4, 2001 Time SVE-1 SVE S stem (min) Vac (ft/min)* I SCFM ACFM ("HZO) (measured)(calculated (calculated) Static --- --- --- --- 5 2 3375 74 74 10 4 4700 102 103 15 6 5140 112 112 t3020 8 5900 129 128 25 10 8010 175 172 12 8750 191 187 Notes: SVE-1 -soil vapor extraction well "HZO-inches of water column SVE System-soil vapor extraction system SCFM-standard cubic feet per minute ACFM-actual cubic feet per minute *Soil vapor flow rates taken from 2-inch diameter PVC pipe,with an anamometer. Summary of SVE/AS Pilot Testing Data Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts May 4,2001 Date: May 4,2001 Extraction Well ID: SVE-1 GSC Job#: 000509 Well Diameter(in): 4" Site ID: EQ/Hyannis Initial DTP(ft): NA Site Address: 1140 Iyanough Road Initial DTW(ft): 31.12 City,State: Hyannis,MA DTB(ft): 35.89 Time @ Soil Vapor Extraction Well After SVE System SVE Off-Gas Treatment1l ASS stem (min) Pressure VOC Flow Rate Flow Rate Temp He Pressure VOC Flow Rate Temp Mid Effluent Pressure Flow ("H2O) (ppmJ (ft/min) (scfm) (`F) (%) ("H2O) (ppmj (ft/min) ('F) (ppmv) (ppmv) (psi) (scfm) 0 --- 4.1 --- --- --- --- --- --- --- --- --- --- --- --- 5 -5.00 765 4900 106.9 66.0 --- 20.30 437 8100 132.0 19.7 0.10 15 -5.00 766 4950 107.9 65.6 --- 19.60 440 8110 133.0 20.1 0.20 --- --- 3 -5.00 659 4900 106.8 65.6 --- 20.58 375 8100 134.0 8.4 0.00 --- --- 45 -5.00 716 4920 107.3 65.2 --- 20.50 409 8100 134.0 19.3 0.00 --- --- 75 -10.50 437 8100 176.6 65.1 --- 19.50 450 75110 132.0 65.5 -- 80 -5.00 --- --- --- --- --- --- --- --- --- --- --- 8.0 3.0 85 -5.00 --- --- --- --- --- --- --- --- --- --- --- 8.0 3.0 90 -5.20 415 4831 105.3 64.5 --- 20.40 240 7900 130.6 44.8 1.3 8.0 3.0 105 -5.11 818 4740 103.4 65.2 --- 20.70 464 7910 130.6 64.2 2 8.0 3.0 120 -5.23 496 4810 104.9 65.2 --- 20.30 285 7910 130.6 58.7 1.3 8.0 3.0 ' 135 -5.21 508 4830 105.3 65.2 --- 20.20 294 7890 130.4 59.7 1.4 8.0 3.0 140 -5.20 --- --- --- --- --- --- --- 9.0 6.5 145 -5.10 --- --- --- --- --- --- --- --- 9.0 6.5 150 -5.12 375 4820 105.1 65.2 --- 21.10 218 7845 131.4 46.7 1.1 9.0 6.5 165 -5.11 464 4820 105.1 64.9 --- 22.30 268 7920 131.2 66.6 1.1 9.0 6.5 180 -5.20 469 4810 104.9 65.1 --- 21.00 271 7855 132.1 71.2 1.3 9.0 6.5 M -5.12 --- --- --- --- - 9.0 6.0 -5.20 --- --- --- --- 9.0 6.0 -5.22 380 4815 105.0 65.3 --- 20.20 220 7850 131.4 48.7 1.2 9.0 6.0 -5.15 372 4910 107.1 65.2 --- 20.40 219 7860 132.1 47.9 1.1 9.0 6.0 Notes: Time-time from beginning of pilot test in minutes(min) ACFM-actual cubic feet per minute SVE-1-soil vapor extraction well Mid-soil vapor sample measured between the two carbon vessels with a PID "1120-inches of water column calibrated to read total VOCs as benzene. Influent-soil vapor samples measured with a photoionization detector(PID)calibrated Effluent-soil vapor sample measured after the last GAC with a PID to read total volatile organic compounds(VOCs)as benzene. calibrated to read total VOCs as benzene. ppm -parts per million per unit volume AS System-air sparge system SVE System-soil vapor extraction system psi-pounds per square inch SUM-standard cubic feet per minute NM-not monitored TABLE 7 Summary of SVE/AS Pilot Testing Data-Monitoring Point Data Texaco Service Station#100083 1140Iyannough Road Hyannis,Massachusetts May 4,2001 Date: May 4,2001 Extraction Well ID: SVE-I GSC Job#: 000509 Site ID: EQ/Hyannis Site Address: 1140 Iyanough Road City,State: Hyannis,MA Time Monitoring Point ID:MP-1 Monitoring Point ID:MP-2 (min) 10.4 ft to AS-1 8.00 ft to SVE-1 15.21 ft to AS-1 17.50 ft to SVE-1 Across Shallow Deep Across Shallow = Deep Pressure VOC DTW DO Pressure He Pressure He Pressure VOC DTW DO Pressure He Pressure He (�,H20)_ _ (PPm.) (ft) (mP,�) ("Hz0) (%) C'H20) (%) ("H:0) (PPmw) (ft) (mg/1) ("Hz0) (%) ("H20) (%) 0 0.00 4.0 32.44 1.4 --- --- --- -- 0 57.0 32.69 0.9 --- --- --- --- 5 -0.77 0.0 32.41 1.0 -- --- --- --- -0.48 0.0 32.67 1.0 --- --- --- --- 15 -0.77 0.0 32.41 1.0 --- --- --- --- -0.48 0.0 32.67 1.0 --- --- --- -- 30 -0.74 0.0 32.42 1.2 --- --- --- -- -0.42 0.0 32.66 1.0 --- --- --- --- 45 -0.65 0.3 32.4 1.2 -- --- --- -- -0.33 0.0 32.67 1.0 -- --- --- --- 75 -1.05 1 0.0 132.39 1.4 -0.65 1 0.0 1 32.66 1 1.2 --- --- - - 80 -0.75 --- 32.36 --- -0.13 --- 0.00 --- -0.37 --- 32.62 --- 0.00 - 0.00 --- 85 -0.75 --- 32.36 --- -0.13 --- -0.01 --- -0.39 --- 32.62 --- 0.01 --- 0.00 -- 90 -0.76 0.0 32.35 2.8 -0.13 --- 0.01 --- -0.41 0.0 32.60 1.5 0.00 --- 0.00 --- 105 -0.65 0.0 32.34 1.8 -0.13 -- 0.02 --- -0.42 0.0 32.60 2.0 0.01 --- 0.00 --- 120 -0.74 0.0 32.35 1.6 -0.12 --- 0.00 --- -0.39 0.0 32.61 1.3 0.00 --- 0.00 --- 135 -0.74 0.0 32.32 1.6 -0.12 -- 0.00 --- -0.42 0.0 32.62 1.3 0.00 --- 0.00 --- 140 -0.78 --- 32.30 --- -0.16 --- -0.03 --- -0.38 --- 32.56 --- 0.00 --- 0.11 145 -0.74 --- 32.29 --- -0.14 --- 0.00 --- -0.38 --- 32.54 --- 0.00 --- 0.00 --- 150 -0.75 0.0 32.28 2.2 -0.14 --- 0.00 --- -0.38 0.0 32.54 1.6 0.00 --- 0.00 --- 165 -0.75 0.0 32.27 3.4 -0.14 --- 0.00 --- -0.37 0.0 32.52 1.6 0.00 --- 0.00 --- 180 -0.75 0.0 32.27 1.8 -0.17 --- 0.00 --- -0.42 0.0 32.51 1.6 0.00 --- 0.00 185 -0.71 --- 32.27 1.8 -0.14 0.01 0.00 0.03 -0.37 --- 32.51 1.5 0.00 0.00 0.15 0.00 190 -0.72 32.27 �17 0.17 0.02 0.00 0.02 0.36 32.51 1.4 0.00 0.00 0.08 0.00 195 -0.71 0.0 32.27 -0.16 0.02 0.00 0.02 -0.38 0.0 32.52 1.4 0.00 0.00 0.00 0.00 210 -0.73 0.0 32.28 -0.15 0.02 0.00 0.02 0.38 0.0 32.53 1.3 0.00 0.00 0.00 0.00 Notes: Time-time from beginning of pilot tests in minutes ppmv-parts per million per unit volume SVE-I-vapor extraction well DTW-depth to water measured in monitoring point using an electronic AS-I-air sparge well interface probe measured in feet(ft) Pressure-observed in monitoring well inches of water column("HQ) DO-dissolved oxygen VOC-soil vapor samples measured with a pbotoionization detector(PID)calibrated mg/l-milligrams per liter to read total volatile organic compounds(VOCs)as benzene. NM-not measured TABLE 7 Continued Summary of SVE/AS Pilot Testing Data-Monitoring Point Data Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts May 4,2001 Date: May 4,2001 Extraction Well ID: SVE-I GSC Job#: 000509 Site ED: EQ/Hyannis Site Address: 1140 Iyanough Road City,State: Hyannis,MA Time Monitoring Point ED:MP-3 Monitoring Point ID:MW-9 (min) 26.32 ft to AS-1 27.00 ft to SVE-1 43.00 ft to AS-1 45.00 ft to SVE-1 Across Shallow Dee Across Pressure i VOC DTW DO Pressure He Pressure He Pressure VOC DTW DO (pp-M) (ft) (mP,/1) ("H:O) (%) ("H20) (%) ("H2O)_ (ppn4) (ft) (mS/1) 0 0:00 1.7 32.79 1.0 --- --- --- 0.00 4.00 32.44 1.4 5 -0.33 0.0 32.80 1.0 --- --- --- --- -0.15 0.00 32.41 1.0 15 -0.33 0.0 32.80 1.0 --- --- --- -0.15 0.00 32.41 1.0 30 -0.27 0.0 32.80 1.0 --- --- --- --- -0.12 0.00 32.42 1.2 45 -0.22 0.1 32.79 1.0 --- --- --- --- -0.11 0.30 32.40 1.2 75 11 -0.35 0.0 32.79 10 - -- 0.18 0.00 32.39 1.4 80 -0.26 --- 32.76 --- -0.02 --- -0.10 --- --- --- 85 -0.24 --- 32.75 --- -0.02 --- -0.09 --- --- --- --- --- 90 -0.24 0.0 32.74 1.6 -0.03 --- -0.09 --- --- --- --- --- 105 -0.22 0.0 32.73 2.4 -0.03 --- -0.09 --- --- --- --- 120 -0.28 0.0 32.73 1.8 -0.05 --- -0.09 --- --- --- --- 135 -0.23 0.0 32.72 1.8 -0.03 -0.07 --- --- --- --- 140 -0.27 -- 32.71 - 0.05 --- -0.13 --- --- --- --- --- 145 -0.27 --- 32.69 --- -0.04 -0.09 --- --- --- --- --- I50 -0.20 0.0 32.68 1.6 -0.03 -0.09 --- --- --- --- --- 165 -0.23 0.0 32.65 1.7 0.04 -0.09 --- --- --- --- --- 180 -0.21 0.0 32.64 1.6 0.04 -0.08 --- --- --- 185 -0.24 32.64 1.6 -0.03 0.02 0.08 0.00 --- --- --- 190 -0.22 --- 32.64 1.5 -0.02 0.01 -0.07 0.00 --- --- --- 195 -0.26 0.0 32.64 1.5 -0.02 0.01 -0.08 0.00 --- --- --- 210 0.23 0.0 32.65 1.4 0.03' 0.02 0.08 0.00 Notes: Time'time from beginning of pilot tests in minutes ppmv-parts per million per unit volume SVE-t-vapor extraction well DTW-depth to water measured in monitoring point using an AS-1-air sparge well electronic interface probe measured in feet(ft) Pressure-observed in monitoring well inches of water column("H20) DO-dissolved oxygen VOC-soil vapor samples measured with a photoionization detector(PID)calibrated mg/I-milligrams per liter to read total volatile organic compounds(VOCs)as benzene. NM-not measured TABLE 8 Summary of SVE/AS Pilot Testing Data Texaco Service Station#100083 1140Iyannough Road Hyannis,Massachusetts May 18,2001 Time SVE-1 AS-1 MP-1 Pressure("H20) MP-2 Pressure("1120) MP-3 Pressure("H20) mtn Pressure "H20 Flow Rate ft/min Pressure(psi) Flow Rate scfm across shallow deepacross shallow dee across shallow deep --- --- I --- I --- --- I --- -- 15 1.3 1300 0 0 -0.2 1 0 0 -0.11 1 0 0 -0.05 1 0 1 0 30 -1.3 1325 0 0 -0.2 1 0 0 -0.11 0 0 -0.05 0 0 Summa Can Sample Taken For SVE Test --- --- --- 0E1.3 1310 10 6 019 0 0 0.1 0 0 0.05 0 0 30 -1.3 1310 10 6 0.19 0 0 0.1 0 0 -0.05 0 0 Summa Can Sam le Taken For SVE/AS Test Notes: Time-time from beginning of pilot tests in minutes SVE-1-vapor extraction well AS-1-air sparge well Pressure-observed in monitoring well inches of water column("HQ) SCFM-standard cubic feet per minute PSI-pounds per square inch Table 9 Summary of SVE/AS Pilot Test Air Sample Analytical Data at SVE-1 Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts May 18, 2001 Sample ID:SVE Compound Results Results (ppb,,) (µg/m') Benzene 31,900 102,000 Eth lbenzene 30,700 133,000 Toluene 318,000 1,200,000 X lens total 132,000 572,000 MTBE 11 79,300 11 285,000 Sample ID: SVE+AS Compound Results Results (ppb,) (µWin) Benzene 28,200 90,000 Eth lbenzene 29,700 129,000 Toluene 204,000 768,000 lens total 149,000 646,000 MTBE 11 72,900 11 262,000 11 Notes: ppb,,-part per billion per unit volume µg/m-micrograms per cubic meter ND-not detected MTBE-Methyl Tertiary Butyl Ether Ref#000509.SVE/AS Appendix C Groundwater Analytical Results EgliNew England ®ACCUTEST 2 ian9rol Teehrical Report fOr Equiva Services GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M22269 Report to: Geologic Services Corp. 15 Bonazzoli Ave Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 50 /e,a&d Lab Director Certifications:MA(MA136) CT(PH-0109) NH(250293) RI(A-71) ME(MA136) This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England ■495 Tech Center West■Building 1 0 Marlborough,MA 01752 0 tel:508A81-6200 0 fax:508A81-7753 ■http://www.accutest.com I _ , Accutest Laboratories Sample Summary Equiva Services Job No: M22269 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA ............... Sample Co&eted> ii Matrix Client ...::.:.:.::.:.::::.............................: Number Date Time By Received Code Type Sample ID ...................................................................................... ........................... ...................................................................................... MLM 12/OS/O1 A Ground Water MWOi 3vIV =1; >>; ;< <<><; M-2226%.' 12/04/01 14:50 M Q ...................................................................................... 12/05/01 A Ground Water - 44 MLM02':' ;r>:>><>>>;>;; ;>> >> ><»> >< >_> M22 b9r 12/04/01 13. Q �!1 y�:..:... .,�..:.....::. ..:; Mti-Z-3 ` 12/04/01 11:00 MLM 12/05/01 AQ Groun ate ,M,.:::.....A:MW.,..A::::,:::::::::::::::::::::::::::::.::::.:..::. 12/05/01 A Ground Water W >: ::<:> .......; M222fi9-4 . 12/04/01 10:37 MLMQ MIA1W ... ... .......: MLM 12/05/01 A Ground Water IUI fl3A-pvl 3-3 > '<< > M226 ;5 > 12/04/01 11:30 Q ::::::::::.............................................-.................::........ ........................... M2 2,fi 6` 12/04/O1 15:45 MLM 12/OS/Ol AQ Ground W e ;M' 44'MW:::::::::::.:.::::::::::.::::.::::: :.::::::::::::. ................................................................................. ...................................................................................... 1 A round Water MVV15:MWS>»<><<> >> >> > <> <<>i Iti22Gg; 12/04/Ol 15:50 MLM 12/OS/0 Q G .......:::::::. 1 Ground Water MLM 12/05/0 A G oun 12 04 O1 14.55 1v ?V `1titV6> >> isi>;>'> > >> > > >< < <> > �'I2b ::8:::. / / Q ........................... 2 5/O1 A Ground Water 11i1ti1 =:YI > > >< > ..................................... ............M2269 . 12/04/Ol 16:00 MLM 1 /0 Q ..................... ........ .... -2- ........ .-* .... :.. ....:.:.:..::.::........::.::.:::.:..:.::::::::::::.::::::::::::::::::::.::::::. :-:M 2f .0: 12/04/01 14:00 MLM 12/05/01 AQ Ground Water NI't W.I. X..........:»>_::<>::»:><::<:::»::::>:>::»:>..........>:::>:>:::::>::;: 01 A Ground Water MwI: Mw,13':::::. <>> > > >«>> > M2261I 12/04/O1 13:10 MLM 12/05/ Q ::::::::::.::::.::.:::::::::::::...........::::::::::::: ................. ...............:.:::.::.:::::::::::::. Water 4: W_::4.;:< :: ::> .........226 1 : 12/04/01 14:10 MLM 12/05/01 AQ Ground MW1: . ::::: .:;. :::: :.: : :::::::::::.::. ...:......................................................................... M22269.13;: 12/04/01 09:35 MLM 12/05/01 AQ Ground Water ........... W15 Iti1W 15 Accutest Laboratories Sample Summary (continued) Equiva Services Job No: M22269 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA .................................................... ........................................ Sample C%Qtecte «> Matrix Client ...:................................... . Number Date Time By Received Code Type Sample ID : 12 M2269 4 /04/O1 09:58 MLM 12 1. /OS/Ol A Ground Water ItIW1 MW>1G .... .....:.... Q 691512/04/01 ML 2 09 55 M 1 /OS/O1 A Gr ound ound Water .................. ......................_... II1�V:16D:MW :>« >>>::= 2; `: 12 4 M 226 ..l /04/01 13. 5 MLM 12 9- 6. /OS/01 A Ground G ou d Water M222.6 -47 12/ / 1 1 94 04 0 6.05 MLM 12 1/OS/0 A Field B . ................................... d lank Water » »< M2. .f9 8 12/04/Ol I :06 MLM 12/05/01 AQ Trip PBln Water ........................... > 2226.:�IA 12 1 4 9 /04/0 1 .50 MLM 12/OS/01 A Groundwater Filtered ........................... QN.::1..::. .......................... ........................... M2 12/04/01 11: L 22269..3A 00 M M 12/0 O1 A/ Groundwater Filtered M222. ':A 2 5 1 /04/O1 11: 0 ML 3 M 12/OS/O1 A w_.... Ground ater Filtered IV1Vlz'�';A:MW�-'. . »:>_>> >>> >> >>><< ........................... 2 222f97A 1 /04/Ol 1 0 ML M 5 5 M 12/OS/O1 AGroundwater .::.... ........................... Q Filtered >a1?IWt 5=M'VVAS:::»::»::>::::>:>;::>::=::>:<::::::= »::::>::»::>::::>:::>::;:«::; ........................... _2i FilteredM .. ::.91 :: .. 11 2/04/O1 13:10 LM 12/OS/O1 AQGroundwater W .............�vt2 414M..WM42l04/O1 14:10 MLM 12/OS/01 AQ Groundwater Filtered ................. ....::............ Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOl-MW-1 Lab Sample ID: M22269-1 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1254.1) 2 12/08/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 4 . 10 ug/I ............_--......... 100-41-4 Ethylbenzene b8 10 ug/I 1634-04-4 Methyl Tert Butyl Etherfi8> < ; lO ug/I 91-20- h 3 Naphthalene D > 10 ug/I ....:...................... ........................... ........................... 108-88-3 Toluene 4A10 ug/I .........:.................. ........................... ............................ m,p-Xylene 18 <> s 10 ugh ........................... ........................... J. ........................... 95-47-6 o Xylene 8i 10 ug/I ........................... CS-C8 Aliphatics (Unadj.) laDQ 100 ug/I C9- C12 Aliphatics(Unadj.) 9 100 ug/I C9-CIO Aromatics (Unadj.) 32{}::>;........:*... 100 ug/I C5- C8 Aliphatics 1 < >s >' i 100 ug/I C9- C12 Aliphatics Y$;I> 100 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 73 ' 70-130% 615-59-8 2,5-Dibromotoluene < {%< 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWO1-MW-1 Lab Sample ID: M22269-1 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a I118741.1) 1 12/10/01 ANJ n/a n/a N:GII937 Run#2 CAS No. Compound Result RL Units Q ........................... ........................... 74-82-8 Methane 747 0.10 ug/1 ........................... ........................... (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOl-MW-1 Lab Sample ID: M22269-1 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistr y Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity, Total ` <` > '; 5.0 mg/l 1 12/11/01 BF EPA 310.1 Carbon Dioxide9 : >< 5.0 mg/1 l 12/11/01 MA SM18 45000O2D ................................. .................................. Nitrogen, Nitrate a Ci0 i11 >; 0.11 mg/l 1 12/12/01 MA EPA 353.2 Nitrogen, Nitrate + Nitrite 0 0.10 mg/l 1 12/12/01 MA EPA 353.2 Nitrogen, Nitrite ()D10 i i>s 0.010 mg/l 1 12/05/01 MA EPA 354.1 Sulfate C#8 ;_ 5.0 mg/1 1 12/10/01 BF EPA 375.4 ................................. .................................. ................................. Sulfide ;2 0 ; _ 2.0 mg/1 1 12/07/01 BF EPA 376.1 (a) Calculated as: (Nitrogen, Nitrate + Nitrite)-(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02-MW-2 Lab Sample ID: M22269-2 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1257.1) 1 12/08/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene N qww:: 5.0 ug/I ........................... ........................... ........................... 100-41-4 Ethylbenzene Tib >' 5.0 ug/I ....:...................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether TTDi .. 5.0 ug/I 91-20-3 Naphthalene TITS >; 5.0 ug/l NT) 108-88-3 Toluene :;`<' 5.0 ug/I m,p-Xylene D ; 5.0 ug/1 95-47-6 o-Xylene NIA < << ug/I C5-C8 Aliphatics(Unadj.) IIII <50 ug/I ... ...........:........ .......................... ..............-........... C9-C12 Aliphatics(Unadj.) TID 50 ug/I C9-C10 Aromatics(Unadj.) ;< 50 ug/I .... ................... ........................... ........................... CS-C8 Aliphatics TID <> «`'<50 ug/I C9-C12 Aliphatics 1IT? `' ><> 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene # dla << » 7U-130 ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 744b> > <; 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound I Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M22269-3 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a . Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1240.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units, Q 71-43-2 Benzene 11 <> 5.0 ug/I 100-41-4 Ethylbenzene5.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 214 ; 5.0 ug/I 91-20-3 Naphthalene NIA;>< ;i<> 5.0 ug/I ........................- ........................... ................. 108-88-3 Toluene IUD::;::< >; 5.0 ug/I m,p-Xylene lib::;::;>>; <; > 5.0 ug/I ........................... ............................ ........................... 95-47-6 o-Xylene 1VD<__'i ` i5.0 ug/I C5-C8 Aliphatics(Unadj.) 28»<;<_< < 50 ug/I C9-C12 Aliphatics (Unadj.) IID'< 50 ug/I C9-C10 Aromatics(Unadj.) IaI 50 ug/I C5-C8 Aliphatics D< 50 ug/I C9-C12 Aliphatics Tom:::: > < 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits ..............I.......... 615-59-8 2,5-Dibromotoluene T4 ; 70-130% .......................- 615-59-8 2,5-Dibromotoluene fi3%«»> > i 70-130% ......................... .......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M22269-3 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II18743.1) 1 12/10/01 ANJ n/a n/a N:GI1937 Run#2 CAS No. Compound Result RL Units Q ...........I............... ........................... 74-82-8 Methane ;5 J3 . 0.10 ug/I ................. ........................... (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M22269-3 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity, Total mg/l 1 12/11/01 BF EPA 310.1 Carbon Dioxide 77 1 ; 5.0 mg/l 1 12/11/01 MA SM18 4500002D ................................. .................................. Nitrogen, Nitrate a i 9i< i> 0.11 mg/l 1 12/12/01 MA EPA 353.2 Nitrogen, Nitrate + Nitrite i::9;:::::::::;:::::::::::::::<::: 0.10 mg/l 1 12/12/01 MA EPA 353.2 ..:............................... ................................. .................................. Nitrogen, Nitrite 1 0.010 mg/1 1 12/05/01 MA EPA 354.1 Sulfate ( G > ; 5.0 mg/l 1 12/10/01 BF EPA 375.4 ................................. .................................. ................................. Sulfide 2 2.0 mg/l 1 12/07/01 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MWOIA-MW-IA Lab Sample ID: M22269-4 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1241.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......................... 71-43-2 Benzene ItD 5.0 ug/1 100414 Ethylbenzene D > :: ':: 5.0 ug/1 ....:...................... ........................... 1634-04-4 Methyl Tert Butyl Ether ITD< 5.0 ug/1 91-20-3 Naphthalene ug/1:108-88-3 Toluene 5.0 ug/1 m,p-Xylene ug/1 95-47-6 o-Xylene AID;:;:: :: ; 5.0 ug/1 C5- C8 Aliphatics (Unadj.) hID<>: 50 ug/1 :.. .................... ........................... C9-C12 Aliphatics(Unadj.) IID`' 50 ug/I C9-CIO Aromatics (Unadj.) 1ID > 50 ug/1 :.. ................... ......................-- ........................... C5-C8 Aliphatics 1'II ` :> 50 ug/1 C9-C12 Aliphatics ND ` > 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene :; 70-130% ......................... ...........I............. 615-59-8 2,5-Dibromotoluene 7:I9 ;`:>'> » 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Y � Client Sample ID: MW03A-MW-3A Lab Sample ID: M22269-5 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1293.1) 1 12/10/01 AF n/a n/a GWX36 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene ND> 5.0 ug/1 ........................... ........................... ........................... ........................... 100-41-4 Ethylbenzene NI) <>: 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether SO fi:'< .... 5.0 ug/1 ........................... ........................... 91-20 3 Naphthalene NTH;.......... 5.0 ug/1 ....:...................... ........................... ........................... 108-88-3 Toluene ND 5.0 ug/1 m,p-Xylene 11 5.0 ug/1 .:......................... ........................... ........................... 95-47-6 o-Xylene ND > 5.0 ug/1 ........................... ............. ........................... C5-C8 Aliphatics(Unadj.) I3::: >> 50 ug/1 ... .................... ........................... ........................... C9-C12 Aliphatics(Unadj.) :N13 ; 50 ug/1 ... .................. ........................... C9-C10 Aromatics(Unadj.) 1iD; : :: >; 50 ug/1 ... . ................. ........................... ........................... C5-C8 Aliphatics :ND: i . 50 ug/1 .:..:...................... ........................... ........................... C9-C12 Aliphatics ::; 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 87 < ;>: 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 84% > >< 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M22269-5 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II18744.1) 1 12/10/01 ANJ n/a n/a N:GII937 Run#2 CAS No. Compound Result RL Units Q 74-82-8 Methane hT0.10 ug/1 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calib_ation range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M22269-5 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method ............................... .................................. Alkalinity, Total » 5£ ;«><< < > 5.0 mg/1 1 12/11/01 BF EPA 310.1 Carbon Dioxide ? ; 5.0 mg/l 1 12/14/01 MA SM18 45000O2D Nitrogen, Nitrate a 2 i; «» <;0.11 mg/l 1 12/12/01 MA EPA 353.2 Nitro en, Nitrate + Nitrite 3; ; <; > 0.10 mg/l 1 12/12/01 MA EPA 353.2 g Nitrogen, Nitrite a01(l< OA10 mg/1 1 12/05/01 MA EPA 354.1 Sulfate C 5{}>< ; ` 5.0 mg/1 1 12/10/01 BF EPA 375.4 ............................... Sulfide >24i i 2.0 mg/1 1 12/07/01 BF EPA 376.1 ....................:............ .................................. (a) Calculated as: (Nitrogen, Nitrate + Nitrite)-(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW04-MW4 Lab Sample ID: M22269-6 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date. Prep Batch Analytical Batch Run#1 WX1294.1) 1 12/10/01 AF n/a n/a GWX36 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene ND 5.0 ug/I 100414 Ethylbenzene ug/I 1634-04-4 Methyl Tert Butyl Ether 15 2> >'5.0 ug/I 91-20-3 Naphthalene NTH_ 5.0 ug/I ........................... ........................... 108-88-3 Toluene 'ND »> = > 5.0 ug/I m,p-Xylene l) 5.0 ug/I ...:....................... ........................... 95-47-6 o-Xylene N ; 5.0 ug/I C5-.C8 Aliphatics (Unadj.) 50 ug/I :.. . ................ ........................... C9-C12 Aliphatics(Unadj.) IID ' _ ; 50 ug/I C9-C10 Aromatics (Unadj.) t 50 ug/I C5-C8 Aliphatics » >> 50 ug/I C9-C12 Aliphatics I ` ' ` 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene . 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene $3 > > 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M22269-7 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX 1255.D 10 12/08/01 AF n/a n/a GWX35 Run#2 WX1295.D 250 12/10/01 AF n/a n/a GWX36 MA-VPH List CAS No. Compound Result RL Units Q Ethylbenzene 71 43-2 Benzene 7; 6():„ s 50 ug/I 100-41-4 13gQ>>>«> 50 ug/I 1634-04-4 Methyl Tert Butyl Ether Cla 1300 ug/I 91-20-3 Naphthalene 0< = < 50 ug/I ........................... ........................... ........................... 108-88-3 Toluene IflU 50 ug/I m,p-Xylene0: < ug/I ........................... ........................... ........................... 95-47-6 o-Xylene 258p <; `'` 50 ug/I C5-C8 Aliphatics(Unadj.) 5GOf); > 500 ug/I C9-C12 Aliphatics(Unadj.) 1'370 < > 500 ug/I C9-C10 Aromatics(Unadj.) A '< 500 ug/I CS-C8 Aliphatics I'II >z><> 500 ug/I 1 C9-C 12 Aliphatics 40 500 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... ......................... 615-59-8 2,5-Dibromotoluene $ °j 70-130% .............. ......................... 615-59-8 2 5-Dibromotoluene S '3 <><>> » 70-130% ......................... ......................... (a)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound t Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M22269-7 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II18745.1) 1 12/10/01 ANJ n/a n/a N:GII937 Run#2 CAS No. Compound Result RL Units Q 74-82-8 Methane 18 1`<;` 0.10 ug/1 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M22269-7 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity, Total I<1.I 5.0 mg/1 1 12/11/01 BF EPA 310.1 .................................. ................................. .................................. Carbon Dioxide . .. 5.0 mg/1 1 12/11/01 MA SM18 4500002D ..........................-..... .................................. .................. Nitrogen, Nitrate a 0 1 i 0.11 mg/1 1 12/12/01 MA EPA 353.2 Nitrogen, Nitrate + Nitrite {?1'2< ' <; 0.10 mg/l 1 12/12/01 MA EPA 353.2 .................. ................................. .................................. Nitrogen, Nitrite Q OIO i 0.010 mg/I 1 12/05/01 MA EPA 354.1 .....................--......... ................................. .................................. Sulfate 5; ; ; 5.0 mg/I 1 12/10/01 BF EPA375.4 ..:.............................. .................................. ................................. Sulfide ;2 Q >< 2.0 mg/I 1 12/07/01 BF EPA 376.1 ................................. .................................. (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW06-MW-6 Lab Sample ID: M22269-8 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1244.D 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene ND 1S G «;; 5.0 ug/1 100-41-4 Ethylbenzene 5.0 ug/1 ........................... -...................--. ........................... 1634-04-4 Methyl Tert Butyl Ether 17:3> >< >; 5.0 ug/1 91-20-3 Naphthalene NIA;;;:::::::::>> 5.0 ug/1 .....::.................... 108-88-3 Toluene III3= ; = 5.0 ug/1 m,p-Xylene ND <`'>< 5.0 ug/1 95-47-6 o-Xylene ND;< >> ' 5.0 ug/1 CS-C8 Aliphatics(Unadj.) 2 ; « 50 ug/1 C9-C12 Aliphatics(Unadj.) NI3 ; ;;>; 50 ug/I C9-C10 Aromatics(Unadj.) `lD`<> > < 50 ug/1 CS-C8 Aliphatics NL) < < 50 ug/1 C9-C 12 Aliphatics KI)> >' " 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits .............. 615-59-8 2,5-Dibromotoluenealo; 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 7 % 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW11-MW-11 Lab Sample ID: M22269-9 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1245.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene 1ID ii;;> < 5.0 ug/1 100-41-4 Ethylbenzene tiTD5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND> r 5.0 ug/1 91-20-3 Naphthalene ..l 5.0 ug/1 108-88-3 Toluene 1tTID><< i 5.0 ug/1 m,p-Xylene ''ND >> >>< 5.0 ug/1 95-47-6 o-Xylene I+ID < 5.0 ug/1 CS-C8 Aliphatics(Unadj.) N13 ''; 50 ug/1 C9-C12 Aliphatics (Unadj.) ITD »> 50 ug/1 C9-C10 Aromatics (Unadj.) hTl °<i 50 ug/1 C5-C8 Aliphatics 1I 50 ug/1 C9-C12 Aliphatics ;;NTH:::;:::::: 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits .................. 615-59-8 2,5-Dibromotoluene >7fia 70-130% 615-59-8 2,5-Dibromotoluene ? % i '>s 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 � Client Sample ID: MW12-MW-12 Lab Sample ID: M22269-10 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1246.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ug/l 100-414 Ethylbenzene ND =< 5.0 ug/I ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether I+t ; 5.0 ug/1 91-20-3 Naphthalene Il ; > ' 5.0 ug/1 ..:..::.................... ........................... 108-88-3 Toluene Np ; »;< 5.0 ug/l m,p-Xylene liD 5.0 ug/1 95-47-6 o-Xylene ND 5.0 ug/I C5-C8 Aliphatics(Unadj.) NI < > 50 ug/1 C9-C12 Aliphatics(Unadj.) hti)= '; 50 ug/1 C9-C10 Aromatics (Unadj.) lt) <> >< 50 ug/1 ... ................... ........................... ........................... C5-C8 Aliphatics NI3 <s 50 ug/1 C9-C12 Aliphatics Nl '' 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits .......................- 615-59-8 2,5-Dibromotoluene To 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene ?5` <_ .... 70-130 ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M22269-11 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1247.13 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 7143-2 Benzene ND 5.0 ug/I 100-41-4 Ethylbenzene ID ; > 5.0 ug/1 ........................... ........................... ........................... 1634-044 Methyl Tert Butyl Ether :..N > ;; 5.0. ug/I 91-20-3 Naphthalene l ' < < ; ;; 5.0 ug/1 ........................... ........................... ........................... 108-88-3 Toluene Nl)... >;>; 5.0 ug/I m,p-Xylene Nll.> s5.0 ug/1 ........................... 95-47-6 o-Xylene ND: 5.0 ug/I C5-C8 Aliphatics (Unadj.) NTH:::;::;... . ug/I C9-C12 Aliphatics(Unadj.) 1ID`> < 50 ug/I C9-C10 Aromatics(Unadj.) 15I}<' ' S0 ug/1 .. .. .............. ........................... ........................... C5-C8 Aliphatics <III3I. 50 ug/I C9-C12 Aliphatics Il > ` 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene "7G o 70-130% ......................... 615-59-8 2,5-Dibromotoluene 76 ; ;; 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M22269-11A Date Sampled: 12/04/01 Matrix: AQ-Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... Iron 12C1 <> >< 100 ug/l 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3016A ........................... ........................... RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M22269-7A Date Sampled: 12/04/01 Matrix: AQ- Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... Iron S 2(IQ<< 100 ug/1 1 12/06/01 12/10/01 LMN SW846 6010B Sw846 3010A .........................- ........................... RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M22269-5A Date Sampled: 12/04/01 Matrix: AQ-Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... Iron <<lf)Q .. 100 ug/1 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3010A .........................- .......................... I RL = Reporting Limit i Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M22269-3A Date Sampled: 12/04/01 Matrix: AQ- Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... Iron 2$ i ;< 100 ugh 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3010A ........................... i RL = Reporting Limit i f Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOI-MW-1 Lab Sample ID: M22269-I A Date Sampled: 12/04/01 Matrix: AQ- Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Iron 214Up`<' ``' 1W ug/I 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TB Lab Sample ID: M22269-18 Date Sampled: 12/04/01 Matrix: AQ-Trip Blank Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1253.1) 1 12/08/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ;71-43-2 Benzene 5.0 ug/1D 100-41-4 Ethylbenzene '1D <>5.0 ug/1 1634-044 Methyl Tert Butyl Ether �l�:::> ':: 5.0 ug/l 91-20-3 Naphthalene :;NI3 ...... 5.0 ug/1 108-88-3 Toluene Ir11); i><>_ 5.0 ug/1 m,p-Xylene D ; <> : >< 5.0 ug/l ........................... ........................... ........................... 95-47-6 o-Xylene ND < ' < 5.0 ug/1 CS-C8 Aliphatics (Unadj.) . N1 50 ug/1 C9-C12 Aliphatics(Unadj.) NDi:«>%> <i 50 ug/l C9-C10 Aromatics(Unadj..) I1D . 50 ug/1 C5-C8 Aliphatics N*D..'iiii > < `: 50 ug/1 ........................... C9- C12 Aliphatics 50 ug/1 ......................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluenea >i i' i 70-130 ......................... ......................... 615-59-8 2,5-Dibromotoluene "? <> 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ' r Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FB Lab Sample ID: M22269-17 Date Sampled: 12/04/01 Matrix: AQ- Field Blank Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1252.1) 1 12/08/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 5.0 71-43-2 Benzene I`D` i >`;< ug/I ........................... ........................... ........................... 10041-4 Ethylbenzene ID 5.0 ug/I ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether N).' < >» 5.0 ug/I 91-20-3 Naphthalene hI3 ` ''> '5.0 ug/I ........................... ........................... 108-88-3 Toluene ND<;; i< '> 5.0 ug/I ........................... ........................... ........................... m,p-Xylene 1tiTD ;>; ; 5.0 ug/I ....:...................... ........................... ........................... 95-47-6 o-Xylene ND > « >' 5.0 ug/I C5-C8 Aliphatics(Unadj.) N >< ;>< > 50 ug/I ... .................... ........................... ........................... C9-C12 Aliphatics(Unadj.) l`II3; 50 ug/I .......................... ........................... C9-C10 Aromatics (Unadj.) (D < <>>50 ug/I ... . ................. ........ .............. ........................... C5- C8 Aliphatics II1 50 ug/I ................ C9- C12 Aliphatics I1 <'< 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits ...... 615-59-8 2,5-Dibromotoluene '#I ;....... 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene $% i>; 70-130% .............. .. . ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW17-MW-17 Lab Sample 11): M22269-16 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1251.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units ........................... 71-43-2 BenzeneNI). ......... . .............. 5.0 ug/I . ................... .......................... 100414 Ethylbenzene -lull:;:;;::;;:;;::;:; ug/I ...................... . ................ 1634-044 Methyl Tert Butyl Ether 5.0 ug/I ...................... ................... 91-20-3 Naphthalene ..........1.. 5.0 ug/I .............. ..................---... ........... .......108-88-3 Toluene 5.0ug/I .................... . .......... ........................... m,p-Xylene 5.0 ug/l .... ..............- --............. ..............- 9547-6 o-Xylene ............ 5.0 ug/I C5-C8 Aliphatics(Unadj.) 50 ug/l .............. ............ .................... ........... C9-C12 Aliphatics(Unadj.) 50 ug/I .... .......... .................... C9- C10 Aromatics(Unadj.) 50 ug/I ............. ...... ......................... ............... C5-C8 Aliphatics N D . ug/I .............. ............... ...................... ......................... ................. C9-C12 Aliphatics 50 ug/l ................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits .................... 615-59-8 2,5-Dibromotoluene 70-130% .......... ........ 615-59-8 2,5-Dibromotoluene . . 70-130% ......... ........ ................. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound i Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: M W 16D-M W-16D Lab Sample ID: M22269-15 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1256.1) 10 12/08/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene 14f#><>»> 50 ug/I ........................... ........................... ........................... 100-41-4 Ethylbenzene 1IDi50 ug/I.. ........................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether 10tY>' 50 ug/I ........................... ........................... ........................... 91-20-3 Naphthalene N1 <>>; ? 50 ug/I :.:........................ ........................... .........................— 108-88-3 Toluene ND50 ug/I m,p-Xylene X..l i >> 50 ugh ........................... ........................... ........................... 95-47-6 o-Xylene NIA'::`::;;::::::;::>s 50 ug/1 ........................... ........................... ........................... CS-C8 Aliphatics(Unadj.) l $4Q < 500 ug/1 .................... ........................... C9-C12 Aliphatics(Unadj.) ?29 500 ug/1 .. .................. ........................... ........................... C9-C10 Aromatics(Unadj.) 55 500 ug/1 ........................... ........................... C5-C8 Aliphatics 500 ug/I ........................... _.......................... ........................... C9-C 12 AliphaticsIT3; :...: 500 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene S% _ 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene i . 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW16-MW-16 Lab Sample ID: M22269-14 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1250.D 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 1NI).. ; ><z5.0 ug/I 100 41-4 Ethylbenzene NI)> ` 5.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 5.0 ug/1 ...........I91-20-3 Naphthalene ............... ............... 5.0 ug/1 :::: ............ ........ 108-88-3 Toluene IUD > ; 5.0 ug/1 ........................... ............I.............. ........................... ........................... m,p-Xylene ND>>< > 5.0 ug/1 95-47-6 o-Xylene N ; ; < 5.0 ug/1 C5-C8 Aliphatics(Unadj.) NID< ''' ; 50 ug/1 C9-C12 Aliphatics (Unadj.) aID >< ; 50 ug/1 C9-C10 Aromatics(Unadj.) NID 50 ug/I ... ................... ........................... ........................... C5-C8 Aliphatics 1I ; <; ; 50 ug/1 C9-C12 Aliphatics IT)>>> < 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 70 70-130% 615-59-8 2,5-Dibromotoluene ?G 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW15-MW-15 Lab Sample 1D- M22269-13 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1249.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene NI)< 5.0 ug/1 ........................... 100-41-4 Ethylbenzene 1 = 5.0 ug/1 .:......................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether NIA:;;:;;;::;::= 5.0 ug/1 91-20-3 Naphthalene 1`II3 5.0 ug/1 .......................... 108-88-3 Toluene NI) ;; 5.0 ug/1 m,P-Xylene D»> < » 5.0 ug/1 95-47-6 o-Xylene NI? 5.0 ug/1 CS-C8 Aliphatics(Unadj.) NTH;;;;:;:;:::::;:> 50 ug/1 C9-C12 Aliphatics(Unadj.) ND>` '< >">' S0 ug/1 ... .................. .....I..................... ........................... C9-C10 Aromatics (Unadj.) htl '> >; 50 ug/1 ... . .............. ........................... ............................ C5-C8 Aliphatics NIA < < 50 ug/1 C9-C12 Aliphatics II 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ............ 615-59-8 2,5-Dibromotoluene 77 70-130% ......................... .....-.................. ......................... 615-59-8 2,5-Dibromotoluene $:.:% < €` <= 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M22269-12 Date Sampled: 12/04/01 Matrix: AQ- Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method ............................... .................................. Alkalinity, Total Q<>i i <i> 5.0 mg/l 1 12/11/01 BF EPA 310.1 Carbon Dioxide 4:1 5.0 mg/1 1 12/14/01 MA SM18 45000O2D ................................: .................................. Nitrogen, Nitrate a 6<n<<>> >< 0.51 mg/1 1 12/12/01 MA EPA 353.2 Nitrogen, Nitrate + Nitrite 6:0;:;:;:;: :;> :; 0.50 mg/1 5 12/12/01 MA EPA353.2 Nitrogen, Nitrite ( i l(l<< 0.010 mg/l 1 12/05/01 MA EPA 354.1 Sulfate $<> ' < »; 5.0 mg/1 1 12/10/01 BF EPA 375.4 .......:......................... .................................. Sulfide 2 mg/l 1 12/07/01 BF -EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M22269-12 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II18747.1) 1 12/10/01 ANJ n/a n/a N:GII937 Run#2 CAS No. Compound Result RL Units P Q ........................... ........................... 74-82-8 Methane ND ; 0.10 ug/1 ........:.................. ........................... (a) Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW14-MW-14 Lab Sample ID: M22269-12 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX1248.1) 1 12/07/01 AF n/a n/a GWX35 Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......................... 71-43-2 Benzene ND>'>ii_ < 5.0 ug/1 ......................... ........................... .......................... ........................... 100-41-4 Ethylbenzene ND' 5.0 ug/1 ............................ _...............__... ........................... 1634-044 Methyl Tert Butyl Ether NIA::::;:;::::::::`; < 5.0 ug/1 91-20-3 Naphthalene I ` '< 5.0 ug/1 .:........................ ........................... .......................... 108-88-3 Toluene ID5.0 ug/1 .......................... ........................... .......................... m,p-Xylene ND <<»>< >; 5.0 ug/1 95-47-6 o-Xylene ND< = ' 5.0 ug/1 ........................... .......................... ........................... C5-C8 Aliphatics (Unadj.) N)?'< - i 50 ug/1 ... ...............:.... C9-C12 Aliphatics(Unadj.) 1tID >;>`'< 50 ug/1 .................. ........................... ........................... C9-C10 Aromatics(Unadj.) ltii . 50 ug/1 ............. ........................... ........................... C5-C8 Aliphatics 1'+ID< 50 ug/1 .:......................... ............................ .......................... C9-C12 Aliphatics I ; 'S0 ugh CAS No. Surrogate Recoveries Run#1 Run#2 Limits .................... 615-59-8 2,5-Dibromotoluene 75%':i 70-130% 615-59-8 2,5-Dibromotoluene ::76.<> 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M22269-11 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity, Total ( .* 5.0 mg/l 1 12/11/01 BF EPA 310.1 ......................:........... ................................. .................................. Carbon Dioxide 21;'T 5.0 mg/1 1 12/14/01 MA SM18 45000O2D ....:............................ .................................. ................................. Nitrogen, Nitrate a 2l?=<< ;>>> ; ; 0.11 mg/1 1 12/12/01 MA EPA 353.2 Nitrogen, Nitrate + Nitrite 2 d = 0.10 m /l 1 12/12/01 MA EPA 353.2 g g.................................. ................................. .................................. Nitrogen, Nitrite <4 f3:10> <0.010, mg/1 1 12/05/01 MA EPA 354.1 Sulfate 7 „ ; ;>; 5.0 mg/1 1 12/10/Ol BF EPA 375.4 Sulfide <2I. mg/1 1 12/07/01 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M22269-11 Date Sampled: 12/04/01 Matrix: AQ-Ground Water Date Received: 12/05/01 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II18746.1) 1 12/10/01 ANJ n/a n/a N:GII937 Run#2 CAS No. Compound Result RL Units Q 74-82-8 Methane III ' 0.10 ug/1 (a) Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M22269-12A Date Sampled: 12/04/01 Matrix: AQ-Groundwater Filtered Date Received: 12/05/01 Percent Solids: n/a Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ...................-...... Iron <1.0(?;! 100 ug/1 1 12/06/01 12/10/01 LMN SW846 6010B SW846 3010A RL = Reporting Limit SAMPLE INFORMATION Aqueous usoji U Sediment Other. Satisfactory U Broken U Leaking: Aqueous U WA r?s NOT pH>2 U Leaking: Soil or LJ WA L.Iserved in Methanol or mL Methanogg soil Sediment Samples rec'd in Methanol: LJ covering soil U not covering sal ❑1:1+/-25% Samples reed in air-fight container. ❑Other. Received on Ice Rec'd at 4 Deg.C LAoth reed at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID FB MW01-MW-1 MW01A-MW-1A Method for Target Analytes:MADEP VPH 98-1 Lab ID M22269-17 M22269-1 M22269-4 VPH Surrogate Standards Date Collected 12/4/01 1214/01 12/4/01 PID:2,5-Dibromotoluene Date Received 12/5/01 12/5/01 12/5/01 FID:2,5-Dibromotoluene Date Analyzed 12/8/01 1218/01 12/7/01 Dilution Factor 1 2 1 %Moisture(soil) Range/Target Analyte Elution Range Units 1 Result RL Q Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) WA ND 50 1000 100 ND 50 Unadjusted C9-C12 Aliphatics(1) N/A ND 50 839 100 ND 50 Benzene C5-C8 ug/I ND 5 42.3 10 ND 5 Ethylbenzene C9-C12 ug/I ND 5 63.8 10 ND 5 Methyl-tert-butylether C5-C8 ug/I ND 5 768 10 ND 5 Naphthalene WA ugA ND 5 ND 10 ND 5 Toluene C5-C8 ugA ND 5 140 10 ND 5 m-&p•Xylenes C9-C12 ug/I ND 5 189 10 ND 5 o-Xylene C9-C12 ugA ND 5 85.1 10 ND 5 C5-C8 Aliphatic Hydrocarbons(1,2) N/A ugA ND 50 ND 100 ND 50 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ugn ND 50 181 100 ND 50 C9-C10 Aromatic Hydrocarbons(1) WA ugA ND 50 320 100 ND 50 PID Surrogate%Recovery 78 74 71 FID Surrogate%Recovery 77 73 71 Surrogate Acceptance Range 70-130% 1 70-130% 1 70-130 1-Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 2-05-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 3-C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-Cl0 Aromatic Hydrocarbons 4-A'J'qualifier indicates an estimated value CERTIFICATION Were all QA/QC procedures REQUIRED by the VPH Method followed? U,Yes Li No-Details Attached Were all performance/acceptance standards for required QA/QC procedures achieved? Q Yes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.37 10 No ❑ Yes-Details Atlatched 1 attest under the pains and penalties of perjury that based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and7behef, rate and complete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 PLE INFORMATION Ld Aqueous usoil U Sediment LJ Other. Satisfactory LJ Broken U Leaking: Aqueous NIA &NOT pH'2 Leaking: Soil or N/A ed in Methanol or mL Methanoltg soil Sediment Samples reed in Methanol: covering soil not covering soil ❑1:1+!-25% Samples rec'd in air-fight container. ❑Other. Received on Ice U Reed at 4 Deg.C .r oth reed at 3 deg C ANALYTICAL RESULTS od for Ranges:MADEP VPH 98-1 Client ID MW02-MW-2 MW02A-MW-2A MW03A-MW-3A od for Target Analytes:MADEP VPH 98-1 Lab ID M22269-2 M22269-3 M22269-5 Surrogate Standards Date Collected 12/4/01 12/4/01 1214/01 ID:2,5-Dibromotoluene Date Received 12/5/01 12/5/01 1215/01 ID:2,5-Dibromotoluene Date Analyzed 12/8/01 12/7/01 12/10/01 Dilution Factor 1 1 1 %Moisture(soil) e/Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q justed C5-C8 Aliphatics(1) N/A ND 50 218 50 ND 50 Jjusted C9-C12 Aliphatics(1) N/A ND 50 ND 50 ND 50 gene C5-C8 ugA ND 5 14.1 5 ND 5 lbenzene C9-C12 ugA ND 5 ND 5 ND 5 yl-tert-butylether C5-C8 ugA ND 5 214 5 50.6 5 thalene N/A ugA ND 5 ND 5 ND 5 ne C5-C8 ugA ND 5 ND 5 ND 5 p-Xylenes C9-C12 ugA ND 5 ND 5 ND 5 lene C9-C12 ugA ND 5 ND 5 ND 5 8 Aliphatic Hydrocarbons(1,2) WA ugA ND 50 ND 50 ND 50 12 Aliphatic Hydrocarbons(1,3) N/A ugA ND 50 ND 50 ND 50 10 Aromatic Hydrocarbons(1) WA ug/I ND 50 ND 50 ND 50 urrogate%Recovery 74 73 84 urrogate%Recovery 73 74 81 ate Acceptance Range I I 170-130% 70-130% 70-130% drocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range -C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-Cl0 Aromatic Hydrocarbons J.qualifier indicates an estimated value TIFICATION II QA/QC procedures REQUIRED by the VPH Method followed? Yes u No-Details Attached II performance/acceptance standards for required QA/QC procedures achieved? .r ❑Yes ❑ No-Details Attached ny significant modifications made to the VPH method,as specified in Sect 11.3? No ❑ Yes-Details Attatched under the pains and penalties ofpelury that,based upon my inquiry of those individuals immediately responsible for ing the information,the material contained in this report is,to the best of my knowledge and belief,accurate and fe. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 SAMPLE INFORMATION 121 Aqueous usoil u Sediment Uother ✓ Satisfactory U Broken U Leaking: Aqueous N/A ✓ 9s NOT UpH>2 U Leaking: Soil or U N/A ILJserved in Methanol or mL Methanol/g soil Sediment U Samples reed in Methanol: covering soil U not covering soil ❑1:1 Other 25% Samples reed in air-tight container. ❑ W Received on Ice U Rec'd at 4 Deg.C ✓Oth reed at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID MW04-MW-4 MW05-MW-5 MW05-MW-5 Method for Target Analytes:MADEP VPH 98-1 Lab ID M2226M M22269-7 M22269-7 VPH Surrogate Standards Date Collected 12/4/01 12/4/01 1214/01 PID:2,5-Dibromotoluene Date Received 12/5/01 12/5/01 12/5/01 FID:2,5-Dibromotoluene Date Analyzed 12/10/01 12/8/01 12/10/01 Dilution Factor 1 10 250 %Moisture(soil) Ranger target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) WA ND 50 56700 500 Unadjusted C9-C12 Aliphatics(1) N/A ND 50 17700 500 Benzene C5-C8 ugA ND 5 2260 50 Ethylbenzene C9-C12 ugA ND 5 1390 50 Methyl-tert-butylether C5-C8 ugA 15.2 5 46900 1300 Naphthalene N/A ugA ND 5 270 50 Toluene C5-C8 ugA ND 5 10000 50 m-&p-Xylenes C9-C12 ugA ND 5 5110 50 o-Xylene C9-C12 ugA ND 5 2580 50 C5-C8 Aliphatic Hydrocarbons(1,2) WA ugA ND 50 ND 500 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ugA ND 50 4400 500 C9-C10 Aromatic Hydrocarbons(1) N/A ugA ND 50 4220 500 PID Surrogate%Recovery 83 82 FID Surrogate%Recovery 80 77 82 Surrogate Acceptance Range 70-130% 70-130% 70-130% 1-Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 2-C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 3-C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons 4-A•J'qualifier indicates an estimated value .CERTIFICATION Were all QArQC procedures REQUIRED by the VPH Method followed? ✓Yes u No-Details Attached Were all performance/acceptance standards for required QA/QC procedures achieved? [21 Yes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.3? O No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this reportis,to the best of my knowledge and belief, rate and complete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 �MPLE.INFORMATION Aqueous U Soil Li Sediment U Other. - Satisfactory Broken U Leaking: Aqueous U N/A &NOT pH>2 u Leaking: Sala N/A served in Methanol or mL MethanoVg soil Sediment Samples reed in Methanol: U covering soil U not covering soil ❑1:1+/-25% Samples reed in air-tight container. [I Other. LA Received on Ice U Reed at 4 Deg.C Woth reed at 3 deg C H ANALYTICAL RESULTS od for Ranges:MADEP VPH 98-1 Client ID MW06-MW-6 MW11-MW-11 MW12-MW-12 od for Target Analytes:MADEP VPH 98-1 Lab ID M22269-8 M22269-9 M22269-10 Surrogate Standards Date Collected 12/4/01 1214/01 12/4/01 PID: Date Received 12/5101 12/5/01 12/5/01 FID:2,5-Dibromotoluene Date Analyzed 12/7/01 1217/01 1217/01 Dilution Factor 1 1 1 %Moisture(soil) ge/Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q adjusted C5-C8 Aliphatics(1) N/A 206 50 NO 50 ND 50 adjusted CO-C12 Aliphatics(1) N/A ND 50 ND 50 ND 50 izene C5-C8 ug/I 15.6 5 ND 5 ND 5 ylbenzene C9-C12 ug/1 ND 5 ND 5 NO 5 thyl-tert-butylether C5-C8 ugA 173 5 ND 5 ND 5 'hthalene N/A ugA ND 5 ND 5 ND 5 e C5-C8 ug/I ND 5 ND 5 ND 5 -Xylenes C9-C12 ug/I ND 5 ND 5 ND 5 ne C9-C12 ug/I ND 5 ND 5 ND 5 Aliphatic Hydrocarbons(1,2) N/A ug/I ND 50 NO 50 ND 50 C12 Aliphatic Hydrocarbons(1,3) N/A ugA ND 50 ND 50 ND 50 C10 Aromatic Hydrocarbons(1) N/A ugA ND 50 ND 50 ND 50 Surrogate%Recovery 73 75 75 Surrogate%Recovery 73 76 76 ate Acceptance Range 70-130% 170-130% 170-130 yMcarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range 9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of Cg-Cl0 Aromatic Hydrocarbons V qualifier indicates an estimated value RTIFICATION all QA/QC procedures REQUIRED by the VPH Method followed? U4 Yes U No-Details Attached all perfomtancelacceptance standards for required QA/QC procedures achieved? QYes ❑ No-Details Attached any significant modifications made to the VPH method,as specified in Sect 11.37 Q No ❑ Yes-Details Attatched >sf under the pains and penalties of perjury that,based upon my inquiry or those individuals immediately responsible for fining the information,the material contained in this report is,to the best of my knowledge and belief,a urate and Mete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 SAMPLE INFORMATION Aqueous usoil U Sediment U Other. Satisfactory U Broken Leaking: Aqueous WA &NOT LJpH'2 U Leaking: Soil or WA Userved in Methanol or mL MethanoUg soil Sediment Samples reed in Methanol: U covering soil U not covering soil ❑1:1+/-25% Samples reed in air-tight container. [I Other. Received on Ice Rec'd at 4 Deg.C .r Oth ec'd at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID MW13-MW-13 MW14-MW-14 MW15-MW-15 Method for Target Analytes:MADEP VPH 98-1 Lab ID M22269-11 M22269-12 M22269-13 VPH Surrogate Standards Date Collected 1214/01 12/4/01 1214/01 PID:2,5-Dibromotoluene Date Received 1215/01 12/5/01 1215/01 FID:2,5-Dibromotoluene Date Analyzed 12/7/011 12/7/01 12/7/01 Dilution Factor 1 1 1 %Moisture(soil) Range/Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 50 ND 50 ND 50 Unadjusted C9-C12 Aliphatics(1) N/A NO 50 ND 50 ND 50 Benzene C5-C8 ugn ND 5 ND 5 ND 5 Ethylbenzene C9-C12 ugn ND 5 ND 5 ND 5 Methyl-tert-butylether C5-C8 ugn ND 5 ND 5 ND 5 Naphthalene N/A ugn ND 5 ND 5 ND 5 Toluene C5-C8 ugn ND 5 ND 5 ND 5 m-$p-Xylenes C9-C12 ugn ND 5 ND 5 ND 5 o-Xylene C9-C12 ugn ND 5 ND 5 ND 5 C5-C8 Aliphatic Hydrocarbons(1,2) N/A ugn ND 50 ND 50 ND 50 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ugn ND 50 ND 50 ND 50 C9-C10 Aromatic Hydrocarbons(1) N/A ug/I ND 50 ND 50 ND 50 PID Surrogate%Recovery 76 76 78 FID Surrogate%Recovery 76 75 77 Surrogate Acceptance Range I 1 1 70-130% 1 70-130% 1 70-130% 1-Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards eluting in that range 2-C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 3-C9C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons 4-A'J'qualifier indicates an estimated value CERTIFICATION Were all QAIQC procedures REQUIRED by the VPH Method followed? WYes U No-Details Attached Were all performance/acceptance standards for required QA/QC procedures achieved? Q Yes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.3? Q No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,acc to and complete. SIGNATURE: POSITION:laboratory Director PRINTED NAME: Reza Tan DATE: 12/19/01 a PLE INFORMATION Aqueous LJ Soil U Sediment Other. Satisfactory LJ Broken U Leaking: Aqueous NIA &NOT UpH>2 Li Leaking: Sal or N/A served in Methanol or mL Methanollg soil Sediment U Samples reed in Methanol: Lj covering soil U not covering soil ❑1:1+/-25% Samples rec'd in air-tight container. ❑Other. Mal U1 Received on Ice U Reed at 4 Deg.C IAOth reed at 3 deg C ANALYTICAL RESULTS od for Ranges:MADEP VPH 98-1 Client ID MW16-MW-16 MW16D-MW-16D MW17-MW-17 od for Target Analytes:MADEP VPH 98-1 Lab ID M22269-14 M22269-15 M22269-16 Surrogate Standards Date Collected 12/4/01 12/4/01 1214/01 ID:2,5-Dibromotoluene Date Received 12/5/01 1215/01 1215101 ID:2,5-Dibromotoluene Date Analyzed 1217/01 12/8/01 12/7/01 Dilution Factor 1 10 1 %Moisture(soil) e/Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q justed C5 C8 Aliphatics(1) WA ND 50 14800 500 ND 50 lusted C9-C12 Aliphatics(1) N/A ND 50 729 500 ND 50 !ene C5-C8 ug/I ND 5 1410 50 ND 5 (benzene C9-C12 ug/I ND 5 ND 50 ND 5 1yl-tert-butylether C5-C8 ug/I ND 5 11500 50 ND 5 thalene N/A ug/I ND 5 ND 50 ND 5 ne C5-C8 ug/I ND 5 ND 50 ND 5 p-Xylenes C9-C12 ug/I ND 5 ND 50 ND 5 lene C9-C12 ug/l ND 5 ND 50 ND 5 Aliphatic Hydrocarbons(1,2) N/A ug/I ND 50 1830 500 ND 50 12 Aliphatic Hydrocarbons(1,3) WA ugA ND 50 ND 500 ND 50 10 Aromatic Hydrocarbons(1) WA ug/I ND 50 555 500 ND 50 urrogate%Recovery 76 76 78 urrogate%Recovery 76 75 78 ate Acceptance Range I 1 1 70-130% 70-130% 70-130 rocarbon Range data exclude concentrations of any sunogatel s)and/or internal standards eluting in that range 8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons X qualifier indicates an estimated value TIFICATION II QA/QC procedures REQUIRED by the VPH Method followed? Yes U o-Details Attached II perfonnance/aa:eptance standards for required QA/QC procedures achieved? El Yes ❑ No-Details Attached ny significant modifications made to the VPH method,as specified in Sect 11.37 No ❑ Yes-Details Attatched under the pains and penalties of perjury that based upon my inquiry of those individuals immediately responsible for ing the information,the material contained in this report is,to the best of my knowledge and belief,accurate and ete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 SAMPLE INFORMATION Ld Aqueous Usoil U Sediment U Other. Satisfactory U Broken U Leaking: Aqueous U N/A &NOT UpH>2 U Leaking: Soil or U N/A rved in Methanol or ml-MethanoVg soil Sediment Samples reed in Methanol: U covering soil U not covering soil ❑1:1+/-25% Samples reed in air-tight container. ❑Other. Received on Ice U Reed at 4 Deg.C Woth reed at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID TB Method for Target Analytes:MADEP VPH 98-1 Lab ID M22269-18 VPH Surrogate Standards Date Collected 12/4/01 PID:2,5-Dibromotoluene Date Received 12/5/01 FID:2,5-Dibromotoluene Date Analyzed 12/8/01 Dilution Factor 1 %Moisture(soil) RangefTarget Analyte Elution Range Units Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 50 Unadjusted C9-C12 Aliphatics(1) N/A ND 50 Benzene C5-C8 ugA ND 5 Ethylbenzene C9-C12 ugA ND 5 Methyl-tert-butylether C5-C8 ugA ND 5 Naphthalene N/A ug/I ND 5 Toluene C5-C8 ugA ND 5 rn-&p-Xylenes C9-C12 ugA ND 5 o-Xylene C9-C12 ugA ND 5 C5-C8 Aliphatic Hydrocarbons(1,2) N/A ugA ND 50 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ugA ND 50 C9-Cl0 Aromatic Hydrocarbons(1) N/A ugA ND 50 PID Surrogate%Recovery 75 FID Surrogate%Recovery 74 Surrogate Acceptance Range 70-130% 1-Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 2-CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 3-C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons 4-A*Jr qualifier indicates an estimated value CERTIFICATION Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes U No-Details Attached Were all performance/acceptance standards for required QA/QC procedures achieved? ❑r Yes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.3? I]No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining Me information,the material contained in this report is,to the best of my knowledge and belief,a to and complete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 12/19/01 Sent By: GEOLOGIC SERVICES CORP; 978 568 9316; Dec-5-01 18:09; rage ite To: A[CUTEST AAA A;: 15084817753 Geologic Services • • • • • Fax Fmc D UmeM ftWow ❑Memo cmwaont D Please Reply O Mease Reayde G-^S �� . �o r:�� �t". �t.. Grp✓� 5 i art Cad*Services Cwpmioa•15 Dvouol Avenw•t k ton.MA 01749•Phona(978)56W40•Fax(97B)56M16 I .=:lr q CHAIN OF CUSTODY ors 1 Fv/Wm tail W 1 G17 w • Bull w a F aai1RL80AD1IBli,A64 017�7 ACC1f f EST GUm is p� a FACILRY INFDRMAT101/ i ANALYTICAL WFORMATION t. 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Z.� C"�s[) Z. S B�f 1� Z. iIENWV mwow.. DAM iNO: lwCRlrmiY IwaWOYwIwO BAfti ES60YloRri m 3. 3. 4. 14. c REUNOWS"M E:r: DAM TXM Ftncvwwovt sEJY,rr MUM wwwEArMEra m ae= nwEYQY1IE ch b- b- Cl ❑ n LiTEST495TECHNOLOGY CENTER WEST • BUILDINGONE -F/a"' Or v7 MARLBOROUGH,MA 01752 rACCUTEST QUOTE t TEL:508-481-6200 • FAX:508-481-7753 CLIENT INFORMATION `FrA-CIILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES i COS' � J`Cb 5fc__ FACILITY 0002 _1 DW- DRINKING WATER NAME PROJECT NAME GW- GROUND l i a?:Rn11 A- Inc: -m 9G a ZsoZR WATER WW- WASTEAD LOCATION WATER I 4 0(7q9 CQ gu n� 4�SO9 SO- SOIL CITY-- ,ff STATE ZIP PROJECT NO. y/ SL- SLUDGE n 'To t/14-(.�Q � IlC'� k4nap;S, rn� � � 01-UQ- OTHER OIL SEND REPORT TO•'' LIQUID PHONE# . C FAX 97& . � SOL•OTHER ACCUTEST COLLECTION x PRESERVATION Q '� SOLID � �( SAMPLE p FIELD ID/POINT OF COLLECTION DATE TIME SA BYLED °m J LAB USE ONLY W-T -- --3 'mw - mw-2A 1100 mw ✓ ✓ ✓ ✓ ✓ y _ m - rn z ✓ ' _ rr) -4 i Z, ✓ ✓ 7 m S - ry\w-S 1 Mc. ,� ✓ -g - rT)W-G Faal -� ✓ ✓ _g ✓ now I — 14 Z �/ ✓ -l� mwl3 - mw - 3 1110 PILM 2 DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTSIREMARKS 0�7 DAYS RUSH DAYS STANDARD APPROVED BY: Qj COMMERCIAL"B"STANDARD Ve sga/n e s �-[+V d b A66C O 48 HOUR EMERGENCY O DISK DELIVERABLE � eA �� D OTHER ❑ STATE FORMS LOG • ok 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX D OTHER(SPECIFY) 3 lam/'e DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVE RELINQUISHED BYiSAMPLER: DATE TIM : RECEIVED BY: RELINQUISHED BY: DATE TIME: RECEIVED BY: 1. I --, of (Um 1. 2. lg20 2. RELINQ ISNED BY: DATt TIME: RECEIVED BY, RELINQUISHED BY: DAT TI : RECEIVED BY: 3. - /2 3. 4. 4. r5.ELINQUISHED BY: DATE TIM RECEIVED BY: SEAL/ PRESERVE WHERE APPLICABLE ON ICES TEWERATURC 5. ['r ^S_2 mild �g L"K " CHAIN OF CUSTODY ACCUTEST JOB IT: MAC CUTEST 495 TECHNOLOGYLSORO GHWET • BUILDING ONE y MA 01752 ACCUTEST QUOTE k TEL:508-481-6200 • FAX 508-481-7753 CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES G!.-oloci-� SQy C't<' C.tr - ar S i.ilor �000 DW' WATER DRINKING NAME i PRZ( ECT NAM (Q� GW- GROUND (S� i•� �lc� l�.502 e WW- WWATER ASTE ADDIR,ESS LOC�A.TION WATER T'W��s6Y� MA �r7�q &=G, mZTbq � y� SO- SOIL CITY, STATE ZIP PROJECT NO. 'J 1 , . -}+ SL- SLUDGE 0AZ Ict �J'���o r �►-1st= Q n O 11 d� �d 4A, O SLITA '� Of- OIL LIO- OTHER SEND REPORT TO: �, ` $OL-OTHER PHONE# C ?R- ti C.51 - K7 C FAX# o-Z i1�S-4 31�' COLLECTION , t H PRESERVATION N SOLID ACCUTEST m SAMPLE# FIELD ID/POINT OF COLLECTION SAMPLED ►- ° _ u, a '� DATE TIME BY; `$ i i g ill a - LAB USE ONLY ✓ J J �aaa6�1144 — of i4 m thw � ✓ ✓ oa ✓' -16 MWI(ab - OqZ om J �' --� - - 1-7 1345 mW Z 1 ✓ - 17 fb ► rnLV\ Z ✓ — (8 10u DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTS/REMARKS 14 DAYS STANDARD APPROVED BY: STANDARD \S�j �Z Sd1Y�Ol _ YJSI 6AL O 7 DAYS RUSH O COMMERCIAL"B" O 48 HOUR EMERGENCY O DISK DELIVERABLE O OTHER O STATE FORMS 1 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX O OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERY 4ti:,• `, RELINQUISHED BY SAMP .R: ?AT TIME: RECEIVED BY: RELINQUISHED BY: DATE TIME: RECEIVED BY: rRELINOUISHED o� '4cv 1. ( F 2. I 2. ELIN UISHE BY:. DA E: RECEIVED BRELINQ ISHED BY: DA ME: RECEIVED BY: . /L .S� 3. 4. 4. BY: DA E T1M : RECEIVED BY: SEAL PRESERVE WHERE APPLICABLE ON IC TEMPERATURE . 5. 0 _0 C Y ' New England OS/17/02 ®ACCUrEST >» echcal Report. o .;.:.... Equiva Services GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Accutest Job Number: M24976 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 76 4T`4���M 11CepAe_� - 1 Op Test results contained within this data package meet the requirements eza d of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications:MA(MA136) CT(PH-0109) NH(250293) RI(A-71) ME(MA136) USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 0 495 Tech Center West■Building 1 0 Marlborough,MA 01752 0 tel:508481-6200■ fax:508-481-7753 0 http://www.accutest.com Accutest Laboratories Sample Summary Equiva Services Job No: M24976 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA .................................................... Sample GoUected' >>[> Matrix Client .................................................... Number Date Time By Received Code Type Sample ID ........................... aVM49?G=1 05/ 1 0 /02 10:00 HG OS/02/02 A r Q Ground Water Ia+1WUlA_:MW�IA> >> > =:>__>:>:>::><:»:><:>:>: <>_ ........................... . >< :»=2 > :>2-4 . 05/01/02 11:25 HG 05/02/02 AQ Ground Water M :::: :::::::: ::::: ......................... M24 97€r-3... OS/Ol/02 1 .,............;::....... 0.30 HG OS/02/02 A Ground Water MV03A:::MW�::3A::>:=<:>>:::>:::s>: ::: >:: Q 9> 05/01/02 15:30 MLM A =4.: fi.:._._. 05/02/02 AQ Ground Water 0::: ::.<T::::>............:> .....<:_: :.............................: M24.7 5< 9. OS/Ol/02 1 3 30 MW 05/ 2 0 0 / 2 A r Q Ground Water M.-W. .. 2;;h -2:::::>:<:::::::;>:;:.::>:<:::::><:::>::::>::«:::<:.......... .. 05/01/02 14.4 .::.....::»::>::>::>::»::>::«::<>:;>:::::;>:;:::<:::>:>.:: �...... 0 HG OS/02/02 AQ Ground Water N IF4 :r 1� :<5.;:.;:.;:.;.;;:.;;;;:.;;;;:.;;;.;;:.;:;:.; ........................... M24::7 16.35 MLM OS/02/02 AQ Ground Water IYIW06..:-...v�`3?V-....<:::>:<:»>::>:<:::>::»»:<::<»::<:>:: ...... :.::::::::::::::.:. .............:.:::.::......::..:::::::::::::::::::.:::::::::::::::::,:._::::::::::.: - >::05/01/02 14:1 - M2A97..... 5 MW OS/02/02 A Ground Water ........................... <M24976= > 4 3. 0 MW 0 2 Q Ground Water1kf �lp::s::: OS/Ol/02 1 ........:::.:..:......... 7 : : :;05 1/ 2/0 0 11:4 M 9.fi-1€�. 0 MW OS/02/02 A .::::::::.:...... Ground Water ........................... ........................... M20 1:OS/Ol/02 1 3.20HG 0 / 2 2 5 0 /0 A Ground Q ound Water MVit:l2:=M3?V:<>12:: _>:>::>:>:> ;;>:: ::>::::><::: >::::::>:>::::: ..........: :iM' 249':64 >2'05/01/02 13:4 LM :.::::.....:::::::::.::::: 1 . 5 M OS/02/02 A Ground Water _.._.............. Q 1tW MW ........................... aI2'4976-13 .. ... 5. 0 RA 05/02/02 AQ Ground Water MW1 .-M :=::4::<:>::>::::>:>;<:>:::<:>:<::<::::<::::::>:>::>::<_::>:<:::; Accutest Laboratories Sample Summary (continued) Equiva Services GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Job No: M24976 Samplettit < > > Matrix Client Number Date Time By Received Code Type Sample ID ........................... 14.451tA OS/02/02 A Ground Water MW�41 ........................... M24 .. 976..1 .05/Ol/02. �. 14:11 RA 05/02/02 A Ground Water 14I =: <:: ::::<:>: ......................................... ........................... <.M 05/O 1/02 09:35 HG OS/02/02 AGround Water ....., 9 ........................... ........................... 97b 7 1 OS/ ...... 09:30 MW OS/02/02 A Ground Water 1: »»>::::::::»::::<;>::::<:>:<:::>::;:;:;::::> «<::: ::><:> ............................ M249 i-1$ 05/01/02 10:05 MW 05/02/02 A Ground Water -W.%- M24:.:::-6- '.. .9 ..9 05/01!02 1 RA 05/02/02 AQ Ground Water IVIVV27:h1W::17:::<:>::><:>»:::<:><:::;::;:;:; :::;:«:»:::>::»:_»:<:;:: M249::.6=..2Q 0.OS/01/02 10:25 MW 05/02/02 A Ground Water A. ..1 OS/O1/ 2 5 MW 05/02/02 A Ground Water MW:1:S:D.� ... .....Q NIW.;:;:$.;; .. .......................... 24 7f 2. 05/O1/02 1 6.4 0 HG 05/02/02 Q Field Blank Water - 3::::::>::>::>::>::>::<:»:: ::>< .......... ivi ':49 . .. 76 2 .OS/Ol .:::::::.::.::::::.::.:.:::::::::.::.::::::::::::::: 3 /02 16:50 MLM 05/02/02 AQ Trip Blank Water ;>T�T$:>::>::::>::>>:::::>::::: P M2497£ A 05/01/02 11:50 MLM 05/02/02 A Ground ................. Q Water ........................... M24976"2$ OS/O1/02 14:00 MLM OS/02/02 A Q Ground Water TM Iai 2 a: ::>:::<:::>::>:::<:>:>»::::»::::«::«<::: ;10.249 6:4A05/01/02 11:25 HG 05/02/02 A Gr un w Q o dater Filtered :ItV�f72A=MVCs2:.'<: ::»>:»«:::>:<:»:>:>:::<:;:::>::>::»:: ................................:..A.:::::::: .:. Accutest Laboratories Sample Summary (continued) Equiva Services Job No: M24976 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA ............................... .................................................... Sample .W Matrix Client Number Date. 1hme By Received Code Type Sample ID ....:.::..::.::::::::: ::.::: iVI24976=3A 05/01/02 10:30 HG 05/02/02 A Groundwater Filtered :::MW#3A:."' A '> >> >>«> ........................... Q ...................... 1+...................... 49.- /01/ 2 1 OS 0 5.30 MLM OS/02/02 A Groundwater Fil Q NIW.;:.;:;.;11'.::::::::.:: ::.:::::::::::::::.:::::....:::... :....:.:.::.::.::.....:.::.. :.:::: ::::::::::::::::::::.::::::.::::.:::. M249W.6A 05/01/02 14:40 HG 05/02/02 A Groundwater Filtered »:: : ::: .... .. ........................... ................... ..................................................................................... UR.7 RA 05/01/02 14:1 5 MW OS/02/02 A Groundwater 9........... G o ater Filtered }V13N .. . W:9 . >` > :. 1H2497. 2 5/O102 1 4:.......:.:.:,.:6.�._A / 3. 5 MLM 05/02/02 A Groundwater Filtered :1viVV :3:MW::13:: ::::><:>::>::<:>::>:::«:>:>:::::»::< ><:::>;:;:> M4:.76>':3P05/O 1/02 1 2 5. 0 RA /02/02 A Groundwater F'OS G ate Filtered :lyll 11 »>>_>> >> < > Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW01A-MW-IA Lab Sample ID: M24976-1 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13195.1) 1 05/12/02 AMY n/a n/a GMN371 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 5.0 ug/1 100-41-4 Ethylbenzene %N 3> 5.0 ug/l 1634-04-4 Methyl Tert Butyl Ether i 5.0 ug/1 91-20-3 Naphthalene II >><` 5.0 ug/1 108-88-3 Toluene Nl 5.0 ug/1 m,p-Xylene 5.0 ug/1 95-47-6 o-XyleneI?:«» ;>' 5.0 ug/1 C5-C8 Aliphatics(Unadj.) hi ' 50 ug/l C9-C12 Aliphatics(Unadj.) l 50 ug/1 C9-C10 Aromatics(Unadj.) NIA<'_< <> 50 ug/1 C5-C8 Aliphatics li <i 50 ug/1 ........................... ................... C9-C12 Aliphatics I?iD< 50 ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 85°J 70-130% 615-59-8 2,5-Dibromotoluene ><» 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M24976-2 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13196.1) 1 05/12/02 AMY n/a n/a GMN371 Run#2 MN13214.1) 2 05/13/02 AMY n/a n/a GMN372 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene `1 >``;<; 5.0 ug/l 100-41-4 Ethylbenzene i 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether �70(3 a ; 10 ug/1 91-20-3 Naphthalene 1 >> 5.0 ug/1 108-88-3 Toluene ]STD:::: :::; >> 5.0 ug/1 m,p-Xylene 1 :Q >< 5.0 ug/1 95-47-6 o-Xylene N1 <> <>` 5.0 ug/1 C5-C8 Aliphatics(Unadj.) ' a 100 ug/l C9-C12 Aliphatics(Unadj.) 1I `'> >< 50 ug/1 C9- C10 Aromatics(Unadj.) 825; > < 50 ug/1 C5-C8 Aliphatics I? 50 ug/1 C9-C12 Aliphatics 1 > >> 50 P ..........1...,.: u /1 g CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 7xo i> >Q9io _ 70-130% 615-59-8 2,5-Dibromotoluene BI T: 8> '= >>>< 7 - .:: 0 130% (a)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M24976-2 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 1121140.1) 1 05/14/02 ANJ n/a n/a N:G111034 Run#2 a 1I21141.1) 5 05/14/02 ANJ n/a n/a N:G111034 CAS No. Compound Result RL Units Q ........................... 74-82-8 Methane 4 ;''<> `< 0.10 ug/l Carbon Dioxide ::-620.i 500 ug/1 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 (b)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 P Y Client Sample ID: MW02A-MW-2A Lab Sample ID: M24976-2 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. ................................ Alkalinity, Total 135;; >< 5.0 mg/1 1 05/10/02 op EPA 310.1 Nitrogen, Nitrate a <.................. 0.I I mg/l 1 05/07/02 SK EPA 353.2 Nitrogen, Nitrate + Nitrite 0.10 mg/l 1 05/07/02 SK EPA 353.2 ........ .................. ................................. Nitrogen, Nitrite {)4L8 0.010 mg/1 1 05/02/02 nBm EPA 354.1 .................................. ................................. .................................. Sulfate I 5.0 mg/l 1 05/03/02 op EPA 375.4 ....... .............. .................................. Sulfide 1.0 ;;; 2.0 mg/1 1 OS/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)-(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW03A-MW-3A Lab Sample ID: M24976-3 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13197.1) 1 05/12/02 AMY n/a n/a GMN371 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND5.0 ug/1 10041-4 Ethylbenzene _ 5.0 ug/I 1634-04-4 Methyl Tert Butyl Ether I l? 5.0 ug/1 91-20-3 Naphthalene ? 5.0 ug/1 108-88-3 Toluene I3 ;;;' 5.0 ug/1 m,p-Xylene Nb > > » 5.0 ug/1 95-47-6 o-Xylene 33>: ;; 5.0 ug/l C5-C8 Aliphatics (Unadj.) I 50 ug/1 C9-C12 Aliphatics(Unadj.) ItID`' >>< 50 ug/I C9-C10 Aromatics(Unadj.) ;AP* ' 50 ug/1 C5-C8 Aliphatics ATT 50 ug/1 C9-C 12 Aliphatics Nib 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 7 70-130% ......................... 615-59-8 2,5-Dibromotoluene % 70-130% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M24976-3 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 1121142.1) 1 . 05/14/02 ANY n/a n/a N:GII1034 Run#2 CAS No. Compound Result RL Units Q ............. ...... ........................ 74-82-8 Methane .. 0.10 ug/I ................................... ........... 12 ........Carbon Dioxide 100 ug/I ........................... (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M24976-3 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method Alkalinity, Total53'> > 5.0 mg/1 1 05/10/02 OP EPA 310.1 Nitrogen, Nitrate a '>' '' 0.11 mg/1 1 05/07/02 Sx EPA 353.2 Nitrogen, Nitrate + Nitrite t1$8;;si 0.10 mg/l 1 05/07/02 Sx EPA 353.2 Nitrogen, Nitrite 0.010 mg/1 1 05/02/02 HBM EPA 354.1 Sulfate 5.0 mg/l 1 05/03/02 op EPA 375.4 Sulfide '. 2.0 mg/1 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOI-MW-1 Lab Sample ID: M24976-4 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13210.1) 1 05/13/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......................... 71-43-2 Benzene j4 > >'> ' ' 5.0 ug/l ........................... 100-41-4 Ethylbenzene 2Q' _` '< ; 5.0 ug/1 ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether 37'' ``<: >5.0 ug/l 91-20-3 Naphthalene » > '»>' 5.0 ug/l ........................... ........................... ........................... 108-88-3 Toluenet8t <' > 5.0 ug/l m,p-Xylened> ;>>::::5.0 ug/1 ........................... ........................... 95-47-6 o-Xylene 2Z9 5.0 ug/1 C5-C8 Aliphatics(Unadj.) i :<: <> : 50 ug/l ........................... ........................... C9-C12 Aliphatics(Unadj.) 1I( <i 50 ug/1 .:......................... ............................ C9-C10 Aromatics(Unadj.) 2 50 ug/1 .... .................. ............................ ........................... C5-C8 Aliphatics I)< ; >>; 50 ug/l .......................... .................-........ ........................... C9-C12 Aliphatics NYC > i ii 50 ug/l CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene $ °do- 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW01-MW-1 Lab Sample ID: M24976-4 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II21143.D 1 05/14/02 ANJ n/a n/a N:GII1034 Run#2 a I121144.1) 5 05/14/02 ANJ n/a n/a N:GH1034 CAS No. Compound Result RL Units Q 74-82-8 Methane I2 ;' ' 0.10 ug/1 Carbon Dioxide 142 S00 ug/1 ......................... (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 (b)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWOI-MW-1 Lab Sample ID: M24976-4 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity,Total bQ > 5.0 mg/l 1 05/10/02 OP EPA 310.1 Nitrogen, Nitrate a 0 1 . 0.11 mg/1 1 05/07/02 sx EPA 353.2 ................................. .................................. ................................. Nitrogen, Nitrate + Nitrite _ >; ; 0.10 mg/l 1 05/07/02 sx EPA 353.2 Nitrogen, Nitrite ()FO t) ' ` 0.010 mg/l 1 05/02/02 HBM EPA 354.1 Sulfate 2 mg/l 1 05/03/02 OP EPA 375.4 Sulfide 2(} < ;;2.0 mg/l 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)-(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02-MW-2 Lab Sample ID: M24976-5 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13215.1) 1 05/13/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene ND 5.0 ug/I 100-414 Ethylbenzene 1 > 5.0 ug/1 1634-044 Methyl Tert Butyl Ether #1 5.0 ug/I 91-20-3 Naphthalene ITT7> << 5.0 ug/I 108-88-3 Toluene ND5.0 ug/I m,p-Xylene 1 >> ' 5.0 ug/I 95-47-6 o-Xylene 1II s 5.0 ug/I C5-C8 Aliphatics(Unadj.) 50 ug/I C9-C12 Aliphatics(Unadj.) 1D 50 ug/l C9-C10 Aromatics(Unadj.) aND 50 ug/I C5-C8 Aliphatics ND ><' <» 50 ug/I C9-C12 Aliphatics Nib:;;:;::::;:::::> 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 1(71% > 70-130% X.:..................... 615-59-8 2,5-Dibromotoluene 18%' ''>< 70-130% .................................................. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M24976-6 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13234.13 50 05/14/02 AMY n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene 1524 >><250 ug/1 ........................... 100-41-4 Ethylbenzene 2d Q 250 ugh 1634-04-4 Methyl Tert Butyl Ether' 250 ug/1 91-20-3 Naphthalene 250 ug/1 :.......................... ................. 108-88-3 Toluene afl4 .. 250 ug/1 m,p-Xylene 71 > > ' ; 250 ug/1 ...:....................... ........................... 95-47-6 o-Xylene 883f1<;' ; 250 ug/1 CS-C8 Aliphatics(Unadj.) 870E 2500 ug/1 .......... ........................... C9- C12 Aliphatics(Unadj.) ` 8(3 ` 25W ug/1 ... C9-C10 Aromatics(Unadj.) 77t 2500 ug/1 .. .................... ........................... C5-C8 Aliphatics N13< ' 2500 ug/l C9- C 12 Aliphatics I 1 ' >` '';` <> 25W ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene <9 ; >< 70-130% ......................... 615-59-8 2,5-Dibromotoluene 99% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M24976-6 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 1121145.1) 1 05/14/02 ANJ n/a n/a N:GI11034 Run#2 a 1121146.1) 5 05/14/02 ANJ n/a n/a N:GII1034 CAS No. Compound Result RL Units Q 74-82-8 Methane 961i''= 0.10 ug/1 Carbon Dioxide 500 ug/1 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 (b)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M24976-6 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. Alkalinity,Total 1Q4>< 5.0 mg/l 1 05/10/02 op EPA 310.1 Nitrogen, Nitrate a 0 1 s 0.11 mg/l 1 05/07/02 SK EPA 353.2 ..............:.................. Nitrogen, Nitrate + Nitrite `0 <; ' 0.10 mg/l 1 05/07/02 SK EPA 353.2 Nitrogen, Nitrite 1t) 0.010 mg/1 1 05/02/02 HBM EPA 354.1 .................................. Sulfate 0 > <> -< 5.0 mg/l 1 05/03/02 op EPA 375.4 Sulfide 2{};; ;; 2.0 mg/1 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite) -(Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW06-MW-6 Lab Sample ID: M24976-7 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA He ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13217.1) 1 05/13/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene $bra'> 5.0 ug/1 ..........:................ 100-414 Ethylbenzene ug/1 1634-044 Methyl Tert Butyl Ether lj (# 5.0 ug/1 91-20-3 Naphthalene > 5.0 ug/1 108-88-3 Toluene ug/1 m,p-Xylene 12 > s> 5.0 ug/1 95-47-6 o-Xylene �t 1> > . >> 5.0 ug/1 C5-C8 Aliphatics(Unadj.) 1 50 ug/l C9-C12 Aliphatics(Unadj.) 2 ` ...........` 50 ug/1 C9-C10 Aromatics(Unadj.) `226 « 50 ug/1 .. . :.................. C5-C8 Aliphatics ug/1 C9-C12 Aliphatics ° '` 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene ] 9:% 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene I ;> 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW09-MW-9 Lab Sample ID: M24976-8 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13235.1) 50 05/14/02 , AMY n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......................... 71-43-2 Benzene I62( s< 250 ug/I 100-41-4 Ethylbenzene 24 > 250 ug/1 ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether $ ( = 250 ug/1 ......:.................... ........................... 91-20-3 Naphthalene 96250 ug/1 ........................... ............................ 108-88-3 Toluene 18Q0> j > ' 250 ug/1 m,p-Xylene '1.. '4 '>s< 250 ug/I 95-47-6 o-Xylene 6flGt ; ;' >250 ug/1 C5-C8 Aliphatics(Unadj.) 5DQ 2500 ug/1 C9-C12 Aliphatics(Unadj.) 39�(Q`< 2500 ug/1 C9-C10 Aromatics (Unadj.) 56 (1 >; '25W ug/1 C5-C8 Aliphatics $ 0';;` ` 2500 ug/1 C9-C12 Aliphatics 33 »>'> ''-»> 2500 g u /1 P .......................... ........................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits ....................... 615-59-8 2,5-Dibromotoluene 9:50 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene )tJ3:%<`ii > 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW09-MW-9 Lab Sample ID: M24976-8 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a II21147.1) 1 05/14/02 ANJ n/a n/a N:GII1034 Run#2 a II21148.1) 5 05/14/02 ANJ n/a n/a N:GII1034 CAS No. Compound Result RL Units Q .................I......... 74-82-8 Methane � 30.10 ug/1 ........................... Carbon Dioxide 439tQbr 500 ug/I (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 (b)Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW09-MW-9 Lab Sample ID: M24976-8 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ............................. Alkalinity, Total $t37 5.0 mg/1 1 05/10/02 op EPA 310.1 Nitrogen, Nitrate a # 's >> 0.11 m /1 1 05/07/02 Sx EPA 353.2 g Nitrogen, Nitrate + Nitrite0 >; 0.10 mg/1 1 05/07/02 Sx EPA 353.2 Nitrogen, Nitrite IQ> 0.010 mg/1 1 05/02/02 HBM EPA 354.1 Sulfate 6tli _ 5.0 mg/l 1 05/03/02 op EPA 375.4 Sulfide ''>` »<<' 2.0 mg/l 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW10-MW-10 Lab Sample ED: M24976-9 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13219.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene ID< 5.0 ug/1 ........................... ........................... ........................... 100-41-4 Ethylbenzene It ><> 5.0 ug/1 ...:....................... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether 1'T� ` < 5.0 ug/1 ........................... ........................... 91-20-3 Naphthalene Nl < «<> s > 5.0 ug/1 108-88-3 Toluene ND ug/1 m,p-Xylene XV > > > ><>> 5.0 ug/1 95-47-6 o-Xylene ND €< < < >> 5.0 ug/1 ........................... ........................... ........................... C5-C8 Aliphatics(Unadj.) N # ' < 50 ug/1 .................... .................... ........................... C9-C12 Aliphatics(Unadj.) NI) i 50 ug/I C9-C10 Aromatics (Unadj.) 1�tI) ;' 50 ug/1 .... . ................. ........................... ........................... C5-C8 Aliphatics P+ID ` 50 ug/1 C9-C 12 Aliphatics NT3''`'< 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $20< <> 70-130% 615-59-8 2,5-Dibromotoluene 9i `"` <' 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MWI I-MW-11 Lab Sample ID: M24976-10 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13220.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene NI) ; i; < 5.0 ug/I 100-41-4 Ethylbenzene D >: 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 1 ::<':> 5.0 ug/I 91-20-3 Naphthalene I1`< 5.0 ug/1 ........................... ........................... 108-88-3 Toluene STD 5.0 ug/1 m,p-Xylene 5.0 ug/1 ........................... ......................-... 95-47-6 o-Xylene D > 5.0 ug/1 C5-C8 Aliphatics (Unadj.) 1 50 ug/1 C9-C12 Aliphatics(Unadj.) )< < >< 50 ug/1 C9-C10 Aromatics(Unadj.) ltiT : : 50 ug/1 C5-C8 Aliphatics ::ND.-.:_ ; >> 50 ug/I C9-C 12 Aliphatics e : >' 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene lfi(}°la >< 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene I:q?%:;' : i 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW12-MW-12 Lab Sample ID: M24976-11 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13221.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene Is ` > 5.0 ug/1 100-41-4 Ethylbenzene 5.0 ug/1 ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether NTH::::;`:::: ::': 5.0 ug/l ........................... ........................... 91-20-3 Naphthalene X,N1 > <> ;< 5.0 ug/1 108-88-3 Toluene ) > > 5.0 ug/1 Nn <«<'>>< 5» 0 ug/1m,p-Xylene < 9547-6 o-Xylene 5.0 ug/1 C5-C8 Aliphatics(Unadj.) 150 ug/1 :.:........................ ........................... C9-C12 Aliphatics(Unadj.) ..... ``' 50 ug/1 .......................... ........................... C9-CIO Aromatics(Unadj.) `' 50 ug/1 ... . ................. ........................... ........................... C5-C8 Aliphatics ND 50 ug/1 C9-C12 Aliphatics I ;<; :> <' 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 82%>>>__ 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene <' <' ` 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M24976-12 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13222.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene hTD> <'< < 5.0 ug/I 100-41-4 Ethylbenzene t5.0 ug/1 ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether s 5.0 ug/1 .....:.:................... ........................... 91-20-3 Naphthalene III ; >5.0 ug/1 ........................... ........................... ........................... 108-88-3 Toluene 1D >> ;> 5.0 ug/I m,P-Xylene 5.0 ug/I , 95-47-6 o-Xylene ;1I ><>><» 5.0 ug/1 C5-C8 Aliphatics(Unadj.) rC...................< 50 ug/l C9-C12 Aliphatics(Unadj.) h1D '< '` 50 ug/1 ................. C9-C10 Aromatics(Unadj.) '<;> 50 ug/1 ............. C5-C8 Aliphatics NI)i 50 ug/1 C9-C12 Aliphatics <NT 50 ug/I ....................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits .......................... 615-59-8 2,5-Dibromotoluene 70-130% 615-59-8 2,5-Dibromotoluene ;IOC:% 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M24976-12 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 1121149.1) 1 05/14/02 ANJ n/a n/a N:GII1034 Run#2 CAS No. Compound Result RL Units Q 74-82-8 Methane 0.10 ug/1 Carbon Dioxide 4$4[ ; ''>"'> 100 ug/1 (a)Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M24976-12 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. Alkalinity,Total $#1' 5.0 mg/l 1 05/10/02 op EPA310.1 Nitrogen, Nitrate a49 0.11 mg/1 1 05/07/02 sK EPA 353.2 Nitrogen, Nitrate + Nitrite 0.10 mg/l 1 05/07/02 SK EPA 353.2 Nitrogen, Nitrite1Q' 0.010 mg/1 1 05/02/02 xBM EPA 354.1 .................................. .........................I.-.... .................................. Sulfate 5 > > 5.0 mg/1 1 05/03/02 op EPA 375.4 Sulfide C2> .. 2.0 mg/1 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) f RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M24976-13 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch . Run#1 MN13223.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71 43-2 Benzene 5.0 ug/1 100414 Ethylbenzene » 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 1T1 € '<> 5.0 ug/1 91-20-3 Naphthalene Imo`< 's ; 5.0 ug/I 108-88-3 Toluene NI3 ; 5.0 ug/1 m,p-Xylene 1iD>> 5.0 ug/1 95-47-6 o-Xylene 1+II1> 5.0 ug/1 C5-C8 Aliphatics (Unadj.) NTJi 50 ug/1 C9-C12 Aliphatics(Unadj.) ND 50 ug/1 C9-C10 Aromatics(Unadj.) 50 ug/1 C5-C8 Aliphatics I+tI)< ''< > 50 ug/I C9-C12 Aliphatics NIA ;> 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene BS ' 70-130% ......:.................. 615-59-8 2,5-Dibromotoluene 9U 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M24976-13 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: SW846 8015 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a 112115O.D 1 05/14/02 ANJ n/a n/a N:GI11034 Run#2 CAS No. Compound Result RL Units Po Q ........................... ........................... 74-82-8 Methane N1 0.10 ug/1 Carbon Dioxide 90( > 100 ug/1 .:..:...::................ (a) Analysis performed by Accutest Laboratories, Dayton, NJ. MA CERT. NJ-141 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M24976-13 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. Alkalinity,Total ... 5.0 mg/l 1 05/10/02 OP EPA 310.1 Nitrogen, Nitrate a ; 0.51 mg/1 1 05/07/02 SK EPA 353.2 ................................. .................................. Nitrogen, Nitrate + Nitrite 15 `': '' '_ 0.50 mg/1 5 05/07/02 SK EPA 353.2 Nitrogen, Nitrite 1€ 0.010 mg/1 1 OS/OZ/02 xB1vt EPA 354.1 ..........................I....... ................................. Sulfate 9 ` ;> > 5.0 mg/1 1 05/03/02 op EPA 375.4 Sulfide 2 ; ;;;;;;;; ;; 2.0 mg/1 1 05/07/02 BF EPA 376.1 (a)Calculated as: (Nitrogen, Nitrate + Nitrite)- (Nitrogen, Nitrite) RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ED: MW14I-MW-14I Lab Sample ID: M24976-14 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GAB543.1) 1 05/03/02 AF n/a n/a GAB15 Run#2 MA-VPH L' CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene lYD5.0 ug/1 100-41-4 Ethylbenzene 1 ' > >> 5.0 ug/1 ........................... 1634-04-4 Methyl Tert Butyl Ether 1'+IT `<><<< 5.0 ug/1 91-20-3 Naphthalene Nl < 5.0 ug/1 ........................... ........................... 108-88-3 Toluene ND «> 5.0 ug/1 m,p-Xylene < > 5.0 ug/1 ........................... ........................... 95-47-6 o-Xylene ND < < 5.0 ug/1 CS-C8 Aliphatics(Unadj.) hTl ; 50 ug/1 ........................... ........................... C9-C12 Aliphatics (Unadj.) 1tIID 50 ug/1 C9-C10 Aromatics(Unadj.) lt ,; 50 ug/1 .... . ................. ........................... C5- C8 Aliphatics III 50 ug/1 C9-C12 Aliphatics 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene $8'% < 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 8i 70-130% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14D-MW-14D Lab Sample ID: M24976-15 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GAB544.1) 1 05/03/02 AF n/a n/a GAB15 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ............-............. 5.0 ug/171-43-2 Benzene ND: ... 100-41-4 Ethylbenzene <> ` >> 5.0 ug/1 ........................... ....................... 1634-04-4 Methyl Tert Butyl EtherI ? 5.0 ug/1 91-20-3 Naphthalene NY?` i5.0 ug/1 :.......................... ..............I.......-... 108-88-3 Toluene IUD;::;:::;::::::;::::: 5.0 ug/1 m,p-Xylene 1ti1D >`< > 5.0 ug/1 ..:........................ ........................ 95-47-6 o-Xylene N1? 5.0 ug/1 C5-C8 Aliphatics(Unadj.) T7 > ;<< 50 ug/1 ..: .................... ........................... ........................... C9-C12 Aliphatics(Unadj.) ll) i':.':.<`: 50 ug/l ........:.................. ........................... C9-C10 Aromatics(Unadj.) . ` '< < 50 ug/I ............. ........................... ........................... C5-C8 Aliphatics ND.:::...::::;::;;;::;;::::::50 ug/1 C9-C12 Aliphatics NI); >< >; 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene S�Jos>><< 70-130% 615-59-8 2,5-Dibromotoluene3%% ' '< 70-130% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW15-MW-15 Lab Sample ID: M24976-16 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA He ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13224.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene I) 5.0 ug/I 100-41-4 Ethylbenzene lt '' ' 5.0 ug/I 1634-04-4 Methyl Tert Butyl Ether < 5.0 ug/I 91-20-3 Naphthalene I13 > < 5.0 ug/I ........................... ........................... ................ 108-88-3 Toluene NDs 5.0 ug/I m,p-Xylene1 >' ' 5.0 ug/I ........................... ........................... ............... 95-47-6 o-Xylene I+T) 5.0 ug/I C5-C8 Aliphatics(Unadj.) hT1 `'' >' 50 ug/l ... .................... ........................... ........................... C9-C 12 Aliphatics(Unadj.) ) ; 50 ug/I ........ ................. ........................... C9-C10 Aromatics(Unadj.) l 50 ug/I .......................... ........................... ........................... C5-C8 Aliphatics NT�i< >_ : 50 ug/I I C9-C12 Aliphatics 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene ')I' 70-130% 615-59-8 2,5-Dibromotoluene $ vii;ii <' ' 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW16-MW-16 Lab Sample ID: M24976-17 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File 11) DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13225.1) 1 05/14/02 AMY n/a n/a GMN372 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene 5.0 ug/l ....................... 100-41-4 Ethylbenzene ug/l 1634 04 4 Methyl Tert Butyl Ether ug/l 91-20-3 Naphthalene NT3......................... 5.0 ug/l ........................... ................... 108-88-3 Toluene 5.0 ug/l ............... N ............. J.V m,p-Xylene ...........* ug/l ...........%............................-..... 9547-6 o-Xylene 5.0 ug/I C5-C8 Aliphatics(Unadj.) ........ ug/l ............... C9-C12 Aliphatics(Unadj.) IUD;;:;::;::;:::':::;::::;::: . 50 ug/l C9-CIO Aromatics(Unadj.) 11 50 ug/l ................. .............................. ..... ............ ... C5-C8 Aliphatics .... ug/l .............X,. :X:-..... ....C9-C12 Aliphatics Du ug/l ..................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits ............ 615-59-8 2,5-Dibromotoluene 83*&.: . . ............ 70-130% .......... . .............. w: .......615-59-8 2,5-Dibromotoluene 15 . 70-130% % ........ ......... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample II): MW16D-MW-161) Lab Sample ID: M24976-18 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13232.1) 1 05/14/02 AMY n/a n/a GMN373 Run#2 QR14492.1) 5 05/15/02 AA n/a n/a GQR663 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 BenzenetI4 ; 5.0 ug/1 100-41-4 Ethylbenzenet 5.0 ug/1 .......:................... ............................ ........................... 1634-04-4 Methyl Tert Butyl Ether2g' > ':25 ug/1 91-20-3 Naphthalene Nl< 5.0 ug/1 ........................... ........................... ........................... 108-88-3 Toluene AID:`:........:::::;::;;; 5.0 ug/1 ........................... ...................I....... m,p-Xylene AID>>> >> > 5.0 ug/I ........................... 95-47-6 o-Xylene T > '< <` 5.0 ug/1 C5-C8 Aliphatics(Unadj.) 3$C1< » 250 ug/1 C9-C12 Aliphatics(Unadj.) 1 : > <ii 50 ug/1 C9-C10 Aromatics(Unadj.) 1 '`< ' 50 ug/1 C5-C8 Aliphatics I+I 50 ug/1 C9-C12 Aliphatics ND ; ' `' 50 ug/1 ..:::::.................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... ......................... 615-59-8 2,5-Dibromotoluene 83d�o>> lf) °f ' ' 70-130% :........................ ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene g$ <> > ` '12%a' ><';` 70-130% _....... ........................ ......................... (a) Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample 111): MW17-MW-17 Lab Sample IUD: M24976-19 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File El) DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13233.1) 1 05/14/02 AMY n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL units Q 7143-2 Benzene 5.0 ug/I 100-41-4 Ethylbenzene ug/1 1634-044 Methyl Tert Butyl Ether 5.0 ug/I ............................ ..................... 91-20-3 Naphthalene .. 5.0 ug/I 108-88-3 Toluene 5.0 ug/I ........................ m,p-Xylene 5.0 ug/I ........... ..........-.............................. .. ... ... 95-47-6 o-Xylene ... . Z).0 ug/1 ... ................................. ,:. . rn C5-C8 Aliphatics(Unadj.) ug/l C9-C12 Aliphatics (Unadj.) ug/l .......... ........... C9-CIO Aromatics(Unadj.) P ug/l X .-.................................................. C5-C8 Aliphatics ...ND . av ug/l .......... ...... .......... ..................... C9-C12 Aliphatics JU ug/1 .................. CAS No. Surrogate Recoveries Run#I Run#2 Limits 615-59-8 2,5-Dibromotoluene 70-130% .... ............. 70-130% 615-59-8 2,5-Dibromotoluene Oa. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW18S-MW-18S Lab Sample ID: M24976-20 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13229.1) 1 05/14/02 AMY n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene I1I) 5.0 ug/1 100-41-4 Ethylbenzene 1 s' < 5.0 ug/1 ........................... ........................... ...............I...... ..... 1634-04-4 Methyl Tert Butyl Ether 2&8 ;> <5.0 ug/1 91-20-3 Naphthalene IY <` ' 5.0 ug/1 ........................... ........................... ........................... 108-88-3 Toluene NI) ii5.0 ug/1 m,p-Xylenet > >> 5.0 ug/1 ........................... ........................... 95-47-6 o-Xylene I1 . 5.0 ug/1 C5-C8 Aliphatics(Unadj.) 5 '9<<>><<» 50 ug/I .. ................... ............................ C9-C12 Aliphatics(Unadj.) I ` > ug/I ........ ................. ........................... C9-C10 Aromatics(Unadj.) 1TD' >; 50 ug/1 ........ ............. ........................... .........................- C5-C8 Aliphatics Nk < '` 50 ug/1 NTH C9-C12 Aliphatics 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 931 < > 70-130% :.:...................... 615-59-8 2,5-Dibromotoluene 9l3 '« <" 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of i Client Sample II): MW18D-MW-18D Lab Sample II): M24976-21 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GAB542.1) 1 05/03/02 AF n/a n/a GAB15 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2. Benzene 1D><<< ; ; 5.0 ug/1 10041-4 Ethylbenzene Nn` = < 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 1+I1) 5.0 ug/1 91-20-3 Naphthalene NIA:» ` >> 5.0 ug/1 108-88-3 Toluene Imo: >: ' 5.0 ug/1 m,p-Xylene >> 5.0 ug/l 95-47-6 o-Xylene NI < '' >`` 5.0 ug/1 C5-C8 Aliphatics(Unadj.) NYI` : <_` 50 ug/1 C9-C12 Aliphatics(Unadj.) 1VD's 50 ug/1 ............-............ C9-C10 Aromatics(Unadj.) tns ; >;i 50 ug/1 .. ............. ........................... C5-C8 Aliphatics NP 50 ug/1 C9-C12 Aliphatics --N. <'<`' 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 93 70 130% ......................... 615-59-8 2,5-Dibromotoluene 92F 70-130% .......................:. ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ' l Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FB-FB Lab Sample ID: M24976-22 Date Sampled: 05/01/02 Matrix: AQ- Field Blank Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 MN13250.1) 1 05/15/02 AMY n/a n/a GMN373 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ...... ............ 5.0D ug/171-43-2 Benzene N 100-414 Ethylbenzene It5.0 ug/1 ........................... ............................ 1634-04-4 Methyl Tert Butyl Ether >' > 5.0 ug/1 D91-20-3 Naphthalene 5.0 ug/I 108-88-3 Toluene 1`II) ; < 5.0 ug/1 m,p-Xylene ND > > >«5.0 ug/1 95-47-6 o-Xylene 5.0 ug/1 C5-C8 Aliphatics(Unadj.) NI3 50 ug/1 .............. .......... C9-C12 Aliphatics(Unadj.) ND ;>;> 50 ug/1 C9-C10 Aromatics(Unadj.) N 50 ug/1 C5-C8 Aliphatics iND 50 ug/1 C9-C12 Aliphatics ND <'><> ' 50 ug/1 ..:::..::............. CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 81;%' >>'>> 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene <>> 70-130% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TB-TB Lab Sample ID: M24976-23 Date Sampled: 05/01/02 Matrix: AQ-Trip Blank Water Date Received: 05/02/02 Method: MADEP VPH 98-1 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GAB684.1) 1 05/10/02 AF n/a n/a GAB20 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene 1"13>i>' ' 5.0 ug/1 100-41-4 Ethylbenzene at _ < < <> 5.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 1'J ; >'` `><5.0 ug/1 91-20-3 Naphthalene IT 5.0 ug/1 108-88-3 Toluene ND0 ug/1 m,p-Xylene <> > 5.0 ug/1 95-47-6 o-XyleneJ „ ug/1 C5- C8 Aliphatics(Unadj.) I ` 'i' i 50 ug/1 C9-C12 Aliphatics(Unadj.) ND = 50 ug/1 C9- C10 Aromatics(Unadj.) `' ><< ' 50 ug/1 C5-C8 Aliphatics NI1 ;` ;< 50 ug/1 C9-C12 Aliphatics NI?> i`>< 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene .............91% 70-130% 615-59-8 2,5-Dibromotoluene2 ;; 70-130% ......................... I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound E Accutest Laboratories Report of Analysis. Page 1 of 1 Client Sample ID: TMP119(78-80') Lab Sample ID: M24976-24 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method ................................. .................................. pH (s9' su 1 05/02/02 sAP EPA 15o.1 it RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TMP119(102-104') Lab Sample ID: M24976-25 Date Sampled: 05/01/02 Matrix: AQ-Ground Water Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA General Chemistry Analyte Result RL Units DF Analyzed By Method PH su 1 05/02/02 SAP EPA 150.1 RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW02A-MW-2A Lab Sample ID: M24976-2A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... IIOII .... ........ 100 ug/1 1 05/08/02 05/10/02 LMN SW846 6010B SW846 3010A RL = Reporting Limit eP g Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW03A-MW-3A Lab Sample ID: M24976-3A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ...................................................... Iron 100 ug/I 1 05/08/02 05/10/02 LmN SW846 6010B Sw846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of i Client Sample ID: MWOI-MW-I Lab Sample ID: M24976-4A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ................:.......... ........................... Iron 1, 100 ug/I 1 05/08/02 05/10/02 LMN SW846 6010E SW846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW05-MW-5 Lab Sample ID: M24976-6A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ...................... ........................... Iron :i5,150 100 ug/I 1 05/08/02 05/10/02 LMx SW846 6010B Sw846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW09-MW-9 Lab Sample ID: M24976-8A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Iron 3 #10 _ 100 ug/1 1 05/08/02 05/10/02 LMN SW846 6010B SW846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW13-MW-13 Lab Sample ID: M24976-12A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... ........................... Iron ....T( .. 100 ug/1 1 05/08/02 05/10/02 LMN sw846 601oB sw846 3010A RL = Reporting Limit Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW14-MW-14 Lab Sample ID: M24976-13A Date Sampled: 05/01/02 Matrix: AQ-Groundwater Filtered Date Received: 05/02/02 Percent Solids: n/a Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method ........................... Iron 100 u9/1 1 05/08/02 05/10/02 LMN SW846 6010B SW846 3010A RL = Reporting Limit MADEP VPH FORM A ueous W Soil R Sediment Other Satisfacto Broken Leakina El N/A H<=2 H>2 Received on Ice F1 Received at 4 Den.C F1 Other W Reed at 3 deg C NIA Method for Ranges: MADEP VPH 98-1 Client ID: MW01A-MW-IA Lab ID: M24976-1 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5112/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ran es CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 ar et Anal es Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ugn ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/l ND 5 m,p-Xylene C9-C12 ug/I ND 5 d usted Ran es C5-C8 Aliphatics N/A ug/1 ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 urro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 85 70-130% PID:2,5-Dibromotoluene % 89 70-130% 0o notes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range. CS-CS Allphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cons of Target Analytes eluting In that range AND concentration of C9470 Aromatic Hydrocarbons. A'J'qualtiler indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No.Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? WNo ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for taining the information,the material contained In this report Is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous Soil F1 Sediment F1 Other SatisfactorvW Broken F1 Leakin N/A F1 DH<=2 W DH>2 Received on Ice F1 Received at 4 Deg. C Other W Rec'd at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW02A-MW-2A Lab ID: M24976-2 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 512/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12102 05/13/02 FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 2 Unadlusted Ran es CAS# Elution Ranae Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I 2770 A 100 C9-C10 Aromatics(Unadj.) N/A ug/I 82.5 A 50 C9-C12 Aliphatics(Unadj.) N/A ugA 116 A 50 Target Anal Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 2700 10 Ethyibenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ug/1 ND 5 Benzene 71-43-2 C5-C8 ugA 122 5 Naphthalene 91-20-3 N/A ug/I 11.3 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ug/1 11 5 Ad lusted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 99 70-130% PID:2,5-Dibromotoluene % 108 70-130% FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 81 70-130% Footnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CS-CO Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9C70 Aromatic Hydrocarbons. A'X qualifler Indicates an estimated value Were all CA/QC procedures REQUIRED by the VPH Method followed? RJYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? BYes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? VNo ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals Immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous W Soil F1 Sediment Other SatisfactoryWI Broken n Leaking N/A F1 PH <=2 H>2 Received on Ice Received at 4 Deg.C Other Rec'd at 3 deg C N/A ethod for Ranges: MADEP VPH 98-1 Client ID: MW03A-MW-3A Lab ID: M24976-3 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Rum PID: 2,5-Dibromotoluene N/A 5112/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 ar et Anal es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ugA ND 5 d usted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ugA ND` 50 urro ate Recoveries Acceotance Range FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 84 70-130% ootn tes Hydrocarbon Range data exclude concentrations of any surtogate(s)andfor internal standards eluting in that range Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range. CS-08 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. AV qualifier Indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for taining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5/17102 MADEP VPH FORM Aqueous Soil n Sediment F1 Other SatisfactoryW Broken F1 Leakin N/A H<=2 W pH>2 Received on Ice Received at 4 Deg. C F1 Other W Rec!d at 3 deg C MEN/A Method for Ranges: MADEP VPH 98-1 Client ID: MW01-MW-I Lab ID: M24976-4 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1102 Date Received: 5/2/02 VPH Surrogate Standards . Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/02 WA FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unad usted Ran es CAS# Elution Ranae Units Re ul RDL f3 C5-C8 Aliphatics(Unadj.) N/A ug/I 725 A 50 C9-C10 Aromatics(Unadj.) N/A ugA 90.2 A 50 C9-C12 Aliphatics(Unadj.) N/A ugA 196 A 50 ar et Analytes Ethylbenzene 100-41-4 C9-C12 ug/I 22 5 Toluene 108-88-3 C5-C8 ugA 48 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 637 5 Benzene 71-43-2 C5-C8 ugA 14.2 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ug/I 22.9 5 m,p-Xylene C9-C12 ugA 44.6 5 Ad us ed Ran es C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ug/l ND° 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 87 7 0 0-130 /e PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Anayies eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. A'X qualiner indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No.Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? RlYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ONo ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous Soil F1 Sediment n Other SatisfactorvW Broken F1 Leaking N/A F1 pH<=2 91 PH>2 Received on Ice F1 Received at 4 Deg.C n Other W Rec'd at 3 deg C N/A ethod for Ranges: MADEP VPH 98-1 Client ID: MW02-MW-2 Lab ID: M24976-5 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1102 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ran es CAS# Elution Range Units Resul RDL 2 C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 ar et Anal es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 20.4 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-17-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ug/I ND 5 d usted Ran es C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ug/l ND c 50 urro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 101 70-130% PID:2,5-Dibromotoluene % 108 70-130% ootnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-CS Aliphatic Hydrocarbons exclude Ow concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or irdemai standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of MOO Aromatic Hydrocarbons. A V quallfler indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? Dyes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my Inquiry of those Individuals Immediately responsible for btaining the Information,the material contained in this report is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous V Soil F1 Sediment F1 Other SatisfactorvW Broken n Leakin N/A F1 PH <=2 H>2 Received on Ice Received at 4 De- . C F1 Other V Rec!d at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW05-MW-5 Lab ID: M24976-6 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 50 N/A Unad usted Ranges CAS# Elution Range Units Resul RDA f� C5-C8 Aliphatics(Unadj.) N/A ug/l 48700 A 2500 C9-C10 Aromatics(Unadj.) N/A ug/I 7730 A 2500 C9-C12 Aliphatics(Unadj.) N/A ug/1 22800 A 2500 Tar et Anal es Ethylbenzene 100-41-4 C9-C12 ug/I 2000 250 Toluene 108-88-3 C5-C8 ug/I 10400 250 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 36000 250 Benzene 71-43-2 C5-C8 ug/I 1520 250 Naphthalene 91-20-3 NIA ug/I 540 250 o-Xylene 95-47-6 C9-C12 ugfl 3830 250 m,p-Xylene C9-C12 ug/I 7710 250 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 2500 C9-C12 Aiiphatics N/A ug/I ND c 2500 Surro ate Recoveries Acceotance Range FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % .99 70-130% Footnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of arty surrogates)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those Individuals Immediately responsible for obtaining the Information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17102 MADEP VPH FORM Aqueous Soil El Sediment F1 Other SatisfactorvW Broken D Leakin INS NIA F1 PH<=2 W PH>2 Received on Ice F1 Received at 4 Den.C Other W Redd at 3 deg C NIA dlethod for Ranges: MADEP VPH 98-1 Client ID: MW06-MW-6 Lab ID: M24976-7 diethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 /PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/02 N/A FID: 2,5-Dibromotoluene %.Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ranaes CAS# Elution Ranoe Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ugA 1110" 50 C9-C10 Aromatics(Unadj.) N/A ugA 226 A 50 C9-C12 Aliphatics(Unadj.) N/A ugA 279 A 50 .arnet Analytes Ethylbenzene 100-41-4 C9-C12 ugA 8.3 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 1170 5 Benzene 71-43-2 C5-C8 ugA 51.4 5 Naphthalene 91-20-3 N/A ugA 33.7 5 o-Xylene 95-47-6 C9-C12 ugA 6.1 5 m,p-Xylene C9-C12 ugA 12.2 5 dusted Ran es C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 urro ate Recoveries Acceptance Ranne FID:2,5-Dibromotoluene % 109 70-130% PID:2,5-Dibromotoluene % 112 70-130% ootnotes Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or internal standards eluting In that range Hydrocarbon Range data exclude concentratlons of any surrogate(s)and/or Internal standards eluting In that range. CS C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Intemal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. A'J'qualifier Indicates an estimated value Ifere all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No.Details Attatched /ere all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No.Details Attatched /ere any significant modifications made to the VPH method,as specified in Sect.11.3? WNo ❑ Yes.Details Attatched ttest under the pains and penalties of perjury that,based upon my inquiry of those individuals Immediately responsible for twining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5117/02 MADEP VPH FORM A ueous Soil F1 Sediment n Other SatisfactorvW Broken F1 Leakin N/A n pH<=2 W PH>2 Received on Ice F1 Received at 4 Deg. C n Other qj Rec'd at 3 deg C Jilin N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW09-MW-9 Lab ID: M24976-8 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 50 N/A U ad u ted Ranges CAS# Elution Ranae Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ugA 33500 A 2500 C9-C10 Aromatics(Unadj.) N/A ugA 15600 A 2500 C9-C12 Aliphatics(Unadj.) N/A ugA 39500 A 2500 Target Analytes Ethylbenzene 100-41-4 C9-C12 ugA 2950 250 Toluene 108-88-3 C5-C8 ugA 16800 250 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 6880 250 Benzene 71-43-2 C5-C8 ug/I 1620 250 Naphthalene 91-20-3 N/A ug/I 968 250 o-Xylene 95-47-6 C9-C12 ugA 6060 250 m,p-Xylene C9-C12 ug/I 11700 250 Ad usted Ran es C5-C8 Aliphatics N/A ug/I 81908 2500 C9-C12 Aliphatics N/A ugA 3230 c 2500 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 95 70-130% PID:2,5-Dibromotoluene % 103 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arty surrogates)and/or Internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any sunogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9410 Aromatic Hydrocarbons. A 7 qualltier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ®Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched i attest under the pains and penalties of penury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report Is,to the best of my knowledge and belief,accurate and complete. Signature --�� Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous W Soil n Sediment El Other SatisfactoryM Broken n Leaking N/A n PH<=2 W DH>2 Received on Ice F1 Received at 4 Den. C D Other Wi Reed at 3 deg C N/A fiethod for Ranges: MADEP VPH 98-1 Client ID: MW 10-MW-10 Lab ID: M24976-9 flethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 512102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ran es CAS# Elution Range Units Result RDA g C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 ar et Anal es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ug/l ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ugA ND 5 dusted Ran es C5-C8 Aliphatics N/A ugA ND` 50 C9-C12 Aliphatics N/A ugA ND° 50 urro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 91 70-130% o tno es Hydrocarbon mange data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.CS-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. AV qualifier Indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? OYes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for taining the information,the material contained in this report Is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director Date 5/17/02 rinted Name Reza Tand MADEP VPH FORM A ueous P1 Soil Sediment F1 Other SatisfactorvW Broken F1 Leakin N/A F1 DH<=2 V PH>2 Received on Ice F1 Received at 4 Deg. C El Other 91 Rec'd at 3 deg C MON/A Method for Ranges: MADEP VPH 98-1 Client ID: MW11-MW-11 Lab ID: M24976-10 Method for Target Analytes• MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadlusled Ranges CAS# Elution Ranae Units Resul RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I 92.2 A 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/l ND" 50 Tar net Anal es Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 102 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ugA ND 5 Ad usted Ranues C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ug/l ND` 50 Surro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 100 70-130% PID:2,5-Dibromotoluene % 107 70-130% Footnotes Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogatels)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. A'J'qua Mer Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 66Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified In Sect.11.3? ©No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals Immediately responsible for obtaining the Information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17102 MADEP VPH FORM Aqueous W Soil Sediment n Other FI SatisfactoryW Broken n Leaking- N/A F1 PH<=2 W PH>2 Received on Ice Received at 4 Deg.C Other W Redd at 3 deg C -O- N N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW 12-MW-12 Lab ID: M24976-11 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 512102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A ad usted Ran es CAS# Elution Ranae Units Resul RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadi.) N/A ug/I ND" 50 ar et Analytes, Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/I ND 5 d usted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND° 50 urro ate Recoveries Acceutance Ranae FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 86 70-130% 0o notes Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting in that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CIO.=aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9C10 Aromatic Hydrocarbons. A'Y qualifier Indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? WNo ❑ Yes-Details Attatched hest under the pains and penalties of perjury that,based upon my inquiry of those individuals Immediately responsible for taining the information,the material contained in this report Is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director Date 5/17/02 rinted Name Reza Tand MADEP VPH FORM A ueous Soil F1 Sediment n Other SatisfactoryWI Broken Leaking- N/A F1 DH<=2 W pH>2 Received on Ice Received at 4 De- . C F1 Other tI Redd at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW 13-MW-13 Lab ID: M24976-12 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1102 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 NIA Unad usted Ran es CAS# Elution Range Units Result RDL (� C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Taroet Analytes Ethylbenzene 100-414 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 7143-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 9547-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ug/I ND 5 Ad lusted Ran es C5-C8 Aliphatics N/A ug/l ND a 50 C9-C12 Aliphatics NIA ug/l ND° 50 Surrogate Recoveries Acceatance Range FID:2,5-Dibromotoluene % 100 70-130% PID:2,5-Dibromotoluene %, 108 70-130% Footnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. CS-C9 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 66Yes ❑ No.Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 66Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified In Sect.11.3? VNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for obtaining the Information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature _ Postition Laboratory Director Printed Name Reza Tand Date 5/17102 MADEP VPH FORM NOA ueous W Soil Sediment Other Satisfacto Broken Leakin N/A H<=2 H>2 El Received on Ice F1 Received at 4 De a. C F1 Other W Rec'd at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW 14-MW-14 Lab ID: M24976-13 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run' PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %.Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ran gs CAS# Elution Ranoe Units Result RDL f3 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/l ND" 50 ar et Analvtes Ethylbenzene 100-414 C9-C12 ug/l ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 5 Benzene 71-43-2 C5-C8 ug/l ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/l ND 5 d usted Ran es C5-C8 Aliphatics N/A ug/l ND B 50 C9-C12 Aliphatics N/A ug/I ND` 50 urn ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 85 70-130% PID:2,5-Dibromotoluene % 90 70-130% ootnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting in that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. 09-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. AV qualffier Indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? RIND ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my Inquiry of those individuals Immediately responsible for taining the Information,the material contained In this report Is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director Tinted Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous W Soil n Sediment Other SatisfactorvW Broken n Leakin Big N/A n DH<=2 W PH>2 Received on Ice Received at 4 Den. C Other W Rec'd at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW141-MW-141 Lab ID: M24976-14 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/3/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unad usted Ranges CAS# Elution Ranae Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/l ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 ar et Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ugll ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/I ND 5 Ad lusted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/1 ND c 50 Surro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 88 70-130% PID:2,5-Dibromotoluene % 86 70-130% Footnotes Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C8C10 Aromatic Hydrocarbons. A'J'qualHler Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? FV]No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those Individuals immediately responsible for obtaining the information,the material contained in this report Is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 f MADEP VPH FORM iN A ueous Soil n Sediment El Other Satisfacto Broken Leakin NIA H<=2 H>2 Received on Ice F1 Received at 4 Den.C F1 Other W Read at 3 deg C NIA ethod for Ranges: MADEP VPH 98-1 Client ID: MW14D-MW-14D Lab ID: M24976-15 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 511/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/3102 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ran es CAS# Elution Ranae Units Result RDL 9 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 ar et Analvtes Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 5 Benzene 71-43-2 C5-C8 ug/l ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/l ND 5 d usted Ran es C5-C8 Aliphatics N/A ug/l ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 rro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 95 70-130% PID:2,5-Dibromotoluene % 93 70-130% otnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentations of any surrogate(s)and/or internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of army surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cons of Target Analytes eluting In that range AND concentration of MOO Aromatic Hydrocarbons. A V qualifier Indicates an estimated value re all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched re all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No.Details Attatched re any significant modifications made to the VPH method,as specified in Sect.11.3? WNo ❑ Yes-Details Attatched est under the pains and penalties of perjury that,based upon my inquiry of those individuals Immediately responsible for Ining the information,the material contained In this report is,to the best of my knowledge and belief,accurate and plete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous Soil F1 Sediment F1 Other Satisfacto Broken M Leakin NIA H<=2 W PH >2 Received on Ice Received at 4 Deg. C F1 Other 91 Rec'd at 3 deg C ENN/A Method for Ranges: MADEP VPH 98-1 Client ID: MW15-MW-15 Lab ID: M24976-16 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution- High Dilution: N/A 1 N/A Unad us ed Ran es CAS# Elution Range Units Resul RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND x 50 Tarnet Anal es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 Ug/I ND 5 Benzene 71-43-2 C5-C8 ug/l ND 5 Naphthalene 91-20-3 N/A ug/1 ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ug/I ND 5 Ad usted Ran es C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ugA ND c 50 Surro ate Recoveries Acceotance Range FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 83 70-130% Footnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CS-C9 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-CID Aromatic Hydrocarbons. AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals Immediately responsible for obtaining the information,the material contained in this report Is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM Aqueous Soil Sediment F1 Other SatisfactoryW Broken F1 Leaking N/A F1 PH <=2 W PH>2 Received on Ice F1 Received at 4 Deg.C F1 Other W Rec'd at 3 deg C NIA ethod for Ranges: MADEP VPH 98-1 Client ID: MW16-MW-16 Lab ID: M24976-17 Mlethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 512/02 'PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ranges CAS# Elution Ranae Units Resul RDL (3 C5-C8 Aliphabcs(Unadj.) N/A ug/l ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 ar et Analytes Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ug/l ND 5 m,p-Xylene C9-C12 ug/I ND 5 d usted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 urro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 83 70-130% PID:2,5-Dibromotoluene % 85 70-130% ootnotes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range.C9C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. AV qualifier Indicates an estimated value ,ere all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No.Details Attatched ,ere all performance/acceptance standards for required GA/QC procedures achieved? ©Yes ❑ No-Details Attatched ,ere any significant modifications made to the VPH method,as specified In Sect.11.3? ONo ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those Individuals immediately responsible for taining the information,the material contained In this report Is,to the best of my knowledge and belief,accurate and mplete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous Soil Sediment Other Satisfacto Broken Leakin N/A F1 PH<=2 H >2 Received on Ice F1 Received at 4 Deg. C Other W Redd at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW 16D-MW-16D Lab ID: M24976-18 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5114/02 05/15/02 FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 5 Unad usted Ran es CAS# Elution Range Units Resul RD (3 C5-C8 Aliphatics(Unadj.) N/A ugA 4380 A 250 C9-C10 Aromatics(Unadj.) N/A ugA 122 A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 149 A 50 Taroet Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 4280 25 Ethylbenzene 100,41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Benzene 7143-2 C5-C8 ug/I 414 5 Naphthalene 91-20-3 N/A ug/1 ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ugA ND 5 Ad usted Ran es C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceotance Range FID:2,5-Dibromotoluene % 107 70-130% PID:2,5-Dibromotoluene % 122 70-130% FID:2,5-Dibromotoluene % 83 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnote A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. A'X qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals immediately responsible for obtaining the Information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM Aqueous Soil Sediment Other atisfacto Broken Leakin N/A H<=2 H>2 eceived on Ice F1 Received at 4 Deg. C Other P1 Reed at 3 deg C N/A llethod for Ranges: MADEP VPH 98-1 Client ID: MW17-MW-17 Lab ID: M24976-19 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 511/02 Date Received: 5/2102 'PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 WA FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Inadlusted Ranges CAS# Elution Range Units Result RDA (3 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 'arnet Analytes Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ugA ND 5 adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ugA ND° 50 luronate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 94 70-130% PID:2,5-Dibromotoluene % 100 70-130% =oo notes Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or Irdemal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Ana"eluting In that range AND concentration of C9,C10 Aromatic Hydrocarbons. A W qualifier Indicates an estimated value ilere all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Jere all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Jere any significant!modifications made to the VPH method,as specified in Sect.11.3? 0No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for btaining the information,the material contained In this report Is,to the best of my knowledge and belief,accurate and omplete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17102 MADEP VPH FORM Aqueous Soil D Sediment M Other Satisfactory Broken M Leakin NIA PH <=2 PH>2 Received on Ice Received at 4 Den. C F1 Other W Reed at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: MW18S-MW-18S Lab ID: M24976-20 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unad usted Ranges ( CAS# Elution Ranae Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 51.9" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Tar et Ana es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ugA ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 26.8 5 Benzene 71-43-2 C5-C8 ug/l ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/l ND 5 m,p-Xylene C9-C12 ug/I ND 5 Ad us ed Ran es C5-C8 Aliphatics N/A ug/I ND s 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surro ate Recoveries Acceptance Ranae FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % 98 70-130% Footnotes Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or internal standards eluting In that range S Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9412 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9410 Aromatic Hydrocarbons. A'X qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 66Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? BNo ❑' Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those Individuals Immediately responsible for obtaining the Information,the material contained In this report Is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/17102 MADEP VPH FORM Actueous W Soil F1 Sediment n Other SatisfactoryPI Broken F1 Leakin NIA F1 PH<=2 W PH>2 Received on Ice F1 Received at 4 Deg. C 0 Other W Rec'd at 3 deg C N/A ethod for Ranges: MADEP VPH 98-1 Client ID: MW18D-MW-18D Lab ID: M24976-21 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 511/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 513/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Lad usted Ranges CAS# Elution Ranne Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ug/l ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/l ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/l ND" 50 ar et Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 5 Benzene 71-43-2 C5-C8 ug/l ND 5 Naphthalene 91-20-3 N/A ug/l ND 5 o-Xylene 95-47-6 C9-C12 ug/l ND 5 Im,p-Xylene C9-C12 ug/l ND 5 dlusted Ran es C5-C8 Aliphatics N/A ug/l ND a 50 C9-C12 Aliphatics N/A ug/l ND° 50 urro ate Recoveries Acceptance Ranoe FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % 92 70-130% ootnotes Hydrocarbon Range data exclude concentrations of any surrogates)ardfor internal standards eluting In that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. A'X qualifler Indicates an estimated value ere all QA/QC procedures REQUIRED by the VPH Method followed? ❑d Yes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No.Details Attatched ere any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my Inquiry of those individuals Immediately responsible for taining the Information,the material contained in this report Is,to the best of my knowledge and belief,accurate and mpiete. Signature _ Postition Laboratory Director rinted Name Reza Tand Date 5/17102 MADEP VPH FORM INKA ueous Soil F1 Sediment F1 Other SatisfactorvW Broken F1 Leakin N/A F1 PH<=2 H>2 Received on Ice Received at 4 Don. C Other Rec'd at 3 deg C N/A Method for Ranges: MADEP VPH 98-1 Client ID: FB-FB Lab ID: M24976-22 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2102 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/15/02 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unad usted Ran es CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/1 ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ug/I ND 5 Naphthalene 91-20-3 N/A ug/I ND 5 o-Xylene 95-47-6 C9-C12 ug/I ND 5 m,p-Xylene C9-C12 ug/I ND 5 Adiusted Ranges C5-C8 Aliphatics N/A ug/l ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 89 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of arty surrogates)andfor httemal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C5-C9 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9410 Aromatic Hydrocarbons. Z A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? RiYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? VNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my Inquiry of those individuals Immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature f�--� Postition Laboratory Director Printed Name Reza Tand Date 5/17/02 MADEP VPH FORM A ueous Soil n Sediment F1 Other SatisfactorvW Broken n Leakin N/A M PH<=2 W PH>2 Received on Ice M Received at 4 De a.C F1 Other W Reed at 3 deg C N/A ethod for Ranges: MADEP VPH 98-1 Client ID: TB-TB Lab ID: M24976-23 ethod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/1/02 Date Received: 5/2/02 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/10102 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A nad usted Ran es CAS# Elution Range Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 ar et Anal es Ethylbenzene 100-41-4 C9-C12 ugA ND 5 Toluene 108-88-3 C5-C8 ug/I ND 5 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 5 Benzene 71-43-2 C5-C8 ugA ND 5 Naphthalene 91-20-3 N/A ugA ND 5 o-Xylene 95-47-6 C9-C12 ugA ND 5 m,p-Xylene C9-C12 ugA ND 5 dusted Ran es C5-C8 Aliphatics N/A ugA ND a 50 C9-C12 Aliphatics N/A ug/l ND` 50 urro ate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 92 70-130% ootno e Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentrations of airy surrogate(s)and/or Internal standards eluting In that range. CS-C9 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9.C10 Aromatic Hydrocarbons. AV qualifier indicates an estimated value I ere all QA/QC procedures REQUIRED by the VPH Method followed? BYes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched ere any significant modifications made to the VPH method,as specified in Sect 11.3? WNo ❑ Yes-Details Attatched ttest under the pains and penalties of perjury that,based upon my Inquiry of those Individuals Immediately responsible for taining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and mpiete. Signature Postition Laboratory Director rinted Name Reza Tand Date 5/17/02 ,l p L ®ACCUTEST 495 TECHNOLOGY CENTER WEST • BUILDING ONE /�V MARLBOROUGH,MA 01752 ACCUTEST QUOTE#: TEL:508-481-6200 • FAX:508-481-7753 CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES 1.�� -� 1�c oog a {>,C DW- DRINKING � WATER NAME A PROJECT NAME `` GW- GROUND C I�I� �.G�/1L API d 1 Jai S - WATER A RESS . l CATION I WW- WASTE sow dV1 l� OI'��I avWQ, AC� cc So G WATER SO- SOIL CITY ` \ STATE ZIP PR ECT NO. SL- SLUDGE (��Q_c1-c her- �r,c "r `�Cog aSo�g a- OIL SEND REPORT TO: ,. ,� 9). LIQ- OTHER LIQUID PHONE# �1.S - n� O FAX# �1� _ 000 - q �p a sol OTHER SOLID ACCUTEST COLLECTION PRESERVATION SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLED } Ivi LAB USE ONLY BY: Q z 9 7b- 07- 1000 l Z X -Z 7Ag2lA _16tiZ5 VkCq 6ih1 17 X x X x I IXIX X X -3 3 - M - A t0-5D �W '7 X X X X �C �C X KA o►•- >v\w- i iS30 m . G �C Y, lC > - MvJ-.s f q 4o taw X -7 mLm �l -- N\ -1 a 1340 m L0 6Wc� WN Ew --2-1 DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTS/REMARKS ❑ 14 DAYS STANDARD APPROVED BY: ❑ STANDARD ❑ 7 DAYS RUSH ❑ COMMERCIAL"B" ❑ 48 HOUR EMERGENCY ❑ DISK DELIVERABLE ❑ OTHER ❑ STATE FORMS - 14 DAY TURNAROUND HAROCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) lac• �D�.6F,3H 6 1 DATA UNLESS PREVIOUSLY APPROVED ( rC! SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLESCHANGE POSSESION,INCLUDING COURIER DELIVERY REUNOUISHED BY SAMPLER DATE TIME: R IV ECEED BY: REUNg pII4 ED BY: DA ME RECEIVE" 1. I 19 I O 1, (�SC 2 2. Y: REUNOUISHED BY: DA E ME: RECEIVED BY: RELINQUISHED BY: bAT11TIMM R Y. 3. 3. 4. 4. RELINOUISHED BY: DATE TIME: RECEIVED BY: SEAL# PRESERVE WHO APPLICABLE ONIC TEMpHp/�{!RE 5. 5. 3 C um MARLBOROUGH,MA 01752 ACCUTEST QUOTE r: TEL:508481-6200 FAX 508.481-7753 CLIENT INFORMATION FACILITY INFORMATION I ANALYTICAL INFORMATION MATRIX CODES DW- DRINKING WATER NAME PROJECT NAME 0'lA - GW- W aERD 1 f C) 1c n rti.,ot L Goa^K1=b ww- WASTE ADD RE LOCATION —� WATER 1 1�A� 1�1•� O t 74� cap 1 u 0 �;, O AC So- SOIL STATE ZIP PROJ�NO. SL- SLUDGE ,,pp � ff � oI- aL =► �4 I�r C�P�/ S.e�„� 4 C�9 aSoaS .V LIO- OTHER SEND REPORT TO: c LIQUID PHONE M FAX 11 O _]2-&(D d - SOL-OTHER ACCUTEST COLLECTION PRESERVATION N SOLID SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLED. ` Q z� j (, CJ LAB USE ONLY i x Z 't -it 02 13Zo CAW I X y -zR m - - fay MLM W 7 X XXtiC -1 M - 1 t 5 Zo 6W`7 �X `4 --1 Li - ^ i ly u 5 4-4 CAW Z /.� —MW— PA () I2A WW Z —/6 — InnW t 4g3S 1 � CsiW Z x x M11J w 2 X X -18 M - 1 Io05 rmAw W Z Y. X �� - w- f 2 -ZO Mi l 1 �- •- \�5 1O�Z5 '�v1 w W Z Mw \$o nr`vJ-i�D 1t1� MW W 2 DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTS/REMARKS ❑ 14 DAYS STANDARD APPROVED BY: O STANDARD �� _ ❑ 7 DAYS RUSH O COMMERCIAL"B" me �tkd C Iicye A b�5s FP ah�A ad 11 O 48 HOUR EMERGENCY O DISK DELIVERABLE c6tXnob O OTHER ❑ STATE FORMS 14 DAY TURNAROUND HAROCOPY.EMERGENCY OR RUSH IS FAX O OTHER(SPECIFY) o DATA UNLESS PREVIOUSLY APPROVED I SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERY RELINQUISHED BY SAMPLER- DATE TIME: RE�IIVED BY: RELIN DISHED BY: D ME RECEIV RELINQUISHED BY. DA E TIME: RECEIVED BY: ELINQUISHED BY: DATE TIME RECEIV Y: 3. 3. 4. 4. RELINQUISHED BY: DATE TIME: RECEIVED BY: SEAL t PRESERVE MMERE APPLICABLE S. 1 15. 0 Y (iHA1N OF CUSTODY ACCUTESTJOB.: UA TEST 495 TECHNOLOGY CENTER WEST• BUILDING ONE Z MARLBOROUGH,MA 01752 ACCUTEST QUOTE r- TEL:508-481-62W • FAX.•508-481-7753 CLIENT INFORMATION FACILITY INFORMATION= ANALYTICAL INFORMATION MATRIX CODES —�QO �Q11�G.C_n # 17 � DW- DRINKING NA[rlFr PROJECT NAME WATER ))I (.Sernr:VuI , r )-2- ` GW• GROUND A RESctn M WATER LOCATION WW. WASTE Sn n rl'1.4 C�'17 q 'a a-1 u .— %s UtsD�' q WATER CITY, STATE ZIP PROJECT N SO- SOIL t` .��lu �-I C f� �hr q(09 aSo ag SL- SLUDGE SEND REPORT Tg, OI- OIL n LKi- OTHER PHONE# "I 7R - SCO 4Z-��Y FAX 11 ci -SYCO?— .Z �� soL-OTHER LIQUID ACCUTEST COLLECTION PRESERVATION SOLID SAMPLE 1l FIELD ID/POINT OF COLLECTION DATE TIME SAM BY:ED J m _ LAB USE ONLY o Z3 T �`� I o 2 1WV o G•I.t7 � X �Z Tin 7 - I ry1 vh 6w I -rmp II - i Vv\l,Pvl GtJ DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTS/REMARKS ❑ 14 DAYS STANDARD APPROVED BY: ❑ STANDARD / ❑ 7 DAYS RUSH ❑ COMMERCIAL'B" ❑ 48 HOUR EMERGENCY ❑ DISK DELIVERABLE ❑ OTHER ❑ STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHA E POSSESION,INCLUDING COURIER DELIVERY RELINQUISHED BY SAMPLER: DATE TIME: RECEIVED BY: REU QUI ED BY: D TI ; RECEIV Y: t. -ell OZ tl* 1. mZ/ 2. RELINQUISHED : DATE TIME: RECEIVED BY: RELINQUISHED BY: ATE TIME: RECEIV Y: 3. 3. 4. 4. RELINOUISHEO BY: DATE TIME: RECEIVED BY: SEAL! 5, 5. - PRESERVE WHERE APPLICABLE ON ICE TEMPER/�URE Appendix D Well Logs GEOLOGIC SERVICES CORPORATION DRILLINGLOG Hydrogeologists and Environmental Scientists AS-1 15 Bonazzoli Avenue,Hudson,MA 01749 978 568-8740 Project Twco Station A 100083 Client Equiva Services LLC Sketch MV(not to male) Location: 1140 Iymmough Road,Hyannis,MA Total Depth: 49 feet Well ID: AS-1 Screen Diameter: 2inch Water Level: 31 feet Slot Size: 0.010 inch Screen Length: 2 feet Casing Diameter. 2 inch Type: 'PVC Type: PVC Casing Length: 47 feet Driller. Mike DCAmicns See Site Plan Top Elevation: 99.09 feet Drilling Company: Cxose—h,ht.. Method Hollow Stem Auger GSC hector: SC/KS Date Start 3/19200/ Date End 3212001 Notes:Testing consists of PID headspwe reponse(ppmv) Sample E; Depth Well Key ID Depth Blows/ti Pen/Rec Sample a feet Construction Description 0 Road box Gripper plug S-1 04 Brown,dry,medium to coarse SAND, ND -2 Concrete some medium to fine gravel,some cobbles a Native Material S-2 4-8' Brown,dry,medium to coarse SAND, ND 6 Casing some medium to fine gravel,some cobbles 8 10 _12 S-3 12-14' Brown,dry,medium to coarse SAND, ND _14 some fine to medium grave],some cobbles 16 4 18 s S4 18-29 Brown,dry,coarse SAND,some fine ND zo gravel,little cobble 22 24 S-5► 24-26 Brown,moist,medium to coarse SAND, 1.5 _26 Grout fine gravel 28 30 S-6 30-32' Brown,wet,medium to coarse SAND, 89 32 some fine gravel 34 _36 S-7 36-38' Brown,wet,coarse SAND 45 38 40 42 S-8 4244' Brown,wet,coarse SAND 35 a 46 Bentonite seal Well sere n 48 Filter sand so End of Exploration @ 49' OSC Project Number: 000509 Checked By: �t Page 1 of 1 Notes: '-Sample taken at this depth GEOLOGIC SERVICES CORPORATION DRILLING LOG Hydrogeologists and Environmental Scientists SVE-1 15 Bonazzoli Avenue,Hudson,MA 01749 978-568-8740 Project: Texaco Station 4100083 Cheat: Equiva Services LLC Sketch Map(not to scale) Location: 1140Iyanuough Road Hyannis,MA Total Depth: 36 feet ell ID: SVE-1 Screen Diameter. 4inch Water Level: —31 feet Slot Size: 0.010 inch Sweat Lengh 10 feet Casing Diameter. 4 inch Type: PVC Type: PVC Casing Lengh 26 feet _ Driller: Mike DeAmicus See Site Plan op Elevation: 99.11 feet Drilling Company: Geosearch,Inc. Method Hollow Stem Auger GSC Inspector: SC/DW Date Start: 3/19/01 Date End: 3/20/01 Notes:Testing consists of PID headspace response(ppmv) ample Depth Well Key ID Depth Blows/6" Pen/Rec Sample w feet Construction Description _0 Road box Gripper plug S-1 0-5' Brown,dry,fine SAND,little fine-medium ND _z Concrete gravel(SP) a 6 Casing S-2 5-10' Brown,dry,fine SAND,little fine gravel ND (SP) a _10 S-3 10-15' Brown,dry,fine SAND,some fine gravel, ND 12 Native Material cobbles(GM) la 16 S4 15-20' Brown,dry,fine SAND,little to some ND fine gravel(SP) 1s z0 S-5 20-25' Brown,dry,fine SAND,little fine gravel ND (SP) Bentonite seal 6 Filter sand S-6 25-30' Brown to tan,dry,fine SAND(SM) 0.2 r 2s —30 Well screen S-7* 30-35' Tan,dry to moist,fine SAND(NE) 111.7 2 _ a �6 S-8 35-36' Tan,moist to wet,fine SAND 78 End of Exploration @ 36' 8 40 GSC Project Number: 000509 Checked By: �' 'f` Page 1 of 1 Notes: *-Sample taken at this depth GEOLOGIC SERVICES CORPORATION DRILLING LOG Hydrogeologists and Environmental Scientists MP-1 15 Bonazzoli Avenue,Hudson,MA 01749(978)-568-8740 Project: Texaco Station#100083 Client Equiva Services LLC Sketch Map(not to scale) Location 1140 lyamough Road,Hyannis,MA Total Depth 43 feet Well ID: MP-1 Screen Diameter. 1.5 inch Water Level: —31 feet Slot Size: 0.010 inch Screen Length: 10,2,2 feet Casing Diameter: 1.5 inch Type: PVC Type: PVC Casing Length: 25,37,41 fed Driller Mile DeAmicus See Site Plan Top Elevation: 98.77 fed Drilling Company: Geoseard4 Inc. Method: Hollow Stem Auger GSC Inspector. DW Date Start 3/202001 Date End: 3/202001 Notes: Testing consists of PID headspace response(ppmv) Sample Depth Well Key ID Depth Blows/6" Pen/Rec Sample (feet)' Construction Description o Road box Gripper plugs S-1 0-5' Brown,dry,fine SAND(SC) ND 2 Concrete 4 6 Casing S-2 5-10' Brown,dry,fine SAND,fine gravel(SW) ND 8 10 S-3 10-15' Brown,dry,fine SAND,fine gravel(SW) ND 12 14 _16 S-4 15-20' Brown,dry,fine SAND,fine gravel(SW) ND 18 Native Material 20 S-5 20-25' Brown to tan,dry,fine SAND(SC) ND 22 24 Bentonite seal zb Filter sand S-6 25-30' Tan,dry to moist,fine SAND(SC) ND zs 30 S-7' 30-35' Brown,dry,fine SAND(SC) 0.5 32 Well screen 34 _36 S-8 35 40' Tan,moist to wet,fine SAND(SC) 1.3 38 Bentonite seal 40 S-9 40-43, Tan,moist to wet,fine SAND(SC) 1.7 a2 44 End of Exploration @ 43' GSC Project Number: 000509 Checked By: n (� Page 1 of 1 Notes: •-Sample taken at this depth I GEOLOGIC SERVICES CORPORATION DRILLING LOG Hydrogeologists and Environmental Scientists MP-2 15 Bonazzoli Avenue,Hudson,MA 01749(978)-568-8740 Project Tezam Station 4 100083 Client Equiva Services LLC Sketch Map(not to scale) Location: 1140 lyannough Road,Hyannis,MA Total Depth: 43 feet Well ID: MP-2 Screen Diameter: 1.5 inch Water Level: —31 feet Slot Size: 0.010 inch Screen Length: 10,2,2 feet Casing Dismet¢ 1.5 inch Type: PVC Type: PVC Casing Length: 25,37,41 fed Driller. Mike DeAmicas See Site Plan Top Elevation: 99.05 feet Dulling Company: Geosearch,Inc. Method Hollow Stem Auger GSC Inspector. SC/MLM Date Star 3/1912001 Date End: 3/222001 Notes:Testing consists of PID headspace response(ppmv) Sample Depth Well Key ID Depth Blows/6" Pen/Rec Sample a (feet) Construction Description o Road box Gripper plugs S-1 0-4' Brown,dry,medium to coarse SAND(SP) z Concrete a I� S-2 4-8' Brown,dry,medium to coarse SAND, _6 Casing some cobble(SW) s S-3 8-12' Brown,dry,medium to coarse SAND, _10 mostly cobble(SW) 12 Boulder 1a _16 S-4 15-20' Brown,dry,medium to coarse SAND, some fine gravel(SW) 1s Native Material zo S-5 20-25' Light brown,dry,medium SAND,some 22 fine gravel(SW) za Bentonite seal z6 Filter sand S-6' 25-30' Tan,dry,medium SAND,little gravel(SP) —zs 30 5 X. S-7 30-35' Tan,dry,medium SAND,little gravel(SP) 32 Well screen 34 36 S-8 35-40' Tan,dry,medium SAND,little gavel(SP) 38 Bentonite seal as S-9 40-43' Light brown,moist,medium SAND,little 42 fine gavel(SP) 44 End of Exploration @ 43' GSC Project Number: 000509 Checked By: ��?� \. Page 1 of 1 Notes: "-Sample taken at this depth GEOUDGIC SERVICES CORPORATION DRILLING LOG Hydrogeologists and Environmental Scientists W-3 15 Bonazzoli Avenue,Hudson,MA 01749(978)-568-8740 Project Texaco Station#10Do83 Client: Egoiva Services LLC Sketch Ma not to scale Location: 1140 Iyannough Road Hyannis,MA Total Depth: 43 feet Well ID MP-3 Screen Diameter. 1.5 inch Water Level: -31 feet Slot Siza 0.010 inch Screen Length: 10,2,2 feet Casing Diameter. 1.5 inch Type: PVC Type: PVC Casing Length: 25,37.41 feet Driller. Mike DeArmcos See Site Plan Top Elevation: 99.07 feet Drilling Company: Geosearck Inc. Method Hollow Stem Auger GSC Impactor. SCKS Date Stan: 3/21/01 Date End 3/21/01 Notes:Te.-Ling consists of PID heads ace response my ample Depth Well Key ID Depth Blows/6" Pen/Rec Sample (feet) Construction Description _o Road box Gripper plugs S-1 0-4' Brown,dry,fore to medium SAND,some ND z Concrete coarse sand,some fine to medium gravel, little cobble(GM) a 6 Casing a S-2 8-10' Brown,dry,fine to medium SAND,some ND 10 fine gravel,little cobble(GP) 12 14 S-3 14-1& Brown,dry,medium to coarse SAND, ND 16 some to little fine gravel(SW) 18 Native Material zo S4 20.2T Brown,moist,medium to coarse SAND ND z2 (SP) z4 Bentonite seal 26 Filter sand S-5# 26-28' Brown,moist,medium to coarse SAND 1.2 28 (SP) 0 z Well screen S-6 32-34' Brown,wet,coarse SAND,some medium 6.2 4 sand(SP) 6 8 Bentonite seal S-7 38-49 Brown,wet coarse SAND,some medium 0.7 40 sand(SP) a2 [7744 End of Exploration @ 43' GSC Project Number: 000509 Checked By: M1�( t^�� Page 1of1 Notes: `-Sample taken at this depth ! Appendix E Soil Sample Analytical Results APR 112001 ®ACCUTEST 04/05/01 Techn�ca7 Report for Equiva Services GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M 17430 Report to: Geologic Services Corp. 15 Bonazzoli Ave Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 6 Reza Tand Lab Director Certifications:MA(MA136) CT(PH-0109) NH(250293) NJ(59928) RI(A-71) ME(MA136) Results relate only to the items tested. This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•fax:508 481 7753•htip://www.accutest.com � APR 11 2001 - ®ACCUTEST Sample Summary Equiva Services GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Job No: M 17430 Sample ICollected Matrix Client .... ............................:........ Number Date Time By Received Code Type Sample ID M17430 1, 03/20/01 10:25 DW 03/21/01 SO Soil 1VIP01 ( 0 31) .........4 03/20/01 13:20 DW 03/21/01 SO Soil 'S�1;0� .30 31}; Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel.508 481 6200•fax:508 481.7753•hitp://www.accutest.com APR 112001 ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MP01 (30-31) Lab Sample ID: M17430-1 Date Sampled: 03/20/01 Matrix: SO-Soil Date Received: 03/21/01 Method: MADEP VPH Percent Solids: 96.9 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR4916.1) 1 04/03/01 JR n/a n/a GQR219 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene .;:.;..;.; 190 ug/kg 100-41-4 Ethylbenzene l :D;:;:::::;::;:;:;:: 190 ug/kg 1634-04-4 Methyl Tert Butyl Ether N.,p. 190 ug/kg 91-20-3 Naphthalene ND 190 ug/kg 108-88-3 Toluene ND 190 ug/kg m,p-Xylene ND 190 ug/kg 95-47-6 o-Xylene N 190 ug/kg C5-C8 Aliphatics(Unadj.) ND; 3800 ug/kg C9-C12 Aliphatics (Unadj.) 1�1 3800 ug/kg C9-C10 Aromatics (Unadj.) I�ID....... 3800 ug/kg CS-C8 Aliphatics h1I):..___ _ 3800 ug/kg C9- C12 Aliphatics ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 89% 70-130% 615-59-8 2,5-Dibromotoluene .:;;> 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough.MA 01752•tel:508 481 6200•tax:508 481 7753•http://www.accutest.com f 73 e ACCUTEST lzl f I l 2001 Report of Analysis Page 1 of 1 Client Sample ID: SVE01 (30-31) Lab Sample ID: M17430-2 Date Sampled: 03/20/01 Matrix: SO - Soil Date Received: 03/21/01 Method: MADEP VPH Percent Solids: 96.7 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR4917.1) 1 04./03/01 JR n/a n/a GQR219 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene NI3 240 ug/kg 100-41-4 Ethylbenzene ND _ 240 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 240 ug/kg 91-20-3 Naphthalene ND 240 ug/kg 108-88-3 Toluene ND 240 ug/kg m,p-Xylene ND 240 ug/kg 95-47-6 o-Xylene ND:.;:.;:.::;:.;:.;::,:; 240 ug/kg C5- C8 Aliphatics(Unadj.) ND. ._:. 4700 ug/kg C9-C12 Aliphatics (Unadj.) ND 4700 ug/kg C9- C10 Aromatics(Unadj.) ND 4700 ug/kg C5-C8 Aliphatics ND.. 4700 ug/kg C9-C12 Aliphatics ND 4700 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 9:9% >«< 70-130% 615-59-8 2,5-Dibromotoluene 9.8 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•let:508 481.6200•lax:508 481 7753•http://www.accutest.com 8 ACCUTEST AMPLE INFORMATION Aqueous Soil Sediment U Other. EDT fflffi MOP" 1WSatisfactory Broken Leaking: Aqueous N/A 6 '50�s NOT pH>2 Leaking: Soil or LJ N/A Userved in Methanol or mL Methanol/g soil Sediment Samples reed in Methanol: 'covering soil Li not covering soil ❑' 1:1+/-25 Samples rec'd in air-tight container. ❑Other: ° Received on Ice Rec'd at 4 Deg.C R10ther reed at 2 deg C - 'H ANALYTICAL RESULTS thod for Ranges:MADEP VPH 98-1 Client ID MP01(30-31) SVE01 (30-31) thod for Target Analytes:MADEP VPH 98-1 Lab ID M17430-1 M17430-2 i Surrogate Standards Date Collected 3/20/01 3120/01 PID:2,5-Dibromotoluene Date Received 3/21/01 3/21/01 FID:2,5-Dibromotoluene Date Analyzed 4/3/01 4/3/01 Dilution Factor 1 1 %Moisture(soil) 3.1 3.3 ige/Target Analyte Elution Range Units Result RL Q Result RL Q djusted C5-C8 Aliphatics(1) N/A ND 3800 ND 4700 djusted C9-C12 Aliphatics(1) N/A ND 3800 ND 4700 zene C5-C8 ug/kg ND 190 ND 240 1benzene C9-C12 ug/kg ND 190 ND 240 nyl-tert-butylether C5-C8 ug/kg ND 190 ND 240 hthalene N/A ug/kg ND 190 ND 240 gene C5-C8 ug/kg ND 190 ND 240 3 p-Xylenes C9-C12 ug/kg ND 190 ND 240 dene C9-C12 ug/kg ND 190 ND 240 38 Aliphatic Hydrocarbons(1,2) N/A ug/kg ND 3800 ND 4700 '.12 Aliphatic Hydrocarbons(1,3) N/A ug/kg ND 3800 ND 4700 ',10 Aromatic Hydrocarbons(1) N/A ug/kg ND 3800 ND 4700 Surrogate%Recovery 96 98 Surrogate%Recovery 89 99 ogate Acceptance Range 70-130% 70-130% rocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range -C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons J'qualifier indicates an estimated value RTIFICATION all(A/QC procedures REQUIRED by the VPH Method followed .Yes U No-Details Attached all performancelacceptance standards for required QA/QC procedures achieved? 0 Yes ❑ No-Details Attached any significant modifications made to the VPH method,as specified in Sect 11.37 Q No ❑ Yes-Details Attatched t under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for ing the information,the material contained in this report is,to the best of my knowledge and belief,acqyfate and ete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 04/05/01 Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•let:508 481 6200•tax:508 481 7753•http://www.accutest.com CHAIN OF CUSTODY ACCUTEST JOB#: ~ ACCUTES 495 Tech Center West,Bldg.I /7 12T Marlborough,MA 01752 ACCUTEST QUOTE#: Tel:508-481-6200• Fax:508-481-7753 z� CLIENT INFORMATION „ � Y �x FACILITY INFORMATION ;,., �._ �,... k ANALYTICAL INFORMATION NMI Consultants Name j Project Name �. y 1 J / ✓l S Addresj_ _,� ; Site Location J- 1 �5 ! City, State -zip Project No. Project Contact: 112; Phone#: i Fax#: 47> -Go -kiNiiM Collection t y PreservatiT- V Field ID/Point of Collection Sampled Date Time B "m° _ Y TURNAROUND INFORMATION x � DATA DELIVERABLE INFORMATION xa. z � COMMENTS/REMARKS A �. . ;d Standard Turnaround Approved By: ❑ Commercial "A" ❑ FULL CLP �Z ❑ .7 Days EMERGENCY ❑ Commercial "B" ❑ State Forms 3 y ❑ 72 hr.EMERGENCY W.Full Deliverables ❑ Disk Deliverable Format ❑ 48 hr.EMERGENCY ❑ 24 hr.EMERGENCY Emergency T/A is for FAX or Lablink Data ❑ Other ��� ��<���``��� �n��r� � Sample Custody Must be Documented Below Each Time Samples C ange Posseston,Including Courier Delivery '� ,� ,�,<r�`���� �R `�;������,�.� �G, Re uis d by ampler•- �W . Da Tlnpe: Received By: Relin ulehed�V J� Date e: �f�� Received �:yr �. 2 G�, .- 2. �. •inquished by Sam er, i at e: �`Y� Received By: R Ilnquished By: D eTl e: Received By: �• tom— 0 3. �—` 4. 4. ®ACCUTEST 04/12/01 Technlcal Report for Equiva Services GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M17520 Report to: Geologic Services Corp. 15 Bonazzoli Ave Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 6 Reza Tand ab Director Certifications: MA(MA136) CT(PH-0109) NH(250293) NJ(59928) RI(A-71) ME(MA136) Results relate only to the items tested. This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Massachusetts•495 Technology Center Wesl•Building One•Marlborough,MA 01752•tel:508 481 6200•lax:508 481 7753•http://www.acculest.com ®ACCUTEST Sample Summary Equiva Services Job No: M 17520 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID ....................I.,.... ........................... M17520 1 <03/21/01 10:45 KS 03/27/01 SO Soil ASQI S. --S20 2 : 03/21/01 14:00 KS 03/27/01 SO Soil MI'03.WWI Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•tax:508 481 7753•http://www.acculest.com ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: ASOI-AS-1-24' Lab Sample ID: M17520-1 Date Sampled: 03/21/01 Matrix: SO- Soil Date Received: 03/27/01 Method: MADEP VPH Percent Solids: 98.0 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5066.D 1 04/11/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene ND; 1-70 ug/kg 100-41-4 Ethylbenzene 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether ,,,,, . .; 170 ug/kg 91-20-3 Naphthalene ND.. 170 ug/kg 108-88-3 Toluene ND>:.__.:.. 170 ug/kg m,p-Xylene ND 170 ug/kg 95-47-6 o-Xylene ND 170 ug/kg C5- C8 Aliphatics (Unadj.) ND; 3400 ug/kg C9-C12 Aliphatics (Unadj.) ND: 3400 ug/kg C9-.C10 Aromatics (Unadj.) ND 3400 ug/kg C5- C8 Aliphatics ND; 3400 ug/kg C9-C 12 Aliphatics ND< 3400 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 70-130% 8..8.........:: .......................:. 615-59-8 2,5-Dibromotoluene 88% >> 70-130% .................. ........... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•lei:508 481 6200•tax:508 481 7753•http://www.accutest.com 05 ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MP03-MP-3-28' Lab Sample ID: M17520-2 Date Sampled: 03/21/01 Matrix: SO- Soil Date Received: 03/27/01 Method: MADEP VPH Percent Solids: 90.4 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5067.D 1 04/12/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene ND 170 ug/kg 100-41-4 Ethylbenzene ND ;;: : ' 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND ;,. j 170 ug/kg 91-20-3 Naphthalene ND 170 ug/kg 108-88-3 Toluene ND 170 ug/kg m,p-Xylene ND 170 ug/kg 95-47-6 o-Xylene ND 170 ug/kg C5- C8 Aliphatics (Unadj.) ND 3300 ug/kg C9- C12 Aliphatics (Unadj.) u ND 3300 /kg ...... . g...... ......................... C9-C10 Aromatics (Unadj.) ND :;..;. :;;; 3300 ug/kg C5- C8 Aliphatics ND 3300 ug/kg C9- C12 Aliphatics ND 3300 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 70-130% ......................... 15-59-8 2,5-Dibromotoluene 1.0.:2.%.._ ..::.. ; 70-130% ........................ ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•lei:508 481 6200•tax:508 481 7753•htip://www.accutest.com ®ACCUTEST MPLE INFORMATION w - _ " Lj Aqueous U4 Soil Sediment LJ Other. Satisfactory LJ Broken El Leaking: Aqueous v N/A 8J e?s NOT pH>2 Leaking: ,� Soil or N/A served in Methanol or mL Methanol/g soil Sediment ' Samples reed in Methanol: covering soilEl not covering soil ❑� 1:1+/_25 sI LJ Samples reed in air-tight container ❑Other. ' Received on Ice Rec'd at 4 Deg.C ✓Other reed at 3 deg C H ANALYTICAL RESULTS hod for Ranges:MADEP VPH 98-1 Client ID AS01-AS-1-24' MP03-MP-3-28' hod for Target Analytes:iMADEP VPH 98-1 Lab ID M17520-1 M17520-2 Surrogate Standards Date Collected 3/21/01 3/21/01 PID:2,5-Dibromotoluene Date Received 3/27/01 3/27/01 FID:2,5-Dibromotoluene Date Analyzed 4/11/01 4/12/01 Dilution Factor 1 1 %Moisture(soil) 2 9.6 gerfarget Analyte Elution Range Units Result RL Q Result RL Q ldjusted C5-C8 Aliphatics(1) N/A ND 3400 ND 3300 adjusted C9-C12 Aliphatics(1) N/A ND 3400 ND 3300 izene C5-C8 ug/kg ND 170 ND 170 benzene C9 C12 ug/kg ND 170 ND 170 hyl-tert-butylether C5-C8 ug/kg ND 170 ND 170 hthalene N/A ug/kg ND 170 ND 170 ene C5-C8 ug/kg ND 170 ND 170 p-Xylenes C9-C12 ug/kg ND 170 ND 170 le C9-C12 ug/kg ND 170 ND 170 Aliphatic Hydrocarbons(1,2) N/A ug/kg ND 3400 ND 3300 12 Aliphatic Hydrocarbons(1,3) N/A ug/kg NO 3400. ND 3300 10 Aromatic Hydrocarbons(1) N/A ug/kg ND 3460 ND 3300 Surrogate%Recovery 88 102 Surrogate%Recovery 88 101 gate Acceptance Range 70-130% 70-130% rocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range rJ�qualifier 2 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons indicates an estimated value 11TIFICATION all QA/QC procedures REQUIRED by the VPH Method followed? Yes No-Details Attached all performance/acceptance standards for required QA/QC procedures achieved? Q Yes ❑ No-Details Attached any significant modifications made to the VPH method,as specified in Sect 11.39 No ❑ Yes-Details Attatched t under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for ing the information,the material contained in this report is,to the best of my knowledge and belief,accu a and to. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tan DATE: 04/12/01 Massachusetts 495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•fax:508 481 7753•http://www.accutest.com CHAINGOB' CUSTY CENTER WEST a NODY ACCUTEST JOB#G ONE �I�.6�O ®AC.CUTEST MARLBOROUGH,MA 01752 ACCUTEST QUOTE#: TEL:508-481-6200 • FAX.508-481-7753 ` rya CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES ,�, �+_ DW- DRINKING _- Ly �1liYl[r_ Sf'i�1lIcNS -C7S�i7� �L ' l Gl V tGC WATER NAME �� PR JECT A GW- GROUND 1:5 Y)0.7T121, 969dSoa ` V`ry a�. WW- WWATER ASTE ADDRE LO ATION WATER sots . ; �U�tt�nts '}� � so. soa CITY, Q STATE ZIP PROJE T N !�i-t(: �' 000 OI- OILDGE SEND REPORT TO:. LIQ- OTHER PHONE# �����`rbg ����D FAX# y7�`.S`� � ��� soL-OLIQUID THER ACCUTEST COLLECTION x w PRESERVATION SOLID SAMPLE# FIELD ID/POINT OF COLLECTION SAMPLED a ° D c c i LL J - DATE TIME BY: m _ z = = Z LAB USE ONLY _F[T DATA TURNAROUND INFORMATION F DATA DELIVERABLE INFORMATION COMMENTS/REMARKS 14 DAYS STANDARD APPROVED BY: STANDARD - ❑ 7 DAYS RUSH D COMMERCIAL"B" O 48 HOUR EMERGENCY ❑ DISK DELIVERABLE O OTHER ❑ STATE FORMS ❑ OTHER SPECIFY 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX �.O C . V 2), 3 F DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERY RELINQUISHED BY.SAMPLER DATE TIME: RECEIVED BY: REUNQUISHE Y: DATE ME: RECEIVED BY: RELINQUISHED BY- DATE TIME: N �. �� L� , R 3. ff /�2;y RECEIVED B�Z _ � REUNQUIS D BY: AT TIME: RECEIVED BY: ,3-��0 3•If 11 4• 4. RELINQUISH BY: DATE TIME: RECEIVED BY: SEAL t PRESERVE WHERE APPLICABLE ON ICE TEMPERATURE n. ®ACCUTEST 04/12/01 APR 13 ?R91 Technlcal Report for Equiva Services GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M 17503 Report to: Geologic Services Corp. 15 Bonazzoli Ave Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 10 Reza Tand Lab Director Certifications:MA(MA136) CT(PH-0109) NH(250293) NJ(59928) RI(A-71) ME(MA136) Results relate only to the items tested. This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•tax:508.481 7753•http://www.accutest.com a® ®ACCUTEST Sample Summary Y Equiva Services Job No: M 17503 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M175034 03/22/01 09:20 MM 03/26/01 SO Soil MWi30') M17S03 2'I!03/22/O1 11:50 MM 03/26/01 SO Soil 11r1P2(25 30'� .. .... ............................ ........................... M17503 3 03/22/01 15:00 MM 03/26/01 SO Soil IvIW12(25 30') M17S03-4 03/23/01 09:25 MM 03/26/01 SO Soil IviW13 (25 30' ........................... M17503.5 <;03/23/01 10:55 MM 03/26/01 SO Soil IvIW14 (Z5z,2 7) Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•fax:508 481.7753•http://www.accutest.com ®AccuTEsT Report of Analysis Page 1 of 1 Client Sample ID: MW11 (25-30') Lab Sample ID: M17503-1 Date Sampled: 03/22/01 Matrix: SO- Soil Date Received: 03/26/01 Method: MADEP VPH Percent Solids: 96.0 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5013.1) 1 04/09/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 190 ug/kg 100-41-4 Ethylbenzene ND 190 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 190 ug/kg 91-20-3 Naphthalene ND 190 uglkg 108-88-3 Toluene ND 190 ug/kg m,p-Xylene ND 190 ug/kg 95-47-6 o-Xylene ND 190 ug/kg C5- C8 Aliphatics(Unadj.) ND 3900 ug/kg C9-C12 Aliphatics (Unadj.) ND 3900 ug/kg C9-C10 Aromatics (Unadj.) ND 3900 ug/kg C5-C8 Aliphatics ND 3900 ug/kg C9- C 12 Aliphatics ND 3900 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 102% _, 70-130% 615-59-8 2,5-Dibromotoluene 100% 70-130% .. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•tax:508 481 7753•hUp://www.accutesi.com . r MACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MP2 (25-30') Lab Sample ID: M17503-2 Date Sampled: 03/22/01 Matrix: SO- Soil Date Received: 03/26/01 Method: MADEP VPH Percent Solids: 93.5 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5014.1) 1 04/09/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 180 ug/kg 100-41-4 Ethylbenzene NI) ; i' i ; 180 ug/kg 1634-04-4 Methyl Tert Butyl Ether IVD :;::: 180 ug/kg 91-20-3 Naphthalene ND ; 180 ug/kg 108-88-3 Toluene N..D.........:::. 180 ug/kg m,p-Xylene ND; 180 ug/kg 95-47-6 o-Xylene ND 180 ug/kg C5- C8 Aliphatics (Unadj.) hiD 3500 ug/kg C9-C12 Aliphatics (Unadj.) ND:.. ....,,, 3500 ug/kg Nb C9-C10 Aromatics (Unadj.) ... ,,,,,,;,< 3500 ug/kg C5- C8 Aliphatics_ NI2_... ;i< 3500 ug/kg C9-C12 Aliphatics ND< 3500 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene01 '; ;; ;i 70-130% ......................... 615-59-8 2,5-Dibromotoluene 93i%> > < > 70-130% ............. ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts 1 495 Technology Center West•Building One•Marlborough,MA 01752•let:508 481 6200•tax:508.481 7753•http://www.acculest.com ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MW12(25-30') Lab Sample ID: M 17503-3 Date Sampled: 03/22/01 Matrix: SO- Soil Date Received: 03/26/01 Method: MADEP VPH Percent Solids: 94.9 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5015.D 1 04/09/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene Nl)::::;;;' 210 ug/kg 100-41-4 Ethylbenzene ND 210 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND..:. 210 ug/kg 91-20-3 Naphthalene 210 ug/kg 108-88-3 Toluene ND 210 ug/kg D m,p-Xylene N 210 ug/kg 95-47-6 o-Xylene ND 210 ug/kg C5- C8 Aliphatics(Unadj.) ND >4200 ug/kg C9- C12 Aliphatics (Unadj.) NID 4200 ug/kg C9- C10 Aromatics(Unadj.) ND 4200 ug/kg C5- C8 Aliphatics XNIJ 4200 ug/kg C9- C12 Aliphatics N...D .......... : 4200 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 9..Ss% 70-130% 615-59-8 2,5-Dibromotoluene 97N 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough;MA 01752•let:508 481 6200•fax:508 481 7753 4 hnp://www.acculest.com ®ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MW13 (25-30') Lab Sample ID: M17503-4 Date Sampled: 03/23/01 Matrix: SO - Soil Date Received: 03/26/01 Method: MADEP VPH Percent Solids: 96.0 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5016.D 1 04/09/01 JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 220 ug/kg 100-41-4 Ethylbenzene ND 220 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 220 ug/kg 91-20-3 Naphthalene ND 220 ug/kg 108-88-3 Toluene ND 220 ug/kg m,p-Xylene ND 220 ug/kg 95-47-6 o-Xylene ND 220 ug/kg C5- C8 Aliphatics (Unadj.) ND 4300 ug/kg C9-C12 Aliphatics (Unadj..) hID 4300 ug/kg C9- C10 Aromatics(Unadj.) ND.. .. 4300 ug/kg C5-C8 Aliphatics ND 4300 ug/kg C9- C12 Aliphatics ND 4300 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ...............:.......- 615-59-8 2,5-Dibromotoluene 96% 70-130% ......................... ......................... ......................... 615-59-8 2,5-Dibromotoluene 94% ;>;; 70-130% ...............:.......:. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•tax:508.481 7753•http://www.accutest.com r e ACCUTEST Report of Analysis Page 1 of 1 Client Sample ID: MW14 (25-27') Lab Sample ID: M17503-5 Date Sampled: 03/23/01 Matrix: SO- Soil Date Received: 03/26/01 Method:: MADEP VPH Percent Solids: 95.8 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID - DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR5017.D 1 04/09/01 ' JR n/a n/a GQR223 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 170 ug/kg 100-41-4 Ethylbenzene ND 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether NI) 170 ug/kg 91-20-3 Naphthalene ND 170 ug/kg _.. . 108-88-3 Toluene I�ID 170 ug/kg m,p-Xylene ND 170 ug/kg 95-47-6 o-Xylene ND 170 ug/kg C5- C8 Aliphatics (Unadj.) ND 3400 ug/kg C9-C12 Aliphatics(Unadj.) ND 3400 ug/kg C9- C10 Aromatics (Unadj.) IUD; 3400 ug/kg C5-C8 Aliphatics ND.. 3400 ug/kg ....... .................. C9-C12 Aliphatics ND: 3400 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 9:1% 70-130% 615-59-8 2,5-Dibromotoluene 98:%_.- 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•tax:508 481 7753•http://www.accutest.com e ®ACCUTEST SAMPLE INFORMATION Li Aqueous 'Soil Li Sediment U Other. Satisfactory U BrokenLJ Leaking: q 13� �NOT LJpH>2 Li Leaking: Soil or LJ N/A Userved in Methanol or mL ves Sediment ' Samples reed in Methanol: ' covering soil LJ not covering soil ❑ LJ Samples rec'd in air-tight container: ❑ Q w T ' Received on Ice U Rec'd at 4 Deg.C 'Other reed at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID MP2(25-30') MW11 (25-30') MW12(25-30') Method for Target Analytes:MADEP VPH 98-1 Lab ID M17503-2 M17503-1 M17503-3 VPH Surrogate Standards Date Collected 3/22/01 3/22/01 3/22/01 PID:2,5-Dibromotoluene Date Received 3/26/01 3/26/01 3/26/01 FID:2,5-Dibromotoluene Date Analyzed 4/9/01 4/9/01 4/9/01 Dilution Factor 1 1 1 %Moisture(soil) 6.5 4 5.1 Range/Target Analyte Elution Range Units Result RL Q Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 3500 ND 3900 ND 4200 Unadjusted C9-C12 Aliphatics(1) N/A ND 3500 ND 3900 NO 4200 Benzene C5-C8 ug/kg NO 180 NO 190 NO 210 Ethylbenzene C9-C12 ug/kg NO 180 NO 190 ND 210 Methyl-tert-butylether C5-C8 ug/kg NO. 180 ND 190 NO 210 Naphthalene N/A ug.fkg ND 180 NO 190 ND 210 Toluene C5-C8 ugikg NO 180 ND 190 NO 210 m-&p-Xylenes C9-C12 ugikg NO 180 NO 190 NO 210 o-Xylene C9-C12 uglkg NO 180 ND 190 ND 210 C5-C8 Aliphatic Hydrocarbons(1,2) N/A ugikg NO 3500 NO 3900 NO 4200 C9-C12 Aliphatic Hydrocarbons(1,3) N/A ug/kg ND 3500 ND 3900 ND 4200 C9-C10 Aromatic Hydrocarbons(1) N/A ugfkg ND 3500 ND 3900 NO 4200 PID Surrogate%Recovery 93 100 97 FID Surrogate%Recovery 101 102 95 Surrogate Acceptance Range 70-130% 70-1 30% 70-130% 1-Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 2-C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range 3-C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons 4-A V qualifier indicates an estimated value CERTIFICATION Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes u No-Details Attached Were all berfornance/acceptance standards for required QA/QC procedures achieved? Q Yes ❑ No-Details Attached Were any significant modifications made to the VPH method,as specified in Sect 11.37 2 No ❑ Yes-Details Attatched I attest underthe pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material oontained in this report is,to the best of my knowledge and belief,a to and complete. SIGNATURE:_ POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 04/12/01 Massachusetts•495 Technology Center Wesl•Building One•Marlborough,MA 01752•tel:508 481 6200•lax:508 481-7753•hitp://www.acculest.com 05 ®ACCUTEST SAMPLE INFORMATION Ma % ,`. " , ,_ Aqueous 'Soil Sediment Other. ?3:. � U4 Satisfactory LJ Broken U Leaking: �.Aqueous ' N/A LJ W —,?s NOT PH>2 U Leaking: Soil or LJ N/A erved in Methanol or ImL E g LUve _ r Sediment U Samples reed in Methanol: 'covering soil U not covering soil ❑v - Samples reed in air-fight container. ❑ Received on Ice Redd at 4 Deg.C 4 Other reed at 3 deg C VPH ANALYTICAL RESULTS Method for Ranges:MADEP VPH 98-1 Client ID MW13(25-30') MW14(25-27') Method for Target Analytes:MADEP VPH 98-1 Lab ID M17503-4 M17503-5 VPH Surrogate Standards Date Collected 3/23/01 3/23/01 PID:2,5-Dibromotoluene Date Received 3/26/01 3/26101 FID:2,5-Dibromotoluene Date Analyzed 4/9/01 4/9/01 Dilution Factor 1 1 %Moisture(soil) 4 4.2 - Rangefrarget Analyte Elution Range Units Result RL Q Result RL Q Unadjusted C5-C8 Aliphatics(1) N/A ND 4300 ND 3400 Unadjusted C9-C12 Aliphatics(1) N/A ND 4300 ND 3400 Benzene C5-C8 ug/kg ND 220 ND 170 Ethylbenzene C9-C12 ug/kg ND 220 ND 170 Methyl-tert-butylether C5-C8 ug/kg ND 220 ND 170 Naphthalene N/A ug/kg ND 220 ND 170 Toluene C5-C8 ug/kg ND 220 ND 170 m-&p-Xylenes C9-C12 ug/kg ND 220 ND 170 o-Xylene C9-C12 ug/kg ND 220 ND 170 C5-C8 Aliphatic Hydrocarbons(1,2) N/A ug/kg ND 4300 ND 3400 CO-C12 Aliphatic Hydrocarbons(1,3) N/A ug/kg ND 4300 ND 3400 C9-C10 Aromatic Hydrocarbons(1) N/A ug/kg ND 4300 ND 3400 PID Surrogate%Recovery 94 98 FID Surrogate%Recovery 96 91 Surrogate Acceptance Range 70-130% 70-130% 132 -Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range -C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range -C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons -A'J'qualifier indicates an estimated value CERTIFICATION ere all QA/QC procedures REQUIRED by the VPH Method followed? U4 Yes Li No-Details Attached ere all performancelacceptance standards for required QA/QC procedures achieved? ❑'Yes ❑ No-Details Attached ere any significant modifications made to the VPH method,as specified in Sect 11.3? 2)No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for btaining the information,the material contained in this report is,to the best of my knowledge and b7rate and mplete. SIGNATURE: POSITION: Laboratory Director PRINTED NAME: Reza Tand DATE: 04/12/01 Massachusetts•495 Technology Center West•Building One•Marlborough,MA 01752•tel:508 481 6200•fax:508 481 7753•http://www.accutest.com 013 CHAIN OF CUSTODY ACCUTEST JOB#: MACCUTEST 495 TECHNOMARLBOROUGH,MA 01752 ILDING ONE ACCUTEST QUOTE#: TEL:508-481-6200 • FAX:508-481-7753 CLIENT INFORMATION FACILITY INFOR`MArTION ANALYTICAL INFORMATION MATRIX CODES . DW- DRINKING NAM PROJECT NAME WATER GW- GROUND ✓IGZ�S✓`� r 1 Z'Id n�... Iff�^ti�,s /� . J' WATER ADD �,,�j�SS� _�!J� 4 LOCATIONq' q� (( WW- WASTE �So�t / 1 �� WATER CRY, .A^ ESTATE ZIP PROJECT NO. SO- SOIL - I_/C,17 r, SL- SLUDGE OI- OIL SEND REPORT TO: LIQ- OTHER PHONE#- 7q—G(�g 7Yc > FAX# 9 1 J b LIQUID SOL-OTHER ACCUTEST COLLECTION x y PRESERVATION. SOLID SAMPLE# FIELD ID/POINT OF COLLECTION SAMPLED �+ DATE TIME BY: 'm _ _ = a oE `3 LAB USE ONLY = z o ;M f 1 ZS—30') z zo V"Lm 5 X X /7 0 Z ZS -3U' 11S G I 150 C2-5--�00 Isow malsk L. S Z?I Z Gl "cx5 i'VI Z k .� toc," 147, g � DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION COMMENTS/REMARKS 14 DAYS STANDARD APPROVED BY: STANDARD Cl 7 DAYS RUSH OMMERCIAL"B" ❑ 48 HOUR EMERGENCY ❑ DISK DELIVERABLE ❑ OTHER ❑ STATE FORMS 1 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES, H OSSESION,INCLUDING COURIER DELIVERY REUt4QUISHE BY DAFE TI E: RECEIVED BY: REU ISHED Y: D E TI E: y5 RECEIVED B R LINOUISHED BY: DATE TIME: RECEIVED BY: REUNQUISHED BY: DATE ME: RECEIVED BY: 3. ��11�' 4. 4. RELINQUISHED DATE TIME: RECEIVED B SEAL# PRESERVE WHERE APPLICABLE ON ICE,," TEMPERATURE Appendix F Charts { Chart 1 Applied Vacuum at SVE-1 vs Flow Rate Texaco Service Station#100083 1140 Iyanough Road Hyannis, MA 14 12 10 o " = 8 _. 6 4 2 0 0 20 40 60 80 100 120 140 160 180 200 Flow Rate (SCFM) Chart 2 Normalized Vacuum vs. Distance from SVE-1 @ 5"H20 Texaco Service Station#100083 1140Iyanough Road Hyannis,MA 1 ♦MP-1 ,a ®MP-2 0 c. 0.1 o MP-3 x MW-9 E A c.� ev d x N E 0.01 — 0 z Radius of Influence of 37 ft 0.001 0 5 10 15 20 25 30 35 40 45 50 Distance(ft) Chart 3 Normalized Vacuum vs. Distance from SVE-1 10"H20 Texaco Service Station#100083 1140 Iyanough Road Hyannis, MA 1 c. 0.1 ♦MP-1 MP-2 o o MP-3 > .a X MW-9 N X •td E 0.01 0 z Radius of Influence of 38 ft 0.001 - 0.0 5.0 10.0 15.0 20.0 25.0 30.0 35.0 40.0 45.0 50.0 Distance (ft) Chart 4 Normalized Vacuum vs. Distance from SVE-1 @ 1.3"H20 Texaco Service Station#100083 1140 Iyanough Road Hyannis,MA 1 Q. 0.1 �a E � ♦MP-1 _ d N E 0.01 `o z Radius of Influence of 33 ft 0.001 0 5 10 15 20 25 30 35 40 45 50 Distance (ft) Chart 5 Influent VOC Concentrations vs. Time Texaco Service Station #100083 1140 lyanough Road Hyannis, MA 900 800 700 Q _a N 600 0 500 m 0 0 400 U O 300 5"H20 10 "H20 5"H20 Vacuum with 2 2 acuum with Vacuum Vacuum Sparge @ 3 scfm Vacuum Helium Injection 200 with S are 6 scfm @ 6.5 scfm 100 0 0 20 40 60 80 100 120 140 160 180 200 220 Time (min) Chart 6 Groundwater Mounding vs. Time Texaco Service Station #100083 1140 lyanough Road Hyannis, MA 0.2 0.18 0.16 � 0.14 5 "H20 Vacuum 10 "H20 5"H20 Vacuum with = Vacuum Sparge @ 3 scfm °a 0.12 0 z 0.1 MP-2 ea 0.08 If 0 0.06 5"H20 Vacuum with 5 "H20 Vacuum with Sparge @ 6.5 scfm Helium Injection 0.04 -- 0.02 - 0 OL 20 40 60 80 100 120 140 160 180 200 220 Time (min) Chart 7 Dissolved Oxygen Content vs. Time Texaco Service Station #100083 1140 lyanough Road Hyannis, MA 4.0 3.5 - ----. 3.0 J E 2.5 m MP-1 x 2.0 M P-2 0 ---A-MP-3 a m > w 1.5 _N 1.0 0.5 5 "H20 Vacuum 10 "H20 5"H20 Vacuum with 5 "H20 Vacuum with 2U Vacuum wi tfF- Vacuum Sparge @ 3 scfm Sparge @ 6.5 scfm Helium Injection @ 0.0 1 1 1 1 1 6 scfm 0 20 40 60 80 100 120 140 160 180 200 220 Time (min) i Appendix G Air Sample Analytical results 06/07/01 .; ?rt:: <:::;>: .: Equiva Services GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA Accutest Job Number: E91703 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 9 ��M IICCpq , Y � t S intent J. Pu liese Test results contained within this data package meet the requirements g of the National Environmental Laboratory Accreditation Conference President and/or state specific certification programs as applicable. Certifications: NJ(12129),NY(10983),CA,CT,DE,FL,MA,MD,NC,PA,RI,SC,VA This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New Jersey 2235 Route 130 ■ Dayton,NJ 08810■tel:732-329-0200■ fax:732-329-3499 E http://www.accutest.com Accutest Laboratories Sample Summary Equiva Services Job No: E91703 GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA .... .:...........................................................Sam le e :: Matrix Client.. Number Date Time By Received Code Type Sample ID E�1`.0 »> .::......... .......................... DF OS/23/01 AIR Air iS+:: .....<:::......::.. ..:.. ::>:«:::... .. T39. - OS/18/ .:... .;:::::::: . 5 DF OS/23/01 AIR Air «:.;.....»::::;:::;::; Accutest Laboratories Report of Analysis Page 1 of 3 Client Sample ID: AS + SVE Lab Sample ID: E91703-1 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 Q10989.1) 800 05/31/01 WG n/a n/a VQ415 Run#2 Q10997.1) 2000 05/31/01 WG n/a n/a VQ415 CAS No. MW Compound Result RL Units Q Result RL Units 71-43-2 78 Benzene 282t30 ;' ' ; 160 ppbv 9pQD' < ' 510 u /m3 :. g 100-41-4 106 Ethylbenzene 297(3t? ; 160 by 1690 u /m3 PP g 1634-04-4 88 Methyl Tert Butyl Ether 77904 4000 ppbv G: p(1fj 14M u /m3 g 91-20-3 128 Naphthalene 28O0>i 160 ppbv 14t Q1 ; MO u /m3 P g 108-88-3 92 Toluene 0 4000PPby 15000 u /m3 74106 m, -X lene >109000a s` 4000 PPby 17000 u /m3a D Q9547-6 106 o-X lene 4000 PPbv0» 1a 7000 ug/m33940 01330-20-7 106 X lens (total) 4000 PPby 000 17000 u /m3 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ........................ ......................... 460-00-4 4-Bromofluorobenzen 1€l . 88 <' ';; 70-130% ......................... ................... CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q ........................... Pentane 5.34 7200 ;ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 5.48 2100; » ppbv J ................:....:..... ........................... C5-C8 Aliphatic 5.64 11fiQ ; i ; ppbv J ..................:........ ........................... ........................... C5-C8 Aliphatic 5.75 3000 ppbv J C5-C8 Aliphatic 6.11 2.I00 ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 6.54 474> < i ppbv J C5-C8 Aliphatic 6.65 101 ppbv J ........................... ........................... CS-C8 Aliphatic 6.85 50#>< ><> ppbv J ........................... ........................... C5-C8 Aliphatic 7.34 79Q0 ppbv J ....:.:.................... ........................... C5-C8 Aliphatic 7.482Q0< >< >` ppbv J ........................... C5-C8 Aliphatic 7.82 8000>< = ppbv J C5-C8 Aliphatic 7.96 (00 '> ppbv J ....................::..... ........................... C5-C8 Aliphatic 8.02 00;>>< ppbv J .....................:..... ........................... ........................... CS-C8 Aliphatic 8.14 240p < <i >i ppbv J C5-C8 Aliphatic 8.24 12{3Q: >€ ; ppbv J C5-C8 Aliphatic 8.43 2O1 >ppbv J C5-C8 Aliphatic 8.57 G3Q >;i;`;>i ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 8.68 5.0 ppbv J ...:.................::.... ........................... C5-C8 Aliphatic 8.75 38{)0 ; ppbv J C5-C8 Aliphatic 8.95O0t < <><ppbv J C5-C8 Aliphatic 9.36 15.0 ppbv J ..........:............... ........................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 2 of 3 Client Sample ID: AS + SVE Lab Sample ID: E91703-1 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q ........................... C5-C8 Aliphatic 9.57 290Q `> :ppbv J C5-C8 Aliphatic 9.67 2 >'> ppbv J ........................... ........................... C5-C8 Aliphatic 9.72 7 ppbv J C5-C8 Aliphatic 9.92 3G000 > ppbv J ........................... .......................::. C5-C8 Aliphatic 10.00 2fJ00Q <'` ppbv J :.............:............ CS-C8 Aliphatic 10.2000: > ppbv J . .......::.................. ........................... C5-C8 Aliphatic 10.28 530-0 ppbv J C5-C8 Aliphatic 10.45 950O ' ` ppbv J ........................... ........................... C5-C8 Aliphatic 10.54 110 ppbv J C5-C8 Aliphatic 10.64 1:600Q>'><« ' ppbv J C5-C8 Aliphatic 10.88 10a ` >'< ppbv J C5-C8 Aliphatic 10.95 2800.0 ppbv J ...:.:..................... ........................... C5-C8 Aliphatic 11.01 170 (l' ; ppbv J C5-C8 Aliphatic 11.09 €;41104 ;;> ppbv J ........................... ........................... C5-C8 Aliphatic 11.16 1bfJ0: > ppbv J C5-C8 Aliphatic 11.25 } ppbv J ........................... ........................... C5-C8 Aliphatic 11.34 1:OQt)4 ';; ppbv J C5-C8 Aliphatic 11.68 18(f[0 ppbv J ...:.::.................... ........................... C5-C8 Aliphatic 11.74 T2*0(3; ; ;> ppbv J C5-C8 Aliphatic 11.94 12+ 00>> ppbv J ........................... ........................... C5-C8 Aliphatic 12.02 ;19.0 <>i ppbv J C5-C8 Aliphatic 12.26 470 > < ppbv J ........................... C5-C8 Aliphatic 12.35 >14Ci0: ppbv J C5-C8 Aliphatic 12.46 3000 ppbv J ........................... ........................... C5-C8 Aliphatic 12.56 4.2(,0 ppbv J C5-C8 Aliphatic 12.88 1G04> ppbv J ........................... C5-C8 Aliphatic 12.97 ;14000'< ppbv J C5-C8 Aliphatic 13.02 14` ;> ppbv J ........................... ........................... C5-C8 Aliphatic 13.11 2'lQd „< ' ppbv J C5-C8 Aliphatic 13.20 1000 ppbv J ................:.......... ........................... C5-C8 Aliphatic 13.39 4700.:'. i ppbv J C5-C8 Aliphatic 13.52 11... 0(1i ppbv J ........................... ........................... C5-C8 Aliphatic 13.66 f9.00ii ppbv J C5-C8 Aliphatic 13.720 »' ppbv J C5-C8 Aliphatic 13.78 .3 ppbv J C5-C8 Aliphatic 13.85 1GOQ » ppbv J ........................... ........................... C5-C8 Aliphatic 13.94 1;1000 ;> ; ppbv J C5-C8 Aliphatic 14.02 2200i `ppbv J .........:................. ........................... C5-C8 Aliphatic 14.15 4fi0O'<; > ; ppbv J C5-C8 Aliphatic 14.28 $5:0; < :ppbv J ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 3 of 3 Client Sample ID: AS + SVE Lab Sample ID: E91703-1 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA CAS No. Tentatively Identified Compounds R.T. Est. Cone. Units Q ........................... C5-C8 Aliphatic 14.34 130 ppbv J C5-C8 Aliphatic 14.45 190(# ppbv J ......:.................... ........................... C5-C8 Aliphatic 14.62 Z73Q`' "; >' ppbv J C5-C8 Aliphatic 14.78 1bQ.> ppbv J ........................... C5-C8 Aliphatic 14.97 490t1;; ppbv J C5-C8 Aliphatic 15.10 $Q( ppbv J .......................... ........................... C5-C8 Aliphatic 15.19 130(<>< > < ppbv J C5-C8 Aliphatic 15.34GU(3 ppbv J ...........:............... ........................... C5-C8 Aliphatic 15.91 3 () ppbv J C5-C8 Aliphatic 16.13 1) . ; ppbv J Hl C9-C12 Aliphatic 16.60 1<?( '< ppbv J C9-C10 Aromatic 17.09 ppbv J ......................:.... ........................... C9-C12 Aliphatic 17.26 1 ppbv J C9-C12 Aliphatic 17.50 .1w. '`' ppbv J ..................:..::.... ........................... C9-Cl0 Aromatic 17.82 42 < _<;;ppbv J C9-C10 Aromatic 17.98 1f00 ' > ppbv J C9-C10 Aromatic 18.04 5 ppbv J C9-C10 Aromatic 18.16 10( „>> i<i ppbv J .......................... ........................... C9-C12 Aliphatic 18.23 11i <»ppbv J C9-C 10 Aromatic 18.43 4flt ppbv J .......:..........:........ ........................... C9-C10 Aromatic 18.78 1503 ppbv J C9-C10 Aromatic 19.4600 ' ppbv J ........................... ........................... C9-C10 Aromatic 19.77 1SQ `> ppbv J ........................... Pha..: .;:.;;;:.;:.;:.;;:.:::. -:: . PPbv ntal.CSC.Ail haucs:::::::::::::::.: ::::: ...::::::. 06t >< u /m3 P.::.::.:.:::. SQO> PPbv Total: >'` < »'` ><' ><<><> >> G ,CI .AII tlalics::::::::::.::.:.: . : 3jf0< >><» u /m3 ::::: »::>:<::<:>: g Total:>: ,._ .,...,:.._:.;.:..:..>: <:>::<::>:Aron}atlas:::::::::::.::::::::..:._:.:._:::::.. 5b >` by PP C9-Cltl ArolilailCS 30600I,.. ug/m3 tal TIC, Yolaiile.;:: 61310 PPbv (a)Result is from Runt/2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 3 Client Sample ID: SVE Lab Sample ID: E91703-2 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/O1 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 Q10990.1) 4000 05/31/O1 WG n/a n/a VQ415 Run#2 Q10998.1) 8000 05/31/O1 WG n/a n/a VQ415 CAS No. MW Compound Result RL Units Q Result RL Units 71-43-2 78 Benzene 3 ( ? > < ><; 800 PPby <i1:02Q141 >`> 2600 ug/m3 1 n 800 by 1330Ot> « 35W u /m3 100-41-4 106 Ethy benze a 3t ( «>`; :: PP g SOf >> >_ 29W u /m3 1634 04 4 88 Methyl Tert Butyl Ether 79.30t7>r» 8W ppbv 2 ...,,,,:,,,,:, g 0><>> 4200 u g/m3><'> 80 PPby91-20-3 128 Naphthalene >__`N ' '8 10 ' s108-88-3 92 Toluene 1600 PPby < 6000 u /m34 . 3500 u /m3106 m� -X lene >99300 <> > 800 PPby : 3500 u g/m39547 6 106 o- lene 22 80 PPby 1A :.:......... 0 572000 3500 u /m31330-20-7 106 X lenes(total) 80 PPby ............... ........................ ............ ........................... CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... ......................... 460-00-4 4-Bromofluorobenzene 0% > > 70-130% ......................... ......................... ......................... ......................... CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q ........................... C5-C8 Aliphatic 5.334E)0(l; ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 5.47 1701)Or >>ppbv J C5-C8 Aliphatic 5.63 '9. O <.ppbv J .............. ........................... ........................... C5-C8 Aliphatic 5.73GOOI' <; ppbv J C5-C8 Aliphatic 5.934 ( I< ppbv J ........................... ........................... C5-C8 Aliphatic 6.09 1800D<i ppbv J 420 C5-C8 Aliphatic 6.53 ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 6.59 3�0..... ppbv J C5-C8 Aliphatic 6.63 3 (? > ; ppbv J C5-C8 Aliphatic 6.83 500(7i>>i '<> ppbv J C5-C8 Aliphatic 6.93 10004 »> ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 7.32GO (? <>» ppbv J C5-C8 Aliphatic 7.46 1O1 ; ppbv J ........................... ........................... C5-C8 Aliphatic 7.94 18{)00> <; < ppbv J C5-C8 Aliphatic 8.01300Q;> ;; ppbv J C5-C8 Aliphatic 8.12 17OQ0 > i ppbv J .::......................... ........................... C5-C8 Aliphatic 8.22 ;1040 ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 8.41 19000: ; ppbv J C5-C8 Aliphatic 8.55 60 ; > < ppbv J st0ot<C5-C8 Aliphatic 8.66 > ppbv J C5-C8 Aliphatic 8.73 300(1; ppbv J ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 2 of 3 Client Sample ID: SVE Lab Sample ID: E91703-2 Date Sampled: 05/18/01 Matrix: AIR-Air Date Received: 05/23/O1 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q ........................... ........................... C5-C8 Aliphatic 9.35 18(H3 __»< ppbv J CS-C8 Aliphatic 9.552b43 ppbv J ....:.:.................... ........................... ........................... C5-C8 Aliphatic 9.65SQ(3i<> < ppbv J C5-C8 Aliphatic 9.71 Jb00 ;> ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 9.89 SSU(f> i :::`ppbv J C5-C8 Aliphatic 9.98 50(3 > ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 10.18 59 < ppbv J C5-C8 Aliphatic 10.299t0<s «< ppbv J ...........:............... ........................... ........................... C5-C8 Aliphatic 10.43 140 ppbv J C5-C8 Aliphatic 10.52 1SOQ ppbv J .......................... C5-C8 Aliphatic 10.63 I2Q0< ppbv J 7{H C5-C8 Aliphatic 10.77 ppbv J C5-C8 Aliphatic 10.86 7300<<< ` >' ppbv J C5-C8 Aliphatic 10.93 37( <> ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 10.99 214(D ;'` ppbv J C5-C8 Aliphatic 11.07 54 ;; ppbv J ....:...................... ........................... ........................... C5-C8 Aliphatic 11.14 25Q1i >< '< ':ppbv J C5-C8 Aliphatic 11.23 fSOQ;<>_<` ppbv J ........................... ........................... .................... C5-C8 Aliphatic 11.32 10( 1 ; < _ ppbv J C5-C8 Aliphatic 11.66 28fl ppbv J C5-C8 Aliphatic 11.93 170ts ppbv J C5-C8 Aliphatic 12.00 90.0.0. ; ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 12.12 ;; ppbv J C5-C8 Aliphatic 12.25 7 {�(3 ppbv J ......................:.... ........................... ........................... C5-C8 Aliphatic 12.4520a ppbv J C5-C8 Aliphatic 12.53 59.0... ; ppbv J ........................... .......................... ........................... C5-C8 Aliphatic 12.81Q ppbv J C5-C8 Aliphatic 12.95 2�U ;` ppbv J ..........:.:.............. ........................... ........................... C5-C8 Aliphatic 13.01 120U %; ppbv J C5-C8 Aliphatic 13.10 500_ ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 13.18 2800.0<<; j ppbv J C5-C8 Aliphatic 13.37 94U4 >> ppbv J ........................... ........................... ........................... C5-C8 Aliphatic 13.51 lfODa<''<> ppbv J C5-C8 Aliphatic 13.65 4;IOi <; ; >> ppbv J ...:.....:................. ........................... ........................... C5-C8 Aliphatic 13.84 22c> <> ><ppbv J C5-C8 Aliphatic 13.92 140O0> ; ppbv J .........................:. ........................... ........................... C5-C8 Aliphatic 14.02 2(OQ ; ppbv J C5-C8 Aliphatic 14.14 ;G50(3'>a;'>;' ppbv J .................:......... ........................... ........................... C5-C8 Aliphatic 14.33 200(; ; <;;ppbv J C5-C8 Aliphatic 14.44 '2:7 ; ppbv J ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 3 of 3 Client Sample ID: SVE Lab Sample ID: E91703-2 Date Sampled: 05/18/O1 Matrix: AIR-Air Date Received: 05/23/O1 Method: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanough Road, Hyannis, MA CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q ........................... .......................... C5-C8 Aliphatic 14.61 350() ppbv J C5-C8 Aliphatic 14.77 2 < »'>`j ppbv J :.......................... ........................... ........................... C5-C8 Aliphatic 14.96 65()( <s ppbv J C5-C8 Aliphatic 15.91 48tQ ; < ppbv J ........................... ........................... ........................... C9-C 10 Aromatic 17.08 OOtI > < i ppbv J ........................... ........................... ........................... ppbv J C9-C10 Aromatic 17.81 3t1(# ; .........:................. ........................... ........................... C9-C10 Aromatic 17.98 13(N)q ; !>; ppbv J. C9-C10 Aromatic 18.03 X.M{1Q; ' ppbv J ........................... ........................... C9-C10 Aromatic 18.16 56 ;s>< >ppbv J ........................... ........................... ........................... C9-C10 Aromatic 18.43 w.34 ppbv J ........................... ........................... ........................... C9-C 10 Aromatic 18.7880f# > < ppbv J ...:........ a : <To s ................................::. ............................................... ................... lacs.:;::> by ............................... PP ota1.C9.C12.Ali ...afics.......................:............... 0><> <» u /m3 P :: .::::::: g X. '..:.a1: ::..:1D:..:...:.:eta[.cs:::::::::::::::::..:.::........::::.: /()4.> b PP Total C9 l0"A—m.t cs< » «' 222: <: > <` u /m3 .................:........................................................................ .............:::........ PP (a)Result is from Run#2 (b)No peaks found for Total C9-C12 Aliphatics ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 495 TECHNOLOGY CENTER WEST • BUILDING ONE T� MARUBOR(X JGH,MA 01752 ACCuiEBT GUOTE 0: TEL:SW 481.62W - FAX:508.481.7753 CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES RVi P T �yACn rJC1WIC1 �Liq�I�•/ $k-�OW DW- DRINKING WATER NAME P 04ECT LA GW- GROUND WknEA RESS CATION WW a WASTE y►'► TER A '�� �� Y hrIAAS' . /MA. 90. SOiL C STATE ZIP 01JQJECT NO. r SL- SLUDGE �.�1t �6�tZ5�Z� d 0. uro SEND REPORT TO:P ' OTHER FAX* - ACCUTEST COLLECTION PRESERVA 4;k. SOLID SAMPLE 4 FIELD ID/POINT OF COLLECTION DATE TIME SA gPPLED 9 ' 2 11111111 LAB USE ONLY 'L ( 1- DATA TURNAROUND INFORMATION DATA DELIVERABLE INFpRMATK)N COMMENTSIREMARKS fk 14 DAYS STANDARD APPROVED BY: ,Bk-S-FANDARD O 7 DAYS RUSH LT COMMERCIAL"B" O 48 HOUR EMERGENCY L:l DISK DELIVERABLE O OTHER O STATE FORMS 14 DAY TURNAROUND HARDCOPY,EMERGENCY OR RUSH IS FAX O OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDIN0 COURIER DELIVERY REL SHED BY SAMPLER: DATE TIME: RECEIV SY: RELLNO ED Y: OAT TIM RECEIVED ir S-N-4 1. o�.e. 2. 1 g.: 2. RECINQUISHE,q BY: DATE TIME: REC ED BY. REUNQUISHRO Dr. Mftrfm [AWED BYI 3. �� 3. 4. [RFRlELlN0k*SHEtfP_- DATETI • N REC ED BY: SEAL ..... PR RVB BBE WHER APPLICABLE ON IC[ TEMPBMTURS . 5. O O �_ _C TAU' . u �tiaiw Vr li U '1'V1� Y ACCUTEST JOB III: N UACCUTEST 495 TECHNOLOGY CENTER WEST • BUILDING ONE MARLBOROUGH,MA 01752 ACCUTEST QUOTE#: TEL:508-481-6200 • FAX 508.481-7753 CLIENT INFORMATION h FACILITY INFORMATION i. ANALYTICAL INFORMATION 7 i <<:k�: MATRIX CODES �^ DW• DRINKIK Qa�o�1 �2t/it,C�S n 2PoR�T�.�l CVAro ,seotl/Ic-e S A��✓ �f70�� wATIO: '� j NAMES-^ nn ` PRg4ECT AME n ( GW• GROUNI�;K ��]. Lle,�,a?3 nl j ✓C_ ��o yn/✓CJ� K9/�"J, WATER:: r A'DpRESS CATION WW• WASTE''::": �7cJ�Sryl l+ Nil A O t SO• 80ATERIL ! C STATE 21P Of- OIL .Ke BP.►�� Y. SL. SLUDGE:. SEND REPORT TO: O / LIO• OTHER PHONE# - o- (1J FAX# UOUID...':ji SOL•OTHER, COLLECTION m PRESERVATION O. SOLID ACCUTEST SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLED = LAB USE ONLI BY: .s r?,l Ala Eva t x DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION '' �r ' COMMENTS/REMARKS 'p $t 14 DAYS STANDARD APPROVED BY: ANDARD Y: ❑ 7 DAYS RUSH COMMERCIAL"B" O 48 HOUR EMERGENCY ❑ DISK DELIVERABLE O OTHER O STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVERYk RELI (SHED BY SAMPLER: DATE TIME: RECEIV BY: RELING SHED Y: DAT TIM : RECEIVED BY: 1• �i� 1- S- �Q-d 1. O�i�t�C. 2. O 2. RECINOUISHED BY: DATE TIME: RECEIVED BY: RELINQUISHED BY: TI E: RECEIVED BY: 3. 3. 4. 4• FRECINQUISHED BY: DATE TIME: RECEIVED BY: SEAL I PRESERVE WHERE APPLICABLE ON ICE TEMPERATURE`. 5. 0 _ 0 C Jun-07-01 02:25pm From- T-333 P-01/07 F-319 ®ACCITEST 2235 Route 130, Rnlding 0, Dayton, New Jersey 08910 WWW.ACCt1TEST.COM j FAX TRANSMISSION Date: 6 1 1101 COVER PAGE Number of pages,including:over: TO: �.� FROM: Marie Rutsky _A:�t%..G, COMPANY: NM A COMPANY: ACCUTEST LABS Phone: Phone: 1732)329-0200(blO) Fax: `(3 L I4 Fax: (732)329-3499 13480 Email: marier(aaccut est.com URGENT R FOR REVIEW _REPLY ASAF Remarks: Accutest cannot be held accountable for the security of the data once media containing the data has left the possession or control of Accutest. Analytical data transmitted via facsimile should be conside►ed preliminary. I N,-w J-ww. •Fresh Pontls Corporate Vinage•Building B•2235 Route 130•Dayton.NJ 08010-tel:732.329.0200•lax.732.3254499•mrp!/www.accutest.com Jun-07-01 02:25pm From- T-333 PIVOT F-319 Aceutest Laboratories Report of Analysis Page 1 of 3 Client Sample ID: AS + SVE Date Sampled: 05/18/01 Lab Sample ID: E91703-1 Date Received: 05/23/01 Matti= AIR-Air Percent Solids: n/a Method: TO-14/TO-15 Project: GSCMAli:96925028 1140 Iyanough Road,Hyannis,MA File lD DF Analyzed By Prep Date 'I'VW Batch Analytical Batch Run#1 Q10989.D 800 05/31/01 WG n/a Ida VQ415 Run#2 Q10997_D 2000 05/31/01 WG n/a 11/a VQ415 CAS No. MW Compound Result RL Units Q Result RL Units 7143-2 78 Benzene 28200 160 ppbv 90000 510 ug/m3 100-41-4 106 Ethylbenzene 29700 160 ppbv 129OW 690 ug/m3 1634044 88 Medryl Teri Buty1 Ether 72900 a 4000 ppbv 2620003 14000 ug/un3 91-20-3 128 Naphthalene 2800 160 ppbv 14600 840 ug/m3 108-89-3 92 y Toluene 204000 a 4000 ppbv 768000 a 15000 ug/m3 106 m,p-Xylene 109000 a 4000 ppbv 472000 a 17000 ug/m3 95-47-6 106 o-Xylene 39400 a 4000 ppbv 1710002 17000 ug/m3 1330-20-7 106 Xylenes(total) 14900011 4000 ppbv 6460000 17000 u9/m3 CAS No. Surrogate Rewver<es Run#i Run#2 Lltnits 460-00-4 4-11mmofluorobenzene 101% 88% 70-130% CAS No. Tentatively Identified Compounds R.T. Est. Conc. 'Units Q Pentane 5.34 7200 _?pbv J C5-C8 Aliphatic 5.48 2100 ?pbv J C5-C8 Aliphatic 5.64 1100 ppbv J CS-C8 Aliphatic 5.75 3000 ppbv J C5-C8 Aliphatic 6.11 2100 ppbv J CS-C8 Aliphatic 6.54 470 ppbv J C5-C8 Aliphatic 6.65 410 ppbv J C5-C8 Aliphatic 6.85 5900 ppbv J C5-C8 Aliphatic 7.34 7900 ppbv J C5-C8 Aliphatic 7.48 22M ppbv J C5-C8 Aliphatic 7.82 8000 ppbv J C5-C8 Aliphatic 7.96 2000 ppbv J C5-C8 Aliphatic 8.02 2600 ppbv J CS-CS Aliphatic 8.14 2000 ppbv J C5-C8 Aliphatic 8.24 1200 ppbv J C5-C8 Aliphatic 8.43 2200 ppbv J C5-C8 Aliphatic 8.57 630 ppbv J C5-C8 Aliphatic 8.68 5600 ppbv J C5-C8 Aliphatic 8.75 3800 ppbv J C5-C8 Aliphatic 9.95 1000 ppbv J CS-CS Aliphatic 9.36 13000 ppbv J ND Not detected J = Indicates an e:timated value RL = Reporting Limit B = Indicates analyte found in associated method blank E =Indicates value exceeds calibration range N = Indicates pre:-umpuve-vWcmo of a compound Jun-07-01 02:26pm From- T-333 P.03/07 F-310 Accutest Laboratories Report of Analysis Page 2 of 3 Client Sample ID: AS + SVE Lab Sample ID: E91703-1 Date Sampled: 05/18/01 bfatri= AIR-Air Date Received: 05/23/01 blethod: TO-14/TO-15 Percent Solids: n/a Project: GSCMAH.96925028 1140 Iyanough Road,Hyannis.MA CAS No. Tentatively Identified Compounds R.T. Est.Conc. Units Q C5-C8 Aliphatic 9.57 2900 ppbv J C5-C8 Aliphatic 9.67 2500 I'pbv J C5-C8 Aliphatic 9.72 6700 I)pbv J C5-C8 Aliphatic 9.92 36000 ppbv J C5-C8 Aliphatic 10.00 20000 ppbv J C5-C8 Aliphatic 10.20 37000 ppbv J C5-C8 Aliphatic 10.28 5300 ppbv J C5-C8 Aliphatic 10.45 9500 ppbv J C5-C8 Aliphatic 10.54 11000 ppbv J C5-C8 Aliphatic 10.64 66000 1)pbv J C5-C8 Aliphatic 10.88 5100 ppbv J C5-C8 Aliphatic 10.95 29000 1?pbv J CS-C8 Aliphatic 11.01 17000 1.)pbv J C5-C8 Aliphatic 11.09 4000 iypbv J C5-C8 Aliphatic 11.16 1600 ppbv J C5-C8 Aliphatic 11.25 4700 •?pbv J C5-C8 Aliphatic 11.34 10000 ppbv J C5-C8 Aliphatic 11.68 18000 ppbv J C5-C8 Aliphatic 11.74 1200 ppbv J C5-C8 Aliphatic 11.94 12000 ppbv J C5-C8 Aliphatic 12.02 19000 ppbv J C5-C8 Aliphatic 12.26 4700 ppbv J C5-C8 Aliphatic 12.35 1400 ppbv J C5-C8 Aliphatic 12.46 3000 ppbv J C5-C8 Aliphatic 12.56 42000 ppbv J CS-C8 Aliphatic 12.88 1600 ppbv J CS-C8 Aliphatic 12.97 14000 ppbv J CS-C8 Aliphatic 13.02 8100 ppbv J C5-C8 Aliphatic 13.11 2700 ppbv J C5-C8 Aliphatic 13.20 19000 ppbv J CS-CS Aliphatic 13.39 4700 ppbv J C5-C8 Aliphatic 13.52 11000 ppbv J C5-C8 Aliphatic 13.66 1900 "ppbv J C5-C8 Aliphatic 13.72 850 ppbv J C5-C8 Aliphatic 13.78 1300 ppbv J C5-C8 Aliphatic 13.85 1600 ppbv J C5-C8 Aliphatic 13.94 11000 ppbv J CS-CS Aliphatic 14.02 2200 ppbv J C5-C8 Aliphatic 14.15 4600 ppbv J CS-C8 Aliphatic 14.28 850 ppbv J ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyze found in associated method blank $ = Indicates value exceeds calibration range N = Indicates preimnptive evidence of a compound Jun-OT-01 02:26pm From- T-333 P-04AT F-319 Accutest Laboratories r Report of Analysis Page 3 of 3 Client Sample ID: AS + SVE 05/18/01 Lab Sample ID: E91703-1 Date m ' Received: OSl23/ Matrix; AIR-Air Date 111 Method: TO-14/TO-15 percent Solids: n/a Project: GSCMAH:96925028 1140 Iyanou&Road, Hyannis,MA CAS No. Tentatively Identified Compounds R.T. Est.Conc. 'Units Q C5-C8 Aliphazic 14.34 1300 FVbv J C5-C8 Aliphatic 14.45 1900 Epbv J CS-C8 Aliphatic 14.62 2700 ppbv J C5-C8 Aliphatic 14.78 1600 l-pbv J C5-C8 Aliphatic 14.97 4900 l►pbv J C5-C8 Aliphatic 15.10 800 ppbv J C5-C8 Aliphatic 15.19 1300 ppbv J C5-C8 Aliphatic 15.34 1600 1►pbv J C5-C8 Aliphatic 15.91 3600 lypbv J C5-C8 Aliphatic 16.13 1000 1)pbv J C9-C12 Aliphatic 16.60 1700 ppbv J C9-CIO Aromatic 17.09 1800 1)pbv J C9-C12 Aliphatic 17.26 1200 ppbv J C9-C12 Aliphatic 17.50 1100 ppbv J C9-C10 Aromatic 17.82 4200 ppbv J C9-CIO Aromatic 17.98 16000 ppbv J C9-CIO Aromatic 18.04 6000 1?pbv J C9-C10 Aromatic 18.16 7100 I?pbv J C9-C12 Aliphatic 18.23 1100 1?pbv J C9-CIO Aromatic 18.43 4700 i?pbv. J C9-C10 Aromatic 18.78 15000 ppbv J C9-C10 Aromatic 19.46 2700 apbv J C9-CIO Aromatic 19.77 1500 ppbv J Total C5-C8 Aliphatics 542000 ppbv Total C5-C8 Aliphatics 2060000 a8/m3 Total C9-C12 Aliphatics 5100 ppbv Total C9-C12 Aliphatics 31100 ug/m3 Total C9-00 Aromatics $9000 ppbv Total C9-CIO Aromatics 306000 u9/tn3 Total TIC. Volatile 613210 ppbv (a)Result is from Run#2 ND Not detected J =Indicates an estimated value RL Reporting Limit B = Indicates analyze found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Jun-07-01 02:27pm From- T-333 P.05/07 F-319 Accutest Laboratories Report of Analysis Page 1 of 3 Client Sample ID: SVE Lab Sample ID: E91703-2 Date Sampled: 05/18/01 Matrix; AIR-Air Date Received: 05/23/01 Method: TO-14/TO-15 Percent Solids: t✓a Pgect, GSCMAH-96925029 1140 lyanough Road,Hyannis,MA )File ID DF Analysed By prep Date )'rep Batch Analytical Batch Run#1 Q10990.1) 4000 OS/31/01 WO n/a I]/a VQ415 Run#2 Q10998-D 8000 05/31/01 WO n/a n/a VQ415 CAS No. M'W Compound Result RL Units Q Result RL Units 71-43-2 78 Benzene 319M 800 ppbv 102000 2600 ug/m3 10041-4 106 Ethylbe=ne 30700 800 ppbv 133000 3500 ug/m3 1634-04-4 88 Methyl Tert Butyl Ether 79300 800 ppbv 285000 2900 ug/m3 9120-3 128 Naphthalene NYC 800 ppbv ND 4200 ug/m3 108-88-3 92 Toluene 3180008 1600 ppbv 1200000 a 6000 ug/m3 106 m.p-Xylene 99300 900 ppbv 430000 3500 ug/m3 95-47-6 106 o-Xylene 32200 800 ppbv 140000 3500 ug/m3 1330-20-7 106 Xylenes(total) 132000 800 ppbv I 572000 3500 ug/m3 CAS No. Surrogate Recoveries Run#i Run#2 Limits 460-004 4-Bromofluorobenzene 90% 90% 70-130% CAS No. Tentatively Identified Compounds R.T. Eat. Conc.; Units Q i C5-C8 Aliphatic 5.33 70000 ! ppbv J C5-C8 Aliphatic 5.47 17000 ppbv J C5-C8 Aliphatic 5.63 9100 ppbv J C5-C8 Aliphatic 5.73 26000 ppbv J CS-C8 Aliphatic 5.93 14000 ppbv J, C5-C8 Aliphatic 6.09 18000 ppbv J C5-C8 Aliphatic 6.53 4200 ppbv J C5-C8 Aliphatic 6.59 2200 ppbv J C5-C8 Aliphatic 6.63 3300 ppbv J C5-C8 Aliphatic 6.93 54000 ppbv J C5-C8 Aliphatic 6.93 120000 I ppbv J C5-C8 Aliphatic 7.32 76000 ppbv J C5-C8 Aliphatic 7.46 19000 ppbv J C5-C8 Aliphatic 7.94 19000 ppbv J C5-C8 Aliphatic 8.01 23000 ppbv J CS-C8 Aliphatic 8.12 17000 ppbv J C5-C8 Aliphatic 8.22 11000 ppbv J C5-C8 Aliphatic 8.41 19000 ppbv J C5-C8 Aliphatic 8.55 5600 ppbv J C5-C8 Aliphatic 8.66 51000 ppbv J C5-C8 Aliphatic 8.73 36000 ppbv J ND = Not detected J = indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exomds calibration range N = Indicates presumptive evidence of a compound Jun-07-01 02:27pm From- T-333 P.06/U( r-Jia Accutest Laboratories RepOrt Of Analysis Page 2 of 3 Client Sample ID: SVE liab Sample ID: E91703-2 Date Sampled: 05/l8/O1 Date Received: 05/2310l Matrix: AIR-Air Method: TO.14/TO-15 Percent Solids: n/a Project: CSCMAH:96925028 1140 Iyanough Road,Hyannis,MA CAS No. Teptatively Identified Compounds R.T. Est. Cone, Units Q C5-C8 Aliphatic 9.35 18000 l)pbv J C5-C8 Aliphatic 9.55 4200 ppbv J CS-C8 Aliphatic 9.65 3500" ppbv J CS-CS Aliphatic 9.71 9600 ppbv J C5-C8 Aliphatic 9.89 55000 ppbv J C5-C8 Aliphatic 9.98 31000 1?pbv J CS-C8 Aliphatic 10.18 59000 1:)pbv J CS-C8 Aliphatic 10.29 6900 1?pbv J CS-C8 Aliphatic 10.43 14000 :?pbv J C5-C8 Aliphatic 10.52 18000 :?pbv J C5-C8 Aliphatic 10.63 120000 ppbv J C5-C8 Aliphatic 10.77 3700 ppbv J C5-C8 Aliphatic 10.86 7300 ppbv J C5-C8 Aliphatic 10.93 37000 ppbv J C5-C8 Aliphatic 10.99 21000 ppbv J C5-C8 Aliphatic 11.07 5400 ppbv J C5-C8 Aliphatic 11.14 2500 ppbv J C5-C8 Aliphatic 11.23 6500 ppbv J CS-CS Aliphatic 11.32 11000 ppbv J CS-C8 Aliphatic 11.66 28000 ppbv J C5-C8 Aliphatic 11.93 17000 ppbv J C5-C8 Aliphatic 12.00 29000 ppbv J C5-C8 Aliphatic 12.12 3000 ppbv J C5-C8 Aliphatic 12.25 7100 ppbv J C5-C8 Aliphatic 12.45 4200 ppbv J CS-C8 Aliphatic 12.53 59000 ppbv J C5-C8 Aliphatic 12.81 20000 ppbv J C5-C8 Aliphatic 12.95 21000 ppbv J C5-C8 Aliphatic 13.01 12000 ppbv J C5-C8 Aliphatic 13.10 3500 ppbv J C5-C8 Aliphatic 13.18 28000 ppbv J C5-C8 Aliphatic 13.37 9400 ppbv J C5-C8 Aliphatic 13.51 16000 ppbv J C5-C8 Aliphatic 13.65 4100 ppbv J C5-C8 Aliphatic 13.84 2200 ppbv J C5-C8 Aliphatic 13.92 14000 ppbv J C5-C8 Aliphatic 14.02 2700 ppbv J C5-C8 Aliphatic 14.14 6500' ppbv J C5-C8 Aliphatic 14.33 _ 2000 ppbv J C5-C8 Aliphatic 14.44 2700 ppbv J ND Not detected J = Indicates an e!;timated value RL = Repotting Limit B = Indicates analyte found in associated method blank lr =Indicates value exceeds calibration range N = Indicates pmnumptive evidence of a compound Jun-07-01 02:27pm From- T-333 P.07/o7 F-318 Accutest Laboratories Report of Analysis Page 3 of 3 Client Sample ID: SVE Lab Sample ID: E91703-2 Date Sampled: OS/18/Ol Matrim AIR_Air Date Received 05/23/0 t moo& TO-14/TO-15 Percent Solids: n/a Project: GSCMAH:96925028 1140 Iyauough Road,Hyannis,MA CAS No. Tentatively Identified Compounds R.T. Est.Conc. Units Q C5-C8 Aliphatic 14.61 3500 t)pbv J CS-CS Aliphatic 14.77 2000 j3pbv J CS-C8 Aliphatic 14.96 6500 1?pbv J C5-C8 Aliphatic 15.91 4800 I?pbv J C9-C10 Aromatic 17.08 2000 upbv J C9-CIO Aromatic 17.81 3500 .apbv J C9-CIO Aromatic 17.98 13000 ppbv J C9-CIO Aromatic 18.03 5400 ppbv J C9-CIO Aromatic 18.16 5600 ppbv J C9-C10 Aromatic 18.43 3400 ppbv J C9-Cl0 Aromatic 18.78 9800 ppbv J Total C5-C8 Aliphatics 1360000 ppbv Total C5-C8 Aliphatics 5170000 ug/m3 Total C9-C12 Aliphatics b 0 ppbv Total C9-C12 AIO Mtics b 0 ug/m3 Total C9-CIO Aromatics 42700 ppbv Total C9-CIO Aromatics 222000 ug/m3 Total TIC,Volatile 1397900 ppbv (a)Result is from Runt!2 (b)No peaks found for Total C9-Cl2 Aliphatics ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound TOXIC AND HAZARDOUS MATERIALS REGISTRATION FORM o 951&4 Mail To: NAME OF BUSINESS: ` _ Board of Health MAILING ADDRESS: - ` Town of Barnstable TELEPHONE NUMBER: 16�zzzl 4z66'� P.O. Box 534 CONTACT PERSON: Hyannis, MA 02601 Does your firm store any of the toxic or hazardous materials listed below, either for sale or for your own use, in quantities totalling, at any time, more than 50 gallons liquid volume or 25 pounds dry weight? YES V NO This form must be returned to the Board of Health regardless of a yes or no answer. Use the enclosed envelope for your convenience. If you answered YES above, please indicate if the materials are stored at a site other than your mailing address: ADDRESS: TELEPHONE: LIST OF TOXIC AND HAZARDOUS MATERIALS The Board of Health has determined that the following products exhibit toxic or hazardous characteristics and must be registered when store ' Please put a check beside each product that you store: Antifreeze (for gasoline or coolant systems) Drain cleaners Automatic transmission fluid Toilet cleaners Engine and radiator flushes Cesspool cleaners Hydraulic fluid (Including brake fluid) Disinfectants P"' Motor o,Is/waate oils Road Salt (Halite) Gasoline, Jet fuel Refrigerants Dig l fuel,d4xesent,7#2 heatingoil Pesticides (insecticides, herbicides, Other petroleum products: grease, lubricants rodenticides) Degreasers for engines and metal Photochemicals (fixers and developers) Degreasers for driveways & garages Printing ink Battery acid (electrolyte) Wood preservatives (creosote) Rustproofers Swimming pool chlorine Car wash detergents Lye or caustic soda Car waxes and polishes Jewelry cleaners Asphalt & roofing tar Leather dyes Paints, varnishes, stains, dyes Fertilizers (if stored outdoors) Paint & lacquer thinners PCB's Paint & varnish removers, deglossers Other chlorinated hydrocarbons, Paint brush cleaners (inc. carbon tetrachloride) Floor & furniture strippers Any other products with "Poison" labels Metal polishes (including chloroform, formaldehyde, Laundry soil & stain removers hydrochloric acid, other acids) (including bleach) Other products not listed which you feel may Spot removers & cleaning fluids be toxic or hazardous (please list): (dry cleaners) Other cleaning solvents Bug and tar removers Household cleansers, oven cleaners White Copy-Health Department/ Canary Copy-Business 'r TOWN OF BARNSTABLE MPIJANCE: CLASS: 1.Marine,Gas Stations,Repair satisfactory 2.Printers BOARD OF HEALTH 3.Auto Body Shops O unsatisfactory- 4.Manufacturers COMPANY ' (see"Orders") 5.Retail Stores 6.Fuel Suppliers ADDR�E•-SS Class: 7.Miscellaneous � + ' QUANTITIES AND STORAGE (IN=indoors; OUT=outdoors) MAJOR MATERIALS Case lots Drums Above Tanks Underground Tanks IN OUT IN OUTI IN OUT #&gallons Age ITest B Fuels: Gasoline,Jet Fuel (A) 4 Diesel,Kerosene, #2 (B) �`?� � Heavy Oils: t waste motor oil (C) new,motor oil (C) transmission/hydraulicf-'�- Synthetic Organics: degreasers Miscellaneous: DISPOSAIJRECLAMATION REMARKS: y9l 1. Sanitary Sewage 2. Water Supply t?' � O Town Sewer QfPublic ` XOn-site OPrivate p J 3. Indoor Floor Drains YES 4 NO !/ Holding tank: MDC O Catch basin/Dry well O On-site system 4. Outdoor Surface drains:YES NO Y ORDERS: O Holding tank: MDC v�� O Catch basin/Dry well -da24 O On-site system 5.Waste Transporter Name of Hauler Destination Waste Product YES I No 2. /� Person s erviewed Inspector Date