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HomeMy WebLinkAbout1140 IYANNOUGH ROAD/RTE132 - HAZMAT (5) 1 FFin � h 141, . ! t A 6l a � " a .i y M 1, d" 4i' ,J'tdw.. .W` ) w 4•'� � y`,. � G-� 4 3 n Y � 4 , �.. LOU t a S�Y 1 t r '.i i x s d. ON ! �.a 4 x�C ..:i✓"`: ,,ar >` r W 1 '+t ;4 r �:. �; i " `nd. t irr�. 1 _{ e' - ;1 toglow _ #t s r 7 r a �fw All 1 ;Y; ti 'i •,'° alp cy r �'` z fir_ :, a y q. +' f Geologic 0 C Services Corporation science,engineering&technology Waybill#22141751450 July 8, 2004 Massachusetts Department of Environmental Protection Southeast Regional Office Bureau of Waste Site Cleanup Attn: Ms.Laura Stanley 20 Riverside Drive Lakeville,MA 02347 Re: Release Abatement Measure Completion Report Former Texaco Service Station#100083 1140Iyannough Road Hyannis,Massachusetts RTN 4-11301 Tier IC Permit#100556 ACO-SE-03-3S-002 Dear Ms. Stanley: Geologic Services Corporation(GSC),on behalf of Motiva Enterprises LLC(Motiva),has prepared this Release Abatement Measure(RAM)Completion Report and associated Massachusetts Department of Environmental Protection(MA DEP)Form BWSC-106 for the above referenced site. This report summarizes the removal of underground storage tanks(USTs),associated UST dispenser equipment,fuel oil UST,and hydraulic lift,as well as the cleaning of an oil/water separator on the subject property. The contact at Motiva responsible for overseeing the response actions associated with this site is Mr.David B. Weeks,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590;(845)462-5225. The attached documents have been prepared under the direction of Licensed Site Professional(LSP)Mr.Scott K.Parker(LSP# 9969)of GSC. The next scheduled regulatory submittal is a Phase IV-Final Inspection Report,anticipated for completion on or before November 1,2004. Should you have any questions or concerns,please do not hesitate to contact Mr.David B.Weeks of Shell Oil Products US(SOPUS)at(845)462-5225 or the undersigned. Sincerely, Geologic Services Corporation 'V Michael C.Bricher Moira S.Walker Project Manager Senior Environmental Scientist cc: Mr.David B.Weeks,SOPUS,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590 Mr.John Klimm,Hyannis Town Administrator,367 Main Street,Hyannis,MA 02601 Mr.Thomas McKean,Hyannis Board of Health,200 Main Street,Hyannis,MA 02601 Mr.Tom Rento,Kimco Realty Corp, 11 Computer Drive West,Suite 210,Albany,NY 12205 Mr.John Roche,The Flately Company,P.O.Box 859206,Braintree,MA 02185 Prime 132,LLC,297 North Street,Hyannis,MA 02601 Enclosures Ref.#000509C Rpt_RAMC 07-04 Providing Environmental Management Solutions to Business and Industry Since 1982 A 100% Employee-Owned ESOP Company 15 Bonazzoli Avenue• Hudson, MA 01749 • Tel: 978.568.8740 1 800.522.8740 • Fax: 978.568.9316 www.gsc-global.com r . - Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup . BWSC106 Release Tracking Number RELEASE ABATEMENT MEASURE (RAM) TRANSMITTAL FORM 4F - 11301 4. < Pursuant to 310 CMR 40.0444-0446(Subpart D) A. SITE LOCATION: 1. Site Name/Location Aid: Texaxo Service Station No. 100083 2. Street Address: 1140 Iyannough Road 3. City/Town: Hyannis 4. ZIP Code: 02060 ® 5. Check here if a Tier Classification Submittal has been provided to DEP for this disposal site. a. Tier IA b. Tier IB © c. Tier IC d. Tier II 6.If a Tier.l Permit has been issued,provide Permit Number: 100556 B.THIS FORM IS BEING USED TO: (check all that apply) 1. List Submittal Date of Initial RAM Written Plan(if previously submitted): (mm/dd/yyyy) 2. Submit an Initial Release Abatement Measure(RAM)Plan. Qa. Check here if this RAM Plan received previous oral approval from DEP as a continuation of a Limited Removal Action(LRA). b. List Date of Oral Approval: (mm/dd/yyyy) 3. Submit a Modified RAM Plan of a previously submitted written RAM Plan. 4. Submit a RAM Status Report. 5. Submit a RAM Completion Statement. 6. Submit a Revised RAM Completion Statement. 7. Provide Additional RTNs: a. Check here if this RAM Submittal covers additional Release Tracking Numbers(RTNs). RTNs that have been previously linked to a Primary Tier Classified RTN do not need to be listed here. This section is intended to allow a RAM to cover more than one unclassified RTN and not show permanent linkage to a Primary Tier Classified RTN. b. Provide the additional Release Tracking Number(s) a _ ❑ _ covered by this RAM Submittal. (All sections of this transmittal form must be filled out unless otherwise noted above) Revised: 11/04/2003 Page 1 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number ' TRANSMITTAL FORM 4❑ - 11301 �aeuewuomuaaeenm:"<ao-xae.+eec•>:, Pursuantto 310 CMR 40.0444-0446(Subpart D) C. RELEASE OR THREAT OF RELEASE CONDITIONS THAT WARRANT RAM: 1. Identify Media Impacted and Receptors Affected: (check all that apply) ❑ a. Air ❑ b. Basement ❑ c. Critical Exposure Pathway 91 d. Groundwater ❑ e. Residence ❑ f. Paved Surface ❑ g.Private Well ❑ h. Public Water Supply ❑ i. School ❑ j. Sediments ® k. Soil ❑ I. Storm Drain ❑ m. Surface Water ❑ n. Unknown ❑ o. Wetland ❑ p. Zone 2 ❑ q. Others Specify: 2. Identify all sources of the Release or Threat of Release,if known: (check all that apply) ❑ a. Above-ground Storage Tank{AST) ❑ b. Boativessel ❑ c. Drums ❑ d.Fuel Tank ❑ e. Pipe/Hose/Line ❑ f. Tanker Truck ❑ g. Transformer ® h. Under-ground Storage Tank(UST) ❑ i. Vehicle ❑ j. Others Specify: 3. Identify Oils and Hazardous Materials Released: (check all that apply) m a. Oils ❑ b. Chlorinated Solvents ❑ c.Heavy Metals ❑ d. Others Specify: D. DESCRIPTION OF RESPONSE ACTIONS: (check all that apply,for volumes list cumulative amounts) ❑ 1. Assessment and/or Monitoring Only ❑ 2. Temporary Covers or Caps ❑ 3. Deployment of Absorbent or Containment Materials ❑ 4. Temporary Water Supplies ❑ 5. Structure Venting System ❑ 6. Temporary Evacuation or Relocation of Residents W1 7. Product or NAPL Recovery ❑ 8. Fencing and Sign Posting ❑ 9. Groundwater Treatment Systems ❑ 10. Soil Vapor Extraction ❑ 11. Bioremediation ❑ 12. Air Sparging ❑ 13. Excavation of Contaminated Soils ❑ a. Re-use, Recycling or Treatment ❑ i.On Site Estimated volume in cubic yards ❑ ii.Off Site Estimated volume in cubic yards iia.Receiving Facility: Town: State: iib.Receiving Facility: Town: State: iii. Describe: Revised: 11/04/2003 Page 2 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 f.. Release Tracking Number RELEASE ABATEMENT MEASURE (RAM) .t . TRANSMITTAL FORM 4a _ 11301 E Pursuant to 310 CMR 40.0444-0446(Subpart D) D. DESCRIPTION OF RESPONSE ACTIONS(cont): (check all that apply,for volumes list cumulative amounts) b. Store i.On Site Estimated volume in cubic yards ❑ ii.Off Site Estimated volume in cubic yards iia.Receiving Facility: Town: State: iib. Receiving Facility: Town: State: c. Landfill QI.Cover Estimated volume in cubic yards Receiving Facility: Town: State: ii. Disposal Estimated volume in cubic yards Receiving Facility: Town: State: 14. Removal of Drums,Tanks or Containers: a. Describe Quantity and Amount: 1347 gallons of water/product; 50 gallons of hydraulic oil; 1600 pounds of oil/debris/sludge b. Receiving Facility: International Petroleum Corporation Town: Wilmington State: DE c. Receiving Facility: Northland Environmental, Inc. Town: Providence State: RI 0 15. Removal of Other Contaminated Media: a.Specify Type and Volume: 250 pounds of paint mixture Northland Environmental, Inc. b.Receiving Facility: Town: Providence State: RI c.Receiving Facility: Town: State: 16. Other Response Actions: Describe: 17. Use of Innovative Technologies: Describe: Revised: 11/04/2003 Page 3 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number TRANSMITTAL FORM 1130 t. © - ,;,,,,,;,;•. Pursuant to 310 CMR 40.0444-0446(Subpart D) E. LSP SIGNATURE AND STAMP: 1 attest underthe pains and penalties of perjury that I have personally examined and am familiarwith this transmittal form, including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of(i)the standard of care in 309 CMR 4.02(1),(ii)the applicable provisions of 309 CMR 4.02(2)and(3),and 309 CMR 4.03(2),and (iii)the provisions of 309 CMR 4.03(3),to the best of my knowledge,information and belief, > if Section B of this form indicates that a Release Abatement Measure Plan is being submitted,the response action(s)that is (are)the subject of this submittal(i)has(have)been developed in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)comply(ies)with the identified provisions of all orders, permits,and approvals identified in this submittal; > if Section B of this form indicates that a Release Abatement Measure Status Report is being submitted,the response action(s)that is(are)the subject of this submittal(i)is(are)being implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)comply(ies)with the identified provisions of all orders,permits,and approvals identified in this submittal; > if Section B of this form indicates that a Release Abatement Measure Completion Statement is being submitted,the response actions)that is(are)the subject of this submittal(i)has(have)been developed and implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)comply(ies) with the identified provisions of all orders,permits,and approvals identified in this submittal: I am aware that significant penalties may result,including,but not limited to,possible fines and imprisonment,if I submit information which I know to be Use,inaccurate or materially incomplete. 1. LSP#: 9969 2. First Name: Scott K. 3. Last Name: Parker 4. Telephone: (978 568-8740 s Ext.: 239 6. FAX: 978 568-9316 7. Signature: t� 8. Date: v 9.LSP Stamp: H pf M ( Y YY) ss9cy scoTr r o K C.> PARKER N 6 Revised: 11/04/2003 Page 4 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number TRANSMITTAL FORM ® _ 11301 Pursuant to 310 CMR 40.0444-0446(Subpart D) F. PERSON UNDERTAKING RAM: 1. Check all that apply: ❑ a.change in contact name b.change of address c. change in the person undertaking response actions P 2. Name of Organization: Motiva Enterprises LLC 3. Contact First Name: David B. 4. Last Name: Weeks 5. Street PMB 301, 1830 South Road, Unit 24 6.Title: Sr. Environmental Engineer 7. cityrrown: Wappingers Falls 8. State: NY s. ZIP Code: 12590 10. Telephone: (845) 462-5225 11.Ext: 12. FAX 845 462-4999 G. RELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON UNDERTAKING RAM: ® 1. RP or PRP a. Owner ❑ b. Operator ❑ c. Generator ❑ d. Transporter ❑ e. Other RP or PRP Specify: 2. Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21E,s.2) 3. Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.50)) 4. An Other Person Undertaking RAM Specify Relationship: y P Y❑ 9 P H.REQUIRED ATTACHMENT AND SUBMITTALS: 1.Check here if any Remediation Waste,generated as a result of this RAM,will be stored,treated,managed,recycled or reused at the site following submission of the RAM Completion Statement. You must submit a Phase IV Remedy Implementation Plan along with the appropriate transmittal form(BWSC108). 2. Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order(s),permit(s) ❑ and/or approval(s)issued by DEP or EPA. If the box is checked,you MUST attach a statement identifying the applicable provisions thereof. ❑ 3. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the implementation of a Release Abatement Measure. ❑ 4. Check here if any non-updatable information provided on this form is incorrect,e.g.Release Address/Location Aid. Send corrections to the DEP Regional Office. ❑ 5. If a RAM Compliance Fee is required for this RAM,check hereto certify that a RAM Compliance Fee was submitted to DEP,P.O.Box 4062,Boston, MA 02211. ❑ 6. Check hereto certify that the LSP Opinion containing the material facts,data,and other information is attached. Revised: 11/04/2003 Page 5 of 6 r Massachusetts Department of Environmental Protection P Bureau of Waste Site Cleanup BWSC106 i RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number TRANSMITTAL FORM a _ 11301 Pursuant to 310 CMR 40.0444-0446(Subpart D) L CERTIFICATION OF PERSON UNDERTAIUNG RAM: 1. 1, David B. Weeks ,attest under the pains and penalties of perjury(i)that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true,accurate and complete,and(iii) that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. I/the person or entity on whose behalf this submittal is made am/is aware that there are significant penalties,including, but not limited to, possible fines nd imprisonment_,foor illfully submitting false,inaccurate,or incomplete information. 2 By: ltll (!'/ram 3. Title: Sr. Environmental Engineer Signature 4. For. Motiva Enterprises LLC 5. Date: 7 Mf (Name of person or entity recorded in Section F) (mm/dd/yyyy) 6. Check here if the address of the person providing certification is different from address recorded in Section F. 7. Street 8. City/Town: 9, State: 10. ZIP Code: 11. Telephone: 12.Ext.: 13. FAX: YOU MUST LEGIBLY COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Date Stamp(DEP USE ONLY:) Revised: 11/04/2003 Page 6 of 6 Geologic Services Corporation science,engineering&technology I RELEASE ABATEMENT MEASURE COMPLETION REPORT FORMER TEXACO SERVICE STATION#100083 1140 IYANNOUGH ROAD HYANNIS,MASSACHUSETTS DEP RTN 4-11301 i TIER IC PERMIT#100556 ACO-SE-03-3S-002 July 2004 Prepared by: Prepared for: Geologic Services Corporation Motiva Enterprises LLC 15 Bonazzoli Avenue PMB 301,1830 South Rd,Unit 24 Hudson,Massachusetts 01749 Wappingers Falls,NY 12590 (978) 568-8740 (845)462-5225 REF.#000509C Providing Environmental Management Solutions to Business and Industry Since 1982 A 100% Employee-Owned ESOP Company 15 Bonazzoli Avenue• Hudson, MA 01749 • Tel: 978.568.8740 1 800.522.8740 - Fax: 978.568.9316 www.gsc-global.com TABLE OF CONTENTS 1.0 INTRODUCTION............................................................................................................................1 2.0 BACKGROUND INFORMATION.................................................:...............................................1 2.1 Regulatory Status................................................................................................................1 2.2 Subject Site and Surrounding Area.....................................................................................4 2.3 Surrounding Potential Receptors.........................................................................................5 3.0 RELEASE ABATEMENT MEASURE ACTIVITIES....................................................................6 3.1 RAM Plan Objective...........................................................................................................6 3.1.1 Hydraulic Lift Removal Activities.........................................................................6 3.1.2 Used Oil AST Removal..........................................................................................7 3.1.3 Gasoline and Diesel UST System Closure and Removal.......................................7 3.1.3.1 Soil Screening Activities........................................................................7 3.1.3.2 Soil Sample Collection and Analytical Methods...................................8 3.1.4 Fuel Oil UST Removal...........................................................................................9 3.1.4.1 Soil Sample Collection and Analytical Methods...................................9 3.1.5 Oil Water Separator Cleaning................................................................................9 3.1.6 Test Pit Advancements.........................................................................................10 3.2 Management of Remediation Waste.................................................................................10 4.0 SUMMARY AND FINDINGS......................................................................................................10 LIST OF APPENDICES Appendix A - Figures Figure 1 —Locus Plan Figure 2—Property Decommissioning Plan Figure;3 —Vicinity Plan Figure 4—In-Situ Sample Location Plan Appendix B - Photographic Documentation and Certificates of UST Destruction Appendix C - Tables Table 1 —In-Situ Soil Sample Analytical Data—Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Table 2—In-Situ Soil Sample Analytical Results—Volatile Petroleum Hydrocarbons Appendix D - Soil Laboratory Analytical Results Appendix E - Disposal Documentation Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 1 1.0 INTRODUCTION Geologic Services Corporation(GSC)was retained by Motiva Enterprises LLC(Motiva)to observe and document excavation activities during planned underground storage tank(UST)system, fuel oil UST, waste oil UST(if present),hydraulic lift, dry well(if present)removal activities,and the advancement of test pits in the vicinity of an on-site catch basin at the former Texaco-branded Service Station##100083 located at 1140 Iyannough Road in Hyannis,Massachusetts. Please refer to Figures 1,2, and 3 in Appendix A for a depiction of the subject property and surrounding area. 2.0 BACKGROUND INFORMATION 2.1 Regulatory Status 'The subject property was listed by the Massachusetts Department of Environmental Protection(MA DEP)based on information reported in a December 28, 1994 2 1 E Site Assessment Report,prepared by Down Cape Engineering,Inc.(DCE)for Cooke's Restaurant located adjacent to the site at 1120 lyannough Road,Hyannis,Massachusetts. As part of this site assessment,DCE collected groundwater samples from three monitoring wells located on the Cooke's Restaurant property. Laboratory analysis indicated the ipresence of benzene,toluene,and xylenes in the sample obtained from a well reported to be downgradient of the Texaco Station. The MA DEP issued release tracking number(RTN)4-11301 on April 6, 1995 in response to these findings. As a result of the 21 E Site Assessment of Cooke's Restaurant,the MA DEP issued a Notice of Responsibility(NOR)to Star Enterprises(Star)owner of the property located at 1140 Iyannough Road in i Hyannis,Massachusetts on August 11, 1995. On October 12, 1995,Star,submitted a Phase I-Initial Site Investigation Report and Tier IC Application to MA DEP for the subject site..,,During the Phase I I investigation,groundwater sampling results of the on-site monitoring wells revealed dissolved-phase petroleum constituents in excess of the MA DEP reportable concentrations for GW-1 groundwater standards. The MA DEP approved the Tier IC Permit Application(No. 100556)for the subject property on September 12, 1996. At this time it was determined that a Substantial Release Migration(SRM)condition may exist and the MA DEP required an Immediate Response Action(IRA)Plan to be submitted. Star submitted an assessment-only IRA Plan proposing tri-annual groundwater monitoring for a one-year period to evaluate seasonal changes in groundwater elevation and quality. A Phase H Scope of Work(SOW)was submitted by Groundwater&Environmental Services, Inc. (GES)on July 25, 1997 for additional subsurface investigations to be completed. This work included the installation of additional monitoring wells and additional groundwater sampling. On September 18, 1998, Ref.#000509C_Rpt RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 2 SAGE submitted an IRA Status report summarizing the installation of three monitoring wells and the advancement of five soil borings. Groundwater samples were collected from ten on-site monitoring wells on May 6, 1998 and analyzed for extractable petroleum hydrocarbons(EPH)and volatile petroleum hydrocarbons(VPH). Soil analytical results for this sampling event indicated concentrations of methyl- tertiary butyl ether(MtBE)above the applicable Method 1 S-1/GW-1 soil standard at soil sample locations MW-9 and SB-11. Dissolved phase petroleum constituents were detected above applicable Method 1 GW-1 standards in samples collected from all site related monitoring wells except MW-3. SAGE submitted a Modification to the Phase II SOW report on August 13, 1998 for the installation of off-site monitoring wells,well surveying,groundwater sampling,and a soil vapor extraction(SVE)pilot test. SAGE was unable to secure off-site access for the installation of downgradient monitoring wells. However,the SVE pilot test and groundwater sampling were completed on March 25, 1999 and June 4, I 1999,respectively. SAGE indicated that the results of the SVE test were skewed due to recent construction activities that may have caused short-circuiting in the airflow diminishing the effective radius of influence. On March 4, 1999,SAGE submitted a Modification to the IRA Plan report in response to extensive excavation activities proposed at the site. The modification addressed excess soil to be generated during the installation of new pump islands and canopy foundations,and the removal and replacement of two leaching i catch basins. It included a work scope for the soil testing of excavated soils,confirmatory sampling,and management of excavated soils. Approximately 556.75 tons of soil was removed from the site on March 4 and 5, 1999 for reuse at a landfill. Approximately 188.47 tons of petroleum-impacted soil was transported to an off-site disposal facility for recycling on March 24, 1999. In 1999,responsibility for the release was transferred to Motiva,which was created in the formation of a joint venture between Shell and the owners of Star. On August 22,2000, SAGE submitted a Phase H and Phase III Report. Groundwater extraction combined with soil vapor extraction technologies were selected as the remedial action alternative for achieving a permanent solution at the subject property. Following review of the Phase 11 and III Reports,additional delineation of the dissolved phase petroleum hydrocarbons related to the subject property was viewed to be warranted prior to the selection/implementation of a remedial action. In conjunction with the installation of the groundwater monitoring wells,pilot test air sparge(AS)and SVE wells were installed at the subject property. In March of 2001,GSC and Motiva were able to secure off-site access to abutting properties. Between March 19 and 23,2001,GSC personnel supervised the installation of four 2-inch diameter groundwater monitoring wells MW-11,MW-12,MW-13,and MW-14 at and in the vicinity of the subject property in order to further delineate petroleum impact to soil and groundwater. During groundwater monitoring well gauging and sampling activities performed on Apri14,2001, approximately 0.60 feet of non-aqueous phase liquid(NAPL)(i.e.;weathered gasoline)was detected in Ref.#000509C R t RAM Co 07-04 _ P_ mP Texaco Service Station#100083 Geologic Services Corporation Page 3 monitoring well MW-9. The MA DEP was verbally notified of the presence of greater than 0.5 inches of NAPL on April 5,2001. The MA DEP subsequently assigned RTN 4-16161 to this 72-hour release condition and verbally approved passive NAPL bailing activities under an IRA. On April 12,2001,Tanknology-NDE of Springfield,Massachusetts performed a pressure tank tightness test for the gasoline UST system at the subject property. All the pressure tests performed on the UST system passed on this date. On June 8,2001,Motiva submitted a Tier IC Permit Renewal Application to the MA DEP in order to allow for the continuation of response actions under RTN 4-11301. In addition,the Tier 1C Permit application detailed the linking of RTN 4-16161 to lead RTN 4-11301. On September 27,2001,a Decision to Grant a Tier IC Permit Extension was approved by the MA DEP. On July 16,2002,the MA DEP issued a Notice of Noncompliance(NON)(NON-SE-02-3S-014)to Motiva for failure to submit an administratively complete Phase H Report and Phase III Plan. IRA Status Reports were submitted to the MA DEP in March and August 2002 detailing NAPL recovery and assessment activities during the period of August 2001 through July 2002. An IRA Plan Design Specification was also submitted to the MA DEP in August 2002 summarizing a SVE/AS pilot test and detailing a remedial design plan to treat the source area. An IRA Status Report was submitted to the MA DEP on February 21,2003 documenting the installation of the SVE/AS remedial system,NAPL recovery,and continued site assessment activities. The SVE and AS systems were activated on March 14, 2003 and April 4,2003,respectively. The SVE/AS system is currently operational. Operation and maintenance of the SVE/AS system is documented in the semi-annual IRA Status Report dated August 22, 2003 and IRA Completion Report dated February 19,2004. Motiva entered into an Administrative Consent Order(ACO)(ACO-SE-03-3S-002)with the MA DEP on February 19,2003. As part of the ACO agreement between Motiva and the MA DEP,the following regulatory deadlines were established for the subject property:Phase lI-Comprehensive Site Assessment and Phase III-Remedial Action Plan-April 15,2003;Phase IV-Remedy Implementation Plan-September 30,2003;and Phase V-Remedy Operation Status-June 30,2004. A Supplemental Phase II Comprehensive Site Assessment Report(Supplemental Phase If)and Phase III-Remedial Action Plan(RAP)Addendum were submitted for the subject property on April 14, 2003. The Supplemental Phase H and Phase III-RAP Addendum documented the installation of fifty monitoring wells,eleven soil vapor extraction wells,eight air sparge wells,three monitoring point triplets, three cone penetrometer testpoint(CPT)borings,and twenty-six temporary well points during the period of October 2000 through March 2003. In addition,twenty-seven groundwater gauging events and thirteen groundwater sampling events were conducted during this time period. The selected remedial action alternative for the reduction of residual petroleum constituents on the property is the installation and Ref.#000509C Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 4 operation of a Groundwater Extraction and Treatment system downgradient of the subject property coupled with the existing SVE/AS system in the tanlfield area. The selected remedial action alternative outside of the target areas of active remediation is monitored natural attenuation(MNA)for management of migration and eventual reduction of dissolved-phase impacts. A Tier IC Permit Extension was submitted to the MA DEP on June 10,2003 in order to allow for the continuation of response actions under RTN 4-11301. In accordance with the revisions to the MCP 310 CMR 40.0720,the Tier 1 C Permit Extension was presumed approved on August 11,2003. The expiration date of the Tier IC Permit is September 12,2005. Based on difficulties securing access to evaluate an off-site remediation system,Motiva requested an extension for the submittal of the Phase IV-Remedy Implementation Plan(RIP). The ACO Amendment #1 dated September 18,2003 extended the Phase IV-RIP to January 31,2004. The effective date for ACO Amendment#1 is October 1,2003. The Phase IV-RIP,dated January 29,2004,detailed the proposed implementation for the off-site Groundwater Extraction and Treatment system,ongoing operation and maintenance of the on-site SVE/AS system,and continuation of MNA. In addition,the Phasc IV-RIP documented the installation of one recovery well,two monitoring points,recovery well development,overburden aquifer pumping and re- injection tests,and sampling of recovery well RW-1. An IRA Completion Report was submitted to the MA DEP on February 19,2004. A RAM Plan was submitted to the MA DEP on March 16,2004. The objective of the proposed RAM activities was to appropriately manage,and to the degree required,transport and dispose of petroleum impacted soil unearthed during the removal of the gasoline and diesel USTs,associated piping, UST system dispenser equipment, fuel oil UST,waste oil UST(if present),hydraulic lift,dry well(if present),and the advancement of test pits in the vicinity of an on-site catch basin at the subject property. 2.2 Subject Site and Surrounding Area The subject property is situated at 1140 Iyannough Road in Hyannis,Massachusetts and was formerly developed as a Texaco branded retail gasoline and automobile repair facility. The facility is currently inactive. The subject property has an area of approximately 47,916.19 square feet(1.1 acres). The majority of the site is paved with asphalt or reinforced concrete,except a small area in the southern portion of the lot,which is landscaped. The northern portion of the property is wooded and covered in gravel. The single-story station formerly housed an office area,restrooms,and three repair service bays. One 12,000 gallon gasoline UST,one 10,000 gallon gasoline UST,one 10,000 gallon diesel UST,one 8,000 gallon gasoline UST,and one 1,000 gallon fuel oil UST were removed during May 2004. The site is serviced by municipal water supply and sewer as well as underground telephone and electric service utilities. The Ref.#000509C Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 5 subject site drainage system is connected to an on-site leachfreld located immediately east of the service station building. Two detention drainage basins are located approximately 80 feet southeast and 90 feet north of the convenience store,respectively. Please refer to Figures 1,2,and 3 for a depiction of the subject property and surrounding area. The surrounding area is zoned for commercial use. Cooke's Seafood Restaurant is located immediately east of the subject property. Parker's Liquor Store is located immediately west of the subject property. A commercial plaza(Festival at Hyannis)is located immediately north of the subject property. A Ramada Inn is located approximately 100 feet south of the subject property across Iyannough Road. A Cumberland Farms Gulf Station is located approximately 210 feet southwest of the subject property. 23 Surrounding Potential Receptors Subsurface structures within 1,000 feet of the site include half and full basements and utility conduits located along Iyannough Road,Bearses Way and Independence Drive. It should be noted that groundwater depth at the site is greater than 20 feet below grade;and thus,impact to the subsurface structures are unlikely. The closest known basement is located approximately 600 feet southwest (upgradient)of the subject property. Subsurface utility conduits located along these streets include,but are not limited to,municipal water,sewer,gas,and storm drainage. Overhead electric and telephone utilities also exist along these streets and subject site. According to the USGS Hyannis,Massachusetts Topographic Map and GSC site reconnaissance there are no schools,institutions,or environmentally sensitive receptors known to exist within 1,500 feet of the subject property. According to the USGS Hyannis,Massachusetts Topographic Map(refer to Figure 1),the closest surface water bodies include an unnamed brook located approximately 1,800 feet east,Hathaway Pond located approximately 2,600 feet northwest,and Shallow Pond located approximately 3,100 feet west of the subject property. Multiple kettle ponds are located approximately 2,000 feet east of the subject property along Independence Drive. Additional ponds are located further northeast and southeast of the property. According to the flood insurance rate map produced by the Federal Emergency Management Agency,the subject property is located within an area designated as Zone C(an area of minimal flooding). According to the Massachusetts Geographic Information System(GIS),the subject property is located within a MA DEP-Approved Zone R and an EPA-designated sole source aquifer. Six municipal public groundwater supply wells are known to exist within a 1.5-mile radius of the subject property. The closest public supply well(Barnstable Fire District Well#2)is located approximately 4,000 feet northwest of the subject property. According to the Barnstable Water Company and the Barnstable Water Department, no private supply wells exist within 1,000 feet of the disposal site. The subject property and surrounding area are serviced by municipal water. Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 6 3.0 RELEASE ABATEMENT MEASURE ACTIVITIES The following sections provide documentation supporting the completion of the RAM activities at the subject site. 3.1 RAM Plan Objective A RAM Plan was submitted to the MA DEP on March 16,2004. The objective of the proposed RAM activities was to appropriately manage,and to the degree required,transport and dispose of petroleum impacted soil unearthed during the removal of the gasoline and diesel USTs,associated piping, UST system dispenser equipment, fuel oil UST,waste oil UST(if present),hydraulic lift,dry well(if present),and the advancement of test pits in the vicinity of an on-site catch basin at the subject property. Upon further inspection,no waste oil USTs or dry wells were present on the subject property. As discussed in Section 3.1.6,the proposed test pit advancement activities were not performed. 3.1.1 Hydraulic Lift Removal Activities On April 26,2004 GSC personnel observed the removal of one underground hydraulic lift from within the subject building former automobile service bay. Please refer to Figure 2 for the location of the former underground hydraulic lift. During these removal activities,excavated soil was field screened for volatile organic compounds(VOCs)utilizing a photoionization detector(PID)calibrated to respond in parts per million by volume(ppmv)as benzene. Field screening of the in-situ soil samples collected from within the lift excavation yielded PID responses below the instrument detection limit(<1.0 ppmv). The final size of the hydraulic lift excavation was approximately 5 feet wide,5 feet long, and 7 feet deep. Upon removal of the hydraulic lift,all excavated soil was re-used as backfill. Visual inspection of the lift did not reveal any structural damage. Approximately 50 gallons of hydraulic fluid were drained from the lift and transported by EQ Northeast of Wrentham,Massachusetts to Northland Environmental, Inc. (Northland)of Providence,Rhode Island. The lift was transported to James G.Grant Company(Grants) of Readville,Massachusetts for disposal. Photographic documentation of the hydraulic lift removal is included in Appendix B. A total of 2 in-situ soil samples were collected from the hydraulic lift excavation on April 26, 2004. These soil samples were submitted to Accutest Laboratories, Inc. (Accutest)of Marlborough, Massachusetts for laboratory analysis of EPH via MA DEP approved methodology and Polychlorinated Bi-Phenyls (PCBs). Soil sample analytical results have been summarized on Table 1 (Appendix Q. The complete soil laboratory analytical results are included as Appendix D. Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 7 3.1.2 Used Oil AST Removal One 240-gallon steel used oil AST,previously located on the southern wall of the northwest automobile service bay,was removed from the subject property on April 27,2004. Prior to removal, Kessler.confirmed that the AST was empty. Photodocumentation is included as Appendix B. 3.1.3 Gasoline and Diesel UST System Closure and Removal GSC observed the cleaning and removal of one 12,000-gallon gasoline UST,one 10,000-gallon gasoline UST,one 8,000-gallon gasoline UST,and one 10,000-gallon diesel UST on May 3 and 4,2004. Representatives on-site during UST removal activities included Lt.Donald Case Jr. of the Hyannis Fire Department(HFD) and Dimitri Gounis of GSC. The locations of the former USTs are illustrated on Figure 2. ,On May 4, 2004,EQ Northeast removed a total of approximately 280 gallons of residual fluid from the USTs. Prior to UST removal,Kessler Installation and Sales(Kessler)of Dedham, Massachusetts,power washed the exterior of each UST,ventilated,and inerted each UST in order to expel existing residual petroleum vapors. Once approved by the HFD,each UST was lifted from the excavation area and inspected. The four USTs were observed to be of single-walled, fiberglass construction. No visually apparent holes were found on the exterior of the four USTs. A concrete pad was encountered under the USTs at approximately 12 feet below grade. This concrete pad was left in- situ. No groundwater was encountered during the excavation activities. Following the inspection,each UST was placed in a roll-off,crushed on-site,and subsequently transported to Grants. Photographic documentation of UST removal activities along with the Certificates of Destruction for the four USTs is included as Appendix B. During the period of May 6 through 10,2004,Kessler removed associated UST piping and dispenser equipment from the subject property. Prior toxemoval,the fiberglass piping and dispenser equipment displayed no visually apparent structural failure. 3.1.3.1 Soil Screening Activities During the excavation of the gasoline and diesel USTs and associated pump dispenser equipment, a total of 26 samples from the excavated peastone and 33 soil samples were collected from the excavated and in-situ soil,and subsequently screened in the field for the presence of VOCs utilizing a PID calibrated to respond in ppmv as benzene. The 26 headspace screening results of the peastone samples collected in the UST area revealed VOC concentrations of up to 95.6 ppmv in a sample collected from the eastern sidewall of Tank#3 (see Figure 4 in Appendix A). The 16 headspace screening results of the soil samples collected in the UST area revealed VOC concentrations of up to 68.1 ppmv in a sample collected from Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 8 underneath Tank#1 (southern most UST). Based on PID field headspace screening results and the absence of visual/olfactory indications of petroleum impact,no over excavation of the UST area was performed. The final size of the gasoline and diesel UST excavation was approximately 57 feet in length, 33.5 feet in width,and 12 feet in depth. The 14 headspace screening results of the soil samples collected from the associated gasoline pump dispenser equipment revealed VOC concentrations of up to 226 ppmv in a sample collected from the beneath the gasoline product lines(EXCOI). As described in the RAM Plan,PID readings in excess of 100 ppmv in soil samples collected from within the UST excavation will not result in a new notification condition to MA DEP as this RAM served as appropriate documentation to manage the impacted soil related to the existing RTN 4-11301. No soil was excavated from the vicinity of soil sample EXCO1 based on the potential of jeopardizing the integrity of the adjacent on-site AS/SVE remediation lines. The 3 headspace screening results of the soil samples collected from the diesel pump dispenser and product lines revealed VOC concentrations up to 1.6 ppmv in a sample collected from beneath the diesel product line(EXC05). Based on PID field headspace screening results and the absence of visual/olfactory an indication of petroleum impact,no over excavation in the gasoline/diesel product line and equipment area was performed. The final sizes of the pump dispenser excavation was approximately 50 feet long,28 feet wide,and 4 feet deep for the gasoline dispensers and 12 feet long, 12 feet wide,and 5 feet deep for the diesel dispenser. The gasoline and diesel product line excavations were approximately 3 feet wide and 3 to 4 feet deep. Clean material transported to the site was utilized to backfill the excavation areas. Please refer to Figure 4 for a depiction of the soil excavation limits. 3.1.3.2 Soil Sample Collection and Analytical Methods A total of 16 in-situ soil samples were collected from the four sidewalls and beneath the gasoline USTs on May 4,2004. Eight in-situ soil samples were collected from the former gasoline pump dispenser and associated product line excavations on May 6 and May 10,2004. Three in-situ soil samples were collected from the former diesel pump dispenser and associated product line excavations on May 10, 2004. Please refer to Figure 4 for the locations of these in-situ soil samples. The gasoline soil samples were submitted to Accutest for laboratory analysis of VPH via MA DEP approved methodology. The diesel soil samples were submitted to Accutest for laboratory analysis of EPH via MA DEP approved methodology. Soil sample analytical results have been summarized on Tables 1 and 2 (Appendix Q. The complete soil laboratory analytical results are included as Appendix D. Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 9 3.1.4 Fuel Oil UST Removal On May 5, 2004,GSC personnel observed the removal of one fuel oil UST at the subject property. The location of the subject fuel oil UST is illustrated on Figures 2 and 4. Previous records indicated the capacity of the fuel oil UST to be 550 gallons. However,upon excavation, the fuel oil UST was determined to be a 1,000-gallon single walled fiberglass UST. The contents of the fuel oil UST were removed prior to excavation. No evidence of rust, staining,or holes were observed on the UST. No petroleum impacted soil was encountered during the excavation of the fuel oil UST. On May 7, 2004, EQ Northeast cleaned the residual from the excavated fuel oil UST. The fuel oil UST was placed in a roll-off,crushed on-site,and transported to Grants for disposal.Photographic documentation of the fuel oil UST removal activities is included as Appendix B. The final size of the fuel oil excavation was approximately 11 feet wide, 14 feet long,and 6 feet deep. 3.1.4.1 Soil Sample Collection and Analytical Methods During the fuel oil UST excavation activities on May 5,2004,a total of five soil samples were collected from the in-situ soil,and subsequently screened in the field for the presence of VOCs utilizing a PID. The soil sample headspace screening results of the in-situ samples revealed all VOC concentrations below 1.0 ppmv. A total of five in-situ soil samples were collected from the sidewalls and bottom of the fuel oil UST excavation area on May 5,2004 and submitted to Accutest for analysis of EPH via MA DEP approved methodology. Please refer to Figure 4 for the locations of these in-situ soil samples. Soil sample laboratory results are presented on Table 1. Soil sample analytical results have been included as Appendix D. 3.1.5 Oil Water Separator Cleaning On May 7,2004,GSC personnel observed the removal of water and sludge from the interior of the oil/water separator located southeast of the station building. Approximately 1,347 gallons of residual water/product mixture(5 gallons of which was estimated to be recovered product)was removed by EQ Northeast on May 7,2004 and transported to International Petroleum Corporation of Wilmington, Delaware for disposal. Approximately 1600 pounds of sludge was removed by EQ Northeast on this date and transported to Northland for disposal on June 3,2004. The oil/water separator will remain on site for future use, as it is part of the on-site drainage system Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 10 3.1.6 Test Pit Advancements As indicated in the RAM Plan dated March 16,2004,Motiva proposed to advance test pits in the vicinity of the on-site catch basin located on the northwest portion of the site. These test pits were not advanced due to the potential of jeopardizing the integrity of the catch basin and the adjacent AS/SVE piping. PID readings collected from in-situ soil from the northern most UST indicated no concentrations of VOCs above 1.0 ppmv. In addition,all analytical results from soil samples collected from the sidewalls and bottom of the northern most tank(Tank#4)were below laboratory detection limits. 3.2 Management of Remediation Waste As noted herein,no over-excavation activities were performed to remove petroleum impacted soil at the site. All excavated soil was re-used as backfill on the subject property. Clean fill was provided by Stocchetti Road Construction of Dennis,Massachusetts to re-grade the excavation areas. On April 26,2004,approximately 50 gallons of hydraulic oil was drained from the hydraulic lift. This hydraulic oil was placed in a DOT Style 17H drum and transported by EQ.Northeast to Northland on June 3,2004 under a Uniform Hazardous Waste Manifest. On May 7,2004,approximately 1,347 gallons of oil/water mixture was removed from the oil/water separator and transported under a Uniform Hazardous Waste Manifest to International Petroleum Corporation. Approximately 1,600 pounds of sludge was removed from the oiUwater separator on May 7, 2004 and transported by EQ Northeast to Northland on June 3,2004. EQ.Northeast transported approximately 250 pounds of paint related materials to Northland on June 3,2004. The paint mixture was not generated during the RAM activities,but was disposed of as part of divestment activities. Copies of the Uniform Hazardous Waste Manifests have been included as Appendix E. 4.0 SUMMARY AND FINDINGS • On April 26,2004, GSC personnel supervised the removal of one hydraulic lift from the subject property. In-situ laboratory analytical results from the hydraulic lift excavation revealed that none of the targeted petroleum analytes were detected in excess of the applicable MCP Method 1 Risk Characterization standards. • Kessler removed one 240-gallon,double walled steel,waste oil AST from within the former service bay on April 27,2004. Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 11 • On May 3 and 4,2004,Kessler removed one 10,000-gallon diesel,one 8,000-gallon gasoline,one 10,000-gallon gasoline,and one 12,000-gallon gasoline UST from the subject property. One UST post excavation in-situ soil analytical sample(Tank 1 Bottom)exhibited a concentration of MtBE in excess of the applicable MCP Method 1 Risk Characterization Soil Standards. All other in-situ laboratory analytical results for samples collected from the gasoline/diesel UST excavation revealed that none of the targeted petroleum analytes were detected in excess of the applicable MCP Method 1 Risk Characterization standards • On May 5, 2004,GSC personnel supervised the removal of one 10,000-gallon single walled fiberglass fuel oil UST from the subject property. hi-situ laboratory analytical results from the fuel oil UST excavation revealed that none of the targeted petroleum analytes were detected in excess of the applicable MCP Method 1 Risk Characterization standards. • _ During the period of May 6 through May 10,2004,Kessler removed piping and pump dispenser equipment associated with the former gasoline/diesel USTs. Post excavation in-situ soil laboratory analytical results indicate concentrations of MtBE,naphthalene, CS-C8 aliphatics, and/or C9-C,0 aromatics above the applicable MCP Method 1 Risk Characterization Soil Standards in select soil samples(EXCO1,and EXCO2)collected during the pump dispenser and piping excavation activities. All other target petroleum analytes were below the applicable MCP Method 1 Risk Characterization Soil Standards. • On May 7,2004,GSC personnel supervised the cleaning and removal of water and sludge from the on-site oil/water separator. • During the UST removal activities occurring in April and May 2004,no over-excavation of petroleum impacted material was performed. All excavated soil was reused on site as backfill. Clean fill was used to re-grade the excavation areas. The objective of this RAM(i.e.,management and removal of petroleum impacted soil and groundwater) has been met. Thus, this RAM described herein is considered complete pursuant to 310 CMR 40.0446(2). Future response actions will continue to be conducted at this site under RTN 4-11301 in accordance with 310 CMR 40.0000. Ref.#000509C Rpt RAM Comp 07-04 APPENDIX A Figures LO .. 7f MR #fi Se • , .,. T-; x `• Wig Eg '���iti\�L• 'Flli[llia".#\ '`/. r't r�'tl:i� �. � �� ,-_._ �� 6�� _. ;���'. �\�.;-� rrFR UTM eiiiiii• �4 COORDINATES: t QUAD RANGLE LOCATION LATITUDE: I LONGITUDE: I' ' FIGURE 1 LOCUSPLAN Notes: 1. Topographic contours are measured in meters. FORMER TEXACO SERVICE STATION C GEOLOGIC SERMCES CORPORATION J Hydrogeologists and Environmental Scientists Source: USGS Topographic Quads-Barnstable,MA 15 Bonazzcl i Avenue * Hudson, MA 01749 * (978)568-8740 Quadrangle 15 Minute Series I TMP-1 20 MW-3A `�. 41- N SYSTEM f I ENCLOSURE MW-2A (BUILDING M W 17 SB-7 SOIL BORING SVE-9 MW-1 A AS-5 � � DESTROYED MONITORING WELL MW-14D \` FORMER HYDRAULIC LIFT MW-1 SVE-3 41 1 ® �CB-2 MW-7 MW-18S MW-14 B_1 O4S-4 ♦ TMP-103 ;""W'18D GROUNDWATER MONITORING WELL MW—i 4S � MW-5 : O ®SVE-8 # / O AIRSPARGE WELL SVE-2 � . ::;__AS-6 MW-6 MW-8 AS-3�0 ;FORM::ER; : ®SVE-10 � / RECOVERY WELL _ UST... SB-8 AREA- SB—10 ® SOIL VAPOR EXTRACTION WELL CPT— _ AS-2 ' MW-9 O .... O ®SV —6 MW-4 / 111 TEMPORARY MONITORING WELL SVE-1 — .. / \FORMER AS 8 MP- 101 - ® CATCH BASIN/POTENTIAL DRYWELL DIESEL AS-1 DISPENSER MP-2 RW-1 SERVICE —-— PROPERTY BOUNDARY ISLAND MP I — 100 ��� �V AS-7SV —7 STATION MP 102 / UST UNDERGROUND STORAGE TANK _ COOKIE'S O/W OIL/WATER MCPT�2 .®CB-1 ® MW-3 % RESTAURANT F/0 FUEL OIL 11' T P��101� SVE-4 �-.. LFORMER MW— NOTE: LOCATION OF SYSTEM ENCLOSURE 00��r �, 1®SVE-5 F/O UST % IS APPROXIMATE MW-12 CB 3® MW-2 O/W SEPARATOR 0 50 FORMER GASOLINE `` / Scale in feet DISPENSER ISLANDS FIGURE 2 PROPERTY DECOMMISSIONING PLAN FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.02DECON I CHECKED BY: MW DRAFTED BY: SAC I DATE: 8412402 REVISED BY: ANG I DATE: 6 11 04 ��GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE * ! Hydrogeologists and Environmental Scientists 15 Bona7zoli Avenue • Hudson,MA 01749 •(978)568-8740 COMMERCIAL PIER 1 k\\ - GRAVEL PAYLESS O PITS W � BLOCKBUSTER Q JENNY C) CRAI/ G ATTRESS / GIANT O CZ) COOKE S ~ LIVE cgRDEN � SEAFOOD x OySRUS DISCOUNT ./ THE RAMADA MARINE SITE DAMES �� REq EHY ��� STATE �� 0 350 CRACKER GULF BARREL PARKER'S STATION Scale in feet OUTSET DISCOUNT KEY LIQUOR FIGURE 3 VICINITY PLAN — - — PROPERTY BOUNDARY FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.01VICINB CHECKED BY: DRAFTED BY: CD DATE: 2 11 02 REVISED BY: ANG DATE: 3 2 2 SOURCE: SAGE ENVIRONMENTAL PLAN AND GSC FIELD GEOLOGIC SERVICES CORPORATION RECONNAISSANCE Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue • Hudson, MA 01749 •(978)568-8740 SB-7 ' SVE-3 \ SVE-90 ®CB-2 ® ® M*7 1 — LIFT BOTT OAS-4 AS-5 2— LIFT ESW SB-1 1 MW-5* KEY 3— TANK 4 NORTHEAST , SOIL BORING 4— TANK 4 NORTHWEST ... OAS-6 ®SVE-8 MW B 5— TANK 4 WEST / # DESTROYED MONITORING WELL SVE-2 6- TANK 3 WEST 0 ' .� ..." MW-6 FORMER HYDRAULIC LIFT 7- TANK 2 WEST AS-30 .FORME ®SVE-10 SB 8 8— TANK 1 WEST GROUNDWATER MONITORING WELL MW-9 , AREA SB-10 9- TANK 1 SOUTHWEST Q O AIRSPARGE WELL 10- TANK 1 SOUTHEAST CPT- 1 - AS-2 �.. O SVE-6 I ♦ RECOVERY WELL 11 - TANK 1 EAST S 12- TANK 2 EAST SVE- 1 1 S=$ MP--101 MW 4 ® SOIL VAPOR EXTRACTION WELL 13- TANK 3 EAST FORMER ®' :� ® .� ♦ % fo TEMPORARY MONITORING WELL 14- TANK 4 EAST DIESEL �.. RW-1 15- TANK 4 BOTTOM DISPENSER , AS-1 MP-102 l ® CATCH BASIN/POTENTIAL DRYWELL 16- TANK 3 BOTTOM ISLAND MP-2 A ' --- PROPERTY BOUNDARY SVE- 1 AS-7 SERVICE I 17- TANK 2 BOTTOM MP-3 ® ® 2 STATION UST UNDERGROUND STORAGE TANK 18- TANK 1 BOTTOM ' MP-1 SVE-7 ®� O/W OIL/WATER 19- FOUSTBOTT MW-1 I 20- FOUSTNW .® ' F/O FUEL OIL 21 - FOUSTEW MW-10* SVE-4 ' NOTE: LOCATION OF SYSTEM ENCLOSURE 22- FOUSTSW CPT-2--.*` ®CB-1 ® ® IS APPROXIMATE 23- FOUSTWW � MW-3� I APPROXIMATE AREA 24— NE DISP BOTT TMP-10\` FORMER MW-11 0 OF EXCAVATION 25— SE DISP BOTT \ SVE-5 F/0 UST 26— SW DISP BOTT \® 27— NW DISP BOTT 28— EXCO 1 29— EXCO2 SB-9 30— EXC03 \� O ' 0 30 31 — EXC04 \ 32— EXC05 MW-12 i Scale in feet 33— EXC06 `\B® Mw-2 � FIGURE 4 34— D DISP BOTT FORMER �\ , IN—SITU SOIL SAMPLE LOCATION PLAN GASOLINE \ �� I FORMER TEXACO SERVICE STATION #100083 DISPENSER ISLANDS 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.021NSITU CHECKED BY: DRAFTED BY: SAC DATE: 8412402 REVISED BY: ANG DATE: 6 11 04 SOURCE: GSC FIELD RECONNAISSANCE ` j GEOLOGIC SERVICES CORPORATION L Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue • Hudson, MA 01749 • (978)568-8740 APPENDIX B Photographic Documentation and Certificates of UST Destruction .7c Vy 74s�'t aA.1u's�crty ��}3�"�Fd'{�1' fia,v $ N ���� • e{`5 ire lry,�,!>}i��s�'I�,�¢7Y}Nx�+y��,�q r� > 4 '� , �'1 ! `,, ' i�,"'m,' I,c,;'..r' >•,»4 r,k' ,,�, ��'�� �� +.�,�:^yyl�il t��.Jp+^��,F.e ry( �xw� R .e� '� � �ec ;�kiS ?�i',i; '' ^�!";: ! �, •�j?. � R;�(S e a +4 v r+� � 1 ' ?5" rK , +'°r+� i P ���PF^' u.,Iw t, .y ✓ �,>x S!�"" yh R,� NO �+m 77 r vl��+�✓s� �f�,.r �w�ir.+`�' ��rr��y�"�a n�,�..�t�� ,.n... �' .0 3�+Y �.„�. ,,),,, x�W:,'' ron'�W ��i� �.f i� � .Nty �.�" ..m.w..—. q , P d yY�+ 51'j r ✓ r ams., � r kf1 � I�h o,wi� risxs� -^�. Yi:�J''�d4 '� F 1Y1. ���g�Y�I'Pi'rI�NA,��I�Yw'al�•°Yryf���{'A. � r.�.,u�`',�y'� - Nr15rp1y bh d 7 a � m1 §F� i� 4 ,.*.n+ � � �"44ih>r r• I,x�i 'u n�r ^fly 1 r } PHOTOGRAPHIC DOCUMENTATION FORMER • SERVICE STATION •••: • IYANNOUGH ROAD u' • _ -A PYA• f t d ... ...... ---------- 44 '.' ¢�'.�`�' VIEW OF GASOLINE UNDERGROUND STORAGE TANK EXCAVATION-5/3/04 POST-EXCAVATION VIEW OF GASOLINE UNDERGROUND STORAGE TANK #1 -5/4/04 PHOTOGRAPHIC DOCUMENTATION FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.05PHOTO CHECKED BY: 91 DRAFTED BY: ANG DATE: 6/1 04 REVISED BY: DATE: GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE Hydrogeologists and Environmental Scientists ♦F Rnnornli n—.—. Lh.4— KAn n17An. 10701 RRO-07An i y �t POST-EXCAVATION VIEW OF GASOLINE UNDERGROUND STORAGE TANK #3-5/4/04 a a POST-EXCAVATION VIEW OF GASOLINE UNDERGROUND STORAGE TANK #4-5/4/04 PHOTOGRAPHIC DOCUMENTATION FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF_: 000509.06PHOTO CHECKED BY: )h uj DRAFTED BY: ANG DATE: 6 14 04 REVISED BY: DATE: `j GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE Hydrogeologists and Environmental Scientists 1 F Rnn—li A—e—. W-4— non n+7nn a l0701 F90.07An k POST—EXCAVATION VIEW OF DIESEL UNDERGROUND STORAGE TANK #2-5/4/04 n 3.STD mS _ m k SK � 4^" f'F, Ml"',ice VIEW OF FUEL OIL UNDERGROUND STORAGE TANK EXCAVATION-5/5/04 PHOTOGRAPHIC DOCUMENTATION FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.07PHOTO CHECKED BY:rn ttj DRAFTED BY: ANG DATE: 6 14 04 REVISED BY: DATE: " � GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE Hydrogeologists and Environmental Scientists 1G Rnn —li Ain . LJ-4— RAA M7An,. 10701 ll:hLQ7An .ram d POST-EXCAVATION VIEW OF FUEL OIL UNDERGROUND STORAGE TANK-5/5/04 MW f - E t r� t VIEW OF GASOLINE DISPENSER ISLAND EXCAVATION-5/7/04 PHOTOGRAPHIC DOCUMENTATION FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.08PHOTO CHECKED BY: M DRAFTED BY: ANG DATE: 6 14 04 REVISED BY: DATE: `j GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE Hydrogeologists and EmAronmental Scientists �.Rn .—fi A-,.. L—4— AAA n17AM. ln741 FC.O_07An $.g7� qc- � VIEW OF GASOLINE PRODUCT PIPING EXCAVATION-5/7/04 f a^C VIEW OF DIESEL DISPENSER ISLAND EXCAVATION-5/10/04 PHOTOGRAPHIC DOCUMENTATION FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.09PHOTO CHECKED BY: lntU DRAFTED BY: ANG DATE: 6 14 04 REVISED BY: DATE: GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE Hydrogeologists and Environmental Scientists iF Anno-ronli A—nnn• L—4— AAA/M7AO& 0701 FRG-07A0 C go • 1 "•1 I A • • • � gas 14 ki 20XPT I-- PHOTOGRAPHIC DOCUMENTATION FORMER • SERVICE STATION •• i • IYANNOUGH ROAD ® • • • •••••i • • 1 RECONNAISSANCE Mai 21 04 08: 45a Kessler Installation 781 326 3189 p. 2 Dc(=,(,Nes 4 �7m 5e�vicea - Ci# od tie State71U N4U'sa�lug RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK F. FP`91 NAME AND ADDRESS OF APPROVED TANK YARD James G. 6vanE Co.,, lac. 79 WoiCOtt St. ------- Readvil,;., MA02?37 -- APPROVED TANK YARD NO. -- _ Tank Yard Ledger 502 CMR 3.03(4)Number: '�< � 1�y I certify under penalty of law I have personally examined the un0ergr0un0 steel storage tank delivered to this"approved Lank yard"by fun),corporation or partnership ���_ and accepted same In conformance with Massachusetts Fire Prevention Regulation 502 CMR 3.0/0 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL tread of File Department FD07 _ _ .- 2 t0 transport this tank to this yard. N a rt of approved tank yard owner or owners authorized representative: _ � _ — G ATURE TITLE _ ATE SIGNED This ned receipt of disposal must be returned to the local head of the fire department FDIDt1 [> f ^� pursuant l0 502 CMR 3.00. EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK DATA TANK REMOVED FROM Gallons R,CCQ r— G �lJ Ank)W (jNo-and Street) Previous Contents GAS Diameter. Length — _.. _..... —(City-or-Town) Date Received -5 5 iJ Fire Department Permit# Serial At(if available) Tank I.D.i#(Form FP-290) Owner/Operator to mail revised copy of Notification Form (FP290, or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road,Stow, MA 01775. May 20 04 05: 37p Kessler Installation 781 32G 3189 p. 4 010Awczcliu� uluri Dowrt�off' 7me Semi" - 4 tlse State 7w X V a 0 RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK Fo m FP t-1 NAME AND ADDRESS OF APPROVED TANK YARD j;aciles C'.Gfant CO-, 1nC. 2S, WOiCOtt St- Reariyilk, MA 02137 APPROVED TANK YARD NO. 4006 Tank Yard Ledger 502 CMR 3.03(4)Number: I certify under penallX of law I have personally examined the underground steel storage tank delivered to this"approved tank yard'by firm.Corporation or partnersnrp ��SLC� and accepted same in cnnfnrrnance with Massachusetts Fire Prevenbon Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL Head of Fire Department. FDIDrt . l 2— to transport this tank to this yard. Name and offic pl title of approved tank yard owner or owners authorized representative. I //.,�1, 104 SIGNATURE TITLE DATE SIGNED This signed receipt of disposal must be returned to the local head of the fire department FDIDrr 0 L Z pursuant to 502 CMR 3.00. EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK DATA TANK REMOVED FROM Gallons I(),Coo 1140 ]1 000Gk R0 o.and Street) Previous Contents GAS �jNDiameter Lengtb (City or Town) Date Received 1,hIS101 Fire Department Permit# Serial#(if available) Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form (FP290, or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road, Stow, MA 01775. Mai 20 04 05: 37p Kessler Installation 781 32G 3189 p. 2 Tare -5cw4eed g the State 7W Wa744d C_ -, lug, RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK F-FP 291 NAME AND ADDRESS OF APPROVED TANK YARD llmr'PC G. xGal1Q Co., InC. 28 woicott St. Rpae)ville, MA 02,137 1CX)=1 S APPROVED TANK YARD NO. 008 =1 HCTank Yard Ledger 502 CMR 3.03(4)Number: 1 certify under penalty of law 1 have personally examined the underground steel storage tank delivered to this"approved tank yard"by firm,corporation or partnership and accepted same in conformance with Massachusetts Fire Prevention Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards A valid permit was issued by LOCAL Head of Fire Department_ FDID#_ _J- to transpo-t this tank to this yard. Name and officiiA tle of approved tank yard owner or owners authorized rcpresentahve: DATE SIGNED SIGNATURE T11LE r pursuant to 502 CMR 3.00 This signed receipt of disposal must be returned to the local head of the fire department FDID# EACH TANK MUST HAVE A RECEIPT OF DISPOSAL_ TANK DATA TANK REMOVED FROM Gallons Box S�AN00&6 I�O (No.and Street) Previous Contents GA S �I�AhV�S Diameter - Length - (Clty or Town) Date Received 55 a Fire Department Permit# Serial#(if available) Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form(FP290,or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road,Stow, MA 01775. Mai 20 04 05: 38p Kessler Installation 781 326 3189 p. 5 �/-e p7yUyl7,p� n M(Lr oYLca � gewc/zj - l�#4ce b lie .SWZ 71/re N s RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK Form FP'91 _ NAME AND ADDRESS OF APPROVED TANK YARD _ J .lE� G- `' �` 'j°' Inc. - 2'� WO:COit St. ti:e�clvle., 02137 -- APPROVED TANK YARD NO. 4K)08 ----.--Tank Yard Ledger 502 CMR 3.U3(a)Number: 200 9-7­9 QZ — I certify under penalty of law I have personally examined the underground steel storage tank delivered to this"approved tank yard"by firm,corporation or partnership ,,'ASS' EV and accepted same in conformance with Massachusetts Fire Prevention Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL Head of Fire Department. FDID# ✓ i �� 2 2- to transport this tank to this yard. Name and officialv title of approved tank yard owner or owners authorized representative: Y 5 DATE SIGNED SI>�IATURiE TITLE J G1 This signed receipt of disposal must be returned to the local head of the.fire department FDID# 0 _� _! _ __pursuant to 502 CMR 3.00. EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK REMOVED FROM TANK DATA Gallons ID,OOQ llg0 AH006N - (No.and Street) Previous Contents�,B�5F:_L-- gNrrs S Length — (Clty or Town) Diameter In Date Received t-6 5 0 Fire Department Permit# ���3 Serial#(if available) Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form(FP290, or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road, Stow, MA 01775. Matj 20 04 05: 37p Kessler Installation 781 326 3189 p. 3 D0414 egt 57me gmAu,ea - 6F#6ce 4 0/fe State 70ze W(=J"l RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK F.—FP 201 NAME AND ADDRESS OF APPROVED TANK'YARD _ IaLnes G_Gsf-ant Con Inc- 2g WoicOtl St. Rtadvilie. MA 02137 APPROVED TANK YARD NO. #008 _Tank Yard Ledger 502 CMR 3.03(4)Number. I certity under penalty of law I have personally examined the underground steel storage tank delivered to this"approved tank yard"by him.corporation Or partnership ;.� G� and accepted same in conformance with Massachusetts Fire Prevention Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL Head of Fire Department. FDID#. _ ��— to transport this tank to this yard. Name end officipl`ti�e of approved tank yard owner or owners authorized representative: -sib 8q SIGNATURE TITLE DATE SIGNED This sighed receipt of disposal must be returned to the local head of the fire department FDID# 7 p f 2 pursuant to 502 CMR 3 00 EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK DATA TANK REMOVED FROM Gallons �t�() �� _-.�-� k t (No.and Street) Previous Contents #Z qN NsS Diameter Length (City or Town) Date Received `'IS Fire Department Permit# ClAsocy Serial#(if available) Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form(FP290, or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road,Stow, MA 01775. APPENDIX C Tables Table 1 Page 1 of I In-Situ Soil Sample Analytical Data-Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Former Texaco Service Station#100083 1140Iyannough Road Hyannis,MA April 26,2004 through May 10,2004 Sample Date Depth Acenaph Acenaph Anthra- Benzo(a) B(a)P B(b)F Benzo(g,h,i)-B(k)F ChryseneDibenz(a,h) Fluor- Fluoren ndeno(1,2,3-cd) 2-Methyl- Naph- Phen- Pyrene C9-C1s C19-C16 C11-C21 ID thene thylene cene anthracene perylene anthracene anthene pyrene naphthalene thylene anthrene Aliphatics Aliphatics Aromatics (feet) (ug/g) (ug1g) (ug1g) (ag/g) (ag/g) (ag/g) (ug/g) (ug/g) (ag/g) (Ug1g) (ug/g) (ug1g) (ug/g) (ug/g) (ag/g) (ug/g) (a€/g) (ag/g) (ug/g) (ug/g) MCP Soil Standard S-1/GW-1 20 100 1000 0.7 0.7 0.7 1000 7.0 7.0 0.7 1000 400 0.7 4.0 4.0 700 700 1000 2500 200 MCP Soil Standard S-1/GW-2 1000 100 1000 0.7 0.7 0.7 1000 7.0 7.0 0.7 1000 1000 0.7 500 100 1000 700 1000 2500 800 MCP Soil Standard S-1/GW-3 1000 100 1000 0.7 1 0.7 0.7 1000 7.0 7.0 0.7 1000 1000 0.7 500 100 100 700 1000 2500 800 MCP Soil Standard S-2/GW-1 20 100 2500 1.0 1 0.7 1.0 2500 10 10 0.7 2000 400 1.0 4.0 4.0 700 2500 2500 5000 200 MCP Soil Standard S-2/GW-2 2500 2500 2500 1.0 0.7 1.0 2500 10 10 0.7 2000 2000 1.0 1000 1000 2500 2500 2500 5000 2000 MCP Soil Standard S-2/GW-3 2500 1000 2500 1.0 0.7 1.0 2500 10 10 0.7 1000 2000 1.0 1000 1000 100 2500 2500 5000 2000 MCP Soil Standard S-3/GW-1 20 100 5000 4.0 0.7 4.0 2500 40 40 0.8 2000 400 4.0 4.0 4.0 700 1000 5000 5000 200 MCP Soil Standard S3/GW-2 5000 2500 5000 4.0 0.7 4.0 2500 40 40 0.8 5000 5000 4.0 2000 1000 2500 5000 5000 5000 5000 MCP Soil Standard S3/GW-3 4000 1000 5000 4.0 0.7 4.0 2500 40 40 0.8 1000 4000 4.0 1000 1000 100 5000 5000 5000 5000 LIFT BOTT 4/26/04 6-7 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 9.87 55.5 18.5 S-1/S-3/GW-1/GW3 LIFT BSW 4/26/04 3-4 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <6.1 <8.1 <17 S-1/S-3/GW-I/GW3 TANK 2 EAST 5/4/04 7 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <6.3 <8.4 <18 S-1/S-3/GW-1/GW3 TANK 2 WEST 5/4/04 7 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <6.1 <8.2 <17 (S-1/S-3/GW-I/GW3 TANK 2 BOTTOM 5/4/04 12 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5.9 <7.9 <17 S-1/S-3/GW-1/GW3 FOUSTBOTT 5/5/04 6-7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <6.0 <8.1 <17 S-1/S-3/GW-1/GW3 FOUSTNW 5/5/04 3-4 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <5.9 <7.8 <17 S-1/S-3/GW-i/GW3 FOUSTSW 5/5/04 3-4 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <6.0 <8.0 <17 S-1/S-3/GW-1/GW 3 FOUSTSW 5/5/04 3-4 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <6.0 <8.0 <17 S-1/S-3/GW-1/GW 3 FOUSTWW 5/5/04 3-4 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <6.4 <8.5 <18 S-1/S-3/GW-I/GW 3 D DISP BOTT 5/10/04 5 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 184 104 57.6 S-1/S-3/GW-l/GW3 EXC05 5/10/04 4 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 162 146 82.8 S-1/S-3/GW-1/GW3 EXC06 5/10/04 4 1 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 1<0.53 <0.53 <0.53 I <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <6.4 <8.5 <18 (S-1/S-3/GW-1/GW3) i Notes: ug/g-micrograms per gram(parts per million) MCP-Massachusetts Contingency Plan B(a)P-Benzo(a)pyrene B(b)F-Benzo(ofluoranthene B(k)F-Benzo(k)fluoranthene <0.56-not detected(method detection limit included) Shading-indicates analyte exceeds MCP Method 1 Risk Characterization Soil Standards 1-this sample also exhibited a concentration of 0.154 ug/g Aroclor 1260 GEOLOGIC SERVICES CORPORATION 6/25/2004 science,engineering&technology Ref.#000509_Tbl_soil-pah+eph 15 Bonazzoli Ave.,Hudson,MA Table 2 Page I of I In-Situ Soil Sample Analytical Results-Volatile Petroleum Hydrocarbons Former Texaco Service Station#100083 1140 lyannough Road Hyannis,MA May 4,2004 through May 10,2004 Sample Date I Depth Benzene Toluene Ethyl- Total MtBE Naphthalene Cs-Cs CrC12 CrCto ID (ft) (ug/g) (ug/g) benzene Xylenes (ug/g) (ug/g) Aliphatics Aliphatics Aromatics (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) MCP Soil Standards S-1/GW-I 10 90 80 500 0.3 4.0 100 1000 100 MCP Soil Standards S-I/GW-2 40 500 500 500 100 100 100 1000 100 MCP Soil Standards S-I/GW-3 40 Soo 500 500 100 100 100 1000 100 MCP Soil Standards S-2/GW-1 10 1 90 80 1 800 0.3 4.0 500 2500 100 MCP Soil Standards S-2/GW-2 60 500 1000 500 200 1000 500 2500 500 MCP Soil Standards S-2/GW-3 60 1000 500 1000 200 1000 500 2500 500 MCP Soil Standards S-3/GW-1 10 90 80 800 1 0.3 4.0 500 5000 100 MCP Soil Standards S-3/GW-2 100 500 2500 500 200 1000 500 5000 500 MCP Soil Standards S-3/GW-3 200 2500 500 2,500 200 1,000 500 5000 500 TANK 4 NORTHEAST 5/4/04 7 <0.180 <0.180 <0.180 <0.180 <0.072 <0.180 <3.6 <3.6 <3.6 (S-3/GW-I/GW-3) TANK 4 NORTHWEST 5/4/04 7 <0.190 <0.190 <0.190 <0.190 <0.075 <0.190 <3.7 <3.7 <3.7 (S-3/G W-1/G W-3) TANK I WEST 5/4/04 7 <0.210 <0.210 <0.210 70.210 <0.083 <0.210 <4.1 <4.1 <4.1 (S-3/GW-1/GW-3) TANK 2 WEST 5/4/04 7 <0.170 <0.170 <0.170 <0.170 <0.066 <0.170 <3.3 <3.3 <3.3 (S-3/GW-I/GW-3) TANK 3 WEST 5/4/04 7 <0.210 <0.210 <0.210 <0.210 <0.086 <0.210 <4.3 <4.3 <4.3 (S-3/GW-I/GW-3) TANK 4 WEST 5/4/04 7 <0.170 <0.170 <0.170 <0.170 <0.069 <0.170 <3.4 <3.4 <3.4 (S-3/G W-I/G W-3) TANK 1 SOUTHWEST 5/4/04 7 <0.230 <0.230 <0.230 <0.230 <0.092 <0.230 <4.6 <4.6 <4.6 (S-3/GW-1/GW-3) TANK 1 SOUTHEAST 5/4/04 7 <0.200 <0.200 <0.200 <0.200 <0.081 <0.200 <4.1 <4.1 <4.1 (S-3/GW-I/GW-3) TANK 1 EAST 5/4/04 7 <0.210 <0.210 <0.210 <0.210 <0.084 <0.210 <4.2 <4.2 <4.2 (S-3/G W-1/G W-3) TANK 2 EAST 5/4/04 7 <0.170 <0.170 <0.170 <0.170 <0.068 <0.170 <3.4 <3.4 <3.4 (S-3/G W-1/G W-3) TANK 3 EAST 5/4/04 7 <0.210 <0.210 <0.210 <0.210 <0.084 <0.210 <4.2 <4.2 <4.2 (S-3/G W-I/G W-3) TANK 4 EAST 5/4/04 7 <0.150 <0.150 <0.150 <0.150 <0.059 <0.150 <2.9 <2.9 <2.9 (S-3/G W-1/G W-3) TANK I BOTTOM 5/4/04 12 <0.210 0.340 <0.210 <0.210 0G6 <0.210 12.7 6.19 6.4 (S-3/G W-1/G W-3) f i TANK 2 BOTTOM 5/4/04 12 <0.170 <0.170 <0.170 <0.170 0.096 <0.170 <3.4 <3.4 <3.4 (S-3/G W-1/G W-3) TANK 3 BOTTOM 5/4/04 12 <0.260 <0.260 <0.260 <0.260 0.207 70.260 <5.3 <5.3 <5.3 (S-3/GW-I/GW-3) TANK 4 BOTTOM 5/4/04 12 <0.240 <0.240 <0.240 <0.240 <0.097 <0.240 <4.8 <4.8 <4.8 (S-3/G W-1/G W-3) NE DISP BOTT 5/6/04 4 <0.400 <0.400 <0.400 <0.400 <0.160 <0.400 <7.9 <7.9 <7.9 (S-3/GW-I/GW-3) SE DISP BOTT 5/6/04 4 <0.340 <0.340 <0.340 <0.340 <0.140 <0.340 <6.8 <6.8 <6.8 (S-3/G W-1/G W-3) SW DISP BOTT 5/6/04 4 <0.390 <0.390 <0.390 <0.390 <0.160 <0.390 <7.8 <7.8 <7,8 (S-3/G W-I/G W-3) NW DISP BOTT 5/6/04 4 <0.380 <0.380 <0.380 <0.380 <0.150 <0.380 <7.5 <7.5 <7.5 (S-3/G W-1/G W-3) EXCOI 5/10/04 3 0.612 31.2 19.3 67.6 MP48 3.06 0,111E <10 ;• (S-3/GW-I/GW-3) EXCO2 5/10/04 3.5 <0.4 19.1 14.9 7254 a 1 4 81.9 <8.0 s #3 (S-3/GW-I/GW-3) :.<.€ „✓ & d ... EXC03 5/]0/04 3.5 <0.390 <0.390 <0.390 <0.390 <0.150 <0.390 <7.7 <7.7 <7.7 (S-3/G W-I/G W-3) EXC04 5/10/04 3.5 <0.370 7370 <0.370 1 <0.370 0.193 <0.370 <7.4 <7.4 <7.4 (S-3/G W-1/G W-3) Notes: MtBE-methyl tert-butyl ether ug/g-micrograms per gram(parts per million) <0.2-not detected(method detection limit included) Shading-reported concentration exceeds the applicable standards MCP Soil Standard-Massachusetts Contingency Plan Method 1 Risk Characterization Standard for soil GEOLOGIC SERVICES CORPORATION 7/8/2004 science,engineering&technology Ref.#000509_Tbl_soil-vph 15 Bonazzoli Ave.,Hudson,MA APPENDIX D Soil Laboratory Analytical Results MAY 2 12004 New England OS/19/04 %c=LrrEm Technical Report for Shell Oil GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Cost Element# 707542 Accutest Job Number: M39256 Sampling Date: 05/05/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 13 mft %0ACCO, 4 Test results contained within this data package meet the requirements Zeza and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications:MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 0 495 Tech Center West 0 Building 1 ■Marlborough,MA 01752 ■ tel:508-481-6200 0 fax:508481-7753 ■ http://www.accutest.com Accutest Laboratories Sample Summary Shell Oil Job No: M39256 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Project No: Cost Element# 707542 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M39256 1 05/05/04 12:00 MW 05/06/04 SO Soil FOJSTBTT(6 7'� ................................ i�39256 05/05/04 12:05 MW 05/06/04 SO Soil FOISTNW:(3 4' IyI39256 3 05/05/04 12:10 MW 05/06/04 SO Soil FOCSTEW(3 1vi392564 05/05/04 12:15 MW 05/06/04 SO Soil FOU;STSIN'(3 4') :; ..... ............................................................... ......... . N13925. 5 05/05/04 12:20 MW 05/06/04 SO Soil F©iJSTVI!ZtJ:{3-4') i Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTBOTT(6-T) Lab Sample ID: M39256-1 Date Sampled: 05/05/04, Matrix: SO- Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 94.1 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P027769.D 1 05/14/04 ME 05/08/04 OP7126 GPO1851 Run#2 Initial Weight Final Volume Run#1 10.6g 2.0ml Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene ND 500 ug/kg 208-96-8 Acenaphthylene ND 500 ug/kg 120-12-7 Anthracene ND 500 ug/kg 56-55-3 Benzo(a)anthracene ND 500 ug/kg 50-32-8 Benzo(a)pyrene ND 500 ug/kg 205-99-2 Benzo(b)fluoranthene ND 500 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 500 ug/kg 207-08-9 Benzo(k)fluoranthene ND.....;.;..., 500 ug/kg 218-01-9 ChryseneiD...;; ..... 500 ug/kg ........................... 53-70-3 Dibenz(a,h)anthracene ND 500 ug/kg 206-44-0 Fluoranthene ND ... 500 ug/kg 86-73-7 Fluorene ND 500 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 500 ug/kg 91-57-6 2-Methylnaphthalene 1VD 500 ug/kg 91-20-3 Naphthalene ND 500 ug/kg 85-01-8 Phenanthrene ND 500 ug/kg 129-00-0 Pyrene NA 500 ug/kg CI I-C22 Aromatics(UnadJ ) ND 17000 ug/kg C9-C18 Aliphatics ND 6000 ug/kg C19-06 Aliphatics ND 8100 ug/kg CI I-C22 Aromatics NU 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 79% 40-140% 321-60-8 2-Fluorobiphenyl $41i 40-140% 580-13-2 2-Bromonaphthalene 56% 40-140% 3386-33-2 1-Chlorooctadecane 87% 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTNW (3-4') Lab Sample ID: M39256-2 Date Sampled: 05/05/04 Matrix: SO- Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 97.3 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27770.D 1 05/14/04 ME 05/08/04 OP7126 GPO1851 Run#2 Initial Weight Final Volume Run#1 10.5 g 2.0 all Run#2 CAS No. Compound Result RL Units Q _._ ... ........................... 83-32-9 Acenaphthene N:..D_..._ .;; 490 ug/kg ND 208-96-8 Acenaphthylene 490 ug/kg 120-12-7 Anthracene ND 490 ug/kg 56-55-3 Benzo(a)anthracene ND 490 ug/kg 50-32-8 Benzo(a)pyrene ND 490 ug/kg 205-99-2 Benzo(b)fluoranthene ND 490 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 490 ug/kg 207-08-9 Benzo(k)fluoranthene ND 490 ug/kg 218-01-9 Chrysene ND 490 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 490 ug/kg 206-44-0 Fluoranthene ND 490 ug/kg 86-73-7 Fluorene ND 490 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 490 ug/kg 91-57-6 2-Methylnaphthalene ND 490 ug/kg 91-20-3 Naphthalene ND:........... . 490 ug/kg 85-01-8 Phenanthrene ND 490 ug/kg 129-00-0 Pyrene :ND.:;;:;::;;::; :::: 490 ug/kg C 11-C22 Aromatics (UnadJ ) .ND.,... 17000 ug/kg C9-C18 Aliphatics N:D. 5900 ug/kg C19-C36 Aliphatics N.:.D .... .._ ..; 7800 ug/kg CI I-C22 Aromatics ND 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 80% <::;: 40-140% 321-60-8 2-Fluorobiphenyl 87% 40-140% 580-13-2 2-Bromonaphthalene 67% 40-140% 3386-33-2 1-Chlorooctadecane 82%... .. :.; 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTEW(3-4') Lab Sample ID: M39256-3 Date Sampled: 05/05/04 Matrix: SO - Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 96.3 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA I File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27771.1) 1 05/14/04 ME 05/08/04 OP7126 GPO1851 Run#2 Initial Weight Final Volume Run#1 10.4g 2.0m1 Run#2 CAS No. Compound Result RL Units Q ........................... 83-32-9 Acenaphthene ND 500 ug/kg 208-96-8 Acenaphthylene ND 500 ug/kg 120-12-7 Anthracene ND 500 ug/kg 56-55-3 Benzo(a)anthracene ND 500 ug/kg 50-32-8 Benzo(a)pyrene ND 500 ug/kg 205-99-2 Benzo(b)fluoranthene ND 500 ug/kg 191-24-2 Benzo(g,h,i)perylene ND; :.<::.:: 500 ug/kg 207-08-9 Benzo(k)fluoranthene ND 500 ug/kg 218-01-9 Chrysene ND 500 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 500 ug/kg 206-44-0 Fluoranthene ND . 500 ug/kg 86-73-7 Fluorene ND ... . 500 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 500 ug/kg 91-57-6 2-Methylnaphthalene ND 500 ug/kg 91-20-3 Naphthalene ND 500 ug/kg 85-01-8 Phenanthrene ND 500 ug/kg 129-00-0 Pyrene ND 500 ug/kg .::::...............:.. :.: ........................... CI I-C22 Aromatics(Unadj ) ND 17000 ug/kg C9-C18 Aliphatics hID 6000 ug/kg C19-C36 Aliphatics ND 8000 ug/kg CI I-C22 Aromatics ND 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 78%,. , 40-140% 321-60-8 2-Fluorobiphenyl &5% 40-140% 580-13-2 2-Bromonaphthalene 61% 40-140% 3386-33-2 1-Chlorooctadecane 8.0%.......; 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTSW(3-4') Lab Sample ID: M39256-4 Date Sampled: 05/05/04 Matrix: SO-Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 97.7 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P027772.D 1 05/14/04 ME 05/08/04 OP7126 GP01851 Run#2 Initial Weight Final Volume Run#1 10.2 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene NI3 500 ug/kg 208-96-8 Acenaphthylene ND 500 ug/kg 120-12-7 Anthracene ND:.;:.;;:.;>::;:.;; 500 ug/kg 56-55-3 Benzo(a)anthracene N.D 500 ug/kg 50-32-8 Benzo(a)pyrene ND:::::::: 500 ug/kg 205-99-2 Benzo(b)fluoranthene N.13 500 ug/kg 191-24-2 Benzo(g,h,i)perylene NI3 500 ug/kg 207-08-9 Benzo(k)fluoranthene ND 500 ug/kg 218-01-9 Chrysene ND 500 ug/kg 53-70-3 Dibenz(a,h)anthracene N..:D 500 ug/kg 206-44-0 Fluoranthene Np 500 ug/kg 86-73-7 Fluorene ND 500 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND.:;:;:;;::;;>;:; 500 ug/kg 91-57-6 2-Methylnaphthalene ND.....:.:. :::.';i. :;; 500 ug/kg 91-20-3 Naphthalene ND.:........ ...' 500 ug/kg 85-01-8 Phenanthrene N.D. ..,.._.;...;'i 500 ug/kg .........................:. ........................... 129-00-0 Pyrene N:.D 500 ug/kg CII-C22 Aromatics(UnadJ ) ND 17000 ug/kg C9-C18 Aliphatics ND 6000 ug/kg C19-06 Aliphatics N.. 8000 ug/kg C11-C22 Aromatics ND 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 84-15-1 o-Terphenyl 7;G%..,.,.,. ;; 40-140% 321-60-8 2-Fluorobiphenyl 82% 40-140% 580-13-2 2-Bromonaphthalene 6Q% 40-140% 3386-33-2 1-Chlorooctadecane 7:9.%;;; 40-140% .................. .... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTWW(3-4') Lab Sample ID: M39256-5 Date Sampled: 05/05/04 Matrix: SO- Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 93.2 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27773.13 1 05/14/04 ME 05/08/04 OP7126 GPO1851 Run#2 Initial Weight Final Volume Run#1 10.1 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene <ND 530 ug/kg 208-96-8 Acenaphthylene N1.D 530 ug/kg 120-12-7 Anthracene ND 530 ug/kg 56-55-3 Benzo(a)anthracene ND 530 ug/kg 50-32-8 Benzo(a)pyrene ND 530 ug/kg 205-99-2 Benzo(b)fluoranthene ND 530 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 530 ug/kg N 207-08-9 Benzo(k)fluoranthene D 530 ug/kg 218-01-9 Chrysene ND 530 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 530 ug/kg ........................... 206-44-0 Fluoranthene ND 530 ug/kg 86-73-7 Fluorene ND 530 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 530 ug/kg 91-57-6 2-Methylnaphthalene ND 530 ug/kg 91-20-3 Naphthalene ND 530 ug/kg 85-01-8 Phenanthrene ND 530 ug/kg 129-00-0 Pyrene ND 530 ug/kg CI I-C22 Aromatics (UnadJ ) ND 18000 ug/kg C9-C18 Aliphatics ND 6400 ug/kg C19-06 Aliphatics ND 8500 ug/kg C11-C22 Aromatics ND 18000 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ....................... 84-15-1 o-Terphenyl $:2..%. 40-140% 321-60-8 2-Fluorobiphenyl 40-140% 580-13-2 2-Bromonaphthalene 52% 40-140% 8' 3386-33-2 1-Chlorooctadecane .1% 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MADEP EPH FORM Nlatrz, A ueous Soil Sediment Other Contarners r -' Satisfacto Broken F1 Leakin A 'ueous Preservatnres N/A H <=2 Ir PH > 2 LI Tem erature . Received on Ice Received at 4 Deg. C Other d Reed at 2 deg C ztractron, Vleth�d SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTBOTT(6-7') Lab ID: M39256-1 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/8/2004 5/14/2004 N/A Solids: Low Dilution: High Dilution: � EPH Fractionation 2-Fluorobiphenyl 9 Surrogate Standards. 2-Bromonaphthalene 94'1 1 N/A Unadjusted Ranges CAS# Units Result RDL C3 C11-C22 Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 500 iPhenanthrene 85-01-8 ug/kg ND 500 Acenaphthene 83-32-9 ug/kg ND 500 Naphthalene 91-20-3 ug/kg ND 500 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 500 Anthracene 120-12-7 ug/kg ND 500 Benzo(a)anthracene 56-55-3 ug/kg ND 500 Benzo(a)pyrene 50-32-8 ug/kg ND 500 Benzo(b)fluoranthene 205-99-2 ug/kg ND 500 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 500 Benzo(k)fluoranthene 207-08-9 ug/kg ND 500 Chrysene 218-01-9 ug/kg ND 500 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 500 Fluoranthene 206-44-0 ug/kg ND 500 Fluorene 86-73-7 ug/kg ND 500 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 500 Pyrene 129-00-0 ug/kg ND 500 Adjusted Ranges C9-C18 Aliphatics ug/kg ND A 6000 C19-C36 Aliphatics ug/kg ND A 8100 C11-C22 Aromatics ug/kg ND B 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 87 40-140% j o-Terphenyl % 79 40-140% 2-Fluorobiphenyl % 84 40-140% 2-Bromonaphthalene % 56 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? Yes ❑ No.Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 0 Yes ❑ No.Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature _ Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP EPH FORM Aqueous Soil W Sediment n Other Contatners>, Satisfacto Broken Leaking A ueousPeservatives= N/A H <= 2 F1 PH > 2 rature y` Received on Ice F1 Received at 4 Deg.C R Other W Rec'd at 2 deg C E>StEactron Method „ . SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTNW(34) Lab ID: M39256-2 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/8/2004 5/14/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 97.3 1 N/A Unadiusted Ranges CAS# Units Result RDL (3 C11-C22 Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 490 Phenanthrene 85-01-8 ug/kg ND 490 Acenaphthene 83-32-9 ug/kg ND 490 fNaphthalene 91-20-3 ug/kg ND 490 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND . 490 Anthracene 120-12-7 ug/kg ND 490 Benzo(a)anthracene 56-55-3 ug/kg ND 490 Benzo(a)pyrene 50-32-8 ug/kg ND 490 Benzo(b)fluoranthene 205-99-2 ug/kg ND 490 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 490 Benzo(k)fluoranthene 207-08-9 ug/kg ND 490 Chrysene • 218-01-9 ug/kg ND 490 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 490 Fluoranthene 206-44-0 ug/kg ND 490 Fluorene 86-73-7 ug/kg ND 490 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 490 Pyrene 129-00-0 ug/kg ND 490 Adjusted Ranges C9-C18 Aliphatics ug/kg ND A 5900 C19-C36 Aliphatics ug/kg ND" 7800 C11-C22 Aromatics ug/kg ND 8 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 82 40-140% o-Terphenyl % 80 40-140% 2-Fluorobiphenyl % 87 40-140% 2-Bromonaphthalene % 67 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A'Y qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? 0 Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.37 V No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP EPH FORM MatciSt Wiz...,. , _ yam;' A ueous Soil Sediment Other Cantatners , Satisfactory n./ Broken Leaking A ueotis�Pr serYatfves' NIA H <=2 F, PH > 2 Teiti ;v ratur _ r Received on Ice Received at 4 De . C Other d Rec'd at 2 deg C F�ctca±cttonNletocC SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTEW(34) Lab ID: M39256-3 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/8/2004 5/14/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 96.3 1 N/A Unadjusted Ranges CAS# Units Result RDL (3 C71-C22 Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 500 Phenanthrene 85-01-8 ug/kg ND 500 Acenaphthene 83-32-9 ug/kg -ND 500 Naphthalene 91-20-3 ug/kg ND 500 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 500 Anthracene 120-12-7 ug/kg ND 500 Benzo(a)anthracene 56-55-3 ug/kg ND 500 Benzo(a)pyrene 50-32-8 ug/kg ND 500 Benzo(b)fluoranthene 205-99-2 ug/kg ND 500 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 500 Benzo(k)fluoranthene 207-08-9 ug/kg ND 500 Chrysene 218-01-9 ug/kg ND 500 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 500 Fluoranthene 206-44-0 ug/kg ND 500 Fluorene 86-73-7 ug/kg ND 500 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 500 Pyrene 129-00-0 ug/kg ND 500 Adiusted Ranges C9-Cl8Aliphatics ug/kg ND" 6000 C19-C36 Aliphatics ug/kg ND" 8000 C11-C22 Aromatics ug/kg ND B 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 80 40-140% o-Terphenyl % 78 40-140% 2-Fluorobiphenyl % 85 40-140% 2-Bromonaphthalene % 61 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 91 Yes ❑ No.Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP EPH FORM Manx Aclueous Soil Sediment i I Other Containers: ,, Satisfacto ry Broken Leaking tfousP-reseatives N/A H<=2 F1 PH > 2 ❑ eri a atu e` Received on Ice Received at 4 Deg. CI Other d Reed at 2 deg C ExtracrttoniAethod _ SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTSW(3-4') Lab ID: M39256-4 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/8/2004 5/14/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 97.7 1 N/A Unadiusted Ranges CAS# Units Result RDL (� C11-C22 Aromatics(Unadj.) ug/kg ND A 17000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 500 Phenanthrene 85-01-8 ug/kg ND 500 Acenaphthene 83-32-9 ug/kg ND 500 Naphthalene 91-20-3 ug/kg ND 500 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 500 Anthracene 120-12-7 ug/kg ND 500 Benzo(a)anthracene 56-55-3 ug/kg ND 500 Benzo(a)pyrene 50-32-8 ug/kg ND 500 Benzo(b)fluoranthene 205-99-2 ug/kg ND 500 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 500 Benzo(k)fluoranthene 207-08-9 ug/kg ND 500 Chrysene 218-01-9 ug/kg ND 500 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 500 Fluoranthene 206-44-0 ug/kg ND 500 Fluorene 86-73-7 ug/kg ND 500 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 500 Pyrene 129-00-0 ug/kg ND 500 Adiusted Ranges C9-C18 Aliphatics ug/kg ND A 6000 C19-C36 Aliphatics ug/kg ND" 8000 C11-C22 Aromatics ug/kg ND a 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 79 40-140% o-Terphenyl % 76 40-140% 2-Fluorobiphenyl % 82 40-140% 2-Bromonaphthalene % 60 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A'X qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? 0 Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 0 Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? V No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP EPH FORM li<latrx f Aqueous Soil Sediment Other ContaiFners �F mWx,: Satisfacto Broken Leakin A�tieotis Prese�rvattves N/A H<=2 F1 PH >2 k .> Redd at 2 de C exn Matte .' Received on Ice Received at 4 Deg. C Other g �icacton'SMe'thol SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTWW(34) Lab ID: M39256-5 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl_ 5/8/2004 5/14/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 93.2 1 N/A Unadjusted Ranges CAS# Units Result RDL Q C11-C22 Aromatics(Unadj.) ug/kg ND A 18000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 530 Phenanthrene 85-01-8 ug/kg ND 530 Acenaphthene 83-32-9 ug/kg ND 530 Naphthalene 91-20-3 ug/kg ND 530 Other Target PAH Analvtes Acenaphthylene 208-96-8 ug/kg ND 530 Anthracene 120-12-7 ug/kg ND 530 Benzo(a)anthracene 56-55-3 ug/kg ND 530 Benzo(a)pyrene 50-32-8 ug/kg ND 530 Benzo(b)fluoranthene 205-99-2 ug/kg ND 530 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 530 Benzo(k)fluoranthene 207-08-9 ug/kg ND_ 530 Chrysene 218-01-9 ug/kg ND 530 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 530 Fluoranthene 206-44-0 ug/kg ND 530 Fluorene 86-73-7 ug/kg ND 530 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 530 Pyrene 129-00-0 ug/kg ND 530 Adiusted Ranges C9-C18 Aliphatics ug/kg ND" 6400 C19-C36 Aliphatics ug/kg ND" 8500 C11-C22 Aromatics ug/kg NO a 18000 Surrogate Recoveries Acceptance Ranqe 1-Chlorooctadecane % 81 40-140% o-Terphenyl % 82 40-140% 2-Fluorobiphenyl % 87 40-140% 2-Bromonaphthalene % 62 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A'J'qual"dier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.37 No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Postition Laboratory Director Signature Printed Name Reza Tand Date 5/19/2004 �t3gas6 ACCUTEST B.: 495 TECHNOLOGY CENTER WEST • BUILDING ONE MARLBOROUGH,MA 01752 ACCUTEST QUOTE rr: L a b o x a t o r i e s TEL:508.481-6200 • FAX.•508-481-7753 CUENT INFORMATION ('� FACILITY INFORMATION7�pp�S ANALYTICAL INFORMATION MATRIX CODES l YPl1rIC)Ej i 7��V I C�� l IJ7rC� S Pm 0.Ard:5 �� DW• DRINKINGPROJECT NAME WATER GW• WATER AD 017q 7 LOCATION. , O WW- WASTE WATER CITY, /� � STATE ZIP PROJECT, 0. SO• SOIL Flo SL• SLUDGE OI• OIL SEND REPORT T O LIQ- OTHER PHONE# -.� --A7�j/(� FAX# 7.Tg-';���• ��f�p LIQUID SOL•OTHER COLLECTION M PRESERVATION ACCUTEST �� Q,,, SOLID SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLEDLij BY: s LAB USE ONLY 1 s -a _ r 3 rQ I I 1 ~ I `s- FO 1 DATA TURNAROUND INFORMATION q r DATA DELIVERABLE INFORMATION ti°{, COMMENTS/REMARKS '' 14 DAYS STANDARD APPROVED BY: ❑ STANDARD `{ AA _ L•V� 7 DAYS RUSH ❑ COMMERCIAL"B" ❑ 48 HOUR EMERGENCY ❑ DISK DELIVERABLE ❑ OTHER ❑ STATE'FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) LOC , '�E DATA UNLESS PREVIOUSLY APPROVED AMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLE E POSSESION,INCLUDING COURIER DELIVERY RE�I/Ij9pUISHED BY SA L . DATE I E: RECEIVED BY: /� REU IS ED. DAT TIM RECEIVED BY: 1./��CCJ) �'s'�r ��6 1. cr �. 1"�-i 2. p! 2. 4-41 RELIN UISHED BY: DATE TIME: , RECEIVED BY: RELINQUISHED BY: D T ME. RECEIVED BY: 7771 3. � � 4. 4. RELINQUISHED BY: DA ET E. RECEIVEb BY: SEAL 0 PRESERVE WHERE APPLICABLE ONg TE P� ERATURE �® New England MAY 2 6 M. 05/25/04 ®ACCUTEST L a b o r a t o r i e s Teenical Rept�rt for Shell Oil GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Cost Element#707542 Accutest Job Number: M39366 Sampling Date: 05/10/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 19 `4E��M h[tpgO'� Z Test results contained within this data package meet the requirements Aand of the National Environmental Laboratory Accreditation Conference Lab b Director and/or state specific certification programs as applicable. Certifications:MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 495 Tech Center West■ Building 1 0 Marlborough,Mt 01752 0 tel:508481-6200■ fax:508481-7753 0 bttp://www.accutest.com -MEN L a b o r a t o r i e s SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M39366 Site: GSCMA:96925028 1140 Iyannough Rd.Hyannis MA Report Date 5/25/2004 2:39:05 PM 3 Sample(s),collected on 05/10/2004 and were received at Accutest on 05/12/2004 properly preserved,at 1.5 Deg.C and intact. These Samples received an Accutest job number of M39366.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Extractables by GC By Method MADEP EPH 98-1 Matrix: SO Batch ID: OP7150 ■ All samples were extracted within the recommended method holding time. ■ All samples were analyzed within the recommended method holding time. ■ All method blanks for this batch meet method specific criteria. ■ Sample(s) M39379-1MS,M39379-1MSD,OP7150-MSMSD were used as the QC samples indicated. Wet Chemistry By Method EPA 160.3 M Matrix: SO Batch ID: GN13858 ■ Sample(s) M39386-14DUP were used as the QC samples for Solids,Percent. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M39366). Tuesday,May 25,2004 Page 1 of 1 2 Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 22 May.2003 Revision No. 3.1 Bureau of Waste Site Cleanup Final Page 13 of 30 Title: MADEP MCP Response Action Analytical Report Certification Form "�K. rrai 1" UP Laboratory Name: Accutest Laboratories of New En land Project#: M39366 Project Location: MADEP RTN None GSCMA:96925028 1140 I annou h Rd.Hyannis MA This form provides certifications for the following data set: M39366-1,M39366-2,M39366-3 Sample Matrices: Groundwater Soil/Sediment X Drinking Water Other: M- 8260B 8151A 8330 601013 7470AIIA otl 8270C 8081A VPH 6020 9014M 2 8082 d 8021 B EPH X 7000 S 3 7196A An affirmative response to questions A,B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with Yes ❑ No ' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards orguidelines? Does the analytical data included in this report meet all the requirements C for"Presumptive Certainty",as described in Section 2.0 of the MADEP F1 Yes ❑No ' document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without Yes ❑No ' significant modifications,as specified in Section 11.3? A response to questions E and F below is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the Yes U No ' s ecified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified Yes U No ' methods reported? AM Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief, accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 5125104 3 Accutest Laboratories Sample Summary Shell Oil Job No: M39366 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Project No: Cost Element #707542 __..._._.. ............................. Sample Coltetei _ Matrix Client ..:............ Number Date Time By Received Code Type Sample ID 2 Soil/04 10:10MW OS/1 /04 SO ,:. ...>>M39366 1: OS/10 .. SP.OTT 5.:.::. S Soil 1 10 20 MW OS/12/04 O M39 6:f 2<<> OS/ 0/04 EGOS:::.. ::«:>:: »»>:»»:::::>::><:>:::::::>.........:::::<::::: ....... ...........:.. /04 1 40 MW OS/12/04 SO Soi l ay1393:6f3> OS/10 0. »]✓XG( > . ;::::>::>::: Soil samples reported on a dry weight basis unless otherwise indicated on result page. 4 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: D DISP BOn (5') Lab Sample ID: M39366-1 Date Sampled: 05/10/04 Matrix: SO- Soil Date Received: 05/12/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 95.3 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25908.13 1 05/18/04 SL 05/13/04 OP7150 GGH2375 Run#2 Initial Weight Final Volume Run#1 10.3 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene Nb 510 ug/kg 208-96-8 Acenaphthylene ND << 510 ug/kg ........................... ........................... ........................... 120-12-7 Anthracene NA;; ;;> ; 510 ug/kg ...................:....... ........................... 56-55-3 Benzo(a)anthracene 1II) ; » 510 ug/kg 50-32-8 Benzo(a)pyrene N] ........._ 510 ug/kg .:.:.:..................... ......................... ........................... 205-99-2 Benzo(b)fluoranthene ND.; 510 ug/kg .:..:...:.................. ........................... ........................... 191-24-2 Benzo(g,h,i)perylene Ni510 ug/kg 207-08-9 Benzo(k)fluoranthene NI3 510 ug/kg 218-01-9 Chrysene D.;_.;::::.;_.;; ;;; 510 ug/kg ........................... ......... ..... 53-70-3 Dibenz(a,h)anthracene ND < 510 ug/kg .......................... ........................... 206-44-0 Fluoranthene N13 < >> ' 510 ug/kg 86-73-7 Fluorene IVD 510 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ;,,:;,;::;:: 510 ug/kg 91-57-6 2-Methylnaphthalene 510 ug/kg ........................... ........................... 91-20-3 Naphthalene Il);<;' ; ; ; 510 ug/kg .......................... ........................... .......................... 85-01-8 Phenanthrene N:I); i ' ; 510 ug/kg ......................:.... __.._......._..... 129-00-0 Pyrene ht "'<<> 510 ug/kg CI I-C22 Aromatics (Unadj.) 57900.::;::;. :::. 17000 ug/kg C9-C18 Aliphatics 1 4fl00 61W ug/kg C19-C36 Aliphatics sI(kt (l4} 8200 ug/kg .................:......... ........................... CI I-C22 Aromatics V60.0;>» >i< 17000 ug/kg ................... CAS No. Surrogate Recoveries Runt/ 1 Run#2 Limits ......_.... 84-15-1 o-Terphenyl 9494 40-140% 321-60 8 2-Fluorobiphenyl 81% 40-140% 580-13-2 2-Bromonaphthalene Ii % 40-140% 3386-33-2 1-Chlorooctadecane 72%. 40-140% ND = Not detected I = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 5 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: EXCOS(4') Lab Sample ID: M39366-2 Date Sampled: 05/10/04 Matrix: SO- Soil Date Received: 05/12/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 92.4 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25909.D 1 05/18/04 SL 05/13/04 OP7150 GGH2375 Run#2 Initial Weight Final Volume Run#1 10.5 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q ........................... 83-32-9 Acenaphthene ND 510 ug/kg 208-96-8 Acenaphthylene I[I s . 510 ug/kg ........................... ........................... ........................... 120-12-7 Anthracene NDi> < : 510 ug/kg 56-55-3 Benzo(a)anthracene ND `<>i.510 ug/kg 50-32-8 Benzo(a)pyrene NTH ; ; 510 ug/kg 205-99-2 Benzo(b)fluoranthene NT�> 510 ug/kg ........................... ........................... ........................... 191-24-2 Benzo(g,h,i)perylene ND< ;> 510 ug/kg 207-08-9 Benzo(k)fluoranthene NI >< 510 ug/kg 218-01-9 Chrysene N1 ; i 510 ug/kg 53-70-3 Dibenz(a,h)anthracene Nt ;' 510 ug/kg 206-44-0 Fluoranthene >ND _510 ug/kg 86-73-7 Fluorene Nn >» > 510 ug/kg ..................I........ ...................... .....D.................. 193-39-5 Indeno(1,2,3-cd)pyrene NI)<>< < ; > 510 ug/kg 91-57-6 2-Methyinaphthalene ND 510 ug/kg 91-20-3 Naphthalene ND 510 ug/kg 85-01-8 Phenanthrene ND 510 ug/kg 129-00-0 Pyrene NDi _' 510 ug/kg C11-C22 Aromatics(Unadj.) $3:20Ori; 17000 ug/kg C9-C18 Aliphatics f62((Q ' 6200 ug/kg ' C19-06 Aliphatics 1;46Q40.:;....; 8200 ug/kg ..:...:.:.................. ........................... ........................... C 11-C22 Aromatics $280( <»»> 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... ......................... 84-15-1 o-Terphenyl 79% 40-140% 321-60 8 2-Fluorobiphenyl 82% 40-140% C 580-13-2 2-Bromonaphthalene :fi% _ 40-140% 3386-33-2 1-Chlorooctadecane 63:%.::::;.;;::: 40-140% ......................... ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: EXCO6(4') Lab Sample ID: M39366-3 Date Sampled: 05/10/04 Matrix: SO- Soil Date Received: 05/12/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 87.3 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25910.D 1 05/18/04 SL 05/13/04 OP7150 GGH2375 Run#2 Initial Weight Final Volume Run#1 10.7 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q ........................... ........................... 83-32-9 Acenaphthene ND<<_> >< 530 ug/kg 208-96-8 Acenaphthylene ;:;;;:;:;: 530 ug/kg 120-12-7 Anthracene ND:.:;.,::: ;` 530 ug/kg 56-55-3 Benzo(a)anthracene NI):;;:;;:::;::::;::: :;:: 530 ug/kg 50-32-8 Benzo(a)pyrene NI3 530 ug/kg 205-99-2 Benzo(b)fluoranthene NTH;;_;;:;:::::> 530 ug/kg 191-24-2 Benzo(g,h,i)perylene ND ; >> 530 ug/kg 207-08-9 Benzo(k)fluoranthene ID ` 530 ug/kg ........:.....:............ .......................... 218-01-9 Chrysene I+1D ; 530 ug/kg 53-70-3 Dibenz(a,h)anthracene I ;, ;;.:,: :::;: 530 ug/kg 206-44-0 Fluoranthene D ;> 530 ug/kg 86-73-7 Fluorene NIA,.;;;:.;;;; 530. ug/kg ..............:............ .......................... .........................- 193-39-5 Indeno(1,2,3-cd)pyrene ND <s 530 ug/kg 91-57-6 2-Methylnaphthalene ND ; :;=530 ug/kg ........................... 91-20-3 Naphthalene NI3...,::,::_, .. 530 ug/kg 85-01-8 Phenanthrene ND 530 ug/kg 129-00-0 Pyrene ND 530 ug/kg CI I-C22 Aromatics (Unadj.) :.NTA.;.:,.>.,,,:;;>:.: 18000 ug/kg ... . .. ............ .................... . C9-C18 Aliphatics h1Di; 6400 ug/kg C19-06 Aliphatics D .: :::; 8500 ug/kg ........................... CI I-C22 Aromatics ND>; 18000 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 84-15-1 o-Terphenyl 5%> 40-140% 321-60-8 2-Fluorobiphenyl ::: 40-140% . 580-13-2 2-Bromonaphthalene 6 % 40-140% ...................... ......................... _.... 3386-33-2 1-Chlorooctadecane 66%.......; r> 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 MADEP EPH FORM Aqueous ❑ Soil Sediment f-1 Other nt `in Satisfactory v' Broken Leaking Ats Ne eserva tuies== NIA .i pH <=2 1 PH > 2 Received on Ice Received at 4 Deg. C F1 Other F,/-1 ReC'd at 1.5 deg C u „ ROOM- SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: D DISP BOTT(5') Lab ID: M39366-1 Method for Targets: MADEP EPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/13/2004 5/18t2004 N/A Solids: Low Dilution: High Dilution: EPH Fractionation 2-Fluorobiphenyl 9 Surrogate Standards. 2-Bromonaphthalene 95"3 1 N/A Unadjusted Ranges CAS# Units Result RDL g C11-C22 Aromatics(Unadj.) ug/kg 57900 A 17000 Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 510 Phenanthrene 85-01-8 ug/kg ND 510 Acenaphthene 83-32-9 ug/kg ND 510 Naphthalene 91-20-3 ug/kg ND 510 Other Target PAH Analvtes Acenaphthylene 208-96-8 ug/kg ND 510 Anthracene 120-12-7 ug/kg ND 510 Benzo(a)anthracene 56-55-3 ug/kg ND 510 Benzo(a)pyrene 50-32-8 ug/kg ND 510 Benzo(b)fluoranthene 205-99-2 ug/kg ND 510 Benzo(g,h,j)perylene 191-24-2 ug/kg ND 510 Benzo(k)fluoranthene 207-08-9 ug/kg ND 510 Chrysene 218-01-9 ug/kg ND 510 Dbenz(a,h)anthracene 53-70-3 ug/kg ND 510 Fluoranthene 206-44-0 ug/kg ND 510 Fluorene 86-73-7 ug/kg ND 510 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 510 Pyrene 129-00-0 ug/kg ND 510 Adiusted Ranges C9-C18 Aliphatics ug/kg 184000 A 6100 C19-C36 Aliphatics ug/kg 104000 A 8200 C11-C22 Aromatics ug/kg 576005 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 72 40-140% o-Terphenyl % 90 40-140% 2-Fluorobiphenyl % 87 40-140% 2-Bromonaphthalene % 71 40-140% Footnotes A Hydrocarbon Range data exclude concenbations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. Ct1-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? d❑No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand 8 Date 5/25/2004 MADEP EPH FORM Nattx F %saw Aqueous Ll Soil -/ Sediment Other 5nitrers � Satisfactory.i Broken Leaking �o�usf'cserr '' NIA H<=2 F1 PH> 2 Received on Ice Received at 4 Deg. C Other r/ Reed at 1.5 deg C a>cW-lV HERB' - SW846 3545 9ethod for Ranges: MADEP EPH 98-1 Client ID: EXC05(4) Lab ID: M39366-2 9ethod for Targets: MADEP EPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 :PH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/13/2004 5/18/2004 N/A Solids: Low Dilution: High Dilution: :PH Fractionation 2-Fluorobiphenyl 9 surrogate Standards. 2-Bromonaphthalene 92.4 1 N/A Inadiusted Ranges CAS# Units Result RDL Q C11-C22 Aromatics(Unadj.) ug/kg 83200 A 17000 Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 510 Phenanthrene 85-01-8 ug/kg ND 510 Acenaphthene 83-32-9 ug/kg ND 510 Naphthalene 91-20-3 ug/kg ND 510 )ther Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 510 Anthracene 120-12-7 ug/kg ND 510 Benzo(a)anthracene 56-55-3 ug/kg ND 510 Benzo(a)pyrene 50-32-8 ug/kg ND 510 Benzo(b)fluoranthene 205-99-2 ug/kg ND 510 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 510 Benzo(k)fluoranthene 207-08-9 ug/kg ND 510 Chrysene 218-01-9 ug/kg ND 510 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 510 Fluoranthene 20644-0 ug/kg ND 510 Fluorene 86-73-7 ug/kg ND 510 lndeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 510 Pyrene 129-00-0 ug/kg ND 510 Ldiusted Ranges C9-C18 Aliphatics ug/kg 162000 A 6200 C19-C36 Aliphatics ug/kg 146000 A 8200 C11-C22 Aromatics ug/kg 828008 17000 >urrogate Recoveries Acceptance Range 1-Chlorooctadecane % 63 40-140% o-Terphenyl % 79 40-140% 2-Fluorobiphenyl % 82 40-140% 2-Bromonaphthalene % 66 40-140% =ootnotes I Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range I Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes AV qualifier indicates an estimated value Nere all QAlQC procedures REQUIRED by the EPH Method followed? WYes ❑ No-Details Attatched Mere all performance/acceptance standards for required QA/QC procedures achieved? 0 Yes ❑ No-Details Attatched Nere any significant modifications made to the EPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the nformation,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand 9 Date 5/25/2004 MADEP EPH FORM Mati k� :1 Aqueous Soil Sediment F1 Other ti�eis Satisfacto Broken F1 Leakin AMP NIA H <=2 H>2 aitIre _ Received on Ice Received at 4 Deg. C Other -FVJ Rec'd at 1.5 deg C actal :`... et�iot� SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: EXC06(4) Lab ID: M39366-3 Method for Targets: MADEP EPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/13/2004 5/18/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 87.3 1 WA Unadiusted Ranges CAS# Units Result RDL (3 C11-C22 Aromatics(Unadj.) ug/kg ND" 18000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 530 Phenanthrene 85-01-8 ug/kg ND 530 Acenaphthene 83-32-9 ug/kg ND 530 Naphthalene 91-20-3 ug/kg ND 530 Other Target PAH Analvtes Acenaphthylene 208-96-8 ug/kg ND 530 Anthracene 120-12-7 ug/kg ND 530 Benzo(a)anthracene 56-55-3 ug/kg ND 530 Benzo(a)pyrene 50-32-8 ug/kg ND 530 Benzo(b)fluoranthene 205-99-2 ug/kg ND 530 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 530 Benzo(k)fluoranthene 207-08-9 ug/kg ND 530 Chrysene 218-01-9 ug/kg ND 530 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 530 Fluoranthene 206-44-0 ug/kg ND 530 Fluorene 86-73-7 ug/kg ND 530 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 530 Pyrene 129-00-0 ug/kg ND 530 Adiusted Ranges C9-C18Aliphatics ug/kg ND" 6400 C19-C36Aliphatics ug/kg ND" 8500 C11-C22 Aromatics ug/kg ND B 18000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 66 40-140% o-Terphenyl % 75 40-140% 2-Fluorobiphenyl % 82 40-140% 2-Bromonaphthalene % 66 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range 13 Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting In that range.C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAR Analytes Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? 0 Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand 10 Date 5/25/2004 Accutest Laboratories `�C Semi VOlatileS. . .. ..... ......... QC Data Summaries Includes the following where applicable: ■ Method Blank Summaries ■ Blank Spike Summaries ■ Matrix Spike and Duplicate Summaries ■ Surrogate Recovery Summaries 11 Method Blank Summary Page I of I Job Number: M39366 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP7150-MB GH25902.1) 1 05/18/04 SL 05/13/04 OP7150 GGH2375 The QC reported here applies to the following samples: Method: MADEP EPH 98-1 M39366-1, M39366-2, M39366-3 CAS No. Compound Result RL Units Q ........................... 83-32-9 Acenaphthene INDr ; i > ;500 ug/kg 208-96-8 Acenaphthylene . ' ;500 ug/kg .........._...._.... .. .................-........ ........................... 120-12-7 Anthracene A1;I) _> 500 ug/kg 56-55-3 Benzo(a)anthracene11 >;> ;500 ug/kg 50-32-8 Benzo(a)pyrene NI <>> ; `; 500 ug/kg 205-99-2 Benzo(b)fluoranthene 1 >> < 500 ug/kg ........................... ........................... 191-24-2 Benzo(g,h,i)perylene NIA> 500 ug/kg 207-08-9 Benzo(k)fluoranthene D ; 500 ug/kg 218-01-9 ChrysenefEa 500 ug/kg 53-70-3 Dibenz(a,h)anthracene 1'+Dz _>; 500 ug/kg 206-44-0 Fluoranthene D`` <; ` ; ; 500 ug/kg 86-73-7 Fluorene NI>; <` ; 500 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene NT ... 500 ug/kg 91-57-6 2-MethylnaphthalenetU> =< 500 ug/kg 91-20-3 Naphthalene NI?. 500 ug/kg ..................--....: ................_ .... 85-01-8 Phenanthrene D500 ug/kg 129-00-0 Pyrene NU:.:::: 500 ug/kg ................__,..... ........................... ........................... CI I-C22 Aromatics(Unadj.) Na 17000 ug/kg C9-C18 Aliphatics N;D . 6000 ug/kg C19-C36 Aliphatics ND....... : ,;: 8000 ug/kg C 11-C22 Aromatics ND.:. .. .:: 17000 ug/kg CAS No. Surrogate Recoveries Limits 7}84-15-1 o-Terphenyl ;1 40 140% 321-60-8 2-Fluorobiphenyl 5:5 40-140% 580-13-2 2-Bromonaphthalene 6:&:"�o:::::;;:::;::: :.;::;: 40-140% 3386-33-2 1-Chlorooctadecane 6?.%:::::::.::;.::: 40-140% .............._ . _.. ..._......._.... ............. 12 Blank Spike Summary Page 1 of 1 Job Number: M39366 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP7150-BS GH25903.1) 1 05/18/04 SL 05/13/04 OP7150 GGH2375 The QC reported here applies to the following samples: Method: MADEP EPH 98-1 M39366-1, M39366-2, M39366-3 Spike BSP BSP CAS No. Compound ug/kg ug/kg % Limits 83-32-9 Acenaphthene 4950 3780 7640-140 208-96-8 Acenaphthylene ND 40-140 120-12-7 Anthracene 4950 4350 $$< > > 40-140 56-55-3 Benzo(a)anthracene ND 40-140 50-32-8 Benzo(a)pyrene ND 40-140 205-99-2 Benzo(k)fluoranthene ND < 40-140 191-24-2 Benzo(g,h,i)perylene ND 40-140 207-08-9 Benzo(k)fluoranthene ND 40-140 218-01-9 Chrysene 4950 4520 9'1 _ 40-140 53-70-3 Dibenz(a,h)anthracene ND 40-140 206-44-0 Fluoranthene ND 40-140 86-73-7 Fluorene ND 40-140 193-39-5 Indeno(1,2,3-cd)pyrene ND 40-140 91-57-6 2-Methylnaphthalene ND 40-140 91-20-3 Naphthalene 4950. 3560 72 < <; 40-140 85-01-8 Phenanthrene ND 40-140 129-00-0 Pyrene 4950 4150 84 > 40-140 CI I-C22 Aromatics(Unadj.) 28100 50-150 a C9-C18 Aliphatics 9900 7040 7I:.,;,:;: : 40-140 C19-C36 Aliphatics 14900 12900 S7, 40-140 .................................. C11-C22 Aromatics ND 50-150 a CAS No. Surrogate Recoveries BSP Limits 84-15-1 o-Terphenyl 8b;lp = 40-140% 321-60-8 2-Fluorobiphenyl $;7:'1 <; 40-140% 580 13-2 2-Bromonaphthalene :;:731:.:;::;.;::::;:; :: 40-140% 3386-33-2 I-Chlorooctadecane 73%v..:.:._.. ;:;: 40-140% (a)Advisory control limits. 13 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M39366 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP7150-MS GH25904.13 1 05/18/04 SL 05/13/04 OP7150 GGH2375 OP7150-MSD GH25905.D 1 05/18/04 SL 05/13/04 OP7150 GGH2375 M39379-1 GH25906.13 1 05/18/04 SL 05/13/04 OP7150 GGH2375 The QC reported here applies to the following samples: Method: MADEP EPH 98-1 M39366-1, M39366-2, M39366-3 M39379-1 Spike MS MS MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPD 83-32-9 AcenaP hthene ND 5090 3470 68 > ' 3620 68< ii >> 40-140/51 Acena hth len 208 96 8 e ND ND ND 4 2-7 n r ne ND 120 1 A th ace 5090 6 - 39 0 fig::: ::: 417 5 - 5- Benzo a anthracene ND - 6 5 3 ND ND 1 ric> > >< 4 0 140/5 5 2-8 Benzo a rene ND 0 3 ND i»` ND n>`: 4 14 2 - -2 Benz fluoranthene ND -OS 99 o ND .. ND >n'> >> (b) C .. 40 140/5 -24-2 Be h i len D i 191 nzo e N ND . ND 4 g Pery 2 7- - Benz k flu ranthene ND 1 0 08 9 0 o ND ND nc». 40 140/ .......: 5 2 O1- sene ND 0 18 9 5090 4 7 1 0 `` 441$2 ...... 0 83 >>s» b > > 40 140/5 Chry ................. 53-70-3 Dibenz a h anthracene ND ND ND nc> >> 40-140/51 ( , ) - - i 206 44 0 Fluoranthene ND ND N D 4 4 /nc 01 05 86-73 7 Fluorene ND ND ND e. 40-140/5 i .:.::::::::: 1 In 2 r - i 93 39 5 deno 1 3 cd ene ND ND ND 14 ( > )PY 91 57 6 2-Meth Ina hthalene ND ND Y P ND 14 1 62 2 <91-20 3 Naphthalene N D 5090 3210 > 40 140/5i3280 85 01-8 Phenanthrene ND ND - i ND »> ' c > > 40 140/5 - - _ ne 129 00 0 re ND 5 0 4 09 110 81— 4360 '82 >< » 40 140/5 Py .:::::::.:::.:.: CI I-C22 Aromatics(Unad'.) ND 27900 30000 7 « 50-150/3 J C9-C18 Ali hatics 5740 10200 12600 <6.> 13500 >?'> 40-140/5 P Z.......... 73 ....,:..... ....... ............................... .._......... ..................... ............ .................- ......... C19-C36 Aliphatics 6850 15300 20200 87 ; 2I100 89<; 4 ; 40-140/5 CI I-C22 Aromatics ND ND »> 50-150/3 i N n`> > . ..... . ....:..:...... CAS No. Surrogate Recoveries MS MSD M39379-1 Limits .................................................................................... 84-15-1 o-Te hen 1 83>a=<> »>< :::> rP Y % 84.%g :>> $ .°�o.<< 40 140% .......... 40- 7 % 0 140%»> > 7 321-60-8 2-Fluorobi hen 1 8?% $ 1 ; : ' : . 7 ::580-13-2 2-Bromonaphthalene 4040%: 6 5: 3386-33-2 1-Chlorooctadecane 7 % 70%r 7 40-140% (a)Advisory control limits. 14 Semivolatile Surrogate Recovery Summary Page 1 of 1 Job Number: M39366 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Method: MADEP EPH 98-1 Matrix: SO Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S2 a S3 a S4 b M39366-1 GH25908.D 90..0. 87.0 7::s :.;:.;:. > 72.0 _._......:.... _..._....._...: ....................... .......-- ........... ............ M39366-2 GH25909.1) 79.0...;:. 82.0 6:6I}. :,.;: 63.0 M39366-3 GH25910.D .Q: :.;;;; 82.0 660.,,;:i;,.;,; 66.0 OP7150 BS GH25903.D 8f:0::::>_>>;:< 87.0 <:73sO; ...... OP7150-MB GH25902.D '9. 85.0 6 < ` 67.0 OP7150-MS GH25904.13 83:0:. 87.0 71*,U::i:< : 73.0 ..... ....................... OP7150-MSD GH25905.D &10 > > >_85.0 73Q >= ; 70.0 ........... Surrogate Recovery Compounds Limits __..__..........._._ Sl = o-Terphenyl 4( 440.. _.._......._.... S2 = 2-Fluorobiphenyl 4044 ...:....................... ........................... ........................... S3 = 2-BromonaphthaleneO-;i401 < S4 = 1-Chlorooctadecane 4(#- i4.p (a)Recovery from GC signal#1 (b)Recovery from GC signal#2 15 Accutest Laboratories ................................... ......... __......_.................................._....__....... . I Custody Documents and Other Forms Includes the following where applicable: ■ Sample Tracking Chronicle 16 Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M39366 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Project No: Cost Element #707542 Sample Number Method Analyzed By Prepped By Test Codes M 3f 6 1 »C rll € s€ >1WMA �11¥'>B:::>MY�t . .. ece . _1. .. A ..B ..Ra...................._... ::: ::::::::::::.:..:.::::::::._::::._::::._:::::._:::..::::::::.::::.: y-::::.::.,............ ----------------------------- M39366-1 EPA 160.3 M 13-MAY-04 OP %SOL M39366-1 MADEP EPH 98-1 18-MAY-04 05:59 SL 13-MAY-04FC BMAEPH 3 _Ci6- i it _:;1:� '�'#t a(3 .....I ........ .:...:.:.........._.:.:......:.:..... A,� ..... .... ....:::.......::::..... .......... :.................:...:.........:.......... :::::....,:.,............................ Y..........................:.._:::.::::::._.::::::::::::::.::.:._ Iy1S..................................: ...::._:. ::::::::::::::::::::::::::::.:_:._ . .:.......................:..::..:::::::::::.::::.::::::.::::::..:._::::.._::.:. ........................................................ :.:....:.:.:................-......................................................:.:...:.:::::::::::::::::.:::::::::::::::.:::.::::::::::::::::. ::: :: : M39366-2 EPA 160.3 M 13-MAY-04 OP %SOL M39366-2 MADEP EPH 98-1 18-MAY-04 06:39 SL 13-MAY-04FC BMAEPH M33`:=::; iect <> M39366-3 EPA 160.3 M 13-MAY-04 OP %SOL M39366-3 MADEP EPH 98-1 18-MAY-04 07:19 SL 13-MAY-04FC BMAEPH Page 1 of I 17 Betty Baer From: Moira Walker[mwalker@ma.gsc-global.com] Sent: Wednesday, May 12,2004 11:24 AM To: Betty Baer Subject: 1140 lyannough Rd, Hyannis Betty, GSC submitted soil samples from Texaco Station#100083 located at 1140 lyannough, Hyannis MA today and during the previous weeks. Please note that these soil samples are from a GWA site and therefore must have the S-1/GW-1 detection limits. Also, because it is in the state of MA,we would like the MCP CAM level of qa/qc. Please contact me at 978-568-8740 x257 should you have any questions or would like me to fax over a revised Chain of Custody. Thank you, Moira Moira Walker Geologist Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 Toll Free:800 522 8740 Tel: 978 568 8740 x257 Fax: 978 568 9316 mwalker@ma.gsc-global.com www.gsc-global.com NOTICE:This e-mail message and any attachment to this e-mail may contain. confidential information that may be legally privileged. If you are not the intended recipient,you must not review,retransmit,convert to hard-copy, copy, use or disseminate this e-mail and any attachment to it. If you have received this e-mail in error, please notify us by return e-mail or by telephone at 978 568 8740 and delete this message. Please note that if this e-mail message contains a forwarded message or is a reply to a prior message, some or all of the contents of this message or any attachments may not have been produced by GSC. This notice is automatically appended to each e-mail message sent from GSC. Thank you. 18 1495TECHNOLOGY CENTER WEST • BUILDING ONE 1 MACCUTEST / l 3 ( 3 b 6 MARI-BOROUGH,MA 01752 ACCUTEST QUOTE r: L a b o r a t o r i e s TEL:508-481.6200 • FAX.,508481-7753 aoffiffi&MW CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION " MATRIX CODES OW- DRINKING �1 n NAME j-7 / PR EC AM WATER - OW• WATER APIRRESS LOC 10 WW• WASTE . WATER SO• SOIL CITY, STATE ZIP PRO ECT NQ. SL- SLUDGE fi1.1,� &I`�✓ 1:( I ah.yQ, C ost 6IQ:mt4 I7a7Sy Z 01- OIL SEND REPORT TO,' 17 LIQ- OTHER A I UOUID PHONE a R �_���$-�7�1C� FAX 4 G - SOL-OTHER ACCUTEST COLLECTION x PRESERVATION SOLID �F2 SAMPLE 4 FIELD 1D/POINT OF COLLECTION DATE TIME SA BY ED `S 2 1 LAB USwm..W� E ONLY 5hbloq I lo r JUt Z I DATA TURNAROUND INFORMATION iATA DELIVERABLE INFORMATION COMMENTS/REMARKS 14 DAYS STANDARD APPROVED BY: O STANDARD 7 DAYS RUSH O COMMERCIAL"B" 2 joit O 48 HOUR EMERGENCY J DISK DELIVERABLE O OTHER O STATE FDRMS 14 DAY TURNAROUND HAROCOPY.EMERGENCY OR RUSH IS FAX 0 OTHER OPECIFY) Lo c, /o c- DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTEDBELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELT7771 FREL1101,11 OU'SMED BY SA P gA REREU U N BY: DATETIME: RECEIVED Y:to N ISM BY: � RECEIVED REU UISNEDBY: DATE TIME: REC BY��. 3. 4. 4. HE0 BY: : RECE EO BY: SEAL 1 PRESERVE WHERE APPUCABUE ON ICFy TEMPERATURE 5. 5. 1 0 MAY 21 2904 New England OS/19/04 ® L zm -a,K- __._ �- Technical Repast fOr Shell Oil GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA GSC PO# 16988 Accutest Job Number: M39303 Sampling Date: 05/04/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 37 4E0 tN ACCpRO Y�O` �Cl► Test results contained within this data package meet the requirements teza and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications:MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 495 Tech Center West 0 Building 1 ■ Marlborough,MA 01752 ■tel:508481-6200■ fax:508481-7753 0 http://www.accutest.com Accutest Laboratories Sample Summary Shell Oil Job No: M39303 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Project No: GSC PO# 16988 Sample Collected: Matrix Client Number Date Time By Received Code Type Sample ID 39303.:1 OS/04l04 13:30 DG OS/10/04 SO Soil AIVK4:>I10RTHEAS'I<:: ............................... .: ................................ 3931D3-2 05/04/04 13:35 DG 05/10/04 SO Soil V Nl 4 ORTNWI�S F 7: .......................... 1v139303 3 : 05/04/04 13:45 DG 05/10/04 SO Soil TANK 4 VyEST 7 .............................. M:3930 4 05/04/04 13:50 DG 05/10/04 SO Soil TANS 3 WEST 7 ;; ........................ M393t35<<< 05/04/04 13:55 DG 05/10/04 SO Soil .:.:..::..:.....:......; 1393133-6 OS/04/04 14:00 DG OS/10/04 SO Soil TANK I SST 7' ............................... M39303-7 _ 05/04/04 14:05 DG 05/10/04 SO Soil SANK laUTHVV> ST 7 ............................. a .39303 8 05/04/04 14:10 DG 05/10/04 SO Soil TANK l SQUTBEAST 7' ................................ M39303 W 05/04/04 14:30 DG 05/10/04 SO Soil TANK 1 EAST? ; ................................ M93�?3 10 05/04/04 14:35 DG 05/10/04 SO Soil TAN 2 l~AST T;..;. ..............- . ......... ................ ........._..........-._............. . M39303- 1 ;:;.05/04/04 14:40 DG 05/10/04 SO Soil ANK 3 EAST Z 1V1...9...03 i2 OS/04/04 14:45 DG OS/10/04 SO Soil IA,NK 4 EAST.7'.'; ............._.. _... _................ __... ......_.........._...................................................................... .................... ..... M39303:13 >;05/04/04 13:40 DG 05/10/04 SO Soil 'TANNIC 4 BOTTOM 12'. Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Sample Summary (continued) Shell Oil Job No: M39303 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Project No: GSC PO# 16988 Sample Collected'......_... ........:: Matrix Client .:.....:::...::.::............................... Number Date Time By Received Code Type Sample ID ............................... Nf39305 4 05/04/04 14:15 DG 05/10/04 SO Soil TANK 3 B TTflM 12' M39303S OS/04/04 14:20 DG OS/10/04 SO Soil TANK 2 BOTTfl1v1 I2' M93i33 05/04/04 14:25 DG 05/10/04 SO Soil TANK 1 BE)TTOTvi:12. Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 4 NORTHEAST 7' Lab Sample ID: M39303-1 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 96.0 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis,MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14872.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 23.2 g 16.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......................... 7143-2 Benzene N:D; ; 180 ug/kg 100-41-4 Ethylbenzene ND.. 180 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND_._... ``::; 72 ug/kg ........:................. 91-20-3 Naphthalene NIJ'. ::; ; ; 180 ug/kg 108-88-3 Toluene ND;:;.:;.:;; :. 180 ug/kg IVD m,p-Xylene 180 ug/kg 95-47-6 o-Xylene ND 180 ug/kg C5- C8 Aliphatics(Unadj ) ND 3600 ug/kg .......::.................. .......... C9- C12 Aliphatics(Unadj.) ND< 3600 ug/kg C9- C10 Aromatics(Unadj.) ND::;;:::;;:; s::::;: 3600 ug/kg C5- C8 Aliphatics .: 36W ug/kg ............... ......... ........ ....... ........................... C9- C12 Aliphatics ND 3600 ug/kg .........................: CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... ......................... 615-59-8 2,5-Dibromotoluene 9;2 _ 70-130% ......................... 615-59-8 2,5-Dibromotoluene 9: °/oi'> ; 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 4 NORTHWEST 7' Lab Sample ID: M39303-2 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.9 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB 14873.D 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 22.5 g 16.0 m1 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......................... 71-43-2 Benzene ND 190 ug/kg ......:................... 100-41-4 Ethylbenzene N➢ 190 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND ::;;: ; 75 ug/kg 91-20-3 Naphthalene ;ND..;,... 190 ug/kg 108-88-3 Toluene NI)._._._.:.;:,:._ 190 ug/kg m,p-Xylene ND >:_ 190 ug/kg 9547-6 o-Xylene ND 190 ug/kg CS- C8 Aliphatics(Unadj.) N'D... ..... :.,,i 3700 ug/kg ... :.. ............ ........................... ........................... C9-C12 Aliphatics(Unadj.) ND< <; «' 3700 ug/kg C9- C10 Aromatics (Unadj.) ND :::;:; ; 3700 ug/kg C5-C8 Aliphatics ;NI .; 3700 ug/kg C9- C12 Aliphatics ND;:;;;:;:;:;:;:;;:; 37W ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 9I% 70-130% 615-59-8 2,5-Dibromotoluene ;92:%::::::;;:> 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 4 WEST 7' Lab Sample ID: M39303-3 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 93.2 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1314874.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 17.1 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71 43-2 Benzene ND <; < 170 ug/kg 100-41-4 Ethylbenzene hIID; ;`;` 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 69 ug/kg 91-20-3 Naphthalene >;I�I`1 i .. 170 ug/kg 108-88-3 Toluene ND '>< < 170 ug/kg m,p-Xylene ND.. 170 ug/kg 95-47-6 o-Xylene ND 170 ug/kg C5- C8 Aliphatics (Unadj.) NTH> i><< 3400 ug/kg C9-C12 Aliphatics(Unadj.) NID 3400 ug/kg C9-C10 Aromatics (Unadj.) ND .. 34W ug/kg C5-C8 Aliphatics ND<s= 3400 ug/kg C9- C12 Aliphatics NCB;. 3400 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene $$ ; 'i 70-130% 615-59-8 2,5-Dibromotoluene 9I°rb.:. 70-130% (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories. Report of Analysis Page I of I Client Sample ID: TANK 3 WEST 7' Lab Sample ID: M39303-4 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 89.6 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID OF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14875.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 20.9 g 16.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene NiD 210 ug/kg 100-41-4 Ethylbenzene 1VD.....:.....:>::. 210 ug/kg 1634-04-4 Methyl Tert Butyl Ether Nl 86 ug/kg 91-20-3 Naphthalene I�It�. 210 ug/kg 108-88-3 Toluene ND 210 ug/kg m,p-Xylene . Ni) 210 ug/kg. 95-47-6 o-Xylene ND 210 ug/kg C5-C8 Aliphatics(Unadj.) N _::.;:.;::,::;< 4300 ug/kg C9-C12 Aliphatics(Unadj ) ND 4300 ug/kg C9-C10 Aromatics(Unadj ) ND 4300 ug/kg C5-C8 Aliphatics ND 4300 ug/kg C9-C12 Aliphatics ND 4300 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 70-130% 615-59-8 2,5-Dibromotoluene ;.:;: 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 2 WEST 7' Lab Sample ID: M39303-5 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 93.5 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14876.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 17.7 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND ; >< 170 ug/kg g g 100-41-4 Ethylbenzene ND:::;;::::;;.:....:;:>: 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 66 ug/kg 91-20-3 Naphthalene T#< ; .. 170 ug/kg 108-88-3 Toluene 170 ug/kg m,p-Xylene Nb>« 170 ug/kg 95-47-6 o-Xylene ND ; i < 170 ug/kg C5-C8 Aliphatics(Unadj.) 1`ID« >«; ` ;;3300 ug/kg C9- C 12 Aliphatics(UnadJ J ND ;::;.; 3300 ug/kg C9-C10 Aromatics(UnadJ ) D 3300 ug/kg C5-C8 Aliphatics NL? 3300 ug/kg C9- C12 Aliphatics NT3 3300 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene g4:% > i; 70-130% 615-59-8 2,5-Dibromotoluene 70-130% ........... ... . .. (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence'of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 1 WEST 7' Lab Sample ID: M39303-6 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.0 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1314877.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 14.0 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q _.........._ .. ..... ........................... 71-43-2 Benzene ND< ; > > 210 ug/kg 100-41-4 Ethylbenzene ND< < ; ;<> 210 ug/kg 1634-04-4 Methyl Tert Butyl Ether �I1?::;: 83 ug/kg 91-20-3 Naphthalene NIA::;:........::.::::::::210 ug/kg 108-88-3 Toluene MID210 ug/kg m,p-Xylene :ND»< 210 ug/kg .:.................._.. _............. ........................... 95-47-6 o-Xylene <ND: 210 ug/kg C5-C8 Aliphatics (Unadj.) ND 4100 ug/kg .:..:...........:........ ........................... C9- C12 Aliphatics(Unadj.) ND ><> ;>i 4100 ug/kg C9- C10 Aromatics (Unadj ) 1D 4100 ug/kg C5-C8 Aliphatics NIA.........::::..::4100 ug/kg ........................... ......................... C9-C12 Aliphatics ND .:.. ;'4100 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ........................ 615-59-8 2,5-Dibromotoluene 1.04% 70-130% 615-59-8 2,5-Dibromotoluene 13.%.: 70-130% ....................... (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 1 SOUTHWEST 7' Lab Sample ID: M39303-7 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 90.9 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14878.1) 1 65/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 13.2 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q _................... ........................... 71-43-2 Benzene ND;; ' 230 ug/kg 100-41-4 Ethylbenzene ; 230 ug/kg .............:............ ........................... 1634 04-4 Methyl Tert Butyl Ether NIJ > < 92 ug/kg 91-20-3 Naphthalene N '< 230 ug/kg ....:...................... _..................... .......... ........ 108-88-3 Toluene ID;< >< 230 ug/kg m,P-Xylene Nz 230 ug/kg .:............:............ .......................... 95-47-6 o-Xylene All <: ; 230 ug/kg C5-C8 Aliphatics(Unadj.) NL < `i 4600 ug/kg ................... .......................... ............ ............ C9-C12 Aliphatics(Unadj.) ND . 4600 ug/kg C9-C10 Aromatics(Unadj.) Nb: :,,:>;;.:<; 4600 ug/kg C5-C8 Aliphatics4600 ug/kg C9- C12 Aliphatics IfU< 4600 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene : > ; 70-130% 615-59-8 2,5-Dibromotoluene 93%::::.:;: ::`.... 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 1 SOUTHEAST 7' Lab Sample ID: M39303-8 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.2 Project: GSCMA:9692.5028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1114879.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 20.7 g 16.0 mI 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene N:I3 200 ug/kg 100-41-4 Ethylbenzene ND.....:.._ .. 200 ug/kg ...:..:.................... 1634-04-4 Methyl Tert Butyl Ether Nib:;::;:::; 81 ug/kg 91-20-3 Naphthalene N:I :.; 200 ug/kg 108-88-3 Toluene ND< 200 ug/kg m,p-Xylene 1VD 200 ug/kg :.:.:............. 9547-6 o-Xylene NI] 200 ug/kg C5-C8 Aliphatics(Unadj.) ND 41W ug/kg .. ...................: ........................... C9-C12 Aliphatics(Unadj.) NDi < : ; 4100 ug/kg C9-C10 Aromatics(Unadj.) ZED;;:;;;:;;::::::` 4100 ug/kg C5-C8 Aliphatics ND 4100 ug/kg C9-C12 Aliphatics NI). . .. .. 4100 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene »92%> 70-130% ......................... 615-59-8 2,5-Dibromotoluene g5i < 70130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL =.Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of i Client Sample ID: TANK 1 EAST 7' Lab Sample ID: M39303-9 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.4 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14880.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 19.9 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... .................... 71-43-2 Benzene ND ; ; 210 ug/kg 100-41-4 Ethylbenzene 11 >< < ; '<` 210 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 84 ug/kg 91-20-3 Naphthalene I�D.__.:.';::.::;; 210 ug/kg ................. ...... __. __.. 108-88-3 Toluene ND ; ' 210 ug/kg m,p-Xylene ND>' 210 ug/kg 95-47-6 o-Xylene NL .:;.;::;.:;.,;.:;.:;: 210 ug/kg C5- C8 Aliphatics('Unadj.) NIA.::>;::;;: ;:;::;< 4200 ug/kg ... .......-........... ........................... ................-......... C9-C12 Aliphatics(Unadj.) hID 4200 ug/kg C9-C10 Aromatics(Unadj.) b:.;:.: :;:;;;: ;>4200 ug/kg C5-C8 Aliphatics TVL?.:.:.::;;;:.,:,: 4200 ug/kg C9- C 12 Aliphatics N13;> 42W ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 9:5;l; > ;> « 70-130% 615-59-8 2,5-Dibromotoluene 1:00% 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 2 EAST 7' Lab Sample ID: M39303-10 Date Sampled: 05/04/04 Matrix: So-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 92.1 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1314881.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 17.6 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND >sssi 170 ug/kg ....:...................... .........................- ........................... 100 41-4 Ethylbenzene NI); 170 ug/kg ...::...............-..... .............. .......................... 1634-04-4 Methyl Tert Butyl Ether NDi 68 ug/kg 91-20-3 Naphthalene NIA: :..:.: 170 ug/kg 108-88-3 Toluene )3170 ug/kg ......................... .......................... ........................... m,p-Xylene II3 170 ug/kg ......:................ ... ........................... ........................... 95-47-6 o-Xylene Nl? >` ; 170 ug/kg C5- C8 Aliphatics(Unadj.) NI#> < '<'< 3400 ug/kg C9-C12 Aliphatics(Unadj.) ND 3400 ug/kg C9-C10 Aromatics(Unadj.) ND;;% ; 3400 ug/kg C5-C8 Aliphatics ID>< < ;_; < 3400 ug/kg C9-C12 Aliphatics 1`II 3400 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 89%a> « 70130% 615-59-8 2,5-Dibromotoluene 93i%.::,.,,,.:;:'; 70130% ............. ... ......................... (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 3 EAST 7' Lab Sample ID: M39303-11 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.4 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14882.13 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 13.9 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND:_ .;..:::: 210 ug/kg 100-41-4 Ethylbenzene NTH::......::.::.::.. 210 ug/kg 1634-04 4 Methyl Tert Butyl Ether NL 84 ug/kg 91-20-3 Naphthalene : 210 ug/kg 108-88-3 Toluene ND 210 ug/kg m,p-Xylene ND_,:::;..: ;: 210 ug/kg 95-47-6 o-Xylene NIA 210 ug/kg C5- C8 Aliphatics(Unadj.) ) :;, ::;;>»> 4200 ug/kg C9- C12 Aliphatics(Unadj ) ND 4200 ug/kg NC9-CIO Aromatics(Unadj ) 4200 ug/kg C5- C8 Aliphatics NI)... 4200 ug/kg C9- C12 Aliphatics NL 42W ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $G%. . 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: TANK 4 EAST 7' Lab Sample ID: M39303-12 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 97.5 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1314883.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 19.2g 11.0m1 100ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene 150 ug/kg 100-41-4 Ethylbenzene 1VID:;;<.;»_ <:;: 150 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND::;:::;::;:;::: 59 ug/kg 91-20-3 Naphthalene ND .;:;:: ; 150 ug/kg 108-88-3 Toluene hID... 150 ug/kg m,p-Xylene N1) 150 ug/kg 95-47-6 o-Xylene NIA..... ::;; 150 ug/kg C5-C8 Aliphatics(Unadj.) ND'.,,,,,,.,,.; 2900 ug/kg .: .......... ............... . .1 .. ..............._..... C9-C12 Aliphatics(Unadj.) NDs ;; ; 2900 ug/kg C9-C10 Aromatics(Unadj.) 1D>;:::<; ::; 2900 ug/kg C5-C8 Aliphatics NIA........:.;;:: : 2900 ug/kg C9-C12 Aliphatics N)3 2900 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 920:;; ; 70-130% 615-59-8 2,5-Dibromotoluene 9 %:;::;:.;::::: 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 4 BOTTOM 12' Lab Sample ID: M39303-13 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 96.3 Project: GSCMA:96925028 (REIMBMA) 1140 lyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB14884.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 17.2 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q N 71-43-2 Benzene :ID ; 240 ug/kg 100-41-4 Ethylbenzene ND_ < ; : 240 ug/kg 1634-04-4 Methyl Tert Butyl Ether ai <> " 97 ug/kg 91-20-3 Naphthalene NTt > >< 240 ug/kg 108-88-3 Toluene I1D240 ug/kg m,p-Xylene : . 240 ug/kg ::......................... ........................... ........................... 9547-6 o-Xylene ATI << 240 ug/kg C5-C8 Aliphatics(Unadj.) 4800 ug/kg ... .................... .......................... ........................... C9-C12 Aliphatics(Unadj.) ND<>= 4800 ug/kg C9-C10 Aromatics(Unadj.) aV >>>;>>< 4800 ug/kg ..... .................. ........................... C5- C8 Aliphatics N1 ;; > 4800 ug/kg C9- C12 Aliphatics .ND.*` > 4800 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 9$%; 70-130% ........................ ........................ 615-59-8 2,5-Dibromotoluene 1:03%:.. 70-130% ......................... ........................ ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 3 BOTTOM 12' Lab Sample ID: M39303-14 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 92.4 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB 14885.D 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 16.4 g 16.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 260 ug/kg 100-41-4 Ethylbenzene D;; ; <i;;; 260 ug/kg 1634-04-4 Methyl Tert Butyl Ether ;2t)Z 110 ug/kg 91-20-3 Naphthalene ND 260 ug/kg 108-88-3 Toluene ND> 260 ug/kg m,p-Xylene NID 260 ug/kg 95-47-6 o-Xylene 1VD;::;;::, :>: 260 ug/kg C5-C8 Aliphatics(Unadj.) ` D > 5300 ug/kg C9- C12 Aliphatics (Unadj.) :,:::.: .:_ 5300 ug/kg C9-C10 Aromatics (Unadj.) ID;::;:;<, :: 5300 ug/kg C5-C8 Aliphatics >.;;::;::; 5300 ug/kg C9-C12 Aliphatics ND 5300 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene70130% 615-59-8 2,5-Dibromotoluene 99%;:........ 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 2 BOTTOM 12' Lab Sample ID: M39303-15 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 96.1 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14886.D 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 16.8 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......... ........................... 71-43-2 Benzene ND> ; ; <;<; 170 ug/kg 100-41-4 Ethylbenzene ND> <>; 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether 9 8>`i; _ 68 ug/kg 91-20-3 Naphthalene Nl ; 170 ug/kg 108-88-3 Toluene ND << ; 170 ug/kg m,p-Xylene N) 170 ug/kg 95-47-6 o-Xylene N 170 ug/kg C5-C8 Aliphatics(Unadj.) III ``;< > ; 3400 ug/kg C9-C12 Aliphatics(Unadj.) ND ; 3400 ug/kg C9-C10 Aromatics(Unadj.) 1T >; '> 3400 ug/kg C5-C8 Aliphatics 'NW* 3400 ug/kg C9-C12 Aliphatics ND. . _' :..; 3400 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene I04:%; 70-130% .......................:. ......................... ........................ 615-59-8 2,5-Dibromotoluene 409% 70-130% (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK I BOTTOM 12' Lab Sample ID: M39303-16 Date Sampled: 05/04/04 Matrix: SO - Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.8 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB 14887.D 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 20.4 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 210 ug/kg 100-41-4 Ethylbenzene D >< >< ` 210 ug/kg 1634-04-4 Methyl Tert Butyl Ether 5f6 82 ug/kg 91-20-3 Naphthalene NO i 210 ug/kg 108-88-3 Toluene 34f1 ;' ; i210 ug/kg m,p-Xylene N 210 ug/kg 95-47-6 o-Xylene AID 210 ug/kg C5- C8 Aliphatics (Unadj.) 1370:;:;: i:;;:::; 4100 ug/kg ........................... C9-C12 Aliphatics(Unadj.) DO(1 ' _4100 ug/kg C9-CIO Aromatics(Unadj.) 64fl0. ;4100 ug/kg C5-C8 Aliphatics 12700 < 4100 ug/kg C9-C12 Aliphatics 619( 4100 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene >124%.> ; 70-130% 615-59-8 2,5-Dibromotoluene 1 ;8;%::::;::;;>;: 70-130% ................ :...... (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MADEP VPH FORM IVtainx �k' W Aqueous F1 Soil Sediment F1 Other Contners .� SatisfactorvW Broken Leaking NIA pH <=2 H> 2 ra i �NNN -- Received on Ice Received at 4 De .C Other Rec'd at 2.7 deg C etfano;.. : Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 NORTHEAST 7' tab ID: M39303-1 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2.5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 96 1 N/A , Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 3600 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3600 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 3600 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 180 Toluene 108-88-3 C5-C8 ug/kg ND 180 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 72 Benzene 71-43-2 C5-C8 ug/kg ND 180 Naphthalene 91-20-3 WA ug/kg ND 180 o-Xylene 9547-6 C9-C12 ug/kg ND 180 m,p-Xylene C9-C12 ug/kg ND 180 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND 8 3600 I C9-C12 Aliphatics N/A ug/kg ND` 3600 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 95 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surtogate(s)and/or Internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9410 Aromatic Hydrocarbons. Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? RJ Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑d Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? R]No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM -Aqueous F1 Soil ny Sediment Other taec a . SatisfactorvW Broken n Leakin uerese�rative�s N/A H <=2 F1 PH>2 f = Received on Ice Received at 4 De .C Other Rec'd at 2.7 deg C Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 NORTHWEST 7' Lab ID: M39303-2 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibrorriotoluene %Solids: Low Dilution: High Dilution: 94.9 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 3700 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3700 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 3700 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 190 Toluene 108-88-3 C5-C8 ug/kg ND 190 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 75 Benzene 71-43-2 C5-C8 ug/kg ND 190 Naphthalene 91-20-3 N/A ug/kg ND 190 I o-Xylene 95-47-6 C9-C12 ug/kg ND 190 m,p-Xylene C9-C12 ug/kg ND 190 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 3700 C9-C12 Aliphatics N/A ug/kg ND` 3700 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CS-C8 Allphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surtogate(s)and/or Internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CID Aromatic Hydrocarbons. Z AV quarter indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM II[atxr� g '_; Aqueous Soil rVA Sediment F1 Other aam Satisfacto Broken Leakin N/A H<=2 H> 2 Ire Received on Ice F1 Received at 4 Deg. C n Other ReCd at 2.7 deg C Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 WEST 7' Lab ID: M39303-3 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 93.2 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND A 3400 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3400 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND A 3400 Target Analytes Ethylbenzene 100-414 C9-C12 ug/kg ND 170 Toluene 108-88-3 C5-C8 ug/kg ND 170 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg ND 69 Benzene 7143-2 C5-C8 ug/kg ND 170 Naphthalene 91-20-3 N/A ug/kg ND 170 o-Xylene 9547-6 C9-C12 ug/kg ND 170 m,p-Xylene C9-C12 ug/kg ND 170 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND B 3400 C9-C12 Aliphatics N/A ug/kg ND` 3400 Surroqate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 88 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of CS-CIO Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM Aqueous F1 Soil Sediment F1 Other , inert Satisfacto Broken F1 Leaking i ea ;�F `ese va taues NIA y pH <=2 n pH> 2 Received on Ice F1 Received at 4 Deg. C n Other d Rec'd at 2.7 deg C Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 3 WEST 7' Lab ID: M39303-4 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run- PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 89.6 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND A 4300 CO,C10 Aromatics(Unadj.) N/A ug/kg ND" 4300 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4300 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 210 Toluene 108-88-3 C5-C8 ug/kg ND 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 86 Benzene 71-43-2 C5-C8 ug/kg ND 210 Naphthalene 91-20-3 N/A ug/kg ND 210 o-Xylene 95-47-6 C9-C12 ug/kg ND 210 m,p-Xylene C9-C12 ug/kg ND 210 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4300 C9-C12 Aliphatics N/A ug/kg ND` 4300 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 84 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM AEInza w .. Aqueous Soil Sediment F1 Other OAR:`alr �� .�� SatisfactorvW Broken F1 Leakin t us�re e e h N/A Fyl pH <=2 H> 2 Received on Ice Received at 4 Deg.C Other d Rec'd at 2.7 deg C NOTIMo ,,_ Methanol Covering Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 2 WEST 7' Lab ID: M39303-5 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution- High Dilution: 93.5 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 3300 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3300 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 3300 Tar et Analytes g vt Ethylbenzene 100414 C9-C12 ug/kg ND 170 Toluene 108-88-3 C5-C8 ug/kg ND 170 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 66 Benzene 71-43-2 C5-C8 ug/kg ND 170 Naphthalene 91-20-3 N/A ug/kg ND 170 i o-Xylene 95-47-6 C9-C12 ug/kg ND 170 m,p-Xylene C9-C12 ug/kg ND 170 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 3300 C9-C12 Aliphatics . N/A ug/kg ND° 3300 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 94 70-130% PID:2,5-Dibromotoluene % 98 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of CS-CIO Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM JM- ,�*,� Aqueous n Soil Sediment Other '�� Contatner Satisfactory Broken F1 Leaking uedisf' eselrvatltre NIA n PH<=2 F PH> 2 :Ve Received on Ice Received at 4 Deg. C Other d Rec'd at 2.7 deg C Me..iai�o Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 WEST 7' Lab ID: M39303-6 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run- PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 4100 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4100 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4100 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 210 Toluene 108-88-3 C5-C8 ug/kg ND 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 83 Benzene 71-43-2 C5-C8 ug/kg ND 210 Naphthalene 91-20-3 N/A ug/kg ND 210 o-Xylene 95-47-6 C9-C12 ug/kg ND 210 m,p-Xylene C9-C12 ug/kg ND 210 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4100 C9-C12 Aliphatics N/A ug/kg ND` 4100 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 100 70-130% PID:2,5-Dibromotoluene % 103 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 91Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑d No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date. 5/19/2004 MADEP VPH FORM Wlat � Aciueous F1 Soil Sediment Other {irv� X SatisfactorvFy Broken F1 Leaking ntatne - Peseiaes NIA PH<=2 H> 2 �' €'a.u v Received on Ice Received at 4 Deg. C Other d Rec'd at 2.7 deg C tfianol ;` _. Methanol Coverin Soil. mL Methanol! soil: Other NOTE: Ratio>1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 SOUTHWEST 7' Lab ID: M39303-7 Method for Target Analytes• MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A F1D: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 90.9 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL 9 i C5-C8 Aliphatics(Unadj_) N/A ug/kg ND" 4600 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4600 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4600 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 230 Toluene 108-88-3 C5-C8 ug/kg ND 230 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 92 Benzene 71-43-2 C5-C8 ug/kg ND 230 Naphthalene 91-20-3 N/A ug/kg NO 230 o-Xylene 95-47-6 C9-C12 ug/kg ND 230 m,p-Xylene C9-C12 ug/kg ND 230 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4600 C9-C12 Aliphatics N/A ug/kg ND c 4600 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 89 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surtogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analyles eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? R Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM NOW-2 -_ � �� ��� Aqueous I Soil F./ Sediment Other c�tatnes= Satisfactory[W] Broken F1 Leaking Prservatis NIA H <=2 H> 2 m ratue� � Received on Ice F1 Received at 4 Deg.C Other d Rec'd at 2.7 deg C efara � Methanol Coverin Soil. mL Methanoll soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 SOUTHEAST 7' Lab ID: M39303-8 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95.2 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 4100 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4100 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4100 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 200 Toluene 108-88-3 C5-C8 ug/kg ND 200 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 81 Benzene 71-43-2 C5-C8 ug/kg ND 200 Naphthalene 91-20-3 N/A ug/kg ND 200 o-Xylene 95-47-6 C9-C12 ug/kg ND 200 m,p-Xylene C9-C12 ug/kg ND 200 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND 8 4100 C9-C12 Aliphatics N/A ug/kg ND` 4100 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 95 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or internal standards eliding In that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'X qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QAIQC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM IVCatrc� _;; Aqueous Soil Sediment Other Con m`ersF Satisfacto Broken Leaking/ii 'eou`.E�reseI _a IV* N/A W1 pH<=2 F1 PH>2 �f1t ll Received on ice F1 Received at 4 Deg.C Other d Redd at 2.7 deg C Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 EAST 7' Lab ID: M39303-9 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95.4 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/kg NO" 4200 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4200 C9-C12 Aliphatics(Unadj.) N/A ug/kg NO" 4200 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg NO 210 Toluene 108-88-3 C5-C8 ug/kg NO 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg NO 84 Benzene 71-43-2 C5-C8 ug/kg NO 210 Naphthalene 91-20-3 N/A ug/kg NO 210 o-Xylene 95-47-6 C9-C12 ug/kg NO 210 m,p-Xylene C9-C12 ug/kg NO 210 IAdiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4200 C9-C12 Aliphatics N/A ug/kg ND` 4200 Surrogate Recoveries Acceptance,Range FID:2,5-Dibromotoluene % 95 70-130% PID:2,5-Dibromotoluene % 100 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arry surrogatels)and/or Internal standards eluting in that range. CS-Cll Aliphatic Hydrocarbons exclude the concentration of Target Analytes ehrting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)ardlor Internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. 1Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM atmc s m � A ueous Soil .r Sediment F1 Other ontatoes� Satisfactory Broken F1 Leakin Quo P eseivatty s N/A. H <=2 PH> 2 Received on Ice Received at 4 Deg.C Other d Rec'd at 2.7 deg C Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 2 EAST 7' Lab ID: M39303-10 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 25-Dibromotoluene %Solids: Low Dilution: High Dilution- 92.1 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 3400 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3400 II C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 3400 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 170 Toluene 108-88-3 C5-C8 ug/kg ND 170 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 68 Benzene 71-43-2 C5-C8 ug/kg ND 170 Naphthalene 91-20-3 N/A ug/kg ND 170 o-Xylene 95-47-6 C9-C12 ug/kg ND 170 m,p-Xylene C9-C12 ug/kg ND 170 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 3400 C9-C12 Aliphatics N/A ug/kg ND` 3400 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 89 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of arry surrogatels)and/or internal standards eluting In that range 6 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogatels)and/or internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM Maix�r F." ri' Aqueous F1 Soil .i Sediment Other :Li Ilner _ Satisfactory Fy-1 Broken F1 Leaking ;at Fes N/A H<=2 F1 PH >2 � ## r Received on Ice .F1 Received at 4 Deg.C n Other d Rec'd at 2.7 deg C Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 3 EAST T Lab ID: M39303-11 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PI D: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.4 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL (q, C5-C8 Aliphatics(Unadj.) WA ug/kg ND" 4200 C9-C10 Aromatics(Unadj.) WA ug/kg ND" 4200 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND A 4200 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 210 Toluene 108-88-3 C5-C8 ug/kg ND 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 84 Benzene 71-43-2 C5-C8 ug/kg ND 210 Naphthalene 91-20-3 N/A ug/kg ND 210 o-Xylene 95-47-6 C9-C12 ug/kg ND 210 m,p-Xylene C9-C12 ug/kg ND 210 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4200 C9-C12 Aliphatics WA ug/kg ND` 4200 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 86 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arry surtogatels)and/or Internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'X qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? R Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect 11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 it MADEP VPH FORM iPV Aqueous F1 Soil ny Sediment Other �onineirs "�`;r SatisfactorvW Broken n Leakin Aous� Fe ervative NIA H <=2 H> 2 NOM"e"RAJOR Received on Ice Received at 4 Deg. C Other Ff Rec'd at 2.7 deg C Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. ,Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 EAST 7' Lab ID: M39303-12 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run- PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 97.5 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 2900 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 2900 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 2900 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 150 Toluene 108-88-3 C5-C8 ug/kg ND 150 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 59 Benzene 71-43-2 C5-C8 ug/kg ND 150 Naphthalene 91-20-3 N/A ug/kg ND 150 o-Xylene 95-47-6 C9-C12 ug/kg ND 150 m,p-Xylene C9-C12 ug/kg ND 150 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 2900 C9-C12 Aliphatics N/A ug/kg ND` 2900 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID2,5-Dibromotoluene % 96 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting in that range. C5-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of arty surrogates)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? V No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 h MADEP VPH FORM A ueous Soil Sediment Other x ... Satisfacto Broken Leakin + N/A pH <=2 F1 PH> 2 1'at Received on Ice Received at 4 Deg.C n Other .i Rec'd at 2.7 deg C Methanol Coverin Soil. mL Methanol! soil: 1:1 +l-25% Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 BOTTOM 12' Lab ID: M39303-13 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 96.3 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 4800 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4800 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4800 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 240 Toluene 108-88-3 C5-C8 ug/kg ND 240 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 97 Benzene 7143-2 C5-C8 ug/kg ND 240 Naphthalene 91-20-3 N/A ug/kg ND 240 o-Xylene 95-47-6 C9-C12 ug/kg ND 240 m,p-Xylene C9-C12 ug/kg ND 240 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4800 C9-C12 Aliphatics N/A ug/kg ND` 4800 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 98 70-130% PID:2,5-Dibromotoluene % 103 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of ary surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'quali ier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? S6Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.37 W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 i MADEP VPH FORM W W<< W Aqueous Soil Sediment F1 Other (041 xY nefs_ Satisfacto v' Broken Leakin ' is�Presel `tatnces NIA .r pH <=2 H> 2 erat�i[ Received on Ice F1 Received at 4 Deg.C Other d Rec'd at 2.7 deg C Methanol {; Methanol Coverin Soil. mL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH 98-1 Client ID: TANK 3 BOTTOM 12' Lab ID: M39303-14 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run- PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 92.4 1 N/A (Unadiusted Ranges CAS# Elution Range Units Result RDL (� C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 5300 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 5300 C9-C12 Aliphatics I.Unadj.) N/A ug/kg ND" 5300 Target Analytes Ethylbenzene 10041-4 C9-C12 ug/kg ND 260 Toluene 108-88-3 C5-C8 ug/kg ND 260 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg 207 110 Benzene 7143-2 C5-C8 ug/kg ND 260 Naphthalene 91-20-3 N/A ug/kg ND 260 o-Xylene 95-47-6 C9-C12 ug/kg ND 260 m,p-Xylene C9-C12 ug/kg ND 260 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 5300 C9-C12 Aliphatics N/A ug/kg ND` 5300 Surrogate Recoveries Acceptance Range 1`I131:25-Dibromotoluene % 95 70-130% PID:2,5-Dibromotoluene % 99 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-CID Aromatic Hydrocarbons. Z A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? V No ❑ Yes-Details Attatched I attest under the pains and penalties of perjuly that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM Aqueous Soil Sediment '—I Other ntali Satisfacto Broken Leaking `ue l - ----- NIA .i pH <=2 PH> 2 ft-anor. Received on Ice El Received at 4 Deg. C Other d Reed at 2.7 deg C ethano :_ Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 2 BOTTOM 12' Lab ID: M39303-15 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 96.1 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 3400 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3400 C9-C12 Aliphatics(Unadj.) WA ug/kg ND" 3400 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 170 Toluene 108-88-3 C5-C8 ug/kg ND 170 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg 95.8 68 Benzene 71-43-2 C5-C8 ug/kg ND 170 Naphthalene 91-20-3 N/A ug/kg ND 170 o-Xylene 95-47-6 C9-C12 ug/kg ND 170 m,p-Xylene C9-C12 ug/kg ND 170 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 3400 CO,C12 Aliphatics N/A ug/kg ND c 3400 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 104 70-130% PID:2,5-Dibromotoluene % 109 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exchide concentrations of any surrogate(s)andlor Internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogatels)and/or Internal standards eluting In that range. C9-C12 allphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'X qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM OWN Aqueous F1 Soil Sediment FJ Other Ir>€a>«ers: SatisfactoryFyl Broken P, Leaking rese>tira N/A pH <=2 Ll PH>2 atu: Received on Ice Received at 4 Deg. C Other d Rec'd at 2.7 deg C row ;: Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 BOTTOM 12' Lab ID: M39303-16 (Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run- PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution- 95.8 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL (� C5-C8 Aliphatics(Unadj.) N/A ug/kg 13700" 4100 C9-C10 Aromatics(Unadj.) N/A ug/kg 6400" 4100 C9-C12 Aliphatics(Unadj.) WA ug/kg 13000" 4100 I Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 210 Toluene 108-88-3 C5-C8. ug/kg 340 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg 566 82 Benzene 71-43-2 C5-C8 ug/kg ND 210 Naphthalene 91-20-3 N/A ug/kg ND 210 o-Xylene 95-47-6 C9-C12 ug/kg ND 210 m,p-Xylene C9-Cl 2 ug/kg ND 210 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg 127000 4100 C9-C12 Aliphatics NIA ug/kg 6190` 4100 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 124 70-130% PID:2,5-Dibromotoluene % 118 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Wer e all QA1QC procedures REQUIRED by the VPH Method followed? W]Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? VYes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 � ��" �n UHAIN UF- UU5 I UUY s�M}� 13 v,L 495 Tech Center West, Bldg.1,Marlboro,MA 01752 1 V� 11ACCUTEST (508)481-6200 Fax: (508)481-7753 Accutest Job#: M 3 g 3-0 j ;v Client Information Facility information "1 Analytical Information Consultants Name Project Name Geolo Ic Services Corporation SOPUS Hyannis 7 Address Street 15 Bonazzoll Ave. 1140 1 anou h Rd Statecity Zip State Hudson MA 01749 Hyannis MA Project Contact: Invoice Contact: Phone#: 978.568-8740 Invoice Phone# fik Fax#: 978.568.9316 Location ID# 100083 AFE# PO# Q`g s _ Collection Preservation x y Field ID/Point of Collection Datf Time Sampled By I Matrix bottles z o 501 A 1XI )4 -1 f � / & x WA,-j t' %71 7r -J t) k _ f X � f x I >e it ! O—L 4 Turnaround Information =v" Data Deliverable Information Accutesl Login Information ®Std.14 Day Turnaround Approved By: ® Commercial"A" Q FULL CLP Q 7 Day EMERGENCY Q Commercial"B" Q State Forms FOIL _ 4 Day EMERGENCY O Full Dellverables Disk Deliverable Format_ ��lt*�l S 3 Day EMERGENCY Other AIM M' C ft 2 Day EMERGENCY L-oc. 3"/�.5- /OR 1 Day EMERGENCY Emergency T/A is for FAX or Lablink Data Commercial"A"=Results Only Sample Custody must be oeumented below each time m les change ossesion,Including courie alive w xe • m ae w e nq a e me: oe vRelift; e' y. u a':. a . .r 2 4ao O� 1 as ve Y: 2a m s a me: oo vo y: e nqu s o mp or. . f 3 4 4 3e nqu a mp er O J eeo s + as reserve w ere app Boa a n oe p C emp. O 5 5 e ACCUTEST (508)481-6200 Fax: (508)481-7753 Accutest Job#: M 39.3 tJ Client Information FacilityInformation Analytical nformation Consultants Name Project Name Geologic Services Corporation SOPUS Hyannis Address Street 15 Bonazzoll Ave. 1140 I anou h Rd Statecity P city State Hudson MA 01749 H annis MA Project Contact: Invoice Contact: Phone#: 978-588-8740 Invoice Phone# Fax#: 978-588-9316 Location ID# 100083 PO# IlU_I AFE# Co lect on Preservation x g _ Field ID/Point of Collection t Time Sampled By Matrix bot/es cz A w b o is y X x �' a 2 �`I -X o •Accutest LIn Information Turnaround Information :f.. „x Data Deliverable Information , t Std,14 Day Turnaround Approved By: Commercial"A" Q FULL CLP O u 7 Day EMERGENCY O Commercial"B" Q State Forms 4 Day EMERGENCY D Full Dellverables Q Disk Deliverable Format_ 3 Day EMERGENCY Other 2 Day EMERGENCY 1 Day EMERGENCY Emergency T/A Is for FAX or Labllnk Data Commercial"A"-Results Only , t & Sample Custody must be do umented below each time samples change possesion,Including er de e u• amp er: e e •: ea•v y: s e a e ime: ecerv• y: ^lo- 2 � eve • Time; Received e s e Date Y' a s. •ea v XYqnq • amp sr. 4 o / /o:/S 3 4 emp. 3 G✓' n e• a nqu y amp e, a e: 50• ❑ tS 5 MAY 2 1 2004 New England 05/18/04 Technlcal Report for Shell Oil GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA . GSC PO# 16988 Accutest Job Number: M39301 Sampling Date: 05/06/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of P report:es in 11 C�N'ACCpq� 46 _ u 4 Test results contained within this data package meet the requirements ta and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications:MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety, without the written approval of Accutest Laboratories. New England 495 Tech Center West 0 Building I ■ Marlborough,MA 01752■ tel: 508481-6200 ■ fax:508-481-7753 ■ http://www.accutest.com Accutest Laboratories Sample Summary Shell Oil Job No: M39301 GSCMA:96925028 (REIMBMA) 1140 lyannough Rd., Hyannis, MA Project No: GSC PO# 16988 _.. .._.........._ . _ _._. Sample Cohectel Matrix Client Number Date Time By Received Code Type Sample ID 1Vf39301 05/06/04 14:50 MW 05/10/04 SO Soil NE�ISP')3QTT(4;') M39301 Z 05/06/04 15:00 MW 05/10/04 SO Soil Sly DISP I301T(4') ............................... M39301 3 05/06/04 15:05 MW 05/10/04 SO Soil SW`DISP BOTT 44.) .:............................. Nf39301 4 05/06/04 15:10 MW 05/10/04 SO Soil NWI)lSl'I. BQTT.{4') Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: NE DISP BOTT(4') Lab Sample ID: M39301-1 Date Sampled: 05/06/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.9 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a QR27554.1) 1 05/13/04 AA n/a n/a GQR1346 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 10.6 g 16.0 m1 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ill)....,:: .. .... 400 ug/kg .....................:....: 100-41-4 Ethylbenzene IND:.;;:.;.;:.;::;.:;. 400 ug/kg 1634-04-4 Methyl Tert Butyl Ether N.A.......::.....: 160 ug/kg 91-20-3 Naphthalene N.D..,._ 400 ug/kg 108-88-3 Toluene Nl7;; ;>: . 400 ug/kg m,p-Xylene ND. ..: 400 ug/kg 95-47-6 o-Xylene 400 ug/kg ............. ........................... C5- C8 Aliphatics (Unadj.) Ni<3> > 7900 ug/kg C9-C12 Aliphatics(Unadj.) 7900 ug/kg C9-C10 Aromatics(Unadj.) ;`;IUD; <;:<;:;7900 ug/kg C5-C8 Aliphatics N7 7900 ug/kg C9-C12 Aliphatics ND ° ; 7900 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 70-130% ......................... 615-59-8 2,5-Dibromotoluene 1 &:%> 70-130% (a) Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: SE DISP BOTT(4') Lab Sample ID: M39301-2 Date Sampled: 05/06/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.7 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR27555.1) 1 05/13/04 AA n/a n/a GQR1346 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 12.4 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene :;::_; 340 ug/kg ..............:............ ........................... 100-414 Ethylbenzene 340 ug/kg ........:..............:... ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether 140 ug/kg 91-20-3 Naphthalene hID 340 ug/kg 108-88-3 Toluene Np: '; ` ; 340 ug/kg m,p-Xylene ND:.;,>::::;:; ;;;:; 340 ug/kg 95-47-6 o-Xylene N i> i><< <> 340 ug/kg C5-C8 Aliphatics(UnadJ.) hID::;::;;:; ;;;:;:;::;6800 ug/kg C9- C 12 Aliphatics (UnadJ ) ND 6800 ug/kg l C9- C10 Aromatics (UnadJ.) ) ;< ; 6800 ug/kg CS- C8 Aliphatics D 6800 ug/kg .....D:*................. ........................... C9-C12 Aliphatics hCD:< > < 6800 ug/kg CAS No. Surrogate Recoveries Run#I Run#2 Limits 615-59-8 2,5-Dibromotoluene $7% ; > 70-130% 615-59-8 2,5-Dibromotoluene 9 %::::::: :: 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: NW DISP BOTT(4') Lab Sample ID: M39301-4 Date Sampled: 05/06/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.2 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 QR27561.1) 1 05/13/04 AA n/a n/a GQR1346 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 11.2 g 16.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene ;:.;:.; ... 380 ug/kg 100-41-4 Ethylbenzene ND 380 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND < 150 ug/kg 91-20-3 Naphthalene ND;::;:;:;;;;:::;;:: 380 ug/kg 108-88-3 Toluene IID._..... 380 ug/kg m,p-Xylene NU:;:;:;;:;::;>:;:;;;> 380 ug/kg 9547-6 o-Xylene 1D 380 ug/kg C5- C8 Aliphatics(Unadj.) hID 7500 ug/kg h C9- C12 Aliphatics(Unadj ) 1D 7500 ug/kg C9- C10 Aromatics(Unadj.) L3::;;;;;::,;;:;:. 7500 ug/kg .. ...._....... C5- C8 Aliphatics ND.;.;.;;;:,;.; 7500 ug/kg C9-C 12 Aliphatics ND;:; 7500 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $2.%.:.._;; 70-130% ......................... ......................... 615-59-8 2,5-Dibromotoluene 891 > 70-130% (a)Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: SW DISP BOTT(4') Lab Sample ID: M39301-3 Date Sampled: 05/06/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.4 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a QR27560.1) 1 05/13/04 AA n/a n/a GQR1346 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 10.9 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ................ 71-43-2 Benzene liD <ii 390 ug/kg 100-41-4 Ethylbenzene 11D . 390 ug/kg 1634-04-4 Methyl Tert Butyl Ether 160 ug/kg 91-20-3 Naphthalene ICI)::::::;;.;:.:.:; 390 ug/kg ......:.................... ........................... ........................... 108-88-3 Toluene «Nps390 ug/kg .............:............. ........................... ........................... m,p-Xylene h D 390 ug/kg 95-47-6 o-Xylene ND << 390 ug/kg C5-C8 Aliphatics (Unadj.) IID::;:;::: 7800 ug/kg C9-C12 Aliphatics(Unadj ) ND 7800 ug/kg ........................... C9-C10 Aromatics(Unadj.) 'hTD ' <; 7800 ug/kg :..: ....:.............. ........................... ........................... C5-C8 Aliphatics NIA 7800 ug/kg C9-C12 Aliphatics . 7800 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits _...._................ 615-59-8 2,5-Dibromotoluene 71 ;<; 70-130% 615-59-8 2,5-Dibromotoluene 74 70-130% ......................... (a) Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MADEP VPH FORM Matflx, ,' cu A ueous Soil Sediment Other Cofattters SatisfactorvW Broken n Leakin A ueous Preseiatfues N/A W pH <=2 F1 PH > 2 etm atiire ,_, x y Received on Ice F1 Received at 4 De . C Other d Redd at 2.7 deg C Meanol _„ Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio<0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: NE DISP BOTT(4) Lab ID: M39301-1 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/6/2004 Date Received:. 5/10/2004 I VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.9 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 7900 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 7900 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND' 7900 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 400 Toluene 108-88-3 C5-C8 ug/kg ND 400 i Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 160 Benzene 71-43-2 C5-C8 ug/kg ND 400 Naphthalene 91-20-3 N/A ug/kg ND 400 o-Xylene 95-47-6 C9-C12 ug/kg ND 400 m,p-Xylene C9-C12 ug/kg ND 400 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 7900 CO,C12 Aliphatics N/A ug/kg ND c 7900 (Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 109 70-130% PID:2,5-Dibromotoluene % 118 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting in that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9C1O Aromatic Hydrocarbons. Z AV Qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 0 Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 91 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 MADEP VPH FORM Mlkrez r. -' Aqueous F1 Soil RV Sediment F1 Other Containers': .: Satisfacto Broken F1 Leakin A ueous Preseruatiues- N/A H <= 2 L1 pH> 2 Tem nature ,z Received on Ice F1 Received at 4 Deg. C F1 Other d Redd at 2.7 deg C Metianpl �; Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH 98-1 Client ID: SE DISP BOTT(4) Lab ID: M39301-2 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/6/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.7 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL t3 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND A 6800 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 6800 C9-C12 Aliphatics(Unadj.). N/A ug/kg ND" 6800 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 340 I Toluene 108-88-3 C5-C8 ug/kg ND 340 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 140 Benzene 71-43-2 C5-C8 ug/kg ND 340 Naphthalene 91-20-3 N/A ug/kg ND 340 o-Xylene 95-47-6 C9-C12 ug/kg ND 340 m,p-Xylene C9-Cl 2 ug/kg ND 340 Adjusted Ranges C5-C8 Aliphatics N/A u 9/kg ND a 6800 P C9-C12 Aliphatics N/A ug/kg ND c 6800 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 87 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C9C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9C10 Aromatic Hydrocarbons. Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director � , Printed Name Reza Tand Date 5/18/2004 MADEP VPH FORM Matx # . r Aqueous Soil Sediment I— Other Corttatners „ kg Satisfactory Broken Leaking A taeousPreservatrves N/A pH <= 2 F1 PH> 2 Received on Ice Received at 4 Deg. C Other d Redd at 2.7 deg C Mefanot „�� Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio<0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: SW DISP BOTT(4) Lab ID: M39301-3 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/6/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/2004 NIA FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.4 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 7800 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 7800 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 7800 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 390 Toluene 108-88-3 C5-C8 ug/kg ND 390 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 160 Benzene 71-43-2 C5-C8 ug/kg ND 390 Naphthalene 91-20-3 N/A ug/kg ND 390 o-Xylene 95-47-6 C9-C12 ug/kg ND 390 m,p-Xylene C9-C12 ug/kg ND 390 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 7800 C9-C12 Aliphatics N/A ug/kg ND` 7800 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 71 70-130% PID:2,5-Dibromotoluene % 74 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range e Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cons of Target Analytes eluting in that range AND concentration of C9C10 Aromatic Hydrocarbons. Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? V Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature. Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 MADEP VPH FORM Aqueous F1 Soil Sediment F Other Canfalners. a .: Satisfactory Broken Leaking A ueous P,resenrattves NIA PH <=2 H > 2 Tm eraXure p Received on Ice Received at 4 Deg. C Other d Rec'd at 2.7 deg C Met[angl, Methanol Coverin Soil. mL Methanol/ soil: Other NOTE. Ratio<0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: NW DISP BOTT(4') Lab ID: M39301-4 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/6/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/2004 1 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95.2 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 7500 C9-C10 Aromatics(Unadj.) N/A ug/kg ND A 7500 C9-C12 Aliphatics(Unadj.) WA ug/kg ND" 7500 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 380 Toluene 108-88-3 C5-C8 ug/kg ND 380 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 150 Benzene 71-43-2 C5-C8 ug/kg ND 380 Naphthalene 91-20-3 N/A ug/kg ND 380 o-Xylene 95-47-6 C9-C12 ug/kg ND 380 m,p-Xylene C9-C12 ug/kg ND 380 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 7500 C9-C12 Aliphatics N/A ug/kg ND` 7500 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 89 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 N c } W =�ymwm QW 0 2/-�HcAF Ju WjWn O - QU U QaQa<Q5,J OJEO W X ~ . c3c�333�,w5.070co ? W m G a CO IAA O O fOA J f' _ O a > O LL0 W W cr cc �O < V W m m 7 U ? W O U �• Z 7 U V 0 W IL Q = �- = IC Q N G W C� � = V z Q W lu lu HdA 1 p = O . NIW p 0 y o 0 N O IL I W W fO111i 0 m to 110� W NOONco a Q 2 Q d MH O U W Z • C S31UOG N a ' o w us ti- ¢ xttuvw z to LA m OQ 4WOg LL G JUF gcc �_ �O IL am Q = acVav w rJaC J Q Q A a ul J U O U " Z = W � O W w mQ 3 U ti Q J � " ' _� Q C V > W d m Qw -AOb olx J tN v 0 GW Wz0O QMW Z O La Q F=- W V O N O IC U r� ❑ ❑❑❑❑ 0 aLu K to W W ILL > LL F- W W N = 0 = 2a � WacO aai P N m J Ix G b W 0 O a I\ v _ � O z t'iW W o o a w o W p � ►- \ W O 0 N 0 p W> QOk� o 41 LL � I a Z }O¢IL 9L N cc 0.9 -0 J \ i 1 LL [�i cc a 0 =j m t° U w Z = W z> z 4LO O cc N cc W at IL m go m ac O NNE acil Q y n W W i V 4, QOW » .. x m x oW W aZ ? Ja I I -erpco �? ��Il a r 10 02 a0 as 2 2 0 tlu 2 MAY 21 2004 ® New England OS/20/04 ®ACCUTEST L a b o r a t o r i e s _....-... _......... ..... -....- _ .......... ..... ...... .......... _.. .... ....._....._. ................ .._...... ......_....... .......... ......._...... . .. Techntcal Report far Shell Oil GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA GSC PO# 16988 Accutest Job Number: M39365 Sampling Date: 05/10/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 21 4�0 04 1"0440Zez - 4� 4 � i Test results contained within this data package meet the requirements and of the National Environmental Laboratory Accreditation Conference Laabb Director and/or state specific certification programs as applicable. Certifications: MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NI(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 0 495 Tech Center West■ Building 1 ■ Marlborough,101752 m tel:508-481-6200 w fax: 508481-7753 E http://www.accutest.com L r� is ... r aI: -> SAMPLE DELIVERY GROUP CASE R P A E NARRATIVE Client: Shell Oil Job No: M39365 Site: GSCMA:96925028(REIMBMA) 1140 tyannough Rd.,Hyannis, M Report Date 5/20/2004 l 1:25:59 A I 4 Sample(s)were collected on 05/10/2004 and were received at Accutest on 05/12/2004 properly preserved,at 1.5 Deg.C and intact. These Samples received an Accutest job number of M39365.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job. For more information,please refer to QC summary pages. Volatiles by GC By Method MADEP VPH 98-1 Matrix: SO Batch ID: GAB743 0 All samples were analyzed within the recommended method holding time. a Sample(s) M39363-1MS,M39363-1MSD were used as the QC samples indicated. a All method blanks for this batch meet method specific criteria. 0 M39363-1MS: Soil to methanol ratio greater than 1.25 to 1. ® M39363-1 MSD: Soil to methanol ratio greater than 1.25 to 1. m M39365-1:Soil to methanol ratio less than 0.75 to 1. M39365-2:Soil to methanol ratio less than 0.75 to 1. M39365-3:Soil to methanol ratio less than 0.75 to 1. Wet Chemistry By Method EPA 160.3 M Matrix: SO Batch ID: GN13856 Sample(s) M39365-1 DUP were used as the QC samples for Solids,Percent. The Accutest Laboratories of New England certifies that all analysis were performed within method specification. It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M39365). Thursday,May 20,2004 Page 1 of 1 � _ 2 Massachusetts Department BWSC-CAM Exhibit VII A-1 LI of Environmental Protection 22 May 2003 Revision No. 3.1 Bureau of Waste Site Cleanup Final Page 13 of 30 Title: MADEP MCP Response Action Analytical Report Certification Form rely, �IUI ®E�r CF Anat�yt�cal efhvd lZeparf Gerttticafta t;Fo � t £' Y Laboratory Name: Accutest Laboratories of New England Project#: M39365 Project Location: GSCMA:96925028(REIMBMA) 1140 lyannough Rd., MADEP RTN None Hyannis, MA This form provides certifications for the following data set: M39365-1,M39365-2,M39365-3,M39365-4 Sample Matrices: Groundwater Soil/Sediment X Drinking Water Other: MGPSW 841 , 8260E 8151A 8330 6010E 7470A/1A s 01 �N[ethodsAled 8270C 8081A VPH X 6020 9014M Z speafied MI MI P 8082 8021 B ( EPH 7000 S 7196A Co endof fVetease h rackurpber( >k FU now a [caTMethods � b 2M,, a hod9014ar ' P �talogrcl A. i [ a r g ems'� �Meoc �' ( hecXc alttfta,apply f 3&S S 846Mejhodo0 Senes�List('rid�viduat me odandan (jtte = ;; An affirmative response to questions A,B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with U, Yes ❑ No ' that described on the Chain=of-Custodydocumentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and 121 Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards orguidelines? Does the analytical data included in this report meet all the requirements C for"Presumptive Certainty",as described in Section 2.0 of the MADEP Yes ❑No ' document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without Yes ❑No ' significant modifications,as specified in Section 11.3? A response to questions E and F below is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the U, Yes LI No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified RI Yes LJ No ' methods reported? All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned,attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,accurate and complete. Signature: � Position: Laboratory Director Printed Name: Reza Tand Date: 5/20/04 3 Accutest Laboratories Sample Summary Shell Oil Job No: M39365 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Project No: GSC PO# 16988 Sample CoUectei Matrix Client Number Date Time By Received Code Type Sample ID M39365 is 05/10/04 09:50 MW 05/12/04 SO Soil EXG01 {3 } M39365 2 05/10/04 09:55 MW 05/12/04 SO Soil JENC.07{3 S') 1vI39365-3 05/10/04 10:00 MW 05/12/04 SO Soil EXC03 (3.5 ) .......... .................... M39365-4 OS/10/04 10:05 MW 05/12/04 SO Soil BXC04 Soil samples reported on a dry weight basis unless otherwise indicated on result page. 4 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: EXCO1 (3') Lab Sample ID: M39365-1 Date Sampled: 05/10/04 Matrix: SO - Soil Date Received: 05/12/04 Method: MADEP VPH 98-1 Percent Solids: 95.2 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1314947.1) 1 05/14/04 DL n/a n/a GAB743 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 8.44 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 6X2 500 ug/kg 10041-4 Ethylbenzene 1:9300 500 ug/kg 1634-044 Methyl Tert Butyl Ether 1480 200 ug/kg 91-20-3 Naphthalene 3060 500 ug/kg 108-88-3 Toluene 3J 200 500 ug/kg m,p-Xylene 46600 500 ug/kg 95 47-6 o-Xylene 21#100 ..500 ug/kg C5-C8 Aliphatics(Unadj ) 145Q00 10000 ug/kg C9-C12 Aliphatics (Unadj ) 2 9000 IWOO ug/kg C9-CIO Aromatics (Unadj ) 127000 10000 ug/kg C5- C8 Aliphatics 1} OQO.; 10000 ug/kg C9-C12 Aliphatics ND 10000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 105% ;i 70-130% 615-59-8 2,5-Dibromotoluene 1p7:%. 70-130% ...................... (a)Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 5 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: EXCO2(3.5') Lab Sample ID: M39365-2 Date Sampled: 05/10/04 Matrix: SO - Soil Date Received: 05/12/04 Method: MADEP VPH 98-1 Percent Solids: 97.0 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14948.1) 1 05/14/04 DL n/a n/a GAB743 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 10.3 g 16.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......................... 7143-2 Benzene ND 400 ug/kg 100-41-4 Ethylbenzene 1.4900 400 ug/kg 1634-04-4 Methyl Tert Butyl Ether 1540 160 ug/kg 91-20-3 Naphthalene 1:2400 400 ug/kg 108-88-3 Toluene 9. OU;:<>:: 400 ug/kg m,p-Xylene 49500..,i_;:: 400 ug/kg 95-47-6 o-Xylene 22500 400 ug/kg C5-C8 Aliphatics(Unadj ) ,1Q30QfJ_.....:..: 8000 ug/kg ................... ........................... C9-C12 Aliphatics (Unadj.) 30300 ;; ; 8000 ug/kg . ......... . .............-............ C9-C10 Aromatics (Unadj.) `213000'.. 8000 ug/kg C5-C8 Aliphatics 8L90(: :;:i::;<: 8000 ug/kg C9-C12 Aliphatics ND :; <> 8000 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 119aa 70-130% 615-59-8 2,5-Dibromotoluene I25%..... < 70-130% (a) Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: EXC03 (3.5') Lab Sample ID: M39365-3 Date Sampled: 05/10/04 Matrix: SO - Soil Date Received: 05/12/04 Method: MADEP VPH 98-1 Percent Solids: 94.1 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB 14949.D 1 05/14/04 DL n/a n/a GAB743 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 11.0 g 16.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 390 ug/kg 100-41-4 Ethylbenzene ND 390 ug/kg ..................... . 1634-04-4 Methyl Tert Butyl Ether ND 150 ug/kg Ib 91-20-3 Naphthalene ::;:;;:>::>;:::;::;;: 390 ug/kg 108-88-3 Toluene lD....,,;;;; 390 ug/kg m,p-Xylene ND 390 ug/kg 95-47-6 o-Xylene ND 390 ug/kg C5-C8 Aliphatics('Unadj.) NI[? ;; ;;>77M ug/kg C9-C12 Aliphatics(Unadj.) ND::: 7700 ug/kg C9- C10 Aromatics(Unadj.) D ::;:::i;;;;>: 7700 ug/kg C5-C8 Aliphatics NI3.....: ......: 7700 ug/kg C9-C 12 Aliphatics hID::::;:;;;:;:::;:; 7700 ug/kg CAS No. Surrogate Recoveries Runt{I Run#2 Limits 615-59-8 2,5-Dibromotoluene 91% <> 70-130% ............... 615-59-8 2,5-Dibromotoluene ?9'0< <i> 70-130% (a) Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: EXC04 (3.5') Lab Sample ID: M39365-4 Date Sampled: 05/10/04 Matrix: SO- Soil Date Received: 05/12/04 Method: MADEP VPH 98-1 Percent Solids: 94.0 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 A1314950.1) 1 05/15/04 DL n/a n/a GAB743 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 11.5 g 16.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Unit s Q ........................... 71-43-2 Benzene > 370 ug/kg 100-41-4 Ethylbenzene NU._._..::i 370 ug/kg 1634-04-4 Methyl Tert Butyl Ether 193 150 ug/kg _.... ........................... 91-20-3 Naphthalene hID 370 ug/kg 108-88-3 Toluene ND 370 ug/kg m,p-Xylene ND 370 ug/kg 95-47-6 o-Xylene U.. ....:: ,i 370 ug/kg CS-C8 Aliphatics(Unadj ) hID,,,,:,.:...... ; 7400 ug/kg :.: ......... ......... ........................... ........................... C9-C12 Aliphatics (Unadj.) <;;hlUi' ; ;;; ; 7400 ug/kg C9-C10 Aromatics (Unadj ) IUD 7400 ug/kg ........................... ........................... C5-C8 Aliphatics NU< >`> 7400 ug/kg C9-C12 Aliphatics NU.:,,. 74W ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 9:3% ; 70-130% 615-59-8 2,5-Dibromotoluene 104;% 70-130% ......................... ........................ ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 MADEP VPH FORM Matrix .:- A ueous Soil Sediment F1 Other Containers"__, Satisfactoryny Broken n Leaking A ueousPreservatives N/A H <=2 PH > 2 Rec'd at 1.5 de Received on Ice Received at 4 Deg. G Other g C Mef[anolJAQ Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio<0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: EXC01 (T) Lab ID: M39365-1 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95.2 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg 145000 A 10000 C9-C10 Aromatics(Unadj.) N/A ug/kg 127000" 10000 C9-C12 Aliphatics(Unadj.) N/A ug/kg 219000 A 10000 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg 19300 500 Toluene 108-88-3 C5-C8 ug/kg 31200 500 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg 1480 200 Benzene 71-43-2 C5-C8 ug/kg 612 500 Naphthalene 91-20-3 N/A ug/kg 3060 500 o-Xylene 95-47-6 C9-C12 ug/kg 21000 500 m,p-Xylene C9-C12 ug/kg 46600 500 Adiusted Ranges C5-C8 Aliphatics WA ug/kg 112000 a 10000 C9-C12 Aliphatics NIA ug/kg ND` 10000 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 105 70-130% PID:2,5-Dibromotoluene % 107 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'J'qualfier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? V Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑d Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑d No ❑ Yes=Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition. Laboratory Director Printed Name Reza Tand 9 Date 5/19/2004 MADEP VPH FORM Mari A ueous Soil Sediment Other Containers Satisfacto Broken- Leaking Aqueous Preservattvest N/A Eyl pH <= 2 F1 PH > 2 ern W,,ratule Received on Ice n Received at 4 Deg.C f Other d Redd at 1.5 deg C Methanol , Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio<0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: EXCO2(35) Lab ID: M39365-2 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 97 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/kg 103000" 8000 C9-C10 Aromatics(Unadj.) N/A ug/kg 213000 A 8000 C9-C12 Aliphatics(Unadj.) N/A ug/kg 303000" 8000 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg 14900 400 Toluene 108-88-3 C5-C8 ug/kg 19100 400 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg 1540 160 Benzene 71-43-2 C5-C8 ug/kg ND 400 Naphthalene 91-20-3 N/A ug/kg 12400 400 o-Xylene 95-47-6 C9-C12 ug/kg 22500 400 m,p-Xylene C9-C12 ug/kg 49500 400 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg 819000 8000 C9-C12 Aliphatics N/A ug/kg ND` 8000 Surrogate Recoveries Acceptance Range 1`0:25-Dibromotoluene % 119 70-130% PID:2,5-Dibromotoluene % 125 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cons of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 0 Yes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? V No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand 10 Date 5/19/2004 MADEP VPH FORM Matrix :r _..W A ueous Soil / Sediment F1 Other oritalnersx y _ Satisfactoryny Broken Leaking A ueousRreserGatnres N/A H<=2 H >2 gym° ratuie _ � r Received on Ice Received at 4 Deg. C Other d Rec'd at 1.5 deg C I Methanol Coverin Soil. mL Methanol! soil: Other NOTE: Ratio<0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: EXC03(3.5') Lab ID: M39365-3 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.1 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 7700 C9-C10 Aromatics(Unadj.) N/A ug/kg ND A 7700 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 7700 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 390 Toluene 108-88-3 C5-C8 ug/kg ND 390 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 150 Benzene 71-43-2 C5-C8 ug/kg ND 390 Naphthalene 91-20-3 N/A ug/kg ND 390 o-Xylene 95-47-6 C9-C12 ug/kg ND 390 m,p-Xylene C9-C12 ug/kg ND 390 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 7700 C9-C12 Aliphatics N/A ug/kg ND` 7700 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 97 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.37 No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand 11 Date 5/19/2004 MADEP VPH FORM Matrix h Aqueous Soil .i Sediment Other Cotilfamers s: Satisfacto Broken Iq Leaking A ueous Preseriratniesr N/A H <=2 L1 PH > 2 Terri eratulre ,' Rec'd at 1.5 deg C Received on Ice Received at 4 Deg. C Other Methanol _ j Methanol Coverin Soil. mL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH 98-1 Client ID: EXC04(3.5') Lab ID: M39365-4 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/15/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL (� C5-C8 Aliphatics(Unadj,) N/A ug/kg ND" 7400 C9-C10 Aromatics(Unadj.) N/A ug/kg ND A 7400 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 7400 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 370 Toluene 108-88-3 C5-C8 ug/kg ND 370 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg 193 150 Benzene 71-43-2 C5-C8 ug/kg ND 370 Naphthalene 91-20-3 NIA ug/kg ND 370 o-Xylene 95-47-6 C9-C12 ug/kg ND 370 m,p-Xylene C9-C12 ug/kg ND 370 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 7400 C9-C12 Aliphatics N/A ug/kg ND c 7400 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % 104 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'X Qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand 12 Date 5/19/2004 Accutest Laboratories GC Volatiles QC Data Summaries Includes the following where applicable: ■ Method Blank Summaries ■ Blank Spike Summaries ■ Matrix Spike and Duplicate Summaries ■ Surrogate Recovery Summaries 13 Method Blank Summary Page 1 of 1 Job Number: M39365 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB743-MB A1314931.1) 1 05/14/04 DL n/a n/a GAB743 The QC reported here applies to the following samples: Method: MADEP VPH 98-1 M39365-1, M39365-2, M39365-3, M39365-4 CAS No. Compound Result RL Units Q 71-43-2 Benzene dQ 250 ug/kg 100-41-4 Ethylbenzene NA 250 ug/kg 1634-04-4 Methyl Tert Butyl Ether it3:::;;;:;>>:>...... : 100 ug/kg 91-20-3 Naphthalene ND . 108-88-3 Toluene IIDr 250 ug/kg m,p-Xylene A 250 ug/kg 95-47-6 o-Xylene NI3:.......... :: 250 ug/kg C5- C8 Aliphatics(Unadj.) AID:.;::;:;::;.::;:;::;:5000 ug/kg ............ :....... C9- C12 Aliphatics (Unadj.) d�? > 5000 ug/kg C9- CIO Aromatics (Unadj ) ND 5000 ug/kg CS- C8 Aliphatics :;;:;<:; :;:; 5000 ug/kg C9- C12 Aliphatics ::;;::;:;::;: 5000 ug/kg CAS No. Surrogate Recoveries Limits . . 615-59-8 2,5-Dibromotoluene 9Q%. - ...__. 615-59-8 2,5-Dibromotoluene 97%a»i `i .. 70-130% 14 Blank Spike Summary Page 1 of 1 Job Number: M39365 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB743-BSP AB14932.D 1 05/14/04 DL n/a n/a GAB743 The QC reported here applies to the following samples: Method: MADEP VPH 98-1 M39365-1, M39365-2, M39365-3, M39365-4 Spike BSP BSP ,CAS No. Compound ug/kg ug/kg % Limits 7143-2 Benzene 1000 977 98 >> 70-130 ._....._.._. ................. 10041-4 Ethylbenzene 1000 1060 106 70-130 ................. 1634-044 Methyl Tert Butyl Ether 3000 3130 104 70-130 91-20-3 Naphthalene 2000 2250 113 70-130 108-88-3 Toluene 3000 2930 70-130 m,p-Xylene 4000 4010 I00.:;. ;; 70-130 _.. .. 95-47-6 o-Xylene 2000 2030 402 70-130 CAS No. Surrogate Recoveries BSP Limits .......... 615-59-8 2,5-Dibromotoluene 86.%.... 70-130% 615-59-8 2,5-Dibromotoluene 935.> <>«< 70-130% 15 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M39365 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M39363-1 MS a AB 14934.D 1 05/14/04 DL n/a n/a GAB743 M39363-1MSD aAB14935.D 1 05/14/04 DL n/a n/a GAB743 M39363-1 a AB14933.1) 1 05/14/04 DL n/a n/a GAB743 The QC reported here applies to the following samples: Method: MADEP VPH 98-1 M39365-1, M39365-2, M39365-3, M39365-4 M39363-1 Spike MS MS MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPI 71-43-2 Benzene ND 746 956 128 . 890 11.9 7 70-130/5 10041-4 Ethylbenzene ND 746 947 127 919 123 3: 70-130/5 1634-04-4 Methyl Tert Butyl Ether ND 2240 2900 130... 2760 123......._:.5... .....:,;. 70-130/5 91-20-3 Naphthalene ND 1490 1760 118 1830 123 4.::.....::; 70-130/5 108-88-3 Toluene ND 2240 2650 :118 2540 70-130/5 m,p-Xylene ND 2990 3590 12Q.: 3470 L1.6..........,3..:;;.,,:„:; 70-130/5 95-47-6 o-Xylene ND 1490 1820 . 1760 I.. . :.::... 70-130/52 ;;::. . :: ;:; CAS No. Surrogate Recoveries MS MSD M39363-1 Limits 615-59-8 2,5-Dibromotoluene 104% 10$% 99°fo. 70-130% 615-59-8 2,5-Dibromotoluene iO4�I 1U3;% 102°b 70-130% (a) Soil to methanol ratio greater than 1.25 to 1. . 16 f Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M39365 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 (REIMBMA) 1140 lyannough Rd., Hyannis, MA Method: MADEP VPH 98-1 Matrix: SO Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b M39365-1 AB14947.D (05 0 107.0 M39365-2 AB 14948.D :119 0 125.0 ....................... M39365-3 A1314949.1) 9 .a.Q ....;;, 97.0 ....................... M39365-4 A1314950.1) 930104.0 ....................... ...................... ....................... GAB743-BSP AB14932.D :86 ....0_ 93.0 ............................................. GAB743-MB AB14931.D 90 0 97.0 ...................... ....................... M39363-1MS A1314934.1) :JAN.iDi 104.0 M39363-1MSD AB14935.D 108:0:::> :: 103.0 ....................... Surrogate Recovery Compounds Limits St = 2,5-Dibromotoluene (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 17 Accutest Laboratories I Mise Forms Custody Documents and Other Forms Includes the following where applicable: ■ Sample Tracking Chronicle 18 Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Job No: M39365 Project No: GSC PO# 16988 Sample Number Method Analyzed By Prepped By Test Codes .................... ................... .......... ..:.x A ....... .... .......... ............ ................................. ............... . ... ....................................... ......... ......... ......................... . ........ . ......... .. ......... . -........... ........... ... .. ........... .... . ................ ...................%............-I....... .... ................. .. .. ................................. .8 . ......... . ......... .... ..... .............. ... ......... ........... ....... ... .................... .. . ...... ............ ----- . ..................... .. ................... .. ... .. . M39365-1 EPA 160.3 M 13-MAY-04 OP %SOL M39365-1 MADEP VPH 98-1 14-MAY-04 22:14 DL VMAVPH ........................... ......... ............ ........ ... . ............. .. ..... .... ............. ... . ............. ... ...................................................... . ... ...................... .65_3 ............... 04- . ....... M5 R ............................... .............. .. ................. .. .......... A ... .. ... . .......... ................... .......... ................................ ... ................. ... ........... . . .................... .. .. ...... .. ... ................ . .................. - .... 1. ...... ...... ....... ............ .. . .... ........... x: ..................... ....................................-+ .... ...... .......... ............................ ..... ........... ... .. ...... ........ ..................... ......... . ... ............ ............ .....................% �-,: ��� .......... ............... ..... . ........... ................ ...... .. ... .... ........... ... ............ .. .. M39365-2 EPA 160.3 M 13-MAY-04 OP %SOL M39365-2 MADEP VPH 98-1 14-MAY-04 22:54 DL VMAVPH ............................. .......... . .. .............. ................................. 't6 ................M....... ............. ................ B"..............................................R........,. .............................J....2............W.......................... ..... ................................................. ............................................................................. ............................................... -....-....-....- ................................ ................................... .................................. ...:. - +:.: ,+ : .. . ........ .... ..+..+.: .":: .............................. .... .... ............ .. .......................... ...... ....... ................. ............... .. ............... .......................... M39365-3 EPA 160.3 M 13-MAY-04 OP %SOL M39365-3 MADEP VPH 98-1 14-MAY-04 23:34 DL VMAVPH . .... .. . ...........................w:..... ........... ............................................ .. ................ ........... ................. . . ...............I'VM14...... ........... .. . ...... 'AY Wo ........... .40 .................A- ............ ................................ ......................... ............ ......................... ......... ....... .......... . . .... . .... . ... ................. .......................... .......... . ....... r-. ......... .... . ..................... .. .......... ........... ... ....... ..... ................................................................... .............. ..................... ............ . ...... . .... .................... ...................... ......................................... M39365-4 EPA 160.3 M 13-MAY-04 OP %SOL M39365-4 MADEP VPH 98-1 15-MAY-04 00:15 DL VMAVPH Page I of I 19 Betty Baer From: Moira Walker[mwalker@ma.gsc-global.com] Sent: Wednesday, May 12, 2004 11:24 AM To: Betty Baer Subject: 1140 lyannough Rd, Hyannis Betty, GSC submitted soil samples from Texaco Station#100083 located at 1140 lyannough, Hyannis MA today and during the previous weeks. Please note that these soil samples are from a GW-1 site and therefore must have the S-1/GW-1 detection limits. Also, because it is in the state of MA,we would like the MCP CAM level of qa/qc. Please contact me at 978-568-8740 x257 should you have any questions or would like me to fax over a revised Chain of Custody. Thank you, Moira Moira Walker Geologist Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 Toll Free: 800 522 8740 Tel:978 568 8740 x257 Fax:978 568 9316 mwalker@ma.gsc-global.com www.gsc-global.com NOTICE: This e-mail message and any attachment to this e-mail may contain confidential information that may be legally privileged. If you are not the intended recipient, you must not review, retransmit, convert to hard-copy, copy,use or disseminate this a-mail and any attachment to it. If you have received this e-mail in error, please notify us by return e-mail or by telephone at 978 568 8740 and delete this message. Please note that if this e-mail message contains a forwarded-message or is a reply to a prior message, some or all of the contents of this message or any attachments may not have been produced by GSC. This notice is automatically appended to each e-mail message sent from GSC. Thank you. 495 TECHNOLOGY CENTER WEST - BUILDING ONE ®ACCUTEST MARLBOROUGH,MA 01752 ACCUTEST QUOTE#: TEL:508-481-6200 • FAX:508.481-7753 CLIENT INFORMATION FACIUITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES O n OW• DRINKING /,� 1 O.1(�1(1 I� S� 1�_ WATER �PD�(�i�y V�C:2� t�7 /� ��� GW- GROUND NAM (i PROJECT NAME }�� ,q� WATER Is �r►a.��; &'tf llyd x.n aAnc a�. J�C.� Lf VIMA� %A _ WW• WASTE AD��<1171 1 iA . d/7Y. / _ LOCATION] __T l000 O 3 WATER SO• SOIL CITY, ,Q {� STATE ZIP P OIJECT NO. Ql� }� Q S01- OIL L- SLUDGE 1'1 f tJ//`tilh0 y 1� 90• T V T� `U6 6 _ L /y� G- OTHER SEND & LIQUID PHONE#RTTo97ff'S�o ��7 FAX 97SS-Ss` / 3f!�� SOL-OTHER COLLECTION x PRESERVATIO ;n SOLtD ACCUTEST SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SA BYLED Q z LAB USE ONLY j 5 �11 W Soi� X X -.;k - C3,s' 3 CxCoRC3�s' l000 -f ' " DATA DELIVERABLE INFORMATION ' a, COMMENTS/REMARKS s' DATA TURNAROUND INFORMATION 14 DAYS STANDARD APPROVED BY: O STANDARD acdl_64/ = Rcu, (7idnQ 7 DAYS RUSH O COMMERCIAL"B" O 48 HOUR EMERGENCY O DISK DELIVERABLE \t_ Q�ITAPA W/ locro 11'l¢ O OTHER c � ❑ STATE FORMS `Q (OG 3 N 7 T� 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) V DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIV RELINOUISNED Y SA NPL.R: DATE TIME: RECEIVED BYE•- REU UISNE BY: DATE TIME: RECEIVED BYi - - Io 1 , t . 2 iaC1416n0 2. 44 RELIN UIS D BY: AT TIME: �;f -RECEIVED B R QUISHED BY: DATE TIME: RECEIVED BY: 3. � . wo RELIN UISHED Y: OA E TI E: RECEI D BY: SEAL 9 PRESERVE WHERE APPLICABLE ON ICE TEMPERATURE S. MAY 12 2004 ®� New England OS/10/04 GJACCUTOWE ® rab Technical Report for Shell Oil GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Cost Element #707542 Accutest Job Number: M39055 Sampling Date: 04/26/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 9 4�C�M 11CCpRO v f Test results contained within this data package meet the requirements /,z a Z.d of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications: MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 495 Tech Center West 0 Building 1 0 Marlborough,MA 01752 0 tel: 508481-6200 0 fax:508-481-7753 0 http://www.accutest.com Accutest Laboratories Sample Summary Shell Oil Job No: M39055 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Project No: Cost Element #707542 _. . . ._._.. . . _.............. Sample Cotlectecl: Matrix Client Number Date Time By Received Code Type Sample ID ................................ Ivi39055 1_: 04/26/04 10:40 MW 04/26/04 SO Soil LIFT B6 7') M39055-2 - <;04/26/04 10:45 MW 04/26/04 SO Soil Soil samples reported on a dry weight basis unless otherwise indicated on result.page. Accutest Laboratories Report of Analysis Page I of I Client Sample ID: LIFT BOTT(6-7') Lab Sample ID: M39055-1 Date Sampled: 04/26/04 Matrix: SO - Soil Date Received: 04/26/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 95.6 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27632_D 1 05/10/04 ME 04/29/04 OP7088 GPO1842 Run#2 Initial Weight Final Volume Run#1 10.1 g 2.0 n-d Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene .... 520 ug/kg 208-96-8 Acenaphthylene ND 520 ug/kg 120-12-7 Anthracene ND 520 ug/kg 56-55-3 Benzo(a)anthracene ND 520 ug/kg 50-32-8 Benzo(a)pyrene ND 520 ug/kg 205-99-2 Benzo(b)fluoranthene :::ND:".. 520 ug/kg 191-24-2 Benzo(g,h,i)perylene ND..........:::: 520 ug/kg 207-08-9 Benzo(k)fluoranthene ND 520 ug/kg 218-01-9 Chrysene ND 520 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 520 ug/kg 206-44-0 Fluoranthene ND 520 ug/kg 86-73-7 Fluorene ND 520 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 520 ug/kg 91-57-6 2-Methylnaphthalene :ND 520 ug/kg 91-20-3 Naphthalene NI1 520 ug/kg 85-01-8 Phenanthrene ND 520 ug/kg 129-00-0 Pyrene N;D 520 ug/kg CI I-C22 Aromatics (UnadJ ) 19200 18000 ug/kg C9-C18 Aliphatics :98:7�.,;.;..;:.;.: . `6200 ug/kg C19-06 Aliphatics 5550.0 8300 ug/kg ........................... ........................... .......................... CI I-C22 Aromatics 1;$500 18000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 7S% 40-140% 321-60-8 2-Fluorobiphenyl 8..1%:..,,;;;; 40-140% .......... ... ..... _.._. 580-13-2 2-Bromonaphthalene 69% 40-140% 3386-33-2 1-Chlorooctadecane 72% 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: LIFT BOTT(6-7') Lab Sample ID: M39055-1 Date Sampled: 04/26/04 Matrix: SO- Soil Date Received: 04/26/04 Method: SW846 8082 SW846 3545 Percent Solids: 95.6 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 EF38743.1) 1 05/07/04 NM 04/28/04 OP7084 GEF1966 Run#2 Initial Weight Final Volume Run#1 15.7 g 10.0 nil Run#2 PCB List CAS No. Compound Result RL Units Q ....._.............._. 12674-11-2 Aroclor 1016 Np _ i 100 ug/kg 11104-28-2 Aroclor 1221 ND 100 ug/kg 11141-16-5 Aroclor 1232 ND _ 100 ug/kg 53469-21-9 Aroclor 1242 ;:.....: 100 ug/kg 12672-29-6 Aroclor 1248 ND: :::> ;:>: 100 ug/kg 1 1 097-69-1 Aroclor 1254 NI 100 ug/kg 11096-82-5 Aroclor 1260 1 < 100 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ........................ 877-09-8 Tetrachloro-m-xylene 1Q(?`J 30-134% 877-09-8 Tetrachloro-m-xylene l:fl %::::;:;;:;»> 30-134% 2051-24-3 Decachlorobiphenyl 1:2 :%;::;_::;;: ' 34-150% 2051-24-3 Decachlorobiphenyl 1j: ;;.< 34-150% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: LIFT ESW(34') Lab Sample ID: M39055-2 Date Sampled: 04/26/04 Matrix: SO- Soil Date Received: 04/26/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 94.6 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27542.1) 1 05/05/04 ME 04/29/04 OP7088 GPO1838 Run#2 Initial Weight Final Volume Run#1 10.4 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q ........................... 83-32-9 Acenaphthene ND.. 510 ug/kg 208-96-8 Acenaphthylene NID 510 ug/kg 120-12-7 Anthracene ND 510 ug/kg 56-55-3 Benzo(a)anthracene ND::,::;::;:;::;:>=;:: 510 ug/kg 50-32-8 Benzo(a)pyrene ND......._ : 510 ug/kg . 205-99-2 Benzo(b)fluoranthene NT3;;;;_.,;; 510 ug/kg 191-24-2 Benzo(g,h,i)perylene NID 510 ug/kg 207-08-9 Benzo(k)fluoranthene IVp 510 ug/kg 218-01-9 Chrysene ND.:;>:::::::; ;:: 510 ug/kg 53-70-3 Dibenz(a,h)anthracene 510 ug/kg 206-44-0 Fluoranthene ND.;..;:.:.:;.:.:;> 510 ug/kg 86-73-7 Fluorene ND 510 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 510 ug/kg 91-57-6 2-Methylnaphthalene ND 510 ug/kg 91-20-3 Naphthalene ND 510 ug/kg .......::................. 85-01-8 Phenanthrene 1VD 510 ug/kg. 129-00-0 Pyrene ND 510 ug/kg CI1-C22 Aromatics(UnadJ ) N:D.,.,,......>.s: 17000 ug/kg C9-C18 Aliphatics ND ._......_i:..;`. 6100 ug/kg C19-C36 Aliphatics Nb._... 8100 ug/kg .......... _. ........................... CII-C22 Aromatics ND : 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-I5-1 o-Terphenyl 40-140% 321-60-8 2-Fluorobiphenyl 82% 40-140% 580-13-2 2-Bromonaphthalene ?D% 40-140% 3386-33-2 1-Chlorooctadecane 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: LIFT ESW (3-4') Lab Sample ID: M39055-2 Date Sampled: 04/26/04 Matrix: SO- Soil Date Received: 04/26/04 Method: SW846 8082 SW846 3545 Percent Solids: 94.6 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 EF38744.1) 1 05/07/04 NM 04/28/04 OP7084 GEF1966 Run#2 Initial Weight Final Volume Run#1 15.4 g 10.0 ml Run#2 PCB List CAS No. Compound Result RL Units Q ........................... 1 2674-1 1-2 Aroclor 1016 NI3i ; ; 100 ug/kg 11104-28-2 Aroclor 1221 100 ug/kg ...:....................... ........................... 11141-16-5 Aroclor 1232 ND 100 ug/kg 53469-21-9 Aroclor 1242 NI? << 100 ug/kg 12672-29-6 Aroclor 1248 ND 100 ug/kg 11097-69-1 Aroclor 1254 N' ; > `; < 100 ug/kg ....:.....................: ........................... 11096-82-5 Aroclor 1260 ND ; 100 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits .-...................... 877-09-8 Tetrachloro-m-xylene ..87%>;;; 30-134% ....................... 877-09-8 Tetrachloro-m-xylene $9 ; <; 30-134% ......................... .......................- 2051-24-3 Decachlorobiphenyl 1Ii3%: _ 34-150% 2051-24-3 Decachlorobiphenyl 106%. 34-150% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound nnHutr trM I-UKM ffaz110.' Aqueous Soil v' Sediment Other Ct[�tarners = - SatisfactorvW Broken F1 Leakin tieustr eafaies NIA H<=2 H>2 r Received on Ice Received at 4 Deg.C Other Rec'd at 1.9 deg C OW-!N tlo et0001M SW846 3545 ,Method for Ranges: MADEP EPH 98-1 Client ID: LIFT BOTT(6-7') Lab ID: M39055-1 Method for Targets: MADEP EPH 98-1 Date Collected: 4/26/2004 Date Received: 4/26/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 4/29/2004 5/10/2004 N/A EPH Fractionation .2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 95.6 1 N/A nad'usted Ran es CAS# Units Result RDL g C11-C22 Aromatics(Unadj.) ug/kg 19200" 18000 iesel PAH Anal es 2-Methylnaphthalene 91-57-6 ug/kg ND 520 Phenanthrene 85-01-8 ug/kg ND 520 Acenaphthene 83-32-9 ug/kg ND 520 Naphthalene 91-20-3 ug/kg ND 520 Other Tar et PAH Anal es Acenaphthylene 208-96-8 ug/kg ND 520 Anthracene 120-12-7 ug/kg ND 520 Benzo(a)anthracene 56-55-3 ug/kg ND 520 Benzo(a)pyrene 50-32-8 ug/kg ND 520 Benzo(b)fluoranthene 205-99-2 ug/kg ND 520 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 520 Benzo(k)fluoranthene 207-08-9 ug/kg ND 520 Chrysene 218-01-9 ug/kg ND 520 Dibenz(a,h)anthrac:ene 53-70-3 ug/kg ND 520 Fluoranthene 206-44-0 ug/kg ND 520 Fluorene 86-73-7 ug/kg ND 520 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 520 Pyrene 129-00-0 ug/kg ND 520 Adiusted Ranges C9-C18 Aliphatics ug/kg 9870" 6200 C19-C36 Aliphatics ug/kg 55500" 8300 C11-C22 Aromatics ug/kg 185008 18000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 72 40-140% o-Terphenyl % 75 40-140% 2-Fluorobiphenyl % 81 40-140% 2-Bromonaphthalene % 69 40-140% ootnotes Hydrocarbon Range data exclude concentrations of any surtogate(s)and/or Internal standards eluting In that range Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? Yes ❑ No-Details Attatched ere all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched ere any significant modifications made to the EPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the nformation,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature ���� Postition Laboratory Director Printed Name Reza Tand Date . 5/10/2004 MADEP EPH FORM Matnz s � Aqueous F1 Soil Sediment n Other SatisfactoryFy Broken n Leaking F1 l�k > s1=eaives N/A PH <=2 n pH> 2 Received on Ice F Received at 4 Deg. C Other Read at 1.9 deg C Try . Eacto )A. lho� SW846 3545 Method for Ranges. MADEP EPH 98-1 Client ID: LIFT ESW(3-4) Lab ID: M39055-2 Method for Targets: MADEP EPH 98-1 Date Collected: 4/26/2004 Date Received: 4/26/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 4/29/2004 5/5/2004 N/A Solids: Low Dilution: High Dilution: EPH Fractionation 2-Fluorobiphenyl 9 Surrogate Standards. 2-Bromonaphthalene 94-6 1 N/A Unadjusted Ranges CAS# Units Result RDL g C11-C22 Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 510 Phenanthrene 85-01-8 ug/kg ND 510 Acenaphthene 83-32-9 ug/kg ND 510 Naphthalene 91-20-3 ug/kg ND 510 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 510 Anthracene 120-12-7 ug/kg ND 510 Benzo(a)anthracene 56-55-3 ug/kg ND 510 Benzo(a)pyrene 50-32-8 ug/kg ND 510 Benzo(b)fluoranthene 205-99-2 ug/kg ND 510 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 510 Benzo(k)fluoranthene 207-08-9 ug/kg ND 510 Chrysene 218-01-9 ug/kg ND 510 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 510 Fluoranthene 206-44-0 ug/kg ND 510 Fluorene 86-73-7 ug/kg ND 510 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 510 Pyrene 129-00-0 ug/kg ND 510 Adiusted Ranges C9-C18 Aliphatics ug/kg ND" 6100 C19-C36 Aliphatics ug/kg ND" 8100 C11-C22 Aromatics ug/kg ND a 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 72 40-140% o-Terphenyl % 77 40-140% 2-Fluorobiphenyl % 82 40-140% 2-Bromonaphthalene % 70 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A V qualifier indicates an estimated value i Were all QA/QC procedures REQUIRED by the EPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ . No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? No ❑ Yes.Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date' 5/10/2004 495 TECHNOLOGY CENTER WEST • BUILDING ONE 12ACCTESTol. MARLBOROUGH,MA 01752 ACCVTEST QUOTE#: TEL:508-481-6200 • FAX.508-481-7753 CLIENT INFORMATION logo= FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES DW. DRINKING WATER NAME PROJECT NAME Q ( r i S �� GW. GROUND �� Z��QVI1�LOl.1 Q�. Afl f`1V(� _ WATER WW• WASTE ADDRESS �1 LOCATION Tr WATER Ha2d m'1 0�74/9 oons e SO- SOIL CITY�1 f/ Q STATE ZIP P JECT NO. '-7' SL- SLUDGE A L�IL e tL Yi �,,ke 't°�'�•e�(L�" /A 7sy z LIO oIL c p G / p / Lb• OLIQUID THER PHONE#SEND RT TQ� _S6 6-k 7 AO FAX# / 7[� -�(O S �I 1 �n SOL-OTHER ��L LZ IU COLLECTION x H PRESERVATION SOLID ACCUTEST SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLE; g „$ LAB USE ONLY '04 d rnw I 01w I Y Loc. 38 y DATA TURNAROUND INFORMATION e, DATA DELIVERABLE INFORMATION ' COI MMENTS/REMARKS .1 14 DAYS STANDARD APPROVED BY: STANDARD �i�� wee>LS" ccnL elernQ, - 7 DAYS RUSH O COMMERCIAL B O 48 HOUR EMERGENCY O DISK DELIVERABLE O OTHER O STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX O OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED ,.",• �, SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIIAE SAMPLES CHANGE POSSESI N,INC UDING COURIE ELIVE Y 111 RELINOUISHED BY S MP OAT TIME: ECEIVED BY: RE U Oull B DAT ME: ;t6 RECENED kREVLINOONED . 2. 02.DAT T RECEIVED B R QUISHE Y: DA TI� 3� c 4.BY TE RE E ED BY: g L 4 PRESERVE WHERRE APPLICABLE ON ICf, TEMPERATURE. 5. [� -�sl -44— New England OS/18/04 12A=LrrEff r. MAY® L __ .... LL.. : ._ _ 29gy Technical Report for Shell Oil GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M39304 Sampling Date: 05/04/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 9 M z Test results contained within this data package meet the requirements teza and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications: MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England ■ 495 Tech Center West■ Building 1 ■ Marlborough,MA 01752 0 tel:508-481-6200 0 fax:508-481-7753 0 http://www.accutest.com Accutest Laboratories Sample Summary Shell Oil Job No: M39304 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID IVI39304 1 05/04/04 14:35 DG 05/10/04 SO Soil TANK 2 EAST ; 1YI.... 2 05/04/04 13:55 DG 05/10/04 SO Soil TANK 2 WEST?' M39304 3; 05/04/04 14:20 DG 05/10/04 SO Soil TANK 2 BOTTI. OM 12 - Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 2 EAST 7' Lab Sample ID: M39304-1 Date Sampled: 05/04/04 Matrix: SO - Soil Date Received: 05/10/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 92.1 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25873.1) 1 05/15/04 SL 05/10/04 OP7134 GGH2373 Run#2 Initial Weight Final Volume Run#1 10.4 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene ND 520 ug/kg 208-96-8 Acenaphthylene ND 520 ug/kg 120-12-7 Anthracene ND 520 ug/kg 56-55-3 Benzo(a)anthracene ND 520 ug/kg 50-32-8 Benzo(a)pyrene ND............... . 520 ug/kg 205-99-2 Benzo(b)fluoranthene ND 520 ug/kg 491-24-2. Benzo(g,h,i)perylene ND...._; < 520 ug/kg 207-08-9 Benzo(k)fluoranthene ND.. 520 ug/kg 218-01-9 Chrysene ND 520 ug/kg 53-70-3 Dibenz(a,h)anthracene N.D..::::>:;:>:; 520 ug/kg 206-44-0 Fluoranthene N520 ug/kg ............. _._._........._... 86-73-7 Fluorene `ND..... 520 ug/kg 193-39-5 Indeno(1,2,3 cd)pyrene ND 520 ug/kg . 91-57-6 2-Methylnaphthalene ND 520 ug/kg 91-20-3 Naphthalene 520 ug/kg 85-01-8 Phenanthrene NQ.......:: .... 520 ug/kg 129-00-0 Pyrene ND 520 ug/kg C11-C22 Aromatics(Unadj ) ND 18000 ug/kg C9-C18 Aliphatics ND 6300 ug/kg ._ ........................... C19-C36 Aliphatics ND 8400 ug/kg CII-C22 Aromatics ND 18000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 84-15-1 o-Terphenyl 81% 40-140% 321-60-8 2-Fluorobiphenyl 40-140% 580-13-2 2-Bromonaphthalene 15% 40-140% 3386-33-2 1-Chlorooctadecane 60% 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 2 WEST 7' Lab Sample ID: M39304-2 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 93.5 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25874.D 1 05/15/04 SL 05/10/04 OP7134 GGH2373 Run#2 Initial Weight Final Volume Run#1 10.5 g 2.0 nil Run#2 CAS No. Compound Result RL Units Q .1........................ 83-32-9 Acenaphthene ND 510 ug/kg 208-96-8 Acenaphthylene N ,. 510 ug/kg 120-12-7 Anthracene ND 510 ug/kg 56-55-3 Benzo(a)anthracene ND 510 ug/kg 50-32-8 Benzo(a)pyrene ND 510 ug/kg 205-99-2 Benzo(b)fluoranthene 510 ug/kg 191-24-2 Benzo(g,h,i)perylene hID 510 ug/kg 207-08-9 Benzo(k)fluoranthene D > 510 ug/kg . 218-01-9 Chrysene ND 510 ug/kg 53-70-3 Dibenz(a,h)anthracene hID 510 ug/kg 206-44-0 Fluoranthene ND 510 ug/kg 86-73-7 Fluorene ] D:<::< :::> :>: 510 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 510 ug/kg 91-57-6 2-Methylnaphthalene I(D_ iii< ` 510 ug/kg 91-20-3 Naphthalene ND 510 ug/kg 85-01-8 Phenanthrene ND......... :..: 510 ug/kg ........................... ............_.. ........................... 129-00-0 Pyrene ND 510 ug/kg CII-C22 Aromatics(Unadj.) .IUD,,,;:.::.;;;:;;:_;;; 17000 ug/kg ........................... ........................... C9-C 18 Aliphatics ND. 6100 ug/kg C19-06 Aliphatics ND:.::;;;::: ..>;:;>>; 8200 ug/kg CII-C22 Aromatics .ND.....:,... .,: 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... ......................... 84-15-1 o-Terphenyl 8S% 40-140 321-60-8 2-Fluorobiphenyl 8.5% 40-140% 580-13-2 2-Bromonaphthalene 7 %.. ::::;::;; 40-140% ......................... ......................... ........................ 3386-33-2 1-Chlorooctadecane 67%...._: .: 40-140% ......................... ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 2 BOTTOM 12' Lab Sample ID: M39304-3 Date Sampled: 05/04/04 Matrix: SO - Soil Date Received: 05/10/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 96.1 l Project: GSCMA:96925028 1140 lyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25875.1) 1 05/15/04 SL 05/10/04 OP7134 GGH2373 Run#2 Initial Weight Final Volume Run#1 10.5 g 2.0 nil Run#2 CAS No. Compound Result RL Units Q ........................... 83-32-9 Acenaphthene ND 500 ug/kg 208-96-8 Acenaphthylene hlD 500 ug/kg 120-12-7 Anthracene I�1D 500 ug/kg 56-55-3 Benzo(a)anthracene ND................ 500 ug/kg 50-32-8 Benzo(a)pyrene ND 500 ug/kg 205-99-2 Benzo(b)fluoranthene ND 500 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 500 ug/kg 207-08-9 Benzo(k)fluoranthene ND.::.,:;;::::,::. 500 ug/kg 218-01-9 Chrysene XND. 500 ug/kg N 53-70-3 Dibenz(a,h)anthracene D... ; 500 ug/kg 206-44-0 Fluoranthene ND 500 ug/kg 86-73-7 Fluorene hID - : 500 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 500 ug/kg 91-57-6 2-Methylnaphthalene ,ND.._. 500 ug/kg 91-20-3 Naphthalene ND......:: ...::: 500 ug/kg ........................... __._.... ........................... 85-01-8 Phenanthrene ND 500 ug/kg 129-00-0 Pyrene ND 500 ug/kg C11-C22 Aromatics (Unadj.) 'h ;:;:;;:; 17000 ug/kg C9-C 18 Aliphatics ND_ 5900 ug/kg C 19-C36 Aliphatics ND 7900 uglkg CII-C22 Aromatics ND 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 75% 40-140% 321-60-8 2-Fluorobiphenyl 40-140% 580-13-2 2-Bromonaphthalene 71% 40-140% 3386-33-2 1-Chlorooctadecane ..59;%.::::.> .:: 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MADEP EPH FORM Ma'T1X A ueous F1 Soil Sediment F Other ❑ Ccintainers batisfactoryny Broken n Leaking A `ueous Preservatives:; N/A H <=2 H > 2 F] Tern '` nature Received on Ice n Received at 4 De- . C ❑ Other d Rec'd at 2.7 deg C Extrctton Method SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: TANK 2 EAST 7' Lab ID: M39304-1 Method for Targets: MADEP EPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/10/2004 5/15/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 92.1 1 N/A Unadiusted Ranges CAS# Units Result RDL G3 C11-C22 Aromatics(Unadj.) ug/kg ND" 18000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 520 Phenanthrene 85-01-8 ug/kg ND 520 Acenaphthene 83-32-9 ug/kg ND 520 Naphthalene 91-20-3 ug/kg ND 520 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 520 Anthracene 120-12-7 ug/kg ND 520 Benzo(a)anthracene 56-55-3 ug/kg ND 520 Benzo(a)pyrene 50-32-8 ug/kg ND 520 Benzo(b)fluoranthene 205-99-2 ug/kg ND 520 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 520 Benzo(k)fluoranthene 207-08-9 ug/kg ND 520 Chrysene 218-01-9 ug/kg ND 520 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 520 Fluoranthene 206-44-0 ug/kg ND 520 Fluorene 86-73-7 ug/kg ND 520 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 520 Pyrene 129-00-0 ug/kg ND 520 Adiusted Ranges C9-C18 Aliphatics ug/kg ND A 6300 C19-C36 Aliphatics ug/kg ND A 8400 C11-C22 Aromatics ug/kg ND 8 18000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 60 40-140% o-Terphenyl % 81 40-140% 2-Fluorobiphenyl % 85 40-140% I 2-Bromonaphthalene % 75 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. Ct t-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? d❑No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature �'��-- Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 MADEP EPH FORM Matrix A ueous F] Soil Sediment n Other Coritatners Satisfactory n Broken I Leaking A ueous_Preservatives N/A P/, pH <= 2 I! pH > 2 T,etn- r'ature , Received on Ice —I Received at 4 Deg. C Other d Rec'd at 2.7 deg C Extractton-Mefhod SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: TANK 2 WEST 7' Lab ID: M39304-2 Method for Targets: MADEP EPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/10/2004 5/15/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 93.5 1 N/A Unadiusted Ranges CAS# Units Result RDL C11-C22 Aromatics(Unadj.) ug/kg ND A 17000 (Diesel PAH Analytes 2-Methyinaphtha'lene 91-57-6 ug/kg ND 510 Phenanthrene 85-01-8 ug/kg ND 510 Acenaphthene 83-32-9 ug/kg ND 510 Naphthalene 91-20-3 ug/kg ND 510 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 510 Anthracene 1120-12-7 ug/kg ND 510 Benzo(a)anthracene 56-55-3 ug/kg ND 510 Benzo(a)pyrene 50-32-8 ug/kg ND 510 i ! Benzo(b)fluoranthene 205-99-2 ug/kg ND 510 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 510 ! Benzo(k)fluoranthene 207-08-9 ug/kg ND 510 Chrysene 218-01-9 ug/kg ND 510 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 510 Fluoranthene 206-44-0 ug/kg ND 510 Fluorene 86-73-7 ug/kg ND 510 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 510 Pyrene 129-00-0 ug/kg ND 510 Adjusted Ranges C9-C18 Aliphatics ug/kg ND" 6100 C19-C36 Aliphatics ug/kg ND" 8200 ! C11-C22 Aromatics ug/kg ND a 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 67 40-140% o-Terphenyl % 85 40-140% 2-Fluorobiphenyl % 85 40-140% 2-Bromonaphthalene % 70 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surtogate(s)and/or internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes 2 A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 MADEP EPH FORM Matrix Aqueous F] Soil Sediment Other Cah inners Satisfacto Lv Broken Leakin A ueous Preservatives'' N/A I./I pH <=2 F PH > 2 m�efature Received on Ice Received at 4 Deg. C I i Other d Rec'd at 2.7 deg C Te Eztract�on,flllethod W SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: TANK 2 BOTTOM 12' Lab ID: M39304-3 Method for Targets: MADEP EPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last.Date Run: Aromatic o-Terphenyl 5/10/2004 5/15/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 96.1 1 N/A IUnadjusted Ranges CAS# Units Result RDL C3 C11-C22 Aromatics(Unadi.) ug/kg ND A 17000 Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 500 Phenanthrene 85-01-8 ug/kg ND 500 Acenaphthene 83-32-9 ug/kg ND 500 Naphthalene 91-20-3 ug/kg ND 500 Other Target PAH Analvtes Acenaphthylene 208-96-8 ug/kg ND 500 Anthracene 120-12-7 ug/kg ND 500 Benzo(a)anthracene 56-55-3 ug/kg ND 500 Benzo(a)pyrene 50-32-8 ug/kg ND 500 Benzo(b)fluoranthene 205-99-2 ug/kg ND 500 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 500 Benzo(k)fluoranthene 207-08-9 ug/kg ND 500 Chrysene 218-01-9 ug/kg ND 500 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 500 Fluoranthene 206-44-0 ug/kg ND 500 Fluorene 86-73-7 ug/kg ND 500 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 500 Pyrene 129-00-0 ug/kg ND 500 Adjusted Ranges C9-C18 Aliphatics ug/kg ND" 5900 C19-C36 Aliphatics ug/kg ND" 7900 C11-C22 Aromatics ug/kg ND a 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 59 40-140% o-Terphenyl % 75 40-140% 2-Fluorobiphenyl % 83 40-1.40% 2-Bromonaphthalene % 71 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surcogate(s)and/or internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A V qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? 66 Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 w 495 Tech Center West,Bldg. 1,Marlboro, 53 01752 MACCUTEMIS (508)481-6200 Fax: (508)481-7753 Accutest Job#: V 3 n 30 is Client information • Faclli In ormation r. r Analytical Information onsultants Name Project Name Geologic Services Corporation SOPUS Hyannis "dress Street City 15 Bonazzoli Ave. state lip a e 1140 I anou h Rd __._. -- Hudson MA 01749 Hyannis MA Project Contact: Invoice Contact, Phone#: 978-568.8740 Invoice Phone# \'t Fax#: 978-568-9316 Location ID# 100083 FE# q 6 11 1zOoZ 0 Collection Preservation #of U O 2 N w $ o Field ID/Point of Collection Qate, Time Sampled 81 Matrix I bottles = Z Sdv C a- WPAf "a Turnaround Information - Data Deliverable Information a.:, ,, S• • 11 Acculesl Log-in Information < Z;Std.14 Day Turnaround Approved By: Commerclal"A" O FULL CLP, V 7 Day EMERGENCY 0 Commercial"B" Q State Forms 4 Day EMERGENCY o Full Dellverables Q Disk Deliverable Format_ 3 Day EMERGENCY Other 2 Day EMERGENCY /� ❑ dC- 0 1 Day EMERGENCY A Emergency T/A Is for FAX or Labllnk Data Commercial"A"-Results Only =hed Sam le Custod must bed cumented below each times pies change posseslon,including course eliv tips L'By:r: a e a ece ve a a e a e ime: ace y:S 1 2r: a eee v e i qu. y: s e ime: ecerve o '3 4 4 3e nq e y amp er �- a e e ea reserve w ere app ca e n ce C emp. 5 5 ❑ l OF tHE 1p� + + * BARNSTABLE, MASS. The Town of Barnstable ODA i639, ♦0 Office of Town Manager 367 Main Street, Hyannis MA 02601 ,vww.town.barn.stable.ma.us Office: 508-862-4610 John C. Klimm, Town Manager Fax: 508-790-6226 Email: john.klimm@a,town.barnstable.ma.us MEMORANDUM TO: Tom eiler, Regulatory G g tort'Services FR: John C. Klimm, Town Manage DT: March 22, 2004 RE: Release Abatement Measure Plan Texaco Service Station #100083 1140 Iyanough Road Hyannis, Massachusetts RTN- 4-11301 Tier IC Permit#100556 ACO-SE-03-3S-002 For your information I am sending to you a packet from the Geologic Services Corporation on the above said matter. Thank you, JCK: smo Attachment �s r Geologic Services Waybill#20874530950r RS.3T ii Corporation TOWN! �Q Q@ e,engineering&technology March 16, 2004 10 'N6 ':: uP '' i= Massachusetts Department of Environmental Protection .� MAR 19 A10 :G4 Southeast Regional Office Bureau of Waste Site Cleanup Attn: Ms. Laura Stanley 20 Riverside Drive Lakeville,MA 02347 Re: Release Abatement Measure Plan Texaco Service Station#100083 1140 Iyannough Road Hyannis,Massachusetts RTN 4-11301 Tier IC Permit#100556 ACO-SE-03-3S-002 Dear Ms. Stanley: Geologic Services Corporation(GSC), on behalf of Motiva Enterprises LLC(Motiva), has prepared this Release Abatement Measure(RAM)Plan for the above referenced site. The objective of this RAM Plan is to appropriately manage petroleum-impacted soil, if encountered,during the construction activities scheduled to begin in April 2004. The original signature copy of BWSC-106 form has been included with this submittal. The contact at Motiva responsible for overseeing the response actions associated with this site is Mr. David B.Weeks,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590; (845)462-5225. The attached documents have been prepared under the direction of Licensed Site Professional(LSP)Mr. Scott K.Parker(LSP#9969)of GSC. Should you have any questions or concerns,please do not hesitate to contact Mr.David B.Weeks of Shell Oil Products US (SOPUS)at(845)462-5225 or the undersigned. Sincerely, Geologic Services Corporation Rol J__,' jM Michael C.Bricher Scott K.Parker,L.S.P. Project Manager Senior Project Manager cc: Mr.David B. Weeks, SOPUS,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590 r..John Kliinm,Hyannis Town Administrator,367 Mdin Street,-Hyannis,MA 02601 Mr.Thomas McKean;Hyannis Board of Health,200 Main Street,Hyannis,MA 02601` Enclosures: Attachment A: Figures Figure 1 —Locus Plan Figure 2—Property Decommissioning Plan Figure 3—Vicinity Plan Ref.#000509C Rpt RAM Plan 03-04 Providing Environmental Management Solutions to Business and Industry Since 1982 A 100% Employee-Owned ESOP Company 15 Bonazzoli Avenue• Hudson, MA 01749 • Tel: 978.568.8740 1 800.522.8740 • Fax: 978.568.9316 www.gsc-global.com Massachusetts Department of Environmental Protection BWSC106 Bureau of Waste Site Cleanup w Release Tracking Number RELEASE ABATEMENT MEASURE (RAM) TRANSMITTAL FORM ® - 11301 Pursuant to 310 CMR 40.0444-0446(Subpart D) A. SITE LOCATION: 1. Site Name/Location Aid: Texaco Service Station #100083 2. Street Address: 1140 I annou h Road 3. City/Town: Hyannis 4. ZIP Code: 02601 5. Check here if a Tier Classification Submittal has been provided to DEP for this disposal site. a. Tier 1 A b. Tier 1 B 0 c. Tier 1 C ❑ d. Tier 2 6. If a Tier U Permit has been issued,provide Permit Number: 100556 B.THIS FORM IS BEING USED TO: (check all that apply) 1. List Submittal Date of Initial RAM Written Plan(if previously submitted): (MMIDD/YYYY) 1/ 2. Submit an-Initial Release Abatement Measure(RAM)Plan. ❑ a. Check here if this RAM Plan received previous oral approval from DEP as a continuation of a Limited Removal Action(LRA). b. List Date of Oral Approval: Q 3. Submit a Modified RAM Plan of a previously submitted written RAM Plan. 4. Submit a RAM Status Report. t 5. Submit a RAM Completion Statement. �. 6. Submit a Revised RAM Completion Statement. 7. Provide Additional RTNs: a. Check here if this RAM Submittal covers additional Release Tracking Numbers (RTNs). RTNs that have been ❑ previously linked to a Primary Tier Classified RTN do not need to be listed here. This section is intended to allow a RAM to cover more than one unclassified RTN and not show permanent linkage to a Primary Tier Classified RTN. b. Provide the additional Release Tracking Number(s) covered by this RAM Submittal. (All sections of this transmittal form must be filled out unless otherwise noted above) Revised: 11/22/2002 Page 1 of 6 BWSC1061102001 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 Release Tracking Number ' . RELEASE ABATEMENT MEASURE (RAM) j. TRANSMITTAL FORM ® - s11301 £ Pursuant to 310 CMR 40.0444-0446(Subpart D) C. RELEASE OR THREAT OF RELEASE CONDITIONS THAT WARRANT RAM: 1. Identify Media Impacted and Receptors Affected: (check all that apply) a. Air b. Basement c. Critical Exposure Pathway ' P y ✓< d. Groundwater e. Residence f. Paved Surface g.Private Well h. Public Water Supply i. School j. Sediments 's✓ k. Soil F I. Storm Drain m. Surface Water i n. Unknown o. Wetland p. Zone 2 q. Others Specify: 2. Identify all sources of the Release or Threat of Release,if known: (check all that apply) a. Above-ground Storage Tank(AST) b. Boat/Vessel € c. Drums d.Fuel Tank e. Pipe/Hose/Line f. Tanker Truck g. Transformer ✓ h. Under-ground Storage Tank(UST) i. Vehicle j. Others Specify: 3. Identify Oils and Hazardous Materials Released: (check all that apply) ✓ a. Oils ....,< b. Chlorinated Solvents c. Heavy Metals d. Others Specify: D. DESCRIPTION OF RESPONSE ACTIONS: (check all that apply,for volumes list cumulative amounts) 1. Assessment and/or Monitoring Only 2. Temporary Covers or Caps 3. Deployment of Absorbent or Containment Materials 4. Temporary Water Supplies 5. Structure Venting System . 6. Temporary Evacuation or Relocation of Residents y7. Product or NAPL Recovery 8. Fencing and Sign Posting s € 9. Groundwater Treatment Systems 10. Soil Vapor Extraction 11. Bioremediation 12. Air Sparging ✓ 13. Excavation of Contaminated Soils Q a. Re-use, Recycling or Treatment i.On Site Estimated volume in cubic yards Q ii.Off Site Estimated volume in cubic yards <1500 iia. Receiving Facility: TBD Town: State: iib. Receiving Facility: Town: State: iii. Describe: Total soil excavated not to exceed 1500 cubic yards Revised: 11122/2002 Page 2 of 6 BWSC1061102002 ■ 0 :Massachusetts Department of Environmental Protection :Bureau of Waste Site Cleanup BWSC106 Release Tracking Number RELEASE ABATEMENT MEASURE (RAM) 4 - 11301 TRANSMITTAL FORM ❑ :...........................; Pursuant to 310 CMR 40.0444-0446(Subpart D) D. DESCRIPTION OF RESPONSE ACTIONS(cont.): (check all that apply,for volumes list cumulative amounts) ❑ b. Store ❑ i.On Site Estimated volume in cubic yards ❑ ii.Off Site Estimated volume in cubic yards iia.Receiving Facility: Town: State: iib.Receiving Facility: Town: State: ❑ c. Landfill ❑ i.Cover Estimated volume in cubic yards Receiving Facility: Town: State: ❑ ii. Disposal Estimated volume in cubic yards Receiving Facility: Town: State: s 14. Removal of Drums,Tanks or Containers: a. Describe Quantity and Amount: b. Receiving Facility: Town: State: c. Receiving Facility: Town: State: ❑ 15. Removal of Other Contaminated Media: a.Specify Type and Volume: b.Receiving Facility: Town: State: c.Receiving Facility: Town: State: 16. Other Response Actions: Describe: 17. Use of Innovative Technologies: Describe: Revised: 11/22/2002 Page 3 of 6 BWSC1061102003 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 Release Tracking Number RELEASE ABATEMENT MEASURE (RAM) ® _ 11301 I L TRANSMITTAL FORM Pursuant to 310 CMR 40.0444-0446(Subpart D) E. LSP SIGNATURE AND STAMP: I attest under the pains and penalties of perjury that I have personally examined and am familiar with this transmittal form, including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of(i)the standard of care in 309 CMR 4.02(1), (ii)the applicable provisions of 309 CMR 4.02(2)and(3),and 309 CMR 4.03(2),and (iii)the provisions of 309 CMR 4.03(3),to the best of my knowledge,information and belief, > if Section B of this form indicates that a Release Abatement Measure Plan is being submitted,the response action(s)that is (are)the subject of this submittal(i)has(have)been developed in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000, (ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21E and 310 CMR 40.0000 and(iii)comply(ies)with the identified provisions of all orders, permits, and approvals identified in this submittal; > if Section 8 of this form indicates that a Release Abatement Measure Status Report is being submitted,the response action(s)that is(are)the subject of this submittal(i)is(are)being implemented in accordance with the applicable provisions of M.G.L.c. 21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L. c.21 E and 310 CMR 40.0000 and(iii)comply(ies)with the identified provisions of all orders, permits,and approvals identified in this submittal; > if Section B of this form indicates that a Release Abatement Measure Completion Statement is being submitted,the response action(s)that is(are)the subject of this submittal(i)has(have)been developed and implemented in accordance with the applicable provisions of M.G.L.c. 21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth it the applicable provisions of M.G.L.c. 21 E and 310 CMR 40.0000 and(iii)comply(ies) with the identified provisions of all orders, permits,and approvals identified in this submittal: I am aware that significant penalties may result,including, but not limited to, possible fines and imprisonment, if I submit information which I know to be false,inaccurate or materially incomplete. 1. LSP#: 9969 2. First Name: Scott K. 3. Last Name: Parker 4. Telephone: (978) 568-8740 5. Ext.: 239 6. FAX: (978) 568-9316 7. Signature 8. Date: 3��0�Vy 9. LSP Stamp: o���P�tN OF MASs9cyG scow o K. P R co B r�nF 9G O�� �sFo ROF�SS� � Revised: 11/22/2002 Page 4 of 6 BWSC1061102004 ■ F Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 .; Release Tracking Number RELEASE ABATEMENT MEASURE (RAM) TRANSMITTAL FORM ® 11301 Pursuant to 310 CMR 40.0444-0446(Subpart D) F. PERSON UNDERTAKING RAM: 1. Check all that apply: a.change in contact name ... b.change of address c. change in the person undertaking response actions 2. Name of Organization: Motiva Enterprises LLC 3. Contact First Name: David B. 4.Last Name: Weeks 5. Street: PMB 301, 1830 South Rd., Unit 24 6.Title: Sr. Environmental Engineer 7. City/Town: Wappingers Falls 8. State: NY 9. ZIP Code: 1250 10. Telephone: (845) 462-5225 11.Ext.: 12. FAX: 845 462-4999 G. RELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON UNDERTAKING RAM: 1. RP or PRP a. Owner b. Operator ❑ c. Generator d. Transporter e. Other RP or PRP Specify: 2. Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.C.21 E,s.2) 3. Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.5(j)) 4. Any Other Person Undertaking RAM Specify Relationship: H.REQUIRED ATTACHMENT AND SUBMITTALS: 1.Check here if any Remediation Waste,generated as a result of this RAM,will be stored,treated,managed,recycled or reused at the site following submission of the RAM Completion Statement. You must submit a Phase IV Remedy Implementation Plan along with the appropriate transmittal form(BWSC108). 2. Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order(s),permit(s) and/or approval(s)issued by DEP or EPA. If the box is checked,you MUST attach a statement identifying the applicable provisiions thereof. 3. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the implementation of a Release Abatement Measure. s 4. Check here if any non-updatable information provided on this form is incorrect,e.g. Release Address/Location Aid. Send corrections to the DEP Regional Office. 5. If a RAM Compliance Fee is required for this RAM,check here to certify that a RAM Compliance Fee was submitted to ` DEP,P.O. Box 4062,Boston, MA 02211. 6. Check here to certify that the LSP Opinion containing the material facts,data,and other information is attached. Revised: 11/22/2002 Page 5 of 6 BWSC1061102005 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number TRANSMITTAL FORM ® - 11301 »>> Pursuant to 310 CMR 40.0444-0446(Subpart D) I. CERTIFICATION OF PERSON UNDERTAKING RAM: 1. I, David B. Weeks attest under the pains and penalties of perjury(i)that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true,accurate and complete,and(iii) that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. I/the person or entity on whose behalf this submittal is made am/is aware that there are significant penalties,including, but not limited to, possible fine impnso nt for . Ifull submitting false,inaccurate,or incomplete information. 2. By: ,;���e 7 3. Title: Sr. Environmental Engineer Signature 4. For: Motiva Enterprises LLC (Name of person or entity recorded in Section F) (mm/dd/yyy ?� 5. Check here if the address of the person providing certification is different from address recorded in Section F. 6. Street: 7. City/Town: 8. State: 9. ZIP Code: 10. Telephone: 11.Ext.: 12. FAX: YOU MUST LEGIBLY COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Date Stamp(DEP USE ONLY:) Revised: 11/22/2002 Page 6 of 6 BWSC1061102006 0 0 Geologic Services Corporation science,engineering&technology RELEASE ABATEMENT MEASURE PLAN TEXACO SERVICE STATION#100083 1140 IYANNOUGH ROAD HYANNIS,MASSACHUSETTS DEP RTN 4-11301 TIER IC PERMIT#100556 ACO-SE-03-3S-002 March 2004 Prepared by: Prepared for: Geologic Services Corporation Motiva Enterprises LLC 15 Bonazzoli Avenue PMB 301,1830 South Road,Unit 24 Hudson, Massachusetts 01749 Wappingers Falls,NY 12590 (978) 568-8740 (845)462-5225 REF. #000509C Providing Environmental Management Solutions to Business and Industry Since 1982 A 100% Employee-Owned ESOP Company 15 Bonazzoli Avenue• :Hudson, MA 01749 • Tel: 978.568.8740 1 800.522.8740 • Fax: 978.568.9316 www.gsc-global.com Texaco Service Station#100083 Geologic Services Corporation Page 1 Release Abatement Measure Objective On behalf of Motiva Enterprises LLC(Motiva),Geologic Services Corporation(GSC)has prepared a Release Abatement Measure(RAM)Plan for the Texaco-branded Service Station#100083 located at 1140 Iyannough Road in Hyannis,Massachusetts. The objectives of the herein-proposed RAM are to excavate, appropriately manage, and to the degree required,transport and dispose of petroleum-impacted soil and groundwater(if encountered)during the removal of the gasoline and diesel underground storage tanks (USTs),dispensers,piping, fuel oil UST,waste oil UST(if present),hydraulic lift,dry well(if present),and the advancement of test pits in the vicinity of an on-site catch basin. Please refer to Figures 1, 2, and 3 (Attachment A) for illustrations of the subject site and surrounding area. Motiva is conducting the RAM activities referenced herein. The contact at Motiva responsible for overseeing the response actions associated with this site is Mr.David B.Weeks,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590; (845)462-5225. Background The subject property was listed by the Massachusetts Department of Environmental Protection(MA DEP) based on information reported in a December 28, 1994 21 E Site Assessment Report,prepared by Down Cape Engineering,Inc. (DCE)for Cooke's Restaurant located adjacent to the site at 1120 Iyannough Road, Hyannis,Massachusetts. As part of this site assessment,DCE collected groundwater samples from three monitoring wells located on the Cooke's Restaurant property. Laboratory analysis indicated the presence of benzene,toluene, and xylenes in the sample obtained from a well reported to be downgradient of the Texaco Station. The MA DEP issued release tracking number(RTN)4-11301 on April 6, 1995 in response to these findings. As a result of the 21 E Site Assessment of Cooke's Restaurant,the MA DEP issued a Notice of Responsibility(NOR)to Star Enterprises(Star)owner of the property located at 1140 Iyannough Road in Hyannis,Massachusetts on August 11, 1995. On October 12, 1995, Star, submitted a Phase I-Initial Site Investigation Report and Tier IC Application to MA DEP for the subject site. During the Phase I investigation,groundwater sampling results of the on-site monitoring wells revealed dissolved-phase petroleum constituents in excess of the MA DEP reportable concentrations for GW-1 groundwater standards. The MA DEP approved the Tier IC Permit Application(No. 100556)for the subject property on September 12, 1996. At this time it was determined that a Substantial Release Migration(SRM)condition may exist and the MA DEP required an Immediate Response Action(IRA)Plan to be submitted. Star submitted an assessment-only IRA Plan proposing tri-annual groundwater monitoring for a one-year period to evaluate seasonal changes in groundwater elevation and quality. A Phase R Scope of Work(SOW)was submitted by Groundwater&Environmental Services,Inc. (GES) on July 25, 1997 for additional subsurface investigations to be completed. This work included the installation of additional monitoring wells and additional groundwater sampling. On September 18, 1998, SAGE submitted an IRA Status report summarizing the installation of three monitoring wells and the advancement of five soil borings. Groundwater samples were collected from ten on-site monitoring wells on May 6, 1998 and analyzed for extractable petroleum hydrocarbons(EPH)and volatile petroleum hydrocarbons(VPH). Soil analytical results for this sampling event indicated concentrations of methyl-tertiary butyl ether (MTBE) above the applicable Method 1 S-1/GW-1 soil standard at soil sample locations MW-9 and S13-11. Dissolved phase petroleum constituents were detected above applicable Method 1 GW-1 standards in samples collected from all site related monitoring wells except MW-3. Ref.#000509C_Rpt_RAM Plan 03-04 Texaco Service Station#100083 Geologic Services Corporation Page 2 SAGE submitted a Modification to the Phase II SOW report on August 13, 1998 for the installation of off- site monitoring wells,well surveying,groundwater sampling,and a soil vapor extraction(SVE)pilot test. SAGE was unable to secure off-site access for the installation of downgradient monitoring wells. However, the SVE pilot test and oundwater sampling were completed on M p �' p g p arch 25, 1999 and June 4, 1999, respectively. SAGE indicated that the results of the SVE test were skewed due to recent construction activities that may have caused short-circuiting in the airflow diminishing the effective radius of influence. On March 4, 1999, SAGE submitted a Modification to the IRA Plan report in response to extensive excavation activities proposed at the site. The modification addressed excess soil to be generated during the installation of new pump islands and canopy foundations,and the removal and replacement of two leaching catch basins. It included a work scope for the soil testing of excavated soils, confirmatory sampling, and management of excavated soils. Approximately 556.75 tons of soil was removed from the site on March 4 and 5, 1999 for reuse at a landfill. Approximately 188.47 tons of petroleum-impacted soil was transported to an off-site disposal facility for recycling on March 24, 1999. In 1999, responsibility for the release was transferred to Motiva,which was created in the formation of a joint venture between Shell and the owners of Star. On August 22,2000, SAGE submitted a Phase II and Phase III Report. Groundwater extraction combined with soil vapor extraction technologies were selected as the remedial action alternative for achieving a permanent solution at the subject property. Following review of the Phase R and III Reports,additional delineation of the dissolved phase petroleum hydrocarbons related to the subject property was viewed to be warranted prior to the selection/implementation of a remedial action. In conjunction with the installation of the groundwater monitoring wells,pilot test air sparge(AS)and SVE wells were installed at the subject property. In March of 2001,GSC and Motiva were able to secure off-site access to abutting properties. Between March 19 and 23,2001,GSC personnel supervised the installation of four 2-inch diameter groundwater monitoring wells MW-11,MW-12,MW-13,and MW-14 at and in the vicinity of the subject property in order to further delineate petroleum impact to soil and groundwater. During groundwater monitoring well gauging and sampling activities performed on April 4,2001, approximately 0.60 feet of non-aqueous phase liquid(NAPL)(i.e.; weathered gasoline)was detected in monitoring well MW-9. The MA DEP was verbally notified of the presence of greater than 0.5 inches of NAPL on April 5,2001. The MA DEP subsequently assigned RTN 4-16161 to this 72-hour release condition and verbally approved passive NAPL bailing activities under an IRA. On April 12,2001,Tanknology-NDE of Springfield,Massachusetts performed a pressure tank tightness test for the gasoline UST system at the subject property. All the pressure tests performed on the UST system passed on this date. On June 8,2001,Motiva submitted a Tier IC Permit Renewal Application to the MA DEP in order to allow for the continuation of response actions under RTN 4-11301. In addition,the Tier 1 C Permit application detailed the linking of RTN 4-16161 to lead RTN 4-11301. On September 27,2001, a Decision to Grant a Tier IC Permit Extension was approved by the MA DEP. On July 16, 2002,the MA DEP issued a Notice of Noncompliance(NON)(NON-SE-02-35-014)to Motiva for failure to submit an administratively complete Phase II Report and Phase III Plan. Ref.#000509C_Rpt_RAM Plan 03-04 -Texaco Service Station#100083 Geologic Services Corporation Page 3 IRA Status Reports were submitted to the MA DEP in March and August 2002 detailing NAPE,recovery and assessment activities during the period of August 2001 through July 2002. An IRA Plan Design Specification was also submitted to the MA DEP in August 2002 summarizing a SVE/AS pilot test and detailing a remedial design plan to treat the source area. An IRA Status Report was submitted to the MA DEP on February 21,2003 documenting the installation of the SVE/AS remedial system,NAPE,recovery, and continued site assessment activities. The SVE and AS systems were activated on March 14,2003 and April 4,2003,respectively. The SVE/AS system is currently operational. Operation and maintenance of the SVE/AS system is documented in the semi-annual IRA Status Report dated August 22,2003 and IRA Completion Report dated February 19,2004. Motiva entered into an Administrative Consent Order(ACO) (ACO-SE-03-35-002)with the MA DEP on February 19, 2003. As part of the ACO agreement between Motiva and the MA DEP,the following regulatory deadlines were established for the subject property:Phase II-Comprehensive Site Assessment and Phase III-Remedial Action Plan-April 15,2003; Phase IV Remedy Implementation Plan- September 30, 2003; and Phase V-Remedy Operation Status-June 30,2004. A Supplemental Phase II Comprehensive Site Assessment Report(Supplemental Phase 11)and Phase III- Remedial Action Plan(RAP)Addendum were submitted for the subject property on April 14, 2003. The Supplemental Phase II and Phase III-RAP Addendum documented the installation of fifty monitoring wells, eleven soil vapor extraction wells,eight air sparge wells,three monitoring point triplets,three cone penetrometer testpoint(CPT)borings,and twenty-six temporary well points during the period of October 2000 through March 2003. In addition,twenty-seven groundwater gauging events and thirteen groundwater sampling events were conducted during this time period. The selected remedial action alternative for the reduction of residual petroleum constituents on the property is the installation and operation of a Groundwater Extraction and Treatment system downgradient of the subject property coupled with the existing SVE/AS system in the tankfield area. The selected remedial action alternative outside of the target areas of active remediation is monitored natural attenuation(MNA) for management of migration and eventual reduction of dissolved-phase impacts. A Tier IC Permit Extension was submitted to the MA DEP on June 10,2003 in order to allow for the continuation of response actions under RTN 4-11301. In accordance with the revisions to the MCP 310 CMR 40.0720,the Tier 1C Permit Extension was presumed approved on August 11,2003. The expiration date of the Tier IC Permit is September 12,2005. Based on difficulties securing access to evaluate an off-site remediation system,Motiva requested an extension for the submittal of the Phase IV-Remedy Implementation Plan(RIP). The ACO Amendment #1 dated September 18,2003 extended the Phase IV-RIP to January 31, 2004. The effective date for ACO Amendment#1 is October 1,2003. The Phase IV-RIP,dated January 29, 2004, detailed the proposed implementation for the off-site Groundwater Extraction and Treatment system, ongoing operation and maintenance of the on-site SVE/AS system, and continuation of MNA. In addition,the Phase IV-RIP documented the installation of one recovery well,two monitoring points,recovery well development,overburden aquifer pumping and re- injection tests, and sampling of recovery well RW-1. An IRA Completion Report was submitted to the MA DEP on February 19,2004. I Ref. #000509C_Rpt_RAM Plan 03-04 Texaco Service Station#100083 Geologic Services Corporation Page 4 Description of Site Conditions/Surrounding Receptors,pursuant to 310 CMR 40.0427(4)(a) The subject property is situated at 1140 Iyannough Road in Hyannis,Massachusetts and is currently an active Texaco branded retail gasoline and automobile repair facility. The subject property has an area of approximately 47,916.19 square feet(I.l acres). The majority of the site is paved with asphalt or reinforced concrete, except a small area in the southern portion of the lot,which is landscaped. The northern portion of the property is wooded and covered in gravel. The single-story Texaco station houses an office area, restrooms,and three repair service bays. One 12,000 gallon gasoline UST,two 10,000 gallon gasoline USTs, one 8,000 gallon diesel fuel UST, and one 550 gallon fuel oil UST currently exist at the site. The site is serviced by municipal water supply and sewer as well as underground telephone and electric service utilities. The subject site drainage system is connected to an on-site leachfield located immediately east of the service station building. Two detention drainage basins are located approximately 80 feet southeast and 90 feet north of the convenience store, respectively. Please refer to Figures 1, 2, and 3 for a depiction of the subject property and surrounding area. The surrounding area is zoned for commercial use. Cooke's Seafood Restaurant is located immediately east of the subject property. Parker's Liquor Store is located immediately west of the subject property. A commercial plaza(Festival at Hyannis)is located immediately north of the subject property. A Ramada Inn is located approximately 100 feet south of the subject property across lyannough Road. A Cumberland Farms Gulf Station is located approximately 210 feet southwest of the subject property. Subsurface structures within 1,000 feet of the site include half and full basements and utility conduits located along Iyannough Road,Bearses Way and Independence Drive. The closest known basement is located approximately 600 feet southwest(upgradient)of the subject property. Subsurface utility conduits located along these streets include,but are not limited to,municipal water, sewer,gas, and storm drainage. Overhead electric and telephone utilities also exist along these streets and subject site. According to the USGS Hyannis,Massachusetts Topographic Map and GSC site reconnaissance there are no schools, institutions,or environmentally sensitive receptors known to exist within 1,500 feet of the subject property. According to the USGS Hyannis,Massachusetts Topographic Map(refer to Figure 1),the closest surface water bodies include an unnamed brook located approximately 1,800 feet east,Hathaway Pond located approximately 2,600 feet northwest, and Shallow Pond located approximately 3,100 feet west of the subject property. Multiple kettle ponds are located approximately 2,000 feet east of the subject property along Independence Drive. Additional ponds are located further northeast and southeast of the property. According to the flood insurance rate map produced by the Federal Emergency Management Agency,the subject property is located within an area designated as Zone C(an area of minimal flooding). According to the Massachusetts Geographic Information System(GIS),the subject property is located within a MA DEP-Approved Zone Il and an EPA-designated sole source aquifer. Six municipal public groundwater supply wells are known to exist within a 1.5-mile radius of the subject property. The closest public supply well(Barnstable Fire District Well#2)is located approximately 4,000 feet northwest of the subject property. According to the Barnstable Water Company and the Barnstable Water Department,no private supply wells exist within 1,000 feet of the disposal site. The subject property and surrounding area are serviced by municipal water. Ref.#000509C_Rpt_RAM Plan 03-04 -Texaco Service Station#100083 Geologic Services Corporation Page 5 Scope of Work The scope of work as it pertains to this RAM includes the management of Remediation Waste associated with the following activities: ■ Selective excavation and off-site disposal of soil during the removal of two 10,000-gallon gasoline USTs, one 12,000-gallon UST, one 10,000 gallon diesel UST, associated product piping, and dispenser equipment; ■ Selective excavation and off-site disposal of soil during the removal of one 550-gallon fuel oil UST; ■ Selective excavation and off-site disposal of soil during the removal of one 550-gallon used oil UST (if present); ■ Selective excavation and off--site disposal of soil during the removal of one hydraulic lift; and ■ Selective excavation and off-site disposal of soil during the removal of dry wells (if present)and installation of test pits in the vicinity of the catch basin located on the northwestern portion of the property. Refer to Figure 2—Site Plan for the locations of the USTs and other site features. In so far as possible, excavated soil will be re-used on-site. Clean fill will be brought in from off-site as needed. Based on historical depth to groundwater, dewatering will not be required during the site construction activities. Environmental Monitoring and Soil Segregation During the equipment removal activities,on-site inspections and field screening of excavated soil will be completed. Field screening of soil sample headspace will be performed using a photo ionization detector (PID)equipped with a 10.6 electron volt(eV)lamp calibrated with an isobutylene span gas to yield total volatile organic compounds (VOCs)in parts per million volume(ppmv)referenced as benzene. No more than 1,500 cubic yards of Remediation Waste will be generated during the RAM activities described herein. Excavated soil will be segregated into three separate soil types based on PID response to soil vapor headspace and visual and olfactory indications of petroleum-impact as follows: • Type A soils will include soils that are observed to have visual evidence of petroleum impact, and with soil headspace PID responses greater than 10 ppm. • Type B soils will include soils that are observed to have no visually apparent evidence of petroleum impact, and with soil headspace PID responses less than 10 ppm. • Type C material will consist of asphalt; concrete and other construction debris removed form the excavation. Any concrete and any suitable construction debris encountered will either be returned to the excavation upon completion or disposed of as construction debris. Following the completion of the soil excavation,composite soil samples will be collected from soil stockpile A and submitted to Accutest Laboratories,Inc. (Accutest)of Marlborough,Massachusetts for analysis of disposal parameters including flashpoint via 1010,pH,reactivity(sulfide and cyanide),VOCs via 8260,total petroleum hydrocarbons(TPH)-gasoline range only(GRO)and diesel range only(DRO), RCRA 8 metals, and Polychlorinated Biphenyls(PCBs)via EPA Method 8080. Ref. #000509C_Rpt_RAM Plan 03-04 Texaco Service Station#100083 Geologic Services Corporation Page � g 6 The results of the Type B stockpile analysis will be compared to the Massachusetts Contingency Plan (MCP)Method 1 Risk Characterization S-1 soil standards. If the concentrations of chemicals of concern (COC)are greater than the Method 1 Risk Characterization soil standards,then the soil will be considered Remediation Waste and transported from the site along with Type A soil under a Massachusetts Bill of Lading for recycling. If the COC concentrations are below the MCP Method 1 Risk Characterization soil standards,than the soil will be considered reusable and may be backfilled in an excavation. Soil Stockpiling Protocol Soil excavated during the RAM activities will be stockpiled on 6 mil thick polyethylene sheeting. The soil pile will be covered with 6 mil polyethylene sheeting and secured at the end of each working day until the soil is either backfilled or removed from the site. Post Excavation Sampling During the gasoline UST, gasoline dispensers, and gasoline product pipe excavations,representative soil samples will be collected from in-situ soil at the side wall(s)and bottom of the excavation for laboratory analysis. Soil samples will be collected and submitted to a laboratory for analysis of VPH via MA DEP- approved methodology,ethylene dibromide(EDB), and lead. Soil samples will be collected at 10 to 15 foot intervals along the product piping. During the diesel UST, diesel dispenser,diesel product pipe,hydraulic lift, and fuel oil UST excavations, representative soil samples will be collected from in-situ soil at the side wall(s)and bottom of the excavations for laboratory analysis. Soil samples will be collected and submitted to a laboratory for analysis of EPH via MA DEP-approved methodology. Soil samples will be collected at 10 to 15 foot intervals along the product piping. During the excavation of the used oil UST(if present)and dry wells(if present),representative soil samples will be collected from in-situ soil at the side wall(s)and bottom of the excavations for laboratory analysis. Soil samples will be collected and submitted to a laboratory for analysis of EPH, VPH,PCBs,total metals via EPA Methods 6010B and 7471A, and VOCs via EPA Method 8260. During the installation of the catch basin test pits,representative soil samples exhibiting the highest PID readings may be collected for laboratory analysis of EPH,VPH,PCBs,total metals via EPA Methods 6010B and 7471 A, and VOCs via EPA Method 8260. Management of Remediation Waste Soil deterrruned to be Remediation Waste as described herein will be transported to a licensed recycling facility for asphalt batching using a MA DEP Bill of Lading in accordance with the provisions of 310 CMR 40.0030. Schedule for RAM Implementation Motiva will obtain the necessary permits from the Barnstable Fire Department prior to removing the USTs. At this time,no additional federal, state, or local permits are required to perform these RAM activities. The RAM activities proposed herein are currently scheduled to commence during the week'of April 1, 2004. RAM activities are anticipated to proceed for approximately two weeks. Actual time may vary in response to conditions encountered during excavation activities. Should the scope of this RAM Plan change significantly prior to or during its implementation, a RAM Addendum specifically outlining Ref. #000509C_Rpt_RAM Plan 03-04 Texaco Service Station#100083 Geologic Services Corporation Page 7 pertinent modifications to the workscope will be prepared for submittal to the MA DEP. PID readings in excess of 100 ppmv in soil samples collected from within the UST excavation may be encountered and will be related to the existing RTN 4-11301; thus,no new notification condition will be made to MA DEP as this RAM Plan will serve as appropriate documentation to manage the impacted soil. RAM Limitations Pursuant to 310 CMR 40.0442(4), a maximum of 1,500 cubic yards of soil may be excavated during the course of this RAM, and classified as Remediation Waste. Please note that excavation on the western edge of the UST area and diesel dispenser may be limited due to the proximity to the property line. If site conditions become significantly different from those previously documented on the site, an Imminent Hazard is identified to exist,or if conditions requiring a 2 or 72 hour notification of a release to the MA DEP pursuant to 310 CMR 40.0300 are encountered, all work being performed in conjunction with the RAM will be terminated. The responsible party(RP)for the RAM will make the appropriate notification to MA DEP. Activities will resume only after such notification has been made and MA DEP approves the continuation of the project. Health& Safety On-site health and safety practices in accordance with standards set forth by the Occupational Safety and Health Administration(29 CFR 1910.120)will be observed by all site personnel associated with the RAM for the duration of field activities. A site specific Health and Safety Plan has been prepared for these activities. Public Involvement By copy of this document, the Chief Municipal Officer and the Board of Health for the Town of Barnstable have been provided notice of the RAM in accordance with 310 CMR 1403(3)(d). Project Completion Pursuant to the provisions set forth in 310 CMR 40.0440, RAM Status and/or Completion Reports will be periodically submitted to the MA DEP detailing the activities completed under the RAM and any change in site conditions subsequent to the implementation of the RAM. Schedule • Construction anticipated to start in early April 2004 • RAM Completion(or Status)Report— 120 days following submittal of this Plan I Ref. #000509C_Rpt_RAM Plan 03-04 ATTACHMENT A Figures Fw J 1 s f ,t t� Alt t,�M�'r(`� / l ',I��,�l � � — � Q�''�� r� _ ry ..i�TYF="•?��1p `'�'.,�'�'.`'+Str =� I e tip —IiiV 1000 0 1000 2000 3000 4000 Feet w�'�,''� �;t'� ��� '�j` •, ` ... 1`` .ems l�//��,�►�'�° --�raw cCe��.�l-ar,��•,1�.,.,�. fir/ „�� �\, ��"��•/�, � !f ;_ r' -\,_ `�� '' L � © I,.-/ 'r'�+�� •+� Ott� V����!-~ I .� F r / `� 1 1 f �� ,!� �rt'�V� \33'yl (� ,•... � /L�� ���\�f�1f���l iAYl.�i��Ld�'�.��ti�f�r�i,�.J IiZ 1111 1111111111/1111111111 j1 111111111111111111111 1111111111111111111111 111.111111111111111111 tc;to t QUADRANGLE • ZONE 1 0• • t 1 , Notes: 1. Topographic measured 1 11•Topographic2. • • 1 meters. TEXACO SERVICE STATION , 1 IYANNOUGH ROAD Source:Hydrogeologists and Environmental Scientists Date: 1/27/03 I I I J .I i • .1s-Barnstable Quadrangle i I TMP-120 MW-3A N % SYSTEM MW-A ENCLOSURE � KEY BUILDING M 1 SB-7 . SOIL BORING SVE-9 MW-11 A DESTROYED MONITORING WELL AS-5 ` MW-14D SVE-3 `` HYDRAULIC LIFT MW-141 CB-2 MW-7 MW-18S MW-14 ® _ MW-14S I B-1 1 OAS * TMP-103 , W'18D GROUNDWATER MONITORING WELL MW-5 0AS-6 0SVE-8 M#8 / O AIRSPARGE WELL SVE-2 10 VE-10 MW-6 RECOVERY WELL AS—* UST + SB-8 / CPT— AREA AS-2 SB-10 . ® SOIL VAPOR EXTRACTION WELL MW-9 OL.,, 0 ®SV —6 � MW-4 / $ TEMPORARY MONITORING WELL \ SVE-1 AS-8 MP-101 DIESEL � UFO OIL RW 1 I ® CATCH BASIN/POTENTIAL DRYWELL DISPENSER MP-2 J QpAS-1 SERVICE , —-— PROPERTY BOUNDARY ISLAND MP/3, *AS1 7®V STATION MP 102 / UST UNDERGROUND STORAGE TANK # w-1 U/0 USED OIL COOKE'S MWC`P_T�2 ,®CB-1 ® MW-3 / RESTAURANT F/O FUEL OIL T P�101 SVE-4 F/0 UST M —1 1 / NOTE: LOCATION OF SYSTEM ENCLOSURE •®SVE-5 IS APPROXIMATE SB— `� GASOLINE / DISPENSER � MW-12 ISLANDS / 4�V CB 3® MW-2 0 50 G Scale in feet FIGURE 2 Q PROPERTY DECOMMISSIONING PLAN `9 TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS FRAFTED 509.01 DECON CHECKED BY: AC DATE: 8 12 02 NG DAE: 3 12 04 GEOLOGIC SERVICES CORPORATIONFIELD RECONNAISSANCE Hydrogeologists and Environmental Scientists 15 Bonaaoli Avenue • Hudson,MA 01749 •(978)568-8740 { COMMERCIAL PIER 1 GRAVEL PAYLESS O , PITS W � BLOCKBUSTER Q � JENNY ATTRESS CRAIG GIANT FR � IENOIY,S ~� OLIVE GAR CppKE,S DEN Q SEA Fpp' x OYSRUS DISCpUNT THE RAMgpq MAR/NE SITE / REq EST ATE 0 350 CRACKER GVCF BgRRE� PARKER'S TAT/pN Scale .in feet OVTC I ET DISCOUNT KEY LIQUOR FIGURE 3 VICINITY PLAN TEXACO SERVICE STATION #100083 — - — PROPERTY BOUNDARY 1 140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.01 VICINB CHECKED BY: IVY, DRAFTED BY: CD DATE: 2 11 02 REVISED BY: ANG DATE: 3 27 02 SOURCE: SAGE ENVIRONMENTAL PLAN AND GSC FIELD GEOLOGIC SERVICES CORPORATION RECONNAISSANCE Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue • Hudson, MA 01749 •(978)568-8740 LVI Environmental Services Inc. _ 401-S Second Street .;. RECEIVE� Everett,MA 02149 SERV�CES Tel: (617)389-8880 fo 8 2004 Fax: (617)389-9502 q5 www.lviservices.com TOWN(UF BARiNSTl BLE 'HEAL'TH:.D.EPT' NOTIFICATION OF ASBESTOS ABATEMENT ATTENTION: Hyannis Health Department PO Box 534 Hyannis, MA 02601 LVI Environmental Services Inc. will be conducting an asbestos abatement project at the following location. Please note the site and dates listed below. Do not hesitate to contact us at(617)389-8880 with any questions on schedule adjustments,as the start and end dates are subject to changes. BUILDING LOCATION: Cape Cod Hospital Whitcomb Pavillion 27 Park Street Hyannis, MA START DATE: 3/22/04 END DATE: 3/23/04 Asbestos signs will be clearly posted in all areas where work is being conducted. Please take the necessary precautions in the event you are required to enter the building.during an emergency. If you have further questions with respect to this project,please do not hesitate to contact our office at any time at(617) 389-8880. Thank you very much for your attention regarding this matter. J Very truly yours, LVI Environmental Services Inc. Sarah Marcone Projects Coordinator I r 4 Commonwealth of Massachusetts ■ 100003027 Asbestos Notification Form ANF-001 ;-___Deyl Number ' Affix Asbestos Notification Decal Here Important: A. Asbestos Abatement Description When filling out forms on the computer,use 1. a. Is this facility fee exempt-city,town, district, municipal housing authority, owner-occupied El only the tab key residence of four units or less? ❑Yes ❑✓ No to move your cursor-do not b. Provide blanket decal number if applicable: Blanket Decal Number use the return key. 2. Facility Location: ®r Cape Cod Hospital 27 Park Street a.Name of Facility b.Street Address Barnstable 1 102601 (508)862-5566 c.City/Town d.State e.Zip Code f.Telephone Number INSTRUCTIONS 3. Worksite Location: 1.All sections of this Whitcomb Pavillion 2nd FI. form must be a.Building Name/Building Location b.Building# c.Wing d.Floor e.Room completed in order to comply with 4. Is the facility occupied? ❑Yes ❑✓ No DEP notification requirements of 310 CMR 7.15 5. Asbestos Contractor: and the Division of Occupational C.LVI ENVIRONMENTAL SERVICES, IN 401-S SECOND STREET Safety(DOS) a.Name • _ b.Address notification EVERETT �� 02149 617-389-8880 requirements of 453 CMR 6.12 c.Cityrrown d.Zip Code e.Telephone Number AC000097 f.DOS License Number g. Contract Type: ❑Written El Verbal Terry Eisen h.Facilitv Contact Person i.Contact Person's Title BROWN BUTLER JR I JAS040959 6' a.Name of On-Site Supervisor/Foreman b.Supervisor/Foreman DOS Certification Number Diversified Environmental AA000107 a.Name of Project Monitor b.Project Monitor DOS Certification Number Yee Consulting Group 1 JAA000145 8' a.Name of Asbestos Analytical Lab b.Asbestos Analytical Lab DOS Certification Number �09 03/22/2004 03123/2004 _ a.Project Start Date mm/dd/ b.End Date mm/dd --0 4pm-12am N/A N c.Work hours Mon-Fri. d.Work hours Sat-Sun. -o 10. a.What type of project is this? 0 ❑Demolition 0 Renovation - ❑Repair ❑Other, please specify: b.Describe 11. a. Check abatement procedures: 0 ❑Glove bag ❑ Encapsulation � 0 ❑Enclosure ❑ Disposal only ••=U. ❑Cleanup ❑Other, specify: ❑✓ Full containment b.Describe Z �Q 12. Is the job being conducted: ❑✓ Indoors? ❑Outdoors? .. ■ an oc-10/02 Asbestos Notification Form•Page 1 of 3■ Commonwealth of Massachusetts ■ 100003027 f Decal Number Asbestos Notification Form ANF-001 A. Asbestos Abatement Description (cont.) 13. Total amount of each type of Asbestos Containing Materials(ACM)to be removed, enclosed, or 1000 —� a.Totalpipes or ducts — enca su ate 0 p p (linear ) 6. 1 otal otner su aces square c.Boiler,breaching,duct,tank d.Insulating cement surface coatings Lin.ft. Sq.ft. Lin.ft. Sq.ft. e.Corrugated or layered paper �—� f.Trowel/Sprayer coatings pipe insulation Lin.ft. Sq.ft. Lin.ft. Sq.ft. g.Spray-on fireproofing Lin Sq� h.Transite board,wall board Lin q� I.Cloths,woven fabrics � j.Other,please specify: � 1000 Lin.ft. S ft. Lin.ft. Sq.ft. k.Thermal,solid core pipe I_J L� 25 fittings insulation Lin.ft. Sq.ft. I.Specify 14. Describe the decontamination system(s)to be used: Three-chambered decon.facility with shower 15. Describe the containerization/disposal methods to comply with 310 CMR 7.15 and 453 CMR 6.14(2)(g): ACM will be wet.ACM will be properly packaged, labeled and transported to Turnkey. 16. For Emergency Asbestos Operations,the DEP and DOS officials who evaluated the emergency: NA a.Name of DEP Official b.Title c.Date mm/dd/ of Authorization d.DEP Waiver# N/A e.Name of DOS Official tDOS OfficialTitle g.Date(mm/dd/yyyy)of Authorization h.DOS Waiver# �0 17. Do prevailing wage rates as per M.G.L. c. 149,§26,27 or 27A—F apply to this project? ❑Yes No B. Facility Description N �o 1. Current or prior use of facility: hospital o 2. Is the facility owner-occupied residential with 4 units or less? ❑Yes 0 No Cape Cod Hosptal 27 Park Street �� 3' a.Facility Owner Name b.Address � 0 Hyannis 102601 508-771-1800 o c.Cityfrown d.Zip Code e.Telephone Number area code and extension �LL Terry Eisen 27 Park Street �—� 4' a.Name of Facility Owner's On-Site Manager b.On-Site Manager Address Z Hyannis —, 02601 508-862-7665 9—Q c.Cityrrown d.Zip Code e.Telephone Number(area code and extension) ■ anf001ap.doc•10/02 Asbestos Notification Form•Pa Commonwealth of Massachusetts 10 0003027 Asbestos Notification Form ANF-001 Decal Number B. Facility Description (cont.) N/A 5' a.Name of General Contractor b.Address F C= c.City/Town d.Zip Code e.Telephone Number area code and extension f.Contractor's Worker's Comp.Insurer ..Policy � hate(mm/dd/yy�, 6. What is the size of this facility? a.Square Feet b.Number of floors C. Asbestos Transportation and Disposal 1. Transporter of asbestos-containing material from site to temporary storage site(if necessary): LVI Environmental Services Inc. 401-S Second Street Note:Transfer a.Name of Transporter b.Address Stations must IlEverett 02149 (617)389-8880 comply with the c.City/rown d.Zip Code e.Telephone Number Solid Waste Division 2. Transporter of asbestos-containing waste material from removal/temporary site to final disposal site: Regulations 310 CMR 19.000 Waste Management NEET 1203 Pickering Street, PO Box 144 a.Name of Transporter b.Address Portland, CT 06480 (800)272-3867 c.City/town d.Zip Code e.Telephone Number 3. N/A a.Refuse Transfer Station and Owner b.Address c.Cit!Town d.Zip Code e.Telephone Number 4. ITURNKEY LANDFILL(WASTE MGT. NH) a.Final Disposal Site Location Name b.Final Disposal Site Location Owner's Name 97 ROCHESTER NECK ROAD I IROCHESTER c.Final Dis osal Site Address d.City/Town NH 03839 1 1(603)332-2386 � e.State f.Zip Code g.Telephone Number Cl) �o D. Certification. 9 �N The undersigned hereby states,under the ISarah Marcone� I �o penalties of perjury,that he/she has read the a.Name b.Authorized Signature E�0 Commonwealth of Massachusetts regulations IlProject Coordinator I for the Removal,Containment or c.Position/Title d.Date mm/ddl Encapsulation of Asbestos,453 CMR 6.00 and (617)389-8880 LVI �� 310 CMR 7.15,and that the information contained in this notification is true and correct e.Tele hone Number f.Representing to the best of his/her knowledge and belief. 401-S Second Street o a.Address Everett,MA -� 02149 -LL h.City/Town I.Zip Code �Q anfo01 ap.doc•10/02 Asbestos Notification Form•Page 3 of 3 l - 5 r /.� (� f ' Geologic Services Waybill#20874530950 Corporation March 16, 2004 science,engineering&technology : Massachusetts Department of Environmental Protection Southeast Regional Office Bureau of Waste Site Cleanup Attn: Ms. Laura Stanley 20 Riverside Drive Lakeville, MA 02347 RECEIVED Re: Release Abatement Measure Plan MAR 1 8 2004 Texaco Service Station#100083 TOWN OF Iyannough Road OF BARNSTABLE HEALTH DEPT. Hyannis,Massachusetts RTN 4-11301 Tier IC Permit#100556 ACO-SE-03-3S-002 Dear Ms. Stanley: Geologic Services Corporation(GSC), on behalf of Motiva Enterprises LLC(Motiva),has prepared this Release Abatement Measure(RAM)Plan for the above referenced site. The objective of this RAM Plan is to appropriately manage petroleum-impacted soil, if encountered,during the construction activities scheduled to begin in April 2004. The original signature copy of BWSC-106 form has been included with this submittal. The contact at Motiva responsible for overseeing the response actions associated with this site is Mr. David B. Weeks,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590; (845)462-5225. The attached documents have been prepared under the direction of Licensed Site Professional(LSP)Mr. Scott K.Parker(LSP#9969)of GSC. Should you have any questions or concerns,please do not hesitate to contact Mr.David B. Weeks of Shell Oil Products US (SOPUS)at(845)462-5225 or the undersigned. Sincerely, Geologic Services Corporation Michael C.Bricher Scott K.Parker,L.S.P. Project Manager Senior Project Manager cc: Mr.David B.Weeks,SOPUS,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590 Mr.John Klimm,Hyannis Town Administrator,367 Main Street,Hyannis,MA 02601 ,Mr. Thomas McKean,Hyannis Board of Health,200 Main Street,Hyannis,MA 02601' ) Enclosures: Attachment A: Figures Figure 1 —Locus Plan Figure 2—Property Decommissioning Plan Figure 3—Vicinity Plan Ref.#000509C Rpt RAM Plan 03-04 Providing Environmental Management Solutions to Business and Industry Since 1982 A 100% Employee-Owned ESOP Company 15 Bonazzoli Avenue• Hudson, MA 01749 • Tel: 978.568.8740 1 800.522.8740 • Fax:978.568.9316 www.gsc-global.com Massachusetts Department of Environmental Protection gWSC106 Bureau of Waste Site Cleanup RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number TRANSMITTAL FORM 4� - 11301 Pursuant to 310 CMR 40.0444-0446(Subpart D) A SITE LOCATION: 1. site Name/Location Aid: Texaco Service Station #100083 2. Street Address: 1140 I annou h Road 3. City/Town: Hyannis 4. ZIP Code: 02601 # J 5. Check here if a Tier Classification Submittal has been provided to DEP for this disposal site. Fla. Tier 1A b. Tier 1 B Q c. Tier 1 C d. Tier 2 6. If a Tier I Permit has been issued,provide Permit Number: 100556 B.THIS FORM IS BEING USED TO: (check all that apply) 1. List Submittal Date of Initial RAM Written Plan(if previously submitted): (MM/DD/YYYY) 2. Submit an-Initial Release Abatement Measure(RAM)Plan. ❑ a. Check here if this RAM Plan received previous oral approval from DEP as a continuation of a Limited Removal Action(LRA). b. List Date of Oral Approval: 3. Submit a Modified RAM Plan of a previously submitted written RAM Plan. 4. Submit a RAM Status Report. i 5. Submit a RAM Completion Statement. �. 6. Submit a Revised RAM Completion Statement. 7. Provide Additional RTNs: a. Check here if this RAM Submittal covers additional Release Tracking Numbers (RTNs). RTNs that have been previously linked to a Primary Tier Classified RTN do not need to be listed here. This section is intended to allow a RAM to cover more than one unclassified RTN and not show permanent linkage to a Primary Tier Classified RTN. b. Provide the additional Release Tracking Number(s) � _ I�� ❑ - �� covered by this RAM Submittal. U (All sections of this transmittal form must be filled out unless otherwise noted above) Revised: 11/22/2002 Page 1 of BWSC1061102001 t ............. Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 Release Tracking Number RELEASE ABATEMENT MEASURE (RAM) 4 _ 11301 TRANSMITTAL FORM Pursuant to 310 CMR 40.0444-0446(Subpart D) C. RELEASE OR THREAT OF RELEASE CONDITIONS THAT WARRANT RAM: 1. Identify Media Impacted and Receptors Affected: (check all that apply) a. Air b. Basement c. Critical Exposure Pathway d. Groundwater a Residence f. Paved Surface I....# g.Private Well h. Public Water Supply i. School s.... j. Sediments k. Soil I. Storm Drain m. Surface Water i� n. Unknown o. Wetland p. Zone 2 q. Others Specify: 2. Identify all sources of the Release or Threat of Release,if known: (check all that apply) a. Above-ground Storage Tank(AST) b. Boat/Vessel € c. Drums d.Fuel Tank e.Pipe/Hose/Line f. Tanker Truck g. Transformer h. Under-ground Storage Tank(UST) i. Vehicle I j. Others Specify: 3. Identify Oils and Hazardous Materials Released: (check all that apply) ✓ a. Oils :•...;? b. Chlorinated Solvents c.Heavy Metals d. Others Specify: D. DESCRIPTION OF RESPONSE ACTIONS: (check all that apply,for volumes list cumulative amounts) 1. Assessment and/or Monitoring Only 2. Temporary Covers or Caps 3. Deployment of Absorbent or Containment Materials 4. Temporary Water Supplies 5. Structure Venting System : 6. Temporary Evacuation or Relocation of Residents 7. Product or NAPL Recovery 8. Fencing and Sign Posting 9. Groundwater Treatment Systems 10. Soil Vapor Extraction I.....{ 11. Bioremediation 12. Air Sparging ✓ 13. Excavation of Contaminated Soils a. Re-use, Recycling or Treatment i.On Site Estimated volume in cubic yards 0 ii.Off Site Estimated volume in cubic yards <1500 iia. Receiving Facility: TBD Town: State: iib. Receiving Facility: Town: State: iii. Describe: Total soil excavated not to exceed 1500 cubic yards Revised: 11/22/2002 Page 2 of 6 BWSC1061102002Ill,, w Massachusetts Department of Environmental Protection I Bureau of Waste Site Cleanup BWSC106 Release TrackingNumber RELEASE ABATEMENT MEASURE (RAM) i TRANSMITTAL FORM ® - 11301 �•��_� Pursuant to 310 CM 40.0444-0446(Subpart D) D. DESCRIPTION OF RESPONSE ACTIONS(cont.): (check all that apply,for volumes list cumulative amounts) b. Store i.On Site Estimated volume in cubic yards ii.Off Site Estimated volume in cubic yards iia.Receiving Facility: Town: State: iib.Receiving Facility: Town: State: c. Landfill i.Cover Estimated volume in cubic yards Receiving Facility: Town: State: ii. Disposal Estimated volume in cubic yards Receiving Facility: Town: State: 's t 14. Removal of Drums,Tanks or Containers: a. Describe Quantity and Amount: b. Receiving Facility: Town: State: c. Receiving Facility: Town: State: 15. Removal of Other Contaminated Media: a.Specify Type and Volume: b.Receiving Facility: Town: State: c.Receiving Facility: Town: State: 16. Other Response Actions: Describe: 17. Use of Innovative Technologies: Describe. Revised: 11/22/2002 Page 3 of 6 BWSC1061102003 0 . Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 Release Tracking Number RELEASE ABATEMENT MEASURE (RAM) ® _ 11301 TRANSMITTAL FORM Pursuant to 310 CMR 40.0444-0446(Subpart D) E. LSP SIGNATURE AND STAMP: I attest under the pains and penalties of perjury that I have personally examined and am familiar with this transmittal form, including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of(i)the standard of care in 309 CMR 4.02(1),(ii)the applicable provisions of 309 CMR 4.02(2)and(3),and 309 CMR 4.03(2),and (iii)the provisions of 309 CMR 4.03(3),to the best of my knowledge, information and belief, > if Section B of this form indicates that a Release Abatement Measure Plan is being submitted,the response action(s)that is (are)the subject of this submittal(i)has(have)been developed in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000, (ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)comply(ies)with the identified provisions of all orders, permits,and approvals identified in this submittal; > if Section B of this form indicates that a Release Abatement Measure Status Report is being submitted,the response action(s)that is(are)the subject of this submittal(i)is(are)being implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)comply(ies)with the identified provisions of all orders, permits,and approvals identified in this submittal; > if Section B of this form indicates that a Release Abatement Measure Completion Statement is being submitted,the response action(s)that is(are)the subject of this submittal(i)has(have)been developed and implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c. 21 E and 310 CMR 40.0000 and(iii)comply(ies) with the identified provisions of all orders, permits,and approvals identified in this submittal: I am aware that significant penalties may result, including,but not limited to, possible fines and imprisonment, if I submit information which I know to be false, inaccurate or materially incomplete. 1. LSP#: 9969 2. First Name: Scott K. 3. Last Name: Parker 4. Telephone: (978) 568-8740 5. Ext.: 239 6. FAX: (978) 568-9316 7. Signature 1 8. Date: 9.LSP Stamp: N 8F M4$s9cyG scow o K. co R 8 ysFO ROE�55� Revised: 11/22/2002 Page 4 of 6 BWSC1061102004 0 0 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 - Release Tracking Number RELEASE ABATEMENT MEAS URE (RAM) TRANSMITTAL FORM ® - 11301 Pursuant to 310 CMR 40.0444-0446(Subpart D) F. PERSON UNDERTAKING RAM: 1. Check all that apply: a.change in contact name b.change of address c, change in the person ...... undertaking response actions 2. Name of Organization: Motiva Enterprises LLC 3. Contact First Name: David B. 4.Last Name: Weeks 5. Street: PMB 301, 1830 South Rd., Unit 24 6.Title: Sr. Environmental Engineer 7. City/Town: Wappingers Falls NY 8. State: 9. ZIP Code: 1250 10. Telephone: (845) 462-5225 11.Ext.: 12. FAX: 845 462-4999 G. RELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON UNDERTAKING RAM: 1. RP or PRP R a. Owner b. Operator c. Generator d. Transporter e. Other RP or PRP Specify: 2. Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E,s.2) 3. Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.50)) s 4. Any Other Person Undertaking RAM Specify Relationship: H.REQUIRED ATTACHMENT AND SUBMITTALS: 1.Check here if any Remediation Waste,generated as a result of this RAM,will be stored,treated,managed,recycled or reused at the site following submission of the RAM Completion Statement. You must submit a Phase IV Remedy Implementation Plan along with the appropriate transmittal form(BWSC108). 2. Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order(s),permit(s) and/or approval(s)issued by DEP or EPA. If the box is checked,you MUST attach a statement identifying the applicable provisions thereof. 3. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the implementation of a Release Abatement Measure. 4. Check here if any non-updatable information provided on this form is incorrect,e.g. Release Address/Location Aid. Send ? corrections to the DEP Regional Office. 5. If a RAM Compliance Fee is required for this RAM,check here to certify that a RAM Compliance Fee was submitted to DEP,P.O.Box 4062,Boston,MA 02211. 6. Check here to certify that the LSP Opinion containing the material facts,data,and other information is attached. Revised: 11/22/2002 Page 5 of 6 B WSC 1061102005 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 f - Release Tracking Number �'. RELEASE ABATEMENT MEASURE (RAM) :......•• TRANSMITTAL FORM ® - 11301 m •,,:<<.:.;;;},.• Pursuant to 310 CMR 40.0444-0446(Subpart D) I. CERTIFICATION OF PERSON UNDERTAKING RAM: 1. I, David B. Weeks ,attest under the pains and penalties of perjury(i)that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is, to the best of my knowledge and belief,true,accurate and complete,and(iii) that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. I/the person or entity on whose behalf this submittal is made am/is aware that there are significant penalties,including, but not limited to, possible fine impriso nt ffor%Afully submitting false,inaccurate,or incomplete information. 2. By: 3. Title: Sr. Environmental Engineer Signature 4. For: Motiva Enterprises LLC (Name of person or entity recorded in Section F) (mm/dd/yyy 5. Check here if the address of the person providing certification is different from address recorded in Section F. 6. Street: 7. Cityrrown: 8. State: 9. ZIP Code: 10. Telephone: 11.Ext.: 12. FAX: YOU MUST LEGIBLY COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Date Stamp(DEP USE ONLY:) Revised: 11/22/2002 Page 6 of 6 BWSC1061102006 Geologic Services Corporation science,engineering&technology RELEASE ABATEMENT MEASURE PLAN TEXACO SERVICE STATION#100083 1140 IYANNOUGH ROAD HYANNIS,MASSACHUSETTS DEP RTN 4-11301 TIER IC PERMIT#100556 ACO-SE-03-3S-002 March 2004 Prepared by: Prepared for: Geologic Services Corporation Motiva Enterprises LLC 15 Bonazzoli Avenue PMB 301,1830 South Road,Unit 24 Hudson, Massachusetts 01749 Wappingers Falls,NY 12590 (978) 568-8740 (845)462-5225 REF. #000509C Providing Environmental Management Solutions to Business and Industry Since 1982 A 100% Employee-Owned ESOP Company 15 Bonazzoli Avenue• Hudson, MA 01749 • Tel: 978.568.8740 1 800.522.8740 • Fax: 978.568.9316 www.gsc-global.com f Texaco Service Station#100083 Geologic Services Corporation Page 1 Release Abatement Measure Objective On behalf of Motiva Enterprises LLC(Motiva),Geologic Services Corporation(GSC)has prepared a Release Abatement Measure(RAM)Plan for the Texaco-branded Service Station#100083 located at 1140 Iyannough Road in Hyannis,Massachusetts. The objectives of the herein-proposed RAM are to excavate, appropriately manage,and to the degree required,transport and dispose of petroleum-impacted soil and groundwater(if encountered)during the removal of the gasoline and diesel underground storage tanks (USTs),dispensers,piping, fuel oil UST,waste oil UST(if present),hydraulic lift,dry well(if present),and the advancement of test pits in the vicinity of an on-site catch basin. Please refer to Figures 1, 2, and 3 (Attachment A)for illustrations of the subject site and surrounding area. Motiva is conducting the RAM activities referenced herein. The contact at Motiva responsible for overseeing the response actions associated with this site is Mr.David B. Weeks,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590; (845)462-5225. Background The subject property was listed by the Massachusetts Department of Environmental Protection(MA DEP) based on information reported in a December 28, 1994 2 1 E Site Assessment Report,prepared by Down Cape Engineering,Inc. (DCE)for Cooke's Restaurant located adjacent to the site at 1120 Iyannough Road, Hyannis,Massachusetts. As part of this site assessment,DCE collected groundwater samples from three monitoring wells located on the Cooke's Restaurant property. Laboratory analysis indicated the presence of benzene, toluene,and xylenes in the sample obtained from a well reported to be downgradient of the Texaco Station. The MA DEP issued release tracking number(RTN)4-11301 on April 6, 1995 in response to these fmdings. As a result of the 21 E Site Assessment of Cooke's Restaurant,the MA DEP issued a Notice of Responsibility(NOR)to Star Enterprises(Star)owner of the property located at 1140 Iyannough Road in Hyannis,Massachusetts on August 11, 1995. On October 12, 1995, Star, submitted a Phase I-Initial Site Investigation Report and Tier IC Application to MA DEP for the subject site. During the Phase I investigation,groundwater sampling results of the on-site monitoring wells revealed dissolved-phase petroleum constituents in excess of the MA DEP reportable concentrations for GW-1 groundwater standards. The MA DEP approved the Tier IC Permit Application(No. 100556) for the subject property on September 12, 1996. At this time it was determined that a Substantial Release Migration(SRM)condition may exist and the MA DEP required an Immediate Response Action(IRA)Plan to be submitted. Star submitted an assessment-only IRA Plan proposing tri-annual groundwater monitoring for a one-year period to evaluate seasonal changes in groundwater elevation and quality. A Phase II Scope of Work(SOW)was submitted by Groundwater&Environmental Services,Inc. (GES) on July 25, 1997 for additional subsurface investigations to be completed. This work included the installation of additional monitoring wells and additional groundwater sampling. On September 18, 1998, SAGE submitted an IRA Status report summarizing the installation of three monitoring wells and the advancement of five soil borings. Groundwater samples were collected from ten on-site monitoring wells on May 6, 1998 and analyzed for extractable petroleum hydrocarbons(EPH)and volatile petroleum hydrocarbons(VPH). Soil analytical results for this sampling event indicated concentrations of methyl-tertiary butyl ether (MTBE)above the applicable Method 1 S-1/GW-1 soil standard at soil sample locations MW-9 and SB-11. Dissolved phase petroleum constituents were detected above applicable Method 1 GW-1 standards in samples collected from all site related monitoring wells except MW-3. I ' Ref. #000509C_Rpt_RAM Plan 03-04 F Texaco Service Station#100083 Geologic Services Corporation Page 2 SAGE submitted a Modification to the Phase 11 SOW report on August 13, 1998 for the installation of off- site monitoring wells,well surveying, groundwater sampling, and a soil vapor extraction(SVE)pilot test. SAGE was unable to secure off-site access for the installation of downgradient monitoring wells. However, the SVE pilot test and groundwater sampling were completed on March 25, 1999 and June 4, 1999, respectively. SAGE indicated that the results of the SVE test were skewed due to recent construction activities that may have caused short-circuiting in the airflow diminishing the effective radius of influence. On March 4, 1999, SAGE submitted a Modification to the IRA Plan report in response to extensive excavation activities proposed at the site. The modification addressed excess soil to be generated during the installation of new pump islands and canopy foundations, and the removal and replacement of two leaching catch basins. It included a work scope for the soil testing of excavated soils,confirmatory sampling, and management of excavated soils. Approximately 556.75 tons of soil was removed from the site on March 4 and 5, 1999 for reuse at a landfill. Approximately 188.47 tons of petroleum-impacted soil was transported to an off-site disposal facility for recycling on March 24, 1999. In 1999,responsibility for the release was transferred to Motiva,which was created in the formation of a joint venture between Shell and the owners of Star. On August 22,2000, SAGE submitted a Phase II and Phase III Report. Groundwater extraction combined with soil vapor extraction technologies were selected as the remedial action alternative for achieving a permanent solution at the subject property. Following review of the Phase II and III Reports,additional delineation of the dissolved phase petroleum hydrocarbons related to the subject property was viewed to be warranted prior to the selection/implementation of a remedial action. In conjunction with the installation of the groundwater monitoring wells,pilot test air sparge(AS) and SVE wells were installed at the subject property. In March of 2001, GSC and Motiva were able to secure off-site access to abutting properties. Between March 19 and 23,2001, GSC personnel supervised the installation of four 2-inch diameter groundwater monitoring wells MW-11,MW-12,MW-13,and MW-14 at and in the vicinity of the subject property in order to further delineate petroleum impact to soil and groundwater. During groundwater monitoring well gauging and sampling activities performed on April 4,2001, approximately 0.60 feet of non-aqueous phase liquid(NAPL)(i.e.;weathered gasoline)was detected in monitoring well MW-9. The MA DEP was verbally notified of the presence of greater than 0.5 inches of NAPL on April 5,2001. The MA DEP subsequently assigned RTN 4-16161 to this 72-hour release condition and verbally approved passive NAPL bailing activities under an IRA. On April 12,2001,Tanknology-NDE of Springfield,Massachusetts performed a pressure tank tightness test for the gasoline UST system at the subject property. All the pressure tests performed on the UST system passed on this date. On June 8,2001,Motiva submitted a Tier IC Permit Renewal Application to the MA DEP in order to allow for the continuation of response actions under RTN 4-11301. In addition,the Tier I Permit application detailed the linking of RTN 4-16161 to lead RTN 4-11301. On September 27,2001, a Decision to Grant a Tier IC Permit Extension was approved by the MA DEP. On July 16, 2002,the MA DEP issued a Notice of Noncompliance(NON) (NON-SE-02-35-014)to Motiva for failure to submit an administratively complete Phase II Report and Phase III Plan. Ref. #000509C_Rpt_RAM Plan 03-04 Texaco Service Station#100083 Geologic Services Corporation Page 3 IRA Status Reports were submitted to the MA DEP in March and August 2002 detailing NAPL recovery and assessment activities during the period of August 2001 through July 2002. An IRA Plan Design Specification was also submitted to the MA DEP in August 2002 summarizing a SVE/AS pilot test and detailing a remedial design plan to treat the source area. An IRA Status Report was submitted to the MA DEP on February 21,2003 documenting the installation of the SVE/AS remedial system,NAPL recovery, and continued site assessment activities. The SVE and AS systems were activated on March 14,2003 and April 4,2003,respectively. The SVE/AS system is currently operational. Operation and maintenance of the SVE/AS system is documented in the semi-annual IRA Status Report dated August 22,2003 and IRA Completion Report dated February 19, 2004. Motiva entered into an Administrative Consent Order(ACO)(ACO-SE-03-3S-002)with the MA DEP on February 19, 2003. As part of the ACO agreement between Motiva and the MA DEP,the following regulatory deadlines were established for the subject property: Phase H-Comprehensive Site Assessment and Phase III-Remedial Action Plan-April 15,2003;Phase IV-Remedy Implementation Plan- September 30,2003; and Phase V-Remedy Operation Status-June 30,2004. A Supplemental Phase H Comprehensive Site Assessment Report(Supplemental Phase II)and Phase III- Remedial Action Plan(RAP)Addendum were submitted for the subject property on April 14,2003. The Supplemental Phase H and Phase III-RAP Addendum documented the installation of fifty monitoring wells, eleven soil vapor extraction wells, eight air sparge wells,three monitoring point triplets,three cone penetrometer testpoint(CPT)borings,and twenty-six temporary well points during the period of October 2000 through March 2003. In addition,twenty-seven groundwater gauging events and thirteen groundwater sampling events were conducted during this time period. The selected remedial action alternative for the reduction of residual petroleum constituents on the property is the installation and operation of a Groundwater Extraction and Treatment system downgradient of the subject property coupled with the existing SVE/AS system in the tankfield area. The selected remedial action alternative outside of the target areas of active remediation is monitored natural attenuation(MNA) for management of migration and eventual reduction of dissolved-phase impacts. A Tier IC Permit Extension was submitted to the MA DEP on June 10,2003 in order to allow for the continuation of response actions under RTN 4-11301. In accordance with the revisions to the MCP 310 CMR 40.0720,the Tier 1C Permit Extension was presumed approved on August 11,2003. The expiration date of the Tier IC Permit is September 12, 2005. Based on difficulties securing access to evaluate an off-site remediation system,Motiva requested an extension for the submittal of the Phase IV-Remedy Implementation Plan(RIP). The ACO Amendment #1 dated September 18,2003 extended the Phase IV-RIP to January 31, 2004. The effective date for ACO Amendment#1 is October 1,2003. The Phase IV-RIP,dated January 29,2004, detailed the proposed implementation for the off-site Groundwater Extraction and Treatment system,ongoing operation and maintenance of the on-site SVE/AS system,and continuation of MNA. In addition,the Phase IV-RIP documented the installation of one recovery well,two monitoring points,recovery well development,overburden aquifer pumping and re- injection tests, and sampling of recovery well RW-1. An IRA Completion Report was submitted to the MA DEP on February 19,2004. Ref. #000509C_Rpt_RAM Plan 03-04 Texaco Service Station#100083 Geologic Services Corporation Page 4 Description of Site Conditions/Surrounding Receptors,pursuant to 310 CMR 40.0427(4)(a) The subject property is situated at 1140 Iyannough Road in Hyannis,Massachusetts and is currently an active Texaco branded retail gasoline and automobile repair facility. The subject property has an area of approximately 47,916.19 square feet(1.1 acres). The majority of the site is paved with asphalt or reinforced concrete,except a small area in the southern portion of the lot,which is landscaped. The northern portion of the property is wooded and covered in gravel. The single-story Texaco station houses an office area, restrooms,and three repair service bays. One 12,000 gallon gasoline UST,two 10,000 gallon gasoline USTs, one 8,000 gallon diesel fuel UST, and one 550 gallon fuel oil UST currently exist at the site. The site is serviced by municipal water supply and sewer as well as underground telephone and electric service utilities. The subject site drainage system is connected to an on-site leachfield located immediately east of the service station building. Two detention drainage basins are located approximately 80 feet southeast and 90 feet north of the convenience store,respectively. Please refer to Figures 1,2, and 3 for a depiction of the subject property and surrounding area. The surrounding area is zoned for commercial use. Cooke's Seafood Restaurant is located immediately east of the subject property. Parker's Liquor Store is located immediately west of the subject property. A commercial plaza(Festival at Hyannis)is located immediately north of the subject property. A Ramada Inn is located approximately 100 feet south of the subject property across Iyannough Road. A Cumberland Farms Gulf Station is located approximately 210 feet southwest of the subject property. Subsurface structures within 1,000 feet of the site include half and full basements and utility conduits located along Iyannough Road,Bearses Way and Independence Drive. The closest known basement is located approximately 600 feet southwest(upgradient)of the subject property. Subsurface utility conduits located along these streets include,but are not limited to,municipal water, sewer,gas, and storm drainage. Overhead electric and telephone utilities also exist along these streets and subject site. According to the USGS Hyannis,Massachusetts Topographic Map and GSC site reconnaissance there are no schools, institutions,or environmentally sensitive receptors known to exist within 1,500 feet of the subject property. According to the USGS Hyannis,Massachusetts Topographic Map(refer to Figure 1),the closest surface water bodies include an unnamed brook located approximately 1,800 feet east,Hathaway Pond located approximately 2,600 feet northwest,and Shallow Pond located approximately 3,100 feet west of the subject property. Multiple kettle ponds are located approximately 2,000 feet east of the subject property along Independence Drive. Additional ponds are located further northeast and southeast of the property. According to the flood insurance rate map produced by the Federal Emergency Management Agency,the subject property is located within an area designated as Zone C(an area of minimal flooding). According to the Massachusetts Geographic Information System(GIS),the subject property is located within a MA DEP-Approved Zone II and an EPA-designated sole source aquifer. Six municipal public groundwater supply wells are known to exist within a 1.5-mile radius of the subject property. The closest public supply well(Barnstable Fire District Well#2)is located approximately 4,000 feet northwest of the subject property. According to the Barnstable Water Company and the Barnstable Water Department,no private supply wells exist within 1,000 feet of the disposal site. The subject property and surrounding area are serviced by municipal water. Ref.#000509C_Rpt_RAM Plan 03-04 Texaco Service Station#100083 Geologic Services Corporation. Page 5 Scope of Work The scope of work as it pertains to this RAM includes the management of Remediation Waste associated with the following activities: ■ Selective excavation and off-site disposal of soil during the removal of two 10,000-gallon gasoline USTs, one 12,000-gallon UST, one 10,000 gallon diesel UST, associated product piping, and dispenser equipment; ■ Selective excavation and off-site disposal of soil during the removal of one 550-gallon fuel oil UST; ■ Selective excavation and off-site disposal of soil during the removal of one 550-gallon used oil UST (if present); ■ Selective excavation and off-site disposal of soil during the removal of one hydraulic lift; and ■ Selective excavation and off-site disposal of soil during the removal of dry wells(if present) and installation of test pits in the vicinity of the catch basin located on the northwestern portion of the property. Refer to Figure 2—Site Plan for the locations of the USTs and other site features. In so far as possible, excavated soil will be re-used on-site. Clean fill will be brought in from off-site as needed. Based on historical depth to groundwater,dewatering will not be required during the site construction activities. Environmental Monitoring and Soil Segregation During the equipment removal activities,on-site inspections and field screening of excavated soil will be completed. Field screening of soil sample headspace will be performed using a photo ionization detector (PID)equipped with a 10.6 electron volt(eV)lamp calibrated with an isobutylene span gas to yield total volatile organic compounds(VOCs)in parts per million volume(ppmv)referenced as benzene. No more than 1,500 cubic yards of Remediation Waste will be generated during the RAM activities described herein. Excavated soil will be segregated into three separate soil types based on PID response to soil vapor headspace and visual and olfactory indications of petroleum-impact as follows: • Type A soils will include soils that are observed to have visual evidence of petroleum impact, and with soil headspace PID responses greater than 10 ppm. • Type B soils will include soils that are observed to have no visually apparent evidence of petroleum impact,and with soil headspace PID responses less than 10 ppm. • Type C material will consist of asphalt; concrete and other construction debris removed form the excavation. Any concrete and any suitable construction debris encountered will either be returned to the excavation upon completion or disposed of as construction debris. Following the completion of the soil excavation,composite soil samples will be collected from soil stockpile A and submitted to Accutest Laboratories,Inc. (Accutest)of Marlborough,Massachusetts for analysis of disposal parameters including flashpoint via 1010,pH,reactivity(sulfide and cyanide),VOCs via 8260,total petroleum hydrocarbons(TPH)-gasoline range only(GRO)and diesel range only(DRO), RCRA 8 metals, and Polychlorinated Biphenyls(PCBs)via EPA Method 8080. Ref.#000509C_Rpt_RAM Plan 03-04 I Texaco Service Station#100083 Geologic Services Corporation Page 6 The results of the Type B stockpile analysis will be compared to the Massachusetts Contingency Plan (MCP)Method 1 Risk Characterization S-1 soil standards. If the concentrations of chemicals of concern (COC)are greater than the Method 1 Risk Characterization soil standards,then the soil will be considered Remediation Waste and transported from the site along with Type A soil under a Massachusetts Bill of Lading for recycling. If the COC concentrations are below the MCP Method 1 Risk Characterization soil standards, than the soil will be considered reusable and may be backfilled in an excavation. Soil Stockpiling Protocol Soil excavated during the RAM activities will be stockpiled on 6 mil thick polyethylene sheeting. The soil pile will be covered with 6 mil polyethylene sheeting and secured at the end of each working day until the soil is either backfilled or removed from the site. Post Excavation Sampling During the gasoline UST, gasoline dispensers,and gasoline product pipe excavations,representative soil samples will be collected from in-situ soil at the side wall(s)and bottom of the excavation for laboratory analysis. Soil samples will be collected and submitted to a laboratory for analysis of VPH via MA DEP- approved methodology, ethylene dibromide(EDB),and lead. Soil samples will be collected at 10 to 15 foot intervals along the product piping. During the diesel UST,diesel dispenser,diesel product pipe,hydraulic lift, and fuel oil UST excavations, representative soil samples will be collected from in-situ soil at the side wall(s)and bottom of the excavations for laboratory analysis. Soil samples will be collected and submitted to a laboratory for analysis of EPH via MA DEP-approved methodology. Soil samples will be collected at 10 to 15 foot intervals along the product piping. During the excavation of the used oil UST(if present)and dry wells(if present),representative soil samples will be collected from in-situ soil at the side wall(s)and bottom of the excavations for laboratory analysis. Soil samples will be collected and submitted to a laboratory for analysis of EPH,VPH,PCBs,total metals via EPA Methods 6010B and 7471A,and VOCs via EPA Method 8260. During the installation of the catch basin test pits,representative soil samples exhibiting the highest PID readings may be collected for laboratory analysis of EPH,VPH,PCBs,total metals via EPA Methods 6010B and 7471A, and VOCs via EPA Method 8260. Management of Remediation Waste Soil determined to be Remediation Waste as described herein will be transported to a licensed recycling facility for asphalt batching using a MA DEP Bill of Lading in accordance with the provisions of 310 CMR 40.0030. Schedule for RAM Implementation Motiva will obtain the necessary permits from the Barnstable Fire Department prior to removing the USTs. At this time,no additional federal, state, or local permits are required to perform these RAM activities. The RAM activities proposed herein are currently scheduled to commence during the week of April 1, 2004. RAM activities are anticipated to proceed for approximately two weeks. Actual time may vary in response to conditions encountered during excavation activities. Should the scope of this RAM Plan change significantly prior to or during its implementation, a RAM Addendum specifically outlining Ref.#000509C_Rpt_RAM Plan 03-04 Texaco Service Station#100083 Geologic Services Corporation Page 7 pertinent modifications to the workscope will be prepared for submittal to the MA DEP. PID readings in excess of 100 ppmv in soil samples collected from within the UST excavation may be encountered and will be related to the existing RTN 4-11301; thus, no new notification condition will be made to MA DEP as this RAM Plan will serve as appropriate documentation to manage the impacted soil. RAM Limitations Pursuant to 310 CMR 40.0442(4), a maximum of 1,500 cubic yards of soil may be excavated during the course of this RAM, and classified as Remediation Waste. Please note that excavation on the western edge of the UST area and diesel dispenser may be limited due to the proximity to the property line. If site conditions become significantly different from those previously documented on the site,an Imminent Hazard is identified to exist,or if conditions requiring a 2 or 72 hour notification of a release to the MA DEP pursuant to 310 CMR 40.0300 are encountered,all work being performed in conjunction with the RAM will be terminated. The responsible party(RP)for the RAM will make the appropriate notification to MA DEP. Activities will resume only after such notification has been made and MA DEP approves the continuation of the project. Health& Safety On-site health and safety practices in accordance with standards set forth by the Occupational Safety and Health Administration(29 CFR 1910.120)will be observed by all site personnel associated with the RAM for the duration of field activities. A site specific Health and Safety Plan has been prepared for these activities. Public Involvement By copy of this document,the Chief Municipal Officer and the Board of Health for the Town of Barnstable have been provided notice of the RAM in accordance with 310 CMR 1403(3)(d). Project Completion Pursuant to the provisions set forth in 310 CMR 40.0440, RAM Status and/or Completion Reports will be periodically submitted to the MA DEP detailing the activities completed under the RAM and any change in site conditions subsequent to the implementation of the RAM. Schedule • Construction anticipated to start in early April 2004 • RAM Completion(or Status)Report— 120 days following submittal of this Plan Ref.#000509C_Rpt_RAM Plan 03-04 I t� ATTACHMENT A Figures S,ifs. t T•.' - _ -�8 - ,l,�r� �0,,.'_ �•fj i* ,?iF��I. ti -ate ..M �1 '° •• �.. � ... .-' .r,, �,•, , '�lam; `�"'•����� :j,��/ �j,�,' � �'�£,��.��'C�� � � �„� � "r �JI'. ; �• _ '_ �r• �;,�%�� l��\ ��'�t��"LF�J��3.�ys, ��r�: \,. ii � V� r •,Aoj .are /i \\ ,�•,,_ r MAN j OR I IT In Nt ��f% � ,�,: � 1 � , �t✓f'4s�,t�+ae�,"r:•� ,i�` ��1 i l ,�,,�i W,01 -A(- 1000 i 1000 2000 3000 4000 Feet — '\ nnununnu■iiii nnnnunnnun■3 u■■nnnnnnnun nnnnnunnnnn ■nnnnnnnnnnn n■nnnnnnuunn n ■unu■ ■ u ■■■ UTM 11 ' II QUADRANGLE / 1 LATITUDE: i ZONE 19 LONGITUDE: I' FIGURE 1 LOCUSPLAN Notes: 1. Topographic contours are measured in meters. 2. Topographic contour interval= 10 meters. 1140 IYANNOUGH ROAD :. : 1. 1 Hydrogeologists and Environmental Scientists . .p.a ..t • .. :.i a MA " 15 :• .i• Avenue * Hudson, W 01749 • •i •i Quadrangle 15 MftMe Series I TMP-120 MW-3A N SYSTEM I ENCLOSURE MW A (BUILDING M i KEY 17 , SB-7 SOIL BORING SVE-9 MW-1 A AS-5 DESTROYED MONITORING WELL MW-14D SVE-3 ' `` HYDRAULIC LIFT MW-141 _1 1 ® CB-2 MW-7 MW-18S MW-14 B WS-10 # TMP-103 ;""W'18D ` GROUNDWATER MONITORING WELL MW-14S � MW-5 OAS-6 ®SVE-8 M#8 / O AIRSPARGE WELL SVE-2 ®SVE-10 MW_#6 ♦ RECOVERY WELL AS-3 UST SB-8 ' CPT— AREA AS-2 SB-10 ® SOIL VAPOR EXTRACTION WELL MW-9 a,_ O ®SV —6 # MW-4 / TEMPORARY MONITORING WELL \ SVE-1 /�S-8 MP-101 # DIESEL i U�0 OIL I lB CATCH BASIN/POTENTIAL DRYWELL DISPENSER MP-2 J tSVE-11 SERVICE RW-1PROPERTY BOUNDARY ISLAND MP_ # — 0 MP 102 Mt 1* AS—7SVL-7 STATION / UST UNDERGROUND STORAGE TANK MW-1 COOKIE'S U/0 USED OIL MWC`PT 02 .®CB-1 ® MW-3 / RESTAURANT F/O FUEL OIL T P�101 SVE-4 # # N" ®SVE-5 F/0 UST M —1 1 / NOTE: LOCATION OF SYSTEM ENCLOSURE IS APPROXIMATE SB ,�. GASOLINDISPENSER ! t lk MW-12 ISLANDS / CB-3® MW— k 0 50 Scale in feet FIGURE 2 ) Qo PROPERTY DECOMMISSIONING PLAN TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS FREVISED 000509.01 DECON CHECKED BY: Y: SAC DATE: 8 12 02 Y: ANG DAE: 3 12 04 ��1GEOLOGIC SERVICES CORPORATIONSC FIELD RECONNAISSANCE � � � Hydrogeologists and Environmental Scientists 15 Bonaaoli Avenue • Hudson,MA 01749 •(978)568-8740 l COMMERCIAL PIER 1 PAYLESS M GRAVEL PITS �O W � BLOCKBUSTER Q � JENNY ATTRESS CRAIG GIANT F OLIVE GA RD COOKE'S ~ EN QSEAPO00 x O)S R VS DISCOVNT ./ THE RAMAOA THE SITE / M�ES REALES AT ��g E 0 350 R GULF RE�R PARKER'S AT ON Scole in feet UTC E DI SCOUNT OUNT T KEY LIQUOR FIGURE 3 VICINITY PLAN TEXACO SERVICE STATION #100083 — - — PROPERTY BOUNDARY 1 140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.01 VICINB CHECKED BY: k DRAFTED BY: CD DATE: 241 02 REVISED BY: ANG DATE: 3 27 02 GEOLOGIC SERVICES CORPORATION SOURCE: SAGE ENVIRONMENTAL PLAN AND GSC FIELD RECONNAISSANCE Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue 9 Hudson, MA 01749 •(978)568-8740 Geologic 6Services c Corporation f L 3.! _ _ Z,7 ^science,engineering&technology Waybill#22141751450 July 8, 2004 Massachusetts Department of Environmental Protection Southeast Regional Office Bureau of Waste Site Cleanup Attn: Ms.Laura Stanley ' 20 Riverside Drive Lakeville,MA 02347 Re: Release Abatement Measure Completion Report Former Texaco Service Station#100083 , e 1140Iyannough Rozd ` Hyannis,Massachusetts RTN 4-11301 Tier IC Permit#100556 ACO-SE-03-3S-002 Dear Ms.Stanley: Geologic Services Corporation(GSC),on behalf of Motiva Enterprises LLC(Motiva),has prepared this Release Abatement Measure(RAM)Completion Report and associated Massachusetts Department of Environmental Protection(MA DEP)Form BWSC-106 for the above referenced site. This report summarizes the removal of underground storage tanks(USTs),associated UST dispenser equipment,fuel oil UST,and hydraulic lift,as well as the cleaning of an oil/water separator on the subject property. The contact at Motiva responsible for overseeing the response actions associated with this site is Mr.David B. Weeks,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590;(845)462-5225. The attached documents have been prepared under the direction of Licensed Site Professional(LSP)Mr. Scott K.Parker(LSP# 9969)of GSC. The next scheduled regulatory submittal is a Phase IV-Final Inspection Report,anticipated for completion on or before November 1,2004. Should you have any questions or concerns,please do not hesitate to contact Mr.David B. Weeks of Shell Oil Products.US(SOPUS)at(845)462-5225 or the undersigned. Sincerely, Geologic Services Corporation Michael C.Bricher Moira S.Walker Project Manager Senior Environmental Scientist cc: Mr.David B.Weeks,SOPUS,PMB 301, 1830 South Road,Unit 24,Wappingers Falls,NY 12590 Mr.John Klimm,Hyannis Town Administrator,367 Main Street,Hyannis,MA 02601 Mr.Thomas McKean,Hyannis Board of Health,200 Main Street,Hyannis,MA 02601 Mr.Tom Rento,Kimco R-.alty Corp, 11 Computer Drive West,Suite 210,Albany,NY 12205 Mr.John Roche,The Flately Company,P.O.Box 859206,Braintree,MA 02185 Prime 132,LLC,297 North Street,Hyannis,MA 02601 Enclosures Ref.#000509C Rpt RAMC 07-04 Providing Environmental Management Solutions to Business and Industry Since 1982 A 100% Employee-Owned ESOP Company 15 Bonazzoli Avenue• Hudson, MA 01749 • Tel: 978.568.8740 1 800.522.8740 • Fax: 978.568.9316 www.gsc-global.com f Massachusetts Department of Environmental Protection gWSC106 Bureau of Waste Site Cleanup RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number TRANSMITTAL FORM 4F - 11301 Pursuant to 310 CMR 40.0444-0446(Subpart D) A. SITE LOCATION: 1. Site Name/location Aid: TexaXo Service Station NO. 100083 2. Street Address: 1140 Iyannough Road 3. Cityrrown: Hyannis 4. ZIP Code: 02060 ® 5. Check here if a Tier Classification Submittal has been provided to DEP for this disposal site. a. Tier IA b. Tier IB © c. Tier IC n d. Tier II 6.If a Tier I Permit has been issued,provide Permit Number: 100556 i B.THIS FORM IS BEING USED TO: (check all that apply) 1. List Submittal Date of Initial RAM Written Plan(if previously submitted): 2. Submit an Initial Release Abatement Measure(RAM)Plan. (mm/dd/yyyy) a. Check here if this RAM Plan received previous oral approval from DEP as a continuation of a Limited Removal Action(LRA). b. List Date of Oral Approval: (mm/dd/yyyy) 3. Submit a Modified RAM Plan of a previously submitted written RAM Plan. 4. Submit a RAM Status Report. ® 5. Submit a RAM Completion Statement. 6. Submit a Revised RAM Completion Statement. 7. Provide Additional RTNs: a. Check here if this RAM Submittal covers additional Release Tracking Numbers(RTNs). RTNs that have been previously linked to a Primary Tier Classified RTN do not need to be listed here. This section is intended to allow a RAM to cover more than one unclassified RTN and not show permanent linkage to a Primary Tier Classified RTN. b. Provide the additional Release Tracking Number(s) a _ � � - covered by this RAM Submittal. (All sections of this transmittal form must be filled out unless otherwise noted above) Revised: 11/04/2003 Page 1 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number ' TRANSMITTAL FORM 4❑ - 11301 w Pursuant to 310 CMR 40.0444-0446(Subpart D) C. RELEASE OR THREAT OF RELEASE CONDITIONS THAT WARRANT RAM: 1. Identify Media Impacted and Receptors Affected: (check all that apply) ❑ a. Air ❑ b. Basement ❑ c. Critical Exposure Pathway d. Groundwater ❑ e. Residence ❑ f. Paved Surface ❑ g.Private Well ❑ h. Public Water Supply ❑ i. School ❑ j. Sediments ® k. Soil ❑ I. Storm Drain ❑ m. Surface Water ❑ n. Unknown ❑ o. Wetland ❑ p. Zone 2 ❑ q. Others Specify: 2. Identify all sources of the Release or Threat of Release,if known: (check all that apply) a. Above-ground Storage Tank(AST) ❑ b. Boat/vessel ❑ c. Drums ❑ d.Fuel Tank ❑ ❑ e. Pipe/Hose/line ❑ f. Tanker Truck ❑ g. Transformer ® h. Under-ground Storage Tank(UST) ❑ i. Vehicle ❑ j. Others Specify: 3. Identify Oils and Hazardous Materials Released: (check all that apply) ma. Oils ❑ b. Chlorinated Solvents ❑ c.Heavy Metals ❑ d. Others Specify: D. DESCRIPTION OF RESPONSE ACTIONS: (check all that apply,for volumes list cumulative amounts) ❑ 1. Assessment and/or Monitoring Only ❑ 2. Temporary Covers or Caps ❑ 3. Deployment of Absorbent or Containment Materials ❑ 4. Temporary Water Supplies ❑ 5. Structure Venting System ❑ 6. Temporary Evacuation or Relocation of Residents 7. Product or NAP Recovery ❑ 8. Fencing and Sign Posting ❑ 9. Groundwater Treatment Systems ❑ 10. Soil Vapor Extraction ❑ 11. Bioremediation ❑ 12. Air Sparging ❑ 13. Excavation of Contaminated Soils ❑ a. Re-use, Recycling or Treatment ❑ i.On Site Estimated volume in cubic yards ❑ ii.Off Site Estimated volume in cubic yards iia.Receiving Facility: Town: State: iib.Receiving Facility: Town: State: iii. Describe: Revised: 11/04/2003 Page 2 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number TRANSMITTAL FORM 40 _ 11301 k Pursuant to 310 CMR 40.0444-0446(Subpart D) D. DESCRIPTION OF RESPONSE ACTIONS(conk): (check all that apply,for volumes list cumulative amounts) b. Store i.On Site Estimated volume in cubic yards ii.Off Site Estimated volume in cubic yards iia.Receiving Facility: Town: State: iib.Receiving Facility: Town: State: c. Landfill Ej i,Cover Estimated volume in cubic yards Receiving Facility: Town: State: ii.Disposal Estimated volume in cubic yards Receiving Facility: Town: State: 14. Removal of Drums,Tanks or Containers: a. Describe Quantity and Amount: 1347 gallons of water/product; 50 gallons of hydraulic oil; 1600 pounds of oil/debris/sludge b. Receiving Facility: International Petroleum Corporation Town: Wilmington State: DE c. Receiving Facility: Northland Environmental, Inc. Town: Providence State: RI 0 15. Removal of Other Contaminated Media: a.Specify Type and Volume: 250 pounds of paint mixture b.Receiving Facility: Northland Environmental, Inc. Town: State:Providence RI c.Receiving Facility: Town: State: 16. Other Response Actions: Describe: El 17. Use of Innovative Technologies: Describe: Revised: 11/04/2003 Page 3 of 6 r Massachusetts Department of Environmental Protection :Bureau of Waste Site Cleanup BWSC106 ' RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number (� TRANSMITTAL FORM 11301 4 Pursuant to 310 CMR 40.0444-0446(Subpart D) E. LSP SIGNATURE AND STAMP: I attest underthe pains and penalties of perjury that I have personally examined and am familiar with this transmittal form, including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of(i)the standard of care in 309 CMR 4.02(1),(ii)the applicable provisionsof 309 CMR 4.02(2)and(3),and 309 CMR 4.03(2),and (iii)the provisions of 309 CMR 4.03(3),to the best of my knowledge,information and belief, > if Section B of this form indicates that a Release Abatement Measure Plan is being submitted,the response action(s)that is (are)the subject of this submittal(i)has(have)been developed in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)comply(ies)with the identified provisions of all orders, permits,and approvals identified in this submittal; > if Section B of this form indicates that a Release Abatement Measure Status Report is being submitted,the response action(s)that is(are)the subject of this submittal(i)is(are)being implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.000C,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)comply(ies)with the identified provisions of all orders,permits,and approvals identified in this submittal; > if Section B of this form indicates that a Release Abatement Measure Completion Statement is being submitted,the response action(s)that is(are)the subject of this submittal(i)has(have)been developed and implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000 and(iii)comply(ies) with the identified provisions of all orders, permits,and approvals identified in this submittal: I am aware that significant penalties may result,including,but not limited to,possible fines and imprisonment,if I submit information which I know to be false,inaccurate or materially incomplete. 1. LSP#: 9969 2. First Name: SCOtt K. 3. Last Name: Parker 4. Telephone: (978 568-8740 5 Ext: 239 6. FAX: 978 568-9316 7. Signature: 8. Date: V -3 9.LSP Stamp: (m►n/dd/Y YY) OF MASS9cyGs sC.OTr o K. u ► c..> PARKER N Q- i Revised: 11/04/2003 Page 4 of 6 L Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number TRANSMITTAL FORM ® _ 11301 Pursuant to 310 CMR 40.0444-0446(Subpart D) F. PERSON UNDERTAKING RAM: 1. Check all that apply: c. change in the person a.change in contact name b.change of address undertaking response actions 2. Name of Organization: MOtiva Enterprises LLC 3. Contact First Name: David B. 4.Last Name: Weeks 5. Street PMB 301, 1830 South Road, Unit 24 6.Title: Sr. Environmental Engineer 7. cityrrown: Wappingers Falls a. state: NY s. ZIP Code: 12590 10. Telephone: (845) 462-5225 11 Ext: 12 FAX 845 462-4999 G. RELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON UNDERTAKING RAM: ® 1. RP or PRP R] a. Owner b. Operator c. Generator d. Transporter e. Other RP or PRP Specify: 2. Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E.s.2) 3. Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.50)) 4. Any Other Person Undertaking RAM Specify Relationship: H.REQUIRED ATTACHMENT AND SUBMITTALS: 1.Check here if any Remediation Waste,generated as a result of this RAM,will be stored,treated,managed,recycled or reused at the site following submission of the RAM Completion Statement You must submit a Phase IV Remedy Implementation Plan along with the appropriate transmittal form(BWSC108). 2. Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order(s),permit(s) and/or approval(s)issued by DEP or EPA. If the box is checked,you MUST attach a statement identifying the applicable provisions thereof. a 3. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the implementation of a Release Abatement Measure. Ej4. Check here if any non-updatable information provided on this form is incorrect,e.g. Release Address/Location Aid. Send corrections to the DEP Regional Office. ❑ 5. If a RAM Compliance Fee is required for this RAM,check hereto certify that a RAM Compliance Fee was submitted to DEP,P.O.Box 4062,Boston,MA 02211. 6. Check here to certify that the LSP Opinion containing the material facts,data,and other information is attached. Revised: 11/04/2003 Page 5 of 6 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC106 RELEASE ABATEMENT MEASURE (RAM) Release Tracking Number TRANSMITTAL FORML 1 4❑ _ 11301 Pursuant to 310 CMR 40.0444-0446(Subpart D) L CERTIFICATION OF PERSON UNDERTAIQNG RAM: 1. 1, David B. Weeks ,attest under the pains and penalties of perjury(i)that I have personally examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form,(ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true,accurate and complete,and(iii) that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. I/the person or entity on whose behalf this submittal is made am/is aware that there are significant penalties,including, but not limited to, possible fines nd imprisonment,for illfully submitting false,inaccurate,or incomplete information. 2 By: �/w � Sr. Environmental Engineer 3. Title: Signature 4. For. Motiva Enterprises LLC 5. Date: (Name of person or entity recorded in Section F) (mm/dd/yyyy) 6. Check here if the address of the person providing certification is different from address recorded in Section F. 7. Street 8. Cityrrown: 9. State: 10. ZIP Code: 11. Telephone: 12.Ext: 13. FAX: YOU MUST LEGIBLY COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Date Stamp(DEP USE ONLY:) Revised: 11/04/2003 Page 6 of 6 —_ w Geologic Services Corporation science,engineering&technology RELEASE ABATEMENT MEASURE COMPLETION REPORT FORMER TEXACO SERVICE STATION#100083 1140 IYANNOUGH ROAD HYANNIS,MASSACHUSETTS DEP RTN 4-11301 TIER IC PERMIT#100556 ACO-SE-03-3S-002 July 2004 Prepared by: Prepared for: Geologic Services Corporation Motiva Enterprises LLC 15 Bonazzoli Avenue PMB 301,1830 South Rd,Unit 24 Hudson, Massachusetts 01749 Wappingers Falls,NY 12590 (978) 568-8740 (845)462-5225 REF. #000509C Providing Environmental Management Solutions to Business and Industry Since 1982 A 100% Employee-Owned ESOP Company 15 Bonazzoli Avenue• Hudson, MA 01749 • Tel: 978.568.8740 1 800.522.8740 • Fax: 978.568.9316 www.gsc-global.com TABLE OF CONTENTS 1.0 INTRODUCTION............................................................................................................................1 2.0 BACKGROUND INFORMATION.................................................................................................1 2.1 Regulatory Status................................................................................................................1 2.2 Subject Site and Surrounding Area......................................................:...............................4 2.3 Surrounding Potential Receptors.........................................................................................5 3.0 RELEASE ABATEMENT MEASURE ACTIVITIES....................................................................6 3.1 RAM Plan Objective...........................................................................................................6 3.1.1 Hydraulic Lift Removal Activities.........................................................................6 3.1.2 Used Oil AST Removal..........................................................................................7 3.1.3 Gasoline and Diesel UST System Closure and Removal.......................................7 3.1.3.1 Soil Screening Activities........................................................................7 3.1.3.2 Soil Sample Collection and Analytical Methods...................................8 3.1.4 Fuel Oil UST Removal...........................................................................................9 3.1.4.1 Soil Sample Collection and Analytical Methods...................................9 3.1.5 Oil Water Separator Cleaning................................................................................9 3.1.6 Test Pit Advancements.........................................................................................10 3.2 Management of Remediation Waste.................................................................................10 4.0 SUMMARY AND FINDINGS......................................................................................................10 LIST OF APPENDICES Appendix A - Figures Figure 1 —Locus Plan Figure 2—Property Decommissioning Plan Figure 3 —Vicinity Plan Figure 4—In-Situ Sample Location Plan Appendix B - Photographic Documentation and Certificates of UST Destruction Appendix C - Tables Table 1 —In-Situ Soil Sample Analytical Data—Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Table 2—In-Situ Soil Sample Analytical Results—Volatile Petroleum Hydrocarbons Appendix D - Soil Laboratory Analytical Results , Appendix E - Disposal Documentation Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 1 1.0 INTRODUCTION Geologic Services Corporation(GSC)was retained by Motiva Enterprises LLC(Motiva)to observe and document excavation activities during planned underground storage tank(UST) system, fuel oil UST,waste oil UST(if present),hydraulic lift,dry well (if present)removal activities,and the advancement of test pits in the vicinity of an on-site catch basin at the former Texaco-branded Service Station#100083 located at 1140 Iyannough Road in Hyannis,Massachusetts. Please refer to Figures 1,2, and 3 in Appendix A for a depiction of the subject property and surrounding area. 2.0 BACKGROUND INFORMATION 2.1 Regulatory Status The subject property was listed by the Massachusetts Department of Environmental Protection(MA DEP)based on information reported in a December 28, 1994 2 1 E Site Assessment Report,prepared by Down Cape Engineering,Inc. (DCE)for Cooke's Restaurant located adjacent to the site at 1120 Iyannough Road,Hyannis,Massachusetts. As part of this site assessment,DCE collected groundwater samples from three monitoring wells located on the Cooke's Restaurant property. Laboratory analysis indicated the presence of benzene,toluene,and xylenes in the sample obtained from a well reported to be downgradient of the Texaco Station. The MA DEP issued release tracking number(RTN)4-11301 on April 6, 1995 in response to these findings. As a result of the 2 1 E Site Assessment of Cooke's Restaurant,the MA DEP issued a Notice of Responsibility(NOR)to Star Enterprises(Star)owner of the property located at 1140 Iyannough Road in Hyannis,Massachusetts on August 11, 1995. On October 12, 1995,Star,submitted a Phase I-Initial Site Investigation Report and Tier IC Application to MA DEP for the subject site. During the Phase I investigation,groundwater sampling results of the on-site monitoring wells revealed dissolved-phase petroleum constituents in excess of the MA DEP reportable concentrations for GW-1 groundwater standards. The MA DEP approved the Tier IC Permit Application(No. 100556)for the subject property on September 12, 1996. At this time it was determined that a Substantial Release Migration(SRM)condition may exist and the MA DEP required an Immediate Response Action(IRA)Plan to be submitted. Star submitted an assessment-only IRA Plan proposing tri-annual groundwater monitoring for a one-year period to evaluate seasonal changes in groundwater elevation and quality. A Phase lI Scope of Work(SOW)was submitted by Groundwater&Environmental Services,Inc. (GES)on July 25, 1997 for additional subsurface investigations to be completed. This work included the installation of additional monitoring wells and additional groundwater sampling. On September 18, 1998, Ref.#000509C Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 2 SAGE submitted an IRA Status report summarizing the installation of three monitoring wells and the advancement of five soil borings. Groundwater samples were collected from ten on-site monitoring wells on May 6, 1998 and analyzed for extractable petroleum hydrocarbons(EPH)and volatile petroleum hydrocarbons(VPH). Soil analytical results for this sampling event indicated concentrations of methyl- tertiary butyl ether(MtBE)above the applicable Method 1 S-1/GW-1 soil standard at soil sample locations MW-9 and SB-11. Dissolved phase petroleum constituents were detected above applicable Method 1 GW-1 standards in samples collected from all site related monitoring wells except MW-3. SAGE submitted a Modification to the Phase 11 SOW report on August 13, 1998 for the installation of off-site monitoring wells,well surveying,groundwater sampling,and a soil vapor extraction(SVE)pilot test. SAGE was unable to secure off-site access for the installation of downgradient monitoring wells. However,the SVE pilot test and groundwater sampling were completed on March 25, 1999 and June 4, 1999,respectively. SAGE indicated that the results of the SVE test were skewed due to recent construction activities that may have caused short-circuiting in the airflow diminishing the effective radius of influence. On March 4, 1999,SAGE submitted a Modification to the IRA Plan report in response to extensive excavation activities proposed at the site. The modification addressed excess soil to be generated during the installation of new pump islands and canopy foundations,and the removal and replacement of two leaching catch basins. It included a work scope for the soil testing of excavated soils,confirmatory sampling, and management of excavated soils. Approximately 556.75 tons of soil was removed from the site on March 4 and 5, 1999 for reuse at a landfill. Approximately 188.47 tons of petroleum-impacted soil was transported to an off-site disposal facility for recycling on March 24, 1999. In 1999,responsibility for the release was transferred to Motiva,which was created in the formation of a joint venture between Shell and the owners of Star. On August 22,2000, SAGE submitted a Phase II and Phase III Report. Groundwater extraction combined with soil vapor extraction technologies were selected as the remedial action alternative for achieving a permanent solution at the subject property. Following review of the Phase II and III Reports,additional delineation of the dissolved phase petroleum hydrocarbons related to the subject property was viewed to be warranted prior to the selection/implementation of a remedial action. In conjunction with the installation of the groundwater monitoring wells,pilot test air sparge(AS)and SVE wells were installed at the subject property. In March of 2001,GSC and Motiva were able to secure off-site access to abutting properties. Between March 19 and 23,2001,GSC personnel supervised the installation of four 2-inch diameter groundwater monitoring wells MW-11,MW-12,MW-13, and MW-14 at and in the vicinity of the subject property in order to further delineate petroleum impact to soil and groundwater. During groundwater monitoring well gauging and sampling activities performed on April 4,2001, approximately 0.60 feet of non-aqueous phase liquid(NAPL)(i.e.;weathered gasoline)was detected in Ref.#000509C_Rpt RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 3 monitoring well MW-9. The MA DEP was verbally notified of the presence of greater than 0.5 inches of NAPL on April 5,2001. The MA DEP subsequently assigned RTN 4-16161 to this 72-hour release condition and verbally approved passive NAPL bailing activities under an IRA. On April 12,2001,Tanknology-NDE of Springfield,Massachusetts performed a pressure tank tightness test for the gasoline UST system at the subject property. All the pressure tests performed on the UST system passed on this date. On June 8,2001,Motiva submitted a Tier IC Permit Renewal Application to the MA DEP in order to allow for the continuation of response actions under RTN 4-11301. In addition,the Tier 1C Permit application detailed the linking of RTN 4-16161 to lead RTN 4-11301. On September 27,2001,a Decision to Grant a Tier IC Permit Extension was approved by the MA DEP. On July 16,2002,the MA DEP issued a Notice of Noncompliance(NON)(NON-SE-02-3 S-0 14)to Motiva for failure to submit an administratively complete Phase II Report and Phase III Plan. IRA Status Reports were submitted to the MA DEP in March and August 2002 detailing NAPL recovery and assessment activities during the period of August 2001 through July 2002. An IRA Plan Design;Specification was also submitted to the MA DEP in August 2002 summarizing a SVE/AS pilot test and detailing a remedial design plan to treat the source area. An IRA Status Report was submitted to the MA DEP on February 21,2003 documenting the installation of the SVE/AS remedial system,NAPL recovery,and continued site assessment activities. The SVE and AS systems were activated on March 14, 2003 and April 4,2003,respectively. The SVE/AS system is currently operational. Operation and maintenance of the SVE/AS system is documented in the semi-annual IRA Status Report dated August 22, 2003 and IRA Completion Report dated February 19,2004. Motiva entered into an Administrative Consent Order(ACO)(ACO-SE-03-3S-002)with the MA DEP on February 19,2003. As part of the ACO agreement between Motiva and the MA DEP,the following regulatory deadlines were established for the subject property: Phase II-Comprehensive Site Assessment and Phase III-Remedial Action Plan-April 15,2003;Phase IV-Remedy Implementation Plan-September 30,2003;and Phase V-Remedy Operation Status-June 30,2004. A Supplemental Phase II Comprehensive Site Assessment Report(Supplemental Phase II)and Phase III-Remedial Action Plan(RAP)Addendum were submitted for the subject property on April 14, 2003. The Supplemental Phase II and Phase III-RAP Addendum documented the installation of fifty monitoring wells,eleven soil vapor extraction wells,eight air sparge wells,three monitoring point triplets, three cone penetrometer testpoint(CPT)borings,and twenty-six temporary well points during the period of October 2000 through March 2003. In addition,twenty-seven groundwater gauging events and thirteen groundwater sampling events were conducted during this time period. The selected remedial action alternative for the reduction of residual petroleum constituents on the property is the installation and Ref.#000509C_Rpt RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 4 operation of a Groundwater Extraction and Treatment system downgradient of the subject property coupled with the existing SVE/AS system in the tanlfield area. The selected remedial action alternative outside of the target areas of active remediation is monitored natural attenuation(MNA)for management of migration and eventual reduction of dissolved-phase impacts. A Tier IC Permit Extension was submitted to the MA DEP on June 10,2003 in order to allow for the continuation of response actions under RTN 4-11301. In accordance with the revisions to the MCP 310 CMR 40.0720,the Tier I Permit Extension was presumed approved on August 11,2003. The expiration date of the Tier IC Permit is September 12,2005. Based on difficulties securing access to evaluate an off-site remediation system,Motiva requested an extension for the submittal of the Phase IV-Remedy Implementation Plan(RIP). The ACO Amendment #1 dated September 18,2003 extended the Phase IV-RIP to January 31,2004. The effective date for ACO Amendment#1 is October 1,2003. The Phase IV-RIP,dated January 29,2004,detailed the proposed implementation for the off-site Groundwater Extraction and Treatment system,ongoing operation and maintenance of the on-site SVE/AS system,and continuation of MNA. In addition,the Phase IV-RIP documented the installation of one recovery well,two monitoring points,recovery well development,overburden aquifer pumping and re- injection tests,and sampling of recovery well RW-1. An IRA Completion Report was submitted to the MA DEP on February 19,2004. A RAM Plan was submitted to the MA DEP on March 16, 2004. The objective of the proposed RAM activities was to appropriately manage, and to the degree required,transport and dispose of petroleum impacted soil unearthed during the removal of the gasoline and diesel USTs, associated piping, UST system dispenser equipment, fuel oil UST,waste oil UST(if present),hydraulic lift,dry well(if present),and the advancement of test pits in the vicinity of an on-site catch basin at the subject property. 2.2 Subject Site and Surrounding Area The subject property is situated at 1140 Iyannough Road in Hyannis,Massachusetts and was formerly developed as a Texaco branded retail gasoline and automobile repair facility. The facility is currently inactive. The subject property has an area of approximately 47,916.19 square feet(1.1 acres). The majority of the site is paved with asphalt or reinforced concrete,except a small area in the southern portion of the lot,which is landscaped. The northern portion of the property is wooded and covered in gravel. The single-story station formerly housed an office area,restrooms,and three repair service bays. One 12,000 gallon gasoline UST,one 10,000 gallon gasoline UST,one 10,000 gallon diesel UST,one 8,000 gallon gasoline UST,and one 1,000 gallon fuel oil UST were removed during May 2004. The site is serviced by municipal water supply and sewer as well as underground telephone and electric service utilities. The Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 5 subject site drainage system is connected to an on-site leachfield located immediately east of the service station building. Two detention drainage basins are located approximately 80 feet southeast and 90 feet north of the convenience store,respectively. Please refer to Figures 1,2,and 3 for a depiction of the subject property and surrounding area. The surrounding area is zoned for commercial use. Cooke's Seafood Restaurant is located immediately east of the subject property. Parker's Liquor Store is located immediately west of the subject property. A commercial plaza(Festival at Hyannis)is located immediately north of the subject property. A Ramada Inn is located approximately 100 feet south of the subject property across Iyannough Road. A Cumberland Farms Gulf Station is located approximately 210 feet southwest of the subject property. 2.3 Surrounding Potential Receptors Subsurface structures within 1,000 feet of the site include half and full basements and utility conduits located along Iyannough Road,Bearses Way and Independence Drive. It should be noted that groundwater depth at the site is greater than 20 feet below grade;and thus,impact to the subsurface structures are unlikely. The closest known basement is located approximately 600 feet southwest (upgradient)of the subject property. Subsurface utility conduits located along these streets include,but are not limited to,municipal water,sewer,gas,and storm drainage. Overhead electric and telephone utilities also exist along these streets and subject site. According to the USGS Hyannis,Massachusetts Topographic Map and GSC site reconnaissance there are no schools,institutions,or environmentally sensitive receptors known to exist within 1,500 feet of the subject property. According to the USGS Hyannis,Massachusetts Topographic Map(refer to Figure 1),the closest i ` surface water bodies include an unnamed brook located approximately 1,800 feet east,Hathaway Pond located approximately 2,600 feet northwest,and Shallow Pond located approximately 3,100 feet west of the subject property. Multiple kettle ponds are located approximately 2,000 feet east of the subject property along Independence Drive. Additional ponds are located further northeast and southeast of the property. According to the flood insurance rate map produced by the Federal Emergency Management Agency,the subject property is located within an area designated as Zone C(an area of minimal flooding). According to the Massachusetts Geographic Information System(GIS),the subject property is located within a MA DEP-Approved Zone H and an EPA-designated sole source aquifer. Six municipal public groundwater supply wells are known to exist within a 1.5-mile radius of the subject property. The closest public supply well(Barnstable Fire District Well#2)is located approximately 4,000 feet northwest of the subject property. According to the Barnstable Water Company and the Barnstable Water Department, no private supply wells exist within 1,000 feet of the disposal site. The subject property and surrounding area are serviced by municipal water. Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 6 3.0 RELEASE ABATEMENT MEASURE ACTIVITIES The following sections provide documentation supporting the completion of the RAM activities at the subject site. 3.1 RAM Plan Objective A RAM Plan was submitted to the MA DEP on March 16, 2004. The objective of the proposed RAM activities was to appropriately manage, and to the degree required,transport and dispose of petroleum impacted soil unearthed during the removal of the gasoline and diesel USTs,associated piping, UST system dispenser equipment, fuel oil UST,waste oil UST(if present),hydraulic lift,dry well(if present),and the advancement of test pits in the vicinity of an on-site catch basin at the subject property. Upon further inspection,no waste oil USTs or dry wells were present on the subject property. As discussed in Section 3.1.6,the proposed test pit advancement activities were not performed. 3.1.1 Hydraulic Lift Removal Activities On April 26,2004 GSC personnel observed the removal of one underground hydraulic lift from within the.subject building former automobile service bay. Please refer to Figure 2 for the location of the former underground hydraulic lift. During these removal activities, excavated soil was field screened for volatile organic compounds(VOCs)utilizing a photoionization detector(PID)calibrated to respond in parts per million by volume(ppmv)as benzene. Field screening of the in-situ soil samples collected from within the lift excavation yielded PID responses below the instrument detection limit(<1.0 ppmv). The final size of the hydraulic lift excavation was approximately 5 feet wide, 5 feet long, and 7 feet deep. Upon removal of the hydraulic lift,all excavated soil was re-used as backfill. Visual inspection of the lift did not reveal any structural damage. Approximately 50 gallons of hydraulic fluid were drained from the lift and transported by EQ Northeast of Wrentham,Massachusetts to Northland Environmental, Inc. (Northland)of Providence,Rhode Island. The lift was transported to James G.Grant Company(Grants) of Readville, Massachusetts for disposal. Photographic documentation of the hydraulic lift removal is included in Appendix B. A total of 2 in-situ soil samples were collected from the hydraulic lift excavation on April 26, 2004. These soil samples were submitted to Accutest Laboratories, Inc. (Accutest)of Marlborough, Massachusetts for laboratory analysis of EPH via MA DEP approved methodology and Polychlorinated Bi-Phenyls(PCBs). Soil sample analytical results have been summarized on Table 1 (Appendix C). The complete soil laboratory analytical results are included as Appendix D. Ref.#000509C Rpt RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 7 3.1.2 Used Oil AST Removal One 240-gallon steel used oil AST,previously located on the southern wall of the northwest automobile service bay,was removed from the subject property on April 27, 2004. Prior to removal, Kessler confirmed that the AST was empty. Photodocumentation is included as Appendix B. 3.1.3 Gasoline and Diesel UST System Closure and Removal GSC observed the cleaning and removal of one 12,000-gallon gasoline UST,one 10,000-gallon gasoline UST,one 8,000-gallon gasoline UST,and one 10,000-gallon diesel UST on May 3 and 4,2004. Representatives on-site during UST removal activities included Lt. Donald Case Jr. of the Hyannis Fire Department(HFD) and Dimitri Gounis of GSC. The locations of the former USTs are illustrated on Figure 2. On May 4, 2004, EQ Northeast removed a total of approximately 280 gallons of residual fluid from the USTs. Prior to UST removal,Kessler Installation and Sales (Kessler)of Dedham, Massachusetts,power washed the exterior of each UST, ventilated,and inerted each UST in order to expel existing residual petroleum vapors. Once approved by the HFD,each UST was lifted from the excavation area and inspected. The four USTs were observed to be of single-walled, fiberglass construction. No visually apparent holes were found on the exterior of the four USTs. A concrete pad was encountered under the USTs at approximately 12 feet below grade. This concrete pad was left in- situ. No groundwater was encountered during the excavation activities. Following the inspection, each UST was placed in a roll-off,crushed on-site,and subsequently transported to Grants. Photographic documentation of UST removal activities along with the Certificates of Destruction for the four USTs is included as Appendix B. During the period of May 6 through 10,2004,Kessler removed associated UST piping and dispenser equipment from the subject property. Prior toxemoval,the fiberglass piping and dispenser equipment displayed no visually apparent structural failure. 3.1.3.1 Soil Screening Activities During the excavation of the gasoline and diesel USTs and associated pump dispenser equipment, a total of 26 samples from the excavated peastone and 33 soil samples were collected from the excavated and in-situ soil,and subsequently screened in the field for the presence of VOCs utilizing a PH)calibrated to respond in ppmv as benzene. The 26 headspace screening results of the peastone samples collected in the UST area revealed VOC concentrations of up to 95.6 ppmv in a sample collected from the eastern sidewall of Tank#3 (see Figure 4 in Appendix A). The 16 headspace screening results of the soil samples collected in the UST area revealed VOC concentrations of up to 68.1 ppmv in a sample collected from Ref.#000509C_Rpt RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 8 underneath Tank#1 (southern most UST). Based on PID field headspace screening results and the absence of visual/olfactory indications of petroleum impact,no over excavation of the UST area was performed. The final size of the gasoline and diesel UST excavation was approximately 57 feet in length, 33.5 feet in width,and 12 feet in depth. The 14 headspace screening results of the soil samples collected from the associated gasoline pump dispenser equipment revealed VOC concentrations of up to 226 ppmv in a sample collected from the beneath the gasoline product lines(EXCO1). As described in the RAM Plan,PID readings in excess of 100 ppmv in soil samples collected from within the UST excavation will not result in a new notification condition to MA DEP as this RAM served as appropriate documentation to manage the impacted soil related to the existing RTN 4-11301. No soil was excavated from the vicinity of soil sample EXCOI based on the potential of jeopardizing the integrity of the adjacent on-site AS/SVE remediation lines. The 3 headspace screening results of the soil samples collected from the diesel pump i dispenser and product lines revealed VOC concentrations up to 1.6 ppmv in a sample collected from beneath the diesel product line(EXC05). Based on PID field headspace screening results and the absence of visuaUolfactory an indication of petroleum impact,no over excavation in the gasoline/diesel product line and equipment area was performed. The final sizes of the pump dispenser excavation was approximately 50 feet long,28 feet wide, and 4 feet deep for the gasoline dispensers and 12 feet long, 12 feet wide, and 5 feet deep for the diesel dispenser. The gasoline and diesel product line excavations were approximately 3 feet wide and 3 to 4 feet deep. Clean material transported to the site was utilized to backfill the excavation areas. Please refer to Figure 4 for a depiction of the soil excavation limits. 3.1.3.2 Soil Sample Collection and Analytical Methods A total of 16 in-situ soil samples were collected from the four sidewalls and beneath the gasoline USTs on May 4,2004. Eight in-situ soil samples were collected from the former gasoline pump dispenser and associated product line excavations on May 6 and May 10,2004. Three in-situ soil samples were collected from the former diesel pump dispenser and associated product line excavations on May 10, 2004. Please refer to Figure 4 for the locations of these in-situ soil samples. The gasoline soil samples were submitted to Accutest for laboratory analysis of VPH via MA DEP approved methodology. The diesel soil samples were submitted to Accutest for laboratory analysis of EPH via MA DEP approved methodology. Soil sample analytical results have been summarized on Tables 1 and 2 (Appendix C). The complete soil laboratory analytical results are included as Appendix D. I Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 9 3.1.4 Fuel Oil UST Removal On May 5,2004,GSC personnel observed the removal of one fuel oil UST at the subject property. The location of the subject fuel oil UST is illustrated on Figures 2 and 4. Previous records indicated the capacity of the fuel oil UST to be 550 gallons. However, upon excavation,the fuel oil UST was determined to be a 1,000-gallon single walled fiberglass UST. The contents of the fuel oil UST were removed prior to excavation. No evidence of rust, staining,or holes were observed on the UST. No petroleum impacted soil was encountered during the excavation of the fuel oil UST. On May 7, 2004, EQ Northeast cleaned the residual from the excavated fuel oil UST. The fuel oil UST was placed in a roll-off,crushed on-site,and transported to Grants for disposal.Photographic documentation of the fuel oil UST removal activities is included as Appendix B. The final size of the fuel oil excavation was approximately 11 feet wide, 14 feet long,and 6 feet deep. 3.1.4.1 Soil Sample Collection and Analytical Methods During the fuel oil UST excavation activities on May 5, 2004,a total of five soil samples were collected from the in-situ soil,and subsequently screened in the field for the presence of VOCs utilizing a PID. The soil sample headspace screening results of the in-situ samples revealed all VOC concentrations below 1.0 ppmv. A total of five in-situ soil samples were collected from the sidewalls and bottom of the fuel oil UST excavation area on May 5,2004 and submitted to Accutest for analysis of EPH via MA DEP approved methodology. Please refer to Figure 4 for the locations of these in-situ soil samples. Soil sample laboratory results are presented on Table 1. Soil sample analytical results have been included as Appendix D. 3.1.5 Oil Water Separator Cleaning On May 7, 2004, GSC personnel observed the removal of water and sludge from the interior of the oil/water separator located southeast of the station building. Approximately 1,347 gallons of residual water/product mixture(5 gallons of which was estimated to be recovered product)was removed by EQ Northeast on May 7,2004 and transported to International Petroleum Corporation of Wilmington, Delaware for disposal. Approximately 1600 pounds of sludge was removed by EQ Northeast on this date and transported to Northland for disposal on June 3,2004. The oil/water separator will remain on site for future use, as it is part of the on-site drainage system Ref.#000509C Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 10 3.1.6 Test Pit Advancements As indicated in the RAM Plan dated March 16,2004,Motiva proposed to advance test pits in the vicinity of the on-site catch basin located on the northwest portion of the site. These test pits were not advanced due to the potential of jeopardizing the integrity of the catch basin and the adjacent AS/SVE piping. PID readings collected from in-situ soil from the northern most UST indicated no concentrations of VOCs above 1.0 ppmv. In addition,all analytical results from soil samples collected from the sidewalls and bottom of the northern most tank(Tank#4)were below laboratory detection limits. 3.2 Management of Remediation Waste As noted herein,no over-excavation activities were performed to remove petroleum impacted soil at the site. All excavated soil was re-used as backfill on the subject property. Clean fill was provided by 'h Stocchetti Road Construction of Dennis,Massachusetts to re-grade the excavation areas. On April 26, 2004,approximately 50 gallons of hydraulic oil was drained from the hydraulic lift. This hydraulic oil was placed in a DOT Style 17H drum and transported by EQ.Northeast to Northland on June 3,2004 under a Uniform Hazardous Waste Manifest. On May 7,2004,approximately 1,347 gallons of oil/water mixture was removed from the oil/water separator and transported under a Uniform Hazardous Waste Manifest to International Petroleum Corporation. Approximately 1,600 pounds of sludge was removed from the oil/water separator on May 7,2004 and transported by EQ Northeast to Northland on June 3,2004. EQ.Northeast transported approximately 250 pounds of paint related materials to Northland on June 3,2004. The paint mixture was not generated during the RAM activities,but was disposed of as part of divestment activities. Copies of the Uniform Hazardous Waste Manifests have been included as Appendix E. 4.0 SUMMARY AND FINDINGS • On April 26,2004, GSC personnel supervised the removal of one hydraulic lift from the subject property. In-situ laboratory analytical results from the hydraulic lift excavation revealed that none of the targeted petroleum analytes were detected in excess of the applicable MCP Method 1 Risk Characterization standards. • Kessler removed one 240-gallon,double walled steel,waste oil AST from within the former service bay on April 27, 2004. Ref.#000509C_Rpt_RAM Comp 07-04 Texaco Service Station#100083 Geologic Services Corporation Page 11 • On May 3 and 4,2004,Kessler removed one 10,000-gallon diesel,one 8,000-gallon gasoline,one 10,000-gallon gasoline,and one 12,000-gallon gasoline UST from the subject property. One UST post excavation in-situ soil analytical sample(Tank 1 Bottom)exhibited a concentration of MtBE in excess of the applicable MCP Method 1 Risk Characterization Soil Standards. All other in-situ laboratory analytical results for samples collected from the gasoline/diesel UST excavation revealed that none of the targeted petroleum analytes were detected in excess of the applicable MCP Method 1 Risk Characterization standards • On May 5, 2004, GSC personnel supervised the removal of one 10,000-gallon single walled fiberglass fuel oil UST from the subject property.In-situ laboratory analytical results from the fuel oil UST excavation revealed that none of the targeted petroleum analytes were detected in excess of the applicable MCP Method 1 Risk Characterization standards. • During the period of May 6 through May 10, 2004,Kessler removed piping and pump dispenser equipment associated with the former gasoline/diesel USTs. Post excavation in-situ soil laboratory analytical results indicate concentrations of MtBE,naphthalene, C5-C8 aliphatics, and/or C9-C10 aromatics above the applicable MCP Method 1 Risk Characterization Soil Standards in select soil samples(EXC01, and EXCO2)collected during the pump dispenser and piping excavation activities. All other target petroleum analytes were below the applicable MCP Method 1 Risk Characterization Soil Standards. • On May 7,2004,GSC personnel supervised the cleaning and removal of water and sludge from the on-site oil/water separator. • During the UST removal activities occurring in April and May 2004,no over-excavation of petroleum impacted material was performed. All excavated soil was reused on site as backfill. Clean fill was used to re-grade the excavation areas. The objective of this RAM(i.e.,management and removal of petroleum impacted soil and groundwater) has been met. Thus, this RAM described herein is considered complete pursuant to 310 CMR 40.0446(2). Future response actions will continue to be conducted at this site under RTN 4-11301 in accordance with 310 CMR 40.0000. Ref.#000509C Rpt RAM Comp 07-04 APPENDIX A Figures h L� S ►•. A` r1 t�\��"�fir"_] ./[����._.�� + u.r j (\��� �: ' ♦ K. � ,�� r4 `�„Y���.•fit.'!• ` �` � ~�l�� v !`�• i^�j ��L_�lt 'i►�� li.. "M y �:,� ,tom- �=. �: ti 1 � � .I rtil �-�' ��_�. •., ��-i r° t� o � � �t %i•` s �� !t, � I b 1•r' � � .�r:r�� ,rs �ie"i1; � m `�� � II'I I 1000 2000 3000 4000 Feet � \ nunnnuuu•iiiip nnnuunnnuu• UTM nnuuuuunuuu ununnnnunuu unnuuuunnuw nnununnuuuw u COORDINATES: t QUADRANGLE 1 1 LATITUDE: I LONGITUDE: I' ' ZONE 19 Notes: FIGURE 1 LOCUSPLAN •••a .pt •t • measured in meters. FORMER •r•a . •t •t • t 1 t , 1 IYANNOUGH . � ,STATION Hydrogeologists and Environmental Scientists Source: USGS •tta .tt • .tBmstable,MA Quadrangle 15 Nfinu Series - i , I TMP-120 MW-3A N , SYSTEM I ENCLOSURE �. MW 4A BUILDING MW/17 ' SB-7 -(V SOIL BORING I VE-9 MW-11 A S-5 � # DESTROYED MONITORING WELL MW-14D SVE-3 FORMER HYDRAULIC LIFT MW-141B-1 1 ® B-2 MW-7 MW-18S MW-14 S-4iic� TMP-10S . ""W-18D GROUNDWATER MONITORING WELL MW—i 4S � MW-5 _ O ®SVE-8 I O AIRSPARGE WELL SVE-2 :AS-6 MW-6 MW-8 AS-3p:,FORMER; : ®SVE-10 � + / RECOVERY WELL -UST..._:: SB-8 CPT— :,.AREA- AS-2 SB-10 ® SOIL VAPOR EXTRACTION WELL MW-9 ( 0 ®SV —6 MW—�4 / TEMPORARY MONITORING WELL SVE-1 � ..�..`.:-_ \FORMER AS MP-101 - ® CATCH BASIN/POTENTIAL DRYWELL DIESEL ` DISPENSER / MP�-2 4AS-1 SERVICE RW-1 I — -— PROPERTY BOUNDARY ISLAND MP— VE-10(& MP 102 1w M�1� AS-7S/&-7 STATION / UST UNDERGROUND STORAGE TANK MW— 0 MW-1 MW-3 , COOKERS O/W OIL/WATER �� j y CPT—t \®CB-1 SV(94 . , RESTAURANT F/0 FUEL OIL P�101 LFORMER MW-1 1 / NOTE: LOCATION OF SYSTEM ENCLOSURE ®SVE-5 F/O UST IS APPROXIMATE 17 ` ,t� 'MW-12 l rO� ® MW-2 O/W SEPARATOR 0 50 FORMER CB 3� I GASOLINE Scale in feet ` DISPENSER ISLANDS �, FIGURE 2 PROPERTY DECOMMISSIONING PLAN FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD \ HYANNIS, MASSACHUSETTS GSC REF.: 000509.02DECON CHECKED BY: DRAFTED BY: SAC DATE: 8412 02 REVISED BY: ANG DATE: 6 11 04 GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE �. Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue • Hudson,MA 01749 •(978)568-8740 COMMERCIAL PIER 1 GRAVEL PAYLESS O PITS W � BLOCKBUSTER Q Q) JENNY 1ATTRESS CRAIG GIANT FR IENOC Y S '�� OuVE RD Q oSEAoKE S ~ Gq EN ppD 0YS R VS DISCOUNT ./ THE RAM,4DA MAR/NE SITE �qM ES R uRPHY RgTATE �� 0 350 c OuRREL R PARKER'S S AT OIV — Scale in feet LET DISCOUNT KEY LIQUOR FIGURE 3 VICINITY PLAN — - — PROPERTY BOUNDARY FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.01 VICINB CHECKED BY: DRAFTED BY: CD DATE: 2 11 02 REVISED BY: ANG DATE: 3 27 02 (L SOURCE: SAGE ENVIRONMENTAL PLAN AND GSC FIELD C-I-p)GEOLOGIC SERVICES CORPORATION RECONNAISSANCE Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue • Hudson, MA 01749 •(978)568-8740 SB-7 ' N ' SVE-3 SVE-9 ® ® O ®CB-2 MW-7 1 — LIFT BOTT OAS-4 * AS-5 KEY 2- LIFT ESW SB-1 1 MW-5 3- TANK 4 NORTHEAST ' OAS-6 ®SVE-8 SOIL BORING 4- TANK 4 NORTHWEST / MW-8 * DESTROYED MONITORING WELL 5- TANK 4 WEST SVE-2® MW_6 FORMER HYDRAULIC LIFT 6— TANK 3 WEST _ : .: — FORME 8 7- TANK 2 WEST AS-30 ;t�ST ®SVE-10 GROUNDWATER MONITORING WELL 8- TANK 1 WEST AREA _ _- SB-10 MW-9 , O AIRSPARGE WELL 9- TANK 1 SOUTHWEST .... 10- TANK 1 SOUTHEAST CPT- 1 AS02 ' RECOVERY WELL 1 1 - TANK 1 EAST - ® ®SVE-6 MW-4 SVE-1 1 S-8'''Q' = MP-101 I SOIL VAPOR EXTRACTION WELL 12- TANK 2 EAST �•.. 13- TANK 3 EAST FORMER A TEMPORARY MONITORING WELL 14- TANK 4 EAST DIESEL �.. ® RW-1 15- TANK 4 BOTTOM DISPENSER ► AS-1 MP-102 I ES CATCH BASIN/POTENTIAL DRYWELL ' — PROPERTY BOUNDARY 16- TANK 3 BOTTOM ISLAND MP-2 O AS-7 SERVICE BOTTOM ®SVE- 1 O / UNDERGROUND STORAGE TANK 18— TANK 1 BOTTOM �—3� MP�1 � SV® 7 ®0 STATION UST UNDERG OU D 0/W OIL/WATER 19- FOUSTBOTT MW_1 I 20- FOUSTNW .® ' F/O FUEL OIL 21 - FOUSTEW MW-10* SVE-4 ' NOTE: LOCATION OF SYSTEM ENCLOSURE 22- FOUSTEW CPT-2, ®CB-1 ® ® MW-3� I IS APPROXIMATE 23- FOUSTWW 24- NE DISP BOTT TMP-10\ FORMER� ' MW-11 0 OFPROXIMATE EXXCAVATIONREA '���• ., I 25- SE DISP BOTT SVE-5 F/O UST 26— SW DISP BOTT \® ' 27— NW DISP BOTT \ 28— EXC01 29— EXCO2 SB-9 30 EXC03 \: O ' 0 30 31 — EXC04 \� � 32— EXC05 MW-12 I Scale in feet ``B® 33— EXC06 MW-2 I FIGURE 4 34- D DISP BOTT FORMER �\ r IN-SITU SOIL SAMPLE LOCATION PLAN GASOLINE \ \ / FORMER TEXACO SERVICE STATION #100083 DISPENSER-, 1140 IYANNOUGH ROAD ISLANDS HYANNIS, MASSACHUSETTS GSC REF.: 000509.021NSITU CHECKED BY: ' DRAFTED BY: SAC DATE: 8 12 02 REVISED BY: ANG DATE: 6 11 04 j � GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE Hydrogeologists and Environmental Scientists 15 Bonazzoli Avenue • Hudson, MA 01749 • (978)568-8740 APPENDIX B Photographic Documentation and Certificates of UST Destruction t�.. V � d SlSI 4��F��'1 �U'.}�"91r n f V�'�i�y�K g.� 4{h �� f �9 �u r'i� L`; flY.7A" :7 L�'•�� 4'��.' stir '�' �+ r:'� t,Id'�I" � ,� �,�c �i �.;� ��'°. t �r�,A° �q r'�,r;�n �7 n �•`� .L'; '�1' 9; Ih R'' ".7�,f�rc�..,� '14!'"�l�' '�,qr r>F;' h", ✓����'�a�'Fv >..?f:ti.; :� t ,:�°5.1�, `;gr� �a� �tr? �� � S ".x r�ti� 'd�,.'Yu�R3 l ';�4 C 3� � h. �• x �'r�aM ��' �AtY SL �(�.�� J 3 r,, .�, ,.:,�"�U,.t„����i�y'S'��1 A��: •fJ � If%3ti.h..,�t5;a+ n���1,��'� *t� , a�fz� { � � ��'�'4 �4�t�4` 5 �,y. )' •�¢,•/u .��.1 i l"'� �flyM [t;8 hi fir � .��",� '• � r :`^ w �Rat, ,�r "' b Ln. ''" ..m �" r , ..^fi'�� ' � 4 4 4� l M•'^q' ��".•.. 0 ���'~ �l�7Ra ��M�1M1� �' rF N ya f1 ,ry n;, 4^�� �„�. i• ti b ��ddl y rs lrw���r E��b}������ ��� �t 4 1 roil t����p�3y��cj � •✓y. 1'G r r o ;. �*a-yrt µ .. ¢ OW I V'i ,yA e 9t a �r , A (ANY r � v�Dt�I�x k� �✓{ '" �r Atli rr�� �� ��� iYrAI' r y � ' PHOTOGRAPHIC DOCUMENTATION FORMER • SERVICE STATION #100083 • IYANNOUGH ROAD CHECKED BY: M-W D- .fNy� as NU + g 4 4s s a VIEW OF GASOLINE UNDERGROUND STORAGE TANK EXCAVATION-5/3/04 y� W4 �� � h x a� z h.- POST-EXCAVATION VIEW OF GASOLINE UNDERGROUND STORAGE TANK #1 -5/4/04 PHOTOGRAPHIC DOCUMENTATION FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.05PHOTO CHECKED BY: 01 DRAFTED BY: ANG DATE: 6 14 04 REVISED BY: DATE: GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE Hydrogeologists and EnArommntal Scientists Ir qnn li n­ . u-4— ann n17An. 107QI FRG_A7An ..1 POST-EXCAVATION VIEW OF GASOLINE UNDERGROUND STORAGE TANK #3-5/4/04 �I 3 T. S: �t K 6` mP POST-EXCAVATION VIEW OF GASOLINE UNDERGROUND STORAGE TANK #4-5/4/04 PHOTOGRAPHIC DOCUMENTATION FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.06PHOTO CHECKED BY: )h DRAFTED BY: ANG DATE: 6 14 04 REVISED BY: DATE: GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE Hvdrogeologists and Environmental Scientists 1S a,,.—li A—no—. u..4— WA n+7Ana 1070\RAO-07An POST—EXCAVATION VIEW OF DIESEL UNDERGROUND STORAGE TANK #2Y-5/4/04 v r y � v L VIEW OF FUEL OIL UNDERGROUND STORAGE TANK EXCAVATION—5/5/04 PHOTOGRAPHIC DOCUMENTATION FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.07PHOTO CHECKED BY:rmn to DRAFTED BY: ANG DATE: 6 14 04 REVISED BY: DATE: j � GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE Hydrogeologists and Environmental Scientists w..ac.... hAA n17nn. f070119a07nn z x a � r `' .•. �r POST-EXCAVATION VIEW OF FUEL OIL UNDERGROUND STORAGE TANK-5/5/04 x,i VIEW OF GASOLINE DISPENSER ISLAND EXCAVATION-5/7/04 PHOTOGRAPHIC DOCUMENTATION FORMER TEXACO SERVICE STATION #100083 1140 IYANNOUGH ROAD HYANNIS, MASSACHUSETTS GSC REF.: 000509.08PHOTO CHECKED BY: Pj . DRAFTED BY: ANG DATE: 6 14 04 REVISED BY: DATE: GEOLOGIC SERVICES CORPORATION SOURCE: GSC FIELD RECONNAISSANCE `j Hydrogeologists and EnWonn-ental Scientists 1F[inns-.-lnli A--so• Nn.4- KAA A17AOm 107M;=-07AA P - ` \�U ? -� rP A' m S F �.si! .T �;. ..'+tom^'•a.* 'y _, _ fir ' ' �t: f �r i 1 {�`j` •� b 3 � �'i 6..�'�ey�4y� F� _ -+sue-Y 111 1. 1•` • • 1 : ® • • ••••e' • Ofelmill I WROM I Is I in R sell E ., P ► v 20XPT 0 PHOTOGRAPHIC DOCUMENTATION FORMER • SERVICE STATION010: 1 IYANNOUGH ROAD REVISED : • May 21 04 08: 45a Kessler Installation 781 326 3189 p. 2 k:> VcA4%4>K 4 57m Seugeed - %w 4 tlse State 7me W aTdd RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK F.—FP'91 NAME AND ADDRESS OF APPROVED TANK YARD )�licS i. �4�S3e Co., IGC.. 7$)Wolcotl St. --- Readvil,d, MA 02137 - APPROVED TANK YARD NO. UO£'>_ Tank Yard Ledger 502 CMR 3.03(4)Number: OW'l 1 1 9y 1 I certlty under penalty of law I have personally examined the underground steel storage tank delivered to lnis 'approved rank yard"by firm,Corporation o: —..c partnership_ F��_- _ and accepted same In conformance with Massachusetts Fife Prevention Regulation 5 02 CMR 3.0/0 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL tread of Fife Oepanment FDIDu C —t— _ 2 2— to transport this lank to this yard. N a It of approved tank yard owner or owners authorized representative: 1. IG ATURE TITLE _ ATE SIGNED n �/ Thi: ned receipt of disposal must be returned to the local head of the fire department FDID# n )_ 9 pursuant to 502 CMR 3.00. EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK DATA TANK REMOVED FROM Gallons 101I020 G U� AWW . o-and Strcet) Previous Contents GAS Pm Diameter. AW th —(Cfq-or-Town) Date Received '-5 S 0 .. _ - Fire Department Permit# Serial#(if available) Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form (FP290, or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road, Stow, MA 01775. May 20 04 05: 37p Kessler Installation 781 326 3189 p. 4 w Do t 4 7W .S - aC sWe 7f4e Vie 0 RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK F.-F P?u i NAME AND ADDRESS OF APPROVED TANK YARD ilaEiies G.Gfant C0 , Inc.. ?S WO)COtl S1. u ea6villc, NIA 02137 APPROVED TANK YARD NO #008 Tank Yard Ledger 502 CMR 3.03(4)Number: 200 3`i7`�0 I certify under penalt of law I have personally examined the underground steel storage tank delivered to this"approved tank yard"by film.corporation or partnersnip ;( -SSL-�- and accepted same in rnnfnrmance with Massachusetts Fire Prevenbon Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL Head of Fire Department. y Z FDIDa ..i 2 to transport this tank to this yard. -- -- Name and offippi litle of approved tank yard owner or owners authorized representative: tt SIGNATURE TITLE DATE SIGNED J This signed receipt of disposal must be returned to the local head of the fire department FDID# 0 1 Cl L Z pursuant to 502 CMR 3 00 EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK DATA TANK REMOVED FROM Gallons ICI QOQ l lg0 a 000(' 1 RD o.and Street) Previous Contents GAS Diameter Length (City or Town) Date Received y+�S 10 9 Fire Department Permit# b� Serial#(if available) Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form (FP290, or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road, Stow, MA 01775. Mad 20 04 05: 37p Kessler Installation 781 32G 3189 p. 2 D�ta� Seaufeee - f e tle SC4& 7me W awe RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK Form FP 291 NAME AND ADDRESS OF APPROVED TANK YARD y�r3GS �xG3llt CO., YQC• 21;'Wolcott St. p,p,aCvjlle, MA 02137 U={=i 1'10 S APPROVED TANK YARD NO. 008 Tank Yard Ledger 502 CMR 3.03(4)Number: 2G _ I certify under penalty of law I have personally examined the underground steel storage tank delivered to this"approved tank yard"by firm.corporation or partnership S)..F=-{Z and accepted same in conformance with Massachusetts Fire Prevention Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL Head of Fire Department_ FDIDrt _J- to transport this tank to this yard. Name and officia We of approved tank yard owner or owners authorized representative: r b --SIGNATURE T11LETE SIGNED ca This signed receipt of disposal must be returned to the local head of the fire department FDIDN U � f � pursuant to 502 CMR 3.00 EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK DATA TANK REMOVED FROM Gallons 8WO IIgO S�ANOUGH 1, Previous Contents GA 5 (No.and Street) ��AhY�T.S Diameter _ Length — (City or Town) Date Received 55 Q _ Fire Department Permit# Serial#(if available) Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form(FP290,or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road,Stow, MA 01775. May 20 04 05: 38p Kessler Installation 781 326 3189 p. 5 U.'r, Dena t 7Gre tlse State 7uce Xzu"' RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK Form FP 291 NAME AND ADDRESS OF APPROVED TANK YARD G` 6``I'f-co ."111C. WO1C011 St. E:e�clvle, !v1 y 02137 APPROVED TANK YARD NO. ik008 ------_Tank Yard Ledger 502 CMR 3.03(4)Number: -9-7 102 I certify under penalty of law I have personally examined the underground steel storage tank delivered to this"approved tank yard"by firm.corporation or partnership =SSLFR- and accepted same in conformance with Massachusetts Fire Prevention Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL Head of Fire Department. FDID# i �� 2- 2- to transport this tank to this yard. Name and official title of approved tank yard owner or owners authorized representalive: u i'• DATE SIGNED SIQNATURE TITLE J q This signed receipt of disposal must be returned to the local head of the fire department FDID0_Q _ — _! _ __pursuant to 502 CMR 3.00. EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK REMOVED FROM TANK DATA Gallons I OOQ TWO AHOOG�1 reef (No.and St ) Previous Contents - ANNS S �Diameter Length _ (City or Town) Date Received '-- 5 0 -Fire Department Permit# 01-503 Serial#(if available) Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form (FP2909 or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road, Stow, MA 01775. May 20 04 05: 37p Kessler Installation 781 326 3189 p. 3 Dena t �7ae .9m a a - O� 4 Ilse St4& lure Xzldd RECEIPT OF DISPOSAL OF UNDERGROUND STEEL STORAGE TANK Form FP for NAME AND ADDRESS OF APPROVED TANK YARD iata-ties Gi_ Grant CO,,YIICo 2Q W01COtt St- Ri ,adv9l@e, MA02137 APPROVED TANK YARD NO. #008 Tank Yard Ledger 502 CMR 3.03(4)Number: i certify under penally of law I have personally examined the underground steel storage lank delivered to this"approved lank yard"by firm,corporation or partnership .�`��G� _ _and accepted same in conformance with Massachusetts Fire Prevention Regulation 502 CMR 3.00 Provisions for Approving Underground Steel Storage Tank dismantling yards. A valid permit was issued by LOCAL Head of Fire Department. FDID# 1 _ 9 (�— to transport this tank to this yard. Name end officiPTilJe of approved tank yard owner or owners authorized representative: SIGNATURE TITLE G7 DATE SIGNED This signed receipt of disposal must be returned to the local head of the fire department FDID#Q 1 + / Z pursuant to 502 CMR 3 00 EACH TANK MUST HAVE A RECEIPT OF DISPOSAL TANK DATA TANK REMOVED FROM Gallons 1,DM W :1Ai mk Zi (No.and Street) Previous Contents #2 qN µzS Diameter Length (City or Tow„) Date Received LSIS Fire Department Permit# Aspc3 Serial#(if available) Tank I.D.#(Form FP-290) Owner/Operator to mail revised copy of Notification Form(FP290, or FP290R) to : UST Compliance, Office of the State Fire Marshal, P.O. Box 1025 State Road, Stow, MA 01775. APPENDIX C Tables Table 1 Page 1 of I In-Situ Soil Sample Analytical Data-Polynuclear Aromatic and Extractable Petroleum Hydrocarbons Former Texaco Service Station#100083 1140Iyannough Road Hyannis,MA April 26,2004 through May 10,2004 Sample Date Depth Acenaph Acenaph Anthra- Benzo(a) B(a)P B(b)F Benzo(g,h,i)-B(k)F Chrysene Dibenz(a,h) Fluor- Fluoren ndeno(1,2,3-cd) 2-Methyl- Naph- Phen- Pyrene Cq-Cis C�9-Cr6 C„-C22 ID thene thylene cene anthracene perylene anthracene anthene pyrene naphthalene thalene anthrene Aliphatics Aliphatics Aromatics (feet) (u€1g) (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) (ug g) (u€1g) (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) (ug/g) (aR1g) MCP Soil Standard S-1/GW-I 20 100 1000 0.7 0.7 0.7 1000 7.0 7.0 0.7 1000 400 0.7 4.0 4.0 700 700 1000 2500 200 MCP Soil Standard S-1/GW-2 1000 100 1000 0.7 0.7 0.7 1000 7.0 7.0 0.7 1000 1000 0.7 500 100 1000 700 1000 2500 800 MCP Soil Standard S-1/GW-3 1000 100 1000 0.7 1 0.7 0.7 1000 7.0 7.0 0.7 1000 1000 0.7 500 100 100 700 1000 2500 800 MCP Soil Standard S-2/GW-1 20 100 1 2500 1.0 0.7 1.0 2500 10 1 10 1 0.7 2000 400 1.0 4.0 1 4.0 700 2500 2500 5000 200 MCP Soil Standard S-2/GW-2 2500 2500 2500 1.0 0.7 1.0 2500 10 10 0.7 2000 2000 1.0 1000 1000 2500 2500 2500 5000 2000 MCP Soil Standard S-2/GW-3 2500 1000 2500 1.0 0.7 1.0 2500 10 10 0.7 1000 2000 1.0 1000 1000 100 2500 2500 5000 2000 MCP Soil Standard S3/GW-1 20 100 5000 4.0 0.7 4.0 2500 40 40 0.8 2000 400 4.0 4.0 4.0 700 1000 5000 5000 200 MCP Soil Standard S3/GW-2 5000 2500 5000 4.0 0.7 4.0 2500 40 40 0.8 5000 5900 4.0 2000 1000 1 2500 5000 5000 5000 5000 MCP Soil Standard S-3/GW-3 1 4000 1000 5000 4.0 0.7 4.0 2500 40 40 0.8 1000 4000 4.0 1000 1000 100 5000 5000 5000 5000 LIFT BOTT 4/26/04 6-7 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 9.87 55.5 18.5 S-1/S-3/GW-1/GW3 LIFT ESW 4/26/04 3-4 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <6.1 <8.1 <17 S-1/S-3/GW-I/GW3 TANK 2 EAST 5/4/04 7 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <6.3 <8.4 <18 S-1/S-3/GW-1/GW 3 TANK 2 WEST 5/4/04 7 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <6.1 <8.2 <17 S-1/S-3/GW-1/GW 3 TANK 2 BOTTOM 5/4/04 12 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5.9 <7.9 <17 S-1/S-3/GW-1/GW 3 FOUSTBOTT 5/5/04 6-7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <6.0 <8.1 <17 S-I/S-3/GW-1/GW 3 FOUSTNW 5/5/04 3-4 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <0.49 <5.9 <7.8 <17 S-1/S-3/GW-1/GW 3 FOUSTEW 5/5/04 3-4 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <6.0 <8.0 <17 S-1/S-3/GW-I/GW3 FOUSTSW 5/5/04 3-4 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <6.0 <8.0 <17 FOUSTWW 5/5/04 3-4 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <6.4 <8.5 <18 S-1/S-3/GW-1/GW3 D DISP BOTT 5/10/04 5 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 184 104 57.6 S-1/S-3/GW-1/GW 3 EXC05 5/10/04 4 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 162 146 82.8 S-1/S-3/GW-1/GW 3 EXC06 5/10/04 4 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 <0.53 70.53 <0.53 <0.53 <0.53 <0.53 <6.4 <8.5 <18 (S-1/S-3/GW-1/GW3) Notes: ug/g-micrograms per gram(parts per million) MCP-Massachusetts Contingency Plan B(a)P-Benzo(a)pyrene B(b)F-Benzo(f)fluoranthene B(k)F-Benzo(k)fluoranthene <0.56-not detected(method detection limit included) Shading-indicates analyte exceeds MCP Method 1 Risk Characterization Soil Standards -this sample also exhibited a concentration of 0.154 ug/g Aroclor 1260 GEOLOGIC SERVICES CORPORATION 6/25/2004 science,engineering&technology Ref.#000509_Tbl_soil-pah+eph 15 Bonazzoli Ave.,Hudson,MA Table 2 Page I of I In-Situ Soil Sample Analytical Results-Volatile Petroleum Hydrocarbons Former Texaco Service Station#100083 1140Iyannough Road Hyannis,MA May 4,2004 through May 10,2004 Sample Date I Depth Benzene Toluene Ethyl- Total MtBE Naphthalene C'Cs C9-C12 i C9-C10 ID (It) (ug/g) (ug/g) benzene Xylenes (ug/g) (ug/g) Aliphatics Alipbatics Aromatics (Uwg) (Uwg) (Uwg) (Uwg) (ug g) MCP Soil Standards S-1/GW-1 10 90 80 Soo 0.3 4.0 100 1000 1 100 MCP Soil Standards S-1/GW-2 40 500 500 500 100 100 100 1000 100 MCP Soil Standards S-I/GW-3 40 500 500 500 100 100 100 1000 100 MCP Soil Standards S-2/GW-1 10 90 80 800 0.3 4.0 500 2500 100 MCP Soil Standards S-2/GW-2 60 500 1000 500 200 1000 500 2500 500 MCP Soil Standards S-2/GW-3 60 1000 500 1000 200 1000 500 2500 500 MCP Soil Standards S-3/GW-1 10 90 80 800 0.3 4.0 500 5000 100 MCP Soil Standards S-3/GW-2 100 500 2500 500 200 1000 500 5000 500 MCP Soil Standards S-3/GW-3 200 2500 5o0 2,500 200 1,000 500 5000 500 TANK 4 NORTHEAST 5/4/04 7 <0.180 <0.180 <0.180 <0.180 <0.072 <0.180 <3.6 <3.6 <3.6 (S-3/G W-1/G W-3) TANK 4 NORTHWEST 5/4/04 7 <0.190 <0.190 <0.190 <0.190 <0.075 <0.190 <3.7 <3.7 <3.7 (S-3/GW-1/GW-3) TANK I WEST 5/4/04 7 <0.210 <0.210 <0.210 <0.210 <0.083 <0.210 <4.1 <4.1 <4.1 (S-3/GW-I/GW-3) TANK 2 WEST 5/4/04 7 <0.170 <0.170 <0.170 <0.170 <0.066 <0.170 <3.3 <3.3 <3.3 (S-3/G W-I/G W-3) TANK 3 WEST 5/4/04 7 <0.210 <0.210 <0.210 <0.210 <0.086 <0.210 <4.3 <4.3 <4.3 (S-3/GW-1/GW-3) TANK 4 WEST 5/4/04 7 <0.170 <0.170 <0.170 <0.170 <0.069 <0.170 <3.4 <3.4 <3.4 (S-3/GW-1/GW-3) TANK 1 SOUTHWEST 5/4/04 7 <0.230 <0.230 <0.230 <0.230 <0.092 <0.230 <4.6 <4.6 <4.6 (S-3/GW-I/GW-3) TANK 1 SOUTHEAST 5/4/04 7 <0.200 <0.200 <0.200 <0.200 <0.081 <0.200 <4.1 <4.1 <4.1 (S-3/GW-1/GW-3) TANK I EAST 5/4/04 7 <0.210 <0.210 <0.210 <0.210 <0.084 <0.210 <4.2 <4.2 <4.2 (S-3/GW-1/GW-3) TANK 2 EAST 5/4/04 7 <0.170 <0.170 <0.170 <0.170 <0.068 <0.170 <3.4 <3.4 <3.4 (S-3/G W-I/G W-3) TANK 3 EAST 5/4/04 7 <0.210 <0.210 <0.210 <0.210 <0.084 <0.210 <4.2 <4.2 <4.2 (S-3/G W-I/G W-3) TANK 4 EAST 5/4/04 7 <0.150 <0.150 <0.150 <0.150 <0.059 <0.150 <2.9 <2.9 <2.9 (S-3/G W-1/G W-3) TANK I BOTTOM 5/4/04 12 <0.210 0.340 <0.210 <0.210 ,w56611 <0.210 12.7 6.19 6.4 (S-3/G W-1/G W-3) TANK 2 BOTTOM 514/04 12 <0.170 <0.170 <0.170 <0.170 0.096 <0.170 <3.4 <3.4 <3.4 (S-3/G W-1/G W-3) TANK 3 BOTTOM 5/4/04 12 <0.260 <0.260 <0.260 <0.260 0.207 <0.260 <5.3 <5.3 <5.3 (S-3/GW-1/GW-3) TANK 4 BOTTOM 5/4/04 12 <0.240 <0.240 <0.240 <0.240 <0.097 <0.240 <4.8 <4.8 <4.8 (S-3/GW-1/GW-3) NE DISP BOTT 5/6/04 4 <0.400 <0.400 <0.400 <0.400 <0.160 <0.400 <7.9 <7.9 <7.9 (S-3/GW-1/GW-3) SE DISP BOTT 5/6/04 4 <0.340 <0.340 <0.340 <0.340 <0.140 <0.340 <6.8 <6.8 <6.8 (S-3/GW-I/GW-3) SW DISP BOTT 5/6104 4 <0.390 <0.390 <0.390 <0.390 <0.160 <0.390 <7.8 <7.8 <7.8 (S-3/GW-1/GW-3) NW DISP BOTT 5/6/04 4 <0.380 <0.380 <0.380 <0.380 <0.150 <0.380 <75 <7.5 <7.5 (S-3/G W-1/G W-3) EXCOI 5/10/04 3 0.612 31.2 19.3 67.6 1 148M, 3.06 i12 <10 t='- (S-3/GW-1/GW-3) EXCO2 5/10/04 3.5 <0.4 19.1 14.9 72 54 0 � 81.9 y <8.0 M-22'1.5 (S-3/GW-1/GW-3) � EXC03 5/10/04 3.5 <0.390 <0.390 <0.390 <0.390 <0.150 <0.390 <7.7 <7.7 <7.7 (S-3/G W-1/G W-3) EXC04 5/10/04 1 3.5 <0.370 <0.370 <0.370 <0.370 1 0.193 1 <0.370 1 <7.4 <7.4 <7.4 (S-3/GW-1/GW-3) Notes: MtBE-methyl tert-butyl ether ug/g-micrograms per gram(parts per million) <0.2-not detected(method detection limit included) Shading-reported concentration exceeds the applicable standards MCP Soil Standard-Massachusetts Contingency Plan Method 1 Risk Characterization Standard for soil GEOLOGIC SERVICES CORPORATION 7/8/2004 science,engineering&technology Ref.#000509_Tbl_soil-vph 15 Bonazzoli Ave.,Hudson,MA APPENDIX D Soil Laboratory Analytical Results MAY 21 2004 New England OS/19/04 Tecln�cal Report far Shell Oil GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Cost Element# 707542 Accutest Job Number: M39256 Sampling Date: 05/05/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 13 uMINFI 4 Test results contained within this data package meet the requirements Zeza and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications:MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 495 Tech Center West 0 Building i ■ Marlborough,MA 01752 ■ tel:508-481-6200 0 fax:508481-7753 ■ http://www.accutest.com Accutest Laboratories Sample Summary Shell Oil Job No: M39256 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Project No: Cost Element# 707542 Sample Cohected ..._...,::i..._.._...:i Matrix Client .... ... ........... .. ... ............... Number Date Time By Received Code Type Sample ID M39256 1 05/05/04 12:00 MW 05/06/04 SO Soil FOUSTI3F)TT(6 7' ................................ 39256 05/05/04 12:05 MW 05/06/04 SO Soil FQUSTN (3 4') M39256 3 :>05/05/04 12:10 MW 05/06/04 SO Soil FOU.;STI✓W.(3 4 Ivi39256 4 05/05/04 12:15 MW 05/06/04 SO Soil FOUSTSW:(3 43 _..... ....... ......... .. _ _ _ _....... ...... .. ...... ......_..._................ .__........._.......... . .. ...... ... ......... M39256 5 <05/05/04 12:20 MW 05/06/04 SO Soil FOUSTWW(3 4'). Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTBOTT(6-7') Lab Sample ID: M39256-1 Date Sampled: 05/05/04 Matrix: SO- Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 94.1 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27769.1) 1 05/14/04 ME 05/08/04 OP7126 GPO1851 Run#2 Initial Weight Final Volume Run#1 10.6 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene ND 5W ug/kg 208-96-8 Acenaphthylene ND 500 ug/kg 120-12-7 Anthracene ND 500 ug/kg 56-55-3 Benzo(a)anthracene ND 500 ug/kg 50-32-8 Benzo(a)pyrene ND 500 ug/kg 205-99-2 Benzo(b)fluoranthene ND 500 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 500 ug/kg 207-08-9 Benzo(k)fluoranthene ND 500 ug/kg 218-01-9 Chrysene ND 500 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 500 ug/kg 206-44-0 Fluoranthene ND 500 ug/kg 86-73-7 Fluorene ND 500 ug/kg N 193-39-5 Indeno(1,2,3-cd)pyrene D 500 ug/kg 91-57-6 2-Methylnaphthalene ND 500 ug/kg 91-20-3 Naphthalene Nl? 500 ug/kg 85-01-8 Phenanthrene ND 500 ug/kg 129-00-0 Pyrene NA... 500 ug/kg CI I-C22 Aromatics (UnadJ ) `hJD 17000 ug/kg C9-C 18 Aliphatics 600 ug/kg C19-C36 Aliphatics ND 8100 ug/kg C11-C22 Aromatics NA 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ...................... 84-15-1 o-Terphenyl 79% 40-140 321-60-8 2-Fluorobiphenyl 40-140% _......> ........................ 580-13-2 2-Bromonaphthalene 56% 40-140% 3386-33-2 1-Chlorooctadecane 87.% 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTNW(3-4') Lab Sample ID: M39256-2 Date Sampled: 05/05/04 Matrix: SO- Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 97.3 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27770.1) 1 05/14/04 ME 05/08/04 OP7126 GPO1851 Run#2 Initial Weight Final Volume Run#1 10.5 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene ND 490 ug/kg 208-96-8 Acenaphthylene ND 490 ug/kg .......... ............. 120-12-7 Anthracene ND 490 ug/kg 56-55-3 Benzo(a)anthracene ND 490 ug/kg 50-32-8 Benzo(a)pyrene ND 490 ug/kg 205-99-2 Benzo(b)fluoranthene NO 490 ug/kg 191-24-2 Benzo(g,h,i)perylene Np.::_::;;:;; ;; 490 ug/kg 207-08-9 Benzo(k)fluoranthene ND 490 ug/kg 218-01-9 Chrysene ND 490 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 490 ug/kg 206-44-0 Fluoranthene ND 490 ug/kg 86-73-7 Fluorene ND 490 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 490 ug/kg 91-57-6 2-Methylnaphthalene NI? 490 ug/kg 91-20-3 Naphthalene ND;;;;:;;;;; ;: 490 ug/kg 85-01-8 Phenanthrene ND.:: 490 ug/kg 129-00-0 Pyrene .Nb..::_:_. 490 ug/kg CII-C22 Aromatics (UnadJ ) ND 17000 ug/kg C9-C18 Aliphatics ND 5900 ug/kg ND.C19-C36 Aliphatics ; > 7800 ug/kg CI I-C22 Aromatics N..D . 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 80%a 40-140% 321-60-8 2-Fluorobiphenyl 87%a 40-140% ........................ 580-13-2 2-Bromonaphthalene 67% 40-140% 3386-33-2 1-Chlorooctadecane $.2% 40-140% i ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTEW(3-4') Lab Sample ID: M39256-3 Date Sampled: 05/05/04 Matrix: SO-Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 96.3 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27771.13 1 05/14/04 ME 05/08/04 OP7126 GPO1851 Run#2 Initial Weight Final Volume Run#1 10.4 g 2.0 ml Run#2. CAS No. Compound Result RL Units Q ........................... 83-32-9 Acenaphthene ND 500 ug/kg 208-96-8 Acenaphthylene ND 500 ug/kg 120-12-7 Anthracene ND 500 ug/kg 56-55-3 Benzo(a)anthracene ND 500 ug/kg 50-32-8 Benzo(a)pyrene ND 500 ug/kg 205-99-2 Benzo(b)fluoranthene ND 500 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 500 ug/kg 207-08-9 Benzo(k)fluoranthene ND 500 ug/kg 218-01=9 Chrysene ND -:: 500 ug/kg 53-70-3 Dibenz(a,h)anthracene ND._,.__: 500 ug/kg 206-44-0 Fluoranthene ND 500 ug/kg 86-73-7 Fluorene ND 500 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 500 ug/kg 91-57-6 2-Methylnaphthalene ND 5W ug/kg 91-20-3 Naphthalene ND 500 ug/kg 85-01-8 Phenanthrene ;:.;;. 500 ug/kg ................ ........................... 129-00-0 Pyrene D500 ug/kg C11-C22 Aromatics(Unadj ) 17000 ug/kg _... . C9-C 18 Aliphatics ND 6000 ug/kg C19-C36 Aliphatics ND 8000 ug/kg CI I-C22 Aromatics ND 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ................ 84-15-1 o-Terphenyl 78% 40-140% 321-60-8 2-Fluorobiphenyl 8S% 40-140% 580-13-2 2-Bromonaphthalene 61% 40-140% 3386-33-2 1-Chlorooctadecane &0.% : >:: 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTSW(3-4') Lab Sample ID: M39256-4 Date Sampled: 05/05/04 Matrix: SO - Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 97.7 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P027772.D 1 05/14/04 ME 05/08/04 OP7126 GP01851 Run#2 Initial Weight Final Volume Run#1 10.2 g 2.0 nil Run#2 CAS No. Compound Result RL Units Q .........,................ 83-32-9 Acenaphthene .. 500 ug/kgN 208-96-8 Acenaphthylene 500 ug/kg 120-12-7 Anthracene .N13._........: < 500 ug/kg 56-55-3 Benzo(a)anthracene 500 ug/kg ........................... _.. 50-32-8 Benzo(a)pyrene ND.::. ::.;;;;.` 500 ug/kg 205-99-2 Benzo(b)fluoranthene I(I)...,.:::,;; 500 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 500 ug/kg 207-08-9 Benzo(k)fluoranthene N.D 500 ug/kg 218-01-9 Chrysene ND 500 ug/kg 53-70-3 Dibenz(a,h)anthracene Nl).—. 500 ug/kg .....................:..... ........................... _._. 206-44-0 Fluoranthene :.,:. :;:; 5W ug/kg 86-73-7 Fluorene iVD.......... ..:. 500 ug/kg .....................:..... ........................... ........................... 193-39-5 Indeno(1,2,3-cd)pyrene ND 500 ug/kg 91-57-6 2-Methylnaphthalene Np : 500 ug/kg 91-20-3 Naphthalene ND 500 ug/kg 85-01-8 Phenanthrene ND;.:. ..;:,;:.; 500 ug/kg ........:.........:........ ........................... 129-00-0 Pyrene 1ID 500 ug/kg C11-C22 Aromatics (UnadJ.) .N:D„ :--- 17000 ug/kg C9-C 18 Aliphatics ND. 6000 ug/kg C19-06 Aliphatics N...ID.,::.;;:,.;:;:;:.;< 8000 ug/kg ...............I........... ........................... C11-C22 Aromatics 17000 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... ......................... 84-15-1 o-Terphenyl 76% 40-140% 321-60-8 2-Fluorobiphenyl ::::;;:;;: :;' 40-140% 58013-2 2-Bromonaphthalene . ...- 40-140% 3386-33-2 1-Chlorooctadecane 7 % 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: FOUSTW'W (3-4') Lab Sample ID: M39256-5 Date Sampled: 05/05/04 Matrix: SO- Soil Date Received: 05/06/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 93.2 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27773.1) 1 05/14/04 ME 05/08/04 OP7126 GPO1851 Run#2 Initial Weight Final Volume Run#1 10.1 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q .............I...........1. .......................... 83-32-9 Acenaphthene ND.:..,.: :.:::< 530 ug/kg 208-96-8 Acenaphthylene ND 530 ug/kg 120-12-7 Anthracene ND 530 ug/kg 56-55-3 Benzo(a)anthracene ND 530 ug/kg 50-32-8 Benzo(a)pyrene ND 530 ug/kg 205-99-2 Benzo(b)fluoranthene ND.......:.... :. 530 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 530 ug/kg 207-08-9 Benzo(k)fluoranthene ND 530 ug/kg 218-01-9 Chrysene ND 530 ug/kg 53-70-3 Dibenz(a,h)anthracene 530 ug/kg 206-44-0 Fluoranthene ND 530 ug/kg 86-73-7 Fluorene ND 530 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 530 ug/kg 91-57-6 2-Methylnaphthalene ND - 530 ug/kg ...................................... ....................... 91-20-3 Naphthalene ND._ .. 530 ug/kg 85-01-8 Phenanthrene N...D:. :,,:::.:..:. 530 ug/kg 129-00-0 Pyrene hID 530 ug/kg C11-C22 Aromatics (UnadJ ) 'ND 18000 ug/kg C9-C18 Aliphatics ND...__. .....; 6400 ug/kg C19-C36 Aliphatics ND 8500 ug/kg CI 1-C22 Aromatics ND 18000 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... ......................... 84-15-1 o-Terphenyl 8.2% ..; 40-140% 321-60-8 2-Fluorobiphenyl 87% 40-140% 580-13-2 2-Bromonaphthalene b2% 40-140% 3386-33-2 1-Chlorooctadecane $l% 40-140% s ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MADEP EPH FORM Matrix Aqueous Soil Sediment n Other Cortamers; = SatisfactoryF1 Broken n Leaking A ueout Preservatives N/A H <=2 H > 2 Tem,= eratue Received on Ice F Received at 4 Deg. C Other Read at 2 deg C ,xtractfon;=Method = SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTBOTT(6-T) Lab ID: M39256-1 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/8/2004 5/14/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 94.1 1 N/A Unadjusted Ranges CAS# Units Result RDL (3 C11-C22 Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 500 Phenanthrene 85-01-8 ug/kg ND 500 Acenaphthene 83-32-9 ug/kg ND 500 Naphthalene 91-20-3 ug/kg ND 500 Other Target PAH Analvtes Acenaphthylene 208-96-8 ug/kg ND 500 Anthracene 120-12-7 ug/kg ND 500 Benzo(a)anthracene 56-55-3 ug/kg ND 500 Benzo(a)pyrene 50-32-8 ug/kg ND 500 Benzo(b)fluoranthene 205-99-2 ug/kg ND 500 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 500 Benzo(k)fluoranthene 207-08-9 ug/kg ND 500 Chrysene 218-01-9 ug/kg ND 500 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 500 Fluoranthene 206-44-0 ug/kg ND 500 Fluorene 86-73-7 ug/kg ND 500 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 500 Pyrene 129-00-0 ug/kg ND 500 Adiusted Ranges C9-C18 Aliphatics ug/kg ND A 6000 C19-C36 Aliphatics ug/kg ND A 8100 C11-C22 Aromatics ug/kg ND" 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 87 40-140% j o-Terphenyl % 79 40-140% 2-Fluorobiphenyl % 84 40-140% 2-Bromonaphthalene % 56 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 0 Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.37 W No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP EPH FORM Aqueous F1 Soil .d Sediment F1 Other Satisfactory Broken n Leakin Aueaus,Peserv-atrves N/A W PH<= 2 H > 2 Tem rature ` Received on Ice Received at 4 Deg.C Other I� Rec'd at 2 deg C ER t action.NlethodY SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTNW(3-4') Lab ID: M39256-2 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/8/2004 5/14/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 97.3 1 N/A Unadjusted Ranges CAS# Units Result RDL (3 C11-C22 Aromatics(Unadj.) ug/kg ND A 17000 Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 490 Phenanthrene 85-01-8 ug/kg ND 490 Acenaphthene 83-32-9 ug/kg ND 490 Naphthalene 91-20-3 ug/kg ND 490 Other Target PAH Anarvtes Acenaphthylene 208-96-8 ug/kg ND . 490 Anthracene 120-12-7 ug/kg ND 490 Benzo(a)anthracene 56-55-3 ug/kg ND 490 Benzo(a)pyrene 50-32-8 ug/kg ND 490 Benzo(b)fluoranthene 205-99-2 ug/kg ND 490 Benzo(g,h,j)perylene 191-24-2 ug/kg ND 490 Benzo(k)fluoranthene 207-08-9 ug/kg ND 490 Chrysene 218-01-9 ug/kg ND 490 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 490 Fluoranthene 206-44-0 ug/kg ND 490 Fluorene 86-73-7 ug/kg ND 490 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 490 Pyrene 129-00-0 ug/kg ND 490 Adjusted Ranges C9-C18 Aliphatics ug/kg ND A 5900 C19-C36 Aliphatics ug/kg ND" 7800 C11-C22 Aromatics ug/kg ND B 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 82 40-140% o-Terphenyl % 80 40-140% 2-Fluorobiphenyl % 87 40-140% 2-Bromonaphthalene % 67 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? 0 Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? d❑Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? V No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP EPH FORM Wfirxwt l Ni Aqueous Soil .i Sediment F1 Other Con`tarners= Satisfactory./ Broken Leaking A ueous Presety Itrvess N/A H <=2 H > 2 Tem 51 nature ' 'm. r ,. Received on Ice Received at 4 Deg. C Other V Rec'd at 2 deg C Extra+etron Nfietio SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTEW(3-4') Lab ID: M39256-3 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/8/2004 5/14/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 96.3 1 N/A Unadjusted Ranges CAS# Units Result RDL 2 C11-C22Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 500 Phenanthrene 85-01-8 ug/kg ND 500 Acenaphthene 83-32-9 ug/kg ND 500 Naphthalene 91-20-3 ug/kg ND 500 Other Target PAH Analvtes Acenaphthylene 208-96-8 ug/kg ND 500 Anthracene 120-12-7 ug/kg ND 500 Benzo(a)anthracene 56-55-3 ug/kg ND 500 Benzo(a)pyrene 50-32-8 ug/kg ND 500 Benzo(b)fluoranthene 205-99-2 ug/kg ND 500 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 500 Benzo(k)fluoranthene 207-08-9 ug/kg ND 500 Chrysene 218-01-9 ug/kg ND 500 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 500 Fluoranthene 206-44-0 ug/kg ND 500 Fluorene 86-73-7 ug/kg ND 500 indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 500 Pyrene 129-00-0 ug/kg ND 500 Adjusted Ranges C9-C18 Aliphatics ug/kg ND A 6000 C19-C36 Aliphatics ug/kg ND" 8000 C11-C22 Aromatics ug/kg ND a 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 80 40-140% o-Terphenyl % 78 40-140% 2-Fluorobiphenyl % 85 40-140% 2-Bromonaphthalene % 61 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes 2 A V qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No.Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? ❑./No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP EPH FORM n.K Aqueous F1 Soil Sediment i Other Cantatners u z SatisfactoryF1 Broken n Leakin tieous�PFeseruattves N/A H <=2 H > 2 gem"etature _. Received on Ice F1 Received at 4 Deg. C Other d Redd at 2 deg C ExtractEon.Methpd_ m: SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTSW(3-4') Lab ID: M39256-4 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/8/2004 5/14/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 97.7 1 N/A Unadiusted Ranges CAS# Units Result RDL g C11-C22 Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 500 Phenanthrene 85-01-8 ug/kg ND 500 Acenaphthene 83-32-9 ug/kg ND 500 Naphthalene 91-20-3 ug/kg ND 500 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 500 Anthracene 120-12-7 ug/kg ND 500 Benzo(a)anthracene 56-55-3 ug/kg ND 500 Benzo(a)pyrene 50-32-8 ug/kg ND 500 Benzo(b)fluoranthene 205-99-2 ug/kg ND 500 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 500 Benzo(k)fluoranthene 207-08-9 ug/kg ND 500 Chrysene 218-01-9 ug/kg ND 500 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 500 Fluoranthene 206-44-0 ug/kg ND 500 Fluorene 86-73-7 ug/kg ND 500 Indeno(1,2,3-od)pyrene 193-39-5 ug/kg ND 500 Pyrene 129-00-0 ug/kg ND 500 Adiusted Ranges C9-C18Aliphatics ug/kg ND" 6000 C19-C36Aliphatics ug/kg ND" 8000 C11-C22 Aromatics ug/kg ND" 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 79 40-140% o-Terphenyl % 76 40-140% 2-Fluorobiphenyl % 82 40-140% 2-Bromonaphthalene % 60 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range IB Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? 0 Yes ❑ No-Details Attatched Were all performancelacceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP EPH FARM Mafoce = ..., A ueous Soil Sediment Other Con`tainers:.- � Satisfactory Broken Leaking A ue°vus Pre'servatoues: N/A V pH <=2 F1 PH> 2 etlr► eratufe ,' Rec'd at 2 de C .�. Received on Ice Received at 4 Deg. C Other � s B�iacttoii`Mettiol SW846 3545 (Method for Ranges: MADEP EPH 98-1 Client ID: FOUSTWW(34') Lab ID: M39256-5 Method for Targets: MADEP EPH 98-1 Date Collected: 5/5/2004 Date Received: 5/6/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/8/2004 5/14/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 93.2 1 N/A Unadiusted Ranges CAS# Units Result RDL (q C11-C22 Aromatics(Unadj.) ug/kg ND" 18000 Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 530 Phenanthrene 85-01-8 ug/kg ND 530 Acenaphthene 83-32-9 ug/kg ND 530 Naphthalene 91-20-3 ug/kg ND 530 Other Target PAH Analvtes Acenaphthylene 208-96-8 ug/kg ND 530 Anthracene 120-12-7 ug/kg ND 530 Benzo(a)anthracene 56-55-3 ug/kg ND 530 Benzo(a)pyrene 50-32-8 ug/kg ND 530 Benzo(b)fluoranthene 205-99-2 ug/kg ND 530 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 530 Benzo(k)fluoranthene 207-08-9 ug/kg ND 530 Chrysene 218-01-9 ug/kg ND 530 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 530 Fluoranthene 206-44-0 ug/kg ND 530 Fluorene 86-73-7 ug/kg ND 530 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 530 Pyrene 129-00-0 ug/kg ND 530 Adiusted Ranges C9-C18 Aliphatics ug/kg ND A 6400 C19-C36 Aliphatics ug/kg ND" 8500 C11-C22 Aromatics ug/kg NO a 18000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 81 40-140% o-Terphenyl % 82 40-140% 2-Fluorobiphenyl % 87 40-140% 2-Bromonaphthalene % 62 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? d❑Yes ❑ No-Details Attatched Were all performancelacceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 12ACCUTEST 495 TECHNOLOGY CENTER WEST • BUILDINGONE I OB M 3 p a S6 MARLBOROUGH,MA 01752 ACCUTEST QUOTE M L a b o x a t o r i e s TEL:508-481-6200 • FAX.508-481-7753 //''s� ( CLIENT INFORMATION (, FACILITY INFORMATION7UMA AICAL INFORMATION MATRIX CODES17�'P �UFjI �(�f �J1 C�� l n I� ��DI Q�n,( J 06 DW• DRINKING N�ult 0 - PRi� —flOJECT NAME WATER ! KCI i G�V• AROUND WATER ADD ESS. LOCATION. 1)11 0 WW• WASTE (SIaS 'r V /7 7 , d O WATER CITY, p STATE ZIP PROJECT, O. SO- SOIL SL- SLUDGE PHONE#SEND RT T S - '�,/ FAX# ��, ��/�p LIO. OTHER - "��� CL�� LIQUID SOL•OTHER COLLECTION x PRESERVATION ACCUTEST �� fl„ SOLID SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLED W l`,Ut BY: $ LAB USE ONLY -1 fb 6- -a I i -3Qlo s `S FOUS oil 1 y^ m DATA TURNAROUND INFORMA;;494�A�� DATA DELIVERABLE INFORMATION a x '` COMMENTS/REMARKS 14 DAYS STANDARD APPROVED BY: ARD �'ll) �A L.V 7 DAYS RUSH O COMMERCIAL"Ell ," nr O 48 HOUR EMERGENCY ❑ DISK DELIVERABLE D OTHER O STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED AMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLE E POSSESION,INCLUDING COURIER DELIVERY RELI DISHED BY SA L DATE 1 E: RECEIVED BY: /�- gELI�ISED DATF TIM . RECEIVED BY: 2. 2. RELIN UISHEO BY: DATE TIME: , RECEIVED BY: REUNOUISHED BY: D T ME. RECEIVED BY: 3. /vr S e /f l 3. 4. 4. RELINOUISHED BY: DAtE T E: RECEIVE BY: SEAL• PRESERVE WHERE APPLICABLE ON ICF� TE PEA URC 5. g, @' �® New England MAY 2 6 200 05/25/04 ®ACCL EST Laboratories Tecvcal Report fir Shell Oil GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Cost Element#707542 Accutest Job Number: M39366 Sampling Date: 05/10/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 19 `440,M 11[epRO'� O O F Test results contained within this data package meet the requirements and of the National Environmental Laboratory Accreditation Conference Laabb Director and/or state specific certification programs as applicable. Certifications:MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 495 Tech Center West 0 Building 1 0 Marlborough,MI 01752 n tel:508481-6200■ fax:508481-7753 0 http://www.accutest_com L a b rs r a i o r i C s SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M39366 Site: GSCMA:96925028 1140 Iyannough Rd.Hyannis MA Report Date 5/25/2004 2:39:05 PM 3 Sample(s),collected on 05/10/2004 and were received at Accutest on 05/12/2004 properly preserved,at 1.5 Deg.C and intact. These Samples received an Accutest job number of M39366.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Extractables by GC By Method MADEP EPH 98-1 Matrix: SO Batch ID: OP7150 ■ All samples were extracted within the recommended method holding time. ■ All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. ■ Sample(s) M39379-1MS,M39379-1MSD,OP7150-MSMSD were used as the QC samples indicated. Wet Chemistry By Method EPA 160.3 M Matrix: SO Batch ID: GN13858 ■ Sample(s) M39386-14DUP were used as the QC samples for Solids,Percent. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M39366). Tuesday,May 25,2004 Page 1 of 1 2 Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 22 May.2003 Revision No. 3.1 Bureau of Waste Site Cleanup Final Page 13 of 30 Title: MADEP MCP Response Action Analytical Report Certification Form Man 1N �E tl%a ,e ode_ earte tf cah . � Laboratory Name: Accutest Laboratories of New England Project#: M39366 Project Location: MADEP RTN None GSCMA:96925028 1140 I annou h Rd.Hyannis MA This form provides certifications for the following data set: M39366-1,M39366-2,M39366-3 Sample Matrices: Groundwater SoiVSediment X Drinking Water Other: C' 8260E 8151A 8330 60106 7470A/1A od 8270C 8081A VPH 6020 9014M 2 tx 8082 8021 B EPH X 7000 S s ) 7196A St.'FxrR I 1560 `t.`". r � 'W'Sefffles-lbl Py _ y 84& eifi s7�0st $trawl arza An affirmative response to questions A,B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with Yes ❑ No ' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and E Yes ❑ No discuss in a narrative QC data that did not meet appropriate performance standards orguidelines? Does the analytical data included in this report meet all the requirements C for"Presumptive Certainty",as described in Section 2.0 of the MADEP 0 Yes ❑No ' document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without I] Yes ❑No ' significant modifications,as specified in Section 11.3? A response to questions E and F below is required for"Presumptive Certainty'status E Were all QC performance standards and recommendations for the Yes —No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified 121 Yes U No ' methods reported? , All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is,to the best of my knowledge and belief, accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 5/25104 3 Accutest Laboratories Sample Summary Shell Oil Job No: M39366 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Project No: Cost Element#707542 ......................................I............. SampleolXetei Matrix Client ...................... ......................:.... Number Date Time By Received Code Type Sample ID .......................... M39366-1 05/10/04 10:10 MW 05/12/04 SO Soil D D SP Bt?1T(5 ................................ M936fa- 05/10/04 10:20 MW 05/12/04 SO Soil <M393'6-3_»'> 05/10/04 10:40 M W 05/12/04 SO Soil »»:«::::<>;:>.: :>:<:»»>::» . ............... EXC( :,X.-- :<:::>s:::>:::::::::<:>:»;;:.;;;;:.;::.;:.;:.;;::;;;::.::.;:.;::.;:.;:.;:.> Soil samples reported on a dry weight basis unless otherwise indicated on result page. 4 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: D DISP BOTT(5') Lab Sample ID: M39366-1 Date Sampled: 05/10/04 Matrix: SO- Soil Date Received: 05/12/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 95.3 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25908.1) 1 05/18/04 SL 05/13/04 OP7150 GGH2375 Run#2 Initial Weight Final Volume Run#1 10.3 g 2.0 nil Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene ND ,:.:: >.; 510 ug/kg 208-96-8 Acenaphthylene ;ND:;: ......... 510 ug/kg 120-12-7 Anthracene 510 ug/kg 56-55-3 Benzo(a)anthracene ND 510 ug/kg 50-32-8 Benzo(a)pyrene :::;,:,;:,; 510 ug/kg ........................... ........................... ........................... 205-99-2 Benzo(b)fluoranthene ND 510 ug/kg 191-24-2 Benzo(g,h,i)perylene N13......,,:..: 510 ug/kg 207-0&9 Benzo(k)fluoranthene IVD........... ..:: 510 ug/kg ....:..::.................. ........................... ........................... 218-01-9 Chrysene ND 510 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 510 ug/kg 206-44-0 Fluoranthene N:D 510 ug/kg 86-73-7 Fluorene IVD::;::::::;; 510 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene N..D.__:..,,::.: :.:. 510 ug/kg ........................... ........................... ........................... 91-57-6 2-Methylnaphthalene N13 510 ug/kg 91-20-3 Naphthalene ND. _ 510 ug/kg 85-01-8 Phenanthrene 510 ug/kg ........................... 129-00-0 Pyrene ND 510 ug/kg CI I-C22 Aromatics (Unadj ) 57.90a 17000 ug/kg C9-C18 Aliphatics I8-. 00 6100 ug/kg C19-06 Aliphatics 1:n40(lQ_ 8200 ug/kg ........................... ........................... CII-C22 Aromatics 57; 00 s 17000 ug/kg ......................... CAS No. Surrogate Recoveries Run#1 Run#2 Limits 84-15-1 o-Terphenyl 90% _. .. 40-140% ......................:. ......................... 321-60 8 2-Fluorobiphenyl .... 40-140% 580-13-2 2-Bromonaphthalene XTISR.........> 40-140% 3386-33-2 1-Chlorooctadecane 72% 40-140% ND = Not detected I = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 5 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: EXCO5 (4') Lab Sample ID: M39366-2 Date Sampled: 05/10/04 Matrix: SO- Soil Date Received: 05/12/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 92.4 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25909.1) 1 05/18/04 SL 05/13/04 OP7150 GGH2375 Run#2 Initial Weight Final Volume Run#1 10.5 g 2.0 ml. Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene NIA 510 ug/kg 208-96-8 Acenaphthylene ND::: ::;::;::>:.>;<; 510 ug/kg 120-12-7 Anthracene ND 510 ug/kg 56-55-3 Benzo(a)anthracene ND 510 ug/kg 50-32-8 Benzo(a)pyrene ND 510 ug/kg 205-99-2 Benzo(b)fluoranthene NT ; 510 ug/kg 191-24-2 Benzo(g,h,i)perylene N ;::;;; ; ;; 510 ug/kg 207-08-9 Benzo(k)fluoranthene ItD 510 ug/kg 218-01-9 Chrysene 1JT 510 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 510 ug/kg 206-44-0 Fluoranthene ND < ; < 510 ug/kg 86-73-7 Fluorene N1 .;;:.:.::..:.:.::, 510 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 510 ug/kg 91-57-6 2-Methylnaphthalene ND 510 ug/kg 91-20-3 Naphthalene IVD 510 ug/kg 85-01-8 Phenanthrene Nl)-...... 5 ug/kg ........................... 129-00-0 Pyrene ND 510 ug/kg C11-C22 Aromatics(Unadj ) 8320Q. ..< 17000 ug/kg C9-C18 Aliphatics ]620:; ;.;.; 6200 ug/kg C19-06 Aliphatics 1;46000 : 8200 ug/kg CI1-C22 Aromatics 82800 17000 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 84-15-1 o-Terphenyl 7;9% :_ 40-140% 321-60-8 2-Fluorobiphenyl 82 ......:;;.: 40140% ................ 580-13-2 2-Bromonaphthalene Cfi°1i » >!` 40-140% 3386-33-2 1-Chlorooctadecane 63 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: EXCO6(4') Lab Sample ID: M39366-3 Date Sampled: 05/10/04 Matrix: SO-Soil Date Received: 05/12/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 87.3 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25910.1) 1 05/18/04 SL 05/13/04 OP7150 GGH2375 Run#2 Initial Weight Final Volume Run#1 10.7 g 2.0 nil Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene NIA NT3 530 ug/kg 208-96-8 Acenaphthylene ;;..;:.;..;..;. i: 530 ug/kg 120-12-7 Anthracene ND 530 ug/kg 56-55-3 Benzo(a)anthracene ND........:..: 530 ug/kg 50-32-8 Benzo(a)pyrene ND.:;:;:;.;:.;:;.;::;:< 530 ug/kg 205-99-2 Benzo(b)fluoranthene IT)<>< ; 530 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 530 ug/kg 207-08-9 Benzo(k)fluoranthene D 530 ug/kg 218-01-9 Chrysene NTH.;:.:.;;.;:.;:.;:;:;;; 530 ug/kg 53-70-3 Dibenz(a,h)anthracene ND;; ;_;z;: .... ug/kg 206-44-0 Fluoranthene ND;_:::;:;;:;: >;: 530 ug/kg 86-73-7 Fluorene _NI......_.... .. 530. ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene NTH............::.; 530 ug/kg 91-57-6 2-Methylnaphthalene ND; ;;;,,;;. ;:; 530 ug/kg 91-20-3 Naphthalene N;D 530 ug/kg 85-01-8 Phenanthrene N...D ..;. :: ;:. 530 ug/kg 129-00-0 Pyrene NI)..._...._::_: 530 ug/kg ...:........................ CI I-C22 Aromatics(UnadJ ) ND 18000 ug/kg C9-C18 Aliphatics ND 6400 ug/kg C19-06 Aliphatics .;;;; .. 8500 ug/kg ...._............. ........................... ........................... CI I-C22 Aromatics ND ; < ; 18000 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 84-15-1 o-Terphenyl 75%::..:::i 40-140% 321-60-8 2-Fluorobiphenyl 82%u;::::;::;::; 40-140% 580-13-2 2-Bromonaphthalene 65`k 40-140% 3386-33-2 1-Chlorooctadecane 6b% 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 MADEP EPH FORM A ueous ❑ Soil Sediment R Other pta tae Satisfactory Broken Leaking i�►. ' o se�vatV N/A PH <= 2 PH > 2 p �'a�t' i_;e,� ::.....___��' Received on Ice (-1 Received at 4 Deg. C ReC'd at 1.5 de Other .i s C m SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: D DISP BOTT(5) Lab ID: M39366-1 Method for Targets: MADEP EPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/13/2004 5/18/2004 N/A Solids: Low Dilution: High Dilution: EPH Fractionation 2-Fluorobiphenyl 9 Surrogate Standards. 2-Bromonaphthalene 95.3 1 N/A Unadjusted Ranges CAS# Units Result RDL g C11-C22 Aromatics(Unadj.) ug/kg 57900" 17000 (Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 510 Phenanthrene 85-01-8 ug/kg ND 510 Acenaphthene 83-32-9 ug/kg ND 510 Naphthalene 91-20-3 ug/kg ND 510 Other Target PAH Analvtes Acenaphthylene 208-96-8 ug/kg ND 510 Anthracene 120-12-7 ug/kg ND 510 Benzo(a)anthracene 56-55-3 ug/kg ND 510 Benzo(a)pyrene 50-32-8 ug/kg ND 510 Benzo(b)fluoranthene 205-99-2 ug/kg ND 510 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 510 Benzo(k)fluoranthene 207-08-9 ug/kg ND 510 Chrysene 218-01-9 ug/kg ND 510 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 510 Fluoranthene 206-44-0 ug/kg ND 510 Fluorene 86-73-7 ug/kg ND 510 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 510 Pyrene 129-00-0 ug/kg ND 510 Adjusted Ranges C9-C18 Aliphatics ug/kg 184000 A 6100 C19-C36 Aliphatics ug/kg 104000 A 8200 C11-C22 Aromatics ug/kg 576000 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 72 40-140% o-Terphenyl % 90 40-140% 2-Fluorobiphenyl % 87 40-140% 2-Bromonaphthalene % 71 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting in that range.C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand 8 Date 5/25/2004 MADEP EPH FORM AAaYK s � r:; Aqueous F1 Soil Fy Sediment F Other > rneas Satisfactory Broken F1 Leakin �rteQus,f'rese�rat es NIA ny pH<=2 pH> 2 Ae '� w Received on Ice Received at 4 De . C Other Rec'd at 1.5 deg C :action',...et - SW846 3545 Method for Ranges: 'MADEP EPH 98-1 Client ID: EXC05(4) Lab ID: M39366-2 Method for Targets: MADEP EPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/13/2004 5/18/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 92.4 1 N/A Unadiusted Ranges CAS# Units Result RDL Q C11-C22 Aromatics(Unadj.) ug/kg 83200" 17000 Diesel PAH Analvtes 2-Methyinaphthalene 91-57-6 ug/kg ND 510 Phenanthrene 85-01-8 ug/kg ND 510 Acenaphthene 83-32-9 ug/kg ND 510 Naphthalene 91-20-3 ug/kg ND 510 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 510 Anthracene 120-12-7 ug/kg ND 510 Benzo(a)anthracene 56-55-3 ug/kg ND 510 Benzo(a)pyrene 50-32-8 ug/kg ND 510 Benzo(b)fluoranthene 205-99-2 ug/kg ND 510 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 510 Benzo(k)fluoranthene 207-08-9 ug/kg ND 510 Chrysene 218-01-9 ug/kg ND 510 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 510 Fluoranthene 206-44-0 ug/kg ND 510 Fluorene 86-73-7 ug/kg ND 510 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 510 Pyrene 129-00-0 ug/kg ND 510 Adiusted Ranges C9-C18 Aliphatics ug/kg 162000 A 6200 C19-C36 Aliphatics ug/kg 146000 A 8200 C11-C22 Aromatics ug/kg 82800 a 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 63 40-140% o-Terphenyl % 79 40-140% 2-Fluorobiphenyl % 82 40-140% 2-Bromonaphthalene % 66 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Anatytes IZ AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature - Postition Laboratory Director Printed Name Reza Tand 9 Date 5/25/2004 MADEP EPH FORM Ma Aqueous Soil Sediment F1 Other 0oinei�s �° Satisfacto Broken F1 Leaking u `ou�iservat�ye: N/A H <=2 F1 PH>2 Received on Ice Received at 4 Deg. C Other d ReC'd at 1.5 deg C ... ._�a6__ ..::et SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: EXC06(4') Lab ID: M39366-3 Method for Targets: MADEP EPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/13/2004 5/18/2004 WA EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 87.3 1 N/A Unadiusted Ranges CAS# Units Result RDL g C11-C22 Aromatics(Unadi.) ug/kg ND" 18000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 530 Phenanthrene 85-01-8 ug/kg ND 530 Acenaphthene 83-32-9 ug/kg ND 530 Naphthalene 91-20-3 ug/kg ND 530 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 530 Anthracene 120-12-7 ug/kg ND 530 Benzo(a)anthracene 56-55-3 ug/kg ND 530 Benzo(a)pyrene 50-32-8 ug/kg ND 530 Benzo(b)fluoranthene 205-99-2 ug/kg ND 530 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 530 Benzo(k)fluoranthene 207-08-9 ug/kg ND 530 Chrysene 218-01-9 ug/kg ND 530 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 530 Fluoranthene 206-44-0 ug/kg ND 530 Fluorene 86-73-7 ug/kg ND 530 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 530 Pyrene 129-00-0 ug/kg ND 530 Adiusted Ranges C9-C18Aliphabcs ug/kg ND" 6400 C19-C36 Aliphatics ug/kg ND" 8500 C11-C22 Aromatics ug/kg ND B 18000 Surrogate Recoveries Acceptance Ranqe 1-Chlorooctadecane % 66 40-140% o-Terphenyl % 75 40-140% 2-Fluorobiphenyl % 82 40-140% 2-Bromonaphthalene % 66 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? ❑d Yes ❑ No-Details Attatched Were all performancelacceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? 0 No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature _ Postition Laboratory Director Printed Name Reza Tand 10 Date 5125/2004 Accutest Laboratories CS volatiles QC Data Summaries Includes the following where applicable: ■ Method Blank Summaries ■ Blank Spike Summaries ■ Matrix Spike and Duplicate Summaries ■ Surrogate Recovery Summaries 11 Method Blank Summary Page I of I Job Number: M39366 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP7150-MB GH25902.1) 1 05/18/04 SL 05/13/04 OP7150 GGH2375 The QC reported here applies to the following samples: Method: MADEP EPH 98-1 M39366-1, M39366-2, M39366-3 CAS No. Compound Result RL Units Q N 83-32-9 Acenaphthene D500 ug/kg 208-96-8 Acenaphthylene iD 500 ug/kg 120-12-7 Anthracene ND < 500 ug/kg 56-55-3 Benzo(a)anthracene NU' 500 ug/kg 500 ug/kg 50-32-8 Benzo(a)PYrene NI 205-99-2 Benzo(b)fluoranthene L? >> 500 ug/kg ....................... ........................... ........................... 191-24-2 Benzo(g,h,i)perylene NIJr< 500 ug/kg 207-08-9 Benzo(k)fluoranthene D> i `> 500 ug/kg 218-01-9 Chryseneil > < 500 ug/kg ........................... 53-70 3 Dibenz(a,h)anihracene '<<' 500 ug/kg 206 44-0 Fluoranthene ;. 500 ug/kg 86-73-7 Fluorene D < ;500 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene3I► 500 ug/kg 91-57-6 2-Methylnaphthalene ND:;:;:::::;;;:; :< 500 ug/kg ...::..................:... ........................... ........................... 91-20-3 Naphthalene NI3 ; 500 ug/kg 85-01-8 Phenanthrene ND 500 ug/kg 129-00-0 Pyrene hLD:::;::;.::<;::;;;:: 500 ug/kg CI I-C22 Aromatics(Unad1.) :N.D. .;:::;; ::< i:<i 17000 ug/kg C9-C18 Aliphatics ND. 6000 ug/kg C 19-C36 Aliphatics Np:::.:;:.;::::.;:: 8000 ug/kg CI I-C22 Aromatics ND.... _., 17000 ug/kg ........... CAS No. Surrogate Recoveries Limits 84-15-1 o-Terphenyl I3% ;« ; 40140% 321-60-8 2-Fluorobiphenyl 85 _:;::;;:;:;::.:; :<i 40-140% 580-13-2 2-Bromonaphthalene 68: 40-140% 3386-33-2 I-Chlorooctadecane 67%.. < 40-140% 12 -Blank Spike Summary Page 1 of 1 Job Number: M39366 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP7150-BS GH25903.1) 1 05/18/04 SL 05/13/04 OP7150 GGH2375 The W reported here applies to the following samples: Method: MADEP EPH 98-1 M39366-1, M39366-2, M39366-3 Spike BSP BSP CAS No. Compound ug/kg ug/kg % Limits 83-32-9 Acenaphthene 4950 3780 ?fz . 40-140 208-96-8 Acenaphthylene ND 40-140 120-12-7 Anthracene 4950 4350 88 '>> 40-140 56-55-3 Benzo(a)anthracene ND 40-140 50 32-8 Benzo(a)pyrene ND 40-140 205-99-2 Benzo(b)fluoranthene ND » 40-140 191-24-2 Benzo(g,h,i)perylene ND 40-140 207-08-9 Benzo(k)fluoranthene ND 40-140 218-01-9 Chrysene 4950 4520 91... 40-140 53-70-3 Dibenz(a,h)anthracene ND 40140 206-44-0 Fluoranthene ND 40-140 86-73-7 Fluorene ND 40-140 193-39-5 Indeno(1,2,3-cd)pyrene ND 40-140 91-57-6 2-Methylnaphthalene ND 40-140 91-20-3 Naphthalene 4950. 3560 72: ';> 40-140 85-01-8 Phenanthrene ND 40-140 129-00-0 Pyrene 4950 4150 ;84 ; 40-140 CI I-C22 Aromatics(Unadj.) 28100 . 50-150 a C9-C18 Aliphatics 9900 7040 ;71:;:;:;;:;; 40-140 C19-06 Aliphatics 14900 12900 87; < 40-140 CI1-C22 Aromatics ND 50-150 a CAS No. Surrogate Recoveries BSP Limits ............................ 84-15-1 o-Terphenyl s8f 40-140% 321-60-8 2-Fluorobiphenyl 87% 40-140% 580-13-2 2-Bromonaphthalene 737' .........>.; 40-140% 3386-33-2 I-Chlorooctadecane 7:3`Yo.;:.;:. 40-140% (a)Advisory control limits. 13 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M39366 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP7150-MS GH25904.D 1 05/18/04 SL 05/13/04 OP7150 GGH2375 OP7150-MSD GH25905.13 1 05/18/04 SL 05/13/04 OP7150 GGH2375 M39379-1 GH25906.13 1 05/18/04 SL 05/13/04 OP7150 GGH2375 The QC reported here applies to the following samples: Method: MADEP EPH 98-1 M39366-1, M39366-2, M39366-3 M39379-1 Spike MS MS MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD Rec/RPI 83-32-9 Acenaphthene ND 5090 3470 6$1 <;> 3620 58><> > 4< <'< 40140/5 208-96-8 Acenaphthylene ND ND ND nc........; 40-140/5. 120-12-7 Anthracene ND 5090 3960 7$`._.._, 4170 8:- $;....::;..: 40-140/5, 56-55-3 Benzo(a)anthracene ND ND ND nc :::: 40-140/5 50 2-8 Benzo a r ne 3 e ND ND ND - O ae= 4 14 . . B u 205 99 2 enzo fl oranthene ND ND ND �::.:::::::. 0-140/5 1 1-24-2 Be h i I n 9 nzo e e ND ND -N D 207-08-9 Benzo fluoranihene ND ND ND ric<>`>> 40 14 (k) `: .::.;;:.;;:.;:.; 0!5 218-01- sene - 9 C ND 5 4 090 170 44 hry 0 140/5 53-70-3 Dibenz a h anthracene ND - ( > ) ND ND n 206 44 0 Fluoranthe a ND ND ND 4040/5 86-73-7 Fluorene ND - ND » ND rie><;> 40 140/5 1 - - - 93 39 5 Indeno 1 2 3 cd rene N - ( , > )PY D ND >> N D - 7- - 91 5 6 2 Meth Ina hthalene N D ND ND < 140/5 nc> »'> 40 140 5 Y P .... 91-2 Naphthalene - 0-3 N h e ND 5 090 3210 63< << 3280 p ;G2 ; 2' ;;;<> 40 140/5 85-01-8 Phenanthrene ND ND ND jnc..::::;;:: 40-140/5 129-00-0 Pyrene ND 5090 4110 SI 4360 82. :;;:::;:;;:;: 40-140/5 CII-C22 Aromatics(Unadj.) ND 27900 30000 ?.: ...:..:.., 50-150/3 C9-C18 Aliphatics 5740 10200 12600 67 13500 73 ._._. .. 7. ........; 40-140/5 _.......... ......................... C19-06 Aliphatics 6850 15300 20200 8 21100 8. ,:, ,4 :. 40-140/5 CII-C22 Aromatics ND ND ND .:,,,nc: ;.;:; 50-150/3 CAS No. Surrogate Recoveries MS MSD M39379-1 Limits 4-1 - - Te 8 5 1 o hen >a<>< «< 84 » rP 1 83 Y °f ......:: : 40 140% 321-60-8 2-Fluorobiphenyl 87% $ :alo.....::.::::.;;.:.,$7%.. 40-140% 580-13-2 2-Bromonaphthalene 7 °lv. 70 65% 40-140% 3386-33-2 1-Chlorooctadecane 73% 70 it.... 72%0. 40-140% ...................................................................... ......_..... (a)Advisory control limits. 14 Semivolatile Surrogate Recovery Summary Page 1 of 1 Job Number: M39366 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Method: MADEP EPH 98-1 Matrix: SO Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S2 a S3 a S4 b M39366-1 GH25908.13 90 0 87.0 71 Q......:: 72.0 _....._........ __.._......: M39366-2 GH25909.D 79..(i;;;: ...... _............. M39366-3 GH25910.D 75:;0:; ; 82.0 66 :; 66.0 OP7150-BS GH25903.D 86.�....::._ 87.0 Z3_Q........_: 73.0 OP7150-MB GH25902.1) ? ,0..... 85.0 �6.&0.::--..... '67.0 OP7150-MS GH25904.13 83,0_..,:: :- 87.0 71.t)...,_._.: 73.0 OP7150-MSD GH25905.13 .84A...... ......85.0. 7a Q._; 70.0 Surrogate Recovery Compounds Limits ........................... S1 = o-Terphenyl T0.4 0% ; ........................... .......................... ........................... S2 = 2-Fluorobiphenyl () dl% ........_.........._... ................- S3 = 2-Bromonaphthalene AQ a4............ i S4 = 1-Chlorooctadecane 1.4 (a)Recovery from GC signal#1 (b) Recovery from GC signal#2 15 Accutest Laboratories IiS F©rFnS. . ' Custody Documents and Other Forms Includes the following where applicable: ■ Sample Tracking Chronicle 16 Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M39366 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Project No: Cost Element#707542 Sample Number Method Analyzed By Prepped By Test Codes ......................................................................................................... ..... . WX ..... ... .............................. . ........................... .. . ................ ....... . ............ W......... ............ .............. ... .. . ... .............. . .. ....... ...... ............................................................................. -...................................... ..............W.-.--.-- ...:. - ........... ...... ......... .................................... ....................... ...........Xw ......DIS .'W"= .. . ................. -........................ . .... .................. ....... ................................................................................................................ ....... ....................*............. M39366-1 EPA 160.3 M 13-MAY-04 OP %SOL M39366-1 MADEP EPH 98-1 18-MAY-04 05:59 SL 13-MAY-04 FC BMAEPH .......... ............ -................ - - --------- ... ...................... .................................... . ............................................................................... ...................... . . ....... ...x b .. ...... ................. .. ...... .................................. .................. .......... ............ M39366-2 EPA 160.3 M 13-MAY-04 OP %SOL M39366-2 MADEP EPH 98-1 18-MAY-04 06:39 SL 13-MAY-04 FC BMAEPH .................................................................-------- ........ ........................ .04......................... . .................................. ..... ............ .... ..................a ................ ..... ..... .. .. ... ... .............. ............. ....... ..... ..... ........ ... . ............................. ... ....... .......................... ..................................................... ...................... ...................... -,-.......... M39366-3 EPA 160.3 M 13-MAY-04 OP %SOL M39366-3 MADEP EPH 98-1 18-MAY-04 07:19 SL 13-MAY-04 FC BMAEPH Page I of 1 17 Betty Baer From: Moira Walker[mwalker@ma.gsc-global.com] Sent: Wednesday, May 12,2004 11:24 AM To: Betty Baer Subject: 1140 lyannough Rd, Hyannis Betty, GSC submitted soil samples from Texaco Station#100083 located at 1140 lyannough, Hyannis MA today and during the previous weeks. Please note that these soil samples are from a GW-1 site and therefore must have the S-1/GW-1 detection limits. Also, because it is in the state of MA,we would like the MCP CAM level of qa/qc. Please contact me at 978-568-8740 x257 should you have any questions or would like me to fax over a revised Chain of Custody. Thank you, Moira Moira Walker Geologist Geologic Services Corporation 15 Bonaaoli Avenue Hudson, MA 01749 Toll Free:800 522 8740 Tel: 978 568 8740 x257 Fax: 978 568 9316 mwalker@ma.gsc-global.com www.gsc-global.com NOTICE:This e-mail message and any attachment to this e-mail may contain_ confidential information that may be legally privileged. If you are not the intended recipient,you must not review,retransmit,convert to hard-copy, copy, use or disseminate this e-mail and any attachment to it. If you have received this e-mail in error, please notify us by return e-mail or by telephone at 978 568 8740 and delete this message. Please note that if this e-mail message contains a forwarded message or is a reply to a prior message, some or all of the contents of this message or any attachments may not have been produced by GSC. This notice is automatically appended to each e-mail message sent.from GSC. Thank you. 18 ka ®ACCUTEST 495 TECHNOLOGY CENTER WEST • BUILDING ONE M 3 3 MARLBOROUGH,MA 01752 ACCUTEST QUOTE•: L a b o r a t o r i e s TEL:508-481.6200 • FAX.508481-7753 ` '' CLIENT INFORMATION " '` FACILITY INFORMATION ANALYTICAL INFORMATION " MATRIX CODES v I S O DW• DRINKING @I '� WATER' NAME PR. EC AM ow• GROUND WATER AP9 3 U `7L/(� LOC 10 WW- WASTE 1"ItitSOYl D I / 7 / WATER. SO- SOIL CITY, r/1, STATE ZIP PRO ECT NO. SL- SLUDGE J,�K-K Cy"► C ✓ _ iI /�Irl' .(/Q. (;ostEl2.tmcv� 707SgZ of. oIL OTHER . SEND REPORT TO: L p UOUID PHONE# / 7 R ��o �7�� FAX N G - SOL•OTHER ACCUTEST COLLECTION P ES RVATIO SOLID SAMPLE 4 FIELD ID/POINT OF COLLECTION SAMPLED DATE TIME BY.. S2 z LAB USE ONLY s _xcosA l 3 y' p DATA TURNAROUND INFORMATION fi ATA DELIVERABLE INFORMATION COMMENTS/REMARKS 14 DAYS STANDARD APPROVED BY:' O STANDARD 7 DAYS RUSH O COMMENCIAL"B" e �Npa1)er .0roi hr, O 48 HOUR EMERGENCY O DISK DELIVERABLE O OTHER O STATE FDRMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX O OTHER CSPECIFY) LoC• /0 DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTEOBELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELI Y M7!1 RE OUISNEO BY SA P DAT TI E: REC IVED B REU U N BY: �A GATE TIME: RECEIVED Y: 1. (0 Q 0 1. �,' 2. N� /13iV5� IGUU 2. RELIN ISN BY: OA M : �/ RECEIVED RE UISNEDBY. DATE RE BY: 3. Gc„�,.. y a J 3. 4Z�_ . 4, RELINOUI HED BY: AT TI E: RECE ED By; SEAL• PRESERVE WHEREAPPUCABLE ON ICFy TEMPERATURE 5. 5. 0 [�j MAY 2 1 2004 ®� New England OS/19/04 �a ® l_ a u.,r f3;__ .-. .L_ `Techntcal Report for Shell Oil GSCMA:96925028 (REIMBMA) 1140 lyannough Rd., Hyannis, MA GSC PO# 16988 Accutest Job Number: M39303 Sampling Date: 05/04/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 37 4f,C�M Acco, � _ 4 Test results contained within this data package meet the requirements teza and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications:MA(M-MA136) Cr(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 495 Tech Center West■Building 1 0 Marlborough,MA 01752 ■ tel:508481-6200■ fax:508481-7753 ■ http://w-ww.accutest.com Accutest Laboratories Sample Summary Shell Oil Job No: M39303 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Project No: GSC PO# 16988 Sample Collected:; Matrix Client .... ..... .:............::.... ..._.. Number Date Time By Received Code Type Sample ID ................................ M39303-1 05/04/04 13:30 DG 05/10/04 SO Soil TANK 4 NORTHEA I'T. ................................ M39303 2 05/04/04 13:35 DG 05/10/04 SO Soil TANK 4 NORTHWEST 7' M39303;3 05/04/04 13:45 DG 05/10/04 SO Soil TANK4:VEST 7' .............................. M39303 4 05/04/04 13:50 DG 05/10/04 SO Soil TANK 3.WEST 7' .............................. M393()3:5 ><< 05/04/04 13:55 D 1 G OS/ 0/04 SO Soil TYNK_< i>VtiFES : ::>':;»>::>:>:::;<:>::«: ............ I 9303 6 05/04/04 14:00 DG 05/10104 SO Soil TANK 1 l ST?' M39303- . <; 05/04/04 14:05 DG 05/10/04 SO Soil TANK 1 SOUTHWEST? ... _...... ............... M39303 8 05/04/04 14:10 DG 05/10/04 SO Soil YANK 1 SOUTHEAST _.:........ :.._.. ._:....:...._ ............... : M393.03 4:. 1 05/04/04 14:30 DG 05/10/04 SO Soil TANK EAST?' M393034 05/04/04 14:35 DG 05/10/04 SO Soil TANK 2 EAST 7' . . .::: M39303 11 05/04/04 14:40 DG 05/10/04 SO Soil TANK 3 EAST 7 _.::. :. M3930312 05/04/04 14:45 DG 05/10/04 SO Soil TANK 4 EAST ' M39303 1;3. .;05/04/04 13:40 DG 05/10/04 SO Soil TANK 4 BOTTOM;1". Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Sample Summary (continued) Shell Oil Job No: M39303 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Project No: GSC PO# 16988 Sample Q11' tm:: _ _.__.:_.._.._.. _ Matrix Client Number Date Time By Received Code Type Sample ID t�f93U3............... 05/04/04 14:15 DG 05/10/04 SO Soil TANK 3 BOTTOM 12' M3930315 05/04/04 14:20 DG 05/10/04 SO Soil TANK 2 BO:.TTOM:12' 1VI 9303 16 05/04/04 14:25 DG 05/10/04 SO Soil TAN: 1 BOTTOlV 12' _.. . . _... .....::..... ..:....__. . Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 4 NORTHEAST 7' Lab Sample ID: M39303-1 Date Sampled: . 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 96.0 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis,MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB 14872.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 23.2 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 180 ug/kg 100-414 Ethylbenzene NU::::.:; 180 ug/kg ........................... 1634-04-4 Methyl Tert Butyl Ether ND 72 ug/kg 91-20-3 Naphthalene 180 ug/kg 108-88-3 Toluene ND _.. . 180 ug/kg m,p-Xylene IVD 180 ug/kg 95-47-6 o-Xylene ND < 180 ug/kg C5- C8 Aliphatics(Unadj.) ND .: ::.::::; 3600 ug/kg C9-C12 Aliphatics(Unadj.) ND:, :: :.:;: 3600 ug/kg C9- C 10 Aromatics(Unadj.) ND. 3600 ug/kg C5- C8 Aliphatics ND 36W ug/kg .................. ........................... C9- C12 Aliphatics ND._ . 3600 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits _.... .. ......................... 615-59-8 2,5-Dibromotoluene , 70-130% 615-59-8 2,5-Dibromotoluene 95% .._ ;.: 70-130% (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: TANK 4 NORTHWEST 7' Lab Sample ID: M39303-2 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.9 Project: GSCMA:96925028 (REIMBMA) 1140 lyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1314873.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 22.5 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 190 ug/kg 100-41 4 Ethylbenzene 11D_... ....... .: 190 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND:::;:: ::::;;: ; :: 75 ug/kg 91-20-3 Naphthalene NU. ;;. ;: 190 ug/kg 108-88-3 Toluene ND 190 ug/kg m,p-Xylene NIA 190 ug/kg 95-47-6 o-Xylene ND..,..,..:.. ' 190 ug/kg C5- C8 Aliphatics(Unadj:) N:D:,.::,.:, .;;;:; 3700 ug/kg C9-C12 Aliphatics (Unadj ) ND. ...__:. 3700 ug/kg C9- C10 Aromatics (Unadj ) N 3700 ug/kg C5-C8 Aliphatics N..I1 ;;;; 3700 ug/kg C9-C12 Aliphatics NIJ 3700 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 70-130% 615-59-8 2,5-Dibromotoluene 92%........:; 70130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 4 WEST 7' Lab Sample ID: M39303-3 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 93.2 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch. Analytical Batch Run#1 a AB14874.1) 1 05112/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 17.1 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ;ND _ _< 170 ug/kg 100-41-4 Ethylbenzene hII) 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether 1VD 69 ug/kg Tf>s 91-20-3 Naphthalene I > > 170 ug/kg 108-88-3 Toluene 1VD.. 170 ug/kg m,p-Xylene ND<< 170 ug/kg 95-47-6 o-Xylene :.: ;::;; 170 ug/kg N C5- C8 Aliphatics (Unadj.) TH>;; < 3400 ug/kg C9- C12 Aliphatics(Unadj.) hID '<>% 3400 ug/kg C9-C10 Aromatics(Unadj.) ND> >' 3400 ug/kg ... ................:.. ........................... ........................... C5- C8 Aliphatics NIA 3400 ug/kg C9- C12 Aliphatics 'N]3 = `< 3400 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene $8%a> 70-130% 615-59-8 2,5-Dibromotoluene 9i.°1.......:.;;. 70-130% ......................... ....................... (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected I = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 3 WEST 7' Lab Sample ID: M39303-4 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 89.6 Project: GSCMA:96925028(REIMBMA) 1140 lyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14875.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 20.9 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene ND 210 ug/kg 10041-4 Ethylbenzene ND__...__...`;:: 210 ug/kg 1634-044 Methyl Tert Butyl Ether ND `. 86 ug/kg .....:........:........ .: 91-20-3 Naphthalene N:b..._..,._ 210 ug/kg 108-88-3 Toluene ND 210 ug/kg m,p-Xylene . ND 210 ug/kg. 95-47-6 o-Xylene NI) 210 ug/kg C5-C8 Aliphatics(Unadj.) NI3 4300 ug/kg C9-C12 Aliphatics(Unadj ) ND 4300 ug/kg C9- C10 Aromatics(Unadj ) ND _. > 4300 ug/kg C5-C8 Aliphatics NI3:::,.,.,:. 4300 ug/kg C9-C12 Aliphatics ::.ND 4300 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 82_%._. 70-130% ......................... 615-59-8 2,5-Dibromotoluene 81i< <`i 70-130% (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 2 WEST 7' Lab Sample ID: M39303-5 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 93.5 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB 14876.D 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 17.7 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q ..............._...._... ........................... 71-43-2 Benzene N3 <; 170 ug/kg 100-41-4 Ethylbenzene 1ti�= `: <>D << 170 ug/kg .......................»... 1634-04-4 Methyl Tert Butyl Ether ND:: 66 ug/kg 91-20-3 Naphthalene NIA. 170 ug/kg 108-88-3 Toluene ND «> »'> 170 ug/kg m,p-Xylene ;;;;;;;, 170 ug/kg 95-47-6 o-Xylene ND 170 ug/kg C5-C8 Aliphatics(Unadj.) NI >< 3300 ug/kg .. ..........._ .... ........................... ........................... C9-C12 Aliphatics(Unadj.) ;ND _ 3300 ug/kg C9-C 10 Aromatics(Unadj.) ND 3300 ug/kg C5-C8 Aliphatics NI) s 3300 ug/kg C9-C12 Aliphatics NT1 3300 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ...................... 615-59-8 2,5-Dibromotoluene 9410< 70 130% 615-59-8 2,5-Dibromotoluene 98 70-130% ......................... ......................... (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 1 WEST 7' Lab Sample ID: M39303-6 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.0 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1314877.1) 1 05/12/04 DL n/a n/a GAB740 . Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 14.0 g 11.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND <s; s 210 ug/kg 100-41-4 Ethylbenzene >lD < 210 ug/kg ........:.................. ........ 1634-04-4 Methyl Tert Butyl Ether NIA:> ; 83 ug/kg 91-20-3 Naphthalene NI ; 210 ug/kg 108-88-3 Toluene N >> 210 D>' ug/kg m,p-Xylene ND> < ; 210 ug/kg 95-47-6 o-Xylene ND210 ug/kg C5- C8 Aliphatics(Unadj.) III 4100 ug/kg C9- C12 Aliphatics(Unadj ) ND 4100 ug/kg C9- C10 Aromatics (Unadj.) ND ;: : 4100 ug/kg C5-C8 Aliphatics ND< _ 4100 ug/kg C9-C12 Aliphatics 4100 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 100% 70130% ........:.............:.. 615-59-8 2,5-Dibromotoluene 10.3'%: 70-130% .................:....... ....................... (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 1 SOUTHWEST 7' Lab Sample ID: M39303-7 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 90.9 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14878.1) 1 65/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 13.2 g 11.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND > 230 ug/kg 100-41-4 Ethylbenzene N1 ;< >`` 230 ug/kg 1634-044 Methyl Tert Butyl Ether N.D. '<<<< 92 ug/kg 91-20-3 Naphthalene Nl >< ; 230 ug/kg 108-88-3 Toluene NID ;i 230 ug/kg m,p-Xylene 1iT); `> 230 ug/kg ........................... 95-47-6 o-Xylene NIl ._ 230 ug/kg C5- C8 Aliphatics(Unadj.) NT ::::_:;::;::.;::;;:<::; 4600 ug/kg C9-C12 Aliphatics(Unadj.) ND. .::.:: :;; 4600 ug/kg C9- C10 Aromatics(Unadj.) NT :; ;;::: 46W ug/kg C5-C8 Aliphatics :.Nj)-< :;:;>; 4600 ug/kg C9- C12 Aliphatics 1 1 46M ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene $9 < ;< 70-130% 615-59-8 2,5-Dibromotoluene3% 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: TANK I SOUTHEAST 7' Lab Sample ID: M39303-8 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.2 Project: GSCMA:96925028(REIMBMA) 1140 lyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14879.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 20.7 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 200 ug/kg 100-41-4 EthylbenzeneD.;;:;.;:.;:;::;;:.;; 2OD ug/kg 1634-04-4 Methyl Ten Butyl Ether NI3 81 ug/kg 91-20-3 Naphthalene ND:; > ::< 200 ug/kg 108-88-3 Toluene ;:;.;: 200 ug/kg m,p-Xylene ND_......._:;. 200 ug/kg 9547-6 o-Xylene ND 200 ug/kg C5-C8 Aliphatics(Unadj.) N:D. ..._.:: 4100 ug/kg C9-C12 Aliphatics(Unadj ) ND 4100 ug/kg C9- C10 Aromatics(Unadj.) N'D> ; ;' =4100 ug/kg C5- C8 Aliphatics NIA._...::. 4100 ug/kg C9-C12 Aliphatics N ,., . 4100 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene ...: 70-130% ................:........ ......................... 615-59-8 2,5-Dibromotoluene 70-130% (a) Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL =.Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: TANK I EAST 7' Lab Sample ID: M39303-9 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.4 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14880.D 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 19.9 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q .......................... 71-43-2 Benzene 1ID < i210 ug/kg 100-41-4 Ethylbenzene )`I <s 210 ug/kg 1634-04-4 Methyl Tert Butyl Ether N ;= 84 ug/kg 91-20-3 Naphthalene NIA ;210 ug/kg ._........._............ ........................... 108-88-3 Toluene ND ` ; 210 ug/kg m,p-Xylene 1VD>> << 210 ug/kg 95-47-6 o-Xylene ND 210 ug/kg C5- C8 Aliphatics(Unadj.) III ; ' 42W ug/kg C9-C12 Aliphatics(Unadj.) ND< ' 4200 ug/kg C9-C10 Aromatics (Unadj.) D 4200 ug/kg ...>.......,.., ...... ._..._......._. ... C5-C8 Aliphatics ND :>:< 4200 ug/kg C9- C12 Aliphatics NTH 4200 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 95;% 70-130% 615-59-8 2,5-Dibromotoluene 1::00.% ;;; 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 2 EAST 7' Lab Sample ID: M39303-10 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 92.1 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run##1 a A1314881.1) 1 05/12/04 DL n/a n/a GAB740 Run#i2 Initial Weight Final Volume Methanol Aliquot Run f/1 17.6 g 11.0 nil 100 ul Run#{2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene N;I) 170 ug/kg 10041-4 Ethylbenzene ND........... .. 170 ug/kg ...::...................... ........................... 1634-04-4 Methyl Tert Butyl Ether NDi; 68 ug/kg 91-20-3 Naphthalene NIA 170 ug/kg . . .............. ........................... 108-88-3 Toluene ND ; »` 170 ug/kg m,p-Xylene 1VD170 ug/kg 95-47-6 o-Xylene ND ;>; i 170 ug/kg C5- C8 Aliphatics(Unadj.) NIA 3400 ug/kg C9-C12 Aliphatics(Unadj.) ND ; i 3400 ug/kg C9- C10 Aromatics (Unadj.) ;:: 3400 ug/kg C5-C8 Aliphatics ND< >< 3400 ug/kg C9-C12 Aliphatics ND,.,,_;,,,,,, ;; 3400 ug/kg CAS No. Surrogate Recoveries Run// 1 Run#/2 Limits 615-59-8 2,5-Dibromotoluene 89 ; 70130% ......... ......................... 615-59-8 2,5-Dibromotoluene 33:%: 70130% ........................ (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: TANK 3 EAST 7' Lab Sample ID: M39303-11 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.4 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14882.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 13.9 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene NDi ; ; 210 ug/kg 100-414 Ethylbenzene NT) `_ 210 ug/kg ...:..:.:...............:.. ........................... ........................... 1634-04-4 Methyl Tert Butyl Ether AIT? 84 ug/kg 91-20-3 Naphthalene NTH 210 ug/kg 108-88-3 Toluene IN<3` 210 ug/kg m,p-Xylene ltl >'> 210 ug/kg 9547-6 o-Xylene NDi210 ug/kg CS-C8 Aliphatics(Unadj.) ..ND:.::....*.:—:- .............. .. 4200 ug/kg C9- C12 Aliphatics(Unadj.) D ; ; 4200 ug/kg C9- C10 Aromatics(Unadj ) tiD 4200 ug/kg C5- C8 Aliphatics il'D... 4200 ug/kg C9-C12 Aliphatics ;;::;;:;:;::; ... 4200 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $:6% ; 70-130% 615-59-8 2,5-Dibromotoluene 92: :;:. :::;: <; 70-130% .... ...... (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound i Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: TANK 4 EAST 7' Lab Sample ID: M39303-12 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 97.5 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1314883.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 19.2 g 11.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q _.._._.............. ........................ 71-43-2 Benzene ND 150 ug/kg 100-414 Ethylbenzene Nll:.:;.;..::.; 150 ug/kg .............:............. ........_._...-........ 1634-04-4 Methyl Tert Butyl Ether NIA ; > 59 ug/kg 91-20-3 Naphthalene ND 150 ug/kg 108-88-3 Toluene ND 150 ug/kg m,p-Xylene D_„.. 150 ug/kg ..... 95-47-6 o-Xylene NI> 150 ug/kg C5-C8 Aliphatics(Unadj.) .... ...:.:`i 2900 ug/kg C9-C12 Aliphatics(Unadj ) ND. . 2900 ug/kg C9-C10 Aromatics(Unadj.) h1D::;<; ;> ;> 2900 ug/kg C5-C8 Aliphatics ND::;:;::;:::;_;; ;: 29W ug/kg .. . C9-C12 Aliphatics NI3 2900 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 92% 70-130% 615-59-8 2,5-Dibromotoluene 96% 70-130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 4 BOTTOM 12' Lab Sample ID: M39303-13 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 96.3 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB14884.1) 1 05,112/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 17.2 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene NI) > 240 ug/kg 100-41-4 Ethylbenzene Nb ; 240 ug/kg 1634-044 Methyl Tert Butyl Ether NL ' ' >> 97 ug/kg NT3 91-20-3 Naphthalene 240 ug/kg 108-88-3 Toluene ND� > < 240 ug/kg m,p-Xylene 1tD <> > 240 ug/kg 95-47-6 o-Xylene N1 >< 240 ug/kg C5- C8 Aliphatics (Unadj.) NT3 >i 4800 ug/kg C9- C12 Aliphatics(Unadj.) NI) 4800 ug/kg C9- C10 Aromatics(Unadj.) T) i<< 4800 ug/kg C5-C8 Aliphatics NI <' '' 4800 ug/kg C9- C12 Aliphatics NIA. 4800 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ......................... 615-59-8 2,5-Dibromotoluene 98a; 70-130% 615-59-8 2,5-Dibromotoluene ;jn3:�?a 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 3 BOTTOM 12' Lab Sample ID: M39303-14 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 92.4 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 A1314885.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 •Initial Weight Final Volume Methanol Aliquot Run#1 16.4g 16.0m1 100u1 Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71 43-2 Benzene NiI) 260 ug/kg 100-41-4 Ethylbenzene ND:;:;::;:;:;:::;:;:::=260 ug/kg 1634-04-4 Methyl Tert Butyl Ether 2Z ; 110 ug/kg 91-20-3 Naphthalene ND:.,:.:.;::..;;;...... 260 ug/kg 108-88-3 Toluene Nv ;: ; 260 ug/kg m,p-Xylene NID 260 ug/kg ........:.................. ........... ............. 9547-6 o-Xylene ND 260 ug/kg C5- C8 Aliphatics(Unadj.) NT<i 5300 ug/kg C9-C12 Aliphatics (Unadj ) ND 5300 ug/kg C9-C10 Aromatics (Unadj.) ND ; 5300 ug/kg C5-C8 Aliphatics Nl3 5300 ug/kg C9-C12 Aliphatics ND 53W ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 95%<`;< :> 70130% 615-59-8 2,5-Dibromotoluene 99 :::::>:::::« 70-130% _....... ND = Not detected I = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 2 BOTTOM 12' Lab Sample ID: M39303-15 Date Sampled: 05/04/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 96.1 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB14886.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 16.8 g 11.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 7143-2 Benzene ND< 170 ug/kg 100414 Ethylbenzene 1ti1D` ;;; 170 ug/kg 1634-04-4 Methyl Tert Butyl Ether 98 >: s< 68 ug/kg 91-20-3 Naphthalene NI#:>:: .. 170 ug/kg 108-88-3 Toluene ND 170 ug/kg m,p Xylene n> ... 170 ug/kg 95-47-6 o-Xylene ND 170 ug/kg CS-C8 Aliphatics (Unadj.) I�ID .< 3400 ug/kg C9-C12 Aliphatics(Unadj.) D> ; ; 3400 ug/kg C9-CIO Aromatics(Unadj.) `1 ;; ; 34W ug/kg C5- C8 Aliphatics NT1.. . 3400 ug/kg C9-C12 Aliphatics ND 3400 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 1fl4% 70-130% 615-59-8 2,5-Dibromotoluene70-130% (a) Soil to methanol ratio greater than 1.25 to 1. I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 1 BOTTOM 12' Lab Sample ID: M39303-16 Date Sampled: 05/04/04 Matrix: SO-Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.8 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#/1 a A1314887.1) 1 05/12/04 DL n/a n/a GAB740 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 20.4 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene N13s;; 210 ug/kg 100-41-4 Ethylbenzene ND, 210 ug/kg 1634-04-4 Methyl Tert Butyl Ether SC6:;.:..;;;::;::;::;: 82 ug/kg 91-20-3 Naphthalene I�II1 210 ug/kg _._.. ........................... 108-88-3 Toluene 30 ;;;` 210 ug/kg m,p-Xylene NI) 210 ug/kg ........:.................. ........................... 95-47-6 o-Xylene ND 210 ug/kg CS- C8 Aliphatics(Unadj.) 13:700;;:: 4100 ug/kg C9-C12 Aliphatics (Unad1.) 1<3 :;;: ;; 4100 ug/kg C9-C10 Aromatics(Unad1 ) 400 4100 ug/kg C5-C8 Aliphatics 127f1 4100 ug/kg C9-C12 Aliphatics b9O 4100 ug/kg CAS No. Surrogate Recoveries Run#1 Run//2 Limits 615-59-8 2,5-Dibromotoluene 124% 70-130% _............. ......_............... 615-59-8 2,5-Dibromotoluene 118%< 70130% (a)Soil to methanol ratio greater than 1.25 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MADEP VPH FORM Mlatx n :'. Aqueous Soil Fy] Sediment Other Coxfatners r_ ' Satisfacto Broken � Leakin UEAItSs seati < N/A FV1 pH <=2 H> 2 Tim T`raf Received on Ice F1 Received at 4 Deg.C F1 Other d Reed at 2.7 deg C etanos Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 NORTHEAST 7' Lab ID: M39303-1 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 96 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 3600 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3600 C9-C12 Aliphatics(Unadj.) NIA ug/kg ND" 3600 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 180 Toluene 108-88-3 C5-C8 ug/kg ND 180 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 72 Benzene 7143-2 C5-C8 ug/kg ND 180 Naphthalene 91-20-3 N/A ug/kg ND 180 o-Xylene 9547-6 C9-C12 ug/kg ND 180 m,p-Xylene C9-C12 ug/kg ND 180 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 3600 I C9-C12 Aliphatics N/A ug/kg ND` 3600 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 95 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. IZ A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? RJYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑d Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 91 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM N`atnx _� Aqueous Soil FV1 Sediment F1 Other C5 ine�N SatisfactoryFyl Broken F1 Leaking rJsr`eetative . N/A W pH <=2 F1 PH>2 Received on Ice Received at 4 De- . C Other d Reed at 2.7 deg C ya n Methanol Coverin Soil. mL Methanol!-q soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 NORTHWEST 7' Lab ID: M39303-2 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.9 1 N/A Unadjusted Ranges CAS# Elution Ranqe Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/kg ND A 3700 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3700 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 3700 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 190 Toluene 108-88-3 C5-C8 ug/kg ND 190 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 75 Benzene 71-43-2 C5-C8 ug/kg ND 190 Naphthalene 91-20-3 N/A ug/kg ND 190 I o-Xylene 95-47-6 C9-C12 ug/kg ND 190 m,p-Xylene C9-C12 ug/kg ND 190 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 3700 C9-C12 Aliphatics N/A ug/kg ND` 3700 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 91Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? YJNo ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature _ Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM Aqueous Soil .r Sediment F Other C3'K Cci Satisfactory.r Broken Leakin Bois eset5at ues NIA Fy] H<=2 H> 2 R Rec'd at 2.7 d C Received on Ice Received at 4 Deg.C Other e9 M {hao Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 WEST 7' Lab ID: M39303-3 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 93.2 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 3400 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3400 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 3400 Target Analvtes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 170 Toluene 108-88-3 C5-C8 ug/kg ND 170 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg ND 69 Benzene 7143-2 C5-C8 ug/kg ND 170 Naphthalene 91-20-3 N/A ug/kg ND 170 o-Xylene 95-47-6 C9-C12 ug/kg ND 170 m,p-Xylene C9-C12 ug/kg ND 170 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 3400 C9-C12 Aliphatics N/A ug/kg ND` 3400 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 88 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CSCS Aliphatic Hydrocarbons exclude the concentration of Target Anaytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Anaytes eluting In that range AND concentration of C9C10 Aromatic Hydrocarbons. Z A'X qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 91 No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director - Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM Ma ` 01 V A_ .._s _ Aqueous Soil Sediment Other , rz � OWHGI P;s N'�- Satisfactory.i Broken n Leaking F1 Iue NIA H <=2 H> 2 att Received on Ice Received at 4 Deg. C Other V Rec'd at 2.7 deg C tVletanQ � Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 3 WEST 7' Lab ID: M39303-4 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 89.6 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 4300 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4300 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4300 Target Analytes; Ethylbenzene 100-41-4 C9-C12 ug/kg ND 210 Toluene 108-88-3 C5-C8 ug/kg ND 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 86 Benzene 71-43-2 C5-C8 ug/kg ND 210 Naphthalene 91-20-3 N/A ug/kg ND 210 o-Xylene 9547-6 C9-C12 ug/kg ND 210 m,p-Xylene C9-C12 ug/kg ND 210 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4300 C9-C12 Aliphatics N/A ug/kg ND` 4300 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 84 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of arty surrogates)and/or internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? V No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 I MADEP VPH FORM MatnX ,s;' A ueou n Soil Sediment F1 Other C�ntatne - Satisfactory V- Broken Leaking Q��piee�w:att esr N/A ny PH <=2 F1 PH> 2 rb; .Urea Received on Ice Received at 4 Deg.C FJ OtherW Rec'd at 2.7 deg C e�ranof f� Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 2 WEST 7' Lab ID: M39303-5 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution- 93.5 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL 9 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 3300 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3300 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND A 3300 Target Analytes Ethylbenzene 10041-4 C9-C12 ug/kg ND 170 Toluene 108-88-3 C5-C8 ug/kg ND 170 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg ND 66 Benzene 71-43-2 C5-C8 ug/kg ND 170 Naphthalene. 91-20-3 N/A ug/kg ND 170 i o-Xylene 95-47-6 C9-C12 ug/kg ND 170 m, X lene C9-C12 P- Y ug/kg ND 170 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 3300 C9-C12 Aliphatics . N/A ug/kg ND" 3300 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 94 70-130% PID:2,5-Dibromotoluene % 98 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-CU aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'X qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 91 Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete, Signature 111 � - Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM Nlatnz� K Aqueous n Soil Sediment F1 Other Confatnery Satisfacto Broken n Leaking ue`o€iisP ese6va a"s' N/A H <= 2 F1 PH> 2 " Received on Ice Received at 4 Deg. C Other deg C Rec'd at 2.7 N[e �iar�oh � � � Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 WEST 7' Lab ID: M39303-6 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL C3 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 4100 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4100 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4100 Target Analvtes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 210 Toluene 108-88-3 C5-C8 ug/kg ND 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 83 Benzene 71-43-2 C5-C8 ug/kg ND 210 Naphthalene 91-20-3 N/A ug/kg ND 210 o-Xylene 95-47-6 C9-C12 ug/kg ND 210 m,p-Xylene C9-C12 ug/kg ND 210 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4100 C9-C12 Aliphatics N/A ug/kg ND` 4100 Surrogate Recoveries Acceptance Range FID:25-Dibromotol'vene % 100 70-130% PID:25-Dibromotoluene % 103 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Anatytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Anatytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. z A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM ::: w Aqueous Soil Sediment Other Satisfacto Broken Leakin I=rese a trral!s NIA ny pH <=2 F1 PH> 2 -Received on Ice Received at 4 Deg. C F1 Other nV g Rec'd at 2.7 de —NOW a Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio>1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 SOUTHWEST 7' Lab ID: M39303-7 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 90.9 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL C� i C5-C8 Aliphatics(Unadj.) N/A ug/kg NO" 4600 C9-C70 Aromatics(Unadj.) N/A ug/kg ND" 4600 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4600 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 230 Toluene 108-88-3 C5-C8 ug/kg ND 230 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg ND 92 Benzene 7143-2 C5-C8 ug/kg ND 230 Naphthalene 91-20-3 N/A ug/kg ND 230 o-Xylene 9547-6 C9-C12 ug/kg ND 230 m,p-Xylene C9-C12 ug/kg ND 230 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4600 C9-C12 Aliphatics N/A ug/kg ND` 4600 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 89 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CS-CS Allphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Y qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No.Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 91Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Date 5/19/2004 Printed Name Reza Tand MADEP VPH FORM Nla % _ �: � A ueous I Soil d Sediment Other � #aine Satisfactory Broken F1 Leakin Leo s Prsettiatt'�"; NIA W PH <=2 F1 PH> 2 prat tip Received on Ice Received at 4 Deg. C Other a ReCA at 2.7 deg C Methanol Covering Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 SOUTHEAST 7' Lab ID: M39303-8 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95.2 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 4100 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4100 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4100 Target Analytes Ethylbenzene 100-414 C9-C12 ug/kg ND 200 Toluene 108-88-3 C5-C8 ug/kg ND 200 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 81 Benzene 7143-2 C5-C8 ug/kg ND 200 Naphthalene 91-20-3 N/A ug/kg ND 200 o-Xylene 95-47-6 C9-C12 ug/kg ND 200 m,p-Xylene C9-C12 ug/kg ND 200 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4100 C9-C12 Aliphatics N/A ug/kg ND` 4100 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 95 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude corn of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ©Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved?. Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM fllatriX�3 4 y -- Aqueous Soil Sediment n Other _ taiihrs �� w; SatisfactoryFyl Broken n Leaking eotisseseaiu N/A H<=2 H>2 Received on Ice Received at 4 Deg.C Other W Redd at 2.7 deg C ants ; Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 EAST 7' Lab ID: M39303-9 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95.4 1 N/A Unadiusted Ranges CAS# Elution Ranne Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 4200 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4200 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4200 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 210 Toluene 108-88-3 C5-C8 ug/kg ND 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 84 Benzene 71-43-2 C5-C8 ug/kg ND 210 Naphthalene 91-20-3 N/A ug/kg ND 210 o-Xylene 95-47-6 C9-C12 ug/kg ND 210 m,p-Xylene C9-C12 ug/kg ND 210 IAdiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4200 C9-C12 Aliphatics N/A ug/kg ND` 4200 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 95 70-130% PID:2,5-Dibromotoluene % 100 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. MCI)Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any sumrgate(s)and/or Internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. 1Z A'J'qualirrer indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 91Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? RJYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? Ri No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date - 5/19/2004 MADEP VPH FORM Aqueous Soil W Sediment Other atnecs Satisfacto Broken Leaking eas ' e�en7atiess NIA H <=2 H>2 ,c-atur. , . Received on Ice Received at 4 Deg.C Other d Rec'd at 2.7 deg C NOW . rFk „ ." Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 2 EAST 7' Lab ID: M39303-10 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A I FID: 25-Dibromotoluene %Solids: Low Dilution: High Dilution: 92.1 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 3400 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3400 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 3400 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 170 Toluene 108-88-3 C5-C8 ug/kg ND 170 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 68 Benzene 71-43-2 C5-C8 ug/kg ND 170 Naphthalene 91-20-3 N/A ug/kg ND 170 o-Xylene 95-47-6 C9-C12 ug/kg ND 170 m,p-Xylene C9-C12 ug/kg ND 170 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 3400 C9-C12 Aliphatics N/A ug/kg ND` 3400 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 89 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualiner Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? VYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No.Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM Aqueous Soil Sediment F1 Other _tafne SatisfactorvW Broken F1 Leakin N/A W pH <=2 F PH >2 > - Received on Ice n Received at 4 Deg.C Other d Rec'd at 2.7 deg C Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 3 EAST T Lab ID: M39303-11 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94-4 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 4200 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4200 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 4200 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 210 Toluene 108-88-3 C5-C8 ug/kg ND 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 84 Benzene 71-43-2 C5-C8 ug/kg ND 210 Naphthalene 91-20-3 N/A ug/kg ND 210 o-Xylene 95-47-6 C9-C12 ug/kg ND 210 m,p-Xylene C9-C12 ug/kg ND 210 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4200 C9-C12 Aliphatics N/A ug/kg ND` 4200 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 86 70-130% P0:25-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogatels)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 91 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM ati=ix -mom Aqueous FJ Soil Sediment n Other oaiii>ie � x Satisfacto Broken Leaking .F Leo sRrese ' #fie NIA pH <=2 F1 PH>2 s = Received on Ice Received at 4 Deg.C Other Rec'd at 2.7 deg C Methanol Covering Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. (Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 EAST 7' Lab ID: M39303-12 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run- PID: 2,5-Dbromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 97.5 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 2900 C9-C10 Aromatics(Unadj.) NIA ug/kg ND" 2900 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND* 2900 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 150 Toluene 108-88-3 C5-C8 ug/kg ND 150 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 59 Benzene 71-43-2 C5-C8 ug/kg ND 150 Naphthalene 91-20-3 N/A ug/kg ND 150 o-Xylene 95-47-6 C9-C12 ug/kg ND 150 m,p-Xylene C9-C12 ug/kg ND 150 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 2900 C9-C12 Aliphatics NIA ug/kg ND' 2900 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 96 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogates)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cons of Target Analytes eluting In that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A Lr qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM A ueous Soil Sediment F1 Other t>recs4= SatisfactorvW Broken n Leakin N/A W pH <=2 F1 PH> 2 ' Rec'd at 2.7 deg C Received on Ice Received at 4 De C Other v' Methanol Coverin Soil. mL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH 98-1 Client ID: TANK 4 BOTTOM 12' Lab ID: M39303-13 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 96-3 1 N/A Unadiusted Ranges CAS Al Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) WA ug/kg ND" 4800 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 4800 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND A 4800 Target Analytes Ethylbenzene 10041-4 C9-C12 ug/kg ND 240 Toluene 108-88-3 C5-C8 ug/kg ND 240 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg ND 97 Benzene 7143-2 C5-C8 ug/kg ND 240 Naphthalene 91-20-3 N/A ug/kg ND 240 o-Xylene 95-47-6 C9-C12 ug/kg ND 240 m,p-Xylene C9-C12 ug/kg ND 240 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 4800 C9-C12 Aliphatics WA ug/kg ND` 4800 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 98 70-130% PID:2,5-Dibromotoluene % 103 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range 8 Hydrocarbon Range data exclude concentrations of arry surrogate(s)and/or internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as.specified in Sect.11.3? RJ No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM 1 tlfafr`� Aqueous Soil Sediment Other Wntaine s"§R M Satisfactory Broken Leaking eAi sieseiratrE NIA pH <=2 H> 2 I P ai r '_ Received on Ice F1 Received at 4 Deg.C Other nl Rec'd at 2.7 deg C hane � Methanol Coverin Soil. mL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH 98-1 Client ID: TANK 3 BOTTOM 12' Lab ID: M39303-14 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 NIA FID: 2,5-Dibromotoluene %Solids: Low Dilution- High Dilution- 92.4 1 N/A IUnadiusted Ranges CAS# Elution Range Units Result RDL _q C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 5300 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 5300 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 5300 Target Analytes; Ethylbenzene 100-41-4 C9-C12 ug/kg ND 260 Toluene 108-88-3 C5-C8 ug/kg ND 260 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg 207 110 Benzene 71-43-2 C5-C8 ug/kg ND 260 Naphthalene 91-20-3 N/A ug/kg ND 260 o-Xylene 95-47-6 C9-C12 ug/kg ND 260 m,p-Xylene C9-C12 ug/kg ND 260 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 5300 C9-C12 Aliphatics N/A ug/kg ND` 5300 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 95 70-130% PID:2,5-Dibromotoluene % 99 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ©Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.31 PI No ❑ Yes-Details Attatched I attest under the pains and penalties of perjuty that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM Aqueous I- Soil Fy-1 Sediment rl Other t�rit`atii . ` Satisfactory Broken n Leakin NIA H<=2 F1 PH> 2 re Received on Ice Received at 4 Deg.C Other Rec'd at 2.7 deg C Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 2 BOTTOM 12' Lab ID: M39303-15 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run- PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 96.1 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) NIA ug/kg ND" 3400 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 3400 C9-C12 Aliphatics(Unadj.) WA ug/kg ND" 3400 Target Analytes Ethylbenzene 10041-4 C9-C12 ug/kg ND 170 Toluene 108-88-3 C5-C8 ug/kg ND 170 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg 95.8 68 Benzene 71-43-2 C5-C8 ug/kg ND 170 Naphthalene 91-20-3 N/A ug/kg ND 170 o-Xylene 95-47-6 C9-C12 ug/kg ND 170 m,p-Xylene C9-C12 ug/kg ND 170 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND B 3400 C9-C12 Aliphatics N/A ug/kg ND` 3400 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 104 70-130% PID:2,5-Dibromotoluene % 109 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 0 No ❑ Yes-Details Attatched attest under:the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/19/2004 MADEP VPH FORM Aqueous F1 Soil Sediment F1 Other t1a>Icte - � Satisfacto Broken Leaking �tteo seseiv� N/A pH <=2 L1 PH> 2 X ro Received on Ice Received at 4 Deg. C Other ./ Rec'd at 2J deg C `ar�o .. .. ........ Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio> 1.25 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: TANK 1 BOTTOM 12' Lab ID: M39303-16 (Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/12/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95.8 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg 13700" 4100 C9-C10 Aromatics(Unadj.) N/A ug/kg 6400 A 4100 C9-C12 Aliphatics(Unadj_) N/A ug/kg 13000" 4100 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 210 Toluene 108-88-3 C5-C8. ug/kg 340 210 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg 566 82 Benzene 71-43-2 C5-C8 ug/kg ND 210 Naphthalene 91-20-3 N/A ug/kg ND 210 o-Xylene 95-47-6 C9-C12 ug/kg ND 210 m,p-Xylene C9-C12 ug/kg ND 210 Adjusted Ranges I C5-C8 Aliphatics N/A ug/kg 12700 a 4100 C9-C12 Aliphatics N/A ug/kg 6190` 4100 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 124 70-130% PID:2,5-Dibromotoluene % 118 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range is Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. CS-CO Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? L7 Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director s Printed Name Reza Tand Date 5/19/2004 CON" aUr495 UHAIN U 5 I UUY �n 9s1tN Tech Center West,Bldg.1,Marlboro,MA 01752 1 ��tT 12ACCUTESTo (508)481-6200 Fax: (508)481-7753 Accutest Job#: M 59 3 03 ZEN Client Information i' ` Facility Information Analytical information MIMI Consultants Name Project Name Geologic Services Corporation SOPUS Hyannis Address Street 15 Bonazzoli Ave. 1140 1 anon h Rd city State 41PState Hudson MA 01749 H annis MA Project Contact: Invoice Contact: Phone#: 978-588-8740 Invoice Phone# Fax#: 978.588.9318 Location ID# 100083Q mobt l g� AFE# PO#Collect on Preservation yy Field ID/Point of Collection DatiF Time Sampled By Matrix bottleal 7s oCIA '4 OAUXA� /3 x Wa t- 71 1 Y, k W a 71 _ _ s 7(uh k f 'st X " -7 I -X I 30 x - r 3 X - -140 k - 4 7 aq �c x 2AZ —� 9. " Turnaround Information m e w Dala Deliverable information 4 x Accutest Log-in Information ®Std.14 Day Turnaround Approved By: ® Commercial"A" Q FULL CLP Q 7 Day EMERGENCY Q Commercial"B" Q State Forms rr 4 Day EMERGENCY 0 Full Dallverables Disk Deliverable Format, �M > S TT�� _ 3 Day EMERGENCY Other 2 Day EMERGENCY I-Gc. 3 v/.�.� 10A 1 Day EMERGENCY Emergency T/A Is for FAX or Labllnk Data Commercial"A"-Results Only Sample Custody must be ocumented below each time m les change osseslon,Including courle elive a m : os w nq e nqu• a mp er. a 1 ce ve Y: s to s a me: 2°eve y: 3 4 en /O�/� $ 4 a reearve w are app ica a 4 n ae C emp. u s mp er + °6° ° 6 q 5 ACCUTEST (508)481-6200 Fax: (508)481-7753 Accutest Job#: M 39 3 U 5 Client nformatlon Facility Information 1 " Analytical Consultants Name Project Name Geologic Services Corporation SOPUS Hyannis Address Street 15 Bonazzoll Ave. 1140 1 anou h Rd city S e zip city State Hudson MA 01749 Hyannis MA Project Contact: Invoice Contact: Phone#: 978-588-8740 Invoice Phone# Fax#: 978.588-9316 Location10# 100083 PO# 1b AFE# Collection Preservation s g� #of cd p g A w 10 8 Z Field ID/Point of Collection t Time Sampled By Matrix bottles " is y X X X 13 a 2 ar X k �K -! Turnaround Information ' ' ' 1' T'-�y9 r• Data Deliverable Information ' `P Accutest Lo •in In�lJormalion �C sh•.�i >fr'a' ^4 " - ®Std.14 Day Turnaround Approved By: F Commercial"A" Q FULL CLIP O v 7 Day EMERGENCY 0 Commercial"B" Q State Forms 4 Day EMERGENCY o Full Dellverables Disk Deliverable Format- 3 Day EMERGENCY Other 2 Day EMERGENCY 1 Day EMERGENCY Emergency T/A Is for FAX or Lablink Data Commercial"A"-Results Only ece vo Sam le Custod must be do umented below each time samples thane osseslon,Including er de e ` •:a a e me: y: P R u s amp er: a e o: R. v y: s e -�o- 2 q • amp or: a e: oae vo y: e q s e n a e me: ece ve y: 3 o r /o:/S 3 4 4 e nqu y amp e. e o: eao y: ea reserve w ere app oa e n ae C eTP• 0 MAY 2 1 2004 New England 05/18/04 12 ® L it-� .. _.. Techntcat Report for Shell Oil GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA . GSC PO# 16988 Accutest Job Number: M39301 Sampling Date: 05/06/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 11 4EC♦K ACCpRC Test results contained within this data package meet the requirements eza Znd of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications:MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England■ 495 Tech Center West■ Building 1 0 Marlborough,MA 01752 ■ tel: 508-481-6200 ■ fax:508-481-7753 ■http://www.accutest.com Accutest Laboratories Sample Summary Shell Oil Job No: M39301 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Project No: GSC PO# 16988 Sample Collect..................... ....... Number Date Time By Received Code Type Sample ID M39301 ;1 05/06/04 14:50 MW 05/10/04 SO Soil NE ?ISP gQTT(4 J _...... M393012 05/06/04 15:00 MW 05/10/04 SO Soil SE DTSP BOIT(4') ............................... M393013 05/06/04 15:05 MW 05/10/04 SO Soil ...SW:.:DISP BOTT(4') ............................... M39301 4 05/06/04 15:10 MW 05/10/04 SO Soil NW WISP 107:7 (4') Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: NE DISP BOTT(4') Lab Sample ID: M39301-1 Date Sampled: 05/06/04 Matrix: SO - Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.9 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a QR27554.1) 1 05/13/04 AA n/a n/a GQR1346 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 10.6 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 400 ug/kg 100-41-4 Ethylbenzene ..ND.: 400 ug/kg 1634-04-4 Methyl Tert Butyl Etherp;,:;.:<:.:, : 160 ug/kg 91-20-3 Naphthalene NU-. .; 400 ug/kg 108-88-3 Toluene N:17;::; ;:..... 400 ug/kg m,p-Xylene I�IID::.:..;;;:.:.::; 400 ug/kg 95-47-6 o-Xylene I1U.,;::,. 400 ug/kg C5- C8 Aliphatics(Unadj.) NU::;::;:;: ; :< 7900 ug/kg C9- C12 Aliphatics(Unadj.) hI.T ;> <'i'::: 7900 ug/kg C9-C10 Aromatics (Unadj.) hID;;:;;;:;>::;::: 7900 ug/kg C5- C8 Aliphatics 1A. 7900 ug/kg C9-C12 Aliphatics 7900 ug/kg .:..:...:.................. CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 09% 70-130% 615-59-8 2,5-Dibromotoluene 1:J:8.:fo:::>::: 70-130% ......................... (a)Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: SE DISP BOTT(4') Lab Sample ID: M39301-2 Date Sampled: 05/06/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.7 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1. QR27555.1) 1 05/13/04 AA n/a n/a GQR1346 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 12.4 g 16.0 nil 100 ul Run#2 I MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene :: 340 ug/kg ........................ .. ........................- 100-414 Ethylbenzene ND,,... 340 ug/kg .......................... 1634-04-4 Methyl Tert Butyl Ether ND.._...._..' 140 ug/kg 91-20-3 Naphthalene ND 340 ug/kg 108-88-3 Toluene <;:; ;;:;I.` 340 ug/kg m,p-Xylene tl :: :<: >340 ug/kg 95-47-6 o-Xylene N2 340 ug/kg C5-C8 Aliphatics(Unadj ) lD 6800 ug/kg C9- C12 Aliphatics (Unadj.) 6800 ug/kg C9- C10 Aromatics (Unadj.) I? <; ; <;; 6800 ug/kg C5-C8 Aliphatics ND 6800 ug/kg C9- C12 Aliphatics I :h ; ; ;` 6800 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $7.%. ;; ; 70-130% 615-59-8 2,5-Dibromotoluene :9 %:::..;:;`i:; 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: NW DISP BOTT(4') Lab Sample ID: M39301-4 Date Sampled: 05/06/04 Matrix: SO - Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 95.2 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a QR27561.1) 1 05/13/04 AA n/a n/a GQR1346 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 11.2 g 16.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... 71-43-2 Benzene ND 380 ug/kg 100-41-4 Ethylbenzene ND__::: .....:< 380 ug/kg --............. 1634-04-4 Methyl Tert Butyl Ether ND 150 ug/kg 91-20-3 Naphthalene ND 380 ug/kg 108-88-3 Toluene ND. 380 ug/kg m,p-Xylene ND 380 ug/kg 95 47-6 o-Xylene N17 380 ug/kg C5- C8 Aliphatics(Unadj ) hED :.::...; 7500 ug/kg C9- C 12 Aliphatics(Unadj ) ND 7500 ug/kg C9- C10 Aromatics(Unadj ) ND 7500 ug/kg .......:................... .......................... C5- C8 Aliphatics > 7500 ug/kg C9- C 12 Aliphatics <ND;;; ; 7500 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene $2`%><< 70-130% 615-59-8 2,5-Dibromotoluene 89...%:::;:_:::;,:;::; 70-130% (a)Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: SW DISP BOTT(4') Lab Sample ID: M39301-3 Date Sampled: 05/06/04 Matrix: SO- Soil Date Received: 05/10/04 Method: MADEP VPH 98-1 Percent Solids: 94.4 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a QR27560.1) 1 05/13/04 AA n/a n/a GQR1346 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 10.9 g 16.0 m1 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q ........................... ........................... 71-43-2 Benzene ::ND 390 ug/kg 100-41-4 Ethylbenzene h1D - 390 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND.;::;::;;.;: 160 ug/kg 91-20-3 Naphthalene ND.. .. 390 ug/kg 108-88-3 Toluene ND 390 ug/kg m,p-Xylene Di; ; 390 ug/kg 95-47-6 o-Xylene NT .;:.:;.<;.;;:.::.;,;; 390 ug/kg C5-C8 Aliphatics(Unadj.) ND::::;:>:;:: ; 7800 ug/kg C9-C12 Aliphatics(Unadj.) ND.;::;:;;,:: :;:;:;;:: 7800 ug/kg C9- C10 Aromatics(Unadj.) 1?ID.:.. 7800 ug/kg C5- C8 Aliphatics >ND <;;<i ;;: 7800 ug/kg C9-C12 Aliphatics IUD:; ; .. 7800 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 71 70-130% 615-59-8 2,5-Dibromotoluene 74% 70-130% (a) Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MADEP VPH FORM Matctx A ueous F1 Soil Sediment F Other Contalnecs ' . Satisfactorvny Broken F1 Leakin A` ueous Preservatives NIA IV PH <=2 H>2 T,em ratt�e _,r Received on Ice Received at 4 Deg. C Other d Rec'd at 2.7 deg C Me.Iianot > r Methanol Coverin Soil. mL Methanol! soil: Other NOTE: Ratio< 0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: NE DISP BOTT(4) Lab ID: M39301-1 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/6/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.9 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND A 7900 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 7900 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 7900 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 400 Toluene 108-88-3 C5-C8 ug/kg ND 400 I Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 160 Benzene 71-43-2 C5-C8 ug/kg ND 400 Naphthalene 91-20-3 N/A ug/kg ND 400 o-Xylene 95-47-6 C9-C12 ug/kg ND 400 m,p-Xylene C9-C12 ug/kg ND 400 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 7900 C9-C12 Aliphatics N/A ug/kg ND c 7900 Surrogate Recoveries Acceptance Range i FID:2,5-Dibromotoluene % 109 70-130% PID:2,5-Dibromotoluene % 118 70-130% Footnotes A Hydrocarbon flange data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C9C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifter indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 511812004 MADEP VPH FORM Aciueous Soil Sediment Other Conarners � SatisfactoryFyl Broken n Leaking A ueos�P�reservatrue N/A H <= 2 H> 2 T_�mrature _ Received on Ice Received at 4 Deg. C Other Rec'd at 2.7 deg C IWehanol .GFu Methanol Covering Soil. mL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH 98-1 Client ID: SE DISP BOTT(4) Lab ID: M39301-2 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/6/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.7 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A - ug/kg ND" 6800 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 6800 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 6800 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 340 Toluene 108-88-3 C5-C8 ug/kg ND 340 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 140 Benzene 71-43-2 C5-C8 ug/kg ND 340 Naphthalene 91-20-3 N/A ug/kg ND 340 o-Xylene 95-47-6 C9-C12 ug/kg ND 340 m,p-Xylene C9-C12 ug/kg ND 340 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND B 6800 C9-C12 Aliphatics N/A ug/kg ND c 6800 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 87 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'S qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Date 5/18/2004 Printed Name Reza Tand MADEP VPH FORM Mafrtz ` A ueous Soil ke Sediment h Other ri C�ntatnecs _�_ SatisfactoryW Broken F Leaking A "teous Preseratives NIA H<=2 F1 PH> 2 T "irature ��, Received on Ice Received at 4 Deg.C Other Redd at 2.7 deg c r _ Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio<0.75 to 1. Me.__ analK Method for Ranges: MADEP VPH 98-1 Client ID: SW DISP BOTT(4') Lab ID: M39301-3 t thod for Target Analytes: MADEP VPH 98-1 Date Collected: 5/6/2004 Date Received: 5/10/2004 H Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.4 1 NIA Unadiusted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 7800 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 7800 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 7800 Target Analvtes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 390 Toluene 108-88-3 C5-C8 ug/kg ND 390 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 160 Benzene 71-43-2 C5-C8 ug/kg. ND 390 Naphthalene 91-20-3 N/A ug/kg ND 390 o-Xylene 95-47-6 C9-C12 ug/kg ND 390 m,p-Xylene C9-C12 ug/kg ND 390 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 7800 C9-C12 Aliphatics N/A ug/kg ND` 7800 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene Q % 71 70-130% PID:2,5-Dibromotoluene % 74 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'J'QualiFer indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑d Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature. Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 MADEP VPH FORM Matrix. ,._``Q,' Aqueous Soil Sediment n Other Cantalners - Satisfactory Broken n Leaking A ueausP;reseryattyes N/A H <=2 H > 2 T in .; ratt rep w Received on Ice n Received at 4 Deg. C F1 Other d Redd at 2.7 deg C Methanol Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio<0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client 1D: NW DISP BOTT(4') Lab ID: M39301-4 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/6/2004 Date Received: 5/10/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/13/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95.2 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL lq C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 7500 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 7500 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 7500 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 380 Toluene 108-88-3 C5-C8 ug/kg ND 380 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 150 Benzene 71-43-2 C5-C8 ug/kg ND 380 Naphthalene 91-20-3 N/A ug/kg ND 380 o-Xylene 95-47-6 C9-C12 ug/kg ND 380 m,p-Xylene C9-C12 ug/kg ND 380 Adjusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 7500 C9-C12 Aliphatics N/A ug/kg ND° 7500 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 89 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C9C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-Cl 0 Aromatic Hydrocarbons. Z AV Qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.37 W No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 OACCUTEST 495 TECHNOLOGY CENTER WEST • BUILDING ONE `5 MARLBOROUGH,MA 01752 ACCUTEST OUOTE•: L a b o r a t o r i e s TEL:508-481-62W • FAX.•508-481-7753 " CLIENT INFORMATION ¢ ". FACILITY INFORMATION , ANALYTICAL INFORMATION ' I '• MATRIX CODES O �i l ✓1 l...LA Jcpus Pun �.1� � CW• WATER DRINKING N ME PROJECT NA-•MBE. OW• GROUND �� �r�� 1 G O �.1 Ay1 � OI _ I WC mif� WATER ADDRESS �^ ,( �// LOCATION p�—'-T� WW- WASTE R, As , r l,4 / 7 9 G611.b i600[S.'1c WATER SO• SOIL CITY _1 STATE ZIP PR�.�� T N � n O ,yJ_ A �n SL• SLUDGE OIL �✓ ..�.f- 1 `'( OI• OIL SEND REPORT T � �} .? / LIO. OTHER PHONE# �7g-�'[o�- $7y C� FAX# 7$- J la$-� 7 /6 L,OUID SOL-OTHER' ACCUTEST COLLECTION PRESERVATIO SOLID SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMBPLED _ / m LAB USE ONLY _ 1 N E I (yij s -.;z sp Dts 1500 vo S I I jr, 1 I DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION HIM IffilgifflM COMMENTS/REMARKS 14 DAYS STANDARD APPROVED BY: O STANDARD 7 DAYS RUSH ❑ COMMERCIAL"B" V b L O 48 HOUR EMERGENCY O DISK DELIVERABLE ❑ OTHER ❑ STATE FORMS 14 DAY TURNAROUND HAROCOPY.EMERGENCY OR RUSH IS FAX ❑ OTHER(SPECIFY) Lo c , 36 y 9 F DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIM SAMPLES CHANGE POSSESION,INCLUDING COURIER 9ELIVERY { RELINQUISHED BY MPLER: OAT TIME: RECEIVED BY' REU ISHE Y: DAT . M (J ;� RECEIVED BY: 1. 2. O O 2. RELINO IS BY: OAT IM RECEIVED B R NOUIBHEO B : DA E RE O Y: 3. /o 3. 4. 4. RELIN (SHED 8 AT TIM : REC O BY: SEAL• PRESERVE WHERE APPLICABLE ON ICE TEMPERITURE 5. 5. 0 eZ.7 C MAY 21 2004 IM® New England OS/20/04 ®A= JTF.ST L a b o r a t o r i e s Tecluuca deport for Shell Oil GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA GSC PO# 16988 Accutest Job Number: M39365 Sampling Date: 05/10/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 21 Q`Eo�M Acco"a /L Test results contained within this data package meet the requirements te and Lab Director of the National Environmental Laboratory Accreditation Conference and/or state specific certification programs as applicable. Certifications: MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 495 Tech Center West 0 Building I ■ Marlborough,M 01752 0 tel:508 481-6200■ fax: 508-481-7753 0 http://www.accutest.com II�T SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No: M39365 Site: GSCMA:96925028(REIMBMA) 1140 lyannough Rd.,Hyannis,M Report Date 5/20/2004 11:25:59 A 4 Sample(s)were collected on 05/10/2004 and were received at Accutest on 05/12/2004 properly preserved,at 1.5 Deg.C and intact. These Samples received an Accutest job number of M39365.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GC By Method MADEP VPH 98-1 Matrix: SO Batch ID: GAB743 ■ All samples were analyzed within the recommended method holding time. Sample(s) M39363-1 MS,M39363-1 MSD were used as the QC samples indicated. ■ All method blanks for this batch meet method specific criteria. ■ M39363-1MS:Soil to methanol ratio greater than 1.25 to I: ■ M39363-IMSD: Soil to methanol ratio greater than 1.25 to 1. ■ M39365-1: Soil to methanol ratio less than 0.75 to 1. M39365-2: Soil to methanol ratio less than 0.75 to 1. ■ M39365-3:Soil to methanol ratio less than 0.75 to 1. Wet Chemistry By Method EPA 160.3 M Matrix: SO Batch ID: GN13856 ■ Sample(s) M39365-1 DUP were used as the QC samples for Solids,Percent_ The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M39365). Thursday,May 20,2004 Page I of 1 2 I Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 22 May 2003 Revision No. 3.1 Bureau of Waste Site Cleanup Final Page 13 of 30 Title: MADEP MCP Response Action Analytical Report Certification Form :ws ,� 2' 414t, � IUTAIE� P Analyttc,al e od RepclrCerttf atioit .d Laboratory Name: Accutest Laboratories of New England Project#: M39365 Project Location: GSCMA:96925028(REIMBMA)1140 lyannough Rd., MADEP RTN None Hyannis, MA This form provides certifications for the following data set: M39365-1,M39365-2,M39365-3,M39365-4 Sample Matrices: Groundwater Soil/Sediment X Drinking Water Other: IGtCPS46 8260B 8151A 8330 6010E 7470A/1A etfiodstd, x; 8270C ) 8081A VPH X 6020 ( 9014M Z % peafie �jMAt3Ef' 8082 8021E ( EPH ( 7000 S 3 7196A bm ium of 1 L+st$Releasef T Nurntrec"lO no w ica 1Wethods 2 M �� Method 90 4 o 1 Ut--P, �y 1 Q§'1 lY rla anti I?EM G r y t, ! , aaPl�x7 S.; w 846Me[fiodsaQO S es t , methoda�. ?,. nx An affirmative response to questions A, B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with U, Yes ❑ No ' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Does the analytical data included in this report meet all the requirements C for"Presumptive Certainty",as described in Section 2.0 of the MADEP Yes ❑No ' document CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without 2 Yes ❑No ' significant modifications,as specified in Section 11.3? A response to questions E and F below is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the W Yes U No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified ❑ Yes UNo ' methods reported? , All Negative responses must be addressed in an attached Environmental Laboratory case narrative. 1 the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 5/20/04 3 Accutest Laboratories Sample Summary Shell Oil Job No: M39365 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Project No: GSC PO# 16988 Sample Colleetecl..._..._: ;:.;_ Matrix Client Number Date Time By Received Code Type Sample ID M39365.* 05/10/04 09:50 MW 05/12/04 SO Soil EXC01 (3 M39365=2 05/10/04 09:55 MW 05/12/04 SO Soil EXCOZ M.39365-3 OS/10/04 10:00 MW 05/12/04 SO Soil EXC03 (3 5 } .................... ........ M39365 4 05/10/04 10:05 MW 05/12/04 SO Soil BXC04 (3 5'} Soil samples reported on a dry weight basis unless otherwise indicated on result page. 4 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: EXCO1 (Y) Lab Sample ID: M39365-1 Date Sampled: 05/10/04 Matrix: SO -Soil Date Received: 05/12/04 Method: MADEP VPH 98-1 Percent Solids: 95.2 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a A1314947.1) 1 05/14/04 DL n/a n/a GAB743 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 8.44 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result p RL Units Q 7143-2 Benzene f12 500 ug/kg 100414 Ethylbenzene 1930.0 500 ug/kg 1634-044 Methyl Tert Butyl Ether 1;4$0 200 ug/kg 91-20-3 Naphthalene 3060 500 ug/kg 108-88-3 Toluene 31200 ' 500 ug/kg ........................... m,p-Xylene 46600 g g 500 u /k 9547-6 o-Xylene 211?00 500 ug/kg C5-C8 Aliphatics(Unadj ) T4.SQOQ. 10000 ug/kg C9-C12 Aliphatics(Unad1 ) 219000 10000 ug/kg C9-CIO Aromatics(Unadj.) 127©00:<:::;: 10000 ug/kg CS- C8 Aliphatics12©tl0 > 10000 ug/kg C9- C12 Aliphatics ND 10000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 70-130% 615-59-8 2,5-Dibromotoluene 1 .fl5..%, ........... _ .. ......................... 615-59-8 2,5-Dibromotoluene 70-130% (a) Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 5 Accutest Laboratories Report.of Analysis Page 1 of 1 Client Sample ID: EXCO2 (3.5') Lab Sample ID: M39365-2 Date Sampled: 05/10/04 Matrix: SO- Soil Date Received: 05/12/04 Method: MADEP VPH 98-1 Percent Solids: 97.0 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File H) DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB 14948.D 1 05/14/04 DL n/a n/a GAB743 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 10.3 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q ......................... 71-43-2 Benzene ND 400 ug/kg 100-414 Ethylbenzene _1;4900 ;::. 400 ug/kg ......_... _....... 1634-04-4 Methyl Tert Butyl Ether ;I54Q..:;:;. 160 ug/kg 91-20-3 Naphthalene 12400..::;._..: 400 ug/kg 108-88-3 Toluene 19.100; .> 400 ug/kg m,p-Xylene 4QS00:.;::;; 400 ug/kg 9547-6 o-Xylene 22500 400 ug/kg C5-C8 Aliphatics(Unadj ) 103 o:_:.::; 8000 ug/kg C9-C12 Aliphatics(Unadj.) 3030QE1<` <i 8000 ug/kg C9-C10 Aromatics (UnadJ ) 213000 8" ug/kg C5-C8 Aliphatics 81"HOC)::;;:::;;::;;:::;:: 8000 ug/kg C9-C12 Aliphatics <hlll> 8000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 119% 70-130% 615-59-8 2,5-Dibromotoluene 15:%.;.:;:: :; 70-130% (a) Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: EXC03 (3.5') Lab Sample ID: M39365-3 Date Sampled: 05/10/04 Matrix: SO - Soil Date Received: 05/12/04 Method: MADEP VPH 98-1 Percent Solids: 94.1 Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a AB 14949.D 1 05/14/04 DL n/a n/a GAB743 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 11.0 g 16.0 ml 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 390 ug/kg 100414 Ethylbenzene ND 390 ug/kg 1634-04-4 Methyl Tert Butyl Ether NIA:;::;:::;:;:::::::::::.::;: 150 ug/kg .........................:. 91-20-3 Naphthalene Nb <; 390 ug/kg 108-88-3 Toluene hID 390 ug/kg m,p-Xylene ND 390 ug/kg 95-47-6 o-Xylene ND.....::.>:. ;> 390 ug/kg ........__.. _._. _.. __. .. ..._..._. C5-C8 Aliphatics(Unadj.) ND; ;; 7700 ug/kg C9-C12 Aliphatics(Unadj.) ND. ..;„_:.,.: 7700 ug/kg . ............. ........................... C9-C10 Aromatics(Unadj.) D 7700 ug/kg C5-C8 Aliphatics NIA::> :;::: 7700 ug/kg C9-C12 Aliphatics ND. 7700 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene ;.,::;: 70-130% ...:....................: ......................... 615-59-8 2,5-Dibromotoluene g7% 70-130% (a) Soil to methanol ratio less than 0.75 to 1. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 Accutest Laboratories Report of Analysis Page I of I Client Sample H): EXC04 (3.5') Lab Sample ID: M39365-4 Date Sampled: 05/10/04 Matrix: SO- Soil Date Received: 05/12/04 Method: MADEP VPH 98-1 Percent Solids: 94.0 Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB14950.1) 1 05/15/04 DL n/a n/a GAB743 Run#2 Initial Weight Final Volume Methanol Aliquot Run#1 11.5 g 16.0 nil 100 ul Run#2 MA-VPH List CAS No. Compound Result RL Units P Q 71-43-2 Benzene ND 370 ug/kg 100-41-4 Ethylbenzene ND 370 ug/kg 1634-04-4 Methyl Tert Butyl Ether 193 150 ug/kg 91-20-3 Naphthalene IUD 370 ug/kg 108-88-3 Toluene ND 370 ug/kg m,p-Xylene ND 370 ug/kg 9547-6 o-Xylene ND 370 ug/kg C5-C8 Aliphatics(Unadj.) ND 7400 ug/kg C9-C12 Aliphatics (UnadJ ) ND 7400 ug/kg C9-C10 Aromatics (UnadJ ) ND. . :.. 7400 ug/kg C5-C8 Aliphatics .ND....,::,:;;;_,, 7400 ug/kg C9-C12 Aliphatics hCD 7400 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 43%...... .`;;' 70-130% ......................... 615-59-8 2,5-Dibromotoluene 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8 MADEP VPH FORM VOAixs~ �x:; �, .= A ueous Soil Sediment OtherSatisfacto y Broken LeakinN/A H <= 2 H> 2 att 3 = Received on Ice Received at 4 Deg.G Other d Redd at 1.5 deg C �llett`aiio " ` �. Methanol Covering Soil. mL Meth nolkq soil: Other NOTE: Ratio< 0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: EXC01 (3') Lab ID: M39365-1 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 95.2 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL (� C5-C8 Aliphatics(Unadj.) N/A ug/kg 145000" 10000 i C9-C10 Aromatics(Unadj.) N/A ug/kg 127000" 10000 C9-C12 Aliphatics(Unadj.) N/A ug/kg 219000 A 10000 Target Analytes Ethylbenzene 10OAlA C9-C12 ug/kg 19300 500 Toluene 108-88-3 C5-C8 ug/kg 31200 500 Methyl Tert Butyl Ether 1634-04A C5-C8 ug/kg 1480 200 Benzene 71 A3-2 C5-C8 ug/kg 612 500 Naphthalene 91-20-3 N/A ug/kg 3060 500 o-Xylene 95-47-6 C9-C12 ug/kg 21000 500 m,p-Xylene C9-C12 ug/kg 46600 500 Adiusted Ranges C5-C8 Aliphatics WA ug/kg 112000 a 10000 C9-C12 Aliphatics N/A ug/kg ND` 10000 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 105 70-130% PID:2,5-Dibromotoluene % 107 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any sunrogate(s)and/or Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or Internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑d No ❑ Yes=Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition, Laboratory Director Prinfnril tJnimn R07a Tanrl 9 Date 5/19/2004 MADEP VPH FORM Matra Aqueous Soil d Sediment n Other Co a Hers'' N Sa tisfactoryFyl Broken r Leaking AgteousPesecvattve N/A Rd pH <=2 H > 2 Received on Ice Received at 4 Deg.C Other g C Redd at 1.5de Mef>tano ,r. �" `� Methanol Coverin Soil. mL Methanol/ soil: Other NOTE: Ratio<0.75 to 1. x Method for Ranges: MADEP VPH 98-1 Client ID: EXCO2(3.5') Lab ID: M39365-2 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PI D: 2,5-Dibromotoluene N/A 5/14/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 97 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL 2 C5-C8 Aliphatics(Unadi.) N/A ug/kg 103000" 8000 C9-C10 Aromatics(Unadj.) WA ug/kg 213000" 8000 C9-C12 Aliphatics(Unadj.) N/A ug/kg 303000" 8000 Target Analytes Ethylbenzene 100414 C9-C12 ug/kg 14900 400 Toluene 108-88-3 C5-C8 ug/kg 19100 400 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg 1540 160 Benzene 71-43-2 C5-C8 ug/kg ND 400 Naphthalene 91-20-3 N/A ug/kg 12400 400 o-Xylene 95-47-6 C9-C12 ug/kg 22500 400 m,p-Xylene C9-C12 ug/kg 49500 400 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg 81906 B 8000 C9-C12 Aliphatics N/A ug/kg ND` 8000 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 119 70-130% PID:2,5-Dibromotoluene % 125 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of arty surrogate(s)and/or internal standards eluting In that range. CSCII Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surtogate(s)and/or Internal standards eluting In that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting In that range AND concentration of C9C10 Aromatic Hydrocarbons. Z A'J'qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? V Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? V No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand 10 Date 5/19/2004 MADEP VPH FORM ffatcEx _ k� �= Aqueous F1 Soil Fy Sediment F1 Other ontamersn. Y� Satisfacto .i Broken n Leaking ueousPreservafrves N/A H <=2 H> 2 T�trt fr tt a Received on Ice Received at 4 De .C Other (� Rec'd at 1.5 deg C e1�>tano Methanol Coverin Soil. mL MethanolI soil: Other NOTE: Ratio<0.75 to 1. Method for Ranges: MADEP VPH 98-1 Client ID: EXC03(3.5') Lab ID: M39365-3 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/14/2004 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: 94.1 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/kg ND" 7700 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 7700 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 7700 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/kg ND 390 Toluene 108-88-3 C5-C8 ug/kg ND 390 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/kg ND 150 Benzene 71-43-2 C5-C8 ug/kg ND 390 Naphthalene 91-20-3 N/A ug/kg ND 390 o-Xylene 95-47-6 C9-C12 ug/kg ND 390 m,p-Xylene C9-C12 ug/kg ND 390 Adiusted Ranges C5-C8 Aliphatics N/A ug/kg ND a 7700 C9-C12 Aliphatics N/A ug/kg ND` 7700 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 97 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any sunogate(s)and/or internal standards eluting in that range * Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surtogate(s)and/or internal standards eluting In that range.C9-C12 aliphatic Hydrocarbons exclude cons of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A*X qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director PrintPrl Name PP7n Tanrf 11 Date 5/19/2004 MADEP VPH FORM Matrix <.- � .= A ueous i Soil al Sediment Other k� Satisfacto Broken F Leakin i ,utz'ous,Presenratrvesr N/A pH<=2 F1 PH>2 T�et 1eatti a � � Received on Ice Received at 4 Deg.C Other Rec'd at 1.5 deg C Me taro( ,,m Methanol Coverinc Soil. ImL Methanol/ soil: 1:1 +/-25% Method for Ranges: MADEP VPH 98-1 Client ID: EXC04(35) Lab ID: M39365-4 Method for Target Analytes: MADEP VPH 98-1 Date Collected: 5/10/2004 Date Received: 5/12/2004 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/15/2004 WA FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution- 94 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/kg ND A 7400 C9-C10 Aromatics(Unadj.) N/A ug/kg ND" 7400 C9-C12 Aliphatics(Unadj.) N/A ug/kg ND" 7400 (Target Analytes Ethylbenzene 100414 C9-C12 ug/kg ND 370 Toluene 108-88-3 C5-C8 ug/kg ND 370 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/kg 193 150 Benzene 71-43-2 C5-C8 ug/kg ND 370 Naphthalene 91-20-3 N/A ug/kg ND 370 o-Xylene 95-47-6 C9-C12 ug/kg ND 370 m,p-Xylene C9-C12 ug/kg ND 370 Adiusted Ranges I C5-C8 Aliphatics N/A ug/kg ND a 7400 C9-C12 Aliphatics N/A ug/kg ND` 7400 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % 104 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any sunogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of arty surrogates)and/or Internal standards eluting In that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting In that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performancelacceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand 12 Date 5/19/2004 Accutest Laboratories GC Vola les QC Data Summaries Includes the following where applicable: ■ Method Blank Summaries ■ Blank Spike Summaries ■ Matrix Spike and Duplicate Summaries ■ Surrogate Recovery Summaries 13 Method Blank Summary Page I of I Job Number: M39365 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB743-MB AB14931.1) 1 05/14/04 DL n/a n/a GAB743 The QC reported here applies to the following samples: Method: MADEP VPH 98-1 M39365-1, M39365-2, M39365-3, M39365-4 CAS No. Compound Result RL Units Q 71-43-2 Benzene ;ND.::,:,.::<;;.=250 ug/kg g 100-41-4 Ethylbenzene NU.......;_.;:.:; 250 ug/kg ....::..................... ........................... 1634-04-4 Methyl Tert Butyl Ether :,ND 100 ug/kg 91-20-3 Naphthalene ,. U;:........... 250 ug/kg .....................:..... ........................... 108-88-3 Toluene U;:.;:,,:;:.; :::.:: 250 ug/kg m,p-Xylene 250 ug/kg .............. ........................... 9547-6 o-Xylene AID:::;:;> <i250 ug/kg C5- C8 Aliphatics(Unadj.) 'NU 5000 ug/kg ..:........................ C9- C12 Aliphatics(Unadj.) iI ` < 5000 ug/kg C9- C10 Aromatics (Unadj.) D;,: ug/kg C5- C8 Aliphatics ;:ND.:.. ::::; 5000 ug/kg C9-C 12 Aliphatics ND` >` 5000 ug/kg CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 901ii ;; 70-130% 615-59-8 2,5-Dibromotoluene 97.%.......: .:.:: 70-130% 14 Blank Spike Summary Page I of 1 Job Number: M39365 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB743-BSP AB 14932.D 1 05/14/04 DL n/a n/a GAB743 The W reported here applies to the following samples: Method: MADEP VPH 98-1 M39365-1, M39365-2, M39365-3, M39365-4 Spike BSP BSP CAS No. Compound ug/kg ug/kg % Limits 71-43-2 Benzene 1000 977 98<>> 70-130 ................. 100-41-4 Ethylbenzene 1000 1060 ;04i[; 70-130 1634-04-4 Methyl Tert Butyl Ether 3000 3130 L134..;;;. 70-130 91-20-3 Naphthalene 2000 225013 ; 70-130 108-88-3 Toluene 3000 293070-130 _..... .... ................. ................. m,p-Xylene 4000 4010 IQQ70-130 ................. 95-47-6 o-Xylene 2000 2030 IO2 70-130 CAS No. Surrogate Recoveries BSP Limits 615-59-8 2,5-Dibromotoluene 86.%.._ > ::;:; 70-130% _. ............. ............................ 615-59-8 2,5-Dibromotoluene 93%.._... 70 1305c _. 15 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M39365 Account: SHELLWIC Shell Oil Project: GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M39363-1MS a AB14934.1) 1 05/14/04 DL n/a n/a GAB743 M39363-1MSD aAB14935.D 1 05/14/04 DL n/a n/a GAB743 M39363-1 a AB14933.1) 1 05/14/04 DL n/a n/a GAB743 The QC reported here applies to the following samples: Method: MADEP VPH 98-1 M39365-1, M39365-2, M39365-3, M393654 M39363-1 Spike MS MS MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg % RPD. Rec/RP] 71-43-2 Benzene ND 746 956 128 < 890 419 7 70-130P 100-41-4 Ethylbenzene ND 746 947 127 919 -I23 3 70-130%` 1634-04-4 Methyl Tert Butyl Ether ND 2240 2900 130....:> 2760 I23...:::..: ::> 70-130/ 91-20-3 Naphthalene ND 1490 1760 >. 1830 70- _130/ 108-88-3 Toluene ND 2240 2650 m,p-Xylene ND 2990 3590 120..,;:. 3470 I1;6. J; ;:::,. 70-130/. lene ND 14 . 95-47-6 o-X y 90 1820 122 1760 l: $.. .... . .; 70 130/. CAS No. Surrogate Recoveries MS MSD M39363-1 Limits 615-59-8 2,5-Dibromotoluene 104% 70-130% 615-59-8 2,5-Dibromotoluene 104% 1Q % i0 70-130% (a) Soil to methanol ratio greater than 1.25 to 1. 16 Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M39365 Account: SHELLWIC Shell Oil Project: GSCMA:96925028(REIMBMA) 1140 Iyannough Rd., Hyannis, MA Method: MADEP VPH 98-1 Matrix: SO Samples and QC shown here apply to the above method Lab Lab Sample ID File ED Sl a S1 b M39365-1 AB14947.D >t00>' 107.0 M39365-2 AB14948.1) 449:-W;;:>:>< 125.0 M39365-3 AB14949.D 9:)::.4:;:: 97.0 ...................... ...................... M39365-4 AB14950.D >93 ` 104.0 _. GAB743-BSP AB 14932.D $((} :<: 93.0 ............:. .. GAB743-MB AB 14931.D I(? : » 97.0 ...................... ....................... M39363-1MS AB14934.D a)Q104.0 ...................... M39363-1MSD AB14935.13 108`( _< 103.0 ..............:........ _.. Surrogate Recovery Compounds Limits ........................... Sl = 2,5-Dibromotoluene 7E)OW i i ........................... (a) Recovery from GC signal#1 (b)Recovery from GC signal #2 17 Accutest Laboratories Mlsc. Forms � Custody Documents and Other Forms Includes the following where applicable: ■ Sample Tracking Chronicle 18 Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M39365 GSCMA:96925028 (REIMBMA) 1140 Iyannough Rd., Hyannis, MA Project No: GSC PO# 16988 Sample Number Method Analyzed By Prepped By Test Codes Ivl 93�i5 1 . .� �1e e ; 5. M39365-1 EPA 160.3 M 13-MAY-04 OP %SOL M39365-1 MADEP VPH 98-1 14-MAY-04 22:14 DL VMAVPH 5-2. : flIteie -: E�It+Itfly SS 8y-M Rece�v d 1 MAC f14 $yS :.>::::: ..;:.: :::.:::::::::::::: .............. ...:.::::::: -::::.::.::::::::::::: ::::::::::::.::::.:::.:. M39365-2 EPA 160.3 M 13-MAY-04 OP %SOL M39365-2 MADEP VPH 98-1 14-MAY-04 22:54 DL VMAVPH tec€ :Iw#4i-iwx If?,€lt#:_:By_.::]tW.:>: ..ReceFved.. ::I Y .; 3 :::R .::::::>. ;::::>:: y :::::::.:............ .... .... . ... ........ M39365-3 EPA 160.3 M 13-MAY-04 OP %SOL M39365-3 MADEP VPH 98-1 14-MAY-04 23:34 DL VMAVPH Cetllected 1€1 A �.;04.112.:1v1Y 1I4 R5 M39365-4 EPA 160.3 M 13-MAY-04 OP %SOL M39365-4 MADEP VPH 98-1 15-MAY-04 00:15 DL VMAVPH Page I of 1 19 Betty Baer From: Moira Walker[mwalker@ma.gsc-global.com] Sent: Wednesday, May 12, 2004 11:24 AM To: Betty Baer h Rd, Hyannis 1140 I annou Subject: Y 9 Betty, GSC submitted soil samples from Texaco Station#100083 located at 1140 lyannough, Hyannis MA today and during the previous weeks. Please note that these soil samples are from a GWA site and therefore must have the S-1/GW-1 detection limits. Also,because it is in the state of MA,we would like the MCP CAM level of qa/qc. Please contact me at 978-568-8740 x257 should you have any questions or would like me to fax over a revised Chain of Custody. Thank you, Moira Moira Walker Geologist Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 Toll Free:800 522 8740 Tel:978 568 8740 x257 Fax: 978 568 9316 mwalker@ma.gsc-global.com www.gsc-global.com NOTICE: This e-mail message and any attachment to this e-mail may contain confidential information that may be legally privileged. If you are not the intended recipient, you must not review, retransmit,convert to hard-copy, copy, use or disseminate this a-mail and any attachment to it. If you have received this e-mail in error, please notify us by return e-mail or by telephone at 978 568 8740 and delete this message. Please note that if this e-mail message contains a forwarded-message or is a reply to a prior message,some or all of the contents of this message or any attachments may not have been produced by GSC. This notice is automatically appended to each e-mail message sent from GSC. Thank you. GU 495 TECHNOLOGY CENTER WEST • BUILDING ONE I v MACCUTEST MARLBOROUGH,MA 01752 LACCUTEST OUOTE#: TEL:508-481.6200 • FAX:508481.7753 CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES 4 So � DW- DRINKING GPD rnd <o✓V l,C.Q N (]L* 7e Q U 5 1 0.1(`,V A �C� ice= GW- GROUND WATER NAM PROJECT NAME / }� '/,. WATER is r►a� (; �t .1 , r�a�nc oh. I',U F' �� 7 WW• WASTE AMC LOCATIO WATER _ (nA a/7V9 TG�,��t lo©0 8 3 - SOIL sL• SLUDGE CITY, M f G STATE ZIP - PROJECT n h /_ ��•) 01- OIL L O- OTHER SEND REPO PHONIE,1#RT�QTo9 7 S'S '�7y(Z FAX# - S�i- / 3�L� soL Uou1D -OTHER COLLECTION PRE ER ;n SOLID ?S � SAMPLE# FIELD ID/POINT OF COLLECTION DATE TIME SAMPLED ACCUTT aBY. .P $ 11 lul li LAB USE ONLY Sow X x -3 (3,5 t000 iT 3,5' o0 DATA TURNAROUND INFORMATION DATA DELIVERABLE INFORMATION ° ' COMMENTS/REMARKS 14 DAYS STANDARD APPROVED 8Y: D STANDARD ; Q� i c n� 7 DAYS RUSH D COMMERCIAL"B" J ,p O 48 HOUR EMERGENCY O DISK DELIVERABLE u V'PH ()'LI n,,ok O OTHER ❑ STATE FORMS Lac I oa 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX Cl OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TIME SAMPLES CHANGE POSSESION,INCLUDING COURIER DELIVEPty RELINQUISHED Y SAMPL.R: DATE TIME: RECEIVED BY: RE UISME BY: DATE TIME: RECEIVED BYi 2 ia�/�o 2. RELIN DISH D BY: YdATTIME: / ECEIVED B R OUISHED BY: GATE TIME: RECEIVED BY3. �. o 3 4. . RELIN UISHED Y: DA E TI E: RECEI D BY: SEAL• PRESERVE WHERE APPLICABLE ON ICE TEMPERATURE 5. SC MAY 1 2 2004 ®� New England OS/10/04 ® Lab.,y., ._..,. Technical Report far Shell Oil GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Cost Element #707542 Accutest Job Number: M39055 Sampling Date: 04/26/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 9 4�V�M kCCpRO �, cs 4 :z Test resuits contained within this data package meet the requirements teza�and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications:MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NI(MA926) IL(000589) NAVY USACE This report shall not'be reproduced,except in its entirety,without the written approval of Accutest Laboratories_ New England 495 Tech Center West■Building I ■ Marlborough,MA 01752 0 tel: 508481-6200 0 fax: 508-481-7753■ http://www.accutest.com Accutest Laboratories Sample Summary Shell Oil Job No: M39055 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Project No: Cost Element #707542 Sample Collected Matrix Client Number Date Time By Received Code Type Sample 1D ..... ....................... _._...... .............. .. ......__ _ ...... _ ...................................... ....._..._..........__......._...._..... .... ....... ..... ....... ....... ...... ......... . M39055,1 04/26/04 10:40 MW 04/26/04 SO Soil LIFT BOTI': 1VT9055 2 04/26/04 10:45 MW 04/26/04 SO Soil LIFT I;SW(3 4') _r Soil samples reported on a dry weight basis unless otherwise indicated on result page. Accutest Laboratories Report of Analysis Page I of I Client Sample ID: LIFT BOTT(6-7') Lab Sample ID: M39055-1 Date Sampled: 04/26/04 Matrix: SO- Soil Date Received: 04/26/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 95.6 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27632.D 1 05/10/04 ME 04/29/04 OP7088 GPO1842 Run#2 Initial Weight Final Volume Run#1 10.1 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene ,,,,,. :;, 520 ug/kg 208-96-8 Acenaphthylene ND__ 520 ug/kg 120-12-7 Anthracene N;D 520 ug/kg 56-55-3 Benzo(a)anthracene ND 520 ug/kg 50-32-8 Benzo(a)pyrene N.D .. .__..::. 520 ug/kg ._...... ........................... 205-99-2 Benzo(b)fluoranthene ND 520 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 520 ug/kg 207-08-9 Benzo(k)fluoranthene ND 520 ug/kg 218-01-9 Chrysene ND 520 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 520 ug/kg 206-44-0 Fluoranthene ND 520 ug/kg 86-73-7 Fluorene ND 520 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 520 ug/kg 91-57-6 2-Methylnaphthalene :ND::,'..,.. 520 ug/kg 91-20-3 Naphthalene ND 520 ug/kg 85-01-8 Phenanthrene N:D 520 ug/kg 129-00-0 Pyrene ND 520 ug/kg CI1-C22 Aromatics(UnadJ ) 19200 18000 ug/kg C9-C 18 Aliphatics 9870 62W ug/kg C19-06 Aliphatics :55500;;:;>::::: 83M ug/kg CI I-C22 Aromatics I8500 18000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 75%.. 40-140% 321-60-8 2-Fluorobiphenyl 81.;% 40-140% 580-13-2 2-Bromonaphthalene 69%.,..., ,. 40-140% 3386-33-2 1-Chlorooctadecane 72% 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: LIFT BOTT(6-T) Lab Sample ID: M39055-1 Date Sampled: 04/26/04 Matrix: SO-Soil Date Received: 04/26/04 Method: SW846 8082 SW846 3545 Percent Solids: 95.6 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 EF38743.1) 1 05/07/04 NM 04/28/04 OP7084 GEF1966 Run#2 Initial Weight Final Volume Run#1 15.7 g 10.0 ml Run#2 PCB List CAS No. Compound Result RL Units Q 1 2674-1 1-2 Aroclor 1016 ND " 100 ug/kg 11104-28-2 Aroclor 1221 ND 100 ug/kg 11141-16-5 Aroclor 1232 ND 100 ug/kg 53469-21-9 Aroclor 1242 ND 100 ug/kg 12672-29-6 Aroclor 1248 N ; > 100 ug/kg 11097-69-1 Aroclor 1254 Nib....,.. , . 100 ug/kg 11096-82-5 Aroclor 1260 lSl 100 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 877-09-8 Tetrachloro-m-xylene 30-134% 877-09-8 Tetrachloro-m-xylene 1Q3% 30-134% 2051-24-3 Decachlorobiphenyl 1.2ME:: ' 34-150% 2051-24-3 Decachlorobiphenyl 11#% 34-150% ND = Not detected I = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: LIFT ESW(3-4') Lab Sample ID: M39055-2 Date Sampled: 04/26/04 Matrix: SO- Soil Date Received: 04/26/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 94.6 Project: GSCMA:969250281140 tyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 PO27542.1) 1 05/05/04 ME 04/29/04 OP7088 GPO1838 Run#2 Initial Weight Final Volume Run#1 10.4 g 2.0 ml Run#2 CAS No. Compound Result RL Units Q ............._.... ... 83-32-9 Acenaphthene ND 510 ug/kg 208-96-8 Acenaphthylene ND. .. 510 ug/kg 120-12-7 Anthracene ND 510 ug/kg 56-55-3 Benzo(a)anthracene ND 510 ug/kg 50-32-8 Benzo(a)pyrene ND 510 ug/kg D 205-99-2 Benzo(b)fluoranthene 510 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 510 ug/kg 207-08-9 Benzo(k)fluoranthene ND..._.,, .:::_ 510 ug/kg 218-01-9 Chrysene ND 510 ug/kg ND 53-70-3 Dibenz(a,h)anthracene 510 ug/kg 20644-0 Fluoranthene ND 510 ug/kg 86-73-7 Fluorene .:;::,:_:> :;_ 510 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND:::.. ,,:,:;`; 510 ug/kg 91-57-6 2-Methylnaphthalene ND 510 ug/kg 91-20-3 Naphthalene ND 510 ug/kg 85-01-8 Phenanthrene ND..._.__, .. 510 ug/kg. 129-00-0 Pyrene ND:::.:.. >.,;; 510 ug/kg CI I-C22 Aromatics (Unadj ) ND 17000 ug/kg C9-C18 Aliphatics ND 6100 ug/kg C19-C36 Aliphatics IUD 8100 ug/kg CI I-C22 Aromatics ND 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 40-140% .......... 321-60-8 2-Fluorobiphenyl 82%.... _...: ; 40-140% ............ ............ 580-13-2 2-Bromonaphthalene 40140% 3386-33-2 1-Chlorooctadecane 72:% 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: LIFT ESW (3-4') Lab Sample ID: M39055-2 Date Sampled: 04/26/04 Matrix: SO- Soil Date Received: 04/26/04 Method: SW846 8082 SW846 3545 Percent Solids: 94.6 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ED DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 EF38744.1) 1 05/0.7/04 NM 04/28/04 OP7084 GEF1966 Run#2 Initial Weight Final Volume Run#1 15.4 g 10.0.ml Run#2 PCB List CAS No. Compound Result RL Units Q 12674-11-2 Aroclor 1016 ND `< 100 ug/kg 11104-28-2 Aroclor 1221 ND..,,,.:: 100 ug/kg 11141-16-5 Aroclor 1232 ND_.. . .::. .. 100 ug/kg 53469-21-9 Aroclor 1242 NIj. .......,.;. 10D ug/kg 12672-29-6 Aroclor 1248 1I:U;:;:;: ;::>:: :i 100 ug/kg 11097-69-1 Aroclor 1254 ND,.,, 100 ug/kg ..:...................:.... ........................... 11096-82-5 Aroclor 1260 ND i 100 ug/kg CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......................... 877-09-8 Tetrachloro-m-xylene 87% 30-134% 877-09-8 Tetrachloro-m-xylene $9 :: ::;: 30-134% 2051-24-3 Decachlorobiphenyl 1,1.3:.°�0.:,;::::;: 34-150% 2051-24-3 Decachlorobiphenyl 106% 34-150% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound J IVIAutr trh r-L)KM ,sue-r1 " latrr<z J� Aqueous Soil r' Sediment F1 Other Go Satisfacto / Broken Leaking �IrflYousreseativs N/A .i PH <=2 F1 PH>2 em` rat � w Received on Ice n Received at 4 Deg.C n Other V Rec'd at 1.9 deg C ErtlonFettod ,,r SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: LIFT BOTT(6-7') Lab ID: M39055-1 Method for Targets: MADEP EPH 98-1 Date Collected: 4/26/2004 Date Received: 4/26/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 4/29/2004 5/10/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 95.6 1 N/A Unadjusted Ranges CAS# Units Result RDL (3 C11-C22 Aromatics(Unadj.) ug/kg 19200" 18000 Diesel PAH Analvtes 2-Methylnaphthalene 91-57-6 ug/kg ND 520 Phenanthrene 85-01-8 ug/kg ND 520 Acenaphthene 83-32-9 ug/kg ND 520 Naphthalene 91-20-3 ug/kg ND 520 Other Target PAH Analvtes Acenaphthylene 208-96-8 ug/kg ND 520 Anthracene 120-12-7 ug/kg ND 520 Benzo(a)anthracene 56-55-3 ug/kg ND 520 Benzo(a)pyrene 50-32-8 ug/kg ND 520 Benzo(b)fluoranthene 205-99-2 ug/kg ND 520 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 520 Benzo(k)fluoranthene 207-08-9 ug/kg ND 520 Chrysene 218-01-9 ug/kg ND 520 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 520 Fluoranthene 20644-0 ug/kg ND 520 Fluorene 86-73-7 ug/kg ND 520 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 520 Pyrene 129-00-0 ug/kg ND 520 Adjusted Ranges C9-C18 Aliphatics ug/kg 9870" 6200 C19-C36 Aliphatics ug/kg 55500" 8300 C11-C22 Aromatics ug/kg 185008 18000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 72 40-140% o-Terphenyl % 75 40-140% 2-Fluorobiphenyl % 81 40-140% 2-Bromonaphthalene % 69 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? 0 Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? No ❑ Yes-Details Attatched 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date . 5/10/2004 MADEP EPH FORM Aqueous Soil v' Sediment Other OBT70' Satisfactory Broken Leaking Itreo N/A nv PH <=2 H> Z FJ _ » Received on Ice FJ Received at 4 Deg. C Other Rec'd at 1.9 deg C actionYliletFioit� % SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: LIFT ESW(3-4) Lab ID: M39055-2 Method for Targets: MADEP EPH 98-1 Date Collected: 4/26/2004 Date Received: 4/26/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 4/29/2004 5/5/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 94.6 1 N/A Unadjusted Ranges CAS# Units Result RDL (q C11-C22 Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analytes 2-Methyinaphthalene 91-57-6 ug/kg ND 510 Phenanthrene 85-01-8 ug/kg ND 510 Acenaphthene 83-32-9 ug/kg ND 510 Naphthalene 91-20-3 ug/kg ND 510 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 510 Anthracene 120-12-7 ug/kg ND 510 Benzo(a)anthracene 56-55 3 ug/kg ND 510 Benzo(a)pyrene 50-32-8 ug/kg ND 510 Benzo(b)fluoranthene 205-99-2 ug/kg ND 510 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 510 Benzo(k)fluoranthene 207-08-9 ug/kg ND 510 Chrysene 218-01-9 ug/kg ND 510 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 510 Fluoranthene 206-44-0 ug/kg ND 510 Fluorene 86-73-7 ug/kg ND 510 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 510 Pyrene 129-00-0 ug/kg ND 510 Adjusted Ranges C9-C18 Aliphatics ug/kg ND" 6100 C19-C36 Aliphatics ug/kg ND" 8100 C11-C22 Aromatics ug/kg ND B 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 72 40-140% o-Terphenyl % 77 40-140% 2-Fluorobiphenyl % 82 40-140% 2-Bromonaphthalene % 70 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? V No ❑ Yes-.Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date' 5/10/2004 ® 495 TECHNOLOGY CENTER WEST • BUILDING ONE MARLBOROUGH,MA 01752 QUOTE N: �CCUTEST TEL:508-481-6200 - FAX.-508-481-7753 ACCUTEST CLIENT INFORMATION FACILITY INFORMATION ANALYTICAL INFORMATION MATRIX CODES ` DW• DRINKING `cLus �Ayo n WATER NAME PROJECT NAME r II i S ^,,q GW- GROUND ��L�O Z�/�y1V101.� ah. �/�'//i WATER -T-�_' WW• WASTE AD RESS // LOCATION WATER Hazd S �� 0/74 9 or <76q SO• SOIL CITY STATE ZIP PROJECT NO. -{� // SL• SLUDGE __s� L.l tl�', L Jam• �I'�� `f" 7a 7s'7 L I. OIL _ IO. OTHER SEND REPORT 7 ��-�� // UOUID PHONE# ��-S(�-S{7 yn FAX N � J (D t� soL•oTNER COLLECTION B PRESERVATION SOLID ACCUTEST SAMPLE p FIELD ID/POINT OF COLLECTION PATE TIME SAMPLED BY. g " LAB USE ONLY I 0140 w I p �11.1) i• Loc. 3.8 DATA TURNAROUND INFORMATION 6 DATA DELIVERABLE INFORMATION COMMENTGS/�REMARKS 14 DAYS STANDARD APPROVED BY: STANDARD E �/ UC1�1P Wee 1.,J " COS Cle ldY 7 DAYS RUSH ❑ COMMERCIAL B O 48 HOUR EMERGENCY O DISK DELIVERABLE - 7'0"]S-Y2 O OTHER ❑ STATE FORMS 14 DAY TURNAROUND HARDCOPY.EMERGENCY OR RUSH IS FAX O OTHER(SPECIFY) DATA UNLESS PREVIOUSLY APPROVED SAMPLE CUSTODY MUST BE DOCUMENTED BELOW EACH TI E SAMPLES CHANGE POSSESI N,INC UDING COURIE ELIVE Y RELINOUISHED BY S. MP DAT TIME: ECEWED BY: �/�- REU OUIS1jo B DAT ME ;f RECEIVEO �. [REL!INQE DAT T RECEIVED B R OUISHE Y: DA T1 D 8Y: l�s 3. 4. T4. TE RE E ED BY: g L PRESERVE WHERE APPUCABLE ON IC 5. 0 t�9 TEMPERATURE: ffinNew England 05/18/04 � %C=U MAY .. . . 1 S 1904 .. Techn�ca Repoi t for Shell Oil GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Accutest Job Number: M39304 Sampling Date: 05/04/04 Report to: Geologic Services Corporation 15 Bonazzoli Avenue Hudson, MA 01749 ATTN: Mike Bricher Total number of pages in report: 9 4�1%0 ACCpRO u - 4 Test results contained within this data package meet the requirements tea and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Certifications: MA(M-MA136) CT(PH-0109) NH(250203) RI(00071) ME(MA136) FL(E87579) NY(11791) NJ(MA926) IL(000589) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. New England 495 Tech Center West■ Building 1 0 Marlborough, MA 01752 ■ tel:508-481-6200 0 fax:508481-7753 ■http://www_accutest.rom Accutest Laboratories Sample Summary Shell Oil Job No: M39304 GSCMA:96925028 1140 Iyannough Rd. Hyannis MA Sample Collected _._ Matrix Client ..:.. .. ....:............... . ........... Number Date Time By Received Code Type Sample ID M393041 05/04/04 14:35 DG 05/10/04 SO Soil TAI�EK.211AST 7 M393042 05/04/04 13:55 DG 05/10/04 SO Soil TAAIK 2 WEST 7' ........................ ................................ v139.. 3 05/04/04 14:20 DG 05/10/04 SO Soil TANK 2 BOTT0141 12' Soil samples reported on a dry weight basis unless otherwise indicated on result page. J Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 2 EAST 7' Lab Sample ID: M39304-1 Date Sampled: 05/04/04 Matrix: SO - Soil Date Received: 05/10/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 92.1 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25873.D 1 05/15/04 SL 05/10/04 OP7134 GGH2373 Run#2 Initial Weight Final Volume Run#1 10.4 g 2.0 nil Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene I�1D 520 ug/kg 208-96-8 Acenaphthylene ND 520 ug/kg 120-12-7 Anthracene Np 520 ug/kg 56-55-3 Benzo(a)anthracene ND 520 ug/kg 50-32-8 Benzo(a)pyrene ND 520 ug/kg 205-99-2 Benzo(b)fluoranthene ND 520 ug/kg 191-24-2 Benzo(g,h,i)perylene ND.......;' 520 ug/kg 207-08-9 Benzo(k)fluoranthene IVD 520 ug/kg 218-01-9 Chrysene 520 ug/kg 53-70-3 Dibenz(a,h)anthracene ND...,.:,;<...;:.: 520 ug/kg 206-44-0 Fluoranthene ND 520 ug/kg 86-73-7 Fluorene hID 520 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 520 ug/kg 91-57-6 2-Methylnaphthalene ND 520 ug/kg 91-20-3 Naphthalene NA ,.: :,::: 520 ug/kg 85-01-8 Phenanthrene ND,::._ 520 ug/kg 129-00-0 Pyrene ND 520 ug/kg CI I-C22 Aromatics (Unadj ) ND .: . . 18000 ug/kg C9-C18 Aliphatics ND 6300 ug/kg C19-06 Aliphatics hID 8400 ug/kg CII-C22 Aromatics ND. .,,,.,,,,.; 18000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl40-140 321-60-8 2-Fluorobiphenyl 85% 40-140% 580-1.3-2 2-Bromonaphthalene 75% 40-140% 3386-33-2 1-Chlorooctadecane 60.%_. ;;;.._' 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page I of I Client Sample ID: TANK 2 WEST 7' Lab Sample ID: M39304-2 Date Sampled: 05/04/04 Matrix: SO - Soil Date Received: 05/10/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 93.5 Project: GSCMA:96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25874.D 1 05/15/04 SL 05/10/04 OP7134 GGH2373 Run#2 Initial Weight Final Volume Run#1 10.5 g 2.0 nil Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene ND 510 ug/kg 208-96-8 Acenaphthylene 1ID 510 ug/kg 120-12-7 Anthracene ND 510 ug/kg 56-55-3 Benzo(a)anthracene ND 510 ug/kg 50-32-8 Benzo(a)pyrene ND 510 ug/kg ND 205-99-2 Benzo(b)fluoranthene 510 ug/kg 191-24-2 Benzo(g,h,i)perylene h1D 510 ug/kg 207-08-9 Benzo(k)fluoranthene 510 ug/kg 218-01-9 Chrysene NII 510 ug/kg 53-70-3 Dibenz(a,h)anthracene I1D 510 u /k g g 206-44-0 FluorantheneID..:.::,; ;i510 ug/kg 86-73-7 Fluorene L\ID:. 510 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene NII 510. ug/kg 91-57-6 2-Methylnaphthalene ND 510 ug/kg 91-20-3 Naphthalene IrID 510 ug/kg 85-01-8 Phenanthrene ND 510 ug/kg 129-00-0 Pyrene ND 510 ug/kg CI I-C22 Aromatics(Unadi ) ND 17000 ug/kg C9-C18 Aliphatics ND.........;.._.< 6100 ug/kg C19-C36 Aliphatics ND 8200 ug/kg CI1-C22 Aromatics ND 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 85% 40-140% 321-60-8 2-Fluorobiphenyl ;85.%:;; „ 40-140% 580-13-2 2-Bromonaphthalene 70% 40-140% ..................... ......................... ........................ 3386-33-2 1-Chlorooctadecane 67% 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: TANK 2 BOTTOM 12' Lab Sample ID: M39304-3 Date Sampled: 05/04/04 Matrix: SO - Soil Date Received: 05/10/04 Method: MADEP EPH 98-1 SW846 3545 Percent Solids: 96.1 Project: GSCMA_96925028 1140 Iyannough Rd. Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 GH25875.1) 1 05/15/04 SL 05/10/04 OP7134 GGH2373 Run#2 Initial Weight Final Volume Run#1 10.5 g 2.0 m1 Run#2 CAS No. Compound Result RL Units Q 83-32-9 Acenaphthene `ND 500 ug/kg 208-96-8 Acenaphthylene ND 500 ug/kg 120-12-7 Anthracene ND 500 ug/kg 56-55-3 Benzo(a)anthracene ND 500 ug/kg 50-32.-8 Benzo(a)pyrene ND 500 ug/kg 205-99-2 Benzo(b)fluoranthene 500 ug/kg 191-2.4-2 Benzo(g,h,i)perylene ND 500 ug/kg 207-08-9 Benzo(k)fluoranthene ND 500 ug/kg 218-01-9 Chrysene ND-::,.,:--. 500 ug/kg 53-70-3 Dibenz(a,h)anthracene ND 500 ug/kg 206-44-0 Fluoranthene ND 500 ug/kg 86-73-7 Fluorene ND 500 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 500 ug/kg 91-57-6 2-Methylnaphthalene ND :1 500 ug/kg 91-20-3 Naphthalene ND 500 ug/kg 85-01-8 Phenanthrene I�1D 500 ug/kg 129-00-0 Pyrene ND 500 ug/kg CI I-C22 Aromatics (Unadj ) ND 17000 ug/kg C9-C18 Aliphatics ND 5900 ug/kg C 19-C36 Aliphatics ND 7900 ug/kg CII-C22 Aromatics ND 17000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 84-15-1 o-Terphenyl 75% 40-140% 321-60-8 2-Fluorobiphenyl 83% 40-140% 580-13-2 2-Bromonaphthalene 71% 40-140% 3386-33-2 1-Chlorooctadecane 59.%::.. ;... 40-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MADEP EPH FORM Matrix A ueous n Soil V Sediment F Other n Containers Satisfacto Broken I Leaking (�l ue`ous PcesenratIves; N/A Fv pH <=2 F PH > 2 Tero erature Received on Ice I-1 Received at 4 Deg.C F1 Other d Rec'd at 2.7 deg C Extraction Method SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: TANK 2 EAST 7' Lab ID: M39304-1 Method for Targets: MADEP EPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/10/2004 5/15/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 92.1 1 N/A Unadiusted Ranges CAS# Units Result RDL g C11-C22 Aromatics(Unadi.) ug/kg ND" 18000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 520 Phenanthrene 85-01-8 ug/kg ND 520 Acenaphthene 83-32-9 ug/kg ND 520 Naphthalene 91-20-3 ug/kg ND 520 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 520 Anthracene 120-12-7 ug/kg ND 520 Benzo(a)anthracene 56-55-3 ug/kg ND 520 Benzo(a)pyrene 50-32-8 ug/kg ND 520 Benzo(b)fluoranthene 205-99-2 ug/kg ND 520 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 520 Benzo(k)fluoranthene 207-08-9 ug/kg ND 520 Chrysene 218-01-9 ug/kg ND 520 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 520 Fluoranthene 206-44-0 ug/kg ND 520 Fluorene 86-73-7 ug/kg ND 520 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 520 Pyrene 129-00-0 ug/kg ND 520 Adiusted Ranges C9-C18 Aliphatics ug/kg ND A 6300 C19-C36 Aliphatics ug/kg ND" 8400 C11-C22 Aromatics ug/kg ND a 18000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 60 40-140% o-Terphenyl % 81 40-140% 2-Fluorobiphenyl % 85 40-140% 2-Bromonaphthalene % 75 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range.C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A'X qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? ❑d Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑d Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 MADEP EPH FORM MatY'Fix A clueous ❑ Soil IV Sediment F1 Other Contamets. Satisfactory Broken I Leakin A ueous:Preservatives' N/A FV PH <= 2 1 pH > 2 Tem'` erattire Received on Ice i Received at 4 Deg. C Other d Rec'd at 2.7 deg C Extiactton€Method SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: TANK 2 WEST 7' Lab ID: M39304-2 Method for Targets: MADEP EPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/10/2004 5/15/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 93.5 1 N/A Unadjusted Ranges CAS# Units Result RDL l� C11-C22 Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 510 Phenanthrene 85-01-8 ug/kg ND 510 Acenaphthene 83-32-9 ug/kg ND 510 Naphthalene 91-20-3 ug/kg ND 510 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 510 Anthracene 120-12-7 ug/kg ND 510 Benzo(a)anthracene 56-55-3 ug/kg ND 510 Benzo(a)pyrene 50-32-8 ug/kg ND 510 i Benzo(b)fluoranthene 205-99-2 ug/kg ND 510 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 510 Benzo(k)fluoranthene 207-08-9 ug/kg ND 510 Chrysene 218-01-9 ug/kg ND 510 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 510 Fluoranthene 206-44-0 ug/kg ND 510 Fluorene 86-73-7 ug/kg ND 510 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 510 Pyrene 129-00-0 ug/kg ND 510 Adiusted Ranges C9-C18 Aliphatics ug/kg ND" 6100 C19-C36 Aliphatics ug/kg ND" 8200 C11-C22 Aromatics ug/kg ND" 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 67 40-140% o-Terphenyl % 85 40-140% 2-Fluorobiphenyl % 85 40-140% 2-Bromonaphthalene % 70 40-140% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or Internal standards eluting in that range. C11-C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? ©No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 MADEP EPH FORM Mat Sediment Other A ueous Soil Containers: Satisfactory Broken F Leakin ❑ A ueous Pi.eservatives N/A H <=2 H> 2 Tem Odra Received on Ice Received at 4 Deg. C I i Other d Rec'd at 2.7 deg C ExtracttonMethod SW846 3545 Method for Ranges: MADEP EPH 98-1 Client ID: TANK 2 BOTTOM 12' Lab ID: M39304-3 Method for Targets: MADEP EPH 98-1 Date Collected: 5/4/2004 Date Received: 5/10/2004 EPH Surrogate Stds. Aliphatic: 1-Chlorooctadecane Date Extracted: First Date Run: Last Date Run: Aromatic o-Terphenyl 5/10/2004 5/15/2004 N/A EPH Fractionation 2-Fluorobiphenyl %Solids: Low Dilution: High Dilution: Surrogate Standards. 2-Bromonaphthalene 96.1 1 N/A IUnadiusted Ranges CAS# Units Result RDLr Q C11-C22 Aromatics(Unadj.) ug/kg ND" 17000 Diesel PAH Analytes 2-Methylnaphthalene 91-57-6 ug/kg ND 500 Phenanthrene 85-01-8 ug/kg ND 500 Acenaphthene 83-32-9 ug/kg ND 500 Naphthalene 91-20-3 ug/kg ND 500 Other Target PAH Analytes Acenaphthylene 208-96-8 ug/kg ND 500 Anthracene 120-12-7 ug/kg ND 500 Benzo(a)anthracene 56-55-3 ug/kg ND 500 Benzo(a)pyrene 50-32-8 ug/kg ND 500 Benzo(b)fluoranthene 205-99-2 ug/kg ND 500 Benzo(g,h,i)perylene 191-24-2 ug/kg ND 500 Benzo(k)fluoranthene 207-08-9 ug/kg ND 500 Chrysene 218-01-9 ug/kg ND 500 Dibenz(a,h)anthracene 53-70-3 ug/kg ND 500 Fluoranthene 206-44-0 ug/kg ND 500 Fluorene 86-73-7 ug/kg ND 500 Indeno(1,2,3-cd)pyrene 193-39-5 ug/kg ND 500 Pyrene 129-00-0 ug/kg ND 500 Adjusted Ranges C9-C18 Aliphatics ug/kg ND" 5900 C19-C36 Aliphatics ug/kg ND' 7900 C11-C22 Aromatics ug/kg ND a 17000 Surrogate Recoveries Acceptance Range 1-Chlorooctadecane % 59 40-140% o-Terphenyl % 75 40-140% 2-Fluorobiphenyl % 83 40-140% 2-Bromonaphthalene % 71 40-140% Footnotes 1 A Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting In that range. C11•C22 Aromatic Hydrocarbons exclude the concentration of Target PAH Analytes Z AV qualifier Indicates an estimated value Were all QA/QC procedures REQUIRED by the EPH Method followed? ❑d Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the EPH method,as specified in Sect.11.3? ❑d No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtainig the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature _ Postition Laboratory Director Printed Name Reza Tand Date 5/18/2004 495 Tech Center West,Bldg. 1,Marlboro, JJACCLffES-%- (508)481-6200 Fax: (508)481-7753 Accutest Job#: M3q3v Client Information Facility Information I �wf , Analytical information a. onsultants Name Project Name Geologic Services Corporation SOPUS Hyannis ddress Street ulty 15 Bonauoli Ave. 1140 I anou h Rd ae p State Hudson MA 01749 Hyannis MA ro ect Contact: Invoice Contact: Phone#: 978-568-8740 Invoice Phone# Fax#: 978-568-9316 Location ID# 100083 AFE# q6 I. 6A Collection Preservation #of = o z N w $ z Field ID/Point of Collection ate Time Sampled By Matrix bottles C Sh 7 23 x - 2- w -a Turnaround Information 01." � �'- ' >�,.�.' '• ,a1�, ' Data Deliverable Information '"c i ?w ' ' Accutest Log-in Information T)a &Std.14 Day Turnaround Approved By: Commercial"A" Q FULL CLP. v 5 c 7 Day EMERGENCY 0 Commercial"a" Q State Forms 4 Day EMERGENCY O Full Deliverables Q Disk Deliverable Format_ 3 Day EMERGENCY Other "se c a v 2 Day EMERGENCY / A 1 Day EMERGENCY l��C' !o Emergency T/A is for FAX or Lablink Data Commercial"A"-Results Only Sample Custody must bed cumented below each time saInples change posseslon•Including couriepereliv pu s y par Date e' Received a a e a e �me: ece ve y: 1 2 e nqu e y per, a ecery y: a e ime: ecerve o r 3 4 4 3e nq e y amp er �_ a e e ea reserve w ere epp oa e n ce OC emp. 5 5 O APPENDIX E Disposal Documentation 06/22i2004 08:30 EQ NORTHEAST. INC. 19785689316 N0.324 D02 i I E AI THEAST INC, 133 INDUSTRIAL ROAD 381 FmPFiELO ROAD 43 1/2 COLONY STREET WORK ORDE79 a FRO 80X 017 0 BOX 19788 SUITE 4,PO 80X BB3 WRENTHAM, MA 020 ORE, MD 21225 MEPIDEN, CT 06451 TFL 508484-8151 FAX 508.364• 8 TEL.41 • 55-7000 FAX 410.355 7768 TEL 109690?472 FAX 703630 2530 0761140, EPA I.D. X MAD064614136 — D.D.Y. A 157372 BILL TO: JOB#E100083 ORIGIN SAP# 1000e3 DESTINATION OTIVA ENTERPRISES, LLC MOTIVA ENTERPRISES, LLC. INTERNATIONAL PETROLEUM CORP 0. BOX 400199 TEXACO, 1140 IYANOUGH RD 505 SOUTH MARKET ST AMBRIDGE MA 02140-0002 HYANNIS, MA 02601 WILMINGTON, DE 19801 r ODY RENOUE (800) 222-2511 MERGENCY RESPONSE TEL.# 0 9300 MANIFEST/DOCUMENT NUMBER PICK-UP DATE 8 TIME I PURGaASE ORDER a FACILITY W/O k OFF LOAD DATE/TIME 076404 97431625 #UNITS TYPE HM DESCRIPTION OF ARTICLES OUANTITY PER UNIT AMOUNT , T X Petroleum pro ucts, n.o.s. , , UN G II G r ERG#126 () c 3.ql Contains approximate y ga ons of recovered product. or night call CHEMTREC at 1-800-424-9300 EQUIPMENT CERTIFICATION USTOMER VERIFIES THAT: TANKER # TRAILER ROLL-OFF CONTAINER # W/LINER? S CLEAN AND SUITABLE FOR THE TRANSPORTATION, STORAGE OR SERVICE TO BE PROVIDED. RIVER'S SIG. DATE: CUSTOMER'S SIG. DATE. PICK UP D TE TIME EXPLANATION OF L OADING TIME ARRIVE AT SHIPPER S A.• {i //D - " p w START LOADING Q 1L-P r FINISH LOADING L LEAVE SfrE HIPLICNT RECENED W APPARENT GOOD ORDER(CNttENTS AND CONDITION OF CONTENTS UNKNOWN) THIS IS TO CEPTIFY THAT THE ADO YE NAMED V ATERIALS ARE pRODERLY CIASSi{•IFD,DESCRIBED. LIWECT TO THE TERMS AND CONDITIONS OF THE UNI(QRM STRAIGHT BILL OF LADING AND ANY PACKAGED,MARKED AND LAOELED AND ARE IN PROPER CONDITION 6DR TRANSPOFTA110N MFINING GLASS)RCATIONS AN I FOFFS VtWFULLY ON FIE ON THE DATE OF SI'IIPMENi ACCORpJpI�TO THE AFPLI B EG�I pJ� �T�1E D tflT -!T Of Tl RTAjIQ� !WI S� � /l° G{� L r� RIVER: DATE:dizen-L SHIPPER: DATE: 6� DELIVERY DATE TIME EXPLANATION OF UNLOADING TIME ARRIVE AT SITE �Z/ BEGIN UNLOADING �- FINISH UNLOADIN13 LEAVE SITE RIVER: DATE: RECEIVER: AP DATE -D DDITIONAL INSTRUCTIONS OR COMMENTS GA-&-RI START TRIP(DATE&TIME) IP DATE 8 TIME aG __ _ _ SE BILL EQ NORTHEAST, INC. 06/22/2004 08:30 ED NORTHEAST. INC. a 19785689316 NO.324 UO3 E Q NORTHEAST INC 195 INDUSTRIAL ROAD 3510 FAIRFIELD ROAD 49 iR COLONY STREET WORK ORDER q PO BOX 617 PO BOX 10788 SUITE 4,PO BOX 899 WRENTHAM, MA 02083 BALTIMORE, MD 21225 MERIDEN, CT 06451 0771101 TEL.508-384-6751 FAX 508-384.6028 TEL.410-356.7000 FAX 410,955-7769 TEL 209-630•2472 FAX 203-630-2530 EPA 1.0. k MAD084014136 — D.O.T.# 157372 91L1.T0: JOBE100083 ORIGIN SAP# 100083 DESTINATION Ff(1i T�jj�FNTFRPAj� � T.L.C_ NORTH•ANn EWVI 0NN2H 'AL, TN(:- TaxACQ tldf] TYAtlXr_ct RD �Z5 �jTSVc nvr:►1(fF 781=6341) rERGENCY RESPONSE TEL.# 1-800- 24-9300 MAMPEST/DOCUMENT NUMBER PICK-UP DATE d TIM PURCHASE ORDER FACILITY W/0 e OFF LOAD DATE/TIME RIPR# 35158 0 07 UNITS TYPE. HM DESCRIPTION OF ARTICLES QUANTITY PER UNIT AMOUNT M X PAINT RELATED MATERIALS - LAB PACK( P EQUIPMENT CERTIFICATION USTOMER VERIFIES THAT: TANKER# TRAILER 8 . ROLL-OFF CONTAINER tt w11,1NEfl;.�- CLEAN AND SUITABLE FOR THE TRANSPORTATION, STORAGE OR SERVICE TO BE PROVIDED. RIVER'S SIG. DATE: CUSTOMER'S SIG. DATE: . �U DATE TIME `:;�XI4ANATI. N R ' 'Ap:IG TIME ARRIVE AT SHIPPER START LOADING FINISH LOADING LEAVE SITE + PNEM RECENED w AYPAREM GOOD ORDER ICONTLNYS AND CONDITION OF CONTENTS UNKNOWN) THIS 16 TO CERTIFY niAi THE A00�NAMEAR�.AAIRAOLSARE PROPEFiLV CIASSIFIEODESCA BED. EJECT TO THE TERMS ANO CONDITIONS OF THE UNIFORM STRAIGHT BILL OF LADINO AND ANY PACKAOED.MAPKED ANO LABELER CONDITION FOR TR ATION Tph10N VEPNING CLASS61CAT10NS AND TARIFFS LAWFULLY LE ON THE DATE OF SHIPMENT ACCORDING TO THE APPLICABLE PEOULATIONS OF THE DEPARTMENT OF TRANSPORTATION SOME, Inc behalf 11 Oil Products E.US�!e al RIVER: DATE: SIPPER: ` a, `Y NA , � IIQ'TIM i ARRIVE AT SITE .3 U BEGIN UNLOADING FINISH UNLOADING L DATE: 7 D7 R DATE: DITIONAL INSTRUCTIONS OR COMMENTS �Of.,paitt�f2eta�ad-i�geria e--R�tarf'r-0er�s -£-aPres�o-EQ� START TRIP DATE&TIME) FINISH TRIP DATE&TIME BPC 06/0242004 06/22/2004 Be:30 EQ NORTHEAST, INC. = 19785689316 N0.324 PO4 DEPARTMENT OF ENVIRONME�NT.AL MANAGEMENT Mer)rdouo Wa MsnifboQBsotlQn. s 235 P*gihade 9t ProWl}IPecp,RIQ2�09 E . d dpi dW on otue 0 tch) I (40.)1QW-2797. fob"AW..�W.'0"No.W4$ 3 FQ V S HeretoLIS EPA WNT grit.sl 2,psi i = IA onnanon one area s NK$ I F .T Dq A,n No. of{ nyt revuireo- Fe �yw bW 1. M'dY t:e ea lhed ty�3le lao S on rators Name" Mailing Addre A St IC.M I_V. O u .En„ K �DT1VA 1 I,, g'c. I If I v 4. 5. !6_aPO13NConpanY- . One A> umber t r rl' a odnpany .eme A is EPA 10 Numbor.7A X 9. nr - ity o* tind ite-,AJ46S UpptI5 lyumwr, .CCntmuiera.. 11;'US QUT.RriCription-(/arc%►�Itrp Propoi SAipping Name. ho.-id Coss, sndaD Mumber Tptal. unit e Quan i I !� (�rtSSI tiGQ �@f"Msgrtd Cl1Vled AbavEi) g. , K i:: • 't t A C 1 ' �0 u,l j 1� I 11' � � S4 I�fP • .1•µ,I�y7 td.,TTi' � I' -;�,;1�yq 6. t.� .•, AJ(l: A,j -lr 41'; ;: � .T:' 1 ,..i... t u• 11^1=}f�y �` � �:I I m a sn0ll*N Inb uctions god Additional.: In orha tan 6. a �P 6o�i bl BA6+e el n v o019 PPirv,' .= r es ec►s In r rar:Bondi toi^ runs st b ihi h ° cor I 'to caw, r pie d ifieQ• ;rparked', and labeled. a _are m all r p P 4P• f�.• Y 9 W3Y V" twftxnatoIll and nali"I goQernffi�M regulellons.. 2 1LL:(,am large puanUly:g alor I'ceerr��dy That.1.hhve proggSam in place to:.Iduce Itte olume'p'd loXlatyof i�as�egenerated to tire-degret�lhave determ wd.to be eoottmtrcally pra[aicable n'�ethod of gealn%pN, storage. or,dlposal currenUy avaltable to mt wtjwh�tm,r>�ze5$m p tl3�G future i OQ txurlan beallfa!and die en0ronmcni.Or ir.I aura small quan0y, I hatte made good faith ftrt;l6mmirr,6 r•rgywaste gC•r3erat,m"•atd"6diWO the.' bleat waMemarYdgetrt t method that i�avQaW-to rr*and (fiat I can allordi "' P tirod�TypW- Name Year r r .T edp'bme6l. of Rocp;pr`of .MaterYa s - y 2.t 3 Pripl /7 . Name :. - ,Signature = Mafirli bad Yee flan 2 E dg8ment or Receip, .nl elerlals O�tA Pri ed/TY Nem4 Sren�lure ; "s _ ndP.ft?± l - :CD .�'8U6p✓t�1Cr01 {r1dICe110n:SPBC� _- m u - - - ml: -.I[ NY .m., •Q.. F� GJwttbr Of operetor, Certlflcarion of f Ceipl of hazardous mjuerlels overVgl D 7inis mPni�@sr �itctipt as no�� ,r1i,` - - •� _ s _- I_ 1� I :. I� �- - psis rib t4eme ,pnalute Me„l� ppy y r 06/22/2004 09:30 EQ NORTHEAST, INC. 19785689316 NO.324 D05 E O NORTHEAST INC. 185 INDUSTRIAL ROAD 3510 FAIRFIELD ROAD 49 112 COLONY STREET WORK WRDEP 1 PO BOX 617 PO BOX 19706 SUITE 4,PO BOX 885 WRENTHAM, MA 02093 BALTlMORE, MO 21225 ME 0-2472 FAX 06451 O TEL,SW w-E151 FAX 508-384.6026 TEL.470-355.70M FAX 410.356-7789 1EL 209 6942472 FAX 1G36902590 EPA W. A MAD084814736 -- D.O.T. H 157372 BILI.T0:` JOB#E100083 ORIGIN SAP# 100083 DESTINATION I r lmr__ 183 ��S nTtp S RVF�NUE D�3 41 T vnn iTnlzTa >" AT neon nA3lTn WEEKS MERGENCY RESPONSE TEL, I-aoo-424-9100 ANIFESM000MENT NUM9ER PICK-UP DA E 8 TIME PURL A6E ORDER.17 FACILITY W/0 4 OFF LOAD DATE/TI E RIPR# 39362 L >1 UNITS TYPE HM DESCRIPTION OF ARTICLES QUANTITY PER UNIT AMOUNT OIL / OIL AND WATER(3D29166G) +� G i EQUIPMENT CERTIFICATION CUSTOMER VERIFIES THAT: TANKER# TRAILER # ROLL-OFF CONTAINER# IS CLEAN AND SUITABLE FOR THE TRANSPORTATION, STORAGE OR SERVICE TO BE PROVIDED, DRIVER'S SIG. DATE. CUSTOMER'S SIG. DATE: RICE .UP PATE, TIME EXPLANATION OF LOAD'iNG:TIME ARRIVE AT SHIPPER START LOADING FINISH LOADING LEAVE SITE 3 SHPMENT RECEIVED IN APPARENT GOOD ORDER(CONTENTS AND CONDITION OF CONTENTS UNKNOWN) TMIE IS TO CERTIFY THAT THE ABOVE NAMED MATERIALS ARE PROPERLY FOR AN RTATIED GUNECT TO THE TERMS AND CONDITIONS OF THE UNIFORM STRAIGHT BILL Of LADING AND ANY PACKAGED,MARKED AND LABELED AND ARE IN PROPER CONDITION FOR TRANSkORTAnD1 GOVERNING CLASSIFICATIONS AND TARIFFS IAWFl/LLY ON FILF E DATE Of SHIPMENT ACCORDING TO THE APPLICABLE REGuuTrONS OF THE DEPARTNTNT 0;7 TRANSPORTATION ERNE, Inc behalf 1 Oil Product& US G DRIVER: DATE: SHIPPER: tAT14N d4� lf�JlAfNP TIME RL�YY.: PATE ARRIVE AT SITE BEGIN UNLOADING FINISH UNLOADING LE DRIVER: �"`� DATE: `�d`f RECEIVER: DATE: —b ADDITIONAL INSTRUCTIONS OR COMMENTS Hydra&rc-krft Oil.-URN p � 0 ^ START TRIP DATE&TIME FINISH TRIP DATE a TIME BPC 06,06/201 06/22/2004 08:30 ED NORTHEAST. INC. a 19?85689316 NO.324 P06 DEPARTMENT O�ENVIRONMENTAL MANAGEMMT Hazardous Waste Manifest Section 236 Promenade Street,Providence,RI 02906 (401)222-2797 Form Approwrd.OMB Nu.2050-0039 r typo.. (Form dbelpned for use on elite(1 2-pitch)typewriler.) Nlf0RM H ZARDOUS enerator s ant Fe 2.page niamai:on SOON are3515 WASTE MANIFEST 9.� 5 Documen Nq. epuieo feay F¢oerallaw.DUi •' b of 1 nar oe reau red oy c at Izw o aanet'etors Name and Ma ling Addre6 A. Seale t✓far p n ber t7 �UUL VI.I. FiWll(:i3, US ion Sam US SIT 24, P "I ��`� ;_: &. :..: "..a? Lit 'TNGM YES AY IZS9O y -+ Generator's Phone 1 mnsponer I ompanY Name US EPA ID Number .. " :: r¢ f.l©/Lice sin raosponei Company ems 8. U5 EPA D umber p pp @r`s Pptp r t4`Trd9spoM®r-I 2Lfc rip,• ..�. ,� �,,. � Designated Faci ity Name and Site Address 10. US EPA D Number r �11 �Il b INC. 175 A3.MS AM= l' o�ilt�;l�1@Ilin dt 8 M . I TYf5.- on 12.Contsinors 13. 14. Pmay'` "r 1.US DOT Description(Including Proper Shipping Nome, Herard Closs. End/D Number, Total Umt No. Type Ouantity AVVolyya j . X&S&JCffUd M S7.Ji1'B REGID.AM OILY 1.I4OID, e 00 ILA d ortal'Dascr(ptions for Materials 1-is'led Above Narldlin CoUes for:Wasted.L IstpQ•.At3gve, iCA E: ..: � ., b Interm' j Ir q ( Final inlgr. Ins. �: d: i i� It•/ pacts endling nstructions end Additional In ormet on a. 76Wy UFf# 34361; INS# X/A m Fla"t� af$ered and VSDS accepted 4drt ie�tf�riea) � 6. R der sec re e T, n. f I to c I r ,,e u�lY a vr3l �iib v roper shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for libnsporl try highway according to applicants international and national government tegulalions. 11 I am a large Quantity generator, I Comity that I nave a program iri place to reduce Me volume and toxicity of waste generated to the degree I have determined to be economically practicable method of 1remment. storage or disposal currently available to me which minimizes the present and future threat to human health and the environment:or, it I am a small quantity, I have made good faith effon to minimize my waste gene-ration and select the, best waste management method(ha(is available to me and thal I can atford. Da1e Printed/Typod Name EW InSi t Q � � Monrn Day —, r i 7.Trans dgemont of Aecoipi of Materials t M Pri ed/Typtad Name Signets Monr.h pay Year — I 064 8.Trenspon er 2 Acknowledgement or Peceipt of Materiels Date Printed/Typed Name Signature monrn Day year Q 6 9. Discrepancy Indication Space C.11. 00 0.Full`Ownet or Opereror C®nification, of racelpt of halar0ou5 mOtonalsi covered by this manilas ercapt as noted to A hem 19. deco d yped Name 1 S gnetura; ice" kl Monrn Ody Yed nl+ i 06/22/2004 08:30 EQ NORTHEAST, INC. 19785689316 NO.324 Del s i i E Q NORTHEAST INC. 186 IA/Du6TRIAL ROAD 3610 FAIRFIELD ROAD 49 1/2 COLONY GTAEE7 WORK ORdER A PO BOX 617 F'O Box.19766 SUITE 4,PO BOX 883 WRENTHAM, MA 02093 BALTIMORE, MD 21225 MERIDEN, CT 06451 TEL. 508.9846151 FAX 588 584-60 9 TEL. 410i55.7000 FAX 410-35.5,7769 TEI,?03.6.90.247? FAX 203-630-2530 O O CPA I.D. A'MAD084674736 — D.O.T. 0 157372 ILL T0: J013 #E100083 ORK3INF1 SAP# 100083 DESTINATION VIVA ENTERPRISES, LLC MOTIVA ENIERPRII596, .LLB. NORTHLAND ENVIROM2 2AI,, 1 0x 400194 TEXACO, 1140 TYANDUGH RD 27S' ALLENS AVERMIF a LTr-Rp MA02_140-0062 HYAN'NIS, MA 02601 PROVTDEACR (401) 7R1-6340 PERGENCY RESPONSE TEL.# 0. F1-800-424-9300 _ AN fES /DOCUMENT NUMBER PICK-UP DATE&TIME I e-L)ACHASE ORDER# FACILITY W/O 0 OFF LOAD DATE/TIME I0000506 IRIPR# 35082 UNITS TYPE HM DESCRIPTION OF ARTICLES OUANTiTY PER UNIT AMOUNT OIL SOLIDS/DEBRIS/SLUDGES(3D24767G) 1� p i EQUIPMENT CERTIFICATION TOMER VERIFIES THAT. TANKER # TRAILER# ROLL-OFF CONTAINER # W INER? LEAN AND SUITABLE FOR THE TRANSPORTATION, STORAGE OR SERVICE TO 8E PROVIDED. EA'S SIG. DATE: CUSTOMER'S SIG. DATE: ' �-S�� �:•� ' 5 .���.•'.r, r 1'I�11,L� e I �� !1� �I_.'yM'c ��I. Ste."1 I�IW� _ i RIVE AT SHIPPER ART LOADING 16H LOADING VE SITE O RECENED IN APPARENT GOOD ORDER(CONTTENTS AND CONOMON OF CONTENTS UNKNOWN) THIS 15 TO CERTIFY THAT THE ABOVC NAMED MATERIALS ARE PROPERLY CLASSIFIED.DESCRIBM GT 10 THE TERLIS AND CONDMONS OF THE UNIFORM 6TRAIGHT BILL OF LADING AND ANY PACKAGED,MARRED AND LAMED AND ARG IN PROPER CONDITION FOR TRANSPORTATION DK�CLASSIFICATIONS AND TARIFFS LAWFULLY ON FILE ON T DATE OF SI.IIPMENT ACCORDING TO THE APPLICABLE RCCUTATIONS OF THE DEPP.RTMENI OF TRANSPORTATION EONS, Inc behalf A I Oil Products, OF R. DATE: 3 SHIPPER: DATE: '..:�r,, .ta1.c�`�tirt' I ..I,�.};?� '�'/t��, `'� I•�' o�'. :,�4 v a,�( .), �� � r >'4 RIVE AT SITE GIN UNLOADING ISH UNLOADING VE BITE ER.. DATE:b 4�L RECEI DATE: ZONAL INSTRUCTIONS OR COMMENTS 77f7 COW-VVa4er 5aperator St��ige-Retrrrm6erreretar CorerTo E fart RT TRIP ATE&TIME FINISH 7 IP DATE 8 TIME BPC 06/02/2004 06/222004 08:30 EQ NORTHEAST, INC. a 19785689316 NO.324 D08 DEPARTMENT OF ENVfRONMENTAL MANAGEMENT Haterdous Ifli Manifest Sbctlon - 235 Promenade Street,Proyldence,R102%8 :.rtTit G team desig►+ed to►use on tJlito 112•pnchl typewriter.) I ti 2z2 vg3 wrm Mprtxrep.OMB No.203>}oo3s . �. N ZAH�OUS Generator's s o. m g ant e s i 2.pa ®t nformimn in the soa0ea areas is poeu enl No. rim rc0uircd try raderal Ww, but WASTE MANIFEST .; z _ �. _S oft 1 nw eauuro ov;t.�1e aW o � - � "- .. •L�.via. 1:1�L:.� b,�"N.�i,Jj �..�,. - .,..'.� i 1 Ii .;l :JU�..Licil I<W Uf.�-_.....� ..� b6A tb�1�►�L-�i e, nqftftma Generator's Phone 4ft 2 rDnSportar 1 Company Narne 6 USEPAKINurribefTrens r]ei•10/Licerise Pletq nsperner 2 Co?npanV Name , 0 US EPAD Number er Q 7rgnsporte s P on Ef Sthl'e Transooner IDILrce�sq' f91e estpnated Facility Name and -Site Addiess 10. US EPA p um er JW 5NVI 7AI+, INC. F T�eps otZer's'Phone 1 ` A>= AY MS G FaoililyMA;u ®Radrjss F' F q iry s PhMOVID2992 By rine P 12 Containers 13 1 1.US DOT Description precluding Proper Shipping Name, Hazard C165s, and/D Number Total Unit Wast® Na No, Type 0uant MUSACUSSM STM REGUUTIM OILY' SOLID* eft D 00 n O Additional Descriptions For M31erial5 Llsled Abo,e K.:}landling Coles 1oi wa$tGS LislAd Above C j d09•01 `MM �EP � lPterim Final Inlenm: Final w j 4+r A.e+[. b I Fin C. b. pacts Hendltrlp Instructions end A ad(Jonaf In ormaUon rXwar4a sfferod M3018 acCOPt �driv* inzieLls) der- e Jrf ion , i I c ul a u o n o roper shipping rtame and are classified. packed, marked. a labeled, and are in al rEspf3cls it proper eonditlt7n IUr Iraraporl by hrynway aCCOr ing to appllcaWe. mloniational and national goyernmonl regulau ns. 11 1.am a large quantify generator. 1.cemly th I have a pfogfam in place to feauce the volume and toxicity of waste generaled to the Degree I have deti tminediQbe economically prariicatUfe melhod of treatment, slorarge of disposal curienuy availanie to me which minimizes the present iqd fufurq: threat ID hurt}an health and Ore environment or. if I am a Small quantity. I nuvo made gpod I@ilh etf,pn to minimize my w:3sle generatton and select Ihq, test waste management method that iS avadaWe'IC Inc and Thal I can allor0 Date 7idttad/Tytped dame $ �II .SIM" 411f e3 "Oi.1 Prodtuttab Us t�o.,th Osy- Year; - A IL-- cknowledpement of Peceipf of Malerials :. s P►inlad/Typed Name sign ro Month Day" Yeas! CW LA TraneRorter 2 Acknowledgement or Receipt of Materials D41e Printed/Typed Name Signature MonUt Osy yQpr� Q C3 Discrepancy lndica(ion Space (� CD Facilityy Owner or Operator Cenilication of receipt of hazardous maienali covered by Inis man,fest except as noted n Kern t8. � , rein yped Nerna , VOW Monti) DaY Ye