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HomeMy WebLinkAbout1140 IYANNOUGH ROAD/RTE132 - HAZMAT �i� `�7 ' ����y� � - - - . - • e-Ha.rdcopy 2.0 Autoutated Report New England 4 ........ ........ ,.- - w. .. __ �. ..... ....«...... t r t ._Iota €a t gig r 03/03/09 Teehh''ical Report for Shell Oil ----____ 'k SCMAW:96925028 (R NIBMA) 1140 Iyannough Road Hyannis ,-'. Ill's EQ711 Accutest Job Number: M80859 �; - —._� I l ' Sampling Drtes-: 02/17/09 - 02/18/09 Report to: Sovereign Consulting Inc. jsherburne@sovcon.com ATTN: Jason Sherburne Total number of pages in report: 63 \N 0 AC- oqy p4 a s • . o 74 / Test results contained within this data package meet the requirements eZaZhd of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. g Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) Y E A R S NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE EEOe. a This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. ®i Test results relate only to samples analyzed. New England • 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • http://www.accutest.com 1 of 63 1\ote: This report is password protected to disallow document modification or assembly. . . A password to unlock this report is available from your client service representative. UACCArrES-- M80859 Sections: Table ®f Contents -1- Section1: Sample Summary ................................................................................................... 3 Section2: Case Narrative/Conformance Summary .............................................................. 5 >. Suction3: Sample Results ........................ --...,.,...,.,...,...,,,.,.............,,......,....,....................-- 3,1.: M80859-1: MW-19 (55) ........................................ ... ... 7 3.2: M80859-2: MW-20 55 8 3.3: M80859-3: MW-21 55 9 3.4. M80859-4: MW-25 (72) ............................................................................................... 10 3.5: M80859-5: MW-26 (72) ............................................................................................... 11 3A M80859-6: MW-29 (68) ............................................................................................... 12 3.7. M80859-7: MW-29 (90) ............................................................................................... 13 3,8: M80859-8: MW-30 (35) ............................................................................................... 14 3.9: M80859-9: MW-30 (4) ........................: 3.10: M80859-10: MW-31 (55) ........................................................................................... 16 3.11.: M80859-11: MW-32 (55) ........................................................................................... 17 .1. : M80859-12: MW-34 (53) ........................................................................................... 18 3.1.3: M80859-13: MW-35 (53) ........................................................................................... 19 3.1.4: M80859-14: MW-37 (53) ........................................................................................... 20 3.15: M80859-15: MW-37 (90) ........................................................................................... 21 3.1.6: M80859-16: MW-37 (105) ......................................................................................... 22 3.1.7: M80859-17: MW-38 (104) ......................................................................................... 23 3.18: M80859-18: MW-38 (89) ............................................................................................ 24 3.19: M80859-19: MW-39 (88) ........................................................................................... 25 3.20: M80859-20: MW-40 (85) ........................................................................................... 26 12.1: M80859-21: RW-101 .................................................................................................. 27 3.22: M80859-22: RW-102 .................................................................................................. 28 Section4: Misc. Forms ............................................................................................................ 29 4.1: Chain of Custody ........................................................................................................... 30 4.2: MCP Form ..................................................................................................................... 32 4.3: VPH Form ...................................................................................................................... 33 4.4: Sample Tracking Chronicle ........................................................................................... 55 Section 5: G(:; Volatiles- QC Data Summaries ......................... 5.1.: Method Blank Summary ................................................................................................ 59 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 61 5.3: Surrogate Recovery Summaries ..................................................................................... 63 f 2 of 63 gJACCUrEM M80859 L 4 Accutest Laboratories Sample Summary Shell Oil Job No: M80859 SCMAW:96925028 (REIMBMA) 1140 lyannough Road Hyannis MA Project No: EQ 711 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M80859-1 02/17/09 11:50 RD 02/20/09 AQ Ground Water MW49(55) M80859-2 02/17/09 12:00 RD 02/20/09 AQ Ground Water MW-20(55) M80859-3 02/17/09 12:20 RD 02/20/09 AQ Ground Water MW-21 (55) M808594 02/17/09 13:20 RD 02/20/09 AQ Ground Water MW-25<(72) M80859-5 02/17/09 13:15 RD 02/20/09 AQ Ground Water IvIW726(72) M80859-6 02/17/09 14:20 RD 02/20/09 AQ Ground Water MW-29(68) M80859-7 02/17/09 14:40 RD 02/20/09 AQ Ground Water MW-29(90) M80859-8 02/17/09 13:40 RD 02/20/09 AQ Ground Water "MW-36(35) M80859-9 02/17/09 13:40 RD 02/20/09 AQ Ground Water MW-30(4) M80859-10 02/17/09 12:30 RD 02/20/09 AQ Ground Water MW-31 (55) M80859.11 02/17/09 11:15 RD 02/20/09 AQ Ground Water MW-32(55) M80859-12 02/18/09 08:20 RD 02/20/09 AQ Ground Water MW-34(53) M80859-13 02/18/09 09:20 RD 02/20/09 AQ Ground Water MW-35 (53) 3 of 63 1 _ '°P M80859 :. . ..........., Accutest Laboratories Sample Summary (continued) Shell Oil Job No: M80859 SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M80859-14 02/18/09 08:20 RD 02/20/09 AQ Ground Water NIW-37(53) M80859-15 02/18/09 09:30 RD 02/20/09 AQ Ground Water 1vIW-37(90) M80859-16 02/18/09 09:00 RD 02/20/09 AQ Ground Water MW-37(105) M80859-17 02/18/09 12:20 RD 02/20/09 AQ Ground Water MW-38(104) M8085-9-18 02/18/09 12:10 RD 02/20/09 AQ Ground Water MW-38 (89) M80859-19 02/18/09 11:15 RD 02/20/09 AQ Ground Water MW-39(88) M80859-20 02/18/09 11:00 RD 02/20/09 AQ Ground Water MW-40°(8'5) M80859-21 02/18/09 10:15 RD 02/20/09 AQ Ground Water RW-101' M80859-22 02/18/09 10:10 RD 02/20/09 AQ Ground Water RW-102 4 of 63 JOACC_.............................e M80859 _...... s S6kE9 ...........----- -................................................ . ...................... SAMPLE DELIVERY GROUP CASE NARRATIVE Client Shell Oil Job No M80859 Site: SCMAW:96925028(REIMBMA)11401yannough Road Hyannis MA Report Date 3/3/2009 2:36:47 PM 22 Sample(s) were collected on between,02/17/2009 and 02/18/2009 and were received at Accutest on 02/20/2009 properly preserved,at 1.8 Deg.C and intact. These Samples received an Accutest job number of M80859.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GBD1225 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GBD1226 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Note:Compounds whose QC limits are outside MCP criteria are designated by the lab as"Difficult".QC criteria for a"Difficult" compound may meet Accutest in-horse generated QC criteria but exceed MCP criteria(compounds exceeding Accutest QC criteria are flagged on the QC summary).Refer to the QC summary pages. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has arthorized the release of this report(M80859} Tuesday,March 03,2009 Page 1 of 1 5 of 63 M80859 New England IM k � AE a .. F ! .. .0 .t t.)r3 's 6 Section f�NL Sample Results Report of Analysis 6 of 63 UTEST. Accutest Laboratories Report of Analysis Page I of I � Client Sample ID: MW-19 (55) Lab Sample ID: M80859-1 Date Sampled: 02/17/09 i Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25619.D 1 02/26/09 AF n/a n/a GBD1225 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene NO . 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics(Unadj.) ND 50 ug/1 C9- C12 Aliphatics(Unadj.) ND 50 ug/1 C9- C10 Aromatics(Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits ......_.............___... . 615-59-8 2,5-Dibromotoluene 92%` ' 70-130% 615-59-8 2,5-Dibromotoluene '93%0 70-130% IUD= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 7 of 63 ` maoa59 f ....... ............ 808N! £91® 9 PEI r punodwoo E 3o aauaptna aAildwnsaid salnipul =N 32uEi uoileiggeo spaaaxa anleA saleaIpul =g xueiq poglaw paleioosse ui puno3 al�leue saleo!pul =g 1!wq Suploda-d —-M anleA palewilsa uE salEaipul —p paloolop TON =QN %0£1-OL %£6 auanlolowoiq!G-S`Z 8-69-919 %0£1-OL %I6,' auanlolowoigiQ-S`Z 8-69-919 sllwl7 Z#unH I#unH salaanoaaH ale2oaanS oil Sd3 I/$n 09 QN sailegdgd ZID -60 I/Sn 09 QN soggd►ld 8o -So I/$n OS CIK ('fpeun)soilrwOJV 010 -6D I/$n 09 CIN ( fpeurl)sailegdtjV ZID -6D I/fin OS a,N- (•fpeun)sailEgdgV 8o-So I/2n 07 UN aualxX-o 9-Lb-56 I/2n 07 (IN' oualXX-d`w I/$n 07 UN' auanlo L £-88-801 I/$n 0'£ (IN oualeglgdEN £-OZ-I6 I/$n 0'1 (IN iaglg [XIng 11aL lXgloW b-b0-b£9i I/$n 07 GR auazuagl,Cglg b-117-001 I/$n 07 GN auozuag Z-£b-IL shun 'IH llnsaH punodwoa 'ON Sdn lsll HdiA-VN Z#un-d lW 0,9 I#and awnloA Aind Z#and SZZIQSJ e/u E/u JV 60/9Z/ZO i Q'OZ99ZQg I#and 4aleg leall,fleud galeg da id ale([dud Stj paz,fleuv 3([ QI all3 vw stuuEXH PEON g2nouuE,Cl 0VI I (dWSW19-I) 8Z05Z696:MVWDS :laafoad E/n :spilos lumad i'l ARI HdA JFIGVW :poglaW 60/OZ/ZO :Panlaaa-d ale([ .[alert punwo-Od :xlalew 60/LI/ZO :PaldweS ale([ Z-69808W :([I aldweS qE I (SS)OZ-MW :([I aldweS lualla n I3O I 32Ed sisXpuV jo podag sauomiogE-1 lsalnaay Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-21 (55) Lab Sample ID: M80859-3 Date Sampled: 02/17/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25621.D 1 02/26/09 AF n/a n/a GBD1225 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l. C5- C8 Aliphatics(Unadj.) ND 50 ug/1 C9-C 12 Aliphatics(Unadj.) ND :50 ug/1 C9-C10 Aromatics(Unadj.) ND 50 ug/1 C5-C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 89% 70-130% 615-59-8 2,5-Dibromotoluene '90% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 9 of 69 W 'q . M80859 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-25 (72) . Lab Sample ID: M80859-4 Date Sampled: 02/17/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25622.D 1 02/26/09 AF n/a n/a GBD1225 Run#2 Purge Volume Rur_#1 5.0 ml Rur-_#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene !ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-.88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics(Unadj.) ND 50 ug/1 C9- C12 Aliphatics(Unadj.) ND, 50 ug/1 C9- C10 Aromatics(Unadj.) ND 50 ug/1 C5-C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 95% 70-130% 615-59-8 2,5-Dibromotoluene 93% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 10 of 63 M80859 Accutest Laboratories Report of Analysis Page 1 of I Ln Client Sample ID: MW-26(72) Lab Sample ID: M80859-5 Date Sampled: 02/17/09 Matrix: AQ -Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25623.D 1 02/26/09 AF n/a n/a GBD1225 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene .ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene NO 3.0 ug/1 108-88-3 Toluene "ND' 2.0 ug/I m,p-Xylene Nal 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics(Unadj.) ND 50 ug/1 C9-C12 Aliphatics(Unadj.) ND,. 50 ug/1 C9-C10 Aromatics(Unadj.) ND 50 ug/1 C5-C8 Aliphatics ND> 50 ug/1 C9-C12 Aliphatics ND' S0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 92% 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 11 of 63 JOACCUTEST ` M80859 :. Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-29 (68) Lab Sample ID: M80859-6 Date Sampled: 02/17/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25624.D 1 02/26/09 AF n/a n/a GBD1225 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 810 1.0 ug/1 91-20-3 Naphthalene ND- 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics(Unadj.) 62.1 .. 50 ug/1 C9-C 12 Aliphatics(Unadj.) ND< 50 ug/1 C9-C10 Aromatics(Unadj.) ND 50 ug/1 C5-C8 Aliphatics ND 50 ug/1 C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 93% 70-130% 615-59-8 2,5-Dibromotoluene 93% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound ' 12 of 63 CIACCUT_— -T M88859 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-29 (90) Lab Sample ID: M80859-7 Date Sampled: 02/17/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25625.D 1 02/26/09 AF n/a n/a GBD1225 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 1;6 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene NI) 2.0 ug/1 C5- C8 Aliphatics(Unadj.) 448 50 ug/I C9- C12 Aliphatics(Unadj.) ,ND 50 ug/I C9- CIO Aromatics(Unadj.) 'ND 50 ug/1 C5- C8 Aliphatics 446 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 86% 70-130% 615-59-8 2,5-Dibromotoluene 86% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 13 of 63 A ....... ............_:............' M80859 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-30(35) Lab Sample ID: M80859-8 Date Sampled: 02/17/09 Matrix: AQ - Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25626.D 1 02/26/09 AF n/a n/a GBD1225 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics(Unadj.) ND 50 ug/1 C9- C12 Aliphatics(Unadj.) ND 50 ug/1 C9- C10 Aromatics(Unadj.) ND= 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics 'ND .50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene '9'1% 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% ND= Not detected J= Indicates an estimated value ' RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound sa 14 of 63 T ............. M80859 :. . L Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW-30(4) Lab Sample ID: M80859-9 Date Sampled: 02/17/09 Matrix: AQ-Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25627.D 1 02/26/09 AF n/a n/a GBD1225 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether "ND" 1.0 ug/1 91-20-3 Naphthalene ND:," 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND= .2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics(Unadj.) ND 50 ug/l C9-C12 Aliphatics(Unadj.) ;ND 50 ug/l C9-C10 Aromatics(Unadj.) ND 50 ug/l C5-C8 Aliphatics ,ND 50 ug/l C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 90% 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 15 of 63 M80859 :..�..... .......i", Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-31 (55) Lab Sample ID: M80859-10 Date Sampled: 02/17/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25643.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether .ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene N,15' 2.0 ug/I C5- C8 Aliphatics(Unadj.) ND 50 ug/I C9- C12 Aliphatics(Unadj.) ND 50 ug/I C9- C10 Aromatics(Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9-C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 92%, 70-130%° 615-59-8 2,5-Dibromotoluene 91% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound Mfl 1s of 63 .... maoess :..3. . . Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-32 (55) 'w3 Lab Sample ID: M80859-11 Date Sampled: 02/17/09 Matrix: AQ-Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25644.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 .5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND- 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene NO 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5-C8 Aliphatics(Unadj.) ND 50 ug/I C9-C12 Aliphatics(Unadj.) ND 50 ug/I C9-C10 Aromatics(Unadj.) ND 50 ug/I C5-C8 Aliphatics ND 50 ug/l C9-C12 Aliphatics ND :50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 92% 70-130% 615-59-8 2,5-Dibromotoluene 91% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 17 of 63 MACCUTEST. M80859 :.' Accutest Laboratories w Report of Analysis Page I of I , Client Sample ID: MW-34(53) Lab Sample ID: M80859-12 Date Sampled: 02/18/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25645.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5-C8 Aliphatics(Unadj.) ND 50 ug/I C9-C12 Aliphatics(Unadj.) ND 50 ug/I C9-C10 Aromatics(Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run#2 Limits ... ............._..._..... 615-59-8 2,5-Dibromotoluene 94% 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 18 of 63 UAC.................................................. Accutest Laboratories t�s Report of Analysis Page 1 of 1 Client Sample ID: MW-35 (53) Lab Sample ID: M80859-13 Date Sampled: 02/18/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25646.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl.Ether 28:0 1.0 ug/l 91-20-3 Naphthalene NI)- 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics(Unadj.) ND, 50 ug/1 C9-C12 Aliphatics(Unadj.) ND" 50 ug/1 C9- C10 Aromatics(Unadj.) ND 50 ug/1 C5-C8 Aliphatics ND 50 ug/1 C9-C12 Aliphatics ND 50 ug/l .. ._.. ........ ... .. CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromot6luene 70-130% 615-59-8 2,5-Dibromotoluene 911% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 19 of 63 GACCUTES_T. Accutest Laboratories to Report of Analysis Page I of I , Client Sample ID: MW-37 (53) Lab Sample ID: M80859-14 Date Sampled: 02/18/09 Matrix: AQ-Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25647.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND: 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-2.0-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics(Unadj.) ND :50 ug/1 C9- C12 Aliphatics(Unadj.) ND 50 ug/1 C9- C10 Aromatics(Unadj.) ;ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics NO 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 93% 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound = 20 of 63 GJACCU. .............. _ ......_.m 69909W £9}® Lz lam punodwoo u 3o aauapiAa antldwnsaid saluoipul =N aSuui uoipuigquo spaaoxa anluA sapuoipal =g )Iuulq poglaw papuToossu ui puno3 apiluuu soluoipul =g piwi-1 Suipodo-d =-Fd onluA papuunISO uu sapuoipul —f palaalap TON =QN %M-OL %Z6 auonlopowojq!G-S`Z 8-69-919 %M-OL %Z6', auanlolowolgiQ-S'Z 8-65-519 slltul'I Z#und I#ung s311anoaa21 alu2ojjnS ON Sdi I/$n 09 QN souugdild ZID -6D 1/$n OS QN sa1lugdijV 83 -So I/Sn OS QN' ('fpuun)s3'Ww0iy 010-60 I/2n 09 QN (•fpuufl)solpugdild ZID-6D I/$n .09 QN ('fpuufl)soipugdily 8D-5o I/$n 07 (IN aualXX-o 9-L7-96 I/$n 07 QN' auojXX-d`w I/$n 07 QN auonlo L £-88-80I I/$n 0*£ GIN aualugpgduN £-OZ-16 I/$n 0•l (I'm jaglg 1XIn9 lia,L IfyaW t-t0-ttrE9 i I/Sn 07 QN ouozuoglXgpg t-It-001 I/Sn O'Z QN ouazuag Z-R-IL a sllull 'IH llnsall punodwoZ) oSI Sdi ls"I HdA-VLSI Z#and lUJ 0'9 1#and atunloA Aind Z#unN 9ZZIGEID u/u u/u dY 60/LZ/ZO I Q'8t99ZQ9 I#end plug luall,fluud galug daxd ale([daad Aft pazxluud AG QI aE3 yyg siuuBXH puo21 g3nouuuXl Otl i (VW9WIU) 8Z09Z696:MVW3S :laafoad u/u :spgoS lu33.1ad I'l AHN HdA dgUVW :poglaW 60/OZ/ZO :panlaaag aluQ njuM punoig -ad :xl.Ijvw 60/81/ZO :paldwuS alrQ 91-69808W :QI aldwuS qE l lei (06)L£-ANW :(1I alduiuS lua�_13 13o I 3212d SISSluuV 3o podag sayopuioquZ psapno:)d Ac.cutest Laboratories Report of Analysis Page I of I , Client Sample ID: MW-37(105) La'b Sample ID: M80859-16 Date Sampled: 02/18/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25649.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene "ND 2.0 ug/1 C5-C8 Aliphatics(Unadj.) ND 50 ug/I C9-C12 Aliphatics(Unadj.) ND. , ug/I C9- C10 Aromatics(Unadj.) ND• 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 92% 70-130% 615-.59-8 2,5-Dibromotoluene 91% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 22 of 63 A .......... ............... .... .e M80859 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-38 (104) Lab Sample ID: M80859-17 Date Sampled: 02/18/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028(REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25650.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND: 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene NI) 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics(Unadj.) ND 50 ug/1 C9- C12 Aliphatics(Unadj.) ND 50 ug/1 C9-C10 Aromatics('Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9-C12 Aliphatics ND 50 ug/1 . .. ..... ..... . CAS No. Surrogate Recoveries Run#I Run#2 Limits 615-59-8 2,5-Dibromotoluene 94% 70-130% 615-59-8 2,5-Dibromotoluene 93% " 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 23 of 63 M80859 .., _.....: :s Accutest Laboratories Report of Analysis Page I of I co Client Sample ID: MW-38 (89) Lab Sample ID: M80859-18 Date Sampled: 02/18/09a Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25651.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND, 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5-C8 Aliphatics(Unadj.) ND 50 ug/I C9- C12 Aliphatics(Unadj.) ND 50 ug/I C9- C10 Aromatics(Unadj.) ;ND 50 ug/l C5-C8 Aliphatics ND 50 ug/1 C9-C 12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 93% 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 24 of 63 M80859 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-39(88) Lab Sample ID: M80859-19 Date Sampled: 02/18/09 Matrix: AQ-Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25652.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-V PH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-8F-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics(Unadj) ND 50 ug/1 C9- C12 Aliphatics(Unadj.) ND 50 ug/1 C9-C10 Aromatics(Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND .50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene .93% 70-130% 615-59-8 2,5-Dibromotoluene 93% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 25 of 63 M80859 --.___...__..- T Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-40(85) Lab Sample ID: M80859-20 Date Sampled: 02/18/09 Matrix: AQ- Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25653.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND' 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene iND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics(Unadj.) ;ND 50 ug/1 C9-C12 Aliphatics(Unadj.) 'ND 50 ug/1 C9-CIO Aromatics(Unadj.) zND 50 ug/1 C5-C8 Aliphatics 'ND 50 ug/I C9-C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 93% 70-130% 615-59-8 2,5-Dibromotoluene `936/o 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound 26 of 63 T. ................................................ M80854 I Accutest Laboratories Report of Analysis Page I of I Client Sample ID: RW-101 Lab Sample ID: M80859-21 Date Sampled: 02/18/09 Matrix: AQ -Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028(REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25654.D 1 02/27/09 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene NO 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics(Unadj.) ND 50 ug/1 C9-C 12 Aliphatics(Unadj.) 4660 50 ug/1 C9-CIO Aromatics(Unadj.) 1090 50 ug/1 C5-C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics 3570` 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 95% 70-130% 615-59-8 2,5-Dibromotoluene 95% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound Mfg 27 of 63 .................................. M80859 :.. .. .. ...... .> Accutest Laboratories Report of Analysis Page I of I Client Sample ID: RW-102 Lab Sample ID: M80859-22 Date Sampled: 02/18/09 Matrix: AQ-Ground Water Date Received: 02/20/09 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:96925028(REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD25655.D 1 02/27/0.9 AF n/a n/a GBD1226 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND �-2.0 ug/1 100-41-4 Ethylbenzene ND" 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether Nl) 1.0 ug/1 91-20-3 Naphthalene ug/1 108-88-3 Toluene ;ND 2.0 ug/1 m,p-Xylene WD 2.0 ug/1 95-47-6 o-Xylene N',D 2.0 ug/1 C5-C8 Aliphatics(Unadj.) 50 ug/l C9-C12 Aliphatics(Unadj.) N&- 50 ug/1 .w� C9- C10 Aromatics(Unadj.) 50 ug/1- C5- C8 Aliphatics NE),."F::_h 50 ug/l C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run#1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 92% 70-130% 615-59-8 2,5-Dibromotoluene `929/o,, 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank _ E= Irdicates value exceeds calibration range N= Indicates presumptive evidence of a compound 28 of 6 IMACCAJTES.. M80859 ; ,. New England .................... Section 4 r Misc. Forms' Custody Documents and Other Forms Includes the following where applicable: • Certification Exceptions • Parameter Certifications(MA) • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle 29 of 63 ` M80859 i LAB(LOCATION) Shell Oil Products Chain Of Custody Record ::,,Please Check:—..10 8 1.t FilintS.ill TO:Cktxa:Naffia;� ::�INCIDE14T:#tENV-SERVICES):��COICHE.CKIFNOENM W#APP�ES ACCUMEST 6 ENV SERVICES K— M1 jjb=AIL .Dave.Weeks ................ ..9.....6. 9 21 51 01 2 1 8 DATE: Z117- TIF [0 LU ................ ...... ❑OTHER 10 OT.— 1,I Oj 01 01 81 31 1 GE: ( of Sovereign Consulting Inc 1140 lyannough Road,Hyannis,MA 905B South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Report to):Jason Sherbul CONSULTANT PROJECT NO.:EQ711 Mansfield,MA 02048 568.339.3200 508�.339324 � 'Sh.rbunTe(5)sovcon.com TURNAROUND TIME(CALENDAR—S): EjSrANoARD(j4QAY) 0 5mTS 03—S 0 2 DAYS 024HOURS REQUESTED ANALYSIS DELIVERABLES: 0 COMM C,COMB 0 mcp 0 POP 00TIiER(SPEC F)__ TEMPERATURE ON RECEIPT C- CA,,#1 lCod.#2 jc-I.r43 SPECIAL INSTRUCTIONS OR NOTES: .... SAMPLING ation containe—DR-di gs Field Sample Idontific DATE TINE IL or Laboratory Notes MW-19(55) Z/17 11fo Gw x z I x MW-20(55) _?J/7 x x MW-21(55) 2117 IM GW X x lza MW-25(72) GW x -W-W GW GW MW-26(72) GW x x M W-29(68) 2117 1q26 Gw x x 2117 Ift GW X x MW.29(90) *.Ili MW-30(35) 1?-117113* Gw Id I ja x MW-30(4) 141 ?IqO GW 1 .1 1 1 1 IR R.r.— (fg.—) Th. /y 6 M80859: Chain of Custody Page I of 2 30 of 63 NZACCUTEST. M80859 LAB(LOCATION) 4 Shell Oil Products Chain Of Custody Record .......;.;(?1698e:C6ebk:!aPPrdPr4ate:Btiz:::::::::: Print:BbtTo:Confaci'N;i*6;::::i::::::::::: :JNCIDENT#IENYBERYICESy: C]O. Nolxc,orrr.A�rDes 171— ❑ENv.semas ❑woIrvA RErAD ❑sxEu aErAn Dave Weeks 9 6 9 21 5 01218 ❑NOrNASD6o1 Q'COxSUlTANf ❑LleES .............. ....... ....... 7 '...0.,.. 0 8 3 ........... PAGE: or 0 ❑trRMR I.... ❑SXE11.DfoaINE ❑OTHER mw�.x��uw.wr R wmevlel,.N,ny.a Y.nl: " Sovereign Cons Iting Inc eR1140 I annou h Road Hyannis,MA 905E South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Repo"to):Jawn Sherburne CONSULTANT PROJECT NO.:EQ711 Mansfield,MA 02048 � i N Y508.339.3200 508.339.3248 isherburne(&sovcon.com I\A �l Jf sc i rIG �<rPA44 AYursoatx�©� 6= iNC(CA ENDARDA.. (re DAY) ❑5MY5 ❑2WY5 ❑2D- ❑24 lxwRs REQUESTED ANA'YSS OEUVERAOLEO. ❑cox.NA ❑Coeiw El— ❑RV ❑OMER(SPEL1F71 _..-.. TEMPk-n ON RECEIPT Cr Colter N, iDede,e2 (Cooler N3 SPECIAL INSTRUCTeONS OR TOTES SAMPLING uRNATN6 .... Field Sample Identification YAma No.of DATE TIME — = Centalm,PID Re1d1191 Mw or LeEorelery Notes / iW. NNOi HiEW NONE OixER T7f:: MW-3l(55) `'117 l-30 Gw x Z x 1:MW-32(55) Gw x x MW-34 53 ;�8 0VJ GIN x MW.35.(53) zn,bw 9`0 Gw X x MW-37(53) y19 OW Gw x x MW.37 90 Z0 ON Gw x x 6.MW-37(105) vis ON Gw x x MW-381U4) 709 (ZZD Gw x x MW-3 89) .-(!t' 1210 Gw x x MW-39(88) ..,)g 1115 Gw x % .`MW-40(85) 2/4 00 GW X % Rw-1o1 ?JIq 10l3 aw x x Rw-Ioz Gw x x nrq:weerl ...el <.ww:l�.a.,l D. - w`qu�e 1 Roe el.fsganl ``✓�J D+r /I Inw. // RNrywreo on IeW�'.1 oY.IW�!I m. M80859: Chain of Custody 'age 2 of 2 31 of 63 UAC............... EST. ................... M80859 . . w8085 MADEP VPH FORM Matux = A ueous Soil Sediment Other onfalners x.m�W. ; Satisfactor ✓ Broken F Leakin ueo'tas Pr.eseruatives-` N/A H <=2 H >2 hem ,eFature ." _, Received on Ice Received at 4 Deg. C Other Rec'd at 1.8 deg c Methanol N/A p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-19(55) Lab ID: M80859-1 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 2/26/2009 N/A x FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tent Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? OYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director i Printed Name Reza Tand Date 3/3/2009 IMEJ 33 of 63 M80859 :..,0 ....,., t � MADEP VPH FORM Matnx ! A ueous ✓ Soil Sediment Other Containers ... Satisfactory✓ Broken F Leakin A ueous Preservatlues= N/A H <=2 PH >2 El ferrt er,ature - Received on Ice Received at 4 Deg. C El Other ✓ Rec'd at 1.8 deg C Methanol r N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-20(55) Lab ID: M80859-2 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/26/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL' Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 91 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value ' Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 34 of 63 A .................... ._..._`T: ` M80859 i MADEP VPH FORM Matrix ,i: Aqueous ✓ Soil F1 Sediment Other Contaln'ers r u. Satjsfactor ✓ Broken Leaking A u.ei tas Pr�esec�ati," N/A H <=2 ✓ H >2El hem ,stature..._ �: Received on Ice Received at 4 Deg. C D Other ✓ Reed at 1.8 deg c Methanol N/A Method for Ranges MADEP VPH REV 1.1 Client ID: MW-21 (55) Lab ID: M80859-3 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A r 2/26/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 . ug/I ND 2 Methyl Tent Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 89 70-130% PID:2,5-Dibromotoluene % 90 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-CB Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C1oAromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tan Date 3/3/2009 MEJ 35 of 63 M80B59 MADEP VPH FORM Ilatrtx. A ueous ✓ Soil Sediment Other JO on'tainers Satisfactory✓ Broken F Leaking A ueaus Pr63sb�vattves N/A El PH <=2 PH >2 Tem Received on Ice Received at 4 Deg. C L1 Other ✓ Read at 1.8deg c M,et h an'o l N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-25(72) Lab ID: M80859-4 W Method for Target Analytes: MADEP VPH REV 1,1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ,µ PID: 2,5-Dibromotoluene N/A 2/26/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 95 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. Cg-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tan Date 3/3/2009 IMEJ 36 of 63 _.............._.. M80859 MADEP VPH FORM Matrix' ... Aqueous W Soil F Sediment F Other Go:ntainers Satisfactor Broken Leakin Ay ueo:u's Pre's:ervatives' N/A pH <=2 W P H >2 Tem erature� �` Received on Ice Received at 4 Deg. C Other El Read at 1.8 deg C MethanYol;- N/A P. - Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-26(72) Lab ID: M80859-5 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/26/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tart Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. - C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value _ Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No .❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 37 of 63 M80859 :.:,t' :.,, L_ - MADEP VPH FORM tX6; Aqueous �ti �r.. �. `' Soil Sediment Other M atr Containers '' Satisfactory Broken F Leaking A ueous„Preservatives N/A H <=2 H >2 Tem, erature„ ; Received on Ice D Received at 4 Deg. C Other Rec'd at 1.8 deg C MetharaQl ;,_ N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-29(68) Lab ID: M80859-6 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 2/26/2009 N/A FID: 2,5-131�bromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unad'Iusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 62.1" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 . C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 81 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibremotoluene % 93 70-130% PID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AU qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards fcr required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 36 of 63 CACCUTEST. M80859 MADEP VPH FORM MwrIX i Aqueous Soil Sediment Other Gontalners,,. Satisfactor Broken Leaking 'A ueous Pres`ervatives N/A H <=2 H >2 Tem 'eature Received on Ice Received at 4 Deg. C Other Rec'd at 1.8 deg C Methan°ol N/A � Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-29(90) Lab ID: M80859-7 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/26/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 448" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 1.6 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I 446 a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 86 70-130% PID:2,5-Dibrcmotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any,surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any.surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 MR 39 of 63 M80859 1.., MADEP VPH FORM M1111", dxzlml Aqueous Soil Sediment Other Containers " Satisfactor Broken Leakin A ueous Preser a IVA N/A El PH <=2 PH >2 em „erat,ure„ Received on Ice Received at 4 Deg. C Other ✓ Rec�d at 1.8 deg c M et h an_o l N/A p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-30(35) Lab ID: M80859-8 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/26/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/1 ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibrc•motoluene % 91 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑.I Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑d No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 40 of 63 GACCUTE_S M80859 a..3-.... ....,..'., MADEP VPH FORM Matnx E Acl ueous ✓ Soil Sediment Other Gontacners Satisfactor ✓ Broken FLeaking A ueoias PreserMiV"s N/A H <=2 ✓ PH >2 Tr M eeature_..�: Received on Ice Received at 4 De . C Other ✓ Read at 1.8 deg C Metiiar'ol N/A A Method for Ranges. MADEP VPH REV 1.1 Client ID: MW-30(4) Lab ID: M80859-9 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/26/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND A 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 90 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of CO-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 Ma 41 of 63 RACCUTEST. M80859 :.. . ...- MADEP VPH FORM MatriX.. ; y A ueous ✓ Soil Sediment 7 Other C.ontaiaers ___..W - W Satisfactory✓ Broken Leakin A ueous Preservatives. N/A El pH <=22 H >2 Tem ' Oture Received on Ice ElReceived at 4 Deg. C F Other ✓ Reed at 1.8 deg C Methanol N/A Method for Ranges. MADEP VPH REV 1.1 Client ID: MW-31 (55) Lab ID: M80859-10 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: `A PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? OYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 ffin 42 of 63 ............. M80859 <., .. MADEP VPH FORM Matnx.... A ueous ✓ Soil Sediment Other Gontalr`ers.. ....., Satisfactor ✓ Broken Leaking A Iueous Preservatives:: N/A El pH <=2 ✓ PH >2 El Tem stature Received on Ice Received at 4 Deg. C Other ✓ Rec'd at 1.8 deg C M,ethar�ol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-32(55) Lab ID: M80859-11 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/17/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 92 70-130% PID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 43 of 63 ................... .............. M80859 :. MADEP VPH FORM Matrix Aqueous ✓ Soil L Sediment Other Containers Satisfactor ✓ Broken F1 Leaking A mus Preservatives N/A H <=2 ✓ PH >2171 Received on Ice Received at 4 Deg. C F1 Other ✓ Read at 1.8 deg c Meth"ano1 N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-34(53) Lab ID: M80859-12 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 -' VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS 4 Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/1 ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tent Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 92 70-130% FID:2,5-Dibromotoluene % 94 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? FV7 Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 MEJ 44 of 63 MACCL................_................. M80859 :. MADEP VPH FORM Match.._: Aqueous ✓ Soil Sediment Other ConCaln'ers ` . Satisfactor ✓ Broken F Leaking A ueous Preservatives N/A F1 pH <=2 ✓ PH >2 Tern erat;ure Received on Ice U Received at 4 Deg. C r Other ✓ Redd at 1.8 deg C Methanol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-35(53) Lab ID: M80859-13 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 28 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 91 70-130% FID:2,5-Dibromotoluene % 91 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Postition Laboratory Director Signature Printed Name Reza Tand Date 3/3/2009 45 of 63 M80859 :., MADEP VPH FORM Matnx-W. Aqueous ✓ Soil El Sediment F1 Other Gontatiers Satisfactory✓ Broken Leaking] A ueo.us,Pres=ervatves:: N/A H <=2 PH >2 Tem ,erature Received on Ice Received at 4 Deg. C Other ✓ Rec'd at 1.8 deg C Metharol = N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(53) Lab ID: M80859-14 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug%I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 92 70-130% FID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AU qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. - Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 CMU 46 of 63 ................ ............................ M80859 L MADEP VPH FORM Matrix A queous ✓ Soil Sediment Other Cont'alners ..._.. Satisfactory✓ Broken F1 Leakin A ueous Preservatives N/A H <=2 ✓ H >2 Tem erature Received on Ice El Received at 4 Deg. C Other ✓ Rec'd at 1.8 deg C Mettianol N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(90) Lab ID: M80859-15 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tent Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND° 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 92 70-130% FID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 47 of 63 M80859 L MADEP VPH FORM Matnx Aqueous Soil F1 Sediment F1 Other Containers __ SatisfactoryFyl Broken F1 Leaking .Y A .u`eo:us P..resQrvatives N/A H <=2 H >2 Received on Ice ElReceived at 4 Deg. C Other Rec'd at 1.8 deg c Metlian'ol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(105) Lab ID: M80859-16 Ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tent Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 91 70-130% FID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 W 48 of 63 OACCU---_._._............._T Ma0859 MADEP VPH FORM Matnx-.`c. Ague ous Soil Sediment R Other Con"tamers SatisfactorF Broken F Leaking A i ueous Oreiervativesr N/A H <=2 PH >2 El m _e,r,,,ature Received on Ice Received at 4 Deg. C Other Rec�d at 1.8 deg c Te N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-38(104) Lab ID: M80859-17 [a Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 ';, VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 m,p-Xylene C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 93 70-130% FID:2,5-Dibromotoluene % 94 70-130% Footnotes A Hydrocarbon Rarge data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Rarge data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Rarge data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? OYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the infcrmation,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 MEJ 49 of 63 _S . ................_ ......� M80859 d MADEP VPH FORM Matux.= = A ueous ✓ Soil Sediment Other Containers Satisfactor ✓ Broken Leaking A u.eoasP.reseruativ'es N/A H <=2 ✓ H >2171 Tem" Ora tu .0 " Received on Ice Received at 4 De . C Other ✓ Rec'd at 1.8 deg c Wthan';0.1. N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-38(89) Lab ID: M80859-18 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/1 ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/1 ND` 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 93 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AU qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 fflfJ 50 of 63 IZACCUT_.........E...............e M80859 ;.., _...... .> _ MADEP VPH FORM MatnX-: . Aqueous Soil Sediment n Other ontai'iers � Satisfactor Broken Leaking A ueo;u€s{i?reseruataes'' N/A H <=2 H >2 Tem, ,er�ature - Received on Ice Received at 4 De . C Other Reed at 1.8 deg c Mettian'ol N/A � - Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-39(88) Lab ID: M80859-19 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 7143-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 93 70-130% FID:2,5-Dibrcmotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 IMEJ 51 of 63 T' ................................................. M80859 r, MADEP VPH FORM Matrtx.,,;, r Aqueous ✓ Soil Sediment Other Gont'afners..' _. SatisfactoryFyl Broken F Leaking A ueo:,tas,Pres'ervatly`es' N/A F PH <=2 ✓ PH >2 em _ rlature�; Received on Ice El Received at 4 Deg. C El Other ✓ Read at 1.8 deg c Methanol. . .'. N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-40(85) Lab ID: M80859-20 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Rancies CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tart Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 93 70-130% FID:2,5-Dibromotoluene % 93 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Malytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. .Z AV qualifier ind cates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Postition Laboratory Director Signature Printed Name Reza Tand Date 3/3/2009 2 of 63 12 _.__-- M80E59 :., MADEP VPH FORM Matnx, Aqueous ✓ Soil Sediment Other Containers- Sat isfactor ✓ Broken F Leaking A ueous PreservativesW' N/A El pH <=2 PH >2 El Tem _eil, ii;_ �t` ,` Received on Ice Received at 4 Deg. C Other ✓ Rec'd at 1.8 deg C Methianol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: RW-101 Lab ID: M80859-21 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dlibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dlibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I 4660" 50 C9-C10 Aromatics(Unadj.) N/A ug/I logo" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I 3570` 50 C5-C8 Aliphatics N/A ug/I ND s 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 95 70-130% FID:2,5-Dibromotoluene % 95 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 53 of 63 MACCUT_E`' T. ..._ M80859 MADEP VPH FORM Matnx '' Aqueous ✓ Soil Sediment 7 Other Con,t"wirers . SatisfactoryWe Leaking A ueo,us Preseruatluesl N/A H <=2 ✓ H >2 terra .erature Received on Ice Received at 4 Deg. C Other ✓ Rec�d at 1.8 deg c Meth'ariQl N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: RW-102 Lab ID: M80859-22 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 2/18/2009 Date Received: 2/20/2009 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 2/27/2009 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 92 70-130% FID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards fcr required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. - Signature Postition Laboratory Director Printed Name Reza Tand Date 3/3/2009 4 of 63 M80859 :. @ I Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M80859 SCMAW:96925028 (REIMBMA) 1140 lyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M80859-1 Collected;. 17-FEB 09 11:>.50 By pRD Received. 20=FEB 09° By: MW-19(55) w M80859-1 MADEP VPH REV 1.126-FEB-09 10:02 AF VMAVPH M80859-2 Collected% 17 F1 B 09 1200 By. RD Received 20 FEB-09`By MW-20 ....,,,,....,...,.,..m.. ,;.,w......wt....................au°.vu.aS:..,...,...:..xR�'�4.3.......,...�£�,..............;,x�✓ .,,,,...,. ,. ......,.tnu�wk»a :. .......o...a.v,.,.., ., - -_ »,...._.'�'.....¢..,_.: M80859-2 MADEP VPH REV 1.126-FEB-09 10:44 AF VMAVPH � � N18085,9 3 Collected17 FE$091�2 20By —RDr Rece�u�ed 20 FEB 097�iy MW 21 (55) d i<;W , M80859-3 MADEP VPH REV 1.126-FEB-09 11:25 AF VMAVPH M80859 4 C,ollected 17.FEB 09 13:20 By RD Rece ved .20 F4EBW09 By ; MW 25 M80859-4 MADEP VPH REV 1.126-FEB-09 12:07 AF VMAVPH M808559 Collect eived 20. E�B 09 By MW?6(72) s v P «.. ..... :. .... M80859-5 MADEP VPH REV 1.126-FEB-09 12:48 AF VMAVPH M80859 6 C©Ilected 17FEB 014 20 09 � M80859-6 MADEP VPH REV 1.126-FEB-09 13:29 AF VMAVPH _u� �.� M80859 7 Collected 17 FEB 09 14;40By RD Received 2Q=FEB,09. MW 29(90) ,ww � ,,. M80859-7 MADEP VPH REV 1.126-FEB-09 14:11 AF VMAVPH M80859 8� Collected 17 FEB 0913 40 ByRD Recezued 20 FEB-09 By. 47 u... y,:,mom» „w.. M80859-8 MADEP VPH REV 1.126-FEB-09 14:52 AF VMAVPH Page 1 of 3 MEJ 55 of 63 M80859 _ ....u> Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M80859 SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M808�9.9 '"Collected`. 17 FEB,09 1340 By:,RD;,;; Received�20A' FEB09, 'By h MW 30 4 M80859-9 MADEP VPH REV 1.126-FEB-09 15:33 AF VMAVPH M808'59 10 C,ollected 17,F,EB 09 12 30 By e�� Received 20 FEB 09a By ' , -. : ........_..... . . ,.a ., F .a Rom,.-• .... M80859-10 MADEP VPH REV 1.127-FEB-09 02:38 AF VMAVPH M80 , 5ByDR ivCed' 1FEB0911 -F 8-09, B 81 MW 32(55) 1 h M80859-11 MADEP VPH REV 1.127-FEB-09 03:20 AF VMAVPH _-: M80859 12 =Collected: 18 FEB 09 08 20 By.;RD Received 20-F B 09 By _ M . ._.._ __-.__ _._ -_ M80859-12 MADEP VPH REV 1.127-FEB-09 04:02 AF VMAVPH M80859 13 Collected 1+8 FEB 09 09 0 By RD Received 20 FEB�Wq By MAW �5 (53) M80859-13 MADEP VPH REV 1.127-FEB-09 04:43 AF VMAVPH M80859 14 Collected 18 FEB,�09 MW 3=7(53) Z M80859-14 MADEP VPH REV 1.127-FEB-09 05:25 AF VMAVPH M8089 15 Collected 18 FEB 09 09 30 ByRD�„•„= Recei ed fi20'FEB 09fBy ,,, .MAW,3�7(90),,,... �,.�.,� ..�, �- -,�,.._��:± . '�-� �� �:• �.a . - � .... �` I M80859-15 MADEP VPH REV 1.127-FEB-09 06:07 AF VMAVPH Iv1808�9 16 Collected R18 FE$09'0 00 By RD Receik e, FEB-09 By h hF M80859-16 MADEP VPH REV 1.127-FEB-09 06:49 AF VMAVPH Page 2 of 3 56 of 63 1 A ............ M80850 c Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M80859 SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M80859 17 Collected� 18 FEB09 1220 By RD Received 20EB09,',By. , M80859-17 MADEP VPH REV 1.127-FEB-09 07:31 AF VMAVPH M80859 alt8 Collected. 18 FEB 09�1�2 10�By� RD ;�R ce eived2®F�EB 09By� ' F� �� OK, "t It � M80859-18 MADEP VPH REV 1.127-FEB-09 08:13 AF VMAVPH M80859 19;Collected: 18 FEB 09 11 15 ByRD Received 2 By MW 39 M80859-19 MADEP VPH REV 1.127-FEB-09 08:55 AF VMAVPH �. �� � � M80859 20 Collected"18 FEB 0911 OOBy RD Received F EB W� M80859-20 MADEP VPH REV 1.127-FEB-09 09:36 AF VMAVPH M80859 211.,11Collected 18 FEB 09 10 135 By:";� Re e ed .20-FEB-09 Bye g k .,.. a ....... M80859-21 MADEP VPH REV 1.127-FEB-09 10:18 AF VMAVPH M80859 22,Collected 18FEB 09�10 0+ By IV 20 FEB 09By M80859-22 MADEP VPH REV 1.127-FEB-09 10:59 AF VMAVPH Page 3 of 3 57 of 63 [JACCUTEST. ................................................... New England 'i' � eelo5 i ..........., ..... a.. ,... ........... _ m........ GC Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries 58 of 63 M80859 ''0 c f. ., . ' Method Blank Summary Page I of I Job Number: M80859 Account: SHELLWIC Shell Oil Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1225-MB BD25612.D 1 02/26/09 AF n/a n/a GBD1225 cre The C reported here applies to the following samples: Method: MADEP VPH REV 1.1 Q P PP g P M80859-1, M80859-2, M80859-3, M80859-4, M80859-5, M80859-6, M80859-7, M80859-8, M80859-9 CAS No. Compound Result RL Units Q 71-43-2 Benzene `ND 2.0 ug/1 100-41-4 Ethylbenzene ND "- 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND. �'3.0 ug/1 108-88-3 Toluene Na 2.0 ug/1 m,p-Xylene ND 2.0. ug/1 95-47-6 o-Xylene ND' 2.0 ug/1 C5- C8 Aliphatics(Unadj.) ND 50 ug/1 C9- C12 Aliphatics(Unadl ) N`D 50 ug/1 C9-C10 Aromatics(Unad1 ) ND 50 ug/l C5- C8 Aliphatics ND .,, 50 ug/1 C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 92% 70-130% 615-59-8 2,5-Dibromotoluene 93% 70-130% F N 59 of 63 .......... ...._ MUM O r Method Blank Summary Page I of I Job Number: M80859 Account: SHELLWIC Shell Oil Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1226-MB BD25636.D 1 02/26/09 AF n/a n/a GBD1226 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M80859-10, M80859-11, M80859-12, M80859-13, M80859-14, M80859-15, M80859-16, M80859-17, M80859-18, M80859-19, M80859-20, M80859-21, M80859-22 CAS No. Compound Result RL Units Q 71-43-2 Benzene I�D,� 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether .ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-8.3-3 Toluene �ND 2.0 ug/1 m,p-Xylene hND 2.0 ug/1 95-47-6 o-XyleneND ' '2.0 ug/1 C5- C8 Aliphatics(Unadj.) N-D. 50 ug/1 C9-C12 Aliphatics(Unadj ) ND., 50 ug/1 C9-C10 Aromatics(Unadl.) ND-' , 50 ug/1 C5- C8 Aliphatics ND ,=. 50 ug/I C9-C12 Aliphatics ND - 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene �96%_ 70-130% 615-59-8 2,5-Dibromotoluene 93 6 70-130% 60 of 63 M80859 :, I v < Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M80859 Account: SHELLWIC Shell Oil Project: SCMAW:96925028(REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1225-BSP BD25613.D 1 02/26/09 AF n/a n/a GBD1225 GBD1:225-BSD BD25614.D 1 02/26/09 AF n/a n/a GBD1225 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M80859-1, M80859-2, M80859-3, M80859-4, M80859-5, M80859-6, M80859-7, M80859-8, M80859-9 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD 71-43-2 Benzene 50 51.2 402 50.5 101 1 70-130/25 100-41-4 Ethylbenzene 50 54.0 108 53.1 106 2 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 54.7 109 53.9 108 1 70-130/25 91-20-3 Naphthalene 50 49.4 99 50.8 102. �:3 70-130/25 108-88-3 Toluene 50 53.3 107 52.7 105 1 70-130/25 m,p-Xylene 100 108 '108 106 106 `2 70-130/25 95-47 6 o-Xylene 50 50.4101 49.4 9.-9 2 70-130/25 C5-C8 Aliphatics(Unadj.) 150 151 101 145 97 4 70-130/25 C9-C12 Aliphatics(Unadj.) 150 162 108 150 100 8 70-130/25 C9-C10 Aromatics(Unadj.) 50 54.0 108 ` ' 52.7 .105= 2- 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 93% 93%q 70-130% 615-59-8 2,5-Dibromotoluene 94% 92% 70-130% 61 of 63 M80859 i Blank Spike/Blank Spike Duplicate Summary Page I of 1 Job Number: M80859 Account: SHELLWIC Shell Oil Project: SCMAW:96925028(REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1226-BSP BD25637.D 1 02/26/09 AF n/a n/a GBD1226 GBD1226-BSD BD25638.D 1 02/26/09 AF n/a n/a GBD1226 to iv TheQC reported here applies to the following samples: Method: MADEP VPH REV 1.1 = M80859-10, M80859-11, M80859-12, M80859-13, M80859-14, M80859-15, M80859-16, M80859-17, M80859-18, M80859-19, M80859-20, M80859-21, M80859-22 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD 71-43-2 Benzene 50 50.8 102 50.3 101 1 70-130/25 100-41-4 Ethylbenzene 50 53.2 106 52.8 106 1 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 54.0 108 53.1 106 2 70-130/25 91-20-3 Naphthalene 50 48.5 97 49.4 99 2 70-130/25 108-88-3 Toluene 50 52.8 A06 52.5 105 1 70-130/25 m,p-Xylene 100 106 :106 105 1;05 r1 70-130/25 95-47-6 o-Xylene 50 49.6 '99 49.1 98' :; 1 70-130/25 C5- C8 Aliphatics(Unadj.) 150 148 99 146 97 1 70-130/25 C9-C12 Aliphatics(Unadj.) 150 161 107. 158 105 2 70-130/25 C9-C10 Aromatics(Unadj.) 50 52.8 106 52.2 104 1: 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 05% 95%0 70-130% 615-59-8 2,5-Dibromotoluene 94% 94% 70-130% 62 of 63 ZA ........... ............._..S.........m M80859 Volatile Surrogate Recovery Summary Page I of I Job Number: M80859 Account: SHELLWIC Shell Oil Project: SCMAW:96925028 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method ca Lab Lab Sample ID File ID S1 a Sl b M80859-1 BD25619.D 92.0 ,._, ',93.0 M80859-2 BD25620.D 91.0 93.0 M80859-3 BD25621.D 89.0' , !!90.0 M80859-4 131325622.D 95.0 93.0 M80859-5 BD25623.D 91.0 92.0 M80859-6 BD25624.D .93.0, 93.0 M80859-7 BD25625.D 86.0 M80859-8 BD25626.D 910 92.0 M80859-9 BD25627.D 90:°0' 92.0 M80859-10 BD25643.D 92:-0u, - 91.0 M80859-11 BD25644.D 92:0` 91.0 M80859-12 BD25645.D 94.0,.;,- ,92.0 M80859-13 BD25646.D �91.0,,,� "" 1191.0 M80859-14 BD25647.D 91,0 92.0 M80859-15 BD25648.D 92 0 ' '92.0 M80859-16 BD25649.D 92,0" "`rv=9 1.0 M80859-17 BD25650.D 94 0;; 93.0 M80859-18 BD25651.D 93 M80859-19 BD25652.D ;�93,0`° ' 93.0 M80859-20 BD25653.D 93.0=" M80859-21 BD25654.D :95.0' ;95.0 M80859-22 BD25655.D92.0 92.0 GBD 1225-BSD BD25614.D 93,0, 9 2.0 GBD 1225-BSP BD25613.D 93 r0,,, . 94.0 GBD 1225-MB BD25612.D 92 0.ts, 93.0 GBD 1226-BSD BD25638.D 45 0, r '94.0 GBD1226-BSP BD25637.D 95 0,, 94.0 GBD1226-MB BD25636.D 96 93.0 Surrogate Recovery Compounds Limits SI = 2,5-Dibromotoluene 70 13,0%0 (a)Recovery from GC signal#1 (b)Recovery from GC signal#2 63 of 63 _...._ M80859 SOVEREIGN CONSULTING INC . 3 January 6,2009 UPS#1Z 969 64F 03 9268 0296 Ms. Donna Z. Miorandi Town of Barnstable Public Health Division 200 Main Street Hyannis,MA 02601 Re: Groundwater Sampling Results,November 2008 In the Vicinity of: Former Texaco Service Station 1140 Iyannough Road RTN 4-11301 Dear Ms. Miorandi; Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH). A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVEREIGN NSULTING,INC. J/sonerburne m Project Manager i E cc: Mr.David Weeks,Motiva MassDEP-SERO Sovereign File-EQ711 6 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan BWSC 123 t This Notice is Related to Release Tracking Number 4� 11301 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Donna Miorandi 2. Street Address: 200 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ✓❑2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne Street Address: 905B South Main St., Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: Sherburne@sovcon.com NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. t e-Hardcopy 2.0 Automated Report r New England T. 4b Labc)raTomes {: �y ti� tx" 'rL ra t=zv. 12/15/08 ........................ -. . - w� .; , Teyc"hmcal Report Shell Oil .. SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA �y EQ 711 Accutest Job Number: M79098 Sampling Dates: 11/24/08 - 11/26/08 Report to: Sovereign Consulting Inc. jsherburne@sovcon.com ATTN: Jason Sherburne Total number of pages in report: 53 C\N ACC0RO V 6 _ - Test results contained within this data package meet the requirements eZa and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) kEn NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. 4 • Test results relate only to samples analyzed. New England • 495 Tech Center West • Building 1 • Marlborough,MA 01752 tel: 508-481-6200 fax: 508-481-7753 http://www.accutest.com Note:This report is password protected to disallow document modification or assembly. "u?l 1 3 of of 5 3 A password to unlock this report is available from your client service representative. M79098 Sections: Table of Contents -1- Section1: Sample Summary ................................................................................................... 3 Section 2: Case Narrative/Conformance Summary 5 Section 3• Sample Results 6 3.1: M79098-1: MW-29 (68) ............................................................................................... 7 3.2: M79098-2: MW-19 (55) ............................................................................................... 8 3.3: M79098-3: MW-31 (55) ............................................................................................... 9 3.4: M79098-4: MW-32 (55) ............................................................................................... 10 3.5: M79098-5: RW-102 ...................................................................................................... 11 3.6: M79098-6: MW-24 (42) ............................................................................................... 12 3.7: M79098-7: MW-26 (72) ............................................................................................... 13 3.8: M79098-8: MW-25 (72) ............................................................................................... 14 3.9: M79098-9: MW-39 (88) ............................................................................................... 15 3.10: M79098-10: MW-40 (85) .............................................................4............................. 16 3.11: M79098-11: MW-38 (89) ........................................................................................... 17 3.12: M79098-12: MW-38 (104) ......................................................................................... 18 3.13: M79098-13: MW-35 (53) ........................................................................................... 19 3.14: M79098-14: MW-34 (53) ........................................................................................... 20 3.15: M79098-15: MW-37 (53) ........................................................................................... 21 3.16: M79098-16: MW-20 (55) ........................................................................................... 22 3.17: M79098-17:J MW-21 (5 5) ........................................................................................... 23 3.18: M79098-18: MW-37 (90) ........................................................................................... 24 Section4: Misc. Forms ............................................................................................................ 25 4.1: Chain of Custody 26 ............................................................................................. i 4.2: MCP Form ..................................................................................................................... 28 4.3: VPH Form ...................................................................................................................... 29 4.4: Sample Tracking Chronicle ........................................................................................... 47 Section 5: GC Volatiles - QC Data Summaries ..................................................................... 50 5.1: Method Blank Summary ................................................................................................ 51 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 52 5.3: Surrogate Recovery Summaries ..................................................................................... 53 ua� 2 of 53 M79098 i Accutest Laboratories Sample Summary Shell Oil Job No: M79098 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID _.._ _ ......._. M79098-1 11/25/08 10:35 AW 12/02/08 AQ Ground Water MW-29'(68) ...._. _.._... ... .... ... M79098-2 11/25/08 10:00 AW 12/02/08 AQ Ground Water M79098-3 11/25/08 09:20AW 12/02/08 AQ Ground Water MW-31',(55) M79098-4 11/25/08 08:45 AW 12/02/08 AQ Ground Water MW-32'(55) M79098-5 11/24/08 10:15 AW 12/02/08 AQ Ground Water RW-102 M79098-6 11/24/08 11:45 AW 12/02/08 AQ Ground Water MW-24 (42) M79098-7 11/24/08 12:45 AW 12/02/08 AQ Ground Water MW-26 (72) M79698-8 11/24/08 13:30AW 12/02/08 AQ Ground Water MW-25'',(72) M79098-9 11/24/08 14:00 AW 12/02/08 AQ Ground Water MW-39 (88)` M79098-10 11/24/08 14:30 AW 12/02/08 AQ Ground Water MW,40 (85) M79098-11 11/24/08 15:00 AW 12/02/08 AQ Ground Water MW-38 (89) M79098-12 11/24/08 15:20 AW 12/02/08 AQ Ground Water MW-38 (104).; M79098-13 11/25/08 09:00 AW 12/02/08 AQ Ground Water MW-35 (53) 3of53 M79098 { Accutest Laboratories I i Sample Summary (continued) Shell Oil Job No: M79098 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Collected Matrix Client Number Date Tune By Received Code Type Sample ID M79098 14. . 11/25/08 09:45 AW 12/02/08 AQ Ground WaterMW34 =M7909& 15 11/25/08 10:45 AW 12/02/08 AQ Ground Water MW 37 (53) M7909,$46 !11/26/08 08:30 AW 12/02/08 AQ Ground Water MW-20r(55) M79098-17 11/26/08 09:35 AW 12/02/08 A Ground Water MW=21 55 Q ( .) M79098 18 11/26/08 10:35 AW 12/02/08 AQ Ground Water MW=37(90) i F 4of53 T M79098 `_a creto r:e, gmAkccuTssm SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M79098 Site: SCMAW:97346878(REIMBMA)1140 lyannough Road Hyannis MA Report Date 12/15/2008 10:52:23 AM 18 Sample(s)were collected on between 11/24/2008 and 11/26/2008 and were received at Accutest on 12/02/2008 properly preserved, at 2 Deg.C and intact. These Samples received an Accutest job number of M79098.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GBD1127 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. ® M79098-11:The pH of the sample aliquot for VOA analysis was>2 at tine of analysis. Note:Compounds whose QC limits are outside MCP criteria are designated by the lab as "Difficult'.QC criteria for a"Difficult" compound may meet Accutest in-house generated QC criteria but exceed MCP criteria(compounds exceeding Accutest QC criteria are flagged on the QC summary).Refer to the QC summary pages. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M79098). Monday,December 15,2008 Page 1 of 1 d; 5 of 53 T M79098 ---- -- Edda New England .x ..... 1 0 Lab ritori Section 3 y C .. W................. M .... .. _....._........ .. ..y ............. .,__.. ......_. .......... Sample Results Report of Analysis a� 6 of 53 M79098 Li orzYa r , Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW-29 (68) Lab Sample ID: M79098-1 Date Sampled: 11/25/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23711.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND ` 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 26.9 1.0 ug/1 91-20-3 Naphthalene r 3.0 ug/l 108-88-3 Toluene ND :'2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) NO. 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics NO 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 77% , 70-130% 615-59-8 2,5-Dibromotoluene 83% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 53 G Accutest Laboratories Report of Analysis Page 1 of I M. A Client Sample ID: MW-19 (55) Lab Sample ID: M79098-2 Date Sampled: 11/25/08 ;t Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV.1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23712.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether =ND 1.0 ug/1 91-20-3 Naphthalene =ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene N D 2.0 ug/1 95-47-6 o-Xylene N'U. 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 78% . 70-130% 615-59-8 2,5-Dibromotoluene 821% 70-130% F ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N Indicates presumptive evidence of a compound a 8 of 53 M79098 Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW-31 (55) Lab Sample ID: M79098-3 Date Sampled: 11/25/08 Pro' Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23713.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND. 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene NO 2.0 ug/I C5-C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9- C10 Aromatics(Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615 59-8 2,5 Dibromotoluene 82% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N= Indicates presumptive evidence of a compound ME] 9 of 53 1 'T> M79098 - Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-32 (55) Lab Sample ID: M79098-4 Date Sampled: 11/25/08 Matrix: AQ-.Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23714.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether NO 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 84% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 10of53 A M79098 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: RW-102 Lab Sample ID: M79098-5 Date Sampled: 11/24/08 Matrix.: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23715.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q _. ._ . ._...._............... 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene N D 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) N1) 50 ug/I C9- C12 Aliphatics (Unadj.) 79.8 50 ug/1 C9- CIO Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics "ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene 85%` 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 of 53 A► M79098 3- f Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-24 (42) ` "'' Lab Sample ID: M79098-6 Date Sampled: 11/24/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23716.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units P Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether NND �' 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene NO.:.: 2.0 ug/l m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene SO% 70-130% 615-59-8 2,5-Dibromotoluene 85% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound .6 12 of 53 Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW-26 (72) Lab Sample ID: M79098-7 Date Sampled: 11/24/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23717.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#'_ 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene "ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 20.7 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene NiD 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) NOD 50 ug/I C9- C12 Aliphatics (Unadj.) N'D 50 ug/I C9- C10 Aromatics (Unadj.) N'D 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 85% 70-130% ND = Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 53 M79098 ='--I- - - Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-25 (72) Lab Sample ID: M79098-8 Date Sampled: 11/24/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23718.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene N.D..... 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 2:4 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene N.D. 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 II CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 85% 70-130% ND= Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound .n 14 of 53 T. M79098 Accutest Laboratories Report of Analysis Page I of I Client:Sample ID: MW-39 (88) Lab Sample ID: M79098-9 Date Sampled: 11/24/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23719.1) 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2. MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene N'D 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I j 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-5 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) NO 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-5S-8 2,5-Dibromotoluene 79% 70-130% 615-55-8 2,5-Dibromotoluene 84% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound sae 15 of 53 AT M79098 Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-40 (85) Lab Sample ID: M79098-10 Date Sampled: 11/24/08 Matrix: AQ -Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23720.D I 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND::,::" 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether N'D 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 12.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) N'D 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 78% 70-130% 615-59-8 2,5-Dibromotoluene 84% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MIN 16 of 53 M79098 _ .... .._. Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-38 (89) Lab Sample ID: M79098-11 Date Sampled: 11/24/08 LI Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a BD23721.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene Nil =2.0 ug/1 100-41-4 Ethylbenzene ND '2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene N=D ;3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47 6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9-C10 Aromatics(Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 4 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene 85% 70-130% (a)The pH of the sample aliquot for VOA analysis was> 2 at time of analysis. ND= Not detected J= Indicates an estimated value r RL= Reporting Limit B= Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound I 17 of 53 M79098 =-- Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-38 (104) Lab Sample ID: M79098-12 Date Sampled: 11/24/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW;97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23722.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene W ND2.0 ug/1 100-41-4 Ethylbenzene ND . :" 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene NO 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND '2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND n 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene il9 70-130% 615-59-8 2,5-Dibromotoluene 84%.__ ', '` 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 53 M79098 Accutest Laboratories Report of Analysis Page 1 of 1 ; Client Sample ID: MW-35 (53) '<r Lab Sample ID: M79098-13 Date Sampled: 11/25/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23723.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q ._-__.___.___..__._......._... 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND. 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene Z1 70-130% 615-59-8 2,5-Dibromotoluene 7'8% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound k 19 of 53 Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW-34 (53) 1: Lab Sample ID: M79098-14 Date Sampled: 11/25/08 '`'''"" Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23724.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND . 2.0 ug/1 .._........ 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 I'. m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) :ND 50 ug/l C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene !71% 70 130% 615-59-8 2,5-Dibromotoluene 77% 70-130% ND= Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ffin 20 of 53 IRACCUTEST M79098 bore; ryes A.ccutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-37 (53) M NI Lab Sample ID: M79098-15 Date Sampled: I1/25/08 Matrix: AQ-Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23725.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND "2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether NDI 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND__ 50 ug/I C5- C8 Aliphatics NDI 50 ug/I C9-C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene 84% 70-130% ND = Not detected J= Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound "a 21 of 53 M79098 �' = ^- t^'; o a Accutest Laboratories c�a Report of Analysis Page 1 of 1 Client Sample ID: MW-20 (55) Lab Sample ID: M79098-16 Date Sampled: 11/26/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23726.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene N D 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/I . .. ..._ .:.. 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics 'ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene :78% 70-130% 615-59-8 2,5-Dibromotoluene 84% 70-130% ND = Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 22 of 53 MACCUTEBT. M79098 Accuteat Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-21 (55) Lab Sample ID: M79098-17 Date Sampled: 11/26/08 Matrix: AQ- Grounl Water Date Received: 12/02/08 Method: MADEP VFH REV 1.1 Percent Solids: n/a Project: SCMAW:9i346878 (REIMBMA) 1140 lyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD23727.D 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND,- 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5-C8 Aliphatics iUnadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) NQ 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene 83% 70-130% M ND = Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E= Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Ma 23 of 53 A M79098 Accutest Laboratories c� Report of Analysis Page I of 1 00 Client Sample ID: MW-37 (90) Lab Sample ID: M79098-18 Date Sampled: 11/26/08 Matrix: AQ- Ground Water Date Received: 12/02/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 131323728.1) 1 12/05/08 AF n/a n/a GBD1127 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units P Q 71-43-2 Benzene ND,,:: 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene NO 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.; ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 72% 70-130% 615-59-8 2,5-Dibromotoluene 79% 70-130% ND = Not detected J = Indicates an estimated value RL= Reporting Limit B= Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 24 of 53 QACCUTEST M79098 e m New England MACCUTEST, Lc._ornlori e , .. - Section 1Vlisc ,Forms Custody Documents and Other Forms Includes the following where applicable: • Certification Exceptions • Parameter Certifications (MA) • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle I I 25 of 53 T M79098 - -- LAB(LOCATION) 4 Shell Oil Products Chain Of Custody Record Please Check'A pro'riatc.96k Print Bill To Contact Name INCIDENT#(ENV SERVICES) in u•LrK Ir No x¢EN a AwuES ICI En A ❑ Dnvn ET n � .. ... _ _ n AccurPSr _ _ Dave Weeks 9 6 9 Z 5 012 8 DATE' � j l Icnva sns,.I I O[unsuL A ...—�LJ wBE[ ;::PO # .: SAP# 1 .. .._. .. .. .--.- PAGE: I Df �� - - � . ._ ❑DIIILN( -_-. _ ..,_,-,_� ❑SHCLL PIP�LI4E I-DTHE't lna,uh '1 01 01 01 81 3 ru�arNn co-+..:., If.nrmnrvs Is ..a Bmlq: Sovereign Consulting Inc .. -- --- ---------- 11401 annough Road,Hyannis,MA A - 905B South Main Street,Unit 202 CONSIILTANT PROJECT CONTACT(Report In):.lason Sherbum CONSULTANT PROJECT NO.:EO/11 s Mansfield,MA 02048 ue:tuse oNLr 5D8.339.3200 508.339.3248 she ume@sovcon.com v - (/�Wr•�ry �eti LC:( 4 �P�. 4 / 7 TURNAROUND TIMC(CALENDAR DArti): I�STANDARD(14 DAY) LJ 5 DAYS ❑3 DArs ❑2 DAr5 ❑2.HOURS REOUESTE NALVSIS DELIVERABLES. ❑co— LJ COmme M mrP ❑arc ❑OTHER(5PECIPf) TEMPERATURE ON RECCIPI C° b.,1 xl ;0001-2 :ruin,— SPECIAL INSTRUCTIONS OR NOTES: SAMP LING sae:: Field Sample Identification BATE TIME ,AATRIM nN a comAINA.PIO Ra.aIP9: NI V; :ICE HNG9 N]EOA.vUrIE,• 7 i n,Lab—tory NO— Z Mw-1`i lb.5 't�7 CIO ---- W A5 17.2 -- -9 w- 3'l l K_ -..._ - 5.1 3,541 -/p Mw 4 tld i y 7 v V V I<ai yu:.eJ ev 1'.nnliim.l; Rccv�a.a�y 1"ianorti:c; �. n,. n �H M79098: Chain of Custody Page 1 of 2 '0 26 of 53 T M79098 acar::t� LAS(LOCATION) Shell Oil Products Chain Of Custody Record Please Check Appro rlato.Bqx PHift Rill.To Contact Name: :,:i INCIDENT#(ENV SERVICES) F, '1 r.0 N11 wCiuLNI 4 A-- ,ioTw -U= AI Dave Weeks 9]6F91 21 51 01 2 L8 OATS III 130.# s4p,It . .... ... PAGE: of ------------j I C1�ELF PHINE AFU O7-k —rJ 1 01 01 01 81 31 1 Sovereign Consulting Inc 1140 Iyannough Road,Hyannis,MA 9056 South Main Street,Unit 202 CIONS1.11 TANT PROJECT CONTACT(Report to):.1-on Sherbum CONSULTANT PROJECT NO EQ?11 Mansfield,MA 02048 8.339.3200 I 508.339.3248 jshwburfw@- QAtmJz—r. G*'O"�, 7q0?— -.�A.Ot- -T 1—11.——,) t�j REQUESTE=YSIS --(',;�'Y) 0,.,� Li 3—s Ll 1.11 U 21�URS 0,:U- Dco— Fl MCP 0 K,, UoIt-tf:;,(gu'm TEMPERATURE ON ACCCIPI R2 1coo—, SPECIAL INSTRUCTIONS OR NOTES; SAMPLING PRESERVATIVE Field Sample Identification ntII..1 PID R..dl.p Usf. DATE TIME j or L.h......Y NoW. GW x 2 X 7!777�7r 'Ijx CI-quo 6� x -3 ujut5 C tj 14, 'S J. X 6 W 6;cd 6 M79098: Chain of Custody Page 2 of 2 as 27 of 53 UACCLMEBT. M79098 Massachusetts Department BWSC-CAM Exhibit VII A-1 LI of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 N Title: MADEP MCP Response Action Analytical Report Certification Form b..., Xt2EF�l�iYPififfa=-- tod, ep erklficatr 1=c� a04 NUL _.MR 40 It, 2 '_ ..... f „w� g Laboratory Name: Accutest Laboratories of New England Project#: M79098 Project Location: SCMAW:97346878(REIMBMA)1140 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M79098-1,M79098-10,M79098-11,M79098-12,M79098-13,M79098-14,M79098-15,M79098-16 M79098-17,M79098-18,M79098-2,M79098-3,M79098-4,M79098-5,M79098-6,M79098-7 M79098-8,M79098-9 Sample Matrices: Groundwater X Soil/Sediment () Drinking Water () Other: () () MCP Wts 8260E 8151 A__L 8330_L 6010E 7470A/1 A ettc;ds�!`sed a 8270C 8081 A VPH X 6020 9014M /is specifiecj}n MADf P 8082 8021 B EPH 7000 S s 7196A 0 p9ndrunl of 1 L1$ le$ a Eraccin-Numq�PJRTN= if I,c,,Dwn y� r ;� Analytical Methods 2 M�SW 846 Method9(i1AX At7EP Phystologicaljy Av�atlable, ya ide(,PAC}Method •„ ' Checkal l tllatir �i 3 55f 846(Wgtho740nesLrst IndividU I m', tfritl;an analy{<: An affirmative response to questions A, B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with Yes ❑ No that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and ❑ Yes ❑ No discuss in a narrative QC data that did not meet appropriate performance standards orguidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty", as described in Section 2.0(a), (b), (c)and i] Yes ❑No (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only: Was the VPH or EPH method run without i] Yes ❑No significant modifications,as specified in Section 11.3? A response to questions E and Fbelow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the J Yes LI No specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified El Yes L No method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is, to the best of my knowledge and belief,accurate and complete. Signature: /' Position: Laboratory Director Printed Name: Reza Tand Date: 12/15/2008 Mel 28 of 53 IRACCMTE.ST. MADEP VPH FORM Mat tr z u Aqueous n Soil ❑ Sediment ❑ Other ❑ Contatners Satisfactor n Broken ❑ Leakin AM ueou Pre srua IVA N/A ❑ H<=2 PI PH>2 ❑ Received on Ice ❑ Received at 4 De . C ❑ Other J Reo'd at 2 deg c Methanol' ' '' N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-29(68) Lab ID: M79098-1 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 26.9 1 Benzene 71-43-2 C5-C8 ug/1 ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and g' complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 Y.g 29 of 53 M79098 '--- - --- MADEP VPH FORM Aqueous n Soil 7 Sediment F Other Container ON Satisfacto ✓ Broken Leakin Aueou""§ Pce"seruatues N/A n pH<=2 ✓ H>2 Terri erature .,, ; : Received on Ice n Received at 4 De . C Other ✓ Rec'd at 2 deg C Meth' WZ N/A 4 Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-19(55) Lab ID: M79098-2 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# , Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 78 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-010 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Iy Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W1 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature- Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 Ma 30 of 53 A M79098 MADEP VPH FORM Matrixk Aqueous n Soil n Sediment ❑ Other ❑ Containers Satisfacto n Broken ❑ Leakin taeous PceservativeW N/A F I PH <=2 F1 oH>2 TAM- erature Received on Ice F Received at 4 Deg. C Other n Rec'd at 2 deg C Methanol . : N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-31 (55) Lab ID: M79098-3 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 1 2/512 0 0 8 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 i Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 Ug/1 ND 2 Naphthalene 91-20-3 N/A Ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:25-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? IVD No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 MEJ 31 of 53 A M79098 - MADEP VPH FORM Aciueous ✓ Soil P Sediment I-1 Other Containers 3 Satisfactor ✓ Broken Leakin = ueovs Prese u fives; N/A DH<=2 ✓ DH>2 Tem060"ature "; „ Received on Ice Received at 4 Deg. C Other ✓ Rec'd at 2 deg C Methanol F N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-32(55) Lab ID: M79098-4 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/l ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug%l ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 84 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-0-10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 MEJ 32 of 53 12ACCLffEST. M79098 - - - MADEP VPH FORM Matnx A ueous I� Soil ❑ Sediment ❑ Other ❑ Contatners�... fir: Satisfactor n Broken ❑ Leakin ❑ l A u.eoisPreservativ. N/A El DH<=2 DH>2 Tem eature �. Received on Ice I Received at 4 De .C Other J Read at 2 deg c Methanol , N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: RW-102 Lab ID: M79098-5 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/24/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last.Date Run: , PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 79.8 A 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 85 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑J Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑J Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 Q 33 of 53 M79098 --- it i MADEP VPH FORM Matrtxz:• _ Aclueous Soil I-1 Sediment F Other F1 Contaii cs.. Satisfactory F41 Broken F1 Leaking W ueou'""kPreset av 6s;l N/A H<=2 n DH >2 Te Received on Ice ❑ Received at 4 Deg. C Other d Reed at 2 deg C Me't anol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-24(42) Lab ID: M79098-6 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/24/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/1 ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/1 ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/l ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/1 ND' 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 85 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C9 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 EMB 34 of 53 A M79099 MADEP VPH FORM tUlatnx r �.. A ueous n Soil ❑ Sediment ❑ Other ❑ Contkalners SatisfactorvFvl Broken 7 Leaking deou ,PcesWativ"es: N/A El PH <=2 ✓ PH>2 T'em e%atureI Received on Ice Received at 4 Deg.C ❑ Other ✓ Rec'd at 2 deg C (Aethanol ❑ N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-26(72) Lab ID: M79098-7 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/24/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/1 ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/l ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 20.7 1 Benzene 71-43-2 C5-C8 ug/1 ND 2 Naphthalene 91-20-3 N/A ug/1 ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/l ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/1 ND a 50 C9-C12 Aliphatics N/A ug/1 ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 85 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 Ma 35 of 53 A MADEP VPH FORM Matnx Aqueous n Soil Sediment F Other F Containers Satisfactory n Broken Leaking `" ueous Pr�ese yr atives N/A PH <=2 PH>2 ❑ Tam e�wature Received on Ice Received at 4 Deg. C Other d Rec'd at 2 deg C IVletYha ol._. ,... :. N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-25(72) Lab ID: M79098-8 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/24/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 2.4 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 85 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. G5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-010 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WDYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 GM21 36 of 53 A M79098 MADEP VPH FORM Matnz A ueous n Soil ❑I Sediment F Other Containers ' Satisfactor i✓I Broken ❑ Leakin ueous Preservatives N/A El PH<=2 ✓ DH>2 Tem erature Received on Ice Received at 4 Deg. C Other ✓ Rec'd at 2 deg C M., ha.n0i - N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-39(88) Lab ID: M79098-9 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/24/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/1 ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/l ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I. ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 84 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9.C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 EMEJ 37 of 53 A MADEP VPH FORM Matr A ueous Soil ❑ Sediment ❑ Other ontiainers G3� Satisfactory Fy-1 Broken F Leaking A ueousgl?r& se er,,vatives N/A DH<=2 W DH>2 Teem efat fe, Received on Ice Received at 4 Deg. C F Other Rec'd at 2 deg C M' at ha of N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-40(85) Lab ID: M79098-10 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/24/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Benzene 71-43-2 C5-C8 ug/1 ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 78 70-130% PID:2,5-Dibromotoluene % 84 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED b the VPH Method followed? Yes ❑ No-Details Attatched P Y Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? IVO]No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 Mffl 38 of 53 OACCLff EST. M79098 u MADEP VPH FORM Matn Aoueous Soil C Sediment F Other ❑ Go.ntainers Satisfactor n Broken ❑ Leaking ❑ ueoi"s Pres"ervatRV` s N/A DH <=2 H>2 ✓ Tem erature _ ° _�' Received on Ice ❑ Received at 4 De .C Other Rec'd at 2 deg c mithan:ol Ell _- N/A P. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-38(89) Lab ID: M79098-11 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/24/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/l ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/1 ND 2 i Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 1 Benzene 71-43-2 C5-C8 ug/1 ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/l ND 2 m,p-Xylene C9-C12 ug/l ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/l ND' 50 C9-C12 Aliphatics N/A Ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 85 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? IV]Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 ME] 39 of 53 I M79098Pe l MADEP VPH FORM Matrix n, Aqueous n Soil ❑ Sediment Other ontalners ....�.r ' Satisfacto ✓ Broken ❑ Leakin A ueous:Preservatives' N/A H<=2 ✓ H>2 Tem erature�, Received on Ice Received at 4 De . C f 1 Other ✓ Rec'd at 2 deg C Met'harol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-38(104) Lab ID: M79098-12 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/24/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Ranqe Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND° 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 84 70-130% FID:2,5-Dibromotoluene % 79 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9=C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 40 of 53 M79098 '_ kb rat: r i F' MADEP VPH FORM Matrix , ., '&ciueous W1 Soil F 1 Sediment ❑ Other Containers ': Satisfactory n Broken ❑ Leaking ❑ .n A ueous Pteservafiues N/A H<=2 n H>2 Tam erature r , Received on Ice ❑ Received at 4 De- . C Other n Reo'd at 2 deg c Methanol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-35(53) Lab ID: M79098-13 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/1 ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/l ND' 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 78 70-130% FID:2,5-Dibromotoluene % 71 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W1Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? Ev No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 MEJ 41 of 53 A M79098 J MADEP VPH FORM Matrix; ` .: A ueous n Soil ❑ Sediment ❑ Other ❑ Containers Satisfactor n Broken ❑ Leaking ueous Preservative N/A ❑ H<=2 n H >2 T,�m, ;erature '.: Received on Ice Received at 4 De .C ❑ Other Redd at 2 deg c Methanol N/AP. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-34(53) Lab ID: M79098-14 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Teri Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 u9/1 ND 2 o-Xylene 95-47-6 C9-Cl 2 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 m,p-Xylene C9-Cl 2 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND' 50 C5-C8 Aliphatics N/A ugh ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 77 70-130% FID:2,5-Dibromotoluene % 71 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value J Were all QA/QC procedures REQUIRED by the VPH Method followed?. IV]Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? UYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 ?.i 42 of 53 1JACCUTIEBT. MADEP VPH FORM Matrix � :.uF, Aqueous n Soil n Sediment F1 Other Co.ar'n"ecs A Satisfactor W Broken I1 Leaking ueou"s P;;resati-e N/A El D H<=2 n PH>2 n hem ,fir turd Received on Ice F1 Received at 4 De C F Other s c Rec'd at 2 de I+1lethanol x xy; N/A P Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(53) Lab ID: M79098-15 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/25/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/1 ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/1 ND' 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibrcmotoluene % 84 70-130% FID:2,5-Dibromotoluene % 77 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indi--ates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes L1 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 43 of 53 ST M79098 MADEP VPH FORM Matrix ,,- ,.. .' A ueous Soil Sediment Other Containers. ' Satisfactor IF Broken ❑ Leakin ueous Preservatives N/A F pH<=2 f H>2 Tem,a ature Received on Ice El Received at 4 Deg. C Other n Rec'd at 2 deg C Methanol _ Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-20(55) Lab ID: M79098-16 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND' 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 84 70-130% FID:2,5-Dibromotoluene % 78 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Ir Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W]Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 0 No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 44 of 53 M79098 - MADEP VPH FORM Matrix = Aclueous ✓ Soil 7 Sediment F Other Coame rs.' . Satis n-t factory✓ Broken F Leaking ❑ Ad'ueaus Preservatives, N/A H<=2 ✓ PH>2 Tem ;eature x uu Received on Ice ❑ Received at 4 Deg.C F Other ✓ Rec'd at 2 deg C Methanol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-21 (55) Lab ID: M79098-17 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dioromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tent Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND' 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 83 70-130% FID:2,5-Dibromotoluene % 77 70-130% Footnotes A Hydrocarbon Range date exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 45 of 53 A M79098 MADEP VPH FORM Matrix A ueous ✓ Soil Sediment F1 Other Ca,ntain""ers ,r 't'A Satisfactory✓ Broken F Leaking Ad"ou"sPreservatry s,, N/A H <=2 ✓ H>2 Received on Ice Received at 4 Deg. C Other ✓ Rec'd at 2 deg C Mletha ofJ N/A c• Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(90) Lab ID: M79098-18 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 11/26/2008 Date Received: 12/2/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 12/5/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/1 ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/1 ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tent Butyl Ether 1634-04-4 C5-C8 ug/I ND 1 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/l ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 79 70-130% FID:2,5-Dibromotoluene % 72 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)end/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)end/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED b the VPH Method followed? ❑✓Yes El NO-Details Attatched P Y Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 12/9/2008 MEJ 46 of 53 M79098 -' Accutest Laboratories Internal Sample Tracking Chronicle A Shell Oil Job No: M79098 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sampu_e Number Method Analyzed By Prepped By Test Codes M79098 1 Collecad 25I ® 08 l035 By W Reece ed�02�DEC 0$' Bygp e M79098-1 MADEP VPH REV 1.105-DEC-08 01:26 AF VMAVPH M790�8 2 Collected�25 N®V�08`�10�"OOBy;AWE Received 02 DEC 08 By "`" F � I M79098-2 MADEP VPH REV 1.105-DEC-08 02:07 AF VMAVPH M79038 3 _oUected 25 NOU 08 O'9'20 B SAW Received 02'DEC 08�B� Y "r Y 10. ��e ` M790)8-3 MADEP VPH REV 1.105-DEC-08 02:48 AF VMAVPH M790 8 4 Collected 25 NOV 08 08::45 By AW �: Received 02aDEC-QS By MW M79098-4 MADEP VPH REV 1.105-DEC-08 03:28 AF VMAVPH M79098 5 Collecte&24�NOU 08 1"0:15 By,`,AW Recei-ved"02=DEC=08 By: M79098-5 MADEP VPH REV 1.105-DEC-08 04:09 AF VMAVPH M79098 6Collectedr24 NOV 08 1'1':45 "By: AW Received 02.DEC 08 By � z MW-24 (42) M79098-6 MADEP VPH REV 1.105-DEC-08 04:49 AF VMAVPH M79098 7 Collec'ted24 NOV 08 12:45 By AW x Received 02-DEC 08 Bye C. M79098-7 MADEP VPH REV 1.105-DEC-08 05:30 AF VMAVPH 'M79098 8 Collected 24-' 08,13,30 l y:'',AW.""'Rem eyed ,02=DEC-0$ By: M79C98-8 MADEP VPH REV 1.105-DEC-08 06:11 AF VMAVPH Page 1 of 3 Q 47 of 53 12ACCUTEST. M79096 -aro'x:cri ; Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M79098 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes IuI 97 098 M79098-9 MADEP VPH REV 1.105-DEC-08 06:52 AF VMAVPH !7�M7�909$ IOCo'ltlected 2`�4AN008 130 By�AUV ��, R�ece�ved02�DEC 08 By� � �� � ' 4 (85) z M79098-10 MADEP VPH REV 1.105-DEC-08 07:32 AF VMAVPH M79098 11 Collected ;24 N0 $ 15 OQ By AW Recceive�d 02 DECO By � M 38 (89) y —EE ..� ,. �.:_ ✓,..; ,..,,H��$,L...� .,fs.. ....u...:...,�,.:.w,a..:mv....,_Gd M79098-11 MADEP VPH REV 1.105-DEC-08 08:13 AF VMAVPH M7�09$ 12 Collected 24'NQ 08 15`,20 By'�AW R ei ed 02 DEC�08 B77 Y ,. _. „ ' ,." •, ..,.., ✓M ,..`` ;' ......`Y.w"?�_z „'ivr�.Yr :.' .,,,x.. _.... _ ..,.0 .., '✓ 'k, .'tea. ."?.h ... ..... ........ :d M79098-12 MADEP VPH REV 1.105-DEC-08 08:54 AF VMAVPH 79,098 13 Collected 25 NO 0$ 09 00 By;,AW Rece�ued 02-DEG 0$ B,y I MWWv M79098-13 MADEP VPH REV 1.105-DEC-08 09:36 AF VMAVPH M79098 14iCollected 25 NOU 08 09.45 By AWE �Rece�ved 02 DEC 0$�W;07 �Y F ..�..,t...o.-�`;4 i , .. .....-.�:- .-,x.f2.�.. <.��a war.era w,_en�. ,...•��..r.�.F> zWk.. AL" :._..,__�' M79098-14 MADEP VPH REV 1.105-DEC-08 10:17 AF VMAVPH M790915 Collected 25 NOU 08 10:45ByAW Re eac ved02 DEC Off By �� '� M79098-15 MADEP VPH REV 1.105-DEC-08 10:58 AF VMAVPH M79098 z1�Collected 2fOV 0ft ByAW F Iece1V 2 DES 08 �By. .sued M W 20 (SSa) ., sue... M79098-16 MADEP VPH REV 1.105-DEC-08 11:39 AF VMAVPH Page 2 of 3 MEJ 48 of 53 Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M79098 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M7909�$�17G� e�d 26 1�1Q�V U8�0 35 $y °AW� �,� Receaved 02 DEC 0$ By ����_' . &�� M79098-17 MADEP VPH REV 1.105-DEC-08 12:20 AF VMAVPH M�79, 98 "Co Collected26OV 08 1o;35By�AWeed 02 �C fl By ��� M W 07 90 M79098-18 MADEP VPH REV 1.105-DEC-08 13:01 AF VMAVPH I Page 3 of 3 49 of 53 T M79098 = New England b r.<I o r ® Section 5 P GC Volatles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Surrogate Recovery Summaries a7� 50 Of 53 OACCUTEST. j Method Blank Summary Page 1 of I Job Number: M79098 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1127-MB B1323705.13 1 12/04/08 AF n/a n/a GBD1127 tie The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79098-1, M79098-2, M79098-3, M79098-4, M79098-5, M79098-6, M79098-7, M79098-8, M79098-9, M79098-10, M79098-11, M79098-12, M79098-13, M79098-14, M79098-15, M79098-16, M79098-17, M79098-18 CAS No. Compound Result RL Units Q ........._..._._................... . 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-C4-4 Methyl Tert Butyl Ether ND 1.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/l 108-8€-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9-C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 78%0 70-130% 615-59-8 2,5-Dibromotoluene 83% 70-130% I u° 51 of 53 A M79098 Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M79098 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD1127-BSP BD23706.D 1 12/04/08 AF n/a n/a GBD1127 GBD1127-BSD BD23707.D 1 12/04/08 AF n/a n/a GBD1127 ev The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M79098-1, M79098-2, M79098-3, M79098-4, M79098-5, M79098-6, M79098-7, M79098-8, M79098-9, M79098-10, M79098-11, M79098-12, M79098-13, M79098-14, M79098-15, M79098-16, M79098-17, M79098-18 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD 71-43-2 Benzene 50 51.5 103 51.3 103 0 70-130/25 100-41-4 Ethylbenzene 50 52.1 '104 51.8 T04 1 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 47.8 96 48.2 .96 1 70-130/25 91-20-3 Naphthalene 50 44.4 .89 45.6 91 3 70-130/25 108-88-3 Toluene 50 52.1 104 51.9 .104 0 70 130/25 m,p-Xylene 100 104 104 104 104 10. 70-130/25 95-47-6 o-Xylene 50 48.4 97 48.3 97 0 70-130/25 C5- C8 Aliphatics (Unadj.) 150 136 91 137 91 1 70-130/25 C9- C12 Aliphatics (Unadj.) 150 139 93 140 93 1 70-130/25 C9- C10 Aromatics (Unadj.) 50 48 95 48 .96 1 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 81% 81% 70-130% 615-59-8 2,5-Dibromotoluene 86% 87% 70-130% I gal 52 of 53 R Volatile Surrogate Recovery Summary Page I of 1 Job Number: M79098 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method w Lab Lab Sample ID File ID Sl a Sl b M79098-1 BD23711.D 77.0 83.0 .... ........... .......... ........ ......... ............... ..... M79098-2 131323712.D 78.0 82.0 M79098-3 BD23713.D 80.0., 82.0 M79098-4 BD23714.D 810 84.0 M79098-5 BD23715.D 79 0 85.0 M79098-6 BD23716.D 80.0 85.0 M79098-7 131323717.D 80.0 .. 85.0 M79098-8 BD23718.D 810 85.0 M79098-9 BD23719.D 79.0 84.0 M79098-10 BD23720.D 78.0 84.0 M79098-11 BD23721.D 79.0 85.0 M79098-12 131323722.D 79.0 84.0 M79098-13 BD23723.D 7.1.0 78.0 ......._.. .. .... M79098-14 BD23724.D 71.0 77.0 M79098-15 131323725.D 77.0 84.0 M79098-16 BD23726.D 78.0 84.0 M79098-17 BD23727.D 77.0 83.0 M79098-18 BD23728.D 72.0 79.0 GBDI127-BSD BD23707.D 8`1.0 87.0 GBD1127-BSP BD23706.D 81.0 86.0 GBD1127-MB BD23705.D 78.0 83.0 Surrogate Recovery Compounds Limits S1 = 2,5-Dibromotoluene 70-130% (a) Recovery from GC signal #1 (b) Recovery from GC signal #2 53 of 53 A M79096 SOVEREIGNig • r September 25,2008 DHL #29116656656 Ms. Donna Z. Miorandi " Town of Barnstable ti w t Public Health Division _. 200 Main Street - , Hyannis,MA 02601 su_ v. }; Re: Groundwater Sampling Results,August 2008 $ In the Vicinity of: Former Texaco Service Station k b 1140 Iyannough Road` Ot RTN 4-11301 Dear Ms. Miorandi =r ¢_ Pursuant to your authorizatidri Sovereign Consulting',`Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced,property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH). A copy of the laboratory analytical is attached. As always, we thank you for your contixiued consideration and-cooperation in our remediation efforts. If you have any questions regarding this,,submittal,,please feel free to contact the undersigned at 508-339-3200. Sin/re SOCONSULTING INC N sN Jasurne .:Prager" -0 ; oc cc: Mr. David Weeks,Motiva MassDEP-SERO ., t Sovereign File-EQ711 ie, tl t g F I 4 f 1 — A� .ter., i .. I 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 f ICI c NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan r' BWSC 123 This Notice is Related to Release Tracking Number 4� 11301 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Donna Miorandi 2. Street Address. 200 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ✓❑2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ✓❑3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code. 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase 1V Remedy Implementation Plan ❑Utility-related Abatement Measure ✓❑ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: El residential ✓❑commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater) to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne Street Address: 90513 South Main St., Suite 202 City own: Mansfield Zip Code: 02048 Telephone: (508) 339-3200 Email: Sherburne@sovcon.com Y yY NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. i e- ardeopy 2.D Automated Report C 6 New England12 } � f A tJTEST - L a b o r a I a r e s " N, :r y ........................................-........._....... 09/02/08.. Technical Report for Shell Oil SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA EQ 711 O , Accutest Job Number: M76363 0 Sampling Date: 08/18/08 Report to: Sovereign Consulting Inc. jsherburne@sovcon.com ATTN: Jason Sherburne Total number of pages in report: 55 \N ACCpR ��O f .mot 4• m• V f .::1 Test results contained within this data package meet the requirements Xe a and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) Y E A R 5 NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England 495 Tech Center West Building 1 Marlborough,MA 01752 tel:508-481-6200 fax:508-481-7753 http://www.accutest.com 1 of 55 JUACCUTEST M76363 '_......:._ Sections: Table ®f Contents -1- Section1: Sample Summary ................................................................................................... 3 Section 2: Case Narrative/Conformance Summary .... 5 Section3: Sample Results ....................................... ,.......,,,..............................,,.............,...... 6 3.1: M76363-1: MW-21 (5 5) ............................................................................................... 7 3.2: M76363-2: MW-24 (42) ............................................................................................... 8 3.3: M76363-3: MW-26 (72) ............................................................................................... 9 3.4: M76363-4: MW-19 (55) ............................................................................................... 10 3.5: .M76363-5: MW-20 (55) ............................................................................................... 11 3.6: M76363-6: MW-29 (68) 3.7: M76363-7: MW-32 (55) ............................................................................................... 13 3.8: M76363-8: MW-35 (53) ............................................................................................... 14 3.9: M76363-9: MW-37 (53) ............................................................................................... 15 3.10: M76363-10: MW-37 (90) ........................................................................................... 16 3.11; M76363-11: MW-37 (105) ......................................................................................... 17 3.12: M76363-12: MW-39 (88) ........................................................................................... 18 3.13: M76363-13: MW-40 (85) ........................................................................................... 19 3.14: M76363-14: MW-38 (104) ......................................................................................... 20 3.15: M76363-15: MW-38 (89) ........................................................................................... 21 3.16: M76363-16: RW-101 .................................................................................................. 22 3.1.7: M76363-17: RW-102 .................................................................................................. 23 3.1 : M76363-18: MW-25 (72) ........................................................................................... 24 Section4: Misc. Forms ............................................................................................................ 25 4.1: Chain of Custody ........................................................................................................... 26 4.2: MCP Form ..................................................................................................................... 28 4.3: VPH Form ...................................................................................................................... 29 4.4: Sample Tracking Chronicle ........................................................................................... 47 Section 5: f.:lf` Volatiles - QC Data :Summaries .....................................................--............ 50 5.1: Method Blank Summary ................................................................................................ 51 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 53 5.3: Surrogate Recovery Summaries ..................................................................................... 55 ® 2 of 55 13ACPVTEST M76363 '.... .......... .: Accutest Laboratories Sample Summary Shell Oil Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Project No: EQ 711 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M76363-1 08/18/08 10:30 AW 08/20/08 AQ Ground Water MW-21;(55) M76363-2 08/18/08 10:55 AW 08/20/08 AQ Ground Water MW-24 (42) M76363-3 08/18/08 10:10 AW 08/20/08 A Ground Water MW-26 72 Q ( ) M76363-4 08/18/08 09:30 AW 08/20/08 AQ Ground Water MW-19 (55) M76363-5 08/18/08 13:35 AW 08/20/08 AQ Ground Water MW-20 (55) M76363-6 08/18/08 14-00 AW 08/20/08 AQ Ground Water MW-29 (68) M76363-7 08/18/08 13:15 AW 08/20/08 AQ Ground Water MW-32 (55) M76363-8 08/18/08 12:45 AW 08/20/08 AQ Ground Water MW-35 (53) M76363-9 08/18/08 11:00 AW 08/20/08 AQ Ground Water MW-37 (53) M76363-10 08/18/08 11:50 AW 08/20/08 AQ Ground Water MW-37 (90) M76363-11 08/18/08 12:15 AW 08/20/08 AQ Ground Water MW-37 (105) M76363-12 08/18/08 12:20 AW 08/20/08 AQ Ground Water MW-39 (88) M76363-13 08/18/08 11:55 AW 08/20/08 AQ Ground Water MW-40 (85) u1�® 3 of 55 ®A M76363 ..:.. ... .:. Accutest Laboratories Sample Summary (continued) Shell Oil Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M76363-14 08/18/08 12:55 AW 08/20/08 AQ Ground Water MW-38 (104) M76363-15 08/18/08 13:30 AW 08/20/08 AQ Ground Water MW-38 (89) M76363-16 08/18/08 09:40 AW 08/20/08 AQ Ground Water RW-101 M76363-17 08/18/08 11:20 AW 08/20/08 AQ Ground Water RW-102 M76363-18 08/18/08 10:30 AW 08/20/08 AQ Ground Water MW-25 (72) ® 4 of 55 ®ACC-TEBT M76363 a L. a- bora. torics SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M76363 Site: SCMAW:97346878(REIMBMA)1140Iyannough Road Hyannis MA Report Date 9/l/2008 1:46:16 PM 18 Sample(s)were collected on 08/18/2008 and were received at Accutest on 08/20/2008 properly preserved,at 2 Deg.C and intact. These Samples received an Accutest job number of M76363.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control perfonnance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GBD990 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GBD991 All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M76363). Monday;September 01.2008 Page l of l ® 5 of 55 13ACCUTE�ST M76363 New England ACC�lTEST _ _. � L a b o r i t o r I e Section E Y_._.. _....._......._.. n.. :. ... 1 L iD THE rtE MI5 T'S2 +' .. Sample Results Report of Analysis ® 6 of 55 ®ACC L EST M76363 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-21 (55) Lab Sample ID: M76363-1 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20859.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND, 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene 86% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q® 7 of 55 13ACPWTWT M76363 = - Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-24 (42) Lab Sample ID: M76363-2 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD2086O.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Puree Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- CIO Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Rung I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-5'9-8 2,5-Dibromotoluene 87% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound a�® 8 of 55 ACGUTEST M76363 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-26 (72) Lab Sample ID: M76363-3 Date Sampled: 08/18/08 > Matrix.: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20861.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 72% 70-130% 615-59-8 2,5-Dibromotoluene 80% 70-130% ND = Not detected J = Indicates an estimated value RL Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound a-1 9 Of 55 ®A M76363 t Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-19 (55) Lab Sample 1D: M76363-4 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20862.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-.2 Benzene ND 2.0 ug/1 100-41.-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 8.1 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 87% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME] 10 of 55 13ACPVTWT M76363 i. --r--1- - Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-20 (55) Lab Sample ID: M76363-5 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method.: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20863.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 78% 70-130% 615-59-8 2,5-Dibromotoluene 86% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound �a® 11 of 55 ®ACCUTEST Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-29 (68) Lab Sample 1D: M76363-6 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20864.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2: MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 90.5 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) 69.0 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND' 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 89% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 1 12 of 55 AC:Gl.ii'EST. M76363 - - - Accutest Laboratories Report of Analysis Page I of 1 Client Sample 1D: MW-32 (55) Lab Sample ID: M76363-7 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20865.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 88% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q® 13 of 55 ®ACCUT'EST ................................................... M76363 Accutest Laboratories Report of Analysis Page 1 of 1 00 Client Sample ID: MW-35 (53) Lab Sample ID: M76363-8 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Methcd: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20866.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#3 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-4'-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 13.3 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 82% 70-130% 615-59-8 2,5-Dibromotoluene 89% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound EY1 B 14 of 55 12AC P TEST ._............................................ M76363 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-37 (53) Lab Sample 1D: M76363-9 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20867.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#'2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1,634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 1,08-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 88% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q® 15 of 55 ®AT .._..... ...... .........__..... ......... ...... M76363 - -- Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-37 (90) Lab Sample ID: M76363-10 Date Sampled: 08/18/08 Matrix. AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20868.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2' MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 87% 70-130% 615-59-8 2,5-Dibromotoluene 94% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q 16 of 55 12ACCLPT EST Accutest Laboratories sa Report of Analysis Page 1 of 1 Client Sample ID: MW-37 (105) Lab Sample 1D: M76363-11 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1. BD20869.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-ViPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics NO 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1, Run# 2 Limits 615-59-8 2,5-Dibromotoluene 83%` 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ® 17 of 55 ®ACCUTEST M76363 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-39 (88) Lab Sample ID: M76363-12 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20870.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634=04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 82% 70-130% 615-59-8 2,5-Dibromotoluene 91% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound nY ® 18 of 55 ®A ........... M76363 i..a Accutest Laboratories Report of Analysis Page 1 of 1 , Client Sample ID: MW-40 (85) Lab Sample ID: M76363-13 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#A BD20871.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9- CIO Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# I Run## 2 Limits 615-59-8 2,5-Dibromotoluene 83% 70-130% 615-59-8 2,5-Dibromotoluene 93% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Ma 19 of 55 ACPVTFPT M76363 = r Accutest Laboratories Ga Report of Analysis Page 1 of 1 Client Sample 1D: MW-38 (104) Lab Sample ID: M76363-14 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20880.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND: 3.0 ug/1 108-83-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 90% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MIN 20 of 55 ®ACC JT.EST M76363 l Accutest Laboratories to Report of Analysis Page 1 of 1 , Client Sample ID: MW-38 (89) Lab Sample ID: M76363-15 Date Sampled: 08/18/08 . Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20881.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume i Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 90% 70-130% ND = Not detected j = Indicates an estimated value f RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound k ® 21 of 55 ®ACCUTEST. M76363 r Accutest Laboratories P Report of Analysis Page 1 of 1 0, Client Sample ID: RW-101 Lab Sample ID: M76363-16 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20882.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS ND. Compound Result RL Units Q 71-43-2 Benzene ND, 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 22.0 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) 1810 50 ug/1 • C9- C10 Aromatics (Unadj.) 506 50 ug/I C5- C8 Aliphatics ND 50 ug/I 'C9- C12 Aliphatics 1310 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 87% 70-130% 615-59-8 2,5-Dibromotoluene 96% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ff l 22 of 55 13A -- M76363 -a_.:.. ....Is i Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: RW-102 Lab Sample ID: M76363-17 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20883.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) 67.4 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 82% 70-130% 615-59-8 2,5-Dibromotoluene 9.1% _ 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound EM® 23 of 55 ®ACCIJTEST M76363 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-25 (72) Lab Sample ID: M76363-18 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20884.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND " 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 14.3 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 8 % 70-130% 615-59-8 2,5-Dibromotoluene 92% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound R 24 of 55 13ACCUTEST. M76363 New England ACCU'I'�ST L a b o r a t o r e SSection 4 Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle Q® 25 of 55 ®ACCL ff.UST< M76363 LAB(LOCATION) 4 Shell Oil Products Chain Of Custody Record 'Please:Cbeck.Appiopilate Box; Pflht:BiH fb:CbfiWCt Nafie. INC.DE T.&:(ERV:SERVICES):::El D(�IF NO IN DENr APPLIES ❑ENV SEAVICFS ..❑IMRIVA RETAIL ff--�� ... �'�... ..y SHELL REIN[ /\ O l pAaurEsr Dave Weeks 9 6 9 2 5 0 2 8 DATE: ❑NOINA SLt9CN p wNwlTAirr ❑LUI1r5 �:P6 it : -SAP. r� ❑O ❑OTHE0. PAGE: r 01 of THER( 1 ❑SHELL PIPFLLtIF 1 0 0 0 8 3 uL u,r ww.ur, AVCR68s Ian..,.CM N BIN.I� Sovereign Consulting Inc B 1140 I annou h Road Hyannis,MA 905B South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Report to).Jasoo Sherburne CONSULTANT PROJECT NO.:EQ711 p Pn~ _ Mansfield,MA 02048 "^ ..... euse s� aeLr/ B 508.339.3200 508.339.3248ALENDAR isherbume(o�sovcon.com r—eR2ir.JIDP TURNAROUNDTwe(CDAYSI: STANDARD(14 DAYI ❑S DAYS ❑3 DAYS ❑2 DAYS ❑24 HOURS REQUESTED ANALYSIS ELNEWLES: ❑COMMA ❑cop ma 17 NEP ❑REP QOTHER(SPEcIm �.. TEMPERATUREONRECEIPTC OBoler Bt ICmler p] :Cooin BO SPECIAL INSTRUCTIONS OR NOTES: _ SAMPLING Field Sample Identification uArwx ygE;_� DATE TIA� d CORt.1n PID R-"119s ::Wit: Or LOEoratory Notes C u 2 lur- J1L1 15 ss 3D l IV" 3Z �r �3rs GJ '3.72`S'3 aVs S -3 ` l U" ros is Z go M76363: Chain of Custody Page 1 of 2 26 of 55 A __-----_..................._.. M76363 .:.. .........1 LAS(LOCATION) 4 Shelf Oil Products Chain Of Custody Record Please chock Appttiprlate8ox Print Bin To:C10160 Name iN�I�EN7. (ENV:6ERV[CE3:.:❑CHECKYNOU, EM a APPLIES ❑E seavl�s Omar+ARETAn ❑sNEUREAa�+ACOl,EST Dave Weeks 91 61 91 21 5 012 18 DATE it`t❑morrvA soeo, p cawLTurr ❑LueEs P.O P SAP A �j ❑oTHEa l ) ❑SHELL PIPRINE ❑on,Ea PAGE: or V t o 0 0 873 Ky Sovereign Consulting Inc ,N1140 l annou h Road,Hyannis,MA 905E South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Repon to):Jason Sherbume CONSULTANT PROJECT NO.:EQ711 p _ Mansfield,MA 02048 —" H 568.339.3200 u 508.339.3248 jsherburne(a),sovcon.com rURHARoumO Tu.IE(GLENDAR DAvst � Q STANDARD tw NT) ❑s DAYS ❑IOATS ❑—S I]1e HOURS REQUESTED ANALYSIS DE-E..ES: ❑cmm ❑comma O� ❑RCP ❑OTHER(SPELIfV) TEWER—UREONRECEIPTC• Cealesl :Coolern tCWld aJ SPECIAL INSTRUCTIONS OR NOTES: SAMPLING Field Sample Identification aurRM °E 2 ConMlner PIDReadil +kf:, DATE TIME a q Laborttory Hales :�PRr: NNW.wd nbE WMFA C /nU �F° h S h 111 Ss MLI 38 5 f33° W 1 oT 014- Imu as IDY1 Ass .aI al 25-0 u.ep 1 •>.1 . y.,.wp�mrH Rs,R:.wh lse.w.l Xnce.m W l,yisv.l �'I76363: Chain of Custody Page 2 of 2 ® 27 of 55 ®ACP4TWT M76363 Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 a N Title: MADEP MCP Response Action Analytical Report Certification Form FW Qt*P M � ca method Re 4 Ificatto �� \\ Laboratory Name: Accutest Laboratories of New England Project#: M76363 Project Location: SCMAW:97346878(REIMBMA)1140 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M76363-1,M76363-1 0,M76363-1 1,M76363-12,M76363-13,M76363-14,M76363-15,M76363-16 M76363-17,M76363-18,M 76363-2,M 76363-3,M76363-4,M 76363-5,M 76363-6,M76363-7 M76363-8,M76363-9 Sample Matrices: Groundwater X Soil/Sediment () Drinking Water () Other: () () MGP�SW 84e- 8260B 8151A � 8330 601013 7470A/1A MethodsUs ii 8270C O 8081A O VPH(X) 6020 O 9014M z () sspeGfie n MRO(' 8082 O 8021 B O EPH O 7000 S 3 O 7196A O Gompend un of 6°1 Ltst Release Tr cking.Nur tber(RTN) if kr©wn a AralyticalEyethods � 2 M SW 846 Method:9014 or M/aDP Phys� og,cI Avai(atrle C amde PAC tethodNowY Meth div,dual me h d a"ri" an lyte ;• An affirmative response to questions A, B, C, and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with Yes ❑ No that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and 121 Yes ❑ No discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty", as described in Section 2.0(a), (b),(c)and El Yes ❑No (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only: Was the VPH or EPH method run without RI Yes ❑No significant modifications,as specified in Section 11.3? A response to questions E and Fbelow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the M Yes ❑ No specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified 2 Yes LI No method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief, accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 09/01/2008 - I 28 of 55 A .._:_UTEST M76363 .._.. = MADEP VPH FORM Matrix -,. ti Aqueous n Soil Sediment n Other ^I Corita,n�ers�: .' Satisfactor Broken CI Leaking l A ueous Preseruattu N/A n PH <=2 Iv PH >2 n T„erri, erat ru e .. Received on Ice n Received at 4 De . C n Other n Rec'd at 2.0 Deg.C Methan'oa Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-21 (55) Lab ID: M76363-1 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Rance data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Rance data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes L] No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? jYes 1 1 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? CINo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 9/1/2008 29 of 55 'Printed Name Reza Tand �A .. M76363 i MADEP VPH FORM MatriX Aclueous W Soil 1-1 Sediment F Other ❑ Containers SatisfactoryW Broken P Leaking A ueous Preservafiv'es` N/A ❑ pH <=2 n PH >2 Temperature Received on Ice ❑ Received at 4 Deg. C ❑ Other F.#] Ree'd at 2.0 Deg.C Methanol = N/A Client ID: MW-24 42 W Method for Ranges: MADEP VPH REV 1.1 ( ) Lab ID: M76363-2 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2;5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12.Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 87 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbcn Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbcn Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No—Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? IV]No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 9/1/2008 ®Printed Name Reza Tand ® 30 of 55 ACCI.I'TEST MADEP VPH FORM Matrix .� Aqueous we Soil 7 Sediment 01 Other I— C.o.�rta n'ers � SatisfactorvEyl Broken F1 Leaking A'-ueous:'_eseruatiue a N/A F1 PH <=2 Fv] PH >2 ❑ ernes erature Received on Ice F1 Received at 4 De- . C ❑ Other n Reed at 2.0 Deg.C l anol ;;I N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-26(72) Lab ID: M76363-3 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/1 ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/1 ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/1 ND a 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 72 70-130% PID:2,5-Dibromotoluene % 80 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? UYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete i Signature Postition Laboratory Director " Printed Name Reza Tan Date 9/1/2008 31 of 55 A M76363 I MADEP VPH FORM Matrix A ueous We Soil F Sediment R Other Containers Satisfactory n Broken F1 Leaking 17 Aqueous Preservatives;` N/A I-1 H <=2 n PH >2 Temperature .,_ Received on Ice n Received at 4 De . C n Other n Rec'd at 2.0 Deg.C Methanol = N/A Client ID: MW-19 55 ca Method for Ranges: MADEP VPH REV 1.1 ( ) Lab ID: M76363-4 Date Collected: 8/18/2008 Date Received: 8/20/2008 Method for Target Analytes: MADEP VPH REV 1.1 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 8.1 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130 PID:2,5-Dibromotoluene % 87 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conic of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? EvYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? C1Yes i_l No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? Ile]No I Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete I Signature Postition Laboratory Director Date 9/1/2008 o n Printed Name Reza Tan �® 32 of 55 AC:r LJ7F_ST M76363 " -..... — MADEP VPH FORM IVlatrlx �,,". Aqueous n Soil Sediment F1 Other ntalrte°rs ,..;., Satisfactory f� Co Broken Leakin 1-1 A ueou's Preservatives N/A L pH <=2 n PH >2 F-I Tem eratu.re Received on Ice Received at 4 De . C 1-1 Other n Rec'd at 2.0 Deg.C Methanol N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-20(55) Lab ID: M76363-5 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analvtes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND e 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 78 70-130% PID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analyles eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analyles eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? LJYes I J No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? kYes U No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? EvelNo U Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 9/1/2008 °r Printed Name Reza Tand �® 33 of 55 MACCUUTEES.T. M76363 MADEP VPH FORM Matrix A ueous ✓ Soil F1 Sediment I-1 Other 1f Containers - Satisfactory✓ Broken F1 Leakin A ueous Preservatives; N/A pH <=2 n PH >2 T n e�ature. ' Received on Ice 1 Received at 4 Deg. C Other [�I Rec'd at 2.0 Deg.C Meth'ano;l N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-29(68) Lab ID: M76363-6 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Ranqe Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 694 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 90.5 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Ali,phatics N/A ug/I ND" 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 89 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ❑✓Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 9/1/2008 Men 34 of 55 Printed Name Reza Tand MACCUTE. M76363 ---., ;.,n MADEP VPH FORM Matrix.`, Aciueous n Soil F1 Sediment ❑ Other Co-ntai.ners Sat isfactor n Broken F1 Leaking A6 uedtas`_Pres;ervatives. N/A ❑ PH <=2 141 PH >2 Tm erature " Received on Ice ❑ Received at 4 Deg. C ❑ Other Rec'd at 2.0 Deg.C Methanol, , ' N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-32(55) Lab ID: M76363-7 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ugh ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130 PID:2,5-Dibromotoluene % 88 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-Cl0 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 9/1/2008 i Printed Name Reza Tand �® 35 of 55 ®AIMUTEST M76363 I MADEP VPH FORM Aqueous Wl Soil F-1 Sediment n Other Co,nt''ain.ersh Satisfactor ✓ Broken 17 Leaking n A" 4W' Prese Vki. . N/A �! �H <=2 � H >2 El T m erature4, ,, Received on Ice Received at 4 Deg. C Other n Rec'd at 2.0 Deg.C Methhanoa N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-35(53) Lab ID: M76363-8 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 811812008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 13.3 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND e 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 89 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range_ C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'X qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? DYes _ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? i�1Yes ✓_ ! No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 141No ! Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tan Date 9/1/2008 r� 36 of 55 M76363 1 -- - r MADEP VPH FORM Aqueous ✓ Soil F1 Sediment n Other o.ntai.ners. Satisfactor Broken n Leakin n u.eous�Preseri- ''hiss N/A pH <=2 PH >2 n Tem >eratuf" Received on Ice n Received at 4 Deg. C Other F I Rec'd at 2.0 Deg.C Methanol N/A ? Client ID: MW-37 53 Lab ID: M76363-9 to Method for Ranges: MADEP VPH REV 1.1 ( ) Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analvtes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND e 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A U qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? LlYes El No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? GYes 1-11 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? kNo C1 Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete `Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 Mn 37 of 55 AEST M76363 ........ ........ f MADEP VPH FORM Matr(x Ag ueous W Soil n Sediment F1 Other Containers Satisfactory F%*1 Broken n Leaking Aciueoius.Preservatiu.:es N/A F pH <=2 n PH >2 n Temperature Received on Ice n Received at 4 De . C n Other I✓I Rec'd at 2.0 Deg.C Methano'I N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(90) Lab ID: M76363-10 cA Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Sta;idards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/1 ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/1 ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Bu:yl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 87 70-130% PID:2,5-Dibromotoluene % 94 70-130 Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Tzrget Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Anayles eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? IV:]YeS 0 No-Details Attatched Were all performance/acceptance standards foc required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 0No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete I Signature Postition Laboratory Director Date 9/1/2008 ®Printed Name Reza Tand ® 38 of 55 ®ACCUTEST M76363 MADEP VPH FORM Matrix: A ueous ✓ Soil F1 Sediment ❑ Other Con.tain.ers Satisfactor ✓ Broken ❑ Leaking I A;ueous Preservatives,' N/A pH <=2 n PH >2 ❑ Tern erature Received on Ice I-1 Received at 4 Deg. C ❑ Other n Reed at 2.0 Deg.C Methanol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(105) Lab ID: M76363-11 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 83 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 Mob®® 39 of 55 : r CC p � ° F14.h..r1..r�W�BT M76363 _ :... ._ MADEP VPH FORM fl &r x .; Aqueous � Soil Sediment F1 Other F] Containers.. ;:" Satis factory n Broken Leaking A-ueous PreservativesW N/A H <=2 n PH >2 1� Tim erature ��, Received on Ice Received at 4 Deg. C F] Other n Redd at 2.0 Deg.C Methanol N/A 4�b Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-39(88) Lab ID: M76363-12 W Method for Target.Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/l ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/1 ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 91 70-130% FID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes D No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes F-1 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo (l Yes-Details Attatched I attest under the jains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature '��-- Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 Mn 40 of 55 ®ACClJI'E.. M76363 - MADEP VPH FORM Matrix i A ueous ICI Soil (1 Sediment Other Co. fairlers Satisfactory f*rl Broken Leaking A�%taeous Preservatives 1.!. N/A F1 pH —2 n PH >2 n Tam `erature Received on Ice (i Received at 4 Deg. C I-1 Other n Rec'd at 2.0 Deg.C M4ethanoL. N/A Method for Ranges: MADEP VPH REV1.1 Client ID: MW-40(85) Lab ID: M76363-13 Ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND c 50 C5-C8 Aliphatics N/A ug/I ND" 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibrorrotoluene % 93 70-130% FID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analoes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indica:es an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ''Yes _ j No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? IV—:Yes J No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? LNo 'J Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature ����— Postition Laboratory Director Printed Name Reza Tand � Date 9/1/2008 P,.�® 41 of 55 y ®AMUTEST M76363 _ . ......_n r I MADEP VPH FORM Matrix _ Aqueous n Soil —I Sediment Other Containers Satisfactory We Broken Leaking A' "u"eo.us Preservatives N/A PH <=2 n PH >2 Tem" erature Received on Ice F1 Received at 4 Deg, C Other hI Rec'd at 2.0 Deg.C Metli"ano N/A Client ID: MW-38 104 Lab ID: M76363-14 w Method for Ranges: MADEP VPH REV 1.1 ( ) Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ugh ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 90 70-130% FID:2,5-Dibromotoluene % 81 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons, Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes U No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ❑d No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand ® Date 9/1/2008 �a ® 42 of 55 - MADEP VPH FORM Matrix Aqueous n Soil I-1 Sediment 1-1 Other Containers Satisfactor Fvl Broken ❑ Leaking 1-1 Aqueous Preservatives' N/A F pH <=2 PH >2 F 1 Tern erature3 Received on Ice ❑ Received at 4 Deg. C ❑ Other F. Read at 2.0 Deg.c NJ'etharipl N/A .0. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-38(89) Lab ID: M76363-15 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Buiyl Ether 1634-04-4 C5-C8 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND c 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 90 70-130% FID:2,5-Dibromotoluene % 81 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Ana ytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified.in Sect. 11.3? ❑✓No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 9/1/2008 = Printed Name Reza Tand ®® 43 of 55 T ...._......_................................... M76363 MADEP VPH FORM Matrix A ueous Soil FJ Sediment n Other Corntainers Satisfactory n Broken F1 Leaking Aqueous Preservatives N/A F� pH <=2 R., PH >2 Temperature ,:` Received on Ice F I' Received at 4 De . C R Other rv] Rec'd at 2.0 Deg.c Methanol N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: RW-101 Lab ID: M76363-16 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I 1810 A 50 C9-C10 Aromatics(Unadj.) N/A ug/I 506' 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 22 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I 1310' 50 C5-C8 Aliphatics N/A ug/I ND" 50 Surrogate Recove-ies Acceptance Range PID:2,5-Dibromotoluene % 96 70-130% FID:2,5-Dibromotoluene % 87 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Ranc a data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W Yes 1 1 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes _J No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No 11 Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the info-mation,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Date 9/1/2008 M 44 of 55 Printed Name Reza Tand ®ACCLITEST ._......................................._...._. M76363 _,. .......... MADEP VPH FORM Matriz� Acl ueous n Soil Sediment F1 Other C°orifainbrs,M .« -- Satisfactor y Fel Broken n Leakinci A' ueous Pres�e:vativeso, N/A F-i H <=2 n PH >2 n Tem, eratur '' Received on Ice n Received at 4 Deg. C 7 Other W Rec'd at 2.0 Deg.C N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: RW-102 Lab ID: M76363-17 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 67.4" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 Target Analvtes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 91 70-130% FID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value - Were all QA/QC procedures REQUIRED by the VPH Method followed? F4—!Yes -_1 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes L._I No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? I�1No ❑ Yes-Details Attatched 4 1 attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 a 45 of 55 ` 13ACPVTWT M76363 p MADEP VPH FORM Matrix y Aqueous F-11 Soil Sediment Other C;ontalners Satisfactor (v Broken n Leaking ueous':Preseyatiue`s N/A �I H <=2 H >2 n Tem eature� t Received on Ice �I Received at 4 De . C Other Rec'd at 2.0 Deg.c Methnol �.,. N/A .p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-25(72) Lab ID: M76363-18 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aroma`ics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analvtes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 14.3 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Adjusted Ranges C9-C12 Aliphat cs N/A ug/I ND' 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromctoluene % 81 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 6 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Tarcet Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any su-rogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conic of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? L ]Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? 411No ❑ Yes-Details Attatched py I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director -Printed Name Reza Tand Date 9/1/2008 Mn46 of 55 ACLU EST M76363 —a....... ...._:. r s , Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M78363 1' C�olected18"AUG 08 1t3 30 B AW Received 20AUG08 By Y y M76363-1 MADEP VPH REV 1.127-AUG-08 01:19 AF VMAVPH M76363 2 Collected 18AUG 08 10 55 ByW� Received 20{AUG Oy M76363-2 MADEP VPH REV 1.127-AUG-08 02:00 AF VMAVPH M76363 3 Collected-i&8 AUG� 0810 10 By A� Received 20'AUG 08By MW M76363-3 MADEP VPH REV 1.127-AUG-08 02:42 AF VMAVPH M76363'4 C©llected 18A�UG 08 0930 By AWERecerved 20 AUG MW 18 M76363-4 MADEP VPH REV 1.127-AUG-08 03:23 AF VMAVPH M7636 3 5 Collected 18 AUG 08 13:35 ByAaW �Rece�ed20 AUG 08 Bye MW 20 (55) FF M76363-5 MADEP VPH REV 1.127-AUG-08 04:04 AF VMAVPH M76363 6 Collected 18 AUGy08 14'00 By AW Rece ved 20�A 08 By " ,• M76363-6 MADEP VPH REV 1.127-AUG-08 04:45 AF VMAVPH M76363 7 ..Collected: 18 AU,G 081�3 15�By AWE Recewed 20 AUG 08 Bye M76363-7 MADEP VPH REV 1.127-AUG-08 05:25 AF VMAVPH M76363 8 Collected 18 AUG 08 12 s45 By NW Received: 2p AUG 08 By M76363-8 MADEP VPH REV 1.127-AUG-08 06:06 AF VMAVPH Page 1 of 3 47 of 55 ACCU'TEST M76363 r . Accutest Laboratories Internal Sample Tracking Chronicle " She110i1 � ' Job No: M76363 SCM.AW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M76363 9 Collected 18 AUG 08 11 00 By ,AW Re ec ived20 AUG 08By MW 3'7 (53) M76363-9 MADEP VPH REV 1.127-AUG-08 06:47 AF VMAVPH M763h3 10,Collected 18 AUG 08 1150 By_-AW ' Received 20 AUG-08 MW7 M76363-10 MADEP VPH REV 1.127-AUG-08 07:28 AF VMAVPH 1VI76333-11 Collected: 18 AUG 08 L2<15 0 By AW,rReceyed 2 `AUG-08 By: k MW-37 (105) t t. M763j3-11 MADEP VPH REV 1.127-AUG-08 08:10 AF VMAVPH M763�3-12 Collected`. 18-AUG-08 12:20 By:AW Received:"20,AUG 08 By-,. MW-�9 (88) M76363-12 MADEP VPH REV 1.127-AUG-08 08:51 AF VMAVPH M76363,13 .Collected: 18 AUG 08 1155 By:,"AW Received: 20-AUG 08 By MW 40 (85)° x" E M76363-13 MADEP VPH REV 1.127-AUG-08 09:32 AF VMAVPH IvI76363 14 yCollected 18-A"UG"08 1255 By; AW Received:20-AUG-08" By: MW-38 (104) M76363-14 MADEP VPH REV 1.127-AUG-08 15:44 AF VMAVPH M763:G3 15 Collected: 18-AUG 08 13:30 Bys AW' '' Received: 20-AUG-08 "By: MW 38 (89), M76363-15 MADEP VPH REV 1.127-AUG-08 16:26 AF VMAVPH M�763G3 16Collected18AUG"08 09 40 "By'"AW Received 207AUG0.8 By ; M76363-16 MADEP VPH REV 1.127-AUG-08 17:07 AF VMAVPH Page 2 of 3 =:F® 48 of 55 ®A M76363 - - Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes RW 102 17 Collected;18 AUG 08 11 20 By <,AW Rec ued p20 AUG 08 By vX � . M76363-17 MADEP VPH REV 1.127-AUG-08 17:49 AF VMAVPH M7636348 Collected`._18 AUG 08 10:30„By:AW Z Received. 20-AUG-08 By MW-25 (72) M76363-18 MADEP VPH REV 1.127-AUG-08 18:30 AF VMAVPH Page 3 of 3 M® 49 of 55 ACCUTEST< M76363 -'. - ,.4-1,7,- f - v r New England ACCUTES'6® I_abora tomes Section 5 .. s h A tH-Tr.hit r°HEMiSYft.V.. _. ._ .......... _ _.., _ . GC Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ® 50 of 55 UACCUTEST• ......._..--....._...._... M76363 i_a_..:...t... . Method Blank Summary Page 1 of I .lob Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID . DF Analyzed By Prep Date Prep Batch Analytical Batch GBD990-MB BD20849.D 1 08/26/08 AF n/a n/a GBD990 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76363-1, M76363-2, M76363-3, M76363-4, M76363-5, M76363-6, M76363-7, M76363-8, M76363-9, M76363-10, M76363-11, M76363-12, M76363-13 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-4--4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 826/. 70-130% 615-59-8 2,5-Dibromotoluene .88% 70-130% k"e® 51 Of 55 ®ACCUTEST. M76363 Method Blank Summary Page 1 of 1 Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD991-MB BD20873.1) 1 08/27/08 AF n/a n/a GBD991 ve i The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76363-14, M76363-15, M76363-16, M76363-17, M76363-18 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND' 2.0 ug/l 100-4±-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/l CAS-No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 82% 70-130% 615-59-8 2,5-Dibromotoluene 91% 70-130% ® 52 of 55 ACCUTEST, M76363 _... ..... .. r Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD990-BSP BD20850.D 1 08/26/08 AF n/a n/a GBD990 GBD990-BSD BD20851.D 1 08/26/08 AF n/a n/a GBD990 iv The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76363-1, M76363-2, M76363-3, M76363-4, M76363-5, M76363-6, M76363-7, M76363-8, M76363-9, M76363-10, M76363-11, M76363-12, M76363-13 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/l % ug/I % RPD Rec/RPD 71-43-2 Benzene 50 51.7 103 51.7 103 0 - 70-130/25 100-41-4 Ethylbenzene 50 52.6 105 52.7 105 0 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 51.6 103 51.7 103 0 70-130/25 91-20-3 Naphthalene 50 48.4 97 49.9 100 3 70-130/25 108-88-3 Toluene 50 52.3 105 52.4 105 0 70-130/25 m,p-Xylene 100 105 105 105 105 0 70-130/25 95-47-6 o-Xylene 50 49.4 99 49.5 99 0 70-130/25 C5- C8 Aliphatics (Unadj.) 150 142 95 144 96 1 70-130/25 C9- C12 Aliphatics (Unadj.) 150 141 94 141 94 0 70-130/25 C9- C10 Aromatics (Unadj.) 50 50.1 100 50.3 101 0 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 81% 83% 70-130% 615-59-8 2,5-Dibromotoluene 89% 91% 70-130% Q® 53 of 55 14CCUTE3T M76363 .. . .......... . Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD991-BSP BD20874.D 1 08/27/08 AF n/a n/a GBD991 GBD991-BSD BD20875.D 1 08/27/08 AF n/a n/a GBD991 CA iv The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76363-14, M76363-15, M76363-16, M76363-17, M76363-18 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/I % ug/I % RPD Rec/RPD 71-43-2 Benzene 50 53.6 167 52.2 164 3 70-130/25 100-41-4 Ethylbenzene 50 54.2 108 52.7 105 3 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 54.1 108 51.2 102 6 70-130/25 91-20-3 Naphthalene 50 53.1 106 50.9 102 4 70-130/25 108-88-3 Toluene 50 53.7 107 52.3 105 3 70-130/25 m,p-Xylene 100 108 108 105 105 3 70-130/25 95-47-6 o-Xylene 50 50.9 102 49.3 99 3 70-130/25 C5- C8 Aliphatics (Unadj.) 150 150 100 141 94 6 70-130/25 C9- C12 Aliphatics (Unadj.) 150 143 95 138 92 4 70-130/25 C9- C10 Aromatics (Unadj.) 50 52.2 104 50.0 100 4 70-130/25 CAS-No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 84% 85% 70-130% 615-59-8 2,5-Dibromotoluene 93% 93% 70-130% R 54 of 55 ...................... ` M76363 _a_.......... .> L Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method w Lab Lab Sample ID File ID S1 a Sl b M76363-1 BD20859.D 79.0 86.0 M76363-2 BD20860.D 800 87.0 M76363-3 BD20861.D 72.0 80.0 M76363-4 BD20862.D 80:0 87.0 M76363-5 BD20863.D 78.0, 86.0 M76363-6 BD20864.D 80.0 89.0 M76363-7 BD20865.D $1.0 88.0 M76363-8 BD20866.D 82.0' 89.0 M76363-9 BD20867.D 81.0 88.0 M76363-10 BD20868.D 87.0 ` 94.0 M76363-11 BD20869.D $3.0 92.0 M76363-12 BD20870.D 82.0' 91.0 M76363-13 BD20871.D 83.0 93.0 M76363-14 BD20880.D 81.0. 90.0 M76363-15 BD20881.D 81.0 90.0 M76363-16 BD20882.D 87.0 96.0 M76363-17 BD20883.D 82.0 91.0 M76363-18 BD20884.D 81.0 92.0 GBD990-BSD BD20851.D 83.0 91.0 GBD990-BSP BD20850.D 81.0 89.0 GBD990-MB BD20849.D 82.0 88.0 GBD991-BSD BD20875.D 85.0 93.0 GBD991-BSP BD20874.D 84.0' 93.0 GBD991-MB BD20873.D 82.0 91.0 Surrogate Recovery Compounds Limits Sl = 2,5-Dibromotoluene 70-130% (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 n.F® 55 of 55 ®ACCUTEST M76363 _>...,.:. .... �T. h. 1 i SOVEREIGN CONSO July 1,2008 DHL#27987250852 Town of Hyannis Town Engineer 367 Main Street Hyannis, Massachusetts 02601 Re: Groundwater Sampling Results,May 2008 In the Vicinity of: Former Texaco Service.5tation 1140 Iyanriough Road 1 RTN 4-11301 To Whom it May Concern; Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH) and _gasoline oxygenates. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVE CONSULTING,INC. Jason Sherburne Project Manager cc: Mr.David Weeks,Motiva MassDEP-SERO Sovereign File—EQ711 � u co W r— M 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: '508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan 2 BWSC 123 This Notice is Related to Release Tracking Number 4 4� 11301 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Hyannis,Town Engineer 2. Street Address: 367 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: Sherburne@sovcon.com NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. T e Hardcopy 2.0 Automated Report New Engl.antl � . x L-alsoratories - - � �L z � {� Shell Oil SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ,. EQ 711 Accutest Job Number: M73538 Sampling Dates: 05/15/08 - 05/16/08 Report to: Sovereign Consulting Inc. jsherburne@sovcon.com ATTN: Jason Sherburne Total number of pages in report: 82 AC a -:• Test results contained within this data package meet the requirements tea and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136)'FL(E87579) A R $,. NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England 495 Tech Center West • Building I • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • http://www.accutest.com 11 1 of 82 CIACC UTEST. M73538 L=trara tore: a �7 Table of Contents Sections: Section1: Sample Summary ........................................................................................... . Section2: Case Narrative/Conformance Summary .............................................................. 5 Section3: Sample Results ........................................................................................................ 7 3.1: M73538-1: MW-9R ...................................................................................................... 8 3.2: M73538-2: MW-21 (55) 3.3: M73538-3: MW-19 (55) ............................................................................................... 12 3AM73538-4: MW-32 (55) ............................................................................................... 14 3.5: M73538-5: MW-26 (72) ............................................................................................... 16 3.6: M73538-6: 1\4W-25 (72) ............................................................................................... 18 • 3.7: M73538-7: MW-24(42) ......................... 3.8: M73538-8: MW-39 (88) ............................................................................................... 22 3.9: M73538-9: MW-40 (85) ............................................................................................... 24 3.10: M73538-10: MW-31 (55) ........................................................................................... 26 3.11: M73538-11: MW-35 (53) ............................................................................................ 28 3.12: M73538-12: MW-34 (53) ........................................................................................... 30 3.13: M73538-13: MW-37 (53) ........................................................................................... 32 3.14: M73538-14: MW-29 (68) ........................................................................................... 34 3.15: M73538-15: MW-20 (55) ........................................................................................... 36 Section4: Misc. Forms ............................................................................................................ 38 4.1: Chain of Custody ........................................................................................................... 39 4.2: MCP Form ...................................................................................................................... 41 4.3: VPH Form ...................................................................................................................... 42 4ASample Tracking Chronicle ........................................................................................... 57 Section 5: GUMS Volatiles- QC Data Summaries .............................................................. 60 5.1: Method Blank Summary .......................................................................... 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 66 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 71 5A Surrogate Recovery Summaries ..................................................................................... 75 Section6: GC Volatiles - QC Data Summaries ..................................................................... 77 6.1: Method Blank Summary ................................................................................................ 78 6.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 80 6.3: Surrogate Recovery Summaries ..................................................................................... 82 2 of 82 12ACCUTEST. M73538 Lz6c.ra turi-es Accutest Laboratories Sample Summary Shell Oil SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Job No: M73538 Project No: EQ 711 Sample Collect = Matrix Chem .,.ems ,FH.,F.__....-. Number Date Time By Received Code Type Sample ID 3538t 05/15/08 09:00 RD 05/19/08 AQ Ground Water 1tNO 338 2� 05/15/08 09:30 RD 05/19/08 AQ Ground Water 1l� � M 353g 3 _=05/15/08 10:10 RD 05/19/08 AQ Ground Water }73'38 4w 05/15/08 10:40 RD 05/19/08 AQ Ground Water M73538 5:, 05/15/08 11:10 RD 05/19/08 AQ Ground Water 1W M7�35o38 6-,. 05/15/08 11:45 RD 05/19/08 AQ Ground Water M (T s c x1V173538 7 05/15/08 12:10 RD 05/19/08 AQ Ground Water 14 42 M73538 8 05/15/08 13:00 RD 05/19/08 AQ Ground Water M73538 9 05/15/08 13:50 RD 05/19/08 AQ Ground Water 4Q 8 M7338 10 05/15/08 14:05 RD 05/19/08 AQ Ground Water MW M7353$11, :05/15/08 13:35 RD 05/19/08 AQ Ground Water MW 3 53 M73538 12 05/15/08 13:00 RD 05/19/08 AQ Ground Water MW 34 (53}3 x M73538 13 05/15/08 12:25 RD 05/19/08 AQ Ground Water ® 3 of 82 IPACCLffr=B7: M73538 Crtr aratorie: Accutest Laboratories Sample Summary Shell Oil (continued) SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Job No: M73538 Project No: EQ 711 Sample �ollCed f a Matrix Client n=.,._.F ...,.,._...,h Number Date Time By Received Code Type Sample ID 10—38 14 :05/16/08 11:15 RD 05/19/08 AQ Ground Water f ?11�@10 05/16/08 08:45 RD 05/19/08 AQ Ground Water W _._._. MO M ® 4 of 82 ��aCc�,.�rEST M73538 =6c ato rle; 'G it Lab0ratorieS SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M73538 Site: SCMAW:97346878(REIMBMA)1140 Iyannough Road Hyannis MA Report Date 6/12/2008 12:05:15 PM 15 Sample(s)were collected on between 05/15/2008 and 05/16/2008 and were received at Accutest on 05/19/2008 properly preserved, at 2.5 De .C and intact. These Samples received an Accutest job number of M73538.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified cahbrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GCMS By Method SW846 8260B Matrix AQ Batch ID: MSG3306 ■ All method blanks for this batch meet method specific criteria. ■ Sample(s) M73491-21MS,M73491-21MSD were used as the QC samples indicated. ■ M73538-5:Elevated RL due to dilution required for matrix interference. ■ Only.MTBE,DIPE,TAME,ETBE and TBA requested. Matrix AQ Batch ID: MSG3307 ■ All samples were analyzed within the recommended method holding time. ■ Sample(s) M73577-2MS,M73577-2MSD were used as the QC samples indicated. ■ All method blanks for this batch meet method specific criteria. ■ Only MTBE,DIPE,TAME,ETBE and TBA requested. Matrix AQ Batch ID: MSG3308 ■ All method blanks for this batch meet method specific criteria. ■ Sample(s) M73586-6MS,M73586-6MSD were used as the QC samples indicated. Matrix AQ Batch ID: MSP952 ■ All method blanks for this batch meet method specific criteria. ■ Sample(s) M73513-5MS,M73513-5MSD.were used as the QC samples indicated. ■ Only MTBE,DIPE,TAME,ETBE and TBA requested. Matrix AQ Batch ID: MSR188 ■ All method blanks for this batch meet method specific criteria. ■ Only MTBE,DIPE,TAME,ETBE and TBA requested. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GAB2377 ■ All samples were analyzed within the recommended method holding time. ■ All method blanks for this batch meet method speck criteria. Matrix AQ Batch ID: GWX1970 ■ All samples were analyzed within the recommended method holding time. ■ All method blanks for this batch meet method specific criteria. Thursday,June 12,2008 Page 1 of 2 11 5 of 82 MACCUTEST. M73538 1-L s---„�c, The Accutest Laboratories of New England certifies that all analysis were performed within method specification.Its further recommended that this report to be used in its entuety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M73538). Thursday,June 12,2008 Page 2 of 2 Lj 6 of 82 OACCUTEST. M73538 tetcrato riez New England ACCLrjj I..abaratorIeISection 3 �k � e s -Avr- Report of Analysis 7 of 82 gAC ; M73538 Mori es . r. Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-26 (72) Lab Sample ID: M73538-5 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Methcd: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#_ a G81910.1) 2 05/29/08 EL n/a n/a MSG3306 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether D 4.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 5'p 8 2.0 ug/I 994-05-8 tert-Amyl Methyl Ether WD 4.0 ug/I 75-65-0 Tert Butyl Alcohol 40 ug/1 637-92-3 tert-Butyl Ethyl Ether D ,: 4.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 79-130% 2037-26-5 Toluene-D8 9>5% 80-120% 460-00-4 4-Bromofluorobenzene 80120% (a) Elevated RL due to dilution required for matrix interference. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 1123 16 of 82 UACCUTEST M73538 LaL c.rtorec Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-26 (72) Lab Sample ID: M73538-5 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#l. WX41554.13 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml. Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene INN 2.0 ug/1 100-41-4 Ethylbenzene -D ;=2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 4 1 2.0 ug/1 91-20-3 Naphthalene P, 3.0 ug/1 108-88-3 Toluene �)\D 2.0 ug/1 m,p-XyleneD 2.0 ug/1 95-47-6 o-Xylene N17 2.0 ug/1 C5-C8 Aliphatics (Unadj) -D �!._; 50 ug/I C9- C12 Aliphatics (Unadj ) << 50 ug/1 C9-C10 Aromatics (Unadj ) IUD t 50 ug/I C5- C8 Aliphatics I1€D 50 ug/1 C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene &gip/o , 70-130% 615-59-8 2,5-Dibromotoluene 86% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 82 UACCLffEBT. M73538 Lsb^.r3to :t: Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-25 (72) Lab Sample ID: M73538-6 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P28623.1) 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether IUD =2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 12 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether AID w 2.0 ug/I 75-65-1 Tert Butyl Alcohol ND - 20 ug/I 637-92-3 tert-Butyl Ethyl Ether IUD 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 79130% 2037-26-5 Toluene-D803°/v, 80-120% 460-00-4 4-Bromofluorobenzene 1D1% 80120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®11 18 of 82 GACCUT'EST; M73538 fat crturi-<c Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-25 (72) Lab Sample ID: M73538-6 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41555.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene N#D2.0 ug/1 100-41-4 EthylbenzeneD : 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 2zl1 2.0 ug/I 91-20-3 Naphthalene III n 3.0 ug/I 108-88-3 Toluene 2.0 ug/1 m,p-Xylene 2.0 ug/1 95-47-6 o-Xylene 2.0 ug/I C5-C8 Aliphatics (Unadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadu) a,50 ug/1 C9- C10 Aromatics (Unad3 ) D - 50 ug/1 C5- C8 Aliphatics N'D 50 ug/1 C9-C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene f3Q% 70130% 615-59-8 2,5-Dibromotoluene 83% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 19 of 82 12p►CCUTES7: M73538 lab c'a curses Accutest Laboratories Report of Analysis Page 1 of 1 Pi Client Sample ID: MW-24 (42) Lab Sample ID: M73538-7 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P28624.D 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 ml Run#? Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether NWID 1.0 ug/1 994-05-8 tert-Amyl Methyl EtherD '2,0 ug/1 75-65 j0 Tert Butyl Alcohol De 20 ug/1 637-92-3 tert-Butyl Ethyl Ether 2.0 ug/1 CAS No. Surrogate Recoveries Run# I Run#2 Limits 1868-53-7 Dibromofluoromethane 105°l0 79-130% 2037-26-5 Toluene-D8 80120% 460-00-4 4-Bromofluorobenzene 1,02°/0 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®O 20 of 82 QACCUTEBT. M73538 t=t=rco ec Accutest Laboratories Report of Analysis Page I of I Client Sample ID: MW-24 (42) Lab Sample ID: M73538-7 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41556.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-NTH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 2.0 ug/I 100-41-4 Ethylbenzene NIk 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 1 I1 2.0 ug/I 91-20-3 Naphthalene IUD 3.0 ug/I 108-88-3 Toluene ltD 2.0 ug/I m,p-Xylene D 2.0 ug/I 95-47-6 o-Xylene 1D 2.0 ug/I-," C5-C8 Aliphatics (Unadj ) m 50 ug/I C9- C12 Aliphatics (Unadj 50 ug/I C9- CIO Aromatics (Unadj ) 1D - 50 ug/I C5- C8 Aliphatics1D 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 14% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 19 21 of 82 QACCUTEST' M73538 t=" Accutest Laboratories Report of Analysis Page I of I co Client Sample ID: MW-39 (88) Lab Sample ID: M73538-8 Date Sampled: 05/15/08 Matrix: AQ- Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P28625.1) 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 nil Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether fD 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 2Q 1# 1.0 ug/1 994-05-8 tert-Amyl Methyl EtherD '2.0 ug/1 75-65-0 Tert Butyl Alcohol D 20 ug/1 637-92-3 tert-Butyl Ethyl Ether 1 ?D 2.0 ug/I CAS No. Surrogate Recoveries Run#1 Run#2 Limits 1868-53-7 DibromofluoromethaneQ5% 79-130% 2037-26-5 Toluene-D8 99°Io = 80-120% 460-00-4 4-Bromofluorobenzene 102% , `' 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 130 22 of 82 CIACCUTEST. ` M73538 L AccutEst Laboratories Report of Analysis Page 1 of I co Client Sample ID: MW-39 (88) Lab Sample ID: M73538-8 Date Sampled: 05/15/08 Matrix: AQ -Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41557.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71 43-2 Benzene 2.0 ug/1 100-41-4 Ethylbenzene ND _ ' 2.0 ug/1 1634-04-4 Methyl Tert Butyl EtherD 2.0 ug/1 91-20-3 Naphthalene 1D x 3.0 ug/1 108-88-3 Toluene IUD 2.0 ug/1 m,p-Xylene 2.0 ug/1 95-47-6 o-Xylene ND =2.0 ug/1 C5- C8 Aliphatics (Unadj) 50 ug/I C9- C12 Aliphatics (Unadj.) D 50 ug/I C9- C10 Aromatics (Unadj ) ND 50 ug/I C5- C8 Aliphatics } D 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene 70130% 615-59-8 2,5-Dibromotoluene 82%, 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 23 of 82 QACCLJTEST. M73538 =6aracorics 1 Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW-40 (85) Lab Sample ID: M73538-9 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P28626.D 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether lip 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 k 637-92-3 tert-Butyl Ethyl Ether iD 2.0 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane05% 79130% 2037-26-5 Toluene-D8 80120% 460-00-4 4-Bromofluorobenzene i'00°!a_ . ' 80 120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®TI 24 of 82 12ACCUTEST. M73538 =b orcoritc Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-40 (85) Lab Sample ID: M73538-9 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41558.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-NTH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 2.0 ug/1 � 100-41-4 Ethylbenzene IUD 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics IUnadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/I C9- C10 Aromatics(Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics 'ND:, � ,�: 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 70 130% 615-59-8 2,5-Dibromotoluene 80% 70-130% ND = Not detected J = Indicates an estimated value RL = 'Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®B 25 of 82 INACCUTEST. M73538 t;.tr c I I--Iw ®� New England Ac UTEsr• r Section 4 r 1Vlisc Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle ®� 38 of 82 UAMUTEST: M73538 tontor.es LAB(LOCATION) Shell Oil Products Chain Of Custody Record Mq1 5?6 Plinsti Check Appropriate :::Ptriptim:r,: Name:CoDtSd ::INC.IDENT:#!ENV.:SERV.IC15S►::Cl El ACCUTEST Dave Weeks 9 7 3 4 6 8 7 8 DATE: 0 OTHM ar.E' PAGE: W 7-OT-05 Sovereign Consulting Inc 1140 Iyannough Road,Hyannis,MA 9058 South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Report Io):Jason She bum CONSULTANT PROJECT NO.:E0711 Mansfield,MA 02048 ............ ................ ..... .......... ........ .. sherburneCmsovcon ....... .... ...... . ........ .... .. T- 508.339.3200 508.339.3248 COM 0 SrMDARD(14 DAY) ❑5 MY$ 0 3 DAYS 0 2 DAYS [124 HMMS REQUESTED ANALYSIS out"ABUS: Do"., 0 ODOM 0"op 0 Ra bore (gwn) TEM TUREONRECEIPT0 Cowan ic. 'z it CoRler Art SPECIAL INSTRUCTIONS OR NOTES; SAMPUNG Field Sample Identification DATE TIME x C a. -bL— D R..dip > O .i ..my NM- lie 5/ir 01160 g�:W XIX I I ow-21 Uq— Ow Mw- f I I I I I q(f5) 10jo + MW-3?"S5 1044 Mw-2eC7Z) 25-(7Z) IIyS zq(142) 210 — ---———————— KW- 31(819) t4w-40 (if) R. —by Tm- 3-Es—) ,3-14 M73538: Chain of Custody Page 1 of 2 39 of 82 MACCUrEErr. M73538 LAB(LOCATION) — 4 Shell Oil Products Chain Of Custody Record V »Pfease:Cfieck pnate BoA: >= PrSritBdl Tfl Gontaot Name <:: INCIDENT 4 tfNYSfRY1GE5).::p aEa vno naDENr b APn Es ❑ENv gRnas ❑mOnvA RETALL ❑snDt RtruL Dave Weeks �'"��T 9 7 3 4 6 817 18 GATE: e ❑Horn.sown O caNsuLTnxr p LueEs PD M SAP>f; ❑OTRER(_. ..J ❑snot mPElalE omen PAGE:. Z of Z 1 0 0 0 8 3 SnEMMe 154va1,Ony.ntl bb�y: Soverei n Consultin Inc 1140 I nnou h Road,H nnis,MA 905E South Main Street,Unit 202 CONSUL7ANi PROJECT CONTACT(Report to)Jason She--, -NSULTANT PROJECT NO.:EQ711 Mansfield MA02048 must NIT K 08.339.3200 508-339.3248 Lherburnea_)sQvgqg,Com CAST NRNNiWND TIME(CAEENDAR DAYS4 O STAWW(1,MY) D s mYs ❑1 DAYS p 2 DAYS ❑r nouns REQUESTED ANALYSIS MLIVEP—ES. 11 co-m ❑wmr i El mcF ❑PlP ❑Or—(VEC-)_ IEMPERATUREONRECE-17 Co al ICbderbi ;Epgxp SPECIAL INSTRUCTIONS OR NOTES: .� SAMPLING vwESERVArnE � Field Sample Identification DATE TIME CONG LL M CO MIRN PID Rud'bgs NLl w,ol MSW NONE OTHER > Q' P LitMM10n'NOiu ow-35 53 133s Gw ul 4 XX MW_3y(r3) 1306 r'$ Mw- 37(S3) 12zS Mlt/-7- (_.-IS l6 lt1� Mw- zc ss s l6 o8y� RN.quene eYl •�j)V//A R.rmw:hda lso• ..I ,...�er.lsronw..: 2. T/(/ o12N6 Re.nm M73538: Chain of Custody Page 2 of 2 40 of 82 93AC CMEST. M73538 L=L�`a co ri Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 N Title: MADEP MCP Response Action Analytical Report Certification Form Laboratory Name: Accutest Laboratories of New England Project#: M73538 Project Location: SCMAW:97346878(REIMBMA) 1140 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M73538-1,M73538-10,M73538-11,M73538-12,M73538-13,M73538-14,M73538-15,M73538-2 M73538-3,M73538-4,M73538-5,M73538-6,M73538-7,M73538-8,M73538-9 Sample Matrices: Groundwater X Soil/Sediment () Drinking Water () Other: () () 8260E X 8151A ( 8330 060106 7470A/1A -00"-, 8270C 8081A VPH X 6020 ) 9014M z t' 8082 8021 B ) EPH ) 7000 S 7196A An affirmative response to questions A,B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with 0 Yes ❑ No that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and O Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards orguidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty",as described in Section 2.0(a),(b),(c)and 21 Yes ❑No (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without 0 Yes ❑No ' significant modifications,as specified in Section 11.3? A response to questions E and Fbelow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the Yes No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified ❑ Yes LJ No ' methods)reported? Refer to Narrative , All Negative responses must be addressed in an attached Environmental Laboratory case narrative. l the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is,to the best of my knowledge and belief,accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 06/12/2008 1011 41 of 82 JUACCUTEST: M73538 -=t=---1,r--- r MADEP VPH FORM flatriz z,fi A ueous Soil Sediment Other ON Satisfacto Broken Leakin F1 ueousresecvattue NIA H<=2 n DH>2 Ten` hatu .,t:b a Received on Ice n Received at 4 De- . C Other .i Redd at 2.5 deg C MO GIs N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-26(72) Lab ID: M73538-5 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL (3 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-414 C9-C12 ugA ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 40.1 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:25-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? OYes E! No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes El No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No �� Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 02®�C 4 XrEST M73538sc• MADEP VPH FORM Matra , K A ueous Soil f 1 Sediment Other obi triers Satisfactory Broken F1 Leaking n �i dies awes N/A pH<=2 H>2 Received on Ice Received at 4 Deg. C h Other d ReC'd at 2.5 deg C Mefa(al f ` N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-25(72) Lab ID: M7353M w Method for Target.Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unai iusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ugfl ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 21.1 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/1 ND e 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. 2 A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes E! No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? Yes 01 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? [/:]No 0 Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 ®19 47 of 82 OACCUTEST. M73538 =bo-a toriF; r. MADEP VPH FORM �r ��ueous W Soil f 1 Sediment n Other on`tiners �� Satisfactory Broken Leaking H�2 _ u us�Pres7�attves� WA H<=2 � etn era�ture � � Received on Ice Received at 4 Deg.C Other I./ Redd at 2.5 deg C WN,biano I. WA A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-24(42) Lab ID: M73538-7 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 H Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unad-usted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) NIA ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ugA ND 2 Toluene 108-88-3 C5-C8 ugA ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 2 Benzene 71-43-2 C5-C8 ug/l ND 2 Naphthalene 91-20-3 N/A ugA ND 3 o-Xylene 95-47-6 C9-C12 ugA ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 84 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes _J F✓J !. No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? WYes !_ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? IV]No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 ®LJ 48 of 82 12AC.CUTEST. M73538 L MADEP VPH FORM rfx A ueous n Soil F1 Sediment Other I-1 G1oi>�ta"ers �� xy Satisfactory I1 Broken F I Leakin n�usy�l t. M a JV° N/A n DH<=2 H>2 Received on Ice Received at 4 Deg. C Other ./ Redd at 2.5 deg C Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-39(88) Lab ID: M73538-8 w Method for Targe-.Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unad'usted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 10OAlA C9-C12 ugA ND 2 Toluene 108-88-3 C5-C8 ugA ND 2 Methyl Tert Butyl Ether 1634-04A C5-C8 ugA ND 2 Benzene 71-43-2 C5-C8 ugA ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95A7-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/1 ND a 50 C9-C12 Aliphatics N/A ugA ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z A'Y qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W]Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? fJYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No 0 Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 uO� 49 of 82 13ACCU TEST. M73538 to.•�t�rlcs MADEP VPH FORM Aqueous 1,,1 Soil F-1 Sediment n Other F� Satisfactoryf/ Broken F Leaking n M e-Ou A N/A F1 PH<=2 F,,] PH>2 n Received on lee n Received at 4 Deg.C n Other ✓ Rec!d at 2.5 deg C F] N/A P, Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-40(85) Lab ID: M73538-9 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL 2 C5-C8 Aliphatics(Unadj.) N/A ugA ND' 50 C9-C10 Aromatics(Unadj.) N/A ugA ND' 50 C9-C 12 Aliphatics(Unadj.) NIA ugA ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ugA ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 2 Benzene 7143-2 C5-C8 ugA ND 2 Naphthalene 91-20-3 N/A ugA ND 3 o-Xylene 95-47-6 C9-C12 ugA ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/l ND 50 C9-C 12 Aliphatics N/A ug/I NDc 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 78 70-130% PID:2,5-,Dibromotoluene % 80 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8AIiphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range date exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Tarjet Analytes eluting in that range AND concentration of C9-1310 Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value Were all QA1QC procedures REQUIRED by the VPH Method followed? Fv—'Yes 11 No-Details Attatched Were all performancetacceptance standards for required QA1QC procedures achieved? 1,11Yes F-1 No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No El Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 IMB 50 of 82 OACCUTEBT. M73538 t o- ,-cc Accutest Laboratories Internal Sample Tracking Chronicle Db Shell Oil a Job No: M73538 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M73538-1 MADEP VPH REV.1.128-MAY-08 05:29 AP VMAVPH M73538-1 SW846 8260B 29-MAY-08 20:37 AA V8260OXY5 M73538-2 MADEP VPH REV 1.128-MAY-08 06:12 AP VMAVPH M73538-2 SW846 8260B 29-MAY-08 21:04 AA V8260OXY5 M7353f3 Coveted15 MAII`I�y� Rei ei�edJIA�Q8� r y M73538-3 MADEP VPH REV 1.128-MAY-08 06:54 AP VMAVPH M73538-3 SW846 8260B 29-MAY-08 21:31 AA V8260OXY5 Mr oiiected 15�MAY 8�10 4f B �R� Rec�rvEd 19 MA '1{l By g 9 M73538-4 MADEP VPH REV 1.128-MAY-08 07:37 AP VMAVPH M73538-4 SW846 8260B 29-MAY-08 21:58 AA V8260OXY5 M73538-5 MADEP VPH REV 1.128-MAY-08 08:19 AF VMAVPH M73538-5 SW846 8260B 29-MAY-08 15:04 EL V8260OXY5 M735 $6 Colleted '15lulAY a38 14B RD <Receivedl9,MAY 0$ B M73538-6 MADEP VPH REV 1.128-MAY-08 09:03 AF VMAVPH M73538-6 SW846 8260B 29-MAY-08 19:11 AMY V8260OXY5 M735387Cflleted15 MAY 38 120 BRbRece�yeclkIti1AY QBy u , �x =.ix-�,x,_- .>,..s ,. _ �i ;��'. � sue✓ « � 3 t a� M73538-7 MADEP VPH REV 1.128-MAY-08 09:47 AF VMAVPH Page 1 of 3 57 of 82 UACCUTEST. M73538 -b^' ;uricz Accutest Laboratories Internal Sample Tracking Chronicle A Shell'Oil Job No: M73538 SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M73538-7 SW846 8260B 29-MAY-08 19:39 AMY V82600XY5 M73538-8 MADEP VPH REV 1.128-MAY-08 10:31 AF VMAVPH M73538-8 SW846 8260B 29-MAY-08 20:07 AMY V82600XY5 Mjl $9,�� � t M73538-9 MADEP VPH REV 1.128-MAY-08 11:16 AF VMAVPH M73538-9 SW846 8260B 29-MAY-08 20:35 AMY V82600XY5 M538 10Callcted 15 itAY 118 05 RI3Rece� ec119p�AY fl8 By M73538-10 MADEP VPH REV 1.128-MAY-08 12:00 AF VMAVPH M73538-10 SW846 8260B 29-MAY-08 21:03 AMY V82600XY5 11� 381tolleced15 M fl8135 B RD Deceived 19 MAY 08 By e � M73538-11 MADEP VPH REV 1.128-MAY-08 12:44 AF VMAVPH M73538-11 SW846 8260B 29-MAY-08 14:05 AA V82600XY5 � 38 i2 Calle tell 15 MAY�00$ 13 OOn B RD - Rece ue -I MAY OS By w M73538-12 MADEP VPH REV 1.128-MAY-08 13:29 AF VMAVPH M73538-12 SW846 8260B 29-MAY-08 14:32 AA V82600XY5 �W 3��53�Coll��td 1�5 MAY 0&�1��5�By RD ,�: Re�eiv�d� 19.MAY 08 By M73538-13 MADEP VPH REV 1.128-MAY-08 14:13 AF VMAVPH M73538-13 SW846 8260B 29-MAY-08 16:53 AA V82600XY5 Page 2 of 3 ®® 58 of 82 ®ACCUTEBT. M73538 _t:- ;o.;..; Accutest Laboratories Internal Sample Tracking Chronicle P, Shell Oil Job No: M73538 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M73538-14 MADEP VPH REV 1.128-MAY-08 14:50 AF VMAVPH M73538-14 SW846 8260B 29-MAY-08 22:57 EL V8260OXY5 M73538-14 SW846 8260B 30-MAY-08 13:59 EL V8260OXY5 M58, Colle ed6 J51AY�flB 085j1Re�ived 191UI=A 08 M73538-15 MADEP VPH REV 1.128-MAY-08 15:34 AF VMAVPH M73538-15 SW846 8260B 29-MAY-08 23:25 EL V8260OXY5 Page 3 of 3 ®P] 59 of 82 ®ACCUTEM.. M73538 =to-]tore[ M New England ACCUTOBT. ..k ... t..r�e �. Section 5. G�C/�YIS �vlatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries 60 of 82 12ACCU"TEST. M73538 trarac<re: Method Blank Summary Page I of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3306-MB G81900.1) 1 05/29/08 EL n/a n/a MSG3306 N The QC reported here applies to the following samples: Method: SW846 8260B M735':8-5 CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether N 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 994-05-8 tert-Amyl Methyl Ether N,p 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromotluoromethane 97% 79-130% 2037-26-5 Toluene-D8 98%, 80120% 460-00-4 4-Bromofluorobenzene 1009/6 80-120% ®� 61 of 82 12ACCUTEST. M73538 �t -t,- E Method Blank Summary Page I of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSP952-MB P28608.1) 1 05/29/08 AMY n/a n/a MSP952 N L The QC reported here applies to the following samples: Method: SW846 8260B M73538-6, M73538-7, M73538-8, M73538-9, M73538-10 CAS No. Compound Result RL Units Q 108-20--3 Di-Isopropyl ether N:D 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether NI3 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether NDT 2.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 102% 79-130% 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene 1Q4% 80-120% 62 of 82 12ACCUTEST. M73538 L=cc' _= i Method Blank Summary Page 1 of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR188-MB R4910.1) 1 05/29/08 AA n/a n/a MSR188 The QC reported here applies to the following samples: Method: SW846 8260B M73538-1, M73538-2, M73538-3, M73538-4, M73538-11, M73538-12, M73538-13 CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl etherID 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92:3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 79 130% 2037-2'6-5 Toluene-D8 .1:630k.., 80120% 460-00-4 4-Bromofluorobenzene 1;Q1°lo 80-120% I �® 63 of 82 ®ACCUTES T; M73538 -= Method Blank Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3307-MB G81926.13 1 05/29/08 EL n/a n/a MSG3307 ca The QC reported here applies to the following samples: Method: SW846 8260B M73538-14, M73538-15 CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol NTH 20 ug/1 637-92-3 ter(-Butyl Ethyl Ether N.D 2.0 ug/I CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 96% 79130% 2037-26-5 Toluene-D8 9.9% 80-120% 460-00-4 4-Bromofluorobenzene 97% 80-120% ®M 64 of 82 UACCUTEST. M73538 Method Blank Summary Page I of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3308-MB G81952.1) 1 05/30/08 EL n/a n/a MSG3308 9" The QC reported here applies to the following samples: Method: _SW846 8260B M73538-14 CAS No. Compound Result RL Units Q 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane �3afo 79-130% 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene 9 %0 80-120% ® 65 of 82 MAT. M73536 tat,-ator c: Blank S ike/Bla p nk Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3306-BS G81898.1) 1 05/29/08 EL n/a n/a MSG3306 MSG3306-BSD G81899.1) 1 05/29/08 EL n/a n/a MSG3306 v~ iv The QC reported here applies to the following samples: Method: SW846 8260B M73538-5 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/1 % ug/1 % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 50.0 100 49.1 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 49.3 99 49.1 98 ; 3'0 70-130/25 994-05-8 tert-Amyl Methyl Ether 50 50.7 40 50.4 1Oi1 1 51 138/25 75-65-0 Tert Butyl Alcohol 500 490 9$ 499 100 2 60-146/25 637-92-3 tert-Butyl Ethyl Ether 50 52.0 104 51.6 �103 1 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 99% 100°l° 79130% 2037 26 5 Toluene-D8 98% 99°// 80 120% 460-004 4-Bromofluorobenzene 80120% ®� 66 of 82 13ACCLr .EST; M73538 horo:or:c_ Blank Spike/Blank Spike Duplicate Summary Page I of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSP952-BS P28605.D 1 05/29/08 AMY n/a n/a MSP952 MSP952-BSD P28606.1) 1 05/29/08 AMY n/a n/a MSP952 N The QC reported here applies to the following samples: Method: SW846 8260B M73538-6, M73538-7, M73538-8, M73538-9, M73538-10 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/l % ug/1 % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 51.0 1(2 51.2 56-145/25 1634 D4-4 Methyl Ter(Butyl Ether 50 50.0 100 49.9 I00 0 70-130/25 994-05-8 tert-Amyl Methyl Ether 50 42.7 85 44.7 89: 5 : ' 51 138/25 75-65-0 Tert Butyl Alcohol 500 531 1Q6_ 517 k031 3 ,- 60-146/25 637-92-3 ter(-Butyl Ethyl Ether 50 44.5 89 45.3 .91;, 2 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868- 3-7 Dibromofluoromethane 1.U0% 102P/ 79-130% 2037-26-5 Toluene-D8 100% I-'0'(1% 80-120% 460-00-4 4-Bromofluorobenzene 80120% 67 of 82 ®ACCUTEST. M73538 _ab crn c or;e_ � I Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR188-BS R4908.1) 1 05/29/08 AA n/a n/a MSR188 MSR188-BSD R4909.D 1 05/29/08 AA n/a n/a MSR188 IV The QC reported here applies to the following samples: Method: SW846 8260B M73538-1, M73538-2, M73538-3, M73538-4, M73538-11, M73538-12, M73538-13 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/1 % ug/1 % RPD Rec/RPD 108-20=3 Di-Isopropyl ether 50 35.0 70 33.6 fi7 ., 4 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 56.5 li 3 53.6 70-130/25 994-05-8 tert-Amyl Methyl Ether 50 60.9 1 2'. 57.0 liT, 7 ' 51-138/25 75-65-0 Tert Butyl Alcohol 500 367 73 W 389 7g 6 60-146/25 637-92-3 tert-Butyl Ethyl Ether 50 47.896 45.6 91` 5 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 100% 98% 79-130% 2037-26-5 Toluene-D8 TOW 80-120% 460-00-4 4-Bromofluorobenzene 101% 102% 80-120% 68 of 82 ®ACCUTEST. M73538 Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF' Analyzed By Prep Date Prep Batch Analytical Batch MSG3307-BS G81924.1) 1 05/29/08 EL n/a n/a MSG3307 MSG3307-BSD G81925.1) 1 05/29/08 EL n/a n/a MSG3307 N The QC reported here applies to the following samples: Method: SW846 8260B M7351';8-14, M73538-15 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/l % ug/1 % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 48.7 ;97 47.1 I 3.. : 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 49.0 98 47.5 95 " "- 3" : 70-130/25 994-05-8 tert-Amyl Methyl Ether 50 51.3 103 '50.8 1©Z '- I` 51 138/25 75-65-0 Tert Butyl Alcohol 500 504 101 486 97 ,. 4 - 60 146/25 637-92-3 tert-Butyl Ethyl Ether 50 51.5 103 50.0 100: 3- " 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 98%" 906 79-130% 2037-26-5 Toluene-D8 -98°/a "99%' 80-120% 460-00-4 4-Bromofluorobenzene 93% 92% 80-120% 69 of 82 11ACC UMST. M73538 !=t orn curies Blank Spike/Blank Spike Duplicate Summary Page 1 of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3308-BS G81949.1) 1 05/30/08 EL n/a n/a MSG3308 MSG3308-BSD G81950.1) 1 05/30/08 EL n/a n/a MSG3308 iv The QC reported here applies to the following samples: Method: SW846 8260B M73538-14 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/1 % ug/l % RPD Rec/RPD 1634-04-4 Methyl Tert Butyl Ether 50 47.4 95 46.3 93 2 " 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 79-130% 2037-26-5 Toluene-D8 160% 99°!0 80-120% 460-00-4 4-Bromofluorobenzene 80-120% ®® 70 of 82 INACCI.ITEBT. M73538 = ' Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73491-21MS G8192LD 1 05/29/08 EL n/a n/a MSG3306 M73491-21MSDG81922.D 1 05/29/08 EL n/a n/a MSG3306 M73491-21 G81919.1) 1 05/29/08 EL n/a n/a MSG3306 L) The QC reported here applies to the following samples: Method: SW846 8260B M735';8-5 M73491-21 Spike MS MS MSD MSD Limits CAS No. Compound ug/1 Q ug/I ug/1 % ug/1 % RPD RecJRPD 108-20-3 Di-Isopropyl ether ND 50 52.7 105 50.3101 5 54-155/30 1634-04-4 Methyl Tert Butyl Ether ND 50 48.9 98, 48.7 97 0 54-144/30 994-05-8 tert-Amyl Methyl Ether ND 50 49.4 50.1 1 47-142/30 75-65-0 Tert Butyl Alcohol ND 500 486 T. 494 99 2 60-148/30 637-92-3 tert-Butyl Ethyl Ether ND 50 52.5 51.4 103 2 46-151/30 CAS No. Surrogate Recoveries MS MSD M73491-21 Limits 1868-53-7 Dibromofluoromethane 1040/. - i01'°!0 104% 79-130% 2037-26-5 Toluene-D8 980/c, 80120% 460-00-4 4-Bromofluorobenzene 94% 93We: 101% 80120% ®® 71 of 82 12ACCUTEST. M73538 bor :o ec Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:9734E-878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73513-5MS P28628.1) 5 05/29/08 AMY n/a n/a MSP952 M73513-5MSD P28629.1) 5 05/29/08 AMY n/a n/a MSP952 M73513-5 P28615.1) 1 05/29/08 AMY n/a n/a MSP952 w The QC reported here applies to the following samples: Method: SW846 8260B M73538-6, M73538-7, M73538-8, M73538-9, M73538-10 M73513-5 Spike MS MS MSD MSD Limits CAS No. Compound ug/1 Q ug/l ug/1 % ug/1 % RPD Rec/RPD 108-20-3 Di-Isopropyl ether ND 250 29518 289 116 2 54-155/30 1634-04-4 Methyl Tert Butyl Esher 1.1 250 245 246 98 0 54-144/30 994-05-8 tert-Amyl Methyl Ether ND 250 164 fib 167 67 2 47-142/30 75-65 0 Tert Butyl Alcohol ND 2500 2820 113 2870 JP 2 60 148/30 637-92-3 tert-Butyl Ethyl Ether ND 250 212 85 20984 1 46 151/30 CAS No. Surrogate Recoveries MS MSD M73513-5 Limits 1868-53-7 Dibromofluoromethane 79130% 2037-26-5 Toluene-D8 102% 103% 100% 80120% 460-00-4 4-Bromofluorobenzene 91% 93% 95% 80120% ®� 72 of 82 13A M73538 �'t ' I,, Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73577-2MS G81945.1) 5 05/30/08 EL n/a n/a MSG3307 M73577-2MSD G81946.1) 5 05/30/08 EL n/a n/a MSG3307 M73577-2 G81939.1) 1 05/30/08 EL n/a n/a MSG3307 w The QC reported here applies to the following samples: Method: SW846 8260B M73538-14, M73538-15 M73577-2 Spike MS MS MSD MSD Limits CAS No. Compound ug/1 Q ug/1 ug/l % ug/I % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 0.48 250 237 227 A,94 4 54-155/30 1634-04-4 Methyl Tert Butyl Ether 531 E 250 827 18 805 1f0 3 54-144/30 994-05-8 tert-Amyl Methyl Ether 1.2 250 254 101 247 98. 3 47-142/30 75-65-0 Tert Butyl Alcohol 2490 2500 4860 S 47509t1' 2 60-148/30 637-92-3 tert-Butyl Ethyl Ether 1.4 250 253D1 246 98 3 '; 46-151/30 CAS No. Surrogate Recoveries MS MSD M73577-2 Limits 1868-53-7 Dibromofluoromethane -97% 9ti%' 95% 79-130% 2037-26-5 Toluene-D8 1QQ% 99°l0' 98% _` 80-120% 460-00-4 4-Bromofluorobenzene 91% 93% 9$% 80-120% 73 of 82 MACCUTEBT M73538 s Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73586-6MS G81965.1) 5 05/30/08 EL n/a n/a MSG3308 M73586-6MSD G81966.1) 5 05/30/08 EL n/a n/a MSG3308 M73586-6 G81964.1) 1 05/30/08 EL n/a n/a MSG3308 w The QC reported here applies to the following samples: Method: SW846 8260B M7353'8-14 M73586-6 Spike MS MS MSD MSD Limits CAS No. Compound ug/1 Q ug/1 ug/l % ug/1 % RPD RecJRPD 1634-04-4 Methyl Tert Butyl Ether 5.3 250 246 9.6 241 94 2 54-144/30 CAS No. Surrogate Recoveries MS MSD M73586-6 Limits 1868 53 7 Dibromofluoromethane 10 % 79-130% 2037-26-5 Toluene-D8 100% 99% 97°h 80120% 460-00-4 4-Bromofluorobenzene 94% 93%; 101% 80120% ®� 74 of 82 ®ACCUTEST. M73538 -at ortori c.: Volatile Surrogate Recovery Summary Page I of 2 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: SW846 8260B Matrix: AQ Samples and QC shown here apply to the above method to Lab Lab Sample ID File ID S1 S2 S3 M73538-1 R4922.1) 94 0 101.0 1Q1 0 M73538-2 R4923.D 103.0 102`0 M73538-3 R4924.1) 88 0 ° 101.0 M73538-4 R4925.1) 9ti 0 104.0 101'0 M73538-5 G81910.1) 03`0 95.0101;0 M73538-6 P28623.1) 10tu`bll, 103.01014,0 ' M73538-7 P28624.1) '1()5 0 100.0 1Q (� M73538-8 P28625.D 1050 99.0 102Y`0 M73538-9 P28626.1) 1{05'0 101:0 100 0 M73538-10 P28627.1) K102�0 100.0 980 M73538-11 R4911.1) 196 0 100.0 101 0 M73538-12 R4912.1) 38 0 ' 103.0 102>>'0„ M73538-13 R4914.1) g7 0 105.0 102'0 M73538-14 G81956.D 9fi 0 98.0 M73538-14 G81927.1) 96 0 97.0 96„Q . M73538-15 G81928.1) 96 0 95.0 97:U M73491-21MS G81921.1) 109 0 98.0 M73491-21MSD G81922.1) 101 0 98.0 93 0 M73513-5MS P28628.1) 105 0 ;?- 102.0 M73513-5MSD P28629.1) F03 0 103.0 93 0 M73577-2MS G81945.1) 97 0 100.0 w: M73577-2MSD G81946.1) 96 0 99.0 M73586-6MS G81965.1) 1010 100.0 90 M73586-6MSD G81966.1) 99 0 99.0 MSG3306-BS G81898.1) 99,0 98.0 93.6 MSG3306-BSD G81899.1) 100 0 99.0 93 0 MSG3306-MB G81900.1) 97 0 :` .. 98.0 100'0 MSG3307-BS G81924.1) 98 0 98.0 93 0 MSG3307-BSD G81925.1) 9.8.0 99.0 9Z U MSG3307-MB G81926.1) 99.0 MSG3308-BS G81949.1) 96 0 100.0 92.0: MSG3308-BSD G81950.1) 99.0 921 MSG3308-MB G81952.1) 93..0_ 99.0 M:SP952-BS P28605.1) 100"0 . 100.0 96:Q MSP952-BSD P28606.1) 102 0 100.0 96.0_. MSP952-MB P28608.D 1'02 0.', 99.0 1040 MSR188-BS R4908.1) 100 0 103.0 41 0 MSR188-BSD R4909.1) 98 0 104.0 1020 MSR188-MB R4910.1) 97 0 103.0 1010 ®� 75 of 82 12AC NJTE3T. M73538 t=bor :oi..c Volatile Surrogate Recovery Summary Page 2 of 2 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA F hod: SW846 8260B Matrix: AQ Samples and QC shown here apply to the above method Surrogate Recover � Y Compounds Limits Surrogate Recovery Compounds Limits SI = Dibromofluoromethane ?79 130°/a S2 = Toluene-D8 S3 = 4-Bromofluorobenzene ®® 76 of 82 ®ACCUTEE3T; M73538 L t c o, ®� New England MACC�;.,, ,t..!'t'EST -Y Section 6 iro VI GC z�T¢iat><1�esF QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ®B 77 of 82 12ACCUTEg'r M73538 L-to"�:uriea Method Blank Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch . Analytical Batch GAB2377-MB AB42642.1) 1 05/27/08 AP n/a n/a GAB2377 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M73538-1, M73538-2, M73538-3, M73538-4 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND - 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Ter(Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene NI? 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND ''``:2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) NYI? 50 ug/1 C9- C12 Aliphatics (Unadj ) N7 =50 ug/1 C9- C10 Aromatics (Unadj ) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene ;85% 70-130% I 78 of 82 11ACCUTEST; M73538 t=t or i e: Method Blank Summary Page 1 of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GWX1970-MB WX41550.1) 1 05/28/08 AF n/a n/a GWX1970 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 N173538-5, M73538-6, M73538-7, M73538-8, M73538-9, M73538-10, M73538-11, M73538-12, M73538-13, M73538- • 14, M73538-15 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene NII =2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 2.0 ug/1 91-20-3 Naphthalene N-A 3.0 ug/I 108-88-3 Toluene ND' 2.0 ug/1 m,p-Xylene ND 2.0 ug/l 95-47=6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (UnadJ) ND 50 ug/1 C9- C10 Aromatics (Unadj.) NO: 50 ug/1 C5- C8 Aliphatics ND 50 ug/l C9- C 12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 79%0 70-130% 615-59-8 2,5-Dibromotoluene 85% 70-130% ®� 79 of 82 ®ACCUTEST. � � 4 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2377-BSP AB42643.1) 1 05/27/08 AP n/a n/a GAB2377 GAB2377-BSD AB42644.1) 1 05/27/08 AP n/a n/a GAB2377 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 iv M73538-1, M73538-2, M73538-3, M73538-4 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/1 % RPD Rec/RPD 71-43-2 Benzene 50 55.2 110 53.0 106 4 %; 70-130/25 100-41-4 Ethylbenzene 50 56.8 114 54.3 09 5 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 53.2 106 51.9 a 70-130/25 91-20-3 Naphthalene 50 50.5 101 47.9 96 ,. 5 70 130/25 108-88-3 Toluene 50 53.8 108 51.5 103 4 70 130/25 m,p-Xylene 100 110 110 106 106 "!r 4 70 130/25 95-47 6 o-Xylene 50 53.9 108 51.5 103 5 70-130/25 C5- C8 Aliphatics (Unadj.) 150 123 82 11979 3 70-130/25 C9- C12 Aliphatics (Unadj.) 150 118 79 127 85 7 70 130/25 C9- C10 Aromatics (Unadj.) 50 56.8 114 54.2 108 5 70 130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 86% 81%0 70-130% 615-59-8 2,5-Dibromotoluene 97% 91% 70130% ® 80 of 82 QACCUTEST. M73538 =t=f,:�� ec Blank Spike/Blank Spice Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GWX1'970-BSP WX41551.1) 1 05/28/08 AF n/a n/a GWX1970 GWX1970-BSD WX41552.D 1 05/28/08 AF n/a n/a GWX1970 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 il) M73538-5, M73538-6, M73538-7, M73538-8, M73538-9, M73538-10, M73538-11, M73538-12, M73538-13, M73538- • 14, M73538-15 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/1 % RPD Rec/RPD 71-43-2 Benzene 50 52.1 If04 52.6 i2rl,05 1 70-130/25 100-41-4 Ethylbenzene 50 49.6 99 49.9 11004 - `1 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 49.8 100 50.2 WOO �1 70 130/25 9120-3 Naphthalene 50 53.5107, 53.6 fi107r 0 70-130/25 108-88-3 Toluene 50 515 x103 51.9 ]04 1 '' 70-130/25 m,p-Xylene 100 101 101 101 l0i 0, 70-130/25 95-47-6 o-Xylene 50 47.6 =95 47.8 961 70-130/25 C5- C8 Aliphatics (Unadj.) 150 149 99 152 10I 2 g 70-130/25 C9- C12 Aliphatics (Unadj.) 150 139 ;9.3 141 94 1 70-130/25 C9 C10 Aromatics (Unadj.) 50 45 90 45 91 I 70 130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 81°fo 81% 70-130% 615-59-8 2,5-Dibromotoluene 88% '88% 70-130% ®® 81 of 82 ®ACCUTEST. M73538 Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b a) is M73538-1 AB42661.D 'AA' 85.0 M73538-2 AB42662.1) 76 0 86.0 M73538-3 AB42663.D 77 0 87.0 M73538-4 AB42664.1) 0 88.0 M73538-5 WX41554.1) `S10 86.0 M73538-6 WX41555.1) 8Q 0 83.0 M73538-7 WX41556.1) 0 84.0 M73538-8 WX41557.1) '79 D 82.0 M73538-9 WX41558.1) 78'0 80.0 M73538-10 WX41559.1) 79 0 83.0 M73538-11 WX41560.1) T4_.0___..- 77.0 M73538-12 WX41561.1) 73 0 76.0 M73538-13 WX41562.D5 Q :I 78.0 M73538-14 WX41563.1) 77:0 81.0 M73538-15 WX41564.1) 75.0__._1 79.0 GAB2377-BSD AB42644.D 810 91.0 GAB2377-BSP AB42643.D 86 0 97.0 GAB2377-MB AB42642.D 77 0 85.0 GWX1970-BSD WX41552.1) 810 88.0 GWXi970-BSP WX41551.1) 810 88.0 GWX1970-MB WX41550.D 79.0 85.0 ..._....... .. Surrogate Recovery Compounds Limits S1 = 2',5-Dibromotoluene 7:0 134°l0 (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 ®� 82 of 82 12ACCUTEST. M73538 t-t o , y + SOVER. EIGN CONSULTING July 1,2008 DHL#27987959053 Ms. Donna Z. Miorandi Town of Barnstable Public Health Division 200 Main Street r Hyannis,MA 02601 _ Re: Groundwater Sampling Results,May 2008 In the Vicinity of: Former Texaco Service Station 1140 Iyannough Road RTN 4-11301 Dear Ms. Miorandi; Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater samples frcm monitoring wells installed at the above referenced property. The samples were submitted ror laboratory analysis of volatile petroleum hydrocarbons (VPH) and gasoline oxygenates. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely ' SOVE I CONSULTING,INC. g t ' Jason Sherburne Project Manager .9 l .. Z cc: Mr.David Weeks,Motiva MassDEP-SERO s Sovereign File-EQ711 9053 S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING j As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan I BWSC 123 € This Notice is Related to Ll Release Tracking Number\ j 4� 11301 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Donna Miorandi 2. Street Address: 200 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): z1.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked,the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will belhas been conducted: 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells _y E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne Street Address: 905B South Main St., Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: Sherburne@sovcon.com NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. e Hardcopy 2.0 r Automated Report New England l a b o r a t o r i e s a w r � Shell Oil Ay Y SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA EQ 711 Accutest Job Number: M73538 Sampling Dates: 05/15/08 - 05/16/08 f Report to: Sovereign Consulting Inc. jsherburne@sovcon.com ATTN: Jason Sherburne Total number of pages in report: 82 XWj: e • • e" Test results contained within this data package meet the requirements , a Z of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) Y ;:E ,A...R :$, NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE o 0 m This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England • 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • http://www.accutest.com 23 1 of 82 UACCUTEST. M73538 Laboratories Table of Contents Sections: -1- Section1: Sample Summary ................................................................................................... 3 Section 2: Case Narrative/Conformance Summary .............................................................. 5 Section3: Sample Results ........................................................................................................ 7 3.1: M73538-1: MW-9R ...................................................................................................... 8 3.2: M73538-2: MW-21 (55) 3.3: M73538-3: MW-19 (55) ............................................................................................... 12 3.4: M73538-4: MW-32 (55) ............................................................................................... 14 3.5: M73538-5: NM-26 (72) ............................................................................................... 16 3.6: M73538-6: MW-25 (72) .................................. .................................................... 18 • 3.7: M73538-7: MW-24 (42) ............................................................................................... 20 3.8: M73538-8: MW-39 (88) ............................................................................................... 22 3.9: M73538-9: MW-40 (85) ............................................................................................... 24 3.10: M73538-10: MW-31 (55) ........................................................................................... 26 3.11: M73538-11: MW-35 (53) ....................................................................................:...... 28 3.12: M73538-12: MW-34 (53) ........................................................................................... 30 3.13: M73538-13: MW-37 (53) ........................................................................................... 32 3.14: M73538-14: MW-29 (68) ........................................................................................... 34 3.15: M73538-15: MW-20 (55) ........................................................................................... 36 Section4: Misc.Forms ............................................................................................................ 38 4.1: Chain of Custody ........................................................................................................... 39 4.2: MCP Form ..................................................................................................................... 41 4.3: VPH Form ...................................................................................................................... 42 4.4: Sample Tracking Chronicle ........................................................................................... 57 Section 5: GUMS Volatiles- QC Data Summaries .............................................................. 60 5.1: Method Blank Summary ................................................................................................ 61 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 66 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 71 5.4: Surrogate Recovery Summaries ..................................................................................... 75 Section6: GC Volatiles - QC Data Summaries ..................................................................... 77 6.1: Method Blank Summary ................................................................................................ 78 6.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 80 6.3: Surrogate Recovery Summaries ..................................................................................... 82 11 2 of 82 12ACCUTEST. M73538 Cab ora t.,"es s �• Accutest Laboratories Sample Summary Shell Oil SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Job No: M73538 Project No: EQ 711 Samplellected Matrix Client W Number Date Time By Received Code Type Sample ID M�58 � 05/15/08 09:00 RD 05/19/08 AQ Ground Water `11�1338 � 05/15/08 09:30 RD 05/19/08 AQ Ground Water � ( S ZIS38 33, 05/15/08 10:10 RD 05/19/08 AQ Ground Water BMW 1€ 173-38 4 .05/15/08 10:40 RD 05/19/08 AQ Ground Water1tW ' M73538 5 05/15/08 11:10 RD 05/19/08 AQ Ground Water 2fi 7 ) M73538 6 05/15/08 11:45 RD 05/19/08 AQ Ground Water ;M7358 7 05/15/08 12:10 RD 05/19/08 AQ Ground Water BMW 24',(42} M73538 8 05/15/08 13:00 RD 05/19/08 AQ Ground Water BMW 39`(881 MT353$9, 05/15/08 13:50 RD 05/19/08 AQ Ground Water MV, V5 10 05/15/08 14:05 RD 05/19/08 AQ Ground Water IVIW 31 y{55} . M73,5,,3811-�. 05/15/08 13:35 RD 05/19/08 AQ Ground Water `1FW 35(53} M73538 12 05/15/08 13:00 RD 05/19/08 AQ Ground Water W 34�,(53} M73538 13, 05/15/08 12:25 RD 05/19/08 AQ Ground WaterIW 37e(�3j j 3 of 82 UACCUTEET. M73538 La borato rre: - Y Accutest Laboratories Sample Summary Shell Oil (continued) Job No: M73538 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Collec ed ' Matrix Client Number Date Time By Received Code Type Sample ID 05/16/08 11:15 RD 05/19/08 AQ Ground Water v, 29 (68}� M73538 t 05/16/08 08:45 RD 05/19/08 AQ Ground Water 2Qz' SS W ® 4 of 82 12A►CCUTEST. M73538 lzbcrcurie: �r La b o rat O: r i e s SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M73538 Site: SCMAW:97346878(REIMBMA)1140 Iyannough Road Hyannis MA Report Date 6/12/2008 12:05:15 PM 15 Sample(s)were collected on between 05/15/2008 and 05/16/2008 and were received at Accutest on 05/19/2008 properly preserved, at 2.5 Deg.C and intact. These Samples received an Accutest job number of M73538.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GCMS By Method SW846 8260B Matrix AQ Batch ID: MSG3306 ■ All method blanks for this batch meet method specific criteria. ■ Sample(s) M73491-21MS,M73491-21MSD were used as the QC samples indicated. ■ M73538-5:Elevated RL due to dilution required for matrix interference. ■ Only MTBE,DIPE,TAME,ETBE and TBA requested. Matrix AQ Batch ID: MSG3307 ■ All samples were analyzed within the recommended method holding time. ■ Sample(s) M73577-2MS,M73577-2MSD were used as the QC samples indicated. ■ All method blanks for this batch meet method specific criteria. ® Only MTBE,DIPE,TAME,ETBE and TBA requested. Matrix AQ Batch ID: MSG3308 ■ All method blanks for this batch meet method specific criteria. ■ Sample(s) M73586-6MS,M73586-6MSD were used as the QC samples indicated. Matrix AQ Batch ID: MSP952 ■ All method blanks for this batch meet method specific criteria. ■ Sample(s) M73513-5MS,M73513-5MSD were used as the QC samples indicated. ■ Only MTBE,DIPE,TAME,ETBE and TBA requested. Matrix AQ Batch ID: MSR188 ■ All method blanks for this batch meet method specific criteria. ■ Only MTBE,DIPE,TAME,ETBE and TBA requested. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GAB2377 ■ All samples were analyzed within the recommended method holding time. ■ All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GWX1970 ■ All samples were analyzed within the recommended method holding time. ■ All method blanks for this batch meet method specific criteria. Thursday,June 12,2008 Page 1 of 2 0 5 of 82 QACCUTEST. M73538 Cab 0 1u t u,i e, Ji The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M73538). Thursday,June 12,2008 Page 2 of Lj 6 of 82 QACC nMBT. M73538 Laboratories New England , .. §: L a b 0 r atones '^`" ^k - Section 3 SmleI RAF ults Report of Analysis Ell 7 of 82 MACCUTES'L M73538 Caboratones • X Accutest Laboratories Report of Analysis Page 1 of 1 Client'Sample ID: MW-9R Lab Sample ID: M73538-1 Date Sampled: 05/15/08 Matrix: AQ -Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB42661.1) 1 05/28/08 AP n/a n/a GAB2377 Run#2. Purge Volume Run#1 5.0 ml Run#2. MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene NI) 2.0 ug/1 1634 04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND R ; 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj ) iEl 50 ug/I C9- C10 Aromatics (Unadi ) N1) 50 ug/1 C5- C8 Aliphatics NIa 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 76% 70-130/o° 615-59-8 2,5-Dibromotoluene 85% 70130% i ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound IN11 9 of 82 12ACCUTEBT. M73538 _nboratorc: Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-9R Lab Sample ID: M73538-1 Date Sampled: 05/15/08 Matrix: AQ- Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R4922.1) 1 05/29/08 AA n/a n/a MSR188 Run#2 I Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether Nb 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/I 637-92-3 tert-Butyl Ethyl Ether 2.0 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 94% 79-130% 2037-26-5 Toluene-D8 1Ql% 80-120% 460-00-4 4-Bromofluorobenzene 1019/c 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®B 8 of 82 UACCUTES'L M73538 iaEartor�e: x Accutest Laboratories Report of Analysis Page 1 of 1 g N Client Sample ID: MW-21 (55) Lab Sample ID: M73538-2 Date Sampled: 05/15/08 Matrix: AQ -Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R4923.D 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether N'D 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether IVD 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether IVI7 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 88% 79-130% 2037-26-5 Toluene-D8 80-120% 460-00-4 4-Bromofluorobenzene 102% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 10 of 82 GACCUTES7; M73538 Lzbprato rues Accutest Laboratories Report of Analysis Page 1 of 1 N Client Sample ID: MW-21 (55) Lab Sample ID: M73538-2 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB42662.13 1 05/28/08 AP n/a n/a GAB2377 Run#2 Purge Volume Run#1 5.0 nil Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND, 2.0 ug/1 91-20-3 Naphthalene NIA �r 3.0 ug/1 108-88-3 Toluene N7 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene NCI) 2.0 ug/1 C5- C8 Aliphatics (Unadj.) N'D` 50 ug/1 C9-C12 Aliphatics (Unadj) N1) `- 50 ug/1 C9- C10 Aromatics (Unadj ) tD 50 ug/1 C5-C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics N.D 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 7;1% 70130% 615-59-8 2,5-Dibromotoluene 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range g N — — Indicates presumptive evidence of a compound 11 of 82 �ACCUTEST. M73538 =to- :ur�ec Accutest Laboratories Report of Analysis Page 1 of 1 g w Client Sample ID: MW-19 (55) Lab Sample ID: M73538-3 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R4924.D 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108 -20-3 Di-Isopropyl ether f`tF1 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether NIA 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol Np 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane $8% 79-130% 2037-26-5 Toluene-D8 T0t% 80-120% 460-00-4 4-Bromofluorobenzene 101% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound TJ 12 of 82 MAC.CUTEST. M73538 Ora to it, Accutest Laboratories Report of Analysis Page 1 of 1 w Client Sample ID: MW-19 (55) Lab Sample ID: M73538-3 Date Sampled: 05/15/08 Matrix: AQ- Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB42663.D 1 05/28/08 AP n/a n/a GAB2377 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether N)3 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene NIO 2.0 ug/1 m,p-Xylene Nl? 2.0 ug/1 95-47-6 o-Xylene ND ` 2.0 ug/1 C5- C8 Aliphatics (Unadj.) N17 � 50 ug/1 C9- C12 Aliphatics (UnadJ ) ND 50 ug/1 C9- C10 Aromatics(Unadj ) ND 50 ug/1 C5- C8 Aliphatics Al=I) 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene 87% , 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 13 of 82 UACCUTEST. M73538 tctrcrato ric Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-32 (55) Lab Sample ID: M73538-4 Date Sampled: 05/15/08 Matrix:: AQ -Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R4925.1) 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume Run#1. 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ,'� 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 2 tj 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether N_)7 2.0 ug/1 75-65-0 Tert Butyl Alcohol NU '20 ug/1 637-92-3 tert-Butyl Ethyl Ether hl' 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 91% z 79-130% 2037-26-5 Toluene-D81t34°fo 80120% 460-00-4 4-Bromofluorobenzene 1=01% 80120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M 14 of 82 MACCUTES . M7353$ �a bcratori'e; c Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-32 (55) Lab Sample ID: M73538-4 Date Sampled: 05/15/08 Matrix: AQ- Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB42664.1) 1 05/28/08 AP n/a n/a GAB2377 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 3 . 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 2;4 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene 1VDt 2.0 ug/1 95-47 6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics (Unadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) f,ND w 50 ug/1 C9- C10 Aromatics (Unadj ) .Np 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics N.D 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 70130% 615-59-8 2,5-Dibromotoluene 880o 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 1311 15 of 82 GACCMEST. M73538 Catorstore: Accutest Laboratories Report of Analysis Page 1 of 1 54 Client Sample ID: MW-26 (72) Lab Sample ID: M73538-5 Date Sampled: 05/15/08 Matrix: AQ -Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a G81910.1) 2 05/29/08 EL n/a n/a MSG3306 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether NA 4.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 50 8 '`2.0 ug/1 994-05-8 tert-Amyl Methyl Ether NI7 4.0 ug/1 75 65 0 Tert Butyl Alcohol N 40 ug/1 637-92-3 tert-Butyl Ethyl Ether N) ��4.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane lll3% 79-130% 2037-26-5 Toluene-D8 95% 80-120% 460-00-4 4-Bromofluorobenzene 101% 80-120% (a) Elevated RL due to dilution required for matrix interference. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®IJ 16 of 82 gACCUTIBT. M73538 L<b�.ra curies i ICI Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-26 (72) Lab Sample ID: M73538-5 Date Sampled: 05/15/08 Matrix: AQ- Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41554.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VI?H List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND w 2.0 ug/I 100-41-4 Ethylbenzene N)3 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 2.0 ug/1 91-20-3 Naphthalene AND 3.0 ug/1 108-88-3 Toluene N10 2.0 ug/1 m,p-Xylene 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/l C9- C10 Aromatics (Unadj ) ND 50 ug/1 C5- C8 Aliphatics NfI) 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®11 17 of 82 12ACCUTEST. M73538 =b�ratorie: w Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-25 (72) Lab Sample ID: M73538-6 Date Sampled: 05/15/08 Matrix: AQ -Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P28623.1) 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 51 2 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2:0 ug/1 Tert Butyl Alcohol ug/175-65-0 637-92-3 tert-Butyl Ethyl Ether NI)N. 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane /a 79-130% 2037-26-5 Toluene-D8 103% 80-120% 460-00-4 4-Bromofluorobenzene l0it% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 0 18 of 82 GACCUr EST. M73538 L:.berturi'e: Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-25 (72) Lab Sample ID: M73538-6 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41555.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 2.0 ug/1 100-41-4 Ethylbenzene1 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 211 2.0 ug/1 91-20-3 Naphthalene 3.0 ug/1 108-88-3 Toluene N 2.0 ug/1 m,p-Xylene N'I) 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics (Unadj.) NI) 50 ug/1 C9-C12 Aliphatics (Unadj) ND 50 ug/1 C9- C10 Aromatics (Unadj) ND 50 ug/I C5- C8 Aliphaticsij 50 ug/1 C9- C12 Aliphatics NIA 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene U '- 70-130% 615-59-8 2,5-Dibromotoluene $3% 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 19 of 82 MACCUTEST. M73538 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-24 (42) Lab Sample ID: M73538-7 Date Sampled: 05/15/08 Matrix: AQ -Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P28624.D 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether AND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether N=I3 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether N'D g 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether 1D 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 1;65% 79-130% 2037-26-5 Toluene-D8 00.%v, 80-120% 460-00-4 4-Bromofluorobenzene l02% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®21 20 of 82 12ACCUTEST. M73538 t::borcur c: � � I Accutest Laboratories Report of Analysis Page 1 of 1 y Client Sample ID: MW-24 (42) Lab Sample ID: M73538-7 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41556.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene AND ; 2.0 ug/1 100-41-4 Ethylbenzene =ND = `2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether AND ''2.0 ug/1 91-20-3 Naphthalene ,3.0 ug/1 108-88-3 Toluene N,D 2.0 ug/1 m,p-Xylene -V, 2.0 ug/I 95-47-6 o-Xylene ND ! 2.0 ug/I C5-C8 Aliphatics (Unadj.) ND 50 ug/1 C9-C12 Aliphatics (Unadj ) lyD 50 ug/1 C9-C10 Aromatics (Unad4 ) N� 50 ug/1 C5-C8 Aliphatics ND 50 ug/1 C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# i Run#2 Limits 615-59-8 2,5-Dibromotoluene 8, 70130% 615-59-8 2,5-Dibromotoluene 84%- 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®P] 21 of 82 UACCUTEST. M73538 het o ra t o rl e, Accutest Laboratories Report of Analysis Page 1 of 1 00 Client Sample ID: MW-39 (88) Lab Sample ID: M73538-8 Date Sampled: 05/15/08 Matrix: AQ- Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P28625.D 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether N " 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 201 -` 1.0 ug/I 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/I 75-65-0 Tert Butyl Alcohol Nla '' 20 ug/I ry 637-92-3 tert-Butyl Ethyl Ether N;D 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 1:05°l0 79130% 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene i02°lo 80120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®M 22 of 82 QA 'T M73538 Accutest Laboratories Report of Analysis Page 1 of 1 00 Client Sample ID: MW-39 (88) Lab Sample ID: M73538-8 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41557.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether N 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene 2.0 ug/1 m,p-Xylene ND PR 2.0 ug/1 95-47-6 o-Xylene l 2.0 ug/1 C5- C8 Aliphatics (Unadj.) p 50 ug/1 C9-C12 Aliphatics (Unadj) ,N- 50 ug/1 C9- C10 Aromatics (Unad4 ) NI) 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene 810 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®21 23 of 82 UACCUTEST. M73538 =t=ra u,ricc Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-40 (85) Lab Sample ID: M73538-9 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P28626.13 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether N 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether N ' 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol Nb120 ug/1 637-92-3 tert-Butyl Ethyl Ether N=D 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 105% 79130% 2037-26-5 Toluene-D8 1'01°l0 80120% 460-00-4 4-Bromofluorobenzene 1U0% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®B 24 of 82 CACC UTEBT. M73538 t=r u r c e Accutest Laboratories Report of Analysis Page 1 of 1 54 to Client Sample ID: MW-40 (85) Lab Sample ID: M73538-9 Date Sampled: 05/15/08 Matrix: AQ -Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41558.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 1 ' 2.0 ug/1 100-41-4 Ethylbenzene NI) 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene N:D 3.0 ug/1 108-88-3 Toluene NUJ 2.0 ug/1 m,p-Xylene N)M 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (UnadJ.) 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/1 C9- C10 Aromatics (Unadj ) 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9 C12 Aliphatics D 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 78% 70130% 615-59-8 2,5-Dibromotoluene 80% 70-130% I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 25 of 82 JOACCUT'EBT. M73538 T'�-'ror�es a Accutest Laboratories Report of Analysis Page 1 of 1 0 Client Sample ID: MW-31 (55) Lab Sample ID: M73538-10 Date Sampled: 05/15/08 Matrix: AQ- Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 P28627.D 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether N5 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether Ni) 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 79-130% 2037-26-5 Toluene-D8 100% 80-120% 460-00-4 4-Bromofluorobenzene 98%. 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 1311 26 of 82 CIACCU TEST. M73538 L .b ora tor;es Accutest Laboratories w Report of Analysis Page 1 of 1 0 Client Sample ID: MW-31 (55), Lab Sample ID: M73538-10 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#RA WX41559.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 EthylbenzeneI) 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene A 3.0 ug/I 108-88-3 Toluene NA 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphatics (Unadj) 50 ug/1 C9- C12 Aliphatics (Unad3 ) ND 50 ug/1 C9 C10 Aromatics (Unad3.) ND 50 ug/1 C5- C8 Aliphatics 50 ug/1 C9 C12 Aliphatics 11� i 50 ug/1 CAS No. Surrogate Recoveries .Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 79%, 70130% 615-59-8 2,5-Dibromotoluene 83% 70-130% ND = Not detected J = Indicates an estimated value RL = .Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates evidence of a compound presumptive p 27 of 82 �AC:Ct.J'f'EST. M73538 [zt'rac c: • 9 Accutest Laboratories 54 Report of Analysis Page 1 of 1 Client Sample ID: MW-35 (53) Lab Sample ID: M73538-11 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R4911.D 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether N'A ' 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 69 7 ' 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether 3'6 =2.0 ug/I 75-65-0 Tert Butyl Alcohol NO.; 20 ug/I 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 96% 79-130% 2037-26-5 Toluene-D8 lQ0% 80120% 460-00-4 4-Bromofluorobenzene 101% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound JOIN 28 of 82 12ACCUTEST. M73538 �aborturi es t l Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-35 (53) Lab Sample ID: M73538-11 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41560.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene Nl] 2.0 ug/1 100-41-4 Ethylbenzene N1) '`2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 6T 7 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) 53 1 50 ug/1 C9- C12 Aliphatics (Unad' ;ND 50 ug/1 C9- C10 Aromatics (Unadj ) ND 50 ug/I C5- C8 Aliphatics 0 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 74% 70-130% 615-59-8 2,5-Dibromotoluene 7Z% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 29 of 82 OAC.CMEST M73538 Laboratories Accutest Laboratories w Report of Analysis Page 1 of 1 ^, Client Sample ID: MW-34 (53) Lab Sample ID: M73538-12 Date Sampled: 05/15/08 Matrix: AQ -Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R4912.13 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether SND ';;°2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether NIa 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol 20 ug/I 637-92-3 tert-Butyl Ethyl Ether N 2.0 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 98% 79130% 2037-26-5 Toluene-D880120% 460-00-4 4-Bromofluorobenzene 102% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 0 30 of 82 1JACCUTEST. M73538 Latnrat—it Accutest Laboratories Report of Analysis Page 1 of 1 N Client Sample ID: MW-34 (53) Lab Sample ID: M73538-12 Date Sampled: 05/15/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA i File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41561.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene Nll 3 2.0 ug/1 100-41-4 Ethylbenzene .0 ug/1 1634-04-4 Methyl Tert Butyl Ether Nil} 2.0ug/1 91-20-3 Naphthalene 3.0 ug/I 108-88-3 Toluene NI7 2.0 ug/1 m,p-Xylene 2.0ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) N 50 ug/1 C9-C10 Aromatics (Unadj ) N� 50 ug/1 C5- C8 Aliphatics ND 50 ug/l C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 90., 70 130% 615 59 8 2,5-Dibromotoluene 7 °fo, 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®P] 31 of 82 IJAC.CLJE M73538 Lab o ra tics • l Accutest Laboratories w Report of Analysis Page 1 of 1 w Client Sample ID: MW-37 (53) Lab Sample ID: M73538-13 Date Sampled: 05/15/08 Matrix: AQ- Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R4914.1) 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether AND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ug/1 994-05-8 tert-Amyl Methyl Ether ug/1 75-65-0 Tert Butyl Alcohol NFL? ;20 ug/I 637 92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I CAS No. Surrogate Recoveries Run#.1 Run#2 Limits 1868-53-7 Dibromofluoromethane 97% 79-130% 2037-26-5 Toluene-D8 1l)5% 80-120% 460-00-4 4-Bromofluorobenzene 102% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound JMTJ 32 of 82 0ACCUTEST. M73538 lz 6 ora tor,cc Accutest Laboratories w Report of Analysis Page I of I W Client Sample ID: MW-37 (53) Lab Sample ID: M73538-13 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41562.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND ':2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene N1 2.0 ug/1 95-47-6 o-Xylene NfJ 2.0 ug/I C5- C8 Aliphatics (Unadj.) N) 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/l C9- C10 Aromatics (Unadj. ND 50 ug/I C5- C8 Aliphatics ND 50 ug/l C9-C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 75% 70130% 615-59-8 2,5-Dibromotoluene 7$Pfp 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Irdicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 33 of 82 12ACCUTEST. M73538 l e 6 r—,-u—c Accutest Laboratories Report of Analysis Page 1 of 1 a Client Sample ID: MW-29 (68) Lab Sample ID: M73538-14 Date Sampled: 05/16/08 Matrix: AQ- Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G81927.1) 1 05/29/08 EL n/a n/a MSG3307 Run#2 G81956.1) 2 05/30/08 EL n/a n/a MSG3308 Purge Volume Run#1 5.0 ml Run#2 5.0 ml Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether N,D 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether A!5 a �,;2.0 ug/I 994-05-8 tert-Amyl Methyl Ether 29 2.0 ug/1 75-65-0 Tert Butyl Alcohol 28 5 20 ug/1 637-92-3 tert-Butyl Ethyl Ether NrD 2.0 ug/1 CAS No. Surrogate Recoveries Run# I Run#2 Limits 1868-53-7 Dibromofluoromethane 96% 96°10: 79-130% 2037-26-5 Toluene-D8 97% 98% 80120% 1,7 460-00-4 4-Bromofluorobenzene 96% 96% 80-120% (a) Result is from Run#2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®P] 34 of 82 12ACC UTEST. M73538 " = Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-29 (68) Lab Sample ID: M73538-14 Date Sampled: 05/16/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41563.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene 4 A` 2.0 ug/1 100-41-4 Ethylbenzene 1�17, 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 512 `'2.0 ug/1 91-20-3 Naphthalene NI) 3.0 ug/1 108-88-3 Toluene 2.0 ug/1 m,p-Xylene h NT5, 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) 385 50 ug/1 C9- C12 Aliphatics (Unadj) ND 50 ug/1 C9-C10 Aromatics (Unad3 ) ND 50 ug/1 C5-C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene 81P 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank. E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M 35 of 82 �ACCUTEST. M73538 L-b crcur ec Accutest Laboratories w Report of Analysis Page 1 of 1 Client Sample ID: MW-20 (55) Lab Sample ID: M73538-15 Date Sampled: 05/16/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 G81928.1) 1 05/29/08 EL n/a n/a MSG3307 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether Nb a 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether I`jb ''ry` 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether Np 3 ;2.0 ug/I 75-65-0 Tert Butyl Alcohol NOD ' - 20 ug/I 637-92-3 tert-Butyl Ethyl Ether 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 1868-53-7 Dibromofluoromethane 96% 79-130% 2037-26-5 Toluene-D8 95% 80-120% 460-00-4 4-Bromofluorobenzene 97% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®11 36 of 82 ®ACCUTIESf; M73538 L>L r r-- r Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-20 (55) Lab Sample ID: M73538-15 Date Sampled: 05/16/08 Matrix: AQ-Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41564.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run Q MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene Nll 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj) ND 50 ug/1 C9- C10 Aromatics (Unadj ) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 75% 70-130% 615-59-8 2,5-Dibromotoluene 79% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®M 37 of 82 QACCUTEBT. M73538 Lab.ratoriec 1 ®� New England Section 4 Mis ms a Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle 4 i ®M 38 of 82 12ACCTEST. M73538 La born to r;e, LAB(LOCATION) Shell Oil Products Chain Of Custody Record VM I S?>6 j 06i Piftit".....T.0466..6..C.N. a.r—ne:, -ANCIDONT.4-(ENV.:SERVIC5Sy::0 C._F No I�NCNT APLE oew.xa�m0MOTARtTAL 5t'D�MtEST Dave Weeks 9 7 3 4 6 8 7 8 DATE:. .. .1 ......... ....... ......0.0,�A so� _j .Pp.:.;. �. :SAP 0 ODER 1 10 a. .................. ...... PAGE:. of — 11 U1 Sovereign Consulting Inc 1140 Iyannough Road,Hvannis,MA 905E South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Report to):Jason Shgrbum CONSULTANT PROJECT NO.:EQ7il Mansfield,MA 020 .............. .............. ...................... .......-... -.............sw ................. . ....... isherburne(a-.sovcon. It/alvefly)4"n 508.339.3200 508.339.3248 COM (r-!qr) TURKMMND TINE(CALENDAR DAYSt ......... ....... EI STMDARD(14 DAY) 050-n 0 3 DAYS 0 2 DAYS 0 24 HOURS REOUEb RED ANALYSIS DELIVERABLES: 0 CWr 0 ODPOW 0 MCP 0AV 0 otHet(SPECIFY) TELPERATUREONRECEIKc Cadwyj lCoolerM2 jom 03 SPECIAL INSTRUCTIONS OR NOTES: SAMPLING Field Sample Identification C�tabw PID R ,x DATE TIMEO. or Lb—tm Not. 14w—lie I I I Ix X1 I I I I gw Mw-32" 1046 U(7Z) nw- 25'(72) 1145 1210 .......... 14w-qo (rF) Hore 4414 Mw I (p , Ili/ rwos —_I-- (A /2! M73538: Chain of Custody Page 1 of 2 39 of 82 0ACCILMESM. M73538 LAB(LOCATION) Shell Oil Products Chain Of Custody Record C Print T.4 MNV.:StRv Ce3j.: C --ase h k 6 rawaint.,_ ANODEN � 0 ACCWER Dave Weeks 9 L 71 31 41 8 8 7 B DATE:. Clonox L. 'j PAGE: z 3* Sovereign Consulting Inc 1140 lyannough Road,Hyannis,MA 905E South Main Street Unit 202 CONSULTANT PROJECT CONTACT(Report tO):JaSon Sherburn CONSULTANT PROJECT NO.:EO711 4V& Mansfield,MA 02048 >YNyANNW= .... 508.339.3248 ..... ... .. ...... 68.339.3200 VZA,, A4. NRWRWI 11­(­PARDAYS� ................. ............. 1B STANOARD(14 DAY) [3 5 DAYS 03MyS 0 2 D., 0 2,.01M REQUESTED ANALYSIS DELIVERABLES. C)a"% 11 COMM El PV 0 RCP 0 011®I(Vtom TEMPERATUREO..ECE­ Coo.., 1C 02 ICooiarq SPECIAL INSTRUCTIONS OR NOTES: Field Sample Identification I CDnU1nffPIDRmcHqx > ftt.. I iw--,g 5(5 3 ;y 61 w x L4 x x �Rz 14tv-31(r3 t300 MW-37(05 1245, —A mw-z (og) —VAI I I mr Mw- ZI(5-5) 51)6 41M, 41 -J t o- T- -F—Z., M73538: Chain of Custody Page 2 of 2 40 of 82 OACCXnEW. M73538 La 1,�r 1,1 7 c, Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 N Title: MADEP MCP Response Action Analytical Report Certification Form r _ Laborato Name: Accutest Laboratories of New England Project#: M73538 Project Location: SCMAW:97346878(REIMBMA)1140 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M73538-1,M73538-10,M73538-11,M73538-12,M73538-13,M73538-14,M73538-15,M73538-2 M73538-3,M73538-4,M73538-5,M73538-6,M73538-7,M73538-8,M73538-9 Sample Matrices: Groundwater X Soil/Sediment O Drinking Water O Other: O () � 8151A 8330 6010E 7470A/1A8260B X��� 8270C 8081A VPH 8082 8021B ) EPH 7000S' 7196A „�i�ttet s 9 r dE y'b rr l ralm Z i9i lY3� An affirmative response to questions A,B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with 121 Yes ❑ No that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required forthe specified analytical method(s) B included in this report followed, including the requirement to note and 0 Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards orguidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty',as described in Section 2.0(a),(b), (c)and 0 Yes ❑No ' (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without O Yes ❑No ' significant modifications,as specified in Section 11.3? A response to questions E and Fbelow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the Yes El No ' specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified ❑ Yes LIJ No ' method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. l the undersigned,attest under the pains and penalties of perjury that,based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is,to the best of my knowledge and belief,accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 06/12/2008 Ell 41 of 82 MACCUTEST. M73538 Labor;-- s t MADEP VPH FORM atix A ueous Soil Sediment Other F` stainers� . , y, Satisfacto Broken F1 Leakin ueo:s Piesvatly s'' N/A H<=2 F1 DH>2 hem er tuie �� _ Received on Ice F1 Received at 4 Deg. C Other Rec'd at 2.5 deg C Wtt a alp v ...may:' N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-9R Lab ID: M73538-1 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 H Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ugll ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND 8 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recover^ies Acceptance Range FID:2,5-Dibromotoluene % 76 70-130% PID:2,5-Dibromotoluene % 85 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes,eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes C! No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? ClYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 1JNo Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/1WO08 ®m 42 of 82 �ACCU'T'1EST. M73538 La bra ra too ri ec MADEP VPH FORM IVlatrt ° ' � Aqueous Soil n Sediment Other f�rttal�es � SatisfactoryFyl Broken n Leaking uus`;t?reservatlre N/A H<=2 H>2 T m erature Received on Ice F1 Received at 4 Deg. C Other y- Redd at 2.5 deg C MethanoK 0-2 N/A ,p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-21(55) Lab ID: M73538-2 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 H Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 25-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ugA ND 2 Toluene 108-88-3 C5-C8 ugA ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ugA ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 76 70-130% PID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C&C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? O No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 43 of 82 MACMXMBT. M73538 L u b o r a for ec y r1F MADEP VPH FORM ' trix � A ueous Ry Soil Sediment F1 Other o�n atc°eisx �� Sat isfacto Broken F1 Leakin tJe sese>ra Ives'' N/A El DH<=2 H>2 eratitr� � Received on Ice F1 Received at 4 Deg.C Other Redd at 2.5 deg C V1 aI " N/A 46 Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-19(55) Lab ID: M73538-3 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Rana§ Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-138 ug/I ND 2 Naphthalene 91-20-3 N/A ug/1 ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 87 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director 6/12/2008 Printed Name Reza Tand Date � IMI Li 44 of 82 12ACCU T1EST. M73538 �aLore:oriec 1 � MADEP VPH FORM y OR G ;: A ueous W1 Soil Sediment Other ontater� Satisfa tory W Broken F Leakina El ii�eaus P eseivatE, N/A F1 DH<=2 W PH>2 e bra, Received on Ice Received at 4 De . C Other Redd at 2.5 deg C hA`e#.al' y� N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-32(55) Lab ID: M73538-4 'ta Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ugA ND 2 Toluene 108-88-3 C5-C8 ugA ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 2.4 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range e Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons, Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes U No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WIND 1_1 Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 M 45 of 82 M73538 =bore;uric: MADEP VPH FORM (tat�txa �<� A ueous Soil F1 Sediment F1 Other uo talneis fr Satisfactory Broken Leaking F ueousfresetvatives NIA F1 DH<=2 H>2 m �e`Eatur, w� Received on Ice Received at 4 Den. C F1 Other Redd at 2.5 deg C N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-26(72) Lab ID: M73538-5 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 139-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ugA ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 40.1 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ugll ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C8-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all perform an ce/acceptan ce standards for required QA/QC procedures achieved? DYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 M 46 of 82 GACCiJTEST. M73538 La boratorie; MADEP VPH FORM A ueous Soil n Sediment R Other orttatnr®rsh y � Satisfacto Broken R Leaking uausPresetuattve :. WAR iffl<=2 Pl DH>2 T rn�eigatu ',01, Received on Ice R Received at 4 Deg. C F Other d Reed at 2.5 deg C Metfth'n WA p. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-25(72) Lab ID: M73538-6 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND A 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-044 C5-C8 ugA 21.1 2 Benzene 7143-2 C5-C8 ugA ND 2 Naphthalene 91-20-3 N/A ugA ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoverues Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? PlYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 11 47 of 82 12ACCUTEST. M73538 C b o r 3 cor es MADEP VPH FORM A ueous Wl Soil I-1 Sediment F1 Other Con atcters Satisfacto Broken Leaking D 9`u ou Preserfia#�ive WA F1 DH<=2 PH>2 El 3erri ratu e � j " Received on Ice Received at 4 De . C Other / Rec'd at 2.5 deg C et atiolf2 o. x ., WA Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-24(42) Lab ID: M73538-7 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 25-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ugll ND" 50 C9-C10 Aromatics(Unadj.) N/A ugfl ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 84 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? WYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? LVINo ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 ®M 48 of 82 ®ACCUTEST. M73538 L e b o r�'r f MADEP VPH FORM trtx 3 A ueous Soil Sediment Other F� o talnecs % Satisfacto Broken Leakin yeous�Prese vM.Vesd WAF1 DH<=2 W DH>2 116—A eratureg :k Received on Ice Received at 4 Deg. C Other Rec'd at 2.5 deg C IAethafiaffig, N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-39(88) Lab ID: M73538-8 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ugA ND 2 Toluene 108-88-3 C5-C8 ug/1 ND 2 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/1 ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? C Yes ❑ No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? JYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? O No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 ®EJ 49 of 82 OACCt,JTEBT. M73538 let-13—it: L MADEP VPH FORM rtxF%f A ueous W Soil Sediment 7 Other ❑ tatners = Satisfacto Broken F1 Leakin ueousFreservattvs N/A D H<=2 H>2 etri�a atue Received on Ice Received at 4 Deg.C F1 Other .i Rec'd at 2.5 deg C � Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-40(85) Lab ID: M73538-9 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 PH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ugA ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/1 ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ugA ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 78 70-130% PID:2,5-Dibromotoluene % 80 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5.C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ❑✓Yes ❑ No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? ❑�Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? O No ❑ Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 I ®B 50 of 82 ®ACCUT'EST. M73538 la to r a to ri e: MADEP VPH FORM A ueous w, Soil Sediment F1 Other n ontattxers� Satisfacto Broken D Leaking u sa#i es. N/A F1 DH<=2 W DH>2 e etatulle� Received on Ice Received at 4 Den. C F1 Other ReC'd at 2.5 deg C N/A 4, Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-31(55) Lab ID: M73538-10 c+o Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ugA ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/1 ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Tar et Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ugA ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ugA ND 2 m,p-Xylene C9-C12 ug/I ND 2 i Adjusted Ranges C5-C8 Aliphatics N/A ug/1 ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-CB Aliphatic Hydrocarbons exclude the concentration of Target Analytas eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? L11Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ' W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and - complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 51 of 82 12ACCUTEW. M73538 L=to-Je ,r isc MADEP VPH FORM ueous Soil Sediment Other I Gonfatner ��� Satisfacto Broken Leaking e�t5seseirat`ives N/A H<=2 H>2 in eatu f% Received on Ice Received at 4 Den. C Other n Rec'd at 2.5 deg C Y$ N/A 46 Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-35(53) Lab ID: M73538-11 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ugR 53.1" 50 C9-C10 Aromatics(Unadj.) N/A Ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analvtes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 61.7 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 Ug/I ND 2 m,p-Xylene C9-C12 ug/1 ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A Ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 74 70-130% PID:2,5-Dibromotoluene % 77 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes J No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? Yes ! No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 gmpq 52 of 82 12ACCUTEST. M73538 Labar�;o ies � r MADEP VPH FORM A ueous Soil 1-I Sediment F1 Other ontatners n�f Sa isfactorvFvl Broken n Leaking I-1 �t�a)tsl�rese> atty N/A H<=2 I✓ H>2 erature � Received on Ice Received at 4 De . C Other Redd at 2.5 deg C MWf ai%dC ..' N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-34(53) Lab ID: M73538-12 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analvtes Toluene 108-88-3 C5-C8 ug/I ND 2 o-Xylene 9547-6 C9-C12 ugA ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 7143-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Ethylbenzene 10041-4 C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A Ug/I ND B 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 76 70-130% FID:2,5-Dibromotoluene % 73 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C8-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? OV Yes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? OYes L No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 R0 53 of 82 gACC nMST. M73538 b=r-o ri es MADEP VPH FORM A ueous Eyl Soil Sediment F Other ❑ G�oi aiiaers ' k, SatisfactorvFzl Broken Leakin uu's lr, seivaty s WA H<=2 H>2 m eraMg. Received on fce Received at 4 De .C Other Rec'd at 2.5 deg C NtefktaN y,_ WA Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(53) Lab ID: M73538-13 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71A3-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04A C5-C8 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 78 70-130% FID:2,5-Dibromotoluene % 75 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogata(s)and/or internal standards eluting in that range. C3C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes ❑ No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? OYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? L�No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 54 of 82 OAS M73538 =t=rotor e: � r MADEP VPH FORM Aclueous n Soil n Sediment I-1 Other n ortt�r r s Satisfactory Broken 71 Leakin ul?resvatt�res WA H<=2 H>2 e e 9 UR Received on Ice F1 Received at 4 De .C F1 Other .i Rec'd at 2.5 deg C A et:arrW WA Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-29(68) Lab ID: M73538-14 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/16/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ugA ND A 50 C5-C8 Aliphatics(Unadj.) N/A ugA 385' 50 C9-C12 Aliphatics(Unadj.) N/A ugA ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I 4 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugA 512 2 Toluene 108-88-3 C5-C8 ugA ND 2 Ethylbenzene 100-41-4 C9-C12 ugA ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 81 70-130% FID:2,5-Dibromotoluene % 77 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5.C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9.C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes i__1 No-Details Attatched Were all perform ance/acceptance standards for required QA/QC procedures achieved? WlYes ❑ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? V:I No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 B 55 of 82 OACC L11 EST. M73538 Lat orator cc MADEP VPH FORM Matrt' f � F t A ueous ICI Soil n Sediment Other f ='ontaIKMWM Satisfacto Broken n Leakin F t�%�a r ueousPr=esenratty N/A F DH<=2 H>2 ¢M 1eratul^e _ Received on Ice Received at 4 De .C Other Redd at 2.5 deg C Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-20(55) Lab ID: M73538-15 is Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/16/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND B 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 79 70-130% FID:2,5-Dibromotoluene % 75 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? I�lYes D. No-Details Attatched Were all performancelacceptance standards for required QA/QC procedures achieved? EVIYes D No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? W No ❑ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 Ell 56 of 82 GACCXJTEEM �M73538 I rlc: Accutest Laboratories Internal Sample Tracking Chronicle P. Shell Oil Job No: M73538 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes 7 3� � M73538-1 MADEP VPH REV 1.128-MAY-08 05:29 AP VMAVPH M73538-1 SW846 8260B 29-MAY-08 20:37 AA V82600XY5 M73538-2 MADEP VPH REV 1.128-MAY-08 06:12 AP VMAVPH M73538-2 SW846 8260B 29-MAY-08 21:04 AA V82600XY5 M73538-3 MADEP VPH REV 1.128-MAY-08 06:54 AP VMAVPH M73538-3 SW846 8260B 29-MAY-08 21:31 AA V82600XY5 M�3538CayIleeted 15����Y�Q8�1Q 40B�R�II�� Received��19 IVI�AY 08 zBy��'�. �� �,�� �°`` `t' M73538-4 MADEP VPH REV 1.128-MAY-08 07:37 AP VMAVPH M73538-4 SW846 8260B 29-MAY-08 21:58 AA V82600XY5 MV3U 538��Coli et d l MBA ��8 O�B�y�RD Receive r NhA�Y O$ B b M73538-5 MADEP VPH REV 1.128-MAY-08 08:19 AF VMAVPH M73538-5 SW846 8260B 29-MAY-08 15:04 EL V82600XY5 11+173538 6Cotlecteil15MAY08 11 45By RDA Received 19MAY 0$F°B " M73538-6 MADEP VPH REV 1.128-MAY-08 09:03 AF VMAVPH M73538-6 SW846 8260B 29-MAY-08 19:11 AMY V82600XY5 Mg735387 CbCieeted5 MA�YO$ 12 40 B RI} Rbceived19 MAYS 8` B+ � K µ.✓r :.,.a.:,a,.�.a ,,, .z.�e°' ., .o-.: ahY�...� ,�,,,^.:x.,.».F. -, �' ,...,.„s'°�',....Y,.3� z ,����` +t���e�. 'r a*. a&k.�..�,..,�xk 1m M73538-7 MADEP VPH REV 1.128-MAY-08 09:47 AF VMAVPH Page 1 of 3 ISTI 57 of 82 QACCtJTE97: M73538 T7 L-r-r--- Accutest Laboratories Internal Sample Tracking Chronicle P. Shell Oil Job No: M73538 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M73538-7 SW846 8260B 29-MAY-08 19:39 AMY V8260OXY5 M73538-8 MADEP VPH REV 1.128-MAY-08 10:31 AF VMAVPH M73538-8 SW846 8260B 29-MAY-08 20:07 AMY V8260OXY5 �� ) t M73538-9 MADEP VPH REV 1.128-MAY-08 11:16 AF VMAVPH M73538-9 SW846 8260B 29-MAY-08 20:35 AMY V8260OXY5 VI7353 10 �Collced 15Af&14t15�By Receluedr k9�MA 'z08 B�y �� ..�_._._..�� M73538-10 MADEP VPH REV 1.128-MAY-08 12:00 AF VMAVPH M73538-10 SW846 8260B 29-MAY-08 21:03 AMY V8260OXY5 h-,173*3�8 t1!1W 35 (53 � � M73538-11 MADEP VPH REV 1.128-MAY-08 12:44 AF VMAVPH M73538-11 SW846 8260B 29-MAY-08 14:05 AA V8260OXY5 �.,,..u... _.,......u&u_.i.m...._. ....a..-.�.�",'1 �i �'� i�''�s '��•' �. f x.Lx "� ",mac� .,awsA✓,..� Y,,...1,•'sT..�a sf,.�.�.. _. +;tt.'zb, .. -at M73538-12 MADEP VPH REV 1.128-MAY-08 13:29 AF VMAVPH M73538-12 SW846 8260B 29-MAY-08 14:32 AA V8260OXY5 Mx73Y538'13 CjL o lectEd15MA 08 2 By r Recelued 191UTAY 08'Bye g A,. „ .,,,..,a,�_ .,kn,.. s�xax�:. ,..,.,aa� � • ,d�.,»,r.,r ,:a t-s �r ��. a.+� �aT� .�=' M73538-13 MADEP VPH REV 1.128-MAY-08 14:13 AF VMAVPH M73538-13 SW846 8260B 29-MAY-08 16:53 AA V8260OXY5 Page 2 of 3 ®19 58 of 82 ®ACC TEST: M73538 La t or 3z—ie, Accutest Laboratories Internal Sample Tracking Chronicle P. Shell Oil Job No: M73538 Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes ---MIMM11, Page ^~ ^ = 3538 | | New England 12 �, Section 5 GC/r1VIS U,Qlatiles �,; QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ®O 60 of 82 MACCUTEST. M73538 lc t ora tors c= Method Blank Summary Page I of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3306-MB G81900.1) 1 05/29/08 EL n/a n/a MSG3306 cn The QC reported here applies to the following samples: Method: SW846 8260B M73538-5 CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND; 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether N _ 2.0 ug/1 75-65-0 Tert Butyl Alcohol N ? 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND - . 2.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 19,11%, 79-130% 2037-26-5 Toluene-D8 98% 80-120% 460-00-4 4-Bromofluorobenzene 100% 80-120% E] 61 of 82 ®ACC UTEST. M73538 L-tn 3-, ;,- Method Blank Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSP952-MB P28608.1) 1 05/29/08 AMY n/a n/a MSP952 v� The QC reported here applies to the following samples: Method: SW846 8260B M73538-6, M73538-7, M73538-8, M73538-9, M73538-10 CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether NIA 2.0 ug/1 1634-04-4 Methyl Ter(Butyl Ether ND 1.0 ug/l 994-05-8 tert-Amyl Methyl Ether 2.0 ug/1 75-65-0 Tert Butyl Alcohol NA 20 ug/l 637-92-3 tert-Butyl Ethyl Ether N:D 2.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 102% 79-130% 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene 109% 80-120% f � 62 of 82 12ACCME .. M73538 L=U=riz ,ie= Method Blank Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR188-MB R4910.1) 1 05/29/08 AA n/a n/a MSR188 The QC reported here applies to the following samples: Method: SW846 8260B M73538-1, M73538-2, M73538-3, M73538-4,M73538-11, M73538-12, M73538-13 CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 994-05-8 tert-Amyl Methyl Ether 5ND x' 2.0 ug/l 75-65-0 Tert Butyl Alcohol iND 20 ug/l 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/l CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 79-130% 2037-26-5 Toluene-D8 1Q % 80120% 460-00-4 4-Bromofluorobenzene 101% 80-120% ®® 63 of 82 ®ACCUTEST. M73538 Lib c ;u.�ec � 7 Method Blank Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3307-MB G81926.1) 1 05/29/08 EL n/a n/a MSG3307 cn The QC reported here applies to the following samples: Method: SW846 8260B M73538-14, M73538-15 CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND° 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 96% 79130% 2037-26-5 Toluene-D8 ° ° 460-00-4 4-Bromofluorobenzene 64 of 82 UACCUTEST. M73538 =Gcroco Ve: Method Blank Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3308-MB G81952.1) 1 05/30/08 EL n/a n/a MSG3308 CA The QC reported here applies to the following samples: Method: SW846 8260B M73538-14 CAS No. Compound Result RL Units Q 1634-04-4 Methyl Tert Butyl Ether Nl), 1.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 93% 79-130% 2037-26-5 Toluene-D8 99% 80120% 460-00-4 4-Bromofluorobenzene 97% 80-120% ..........................._...___ ®� 65 of 82 0ACCUTEEM M73538 =borco c= Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3306-BS G81898.D 1 05/29/08 EL n/a n/a MSG3306 MSG3306-BSD G81899.1) 1 05/29/08 EL n/a n/a MSG3306 cn iv The QC reported here applies to the following samples: Method: SW846 8260B M73538-5 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 50 0 A,00= 49.1 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 49.3 99 49.1 98 0 70 130/25 994-05-8 tert-Amyl Methyl Ether 50 50.7 "101 50.4 101 1 51 138/25 75-65-6 Tert Butyl Alcohol 500 490 '98 = 499 100 2 60 146/25 637-92-3 tert-Butyl Ethyl Ether 50 52.0 a04 51.6 103 1 w' 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 990 100°l0 " 79-130% 2037-26-5 Toluene-D8 9S°lo: 99%' 80-120% 460-00-4 4-Bromofluorobenzene 93% 939 80-120% i 66 of 82 MACCUTEST. M73538 let'o c cs Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSP952-BS P28605.1) 1 05/29/08 AMY n/a n/a MSP952 MSP952-BSD P28606.1) 1 05/29/08 AMY n/a n/a MSP952 IV NINE The QC reported here applies to the following samples: Method: SW846 8260B M73538-6, M73538-7, M73538-8, M73538-9, M73538-10 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/l % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 51.0 102 51.2 102, 0 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 50.0 1100 49.9 100 0. ,'': 70 130/25 994-05-8 tert-Amyl Methyl Ether 50 42.7 85 44.7 51-138/25 75-65-0 Tert Butyl Alcohol 500 531 106 517 103 3 x 60-146/25 637-92-3 tert-Butyl Ethyl Ether 50 44.5 89 45.3 91 2 46 147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 100% 102%. 79130% 2037-26-5 Toluene-D8 l0U% 1'00% 80-120% 460-00-4 4-Bromofluorobenzene 96% 96% 80120% ®B 67 of 82 ®ACCUTEST. M73538 21t="3 t or;cs i Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number. M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR188-BS R4908.D 1 05/29/08 AA n/a n/a MSR188 MSR188-BSD R4909.1) 1 05/29/08 AA n/a n/a MSR188 v, N The QC reported here applies to the following samples: Method: SW846 8260B M73538-1, M73538-2, M73538-3, M73538-4, M73538-11, M73538-12, M73538-13 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/1 % RPD Rec/RPD 108-20-.3 Di-Isopropyl ether 50 35.0 70 33.667PiIi. 4 r 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 56.5 113 53.6 107 5 70 130/25 994-05-8 tert-Amyl Methyl Ether 50 60.9 .122 57.0 114 , 7 51-138/25 75-65-0 Tert Butyl Alcohol 500 367 73 389 78 6 60-146/25 637-92-.3 tert-Butyl Ethyl Ether 50 47.8 96 45.6 91 5 46 147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868 53 7 Dibromofluoromethane 100% 98% 79-130% 2037-26-5 Toluene-D8 10 % 80-120% 460-00-4 4-Bromofluorobenzene 80120% �® 68 of 82 ®ACCUTEST. M73538 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3307-BS G81924.1) 1 05/29/08 EL n/a n/a MSG3307 MSG3307-BSD G81925.D 1 05/29/08 EL n/a n/a MSG3307 (n iv The QC reported here applies to the following samples: Method: SW846 8260B M73538-14, M73538-15 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/1 % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 48.7 `9Z ° ' 47.1 94, 3 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 49.0 98 47.5 95 3 70-130/25 994-05-8 tert-Amyl Methyl Ether 50 51.3 103 50.8 51 138/25 75-65-0 Tert Butyl Alcohol 500 504101 486 s7. 4, = 60-146/25 637-92-3 tert-Butyl Ethyl Ether 50 51.5 =103 50.0 DO!' 3. 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 8%-9$9/0 79-130% 2037-26-5 Toluene-D8 9. 99% 80-120% 460-00-4 4-Bromofluorobenzene 93% 92% 80-120% 69 of 82 12ACCU TEST. M73538 t ztoln tofiec Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3308-BS G81949.1) 1 05/30/08 EL n/a n/a MSG3308 MSG3308-BSD G81950.1) 1 05/30/08 EL n/a n/a MSG3308 N The QC reported here applies to the following samples: Method: SW846 8260B M73538-14 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/1 % ug/1 % RPD Rec/RPD 1634-04-4 Methyl Tert Butyl Ether 50 47.4 x 95 46.3 93 2 70 130/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 90 96% 79130% 2037-26-5 Toluene-D8 100% 99% 80-120% 460-00-4 4-Bromofluorobenzene 92% 92% 80-120% ® 70 of 82 12ACCUTEST. M73538 =bo- t� icc Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73491-21MS G81921.1) 1 05/29/08 EL n/a n/a MSG3306 M73491-21MSDG81922.D 1 05/29/08 EL n/a n/a MSG3306 M73491-21 G81919.1) 1 05/29/08 EL n/a n/a MSG3306 w The QC reported here applies to the following samples: Method: SW846 8260B M73538-5 M73491-21 Spike MS MS MSD MSD Limits CAS No. Compound ug/I Q ug/l ug/I % ug/I % RPD Rec/RPD 108-20-3 Di-Isopropyl ether ND 50 52.7 0MV601,111 50 3 06IIIEnUE p54-155/30 1634-04-4 Methyl Tert Butyl Ether ND 50 48.9 9�8 48 7 �,W7 U 54-144/30 994-05-8 tert-Amyl Methyl Ether ND 50 49.499; 50.1 1 47-142/30 75 65 0 Tert Butyl Alcohol ND 500 486 97 494 99 2 60-148/30 637-92-3 tert-Butyl Ethyl Ether ND 50 52.5 $105 51.4 1'03 2 46 151/30 CAS No. Surrogate Recoveries MS MSD M73491-21 Limits 1868-53-7 Dibromofluoromethane 104% 101% 104% 79-130% 2037 26 5 Toluene-D8 98°l0 ' 98% 990YC. 80-120% 460-00-4 4-Bromofluorobenzene 94% 939Yc 101% 80-120% I ®® 71 of 82 UACCLffEST. M73538 L=torat-1es L i Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73513-5MS P28628.1) 5 05/29/08 AMY n/a n/a MSP952 M73513-5MSD P28629.1) 5 05/29/08 AMY n/a n/a MSP952 M73513-5 P28615.1) 1 05/29/08 AMY n/a n/a MSP952 w The QC reported here applies to the following samples: Method: SW846 8260B M73538-6, M73538-7, M73538-8, M73538-9, M73538-10 M73513-5 Spike MS MS MSD MSD Limits CAS No. Compound ug/l Q ug/l ug/1 % ug/l % RPD Rec/RPD 108-20-3 Di-Isopropyl ether ND 250 295 131i` 289 116 .2 54-155/30 1634-04-4 Methyl Tert Butyl Ether 1.1 250 245 98 3' 24698 . U '. 54-144/30 994-05-8 tert-Amyl Methyl Ether ND 250 164 66 167 2 47-142/30 75-65 0 Tert Butyl Alcohol ND 2500 2820 1I3 2870 1';15 60-148/30 637-92-3 tert-Butyl Ethyl Ether ND 250 212 V85' ; 209 84 a.... 46-151/30 CAS No. Surrogate Recoveries MS MSD M73513-5 Limits 1868-53-7 Dibromofluoromethane -105% I00% 79130% 2037 26 5 Toluene D8 102% 1039/c,: 1009/0 80 120% 460-00-4 4-Bromofluorobenzene 91% 93% 95% 80-120% ®� 72 of 82 ®A M73538 -=t orcories Matrix Spike/Matrix Spike Duplicate Summary Page I of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73577-2MS G81945.1) 5 05/30/08 EL n/a n/a MSG3307 M73577-2MSD G81946.1) 5 05/30/08 EL n/a n/a MSG3307 M73577-2 G81939.1) 1 05/30/08 EL n/a n/a MSG3307 w The QC reported here applies to the following samples: Method: SW846 8260B M73538-14, M73538-15 M73577-2 Spike MS MS MSD MSD Limits CAS No. Compound ug/1 Q ug/1 ug/1 % ug/I % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 0.48 250 23795; 227 9I 4 54-155/30 1634-04-4 Methyl Tert Butyl Ether 531 E 250 827 118 �,. 805 �°LIO 3 54-144/30 994-05-8 tert-Amyl Methyl Ether 1.2 250 254 10 2478 3 47-142/30 75-65-0 Tert Butyl Alcohol 2490 2500 4860 95 4750 90 2 60-148/30 637-92-3 tert-Butyl Ethyl Ether 1.4 250 253 I01 246 98 3 46 151/30 CAS No. Surrogate Recoveries MS MSD M73577-2 Limits 1868-53-7 Dibromofluoromethane 97% 96% '95% 79130% 2037-26-5 Toluene-D8 98% 80 1200YO 460 00-4 4 Bromofluorobenzene 91% 93/ 98% 80 1Z0% i ®B 73 of 82 QACCUTEST. M73538 Lato,�to,tt, 9. D Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project:: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73586-6MS G81965.1) 5 05/30/08 EL n/a n/a MSG3308 M73586-6MSD G81966.1) 5 05/30/08 EL n/a n/a MSG3308 M73586-6 G81964.1) 1 05/30/08 EL n/a n/a MSG3308 w The QC reported here applies to the following samples: Method: SW846 8260B M73538-14 M73586-6 Spike MS MS MSD MSD Limits CAS No. Compound ug/l Q ug/l ug/1 % ug/1 % RPD Rec/RPD 1634-04-4 Methyl Tert Butyl Ether 5.3 250 246 96 30� 241 94 2 54-144/30 CAS No. Surrogate Recoveries MS MSD M73586-6 Limits 1868-53-7 Dibromofluoromethane 101% 99% ' 99% 79 130% 2037 26-5 Toluene-D8 I00% <979 _ 80 120% 460-00-4 4-Bromofluorobenzene 94% 93% 01% 80 120% 74 of 82 M73538 lab orto r{c: Volatile Surrogate Recovery Summary Page 1 of 2 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: SW846 8260B Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 S2 S3 M73538-1 R4922.D 9`9 0 101.0 10I0 M73538-2 R4923.D 8 0 _ 103.0 1020 M73538-3 R4924.1) & 0 101.0 LtII 0 M73538-4 R4925.1) 104.0 1�010 M73538-5 G81910.1) 1.43`0 95.0 I01 0 M73538-6 P28623.D 1:011) 103.0 101'0 M73538-7 P28624.1) .a5 0 100.01"O�,A M73538-8 P28625.1) b5�0 99.0 102,0 M73538-9 P28626.1) 1(}50 101.0 1000 M73538-10 P28627.1) 0 100.0 98 0 M73538-11 R4911.D 119,6 ff 100.0 1010 M73538-12 R4912.1) =9S 0 103.0 102,'0 M73538-13 R4914.1) 97 0 105.0 1020 M73538-14 G81956.1) $fi 0 98.0 96 0}, M73538-14 G81927.1) 96 0 97.0 96 0'i M73538-15 G81928.1) 9 0 95.0 97,0 M73491-21MS G81921.1) 184 0 98.0 94 0" M73491-21MSD G81922.1) 4, 0 98.0 M73513-5MS P28628.1) 105 0 102.0 9I Q' M73513-5MSD P28629.1) 103 0 103.0 93 0! M73577-2MS G81945.D 97.0 100.0 91.0 M73577-2MSD G81946.1) 9&0 99.0 93:0 M73586-6MS G81965.1) 131.0 100.0 M73586-6MSD G81966.D 99A 99.0 93.6. MSG3306-BS G81898.D 99 0 98.0 93 0 MSG3306-BSD G81899.1) 100.0 99.0 93.0 MSG3306-MB G81900.1) 99,0 98.0 100:0 MSG3307 BS G81924.1) 98 0 98.0 9,3:0' MSG3307-BSD G81925.1) 9$.0 99.0 92.6 MSG3307 MB G81926.1) 96.0 99.0 97.:0'i, MSG3308-BS G81949.1) 96:0 100.0 92 0; , MSG3308-BSD G81950.1) 96 0 99.0 MSG3308-MB G81952.1) 910 99.0 97:0' MSP952-BS P28605.1) 1,00 0 100.0 96.0 , MSP952-BSD P28606.1) 102 0 100.0 MSP952-MB P28608.1) 102 0 99.0 104.;0 MSR188-BS R4908.D AD:0 103.0 101 0 MSR188-BSD R4909.D 98 0 104.0 102 0 MSR188-MB R4910.1) 97.0 103.0 101."0 ®� 75 of 82 MACCLffEST M73538 L.bor ;orici i Volatile Surrogate Recovery Summary Page 2 of 2 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: SW846 8260B Matrix: AQ Samples and QC shown here apply to the above method w Surrogate Recovery Compounds Limits Surrogate Recovery Compounds Limits S1 = Dibromofluoromethane S2 = Toluene-D8 S3 — 4-Bromofluorobenzene &Tl 120°fog, �® 76 of 82 ®ACCU'TEST. M73538 -to: ;orles �® New England ACCUTEST. Section 6 GC `Folatiles, .��. QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries ®B 77 of 82 IN A = TTEST. M73538 � t--- I n Method Blank Summary Page 1 of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2377-MB AB42642.1) 1 05/27/08 AP n/a n/a GAB2377 o� The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 =• M73538-1, M73538-2, M73538-3, M73538-4 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND'& Ai 2.0 ug/1 100-41-4 Ethylbenzene ND" 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND' 2.0 ug/1 91-20-c: Naphthalene ND 3.0 ug/1 108-88-3 Toluene Nl 2.0 ug/1 m,p-Xylene ND' 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9- C10 Aromatics (Unadj.) ND..". 50 ug/1 C5- C8 Aliphatics ND` 50 ug/I C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate g Recoveries Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene 859/cv 70-130% ®B 78 of 82 MACCU TEST. M73538 =boraturics Method Blank Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sampi±e File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GWX1970-MB WX41550.1) 1 05/28/08 AF n/a n/a GWX1970 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M73538-5, M73538-6, M73538-7, M73538-8, M73538-9, M73538-10, M73538-11, M73538-12, M73538-13, M73538- • 14, M73538-15 CAS No. Compound P Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether NIT 2.0 ug/1 91-20-.3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene NI3 2.0 ug/l m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND., 50 ug/1 C9- C12 Aliphatics (Unadj.) ND„ 50 ug/1 C9- C10 Aromatics (Unadj ) ND. 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 79 70130% 615-59-8 2,5-Dibromotoluene 85% 70-130% 0 ®� 79 of 82 ®ACCMEST. M73538 La to"nco ri cs Y Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2377-BSP AB42643.13 1 05/27/08 AP n/a n/a GAB2377 GAB2377-BSD AB42644.1) 1 05/27/08 AP n/a n/a GAB2377 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M735',38-1, M73538-2, M73538-3, M73538-4 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/1 % RPD Rec/RPD 71-43-2 Benzene 50 55.2 11'0 53.0 R1601Z Y 4 70-130/25 100-41-4 Ethylbenzene 50 56.8 114` 54.3 109 5 70 130/25 1634-04-4 Methyl Tert Butyl Ether 50 53.2 106 51.9 104 2 70-130/25 91 20-.3 Naphthalene 50 50.5 `101 47.9 96 5 70 130/25 108-88-3 Toluene 50 53.8 51.5 1`03 4 70-130/25 m,p-Xylene 100 110 110 106 106 4 70 130/25 95-47-6 o-Xylene 50 53.9 .108 51.5 103 5 70 130/25 C5 C8 Aliphatics (Unadj.) 150 123 82 119 79 3 70 130/25 C9- C12 Aliphatics (Unadj.) 150 118 79 127 85 7 70 130/25 C9- C10 Aromatics (Unadj.) 50 56.8 114 54.2 1308 5 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 70-130% 615 59-8 2,5 Dibromotoluene 97% 91% 70-130% 80 of 82 U ACCUTEST. M73538 Calera;urles i Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GWX1970-BSP WX41551.1) 1 05/28/08 AF n/a n/a GWX1970 GWX1970-BSD WX41552.1) 1 05/28/08 AF n/a n/a GWX1970 as The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M73538-5, M73538-6, M73538-7, M73538-8, M73538-9, M73538-10, M73538-11, M73538-12, M73538-13, M73538- • 14, M73538-15 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/1 % RPD Rec/RPD 71-43-2 Benzene 50 52.1 204 52.6 105 I ~" 70-130/25 100-41-4 Ethylbenzene 50 49.6 99 49.9 100 1, 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 49.8 *100 50.2 100 1 70 130/25 91-20-3 Naphthalene 50 53.5 �107 ' 53.6 107 0 �'� 70-130/25 108-88-3 Toluene 50 51.5 A03 , 51.9 1041. 1° 70 130/25 m,p-Xylene 100 10110 101 101 0 70-130/25 95-47-6 o-Xylene 50 47.6 95 ; 47.8 70-130/25 C5-C8 Aliphatics (Unadj.) 150 149 ��9, " ' 152 10 2 �i 70-130/25 C9- C12 Aliphatics (Unadj.) 150 139 93 ' 141 94. I 70-130/25 C9- C10 Aromatics (Unadj.) 50 45 90 45 91 1 70-I30/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene81°0 81%, 70-130% 615-59-8 2,5-Dibromotoluene $8% 88% 70-130% ®� 81 of 82 ®ACCLJ' EST. M73538 - c .•.,c o r;,. Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a S1 b w M73538-1 AB42661.1) 76 0 85.0 M73538-2 AB42662.D 76 0 86.0 M73538-3 AB42663.D 87.0 M73538-4 AB42664.1) T9 0 88.0 M73538-5 WX41554.D 1810 86.0 M73538-6 WX41555.D 80 0 83.0 M73538-7 WX41556.1) 84.0 Y Y M73538-8 WX41557.1) 79 0 '82.0 M73538-9 WX41558.D 78A..iN - 80.0 M73538-10 WX41559.1) 79 0 83.0 M73538-11 WX41560.1) 7t 0 77.0 M73538-12 WX41561.1) 73 0 76.0 M73538-13 WX41562.1) 115, 5 ` _F.' 78.0 ........................._. . M73538-14 WX41563.D 77 0 81.0 M73538-15 WX41564.1) 7'S 0 79.0 GAB2377-BSD AB42644.1) -8°1.0 91.0 GAB2377-BSP AB42643.D 86 0 97.0 ................_.. ....._.......... ... .._ GAB2377-MB AB42642.D 77 0. _ 85.0 GWX1970-BSD WX41552.1) 810 88.0 GWX1970-BSP WX41551.D 88.0 GWX1970-MB WX41550.1) 79 0 85.0 Surrogate Recovery Compounds Limits S1 = 2,5-Dibromotoluene 70 13,0% (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 82 of 82 12AC.CU TEST. M73538 L-b ot]to ri*G rj s SOVEKEIGN CONSULTING INC . September 25,2008 DHL#29116771655 Town of Hyannis Town Engineer 367 Main Street Hyannis, Massachusetts 02601 Re: Groundwater Sampling Results,August 2008 In the Vicinity of: Former Texaco Service Station 1140 Iyannough Road RTN 4-11301 To Whom it May Concern; Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted.for laboratory analysis of volatile petroleum hydrocarbons (VPH). As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVE IV CONSULTING,INC. J so Sherburne Project Manager i cc: Mr.David Weeks,Motiva g MassDEP-SERO Sovereign File.-EQ711 O :ts � c�> ,1` W W rn//ram� 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan r` BWSC 123 This Notice is Related to Release Tracking Number 4a 11301 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Hyannis, Town Engineer 2. Street Address: 367 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ✓❑ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ✓❑3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater) to the extent known at the time of this notice. Groundwater from monitoring wells E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne Street Address: 905E South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508) 339-3200 Email: Sherburne@sovcon.com NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at hftp://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass..qov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. Automated Report New England a . ... n 09/02/08 Technical Report for Shell Oil y K SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ` 4 EQ 711 Accutest Job Number: M76363 " Sampling Date: 08/18/08 Report to: Sovereign Consulting Inc. jsherburne@sovcon.com ATTN: Jason Sherburne Total number of pages in report: 55 ,p AC Cp 0 u Test results contained within this data package meet the requirements eezaZnd of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) Q R $ NY(11791) NJ'(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. New England 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • http://www.accutest.com 1 of 55 IJST M76363 Table of Contents Sections: -1- Section1: Sample Summary ................................................................................................... 3 Section2: Case Narrative/Conformance Summary .............................................................. 5 Section3: Sample Results ........................................................................................................ 6 3.1: M76363-1: MW-21 (55) ............................................................................................... 7 3.2: M76363-2: MW-24 (42) ............................................................................................... 8 3.3: M76363-3: MW-26 (72) ............................................................................................... 9 3.4: M76363-4: MW-19 (5 5) ............................................................................................... 10 3.5: M76363-5: MW-20 (55) ............................................................................................... 11 3.6: M76363-6: MW-29 (68) ............................................................................................... 12 3.7: M76363-7: MW-32 (55) ............................................................................................... 13 3.8: M76363-8: MW-35 (53) ............................................................................................... 14 3.9: M76363-9: MW-37 (53) ............................................................................................... 15 3.10: M76363-10: MW-37 (90) ........................................................................................... 16 3.11: M76363-1 l: MW-37 (105) ......................................................................................... 17 3.12: M76363-12: MW-39 (88) ........................................................................................... 18 3.13: M76363-13: MW-40 (85) ........................................................................................... 19 3.14: M76363-14: MW-38 (104) ......................................................................................... 20 3.15: M76363-15: MW-38 (89) ........................................................................................... 21 3.16: M76363-16: RW-101 .................................................................................................. 22 3.17: M76363-17: RW-102 .................................................................................................. 23 3.18: M76363-18: MW-25 (72) ........................................................................................... 24 Section4: Misc. Forms ............................................................................................................ 25 4.1: Chain of Custody ........................................................................................................... 26 4.2: MCP Form ..................................................................................................................... 28 4.3: VPH Form ...................................................................................................................... 29 4.4: Sample Tracking Chronicle ........................................................................................... 47 Section5: GC Volatiles - QC Data Summaries ..................................................................... 50 5.1: Method Blank Summary ................................................................................................ 51 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 53 5.3: Surrogate Recovery Summaries ..................................................................................... 55 Q 2of55 M76363 Accutest Laboratories Sample Summary Shell Oil Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample YCollected,;' Matrix Client Number Date Time By Received Code Type Sample ID M76363�1' 08/18/08 10:30 AW 08/20/08 AQ Ground Water MW 21 (6' w M76363 2_ <08/18/08 10:55 AW 08/20/08 AQ Ground Water 1VIW-24�M) M76363 '. 08/18/08 10:10 AW 08/20/08 AQ Ground Water MW M763634 08/18/08 09:30 AW 08/20/08 AQ Ground Water N W 19 (55) M76363-5 08/18/08 13:35 AW 08/20/08 AQ Ground Water 11IW-20 (55) M76363 6 08/18/08 14:00 AW 08/20/08 AQ Ground Water MW-29 (68) M76363-7 08/18/08 13:15 AW 08/20/08 AQ Ground Water MW.-32 (55) M76363-8 08/18/08 12:45 AW 08/20/08 AQ Ground Water MW 35 (53) M76363 9 08/18/08 11:00 AW 08/20/08 AQ Ground Water M'W-37 (53) M76363-10 08/18/08 11:50 AW 08/20/08 AQ Ground Water MW-37 (90) M76363 11 08/18/08 12:15 AW 08/20/08 AQ Ground Water MW=37 405) M76363 12' 08/18/08 12:20 AW 08/20/08 AQ Ground Water 1VIW=39 (88) M76363-1.3 08/18/08 11:55 AW 08/20/08 AQ Ground Water MW 40 (85) 3of55 AMU'irEST M76363 .. .... :: ,> Accutest Laboratories Sample Summary (continued) Shell Oil Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Cgllected Matrix Client Number Date Time By Received Code Type Sample ID M76363 14 a 08/18/08 12:55 AW 08/20/08 AQ Ground Water MW„38 (104) IVI76363 1 08/18/08 13:30 AW 08/20/08 AQ Ground Water MW 38 (89) M76363 1G 08/18/08 09:40 AW 08/20/08 AQ Ground Water kw,461 M76363 1 :,,:08/18/08 11:20 AW 08/20/08 AQ Ground Water RW 102 M76363-1:8 08/18/08 10:30 AW 08/20/08 AQ Ground Water MW45 (72) I 4 of 55 A=U EST. M76363 _____._....._.........._.................._..._________.._..._.. SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M76363 Site: SCMAW:97346878(REIMBMA) 1140 lyannough Road Hyannis MA Report Date 9/1/2008 1:46:16 PM 18 Sample(s)were collected on 08/18/2008 and were received at Accutest on 08/20/2008 properly preserved,at 2 Deg.C and intact. These Samples received an Accutest job number of M76363.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GBD990 ® All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GBD991 ® All samples were analyzed within the recommended method holding time. All method blanks for this batch meet method specific criteria. The Accutest Laboratories of New England ce rtifies erttfies that all analysis were performed within method specification. It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M76363). I Monday,September01,2008 Page 1 of 1 arl 5 of 55 ACCUT EST. M76363 i .......,.,,.. ; - New England Section { Sample Results Report of Analysis 6 of 55 U'iEB .._.......... .................... Accutest Laboratories Report of Analysis Page 1 of 1 ; Client Sample ID: MW-24 (42) Lab Sample ID: M76363-2 Date Sampled:. 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20860.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND::-: 2.0 ug/1 m,p-Xylene ND = 2.0 ug/l 95-47-6 o-Xylene 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) N"D" 50 ug/1 C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics N`D 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 805/0 70-130% 615-59-8 2,5-Dibromotoluene 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Ma 8 of 55 __............................. M76363 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-26 (72) Lab Sample ID: M76363-3 Date Sampled: 08/18/08 F Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20861.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND -: 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether NI) 2.0 ug/1 91-20-3 Naphthalene Np 3.0 ug/1 108-88-3 Toluene ND " 2.0 ug/I m,p-Xylene ND '; 2.0 ug/1 95-47-6 o-Xylene ND. ` 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND.::: 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) NO !, 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics NO 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 72%; 70-130% 615-59-8 2,5-Dibromotoluene 80%% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound BE2 9 of 55 faACCUTEST. M76363 .. _......,.._, Accutest Laboratories w Report of Analysis Page 1 of 1 , Client Sample ID: MW-39 (88) Lab Sample ID: M76363-12 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20870.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene NI 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether NO: 2.0 ug/I 91-20-3 Naphthalene NO 3.0 ug/I 108-88-3 Toluene ND; 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene NO 2.0 ug/1 C5- C8 Aliphatics (Unadj.) NO 50 ug/l C9- C12 Aliphatics (Unadj.) NO. 50 ug/1 C9- C10 Aromatics (Unadj.) ND ' 50 ug/l C5- C8 Aliphatics NO 50 ug/l C9- C12 Aliphatics NO 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 82% 70-130% 615-59-8 2,5-Dibromotoluene 91% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound EJEJ 18 of 55 6J'T7l=S'i' M76363 s........:; ,> .;,. Accutest Laboratories Report of Analysis Page 1 of 1 , Client Sample ID: MW-40 (85) Lab Sample ID: M76363-13 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20871.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND <: 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene N1). 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND` 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 83% 70-130% 615-59-8 2,5-Dibromotoluene 93%.. 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound EMEJ 19 of 55 AlU M76363 ....> , :• Accutest Laboratories P Report of Analysis Page 1 of I Client Sample ID: MW-38 (104) Lab Sample ID: M76363-14 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20880.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene AND "' 2.0 ug/I 100-41-4 Ethylbenzene ND:'-.:,!: 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND" 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND " 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND _ 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene70130% 615-59-8 2,5-Dibromotoluene 90%: 70130% ............ .. . . ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 20 of 55 UTEST. .............................. ... M76363 Accutest Laboratories 4� Report of Analysis Page 1 of 1 Client Sample ID: MW-38 (89) Lab Sample ID: M76363-15 Date Sampled: 08/18/08 Matrix: AQ- Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20881.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene N1Y 2.0 ug/1 95-47 6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) N0z 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/t C9- C10 Aromatics (Unadj.) ND: 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% 615-59-8 2,5-Dibromotoluene 90% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME] 21 of 55 ACCUT EST. M76363 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-25 (72) Lab Sample ID: M76363-18 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 BD20884.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND . 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 14 3 ............:. 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND,' 2.0 ug/1 95-47-6 o-Xylene Np 2.0 ug/1 C5- C8 Aliphatics (Unadj.) NO 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ...... ...... . . 615-59-8 2,5-Dibromotoluene 81°fo 70-130% 615-59-8 2,5-Dibromotoluene 92% .-- 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MEJ 24 of 55 12ACCUTEST M76363 c F New England .40 IRACCUTEST. Section 4 A,s,E:,,.7 Sa T Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle Q 25 of 55 M76363 ..........,.>. I • LAB(LOCATION) Q Shell Oil Products Chain Of Custody Record 'Please Check:. ro Plate l3oi(: --:-::FAhl BAI}`c:GbnfaclNel :.111.IDE T..S:IENV.6ERVtCES):;.OaEacvrrot DENT AvauEs ❑ENV SFRVRES ❑NOTNA RETAp O A ELL RET t.. .. O 1� OCR (]ACCUIEST Dave Weeks 9 6 9 2 5 012 $ DATE: E ❑RaTnA soeEN pconwETuar ❑weFs Pi7:p.: SAP.d ❑OTHER t _ ❑SHELL RIPE;iNF ❑OTHER PAGE: I OI _ 1 0 0 0 8 3 cw....,m...... .OeaEss I•e..a eM�uuy� Sovereign Consulting Inc 1140 I annou h Road,Hyannis,MA 905E.South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Report to):Jason Sherburne CONSULTANT PROJECT NO.:EQ711 A _ Mansfield,MA 02048 �^ API n L1eosEDR✓::: 508.339.3200 508.339.3248 )sherburne(DDscvcon.com j— A/q , M j 2 ter;d 1.7 TURNAROUND TA (C MOAR DAYS): O STANDARD(14MY) ❑swos ❑Twos ❑2DAYS 024I REQUESTED ANALYSIS DEENERAELES: ❑ET— ❑CONNB l7l C ORCF O OTHER(SPF(]FY) TEI.PERATUREONRECEF C' Cmin Fr (Codbpl ;Cooinu SPECIAL INSTRUCTIONS OR NOTES: SAMPLING EAYAmF Field Sample Identification +?E:.- DATE TIME a CCnILabo to HoWs s ::rypg; Hrm xssa rwn � Or laDoralory Nofes mu- 10Jv C u • f ,terI I—FTT--f+ a, sz S7tY !. U yap IAl S3' x, ",v -3y s Ilob l U- 1 1q Via,. �M1 Ri Mlcm+�•1 "°°M.f�m•• Rae..0 M fBb�nvq Pyv M76363: Chain of Custody Page 1 of 2 26 of 55 AG'Cl.TEES .. ..... . f LAS(LOCATION) Q Shell Oil Products Chain Of Custody Record Please Cheek:AP bapA lellimc..... Pnnt gift.To Contact Name ., �:�iN�l0ENT 8a MI�6ERVlCE$j:�:pwLCK 1E NOw DEra a APPLIES .. .. l7Accuresr ❑ErN seancEs ❑aronvARETUL ❑SMELIRETALL Dave Weeks 9 6 9 1 2 5 0 2 8 DATE: �T ❑MDTnAwaa D+mNwLTANr OweEs PO�.: - 8Ap71 a ❑—ERI ) ❑ENEU GIRIV,E C]Onca - - PAGE: 02 1 0 0 0 8 3 Sovereign Consulting Inc an1140 I annou h Road,Hyannis,MA 905E South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Report to):Jason SherOurne CONSULTANT PROJECT NO.:EQ711 A _ Mansfield,MA 02048 508.339.3200 508.339.3248 IsherburneRsovcon.com TURNAROUND Tam ICALENOAR D4 a): \ �sT.NDneD(14 MY) ❑5-IS ❑3Mre E)2 Mrs ❑NHOURS REQUESTED ANALYSIS DELNEiUKM ❑OOMMA 0:21aIMs OMrr ❑RCP ❑OTHER(SPEOFY) TEMPEMTUREONRECEd C' CWIWOI ICeub 02 iCoslIXp SPECIAL INSTRUCTIONS OR NOTES: SAMPLING Field Sample Identification wrlml ar = Container PlD Readings ' DATE nME n. aLaberomry Nales ::anr: R2a2 rasa mnEA /) ({-o b s iC tl SsCU 3V &"1 1330 W - )0[ 614.e S IDYL "v.cn�a.0 1 w 1 ey.lao�++el Dse. .. UqL Ad M76363: Chain of Custody Page 2 of 2 27 of 55 t.lTEST ............................................ M76363 Massachusetts Department BWSC-CAM Exhibit VI I A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 Title: MADEP MCP Response Action Analytical Report Certification Form �ffilllftl'02 Laboratory Name: Accutest Laboratories of New England Project#: M76363 Project Location: SCMAW:97346878(REIMBMA) 1140 lyannough Road MADEP RTN None Hyannis MA This form provides certifications for the following data set: M76363-1,M76363-1 0,M76363-1 1,M76363-12,M76363-13,M76363-14,M76363-15,M76363-16 M76363-17,M76363-18,M76363-2,M76363-3,M76363-4,M76363-5,M76363-6,M76363-7 M76363-8,M76363-9 Sample Matrices: Groundwater X Soil/Sediment Drinking Water Other: 8260B 8151A 8330 60106 0 7470A/1A 8270C 8081 A VPHJX) 6020 9014M 2 -L 8082 8021 B EPH 7000 S3 7196A s,Refe is& Analytical Methods I'M P� M 2- SW-84� 3,,S--, W84 An affirmative response to questions A, B, C,and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with Yes L1 No that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this-eport followed,including the requirement to note and 21 Yes ❑ No discuss in a narrative QC data that did not meet appropriate performance Istandards or guidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty",as described in Section 2.0(a),(b), (c)and El Yes ❑No (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without El Yes [I No significant imodifications,as specified in Section 11.3? A response to questions E and F below is required for"Presumptive Certainty" status E Were all QC performance standards and recommendations for the U, Yes [I No specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified 121 Yes U No method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. 'the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information,the material contained in this analytical report is,to the best of my knowledge and belief, accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 09/01/2008 28 of 55 13ACCLffEST. M76363 MADEP n VPH FORM Matr „ A ueous Soil _ Sediment �r; Other I Containers h Satisfactor ✓ Broken F1 Leakin 1 A ueous,Peserva>¢ues N/A 1_1 oH <= 2 PH > 2 Received on Ice n Received at 4 Deg. C 1-1 Other [;' Rec'd at 2.0 Deg.C Methanol , N/A p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-24(42) Lab ID: M76363-2 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/1 ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugh ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 87 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. c Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C 12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ✓'Yes _ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 4 Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ��No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 OEJ 30 of 55 FgACCUTEST. M76363 _ MADEP VPH FORM IUlarx,, .,y . .,fir.. A ueous �i Soil Sediment I Other Contafners.,j Satisfactor 'mil Broken i Leakinci A. ueous."Press% trues N/A ! PH <= 2 H > 2 T.er11='eFiure Received on Ice Received at 4 Deg. C F_i Other ( ' Rec'd at 2.0 Deg.C Mthanvk .. N/A ? Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-26(72) Lab ID: M76363-3 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics�(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND 50 Target Anal, es Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 72 70-130% PID:2,5-Dibromotoluene % 80 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-Cl 2 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes !..: No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? I�!Yes I__l No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? L16No _ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 Mffl 31 of 55 A .. U M76363 MADEP VPH FORM Aqueous LVl Soil 17, Sediment FI Other fi% Y' Satisfactor k.-I Broken F1 Leaking F, A iieous1 Pf,eseruat yes N/A F , pH <= 2 -, H > 2 F—' Tern'>eratures. Received on Ice i� Received at 4 De . C i Other i✓1 Rec'd at 2.0 Deg.C Metfianoj� r � _ N/A P. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-39(88) Lab ID: M76363-12 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CA's# Elution Range Units Result RDL 4 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/1 ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND c 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 91 70-130% FID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-Cl 2 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Y qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes ❑ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? i�!No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 40 of 55ACCUTEBT M76363 > ' MADEP VPH FORM M Aqueous vi Soil i Sediment Other 11 h Satisfactor Broken Leaking I C®.ntarners : A ueousPrservfRues N/A r H <= 2 pH > 2 'T Rec'd at 2.0 De C Received on Ice i Received at 4 Deg. C f '� Other �� g Methanol a N/A {' Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-40(85) Lab ID: M76363-13 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dit:romotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target AnalAes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND B 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 93 70-130% FID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WIYes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? LINO !_ Yes-Details Attatched I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 41 of 55 ACCU TEST. M76363 MADEP VPH FORM Matti Aqueous �i Soil Sediment r! Other FI Coraiatners Satisfactory I✓i Broken C i Leaking Fi Ab,ueous Preservatives: N/A FEI oH <= 2 pH > 2 E Tem el`ature &` Received on Ice Received at 4 Deg. C 11 Other '�, Rec'd at 2.0 Deg.C Mfkanol 1 . N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-38(104) Lab ID: M76363-14 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: . First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL 4 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target AnalAes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 7143-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ug/I ND' 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 90 70-130% FID:2,5-Dibromotoluene % 81 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-Cl 2 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? LaVIYes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ✓/Yes '.. No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ivil No '_. Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 Ma 42 of 55 A UTES'T. M76363 a MADEP VPH FORM Of Aqueous ✓I Soil Sediment ! Other C.oifalnersk m._ s-.'.. Satisfactor Imo! Broken 1 Leakin 1 A�ausPrese atvs N/A H <= 2 PH > 2 Tem era ur � Received on Ice Received at 4 Deg. C 1 Other ✓ Rec'd at 2.0 Deg.C N/A ? Methanol ��.� af�: Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-38(89) Lab ID: M76363-15 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL 4 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 7143-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Etf,er 1634-04-4 C5-C8 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 90 70-130 FID:2,5-Dibrorriotoluene % 81 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Aralytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? i��Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? i—,!'Yes E.! No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WO�1'1\10 _! Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 ME2 43 of 55 ACCU EBT. M76363 s Iten e•. r MADEP VPH FORM Mat`r -' Aqueous Soil L' Sediment Other Contaliners� �; Satisfactor ✓ Broken F1 Leaking A `ueyOtas Pre5eruatives N/A FJ H <= 2 H > 2 FI T�rrty.e`,tafure � �� Received on Ice p Received at 4 Deg. C r 1. Other Ftj Rec'd at 2.0 Deg.C Meth N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-25(72) Lab ID: M76363-18 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL g C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 14.3 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 10041-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Ranqe FID:2,5-Dibromotoluene % 81 70-130 PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)andlor internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. c Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? W'Yes '__ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 111011 Yes ! No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? ✓No !_._`. Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Postition Laboratory Director Signature Printed Name Reza Tand Date 9/1/2008 EMEJ 46 of 55 J4MU'P>E8 - M76363 ....... f Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M763 -3 1' Collected I$AUG 0810 30 B AW �R�eceiu d O AU 08 B M76363-1 MADEP VPH REV 1.127-AUG-08 01:19 AF VMAVPH 1UI76363 2 Collecte���18At�G-�08�10 55 ByAW� Re�ceived 20 A&UG 08 By � �� � �4 vgs� % MW?4 M76363-2 MADEP VPH REV 1.127-AUG-08 02:00 AF VMAVPH M76363 3 Collected 18 AU08 1010 ByAW Reued:20 AUG 08 Bye i r s b M76363-3 MADEP VPH REV 1.127-AUG-08 02:42 AF VMAVPH N176363 h4 y Collected f18AUG 08 09 30 By AWReceived 20AUG 08��y ��,�� � � �� M76363-4 MADEP VPH REV 1.127-AUG-08 03:23 AF VMAVPH M76363 5; Collected 18 AUG'08 13 35 By AW �Received 20 AUG 08a By , ' MNV 20 (5.5) _.... M76363-5 MADEP VPH REV 1.127-AUG-08 04:04 AF VMAVPH M76363 6 Collected 18 AUG 08 14 0'0 By AW Recerued 20 AUG 08 By E Mt�u 29 (68)„ M76363-6 MADEP VPH REV 1.127-AUG-08 04:45 AF VMAVPH M76363 T Collectedl8 AUG 0$yi3 15 By AW r 4 Rece�ved�20 AUG 08 $y 3 M76363-7 MADEP VPH REV 1.127-AUG-08 05:25 AF VMAVPH MI636£3 S� C�olleeted 18°AUG OS y12�45,By AU1/� `�Receiued ZO AUG 08 By�� MW 35�53 � k M76363-8 MADEP VPH REV 1.127-AUG-08 06:06 AF VMAVPH Page 1 of 3 Rl 47 of 55 Al fU.I..'ES7: M76363 '....... ::i•, r Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil - Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M76363 9' Collected�1$E1UG08�ll�00By�A����cei�gd 20£AU�G OS Bye ��� � `���� � M76363-9 MADEP VPH REV 1.127-AUG-08 06:47 AF VMAVPH M76363`1C�CoUected i$j�AUG DS 11`50��B �A�W� Received;2'0 AUG�08�B ����� M76363-10 MADEP VPH REV 1.127-AUG-08 07:28 AF VMAVPH M76363�11 )Collected 18 AUG081��15ByE1W ` Recved20 AUG'p8 B d MW 37 M76363-11 MADEP VPH REV 1.127-AUG-08 08:10 AF VMAVPH M76363 1 Collected 18 AUG 08 1� 20By AW� Receued20 5m Y M76363-12. MADEP VPH REV 1.127-AUG-08 08:51 AF VMAVPH M 16363 1 Collected 18 AUG 08 1155" By A � Rec�eiued20 AUG�08 By 3 M:W 40F(85) � � � z2 cru M76363-13 MADEP VPH REV 1.127-AUG-08 09:32 AF VMAVPH M76363 1 Collected 18 AUG 08 12 55 B AUU Received 20 AUG 08 B _ ` IVIUV 38(104) Y t� Y� M76363-1,� MADEP VPH REV 1.127-AUG-08 15:44 AF VMAVPH U7,630,15 Collected 18'AUG 08 13 30 By AW a Received 20 A(JG o$ ,By W-40 M76363-15 MADEP VPH REV 1.127-AUG-08 16:26 AF VMAVPH M76363 1" Collected 18iAUG08 09,40�By AW�� Received` 20AUG 08 By z' M76363-16 MADEP VPH REV 1.127-AUG-08 17:07 AF VMAVPH Page 2 of 3 Q 48 of 55 A=U—TEST. ............... M76363 r Accutest Laboratories P. Internal Sample Tracking Chronicle rx Shell Oil Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project no: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M�76363�1�'Collectedl8�AUG�08�1�1 20�By AW Reee�v3"ei120�U�G�08 By,; � � � � � � M76363-17 MADEP VPH REV 1.127-AUG-08 17:49 AF VMAVPH M16363�Collected M76363-18 MADEP VPH REV 1.127-AUG-08 18:30 AF VMAVPH Page 3 of 3 49 of 55 A UTEST. M76363 _--„-=t; €,r•. o• i New England .,-. Section 5 WOO - � �� � eR GC V" atiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries 50 of 55 . r Method. Blank Summary Page 1 of i Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 ;REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD990-MB BD20849.D 1 08/26/08 AF n/a n/a GBD990 trr :.a The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76363-1, M76363-2, M76363-3, M76363-4, M76363-5, M76363-6, M76363-7, M76363-8, M76363-9, M76363-10, M76363-11, M76363-12, M76363-13 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene N'D 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND . 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND. 50 ug/1 C9- C12 Aliphatics (Unadj.) ND., 50 ug/1 C9- C10 Aromatics (Unadj.) ND` 50 ug/1 C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND : 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 82% 70-130% 615-59-8 2,5-Dibromotoluene 88% 70-130% 51 of 55 A _. L9__..._._._ • M76363 ......,. .,...., r Method Blank Summary Page I of 1 Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD991-MB BD20873.1) 1 08/27/08 AF n/a n/a GBD991 The C reported here applies to the following samples: Method: MADEP VPH REV 1.1 Q P PP g P M76363-14, M76363-15, M76363-16, M76363-17, M76363-18 CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene ND, 3.0 ug/1 108-88-3 Toluene ND - 2.0 ug/l m,p-Xylene N. 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 82% 70-130% 615-59-8 2,5-Dibromotoluene 91% 70-130% 52 of 55 �1CUTEST. ......................................... M76363 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD990-BSP BD20850.D 1 08/26/08 AF n/a n/a GBD990 GBD990-BSD BD2085I.D 1 08/26/08 AF n/a n/a GBD990 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76363-1, M76363-2, M76363-3, M76363-4, M76363-5, M76363-6, M76363-7, M76363-8, M76363-9, M76363-10, M76363-11, M76363-12, M76363-13 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/I % ug/I % RPD Rec/RPD 71-43-2 Benzene 50 51.7 103' 51.7 d03., "0 70-130/25 100-41-4 Ethylbenzene 50 52.6 105 52.7 165' 10 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 51.6 103 51.7 1'03: 0 70-130/25 91-20-3 Naphthalene 50 48.4 97 49.9 70-130/25 108-88-3 Toluene 50 52.3 105 52.4 105 . 0' 70-130/25 m,p-Xylene 100 105 105 105 1'5 0 70-130/25 95-47-6 o-Xylene 50 49.4 99 49.5 99 01 70-130/25 C5- C8 Aliphatics (Unadj.) 150 142 95 > 144 96 1 70-130/25 C9- C12 Aliphatics (Unadj.) 150 141 94 141 94 0 70-130/25 C9- C10 Aromatics (Unadj.) 50 50.1 100 50.3 101 0 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 816/.: 83% 70-130% 615-59-8 2,5-Dibromotoluene 89% 91% 70-130% 53 of 55 12ACCUTEST. M76363 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M76363 Account: SHELLWIC Shell Gil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD991-BSP BD20874.D 1 08/27/08 AF n/a n/a GBD991 GBD991-BSD BD20875.D 1 08/27/08 AF n/a n/a GBD991 N The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76363-14, M76363-15, M76363-16, M76363-17, M76363-18 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/1 ug/1 % ug/1 % RPD Rec/RPD 71-43-2 Benzene 50 53.6 107;" . 52.2 104,;. 3 70-130/25 100-41-4 Ethylbenzene 50 54.2 108 52.7 A05"! ` 3 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 54.1 108 51.2 102 6 70-130/25 91-20-3 Naphthalene 50 53.1 106 ,' 50.9 IO2 4 70-130/25 108-88-3 Toluene 50 53.7 107: 52.3 105 3 70-130/25 m,p-Xylene 100 108 109 105 i;Q5 3 70-130/25 95-47-6 o-Xylene 50 50.9 102 49.3 99 3 70-130/25 C5- C8 Aliphatics (Unadj.) 150 150 100 141 9,4 6 70-130/25 C9- C12 Aliphatics (Unadj.) 150 143 95 138 92 , 4 70-130/25 C9- C10 Aromatics (Unadj.) 50 52.2 104 50.0 100 4 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 84% 85% '- 70-130% 615-59-8 2,5-Dibromotoluene 93% 93% 70-130% y- 54 of 55 gJACCUTEST. M76363 .._...:..,. . a Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method , is Lab Lab Sample ID File ID S1 a S1 b M76363-1 BD20859.D 79:0 ._;. 86.0 M76363-2 BD20860.D 80.0 .. . 87.0 M76363-3 BD20861.D 72:0 80.0 M76363-4 BD20862.D 80.0 87.0 M76363-5 BD20863.D 78.0 86.0 M76363-6 BD20864.D 80:.0: 89.0 M76363-7 BD20865.D 81.0, 88.0 M76363-8 BD20866.D M76363-9 BD20867.D 81L.ff M76363-10 BD20868.D 87A 94.0 M76363-11 BD20869.D 83:0'' 92.0 M76363-12 BD20870.D 82.0!` 91.0 M76363-13 BD20871.D 83:0', .: 93.0 M76363-14 BD20880.D 81;.0> 90.0 M76363-15 BD20881.D 81.0: 90.0 M76363-16 BD20882.D 87.0 96.0 M76363-17 BD20883.D 82.0 91.0 M76363-18 BD20884.D 81.0 92.0 GBD990-BSD BD20851.D 83.0 91.0 GBD990-BSP BD20850.D 81.0 89.0 GBD990-MB BD20849.D 82.0 88.0 GBD991-BSD BD20875.D 85.0 93.0 GBD991-BSP BD20874.D 84.0 93.0 GBD991-MB BD20873.D $2.0 91.0 Surrogate Recovery Compounds Limits S1 = 2,5-Dibromotoluene 70-1306/o (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 55 of 55 12AC=UTEST. M76363 1 ' October 17,2008 Via eDEP Electronic Upload Commonwealth of Massachusetts Department of Environmental Protection-SERO ' 20 Riverside Drive Lakeville., Massachusetts 02347 Ph:508-946-2700 r, Re: INSPECTION AND MONITORING REPORT# 7 FOR PHASE V REMEDY OPERATING STATUS ' Former Texaco-Branded Service Station 1140 Iyannough Road Hyannis,Massachusetts 02072 RTN 4-11301 To Whom It May Concern: ' On behalf of Motiva Enterprises LLC (Motiva), Sovereign Consulting Inc. (Sovereign) is submitting the attached Inspection and Monitoring (I&M) Report for Phase V Remedy ' Operating Status regarding the above-referenced disposal site. This I&M report was prepared in accordance with the Massachusetts Contingency Plan (MCP) and summarizes response actions conducted between April 2008 through October 2008. ' If you have any questions regarding this submittal,please feel free to contact the undersigned. Sincerely, SOVEREIGN CONSULTING,INC. C"C'c v ` John Bender Eric D.Simpson,P.G.,LSP ' Geologist Operations Manager Attachments: I&M Report Transmittal Form BWSC-108 ' cc: With Attachments: D.Weeks,Motiva Enterprises LLC Ms.Donna Miorandi,Town of Barnstable,Health Inspector Mr.Hans Keijser,Town of Barnstable Water Supply Division Ms.Mary Ellen Cunha,The Wilder Companies Sovereign File-EQ 711 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 Massachusetts De partment of Environmental Protection Bureau of Waste Site Cleanup BWSC108 Lt7 Y' COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM& PHASE I COMPLETION STATEMENT a - 11301 Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) A. SITE LOCATION: 1. Site Name:TEXACO STATION 2. Street Address: 11140 RTE 132 3. City/Town: HYANNIS 4. ZIP Code:1.026010000 5.UTM Coordinates: a.UTM N: 14614197 b. UTM E: 1391208 --� ' ❑ 6. Check here if a Tier Classification Submittal has been provided to DEP for this disposal site. ❑ a. Tier IA ❑ b. Tier IB © c. Tier IC ❑ d. Tier II ' 7. If applicable,provide the Permit Number: 100556 B.THIS FORM IS BEING USED TO: (check all that apply) ' ❑ 1. Submit a Phase I Completion Statement,pursuant to 310 CMR 40.0484. ❑ 2. Submit a Revised Phase I Completion Statement,pursuant to 310 CMR 40.0484. ❑ 3. Submit a Phase II Scope of Work,pursuant to 310 CMR 40.0834. ❑ 4. Submit an interim Phase II Report. This report does not satisfy the response action deadline requirements in 310 CMR 40,0500. ,' ❑ 5. Submit a final Phase II Report and Completion Statement,pursuant to 310 CMR 40.0836. ❑ 6.Submit a Revised Phase II Report and Completion Statement,pursuant to 310 CMR 40.0836. ' ❑ 7. Submit a Phase III Remedial Action Plan and Completion Statement,pursuant to 310 CMR 40.0862. ❑ 8. Submit a Revised Phase III Remedial Action Plan and Completion Statement,pursuant to 310 CMR 40.0862. ❑ 9. Submit a Phase IV Remedy Implementation Plan,pursuant to 310 CMR 40.0874. ❑ 10. Submit a Modified Phase IV Remedy Implementation Plan,pursuant to 310 CMR 40.0874. ❑ 11. Submit an As-Built Construction Report,pursuant to 310 CMR 40.0875. ' ❑ 12. Submit a Phase IV Status Report,pursuant to 310 CMR 40.0877. ❑ 13. Submit a Phase IV Completion Statement,pursuant to 310 CMR 40.0878 and 40.0879. Specify the outcome of Phase IV activities:(check one) ❑ a. Phase V Operation,Maintenance or Monitoring of the Comprehensive Remedial Action is necessary to achieve a Response Action Outcome. ' b. The requirements of a Class A Response Action Outcome have been met. No additional Operation,Maintenance or ❑ Monitori'ng is necessary to ensure the integrity of the Response Action Outcome. A completed Response Action Outcome Statement and Report(BWSC104)will be submitted to DEP. ' c. The requirements of a Class C Response Action Outcome have been met. No additional Operation,Maintenance or ❑ Monitoring is necessary to ensure the integrity of the Response Action Outcome. A completed Response Action ' Outcome Statement and Report(BWSC104)will be submitted to DEP. d. The requirements of a Class C Response Action Outcome have been met. Further Operation,Maintenance or ❑ Monitoring of the remedial action is necessary to ensure that conditions are maintained and that further progress is made toward a Permanent Solution. A completed Response Action Outcome Statement and Report (BWSC104)will ' be submitted to DEP. (All sections of this transmittal form must be filled out unless otherwise noted above) ' Revised:2/15/2005 Page 1 of 5 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC108 -, COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM & PHASE I COMPLETION STATEMENT 4 113 zt Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) B.THIS FORM IS BEING USED TO(coat): (check all that apply) ❑ 14. Submit a Revised Phase IV Completion Statement,pursuant to 310 CMR 40.0878 and 40.0879. ' ❑ 15. Submit a Phase V Status Report,pursuant to 310 CMR 40.0892. ❑✓ 16. Submit a Remedial Monitoring Report.(This report can only be submitted through eDEP.) ' a.Type of Report:(check one) ❑ i. Initial Report ❑✓ ii. Interim Report ❑ iii. Final Report b.Frequency of Submittal:(check all that apply) ❑ i. A Remedial Monitoring Report(s)submitted monthly to address an Imminent Hazard. ' ❑ ii. A Remedial Monitoring Report(s)submitted monthly to address a Condition of Substantial Release Migration. ❑✓ iii. A Remedial Monitoring Report(s)submitted concurrent with a Status Report. ' c.Status of Site:(check one) ❑ i. Phase V ❑✓ ii. Remedy Operation Status ❑ iii.Class C RAO d. Number of Remedial Systems and/or Monitoring Programs: 11 ' A separate BWSC108A,CRA Remedial Monitoring Report,must be filled out for each Remedial System and/or Monitoring Program addressed by this transmittal form. ❑ 17. Submit a Remedy Operation Status,pursuant to 310 CMR 40.0893. ' © 18. Submit a Status Report to maintain a Remedy Operation Status,pursuant to 310 CMR 40.0893(2). ❑ 19. Submit a Modification of a Remedy Operation Status,pursuant to 310 CMR 40.0893(5). ' ❑ 20. Submit a Termination of a Remedy Operation Status,pursuant to 310 CMR 40.0893(6). ❑ 21. Submit a Phase V Completion Statement,pursuant to 310 CMR 40.0894. ' Specify the outcome of Phase V activities: (check one) a. The requirements of a Class A Response Action Outcome have been met. No additional Operation,Maintenance or ❑ Monitoring is necessary to ensure the integrity of the Response Action Outcome. A completed Response Action ' Outcome Statement(BWSC104)will be submitted to DEP. b. The requirements of a Class C Response Action Outcome have been met. No additional Operation,Maintenance or ❑ Monitoring is necessary to ensure the integrity of the Response Action Outcome. A completed Response Action ' Outcome Statement and Report(BWSC104)will be submitted to DEP. c. The requirements of a Class C Response Action Outcome have been met. Further Operation,Maintenance or ❑ Monitoring of the remedial action is necessary to ensure that conditions are maintained and/or that further progress is made toward a Permanent Solution. A completed Response Action Outcome Statement and Report(BWSC104)will be submitted to DEP. ❑ 22. Submit a Revised Phase V Completion Statement,pursuant to 310 CMR 40.0894. ❑ 23. Submit a Post-Class C Response Action Outcome Status Report,pursuant to 310 CMR 40.0898. (All sections of this transmittal form must be filled out unless otherwise noted above Revised: 2/15/2005 Page 2 of 5 Massachusetts Department of Environme ntal ental Protection Bureau of Waste Site Cleanup BWSC108 COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM& PHASE I COMPLETION STATEMENT 4 11301 �' Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) C. LSP SIGNATURE AND STAMP: I attest under the pains and penalties of perjury that I have personally examined and am familiar with this transmittal form, ' including any and all documents accompanying this submittal. In my professional opinion and judgment based upon application of(1)the standard of care in 309 CMR 4.02(1),(ii)the applicable provisions of 309 CMR 4.02(2)and(3),and 309 CMR 4.03(2),and (iii)the provisions of 309 CMR 4.03(3),to the best of my knowledge,information and belief, > if Section B indicates that a Phase 1,Phase It,Phase/it,Phase IV or Phase V Completion Statement is being submitted,the response action(s)that is(are)the subject of this submittal(i)has(have)been developed and implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the ' purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,and(iii) comply(ies)with the identified provisions of all orders,permits,and approvals identified in this submittal; > if Section B indicates that a Phase H Scope of Work or a Phase IV Remedy Implementation Plan is being submitted,the response action(s)that is(are)the subject of this submittal(i)has(have)been developed in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,and(iii)comply(ies)with the identified provisions of all orders,permits,and approvals identified in this submittal; > if Section B indicates that an As-Built Construction Report,a Remedy Operation Status,a Phase IV,Phase V or Post-Class C RAO Status Report,a Status Report to Maintain a Remedy Operation Status and/or a Remedial Monitoring Report is being submitted,the response action(s)that is(are)the subject of this submittal(i)is(are)being implemented in accordance with the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,(ii)is(are)appropriate and reasonable to accomplish the purposes of such response action(s)as set forth in the applicable provisions of M.G.L.c.21 E and 310 CMR 40.0000,and(iii)comply(ies) with the identified,provisions of all orders,permits,and approvals identified in this submittal. ' I am aware that significant penalties may result,including,but not limited to,possible fines and imprisonment,if I submit information which I know to be false,inaccurate or materially incomplete. 1. LSP#: 8881 r � �&eYaw K �� MAN 2. First Name: ERIC D 4 � � 3. Last Name.SO SIMPSON� 4. Telephone. �'_01W ER,, ' 5. Ext.: 6. FAX: e ti "'m k. _ w w, 7. Signature. DilttpsOn �N- f T 8. Date: 10/T�I2008, ; 9.LSP Stamp: (mm/dd/yyyy) Electronic Seal 1 ' Revised: 2/15/2005 Page 3 of 5 ' Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC108 ' COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM& PHASE I COMPLETION STATEMENT '4 130 ' Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) D. PERSON UNDERTAKING RESPONSE ACTIONS: ' 1. Check all that apply: ❑ a.change in contact name ❑ b.change of address ❑ c. change in the personundertaking response actions 2. Name of Organization: SHELL OIL PRODUCTS CO Contact First Name: D"ID 4.Last Name: WEEKS 5. Street: PMB 301 1830 SOUTH RD UNIT 24 6.Title: ' WAPPINGERS FALLS NY 7. City/Town. 8. State: �� 9. ZIP Code: 125900000 ' 10. Telephone: 8454625225 11.Ext.: 12. FAX: E. RELATIONSHIP TO SITE OF PERSON UNDERTAKING RESPONSE ACTIONS: ❑✓ 1. RP or PRP ❑ a. Owner ❑ b. Operator ❑ c. Generator ❑ d. Transporter © e. Other RP or PRP Specify: PRP GENERIC OR NON-SPECIFIED ' ❑ 2. Fiduciary,Secured Lender or Municipality with Exempt Status(as defined by M.G.L.c.21 E,s.2) ❑ 3. Agency or Public Utility on a Right of Way(as defined by M.G.L.c.21 E,s.50)) ' ❑ 4. Any Other Person Undertaking Response Actions Specify Relationship: ' F. REQUIRED ATTACHMENT AND SUBMITTALS: 1. Check here if the Response Action(s)on which this opinion is based,if any,are(were)subject to any order(s),permit(s) ❑ and/or approval(s)issued by DEP or EPA. If the box is checked,you MUST attach a statement identifying the applicable ' provisions thereof. ❑ 2. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the submittal of any Phase Reports to DEP. ❑ 3. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the availability of a Phase III Remedial Action Plan. ' ❑ 4. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of the availability of a Phase IV Remedy Implementation Plan. ❑ 5. Check here to certify that the Chief Municipal Officer and the Local Board of Health have been notified of any field work ' involving the implementation of a Phase IV Remedial Action. ❑ 6. If submitting a Modification of a Remedy Operation Status,check here to certify that a statement detailing the compliance history,as per 310 CMR 40.0893(5),for the person making this submittal is attached. ' ❑ 7. If submitting a Modification of a Remedy Operation Status,check here to certify that written consent of the person who submitted the Remedy Operation Status submittal,as per 310 CMR 40.0893(5),is attached. ❑ 8. Check here if any non-updatable information provided on this form is incorrect,e.g.Site Name. Send corrections to the ' DEP Regional Office. © 9. Check here to certify that the LSP Opinion containing the material facts,data,and other information is attached. Revised: 2/15/2005 Page 4 of 5 ' Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC108 COMPREHENSIVE RESPONSE ACTION TRANSMITTAL Release Tracking Number FORM& PHASE 1 COMPLETION STATEMENT 4 1130'V ' Pursuant to 310 CMR 40.0484(Subpart D)and 40.0800(Subpart H) G. CERTIFICATION OF PERSON UNDERTAKING RESPONSE ACTIONS: 1. I,DAVID WEEKS ,attest under the pains and penalties of perjury(i)that I have personally ' examined and am familiar with the information contained in this submittal,including any and all documents accompanying this transmittal form, (ii)that,based on my inquiry of those individuals immediately responsible for obtaining the information,the material information contained in this submittal is,to the best of my knowledge and belief,true,accurate and complete,and(iii) ' that I am fully authorized to make this attestation on behalf of the entity legally responsible for this submittal. I/the person or entity on whose behalf this submittal is made am/is aware that there are significant penalties,including,but not limited to, possible fines and imprisonment,for willfully submitting false,inaccurate,or incomplete information. 2. By davld weeks ,�>9 c_: g ,^ . ,..,� , �t �r 3. Title: Signature ' 4. For: ISHELL OIL PRODUCTS CO 5. Date: 10/17/2008 (Name of person or entity recorded in Section D) (mm/dd/yyyy) ❑ 6. Check here if the address of the person providing certification is different from address recorded in Section D. 7. Street: ' 8. City/Town: 9. State: 10. ZIP Code: 11. Telephone: 12.Ext.: 13. FAX: ' YOU ARE SUBJECT TO AN ANNUAL COMPLIANCE ASSURANCE FEE OF UP TO$10,000 PER BILLABLE YEAR FOR THIS DISPOSAL SITE. YOU MUST LEGIBLY COMPLETE ALL RELEVANT SECTIONS OF THIS FORM OR DEP MAY RETURN THE DOCUMENT AS INCOMPLETE. IF YOU SUBMIT AN INCOMPLETE FORM,YOU MAY BE PENALIZED FOR MISSING A REQUIRED DEADLINE. Date Stamp(DEP USE ONLY:) ' Received by DEP on ' 10/17/2008 3:21:36 PM Revised: 2/15/2005 Page 5 of 5 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC108A ' CRA REMEDIAL MONITORING REPORT Release Tracking Number Pursuant to 310 CMR 40.0800(SUBPART H) a - 11301 ' Remedial System or Monitoring Program: ff_�_ of:L�I A. DESCRIPTION OF ACTIVE REMEDIAL SYSTEM OR ACTIVE REMEDIAL MONITORING PROGRAM: ' 1. Type of Active Remedial System or Active Remedial Monitoring Program:(check all that apply) ❑ a. Active Remedial System:(check all that apply) ❑ i.NAPL Recovery ❑ ii. Soil Vapor Extraction/Bioventing ❑ iii. Vapor-phase Carbon Adsorption ❑ iv.Groundwater Recovery ❑ v. Dual/Multi-phase Extraction ❑ vi. Aqueous-phase Carbon Adsorption ' ❑ vii.Air Stripping ❑ viii. Sparging/Biosparging ❑ ix. Cat/Thermal Oxidation ❑ x. Other Describe: ' ❑ b. Application of Remedial Additives:(check all that apply) ❑ i.To the Subsurface ❑ ii. To Groundwater(Injection) ❑ iii. To the Surface ' c. Active Remedial Monitoring Program Without the Application of Remedial Additives:(check all that apply;Sections C,D and E are not required;attach supporting information,data,maps and/or sketches needed by checking Section F5) ❑ i. Reactive Wall ❑✓ ii. Natural'Attenuation ❑ iii. Other Describe: 2. Mode of Operation:(check one) ❑ a. Continuous ❑ b. Intermittent ❑ c. Pulsed ❑ d. One-time Event Only ✓0 e. Other:IQUARTERLY 3. System Effluent/Discharge:(check all that apply) ' ❑ a.Sanitary Sewer/POTW ❑ b.Groundwater Re-infiltration/Re-injection:(check one) ❑ i. Downgradient ❑ ii. Upgradient ❑ c. Vapor-phase Discharge to Ambient Air:(check one) ❑ i. Off-gas Controls ❑ ii. No Off-gas Controls ' ❑ d. Drinking Water Supply ❑ e. Surface Water(including Storm Drains) . ' ❑ f. Other Describe: B. MONITORING FREQUENCY: 1. Reporting period that is the subject of this submittal: From: 4/30/2008 To: 10/7/2008 (mm/dd/yyyy) (mm/dd/yyyy) 2. Number of monitoring events during the reporting period:(check one) ❑ a.System Startup:(if applicable) ❑ i. Days 1,3,6,and then weekly thereafter,for the first month. ❑ ii. Other Describe: ' 0✓ b.Post-system Startup(after first month)or Monitoring Program: ❑ i.Monthly ❑✓ ii.Quarterly ' ❑ iii. Other Describe: �✓ 3. Check here to certify that the number of required monitoring events were conducted during the reporting period. ' C. EFFLUENT/DISCHARGE REGULATION:(check one to indicate how the effluent/discharge limits were established) 1.NPDES:(check one) ❑ a. Remediation General Permit ❑ b. Individual Permit ❑ c. Emergency Exclusion Effective Date of Permit: ' ❑ 2. MCP Performance Standard MCP Citations(s): ❑ 3. DEP Approval Letter Date of Letter: mm/dd/ ❑ 4. Other Describe: Revised: 2/9/2005 Page 1 of 3 J Massachusetts Department '7 __ p ent of Environmental Protection Bureau of Waste Site Cleanup BWSC108A CRA REMEDIAL MONITORING REPORT Release Tracking Number Pursuant to 310 CMR 40.0800(SUBPART H) 4] - 11301 ' Remedial System or Monitoring Program: L' J of:L J D. WASTEWATER TREATMENT PLANT OPERATOR:(check one) ' ❑ 1. Required due to Remedial Wastewater Treatment Plant in place for more than 30 days. a. Name: b. Grade: c.License No.: J d.License Exp. Date: ❑ 2. Not Required (mm/dd/yyyy) ❑ 3. Not Applicable ' E. STATUS OF ACTIVE REMEDIAL SYSTEM OR ACTIVE REMEDIAL MONITORING PROGRAM DURING REPORTING PERIOD: (check all that apply) ' ❑ 1.The Active Remedial System was functional one or more days during the Reporting Period. a. Days System was Fully Functional: b.GW Recovered(gals): c. NAPL Recovered(gals): d.GW Discharged(gals): e.Avg.Soil Gas Recovery Rate(scfm): f. Avg.Sparging Rate(scfm): ❑ 2.Remedial Additives:(check all that apply) ' ❑ a.No Remedial Additives applied during the Reporting Period. ❑ b. Enhanced Bioremediation Additives applied:(total quantity applied at the site for the current reporting period) ❑ i.Nitrogen/Phosphorus: ❑ ii. Peroxides: ' Name of Additive Date Quantity I Units Name of Additive Date lQuantity Units tE - F1 iii.Microorganisms: ❑ iv.Other: Name of Additive Date Quantity Units Name of Additive Date Quantity Units ❑ c.Chemical oxidation/reduction additives applied:(total quantity applied at the site for the current reporting period) El i.Permanganates: ❑ ii.Peroxides: Name of Additive Date Quantity Units Name of Additive Date Quantity Units ' ❑ iii. Persulfates: ❑ iv.Other: Name of Additive Date Quantity Units Name of Additive Date Quantity Units Revised: 2/9/20C-5 Page 2 of 3 Massachusetts Department of Environmental Protection Bureau of Waste Site Cleanup BWSC108A ' CRA REMEDIAL MONITORING REPORT Release Tracking Number Pursuant to 310 CMR 40.0800(SUBPART H) L �� - 11301 Remedial System or Monitoring Program: Q of:L�I E. STATUS OF ACTIVE REMEDIAL SYSTEM OR ACTIVE REMEDIAL MONITORING PROGRAM DURING REPORTING PERIOD:(cont.) (check all that apply) ' ❑ d.Other additives applied:(total quantity applied at the site for the current reporting period) Name of Additive Date Quantity Units Name of Additive Date Quantity Units ' ❑ e. Check here if any additional Remedial Additives were applied. Attach list of additional additives and include Name of Additive,Date Applied,Quantity Applied and Units(in gals.or lbs.) ' F. SHUTDOWNS OF ACTIVE REMEDIAL SYSTEM OR ACTIVE REMEDIAL MONITORING PROGRAM:(check all that apply) ❑ 1. The Active Remedial System had unscheduled shutdowns on one or more occasions during the Reporting Period. a. Number of Unscheduled Shutdowns: b.Total Number of Days of Unscheduled Shutdowns: ' c. Reason(s)for Unscheduled Shutdowns: ' ❑ 2. The Active Remedial System had scheduled shutdowns on one or more occasions during the Reporting Period. a.Number of Scheduled Shutdowns: b.Total Number of Days of Scheduled Shutdowns: ' c.Reason(s)for Scheduled Shutdowns: 3. The Active Remedial System or Active Remedial Monitoring Program was permanently shutdown/discontinued during the Reporting Period. a.Date of Final System or Monitoring Program Shutdown: ❑ b. No Further Effluent Discharges. (mm/dd/yyyy) ' ❑ c. No Further Application of Remedial Additives planned;sufficient monitoring completed to demonstrate compliance with 310 CMR 40.0046. ' El d. No Further Submittals Planned. ❑ e. Other: Describe: ' G. SUMMARY STATEMENTS:(check all that apply for the current reporting period) ❑ 1. All Active Remedial System checks and effluent analyses required by the approved plan and/or permit were ' performed when applicable. ❑ 2. There were no significant problems or prolonged(>25%of reporting period)unscheduled shutdowns of the Active Remedial System. ' m 3. The Active Remedial System or Active Remedial Monitoring Program operated i n conformance with the MCP,and all applicable approval conditions and/or permits. 4. Indicate any Operational Problems or Notes: ' ❑✓ 5. Check here if additional/supporting Information,data,maps,and/or sketches are attached to the form. Revised: 2/9/2005 Page 3 of 3 SOVEREIGN • INSPECTION AND MONITORING REPORT#7 FOR ' PHASE V REMEDY OPERATING STATUS Former Texaco-Branded Service Station 1140 Iyannough Road Hyannis,Massachusetts 02072 Location# 100083 October 17, 2008 ' MassDEP RTN 4-11301 Prepared for: Motiva Enterprises LLC 1830 South Road,PMB 301, Unit 24 Wappingers Falls,New York 12590 Prepared by: ' Sovereign Consulting,Inc. 905E South Main Street ' Suite 202 Mansfield, Massachusetts 02048 Project Number: EQ711 Inspection.and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts ' TABLE OF CONTENTS 1.0 INTRODUCTION......................................................................................................................... 1 2.0 SITE DESCRIPTION AND BACKGROUND.........................................................................1 2.1 SITE DESCRIPTION...................................................................................................................................... 1 2.2 SENSITIVE RECEPTORS................................................................................................................................ 1 2.3 SUMMARY OF THE PHASE IV REMEDY IMPLEMENTATION PLAN............................................................ 2 ' 3.0 INSPECTION AND MONITORING REPORT.......................................................................3 3.1 DESCRIPTION OF THE TYPE AND FREQUENCY OF ACTIVITIES CONDUCTED:310 CMR 40.0892(2)(A) 3 3.1.1 AS/SVE Operation...............................................................................................................................3 ' 3.1.2 GWPT System Operation.....................................................................................................................3 3.1.3 Groundwater Sailing and MNA.......................................................................................................3 3.2 DATA:310 CMR 40.0892(2)(C) ..................................................................................................................4 ' 4.0 MCP DATA QUALITY REVIEW...............................................................................................4 4.1 PROJECT DATA QUALITY OBJECTIVES......................................................................................................5 4.1.1 Field Data Collection............................................................................................................................ 5 ' 4.2 PRESUMPTIVE CERTAINTY AND CAM COMPLIANCE..............................................................................5 4.2.1 CAM Complaint Data.......................................................................................................................... 6 4.2.2 CAM-Non Compliant Data.................................................................................................................. 6 5.0 DATA USABILITY ASSESSMENT CONCLUSIONS........................................................... 6 6.0 SIGNIFICANT MODIFICATIONS SINCE SUBMITTAL OF PRECEDING I&M REPORT: 310 CMR 40.0892(2)(B)........................................................................................................... 6 7.0 CONDITIONS AND/OR PROBLEMS AFFECTING REMEDIAL ACTION PERFORMANCE: 310 CMR 40.0892(2)(D)...........................................................................................6 8.0 MEASURE TAKEN TO CORRECT CONDITIONS AND/OR PROBLEMS:310 CMR 40.0892(2)(D)..............................................................................................................................................6 9.0 EVALUATION PERFORMANCE OF THE REMEDIAL ACTION....................................7 ' 10.0 PROJECTED SCHEDULE........................................................................................................ 7 ' 11.0 PUBLIC INVOLVEMENT........................................................................................................7 i Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former;exaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts it FIGURES ' Figure 1 Site Locus Map Figure 2 Site Plan ' Figure 3 Mass GIS Site Scoring Map ' TABLES Table 1 Summary of Groundwater Monitoring Data-VPH ' Table 2 Summary of Groundwater Monitoring Data-EPH Table 3 Summary of Groundwater Monitoring Data-MNA Table 4 Summary of Groundwater Monitoring Data-Oxygenates ' Table 5 Summary of GWPT System Monitoring Data ' ATTACHMENTS Attachment A Laboratory Analytical Data-Groundwater Sampling ' Attachment B Copy of Third Party Results Letters 1 1 ii ' Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts 1.0 INTRODUCTION ' Sovereign Consulting Inc. (Sovereign) prepared this Phase V Remedy Operating Status Inspection and Monitoring (Phase V I&M) Report on behalf of Motiva Enterprises LLC ' (Motiva). The report presents information related to the operation; maintenance, and/or monitoring of the selected remedial action (RAs) for Massachusetts Department of Environmental Protection(MassDEP) Release Tracking Number (RTN) 4-11301. For the purpose of this report, the "facility" is defined as the area located within the legal property boundaries of the former Texaco-branded service station located at 1140 Iyannough ' Road in Hyannis, Massachusetts. The "disposal site" for RTN 4-11301 is defined as the facility and other properties where oil and/or hazardous material (OHM) have come to be located as a result of a release at the facility. Currently, the other properties within the boundary of the ' disposal site include several commercial properties on Iyannough Road, Independence Drive, Attucks Lane, and Airport Road. Please refer to Figure 1-Site Locus for the site location and Figure 2-Site Plan for a depiction of the disposal site. This document summarizes activities performed at the disposal site from April 2008 through October 2008. In accordance with 310 CMR 40.0892, this report discusses the type, frequency, modifications, ' conditions, problems, measures, and sampling conducted with regard to the selected Remedial Alternatives (RA) to support the implementation of the Comprehensive Remedial Action (CRA) at the site. 2.0 SITE DESCRIPTION AND BACKGROUND ' 2.1 Site Description The facility is a former Texaco-branded service station which was redeveloped into a Towne Fair Tire retail store and retail jewelry store. A release of gasoline at the former Texaco-branded gasoline station at 1140 Iyannough Road is the subject of RTN 4-11301. The disposal site (as depicted in Figure 2), encompasses several properties to the east of the former Texaco facility. The disposal site extends beneath commercially developed properties, roads and several ponds. Properties included within the boundary of the disposal site include ' several commercial properties,undeveloped land, and three surface water bodies. 2.2 Sensitive Receptors Accordingto data obtained from Massachusetts Geographic Information Systems Mass GIS Y ( ) maps, groundwater beneath the disposal site is located within a Zone II Wellhead protection district. According to data obtained from the Mass GIS site scoring map (Figure 3), groundwater beneath the disposal site is mapped as part of a Zone II Wellhead Protection Area, EPA Sole Source Aquifer, and a medium yield Non-Potential Drinking Water Source Area. There are four municipal wells located approximately 1 mile from the disposal site. Municipal wells 4020000- ' 1 ' Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts 04G and 4020000-03G are located to the northeast, municipal well 4020000-02G is located to the northwest, and municipal well 2316000-01G is located approximately 1 mile southeast of the ' disposal site. The closest surface water body is an un-named intermittent stream and a tributary of Mill Brook located approximately 520 feet to the west-northwest of the site. Two un-named ponds are located approximately 1,050 feet south and 1,450 feet east, respectively, of the site. In addition, Mill Brook located approximately 1,584 feet to the north-northeast of the site. ' Based on information provided by the Town of Webster's Board of Health and Department of Public Works (DPW), there are no known private drinking water wells within 1/4 mile of the site. No schools, hospitals, daycare centers, or long-term health care facilities were identified within 500 feet of the site. There are no interim well head protection areas, surface water supply Zone A areas, Potentially ' Productive Aquifers, wetlands, Protected Open Spaces, Priority Habitats of Rare Species, vernal pools, or Areas of Critical Environmental Concern(ACEC) identified within 500 feet of the site. Applicable groundwater categories for this disposal site include: • GW-1,GW-3: Depth to water exceeds 15 feet below grade surface (bgs), therefore GW-2 ' standards do not apply to groundwater sampled from any wells at the disposal site. 2.3 Summary of the Phase IV Remedy Implementation Plan ' The selected remedial alternatives RA for the contaminant plume are Air S are Soil Vapor ( ) P p g / P Extraction (AS/SVE), a groundwater pump and treatment (GWPT) and monitored natural I ' attenuation(MNA). The AS/SVE system was deactivated in July 2005 based on asymptotic decline in extracted ' volatile organic compounds (VOCs) with the SVE airstream and the declining concentrations present in groundwater within the radius of influence of the AS/SVE system. ' Following the November 8, 2007 O&M, the GWPT system was shut down due to consistently low levels of COCs in the monitoring wells, therefore there was believed to be little benefit for continuing system operation. Reactivation of the system will depend on future groundwater ' sampling results through 2008.The GWPT system is being maintained as fully functional. Currently, the only active RA is MNA, which is documented through quarterly groundwater sampling and monitoring. Summaries of historical groundwater quality data are provided in Tables 1,2,and 3. MNA parameter measurements are included in Table 4. ' On January 29, 2004, a Phase IV - RIP, GSC was submitted that detailed a proposed implementation of an off-site groundwater pump and treat (GWPT) system, ongoing operation and maintenance of an on-site soil vapor-extraction/air sparge (SVE/AS) system, the continuation of MNA and the sampling of recovery well RW-1, as well as the installation of one recovery well, two monitoring points, recovery well development, overburden aquifer pumping and reinjection tests. ' 2 i Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts ' On April 28, 2005, a Phase V Remedy Operating Status (ROS) Opinion was submitted with a Substantial Hazard Evaluation to the MassDEP. Inspection and Monitoring Reports for Phase V ' ROS Reports were submitted on November 1, 2005, May 1, 2006, November 2, 2006, May 3, 2007, November 1,2007,and May 1, 2008. ' 10 INSPECTION AND MONITORING REPORT 3.1 Description of the Type and Frequency of Activities Conducted: 310 CMR ' 40.0892(2)(a) The current active RA for this disposal site is MNA, documented through quarterly ' groundwater sampling and monitoring. As stated previously, AS/SVE remedial actions were conducted between March 2003 and July 2005 while GWPT actions were conducted between May 3,2006 and November 8,2007. ' 3.1.1 AS/SVE aeration The AS/SVE system was deactivated in July of 2005 due to an asymptotic decline in extracted volatile organic compounds (VOCs) with the SVE airstream and the declining concentrations present in groundwater within the radius of influence of the AS/SVE system. At the time of ' deactivation all COCs in the zone of influence of the AS/SVE were below GW-1 standards. To date, there has not been any rebounding of concentrations of COCs in groundwater requiring the system to be restarted. ' Since the Motiva and Mobil AS/SVE systems were inactive during the reporting period, no O&M visits were performed. 3.1.2 GWPT System Operation The GWPT system was shut down on November 8, 2007 due to consistently low levels of COCs ' in the monitoring wells. To date, there has not been any rebounding of concentrations of COCs in groundwater requiring the system to be restarted, however, the GWPT system is being maintained as fully functional. ' Since the Motiva and Mobil AS SVE systems were inactive during the reporting/ Y P gperiod no O&M visits were performed. Historic GWPT system data is summarized in Table 5. 3.1.3 Groundwater Sampling and MNA ' As stated above, the remaining RA for this disposal site is MNA documented through quarterly groundwater sampling and monitoring. On May 15-16, 2008, and August 18, 2008 Sovereign conducted personnel collected groundwater samples from select monitoring wells at the disposal site. During each event, ' depth to water was measured from top of casing and a minimum of three well volumes were purged prior to collecting groundwater samples. Groundwater samples were submitted to 3 Inspection and Monitoring Report for Phase p g p se V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts Accutest Laboratories of Marlborough, Massachusetts in accordance with chain of custody procedures for analysis of: ' • Volatile petroleum hydrocarbons (VPH) An electronic water level meter was used to measure depth to water (DTW) and/or non- aqueous phase liquid (NAPL) with an accuracy of±0.01 feet. A YSI multi-meter was utilized to measure the following field parameters: conductivity, temperature, oxidation/reduction ' potential (ORP), dissolved oxygen (DO), and pH in each monitoring well. The results of groundwater sampling and field measurements are summarized in Tables 1 through 3. Refer to Attachment A for copies of the laboratory analytical reports. ' 3.2 Data: 310 CMR 40.0892(2)(c) ' Overall, COC concentrations measured in groundwater samples collected from monitoring wells located at the disposal site are generally decreasing and/or stable. ' On May 15-16, 2008 a groundwater sampling event was conducted as part of the quarterly groundwater monitoring program. During this groundwater sampling event, 15 monitoring wells were sampled for VPH and gasoline oxygenate analysis. Only groundwater sampled from monitoring well MW-29(68) contained concentrations of MTBE above applicable Method 1 GW- 1/3 standards. Out of the 15 monitoring wells sampled, groundwater sampled from 11 monitoring wells contained COC concentrations below laboratory detection limits. MTBE was ' present above laboratory detection limits, but below applicable GW-1/3 standards, in monitoring wells MW-25(72), MW-26(72), MW-32(55), and MW-35(53). Benzene was present above laboratory detection limits, but below GW-1/3 standards in monitoring well MW-29(68). ' No other COCs were detected in groundwater sampled during the May 15-16, 2008 sampling event. During the August 18, 2008 groundwater sampling event 18 monitoring wells were sampled for VPH analysis. Only groundwater sampled from monitoring well MW-29(68) contained concentrations of MTBE above applicable Method 1 GW-1/3 standards. Out of the 18 monitoring wells sampled, groundwater sampled from 13 monitoring wells contained COC concentrations below laboratory detection limits. MTBE was present above laboratory detection limits, but below applicable GW-1/3 standards, in monitoring wells MW-19(55), MW-25(72), MW-35(53), and RW-101. C9-C12 aliphatic fractions and C9-C10 aromatic fractions were present above laboratory detection limits,but below GW-1/3 standards in monitoring well RW-101. No other COCs were detected in groundwater sampled during the August 18,2008 sampling event. ' 4.0 MCP DATA QUALITY REVIEW ' In accordance with Sections 310 CMR 40.0017 and 310 CMR 40.0191 of the MCP, a Data Usability Assessment is now required to more formally document that data is scientifically valid and defensible, and of a sufficient level of precision and accuracy and completeness to ' support "Presumptive Certainty'. Pursuant to 310 CMR 40.0191 of the MCP, the analytical data used to support this Phase V Remedy Operation Status Inspection and Monitoring (ROS I&M) Report was reviewed utilizing procedures outlined in MassDEP's Compendium of Qualihj 4 Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts Assurance/Quality Control (QA/QC) Requirements and Performance Standards or Selected Analytical q f f J Methods (CAM) (WSC-02-320.June 18, 2003). ' As discussed previously, field sampling, QA/QC requirements and laboratory testing and QA/QC procedures are consistent with the CAM presumptive certainty requirements ' regarding the data quality and/or demonstrate compliance with the Remedial Action Performance Standards (RAPS) set forth in 310 CMR 40.0191 of the MCP. In addition, the data utilized and relied upon in this ROS I&M Report was evaluated per the guidance set forth by MassDEP WSC Policy #07-350 MCP Representativeness Evaluations and Data Usabilihj Assessments of September 19, 2007. ' 4.1 Project Data Quality Objectives 4.1.1 Field Data Collection ' Evaluation of the field component of the data quality objectives includes the consideration of sample collection techniques and potential issues arising from such techniques including equipment cross-contamination, proper field selection of sampling points (i.e. groundwater sample collection from disposal site monitoring well network), appropriate sampling containers, and the proper handling and management of samples collected while en-route to the laboratory. For data relied upon for this report: • All field notes were reviewed for sampling methodology, notations on sample ' collection, sample preservation and handling, and deviations from the scope of work (i.e. weather, sample point conditions, and/or inability to access sample points), as applicable. Based upon a review of field notes and Chains-of-Custody, no concerns are ' noted. • All samples were collected using properly decontaminated equipment. Based upon a review of field notes,no decontamination concerns are noted. ' • A review of laboratory analytical receipt logs document that all samples were received properly preserved, within holding time and at the appropriate chilled temperature. No exceptions were noted. 4.2 Presumptive Certainty and CAM Compliance ' In accordance with the WSC #07-350, CAM compliant data are of known accuracy, precision and sensitivity and therefore should not require an Analytical Data Usability Assessment. The CAM provides the regulated community with a compilation of recommended laboratory ' procedures (MCP Analytical Methods) for the most common constituents of concern (COCs) that may be used to support MCP Response Actions. These procedures include detailed method-specific QA/QC requirements and performance standards for achievement of a Presumptive Certainty status. Two types of data were evaluated to support the conclusions presented in this ROS I&M: data collected in accordance with CAM guidance (CAM Compliant) and CAM Non-Compliant data. Accordingly, this evaluation of data usability considers these two data sets separately. 5 ' Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts 4.2.1 CAM Complaint Data ' Based upon a review of laboratory data analyzed in accordance with CAM and included in this I&M report, each laboratory report for the samples from the May 15-16, 2008 and August 18, 2008 sampling events were determined by the laboratory to meet the CAM for VPH and ' gasoline oxygenate analysis. Therefore, Presumptive Certainty was achieved for both samples analyzed by these methods. Sampling events that met Presumptive Certainty are listed below: • Groundwater sampling events (May 15-16, 2008;August 18,2008) The following QC performance standard was not met for the select laboratory analytical suites ' summarized for this report. Sample Date Field Sample ID Parameter/Comment Potential ' Lab Report Bias May 15-16,2008 Batch ID MSG3306 The results for all analyte-list None Accutest compounds/elements for the specified M73538 method was not reported 4.2.2 CAM-Non Compliant Data There was no CAM Non-Compliant Data during this reporting period. 5.0 DATA USABILITY ASSESSMENT CONCLUSIONS For these samples, Sovereign reviewed potential data usability issues with a potential to affect ' data quality in the data described for the time periods indicated above. No major QA/QC issues were reported by the laboratory that will affect data usability for MCP decision-making. No data was discarded due to QA/QC issues. ' 6.0 SIGNIFICANT MODIFICATIONS SINCE SUBMITTAL OF PRECEDING I&M REPORT:310 CMR 40.0892(2)(B) No modifications were initiated during this reporting period. 7.0 CONDITIONS AND/OR PROBLEMS AFFECTING REMEDIAL ACTION PERFORMANCE: 310 CMR 40.0892(2)(D) There were no conditions or problems affecting the remedial action performance during this ' reporting period. 8.0 MEASURE TAKEN TO CORRECT CONDITIONS AND/OR PROBLEMS:310 CMR ' 40.0892(2)(D) There were no measures taken to correct conditions or problems affecting the remedial action performance. ' 6 ' Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts 9.0 EVALUATION PERFORMANCE OF THE REMEDIAL ACTION Concentrations of COCs are generally decreasing and/or stable in all monitoring wells. Of the 80 wells located at the disposal site the following monitoring well is above GW-1 standards: Monitoring COC Measurement above Well standards MW-29(68) MBTE 20.5 µg/L Based on the historic groundwater information and the results of the May 15-16 and August gust 18 2008 field events,reactivation of the GWPT system is not anticipated as data suggests there is ' little benefit for continuing system operation. Evaluation of groundwater COCs will continue in order to determine if reactivation of the systems is necessary in the future. Groundwater sampling will continue on a quarterly schedule. ' 10.0 PROJECTED SCHEDULE Phase V ROS reports will be submitted to the MassDEP in accordance with the schedule set forth in 310 CMR 40.0892 of the Massachusetts Contingency Plan (MCP) (every six months). Activities planned for the next monitoring period include the following: Groundwater g November Sampling p o ember 2008, and February 2009 Inspections and Monitoring Report April 28,2009 ' 11.0 PUBLIC INVOLVEMENT ' In accordance with public involvement activities as required by 310 CMR 40.1403 of the MCP, notices of the availability of this I&M Report have been forwarded to the Town of Barnstable Public Health Division, and the Barnstable Water Supply Division. As required by 310 CMR 40.1403 10 , third party property owners with wells located on their ( )ro) p �' p p �' property,which have been sampled as a result of the Phase V ROS activities, have been notified ' in advance of the sampling and provided the sample analytical results. The following individuals or entities received such notifications during this 6-month monitoring period: • Prime 123,LLC, 1140 Iyannough Road, Hyannis,MA 02601 • Festival of Hyannis,3333 NY Hyde Park, New Hyde Park,NY 11042 • The Wilder Companies Attn: Mary Ellen Cunha 800 Boylston Street Suite 1300, Boston ' MA 02199 • Mr. Hans Keijser,Town of Barnstable,Water Supply Division,47 Old Yarmouth Road, Hyannis, MA 02601 ' • Ms. Donna Z Miorandi,Town of Barnstable, Public Health Division,200 Main Street, Hyannis,MA 02601 • Town of Hyannis,Town Engineer,367 Main Street,Hyannis, MA 02601 Copies of all public involvement correspondence are included in Attachment B. 7 ' Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts ' FIGURES 4' I �.< ads 5 y'�"x'�� r���. sy `�..J' �` y�.£.�'°' ��✓�✓ a,.,.f � € vJ �x ��s ¢"z''' ,a��; 3 z� �. r x. i,. •a f � 9 k :3 � � f Sk .ate. '`�• � _ ,_... T �� � a a i. `�,� � , ice r,� � i $ . ' ...0 .,... ��' �zz MA 7 � � SITE LOCATION � �k Y r kk �p F R Z g i "" ,SOVEREIGN CONSULTING INC. Reference: Hyannis, MA Quadrangle- USGS 1988 FIGURE 1 Contour Interval = 3 meters SITE LOCATION MAP Former Texaco Service Station UTM 19 391208E, 4614197N 1140 Iyannough Road, Hyannis, MA Sovereign Scale(approx.) Job No. 1"= 1000' EQ711 To �RIO O ✓ l5 \\ � `I / ` 1 1 \ 'zf £1 f U �, • iy 1 `/ "f;j �„ �►' {(b R�0 sfi�ll ,:. ? �, d .O rs,..],W j� '; err �,'' �•" q� '�. �,a T. .,,�., �,' - 1 r _,• � /...: �' • - ., � � � L� �^' i l .. ��'""�, it�! xp]I 1°�-' `,✓ -a /fir-o i s 1 s, .�I O } -Ara ps "�,. \ - �' / ref• ►A.' () __ a A x; M1^ - 10..1.f!)1 J+� B _.. ® � �,rD � -' � "°"° _]•Imo, Ld IK 77, ly A N QO ] \r V Q � FIGUIca RE 2 I / SITE PLAN ' ) FORMER SHELL—BRANDED SERWCE STATION LOCATED AT KEr 1140 ►YANNOUGH ROAD HYANNIS. MASSACHUSETTS ® VAPOR EXTRACTION WELL � TEMPORARY MONITORING WELL — LOT BOUNDARY,LINE 9/4/02 GROUNDWATER CONTOUR FOR SHALLOW SCREENED DEPTH PREPARED FOR O AIR SPARGE WELL • MAtwgLE — BIALDRK',LNK NOTE:NW-UNK 5 A YONffORDK;WELL O 120 9 MONITORING WELL ♦ MANHO E SURFACE ELEVATION CONTOUR(FEET) - 9/4/02 GROUNDWATER CONTOUR FOR 04TEMIEDIATE SCREENED DEPTH OBSERVED IN THE SUBJECT:AREA AND IS m MOTIVA ENTERPRISES LLC UTU" NOT PART OF THE SITE WELL NETWORK Approzimote Stole AIAW�� NRAW�A,dD ® CONE PENETROMETER LOCATION ® CATCH BASIN .-- EDGE OF SURFACE WATER .... 9/{/02 GROUNDWATER CONTOUR FOR DEEP SCREENED DEPTH • RECOVERY WELL Q IRRIGATION WELL 4 ' ]INJECTION WELL • PROPOSED SO4 -SOVEREIGN CONSULTING INC,905B SOUTH MAIN STREET r MANSFIELD,MA 02048 1I TEL:1508)339-3200 FAX(508)339-3248 _ 1 1 • � MASS � �� �1 I Mrs ®RRIN qns�N wf 'o VONfflal off, :.. a ® ®®•�� Q AON A IN PIIM ; .-. Nh Ll Mi . ` '` ' RIO a . "�MORIN IW MON OR 14 ON EVERSON R. WON MMW I �• 111 - • • - 11 : ' Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts I 1 1 ' TABLES TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH . Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA ...._ _.. Ethyl- Total Dissolved Ethylene CS-CB C9-C12 C9-C10 Naphtha- IX m Naphth a- MethodBenzene Toluene benzene X lenes BT MTBE Lead Dibmid Ali hatics Ali hatics Aromatics ene Standa (BP(L) (uq(L) (ug/l.) (ng/L) (ng/L) (ugfl.) (nen) (nfl) 0.0.) 0.0) 00.) (re^) GW-1 5 1,000 700 10,000 N/A 70 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 11000 5,000 1,000 G W-3 10,000 40,000 5 000 500 N/A 50,000 10 50,000 50,000 20,000 50,000 20,000 Well Data Usability Sample Groundwater Corrected °� �`„ ' i� � � r y �;. � �iM �� �'� � � TOC EIev. Assessment Bias Date Depth(ftl GW Elev.(ft) �,ux==, �� e ,3. o?:� ..,.. i,'t°• .��� .� -° "b'. - ���• 4. AS-1 4/4/2001 32.42 32.92 15 15.6 <5 33.8 59.4 6.5 - - 91.3 <50 <50 <5 (GW-1,GW-3) 8/16/2001 32.29 33.05 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 TOC Elev. 6/12/2002 32.51 32.83 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 65.34 5/22/2008 Could not locate INJ-1 6/3/2004 22.23 33.17 <1.0 <1.0 <1.0 <1.0 ND <1.0 - - - (GW-1,.GW-3) 7/21/2004 22.56 32.84 - - - - - - - - - - TOC El.,. 10/4/2004 22.55 32.85 <0.50 <1.0 <7.0 <1.0 ND <1.0 - - - 55.90 10/19/2005 NM NM <2.0 <2.0 <2,0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 IW-1 5/13/2002 NM NM <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 (GW-1,GW-3) 10/19/2005 NM NM <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 TOC Elev. NSVD 1,W-1 6/4/1999 30.13 34.75 418.0 2,700.0 435.0 2,747.0 6,300.0 2,060.0 - - 1,040.0 <1000 <1000 77.4 (GW-1,GW-3) 10/12/2000 32.32 32.56 371.0 1,090.0 485.0 2,243.0 4,189.0 3,800.0 - - 757.0 4,890.0 2,470.0 90.0 TOC Elev. 4/4/2001 31.93 32.95 199.0 376.0 257.0 1,141.0 1,973.0 889.0 - - <100 407.0 1,130.0 14.8 64.88 8/16/2001 32.82 32.06 116.0 364.0 162.0 810.0 1,452.0 1,770.0 - - <250 <250 747.0 33.9 12/4/2001 3CO2 30.86 42.3 140.0 63.8 274.0 520.1 769.0 - - <100 181.0 320.0 <10 5/1/2002 32.78 32.10 14.2 48.0 22.0 67.5 151.7 637.0 - - <50 <50 90.2 <5 6/12/2002 32.04 32.84 14.4 71.7 28.7 106.2 221.0 604.0 - - 174.0 <50 128.0 <5 1/13/2003 32.35 32.53 8.1 14.3 19.3 38.1 79.8 570.0 - - <50 <50 69.3 <3.0 4/30/2003 28.63 36.25 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 150 <50 <3.0 7/24/2003 29.33 35.55 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 10/28/2003 30.90 33.98 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 1/12/2004 30.53 34.35 <2 <2 <2 <2 ND <2 - - <50 60 <50 <3 3/25/2004 30.60 34.28 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 7/21/2004 1 30.68 34.20 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - <50 <50 <50 <3.0 MW-1A 12/4/2001 34.43 31.10 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 (GW-1,GW-3) 5/l/2002 33.57 31.96 <5 <5 <5 <10 ND <5 - _ <50 <50 <50 <5 TOC Elev. 6/12/2002 3288 32.65 <5 <5 <5 <10 ND <5 - <50 <50 <50 <5 65.53 3/22/2007 29.82 35.71 - - - " 8/28/2007 30.65 34.88 - - - - - - - - - MW-2 - 6/4/1999 29.93 34.62 <5 <5 <5 Qp ND <5 - - <100 <100 <100 <5 (GIN-1,GW-3) 10/12/2000 32.11 32.44 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 TOC Elev. 4/4/2001 32.55 32.00 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 64.55 8/16/2001 31.50 33.05 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 - <50 <50 <5.0 12/4/2001 33.31 31.24 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 5/l/2002 32.40 32.15 <5 <5 <5 <10 ND 20.4 - - <50 <50 <50 <5 1/13/2003 32.01 32.54 <0.50 <1.0 <1.0 <1.0 ND 3.4 - - - None 5/22/2008 29.46 35.09 - - - - Page 1 of 17 TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene C5-C8 C9-Cl2 C9-Clo Naphtha- Method1 Benzene Toluene benzene X lens BTEX MTBE Lead Dibromide Ali hatics Ali hatics Aromatics lene Standards (AWL) (pg/L) (p8/L) (n L) _ (ug/L)-- ("9/L) (n ) (n ) ___(uS/�.l__.. ___WIL) (uv/L) (us/L) GW-1 5 1,000 700 10,000 N/A 70 15 0.02 300 4,000 700 140 GW-2 IL 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 1,000 51000 1,000 GW-3 30,000 40,000 51000 500 N/A 50,000 10 50,000 50,000 20,000 50,000 20,000 Well Data Usability Sample Groundwater Corrected *\ 1 ;: TOC Elev. Assessment Bias Date Depth(ft) GW Elev.(ft) �' ,� i \ r,� ,� \ ",�„ NM-ZA 4/4/2001 33.64 32.85 524.0 92.0 147.0 251.0 1,014.0 5,340.0 - - <50 142.0 389.0 43.3 (GW-1,GW-3) 8/16/2001 33.52 32.97 17.1 <5.0 <5.0 <10.0 17.1 364.0 - - <50 <50 <50 <5.0 TOC Ele, 12/4/2001 35.32 31.17 14.1 <5,0 <5.0 <10.0 14.1 214.0 - - <50 <50 <50 <5.0 66.49 5/1/2002 34.50 31.99 122.0 <5 <5 11.0 133.0 2,700.0 - - <50 <50 82.5 11.3 6/12/2002 33.80 32.69 39.7 <5 <5 <10 39.7 1,140.0 - - <50 <50 <50 <5 8/15/2003 31.29 35.20 <1.0 <1.0 <1.0 <1.0 ND 1.4 - - - - - - 7/11/2005 29.66 36.83 <2.0 <2.0 <2.0 <4.0 ND <1.0 <50 <50 <50 <3.0 10/19/2005 30.84 35.65 <2.0 <2.0 <2.0 14.0 ND <1.0 - - <50 <50 <50 <3.0 1/23/2006 30.20 36.29 <1.00 <1.00 <1.00 <3.00 ND <1.00 <100 <100 <100 <5.00 10/18/2006 30.85 35.64 <1.00 <1.00 <1.00 <3.00 ND <1.00 - - <100 <100 <100 <5.00 3/22/2007 29.63 36.86 - - - - - - - 8/28/2007 31.51 34.98 - - - - - - - - MW_3A 4/4/2001 32.48 32.84 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 6.1 (GW-1,GW-3) 8/16/2001 32.35 32.97 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 TOC Elev. 12/4/2001 34.12 31.20 <5.0 <5.0 <5.0 <10.0 ND 50.6 - - <50 <50 <50 <5.0 65.32 5/1/2002 33.35 31.97 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 6/12/2002 32.63 32.69 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 1/13/2003 32.85 32.47 <0.50 <1.0 <1.0 <1.0 ND 2.8 - - - - - - 8/28/2007 30.37 34.95 - - - - - - - - - - MW4 6/4/1999 30.11 34.73 <11000 <1,000 <1,000 Q1000 ND 139,000.0 - - <20,000 <20,000 <20,000 <1,000 (GW-1,GW-3) 10/12/2000 32.31 32.53 <5 <5 <5 <10 ND 2,770.0 - - <50 <50 <50 <5 TOC Ele, 4/4/2001 31.92 32.92 <5.0 <5.0 <5.0 <10.0 ND 41.7 - - <50 <50 <50 <5.0 64.84 8/16/2001 31.82 33.02 <5.0 <5.0 <5.0 <10.0 ND 12.0 - - <50 <50 <50 <5.0 12/4/2001 33.61 31.23 <5.0 <5.0 <5.0 <10.0 ND 15.2 - - <50 <50 <50 <5.0 6/12/2002 32.06 32.78 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 7/24/2003 29.38 35.46 <2.0 <2.0 <2.0 1 <4.0 ND <2.0 - - <50 BO <50 <3.0 MW-5 6/4/1999 29.71 34.76 22.0 <5 <5 5.2 27.2 510.0 - - <100 <100 <100 <5 (GW-1,GW-3) 10/12/2000 31.57 32.90 1,320.0 5,130.0 550.0 2,434.0 9,434.0 23,400.0 - - <50 2,580.0 1,820.0 120.0 TOC El- 4/4/2001 31.94 32.53 508.0 2,570.0 384.0 2,014.0 5,476.0 26,000.0 - - <100 821.0 1,160.0 60.0 64.47 8/16/2001 31.43 33.04 423.0 2,500.0 343.0 1,938.0 5,204.0 12,500.0 - - <2000 <2000 <2000 <200 12/4/2001 33.20 31.27 2,260.0 10,000.0 1,390.0 7,690.0 21,340.0 46,900.0 - - <500 4,400.0 4,220.0 270.0 _ 5/1/2002 32.42 32.05 1,520.0 10,400.0 2,000.0 11,540.0 25,460.0 36,000.0 - - <2500 <2500 7,730.0 540.0 6/12/2002 31.71 32.76 2,000.0 11,200.0 1,500.0 8,530.0 23,230.0 43,400.0 - - 3,770.0 <2500 4,970.0 323.0 1/13/2003 31.95 32.52 203.0 1,360.0 743.0 4,100.0 6,406.0 6,690.0 - - <500 <500 4,060.0 211.0 1/12/2004 30.12 34.35 <2 <2 <2 <2 ND 10.0 - - <50 <50 <50 <3 3/25/2004 30.20 34.27 <2.0 <2.0 <2.0 <4.0 ND 59.3 - - <50 <50 <50 <3.0 7/21/2004 30.31 34.16 <0.50 <1.0 <1.0 <1.0 ND 1.0 - - <50 <50 <50 <3.0 < <4.0 ND <1.0 - - <50 <50 <50 <3.0 3 2 2005 29.75 34.72 <2.0 2.0 <2.0 / / 7/11/2005 27.65 1 36.82 <2.0 <2.0 c2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 10/18/2006 weB destroyed Page 2 of 17 TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissntvod Ethylene 1 C5-C8 C9-C12 C9-00 Naphtha- Method1 Benzene Toluene benzene X lenes BTEX MTBE Lead Dibromide Ali hatics Ali hatics Aromatics lene Standards OWL) I (p6/L) (p8/L) (vP/L) (p8(L) OWL) (ug(l) (W) IptJL1 (116/1-) (PWL) (p6(L) G1V-1 5 1A00 700 IU,1881 N/A 70 15 0.02 300 4,000 700 140 GW-2 2A00 50,000 20,000 91000 N/A 50,000 NE 2 31000 1,000 5,000 11000 GW-3 10,000 40A00 5,000 500 N/A 50,000 10 50,OW 50,000 20,000 50,000 20,000 Well Data Usability Sample Groundavater Corrected "" TOC Elev. Assessment Bias Date Depth(R) GW Elev.(k) _:. „„ C.� 1 � `' •� E 'q,,y' �vsi'19.p4*�`, ik"dwl .`4 ,r - k j MW-6 6/4/1999 30.01 34.74 <25 <25 <25 <50 ND 4550.0 - - <500 <500 <500 <25 (GW-1,GW-3) 10/12/2000 32.20 32.55 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 TOC Elev. 4/4/2001 32.83 31.92 114.0 6.2 5.5 <10.0 125.7 1A00.0 - - <50 <50 97.0 <5.0 64.75 8/16/2001 31.76 32.99 <5.0 <5.0 <5.0 <10.0 ND 15.6 - - <50 <50 <50 <5.0 12/4/2001 33.53 31.22 15.6 <5.0 <5.0 <70.0 15.6 173.0 - - <50 <50 <50 <5.0 5/l/2002 32.70 32.05 51.4 <5 8.3 18.3 78.0 1,170.0 - - <50 <50 226.0 33.7 7/24/2003 29.25 35.50 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 10/28/2003 30.81 33.94 <2.0 <2.0 <2.0 <4.0 ND 2.9 - - <50 <50 <50 4.6 1/12/2004 30.41 34.34 <2 <2 <2 <2 ND 47.1 - - <50 <50 <50 <3 3/25/2004 30.49 34.26 <2.0 <2.0 <2.0 3.1 3.1 609.0 - - <50 <50 <50 <3.0 7/21/2004 30.57 34.19 <0.50 <1.0 <1.0 <7.0 ND <1.0 - - <50 <50 <50 <3.0 3/2/2005 30.06 34.69 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <.50 <3.0 7/11/2005 27.90 36.95 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 MW-9 6/4/1999 31.04 34.75 3,380.0 22,800.0 2,620.0 18,070.0 46,870.0 IOA00.0 - <5000 <5000 10,800.0 328.0 (GW1,CW-3) 10/12/2000 32.23 33.56 2,750.0 15,800.0 2A30.0 15,380.0 36,360.0 2,830.0 - - 12,300.0 7A00.0 19A00.0 1,040.0 TOC Elev. 5/l/2002 33.70 32.09 1,620.0 16,800.0 2,950.0 17,760.0 39,130.0 6,880.0 - - 8,190.0 3,230.0 15AN.0 968.0 65.79 6/12/2002 32.97 32.82 1,540A 14A00.0 2A40.0 14A90.0 32,870.0 SA30.0 - - 8,970.0 6,590.0 12,600.0 832.0 1/13/2003 33.30 32.49 831.0 11500.0 2,290.0 14,140.0 28,761.0 7,570.0 - - 8A30.0 <500 11A00.0 831.0 7/24/2003 30.25 35.54 SA 399.0 143.0 1,735.0 2,282.4 2,350.0 - - 769.0 <50 3,580.0 105.0 10/28/2003 31.80 33.99 <4.0 717.0 589.0 6,040.0 7,346.0 262.0 - - 1,240.0 3,740.0 7,270.0 300.0 1/12/2004 31.42 34.37 <4 202.0 237.0 2,810.0 3,249.0 858.0 - - 552.0 <100 5,310.0 183.0 3/25/2004 31.45 34.34 <4.0 73.8 217.0 2,610.0 2,900.8 82.1 - - 466.0 <100 4,680.0 196.0 7/21/2004 31.50 34.29 <2.0 23.2 87.7 1,080.0 11190.9 3.0 - - 344.0 810.0 3,240.0 104.0 10/4/2004 31.81 33.98 <2.0 196.0 172.0 1,494.0 1,862.0 <2.0 - - 830.0 4,440.0 4,150.0 139.0 3/2/2005 31.00 34.79 5.1 526.0 250.0 1,647.0 2,428.1 <1.0 - - 975.0 875.0 3A00.0 148.0 7/11/2005 28.91 36.88 <2.0 218.0 116.0 735.0 1,069.0 <1.0 - - 363.0 321.0 580.0 32.3 10/19/2005 30.16 35.63 <2.0 174.0 202.0 1,036.0 1,412.0 <1.0 - - 458.0 1,280.0 1,720.0 87,5 4/19/2006 NM NM 1.1 215.0 264.0 1M8.0 1,868.1 <1.00 - - 721.0 1,980.0 1,680.0 177.0 10/18/2006 Destroyed_Replace<1w.0it0 MWAR _______ _ ___________________________ 4/11/2007 ___3016_____ _ _ NM _ <300____ ____ 0____--------130------- ----- ___- _____<_3__0_____------------- _-_____------ -------<_1_0_0------- -----<_7_0__0---- -------<__7_0_0-------------<_5__.0_0___-_ (CW-1,CW-3) 6/25/2007 29.92 NM <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 8/28/2007 31.66 NM <1.00 <3.00 <7.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 1/3/2008 32.94 NM <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 None 5/15/2008 31.04 NM <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-10 6/4/1999 30.39 35.40 <5 63.8 8.2 50.1 122.1 <5 - - <100 <100 <100 <5 (CW-1,GW,3) 10/12/2000 32.60 33.19 G5 <5 <5 <10 ND 27.2 - - 719.0 98.9 293.0 36.9 TOC Ele, 4/4/2001 32.96 32.83 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 100.0 9.5 <50 <50 <50 <5.0 <5.0 <5.0 <10.0 ND <5.0 65.79 8/16/2001 31.08 34.71 <5.0 - - 5/l/2002 33.04 32.75 <5 <5 <5 <10 ND <5 - - <50 1 <50 <50 <5 Page 3 of 17 TABLE SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene I C5-C8 C9-C12 C9-C10 Naphtha- Method I Benzene Toluene benzene X lenes BTEX MTBE Lead Dibmniido Ali hatics Ali hatics Aromatics lene Standards f (PS(L) (AWL) (u8/L) (p8/L)- W/L) (AS(L) (u8/1) (ug(l) (u8(L) (1+8/L) (NS/L) (uB/L) - - - - 10,000 N- - , -_/._ _ -_..._. Gyy_j 5 1,000 700 A 70 15 0.02 300 4,000 700 1 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 1,000 5,000 1,000 GW-3 10,000 40,000 5,000 Soo N/A 501000 10 50,000 50,000 20,000 50,000 20,000 Well Data Usability Sample Groundwater Corrected c TOC Elev. Assessment Bias Date Depth(W GW Elev.(ft) ' MW-11 4/4/2001 32.96 32.83 <5.0 <5.0 <5.0 <10.0 ND 7.0 - - <50 <50 <50 5.0 (GW-1,GW-3) 8/16/2001 32.88 32.91 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 TOC Elev. 12/4/2001 34.72 31.07 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 65.79 5/1/2002 33.83 31.96 <5 <5 <5 <10 ND 102.0 - - <50 <50 <50 <5 6/12/2002 33.12 32.67 <5 <5 <5 <10 ND 21.9 - - <50 <50 <50 <5 7/11/2005 29.05 36.74 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 13.0 1/23/2006 29.06 36.73 <1.00 <1.00 <1.00 <3.00 ND <1.00 - - <100 <100 <100 <5.00 4/19/2006 30.04 35.75 <1.00 13.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 14.6 10/18/2006 31.14 34.65 <1.00 <3.00 <1.00 <6.00 ND 11.00 - - <1UU <lU0 <1UU <5.UU 3/22/2007 30.18 35.61 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 6/25/2007 29.20 36.59 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <700 <100 <5.00 8/28/2007 31.03 34.76 - - - - _ _ - - - - 5/22/2008 30.13 35.66 - - - - _ - - - - NM-12 4/4/2001 32.43 32.99 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 (GW-1,GW-3) 8/16/2001 32.36 33.06 <5.0 15.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 TOC Elev. 12/4/2001 34.13 31.29 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 65.42 5/1/2002 33.30 32.12 <5 <5 <5 <10 ND <5 - - <50 <50 <30 <5 MW-13 4/4/2001 31.67 33.03 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 (GW-1,GW-3) 8/16/2001 31.60 33.10 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 TOC Elev. 12/4/2001 33.42 31.28 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 64.70 5/1/2002 32.50 32.20 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 MW-14 25) 4/4/2001 33.74 32.88 <5.0 <5.0 <5.0 <10.0 ND <5.0 - <50 <50 <50 <5.0 (GW-1,GW(3) 8/16/2001 33.59 33.03 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 TOC Elev. 12/4/2001 35.33 31.29 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 2 5 1/2002 3 4.57 32.05 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 66.6 / < 6/12/2002 33.63 32.79 <5 <5 <5 <70 ND <5 - - c50 <50 <50 5 3/22/2007 30.91 35.71 - - - _ - - - - - 8/28/2007 31.66 34.96 - - - _ _ - I _ MW-14(55) 8/14/2002 34.81 31.58 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 (GW.1,GW-3) 9/17/2002 35.15 31.24 <2 <2 <2 <4 ND <2 = - <50 <50 <30 <3 TOC Elev. 3/22/2007 30.63 35.74 66.39 8/28/2007 31.33 35.06 - - - - - - - - - MW-14(70) 5/1/2002 34.31 32.07 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 (GW-1,GW-3) 6/12/2002 33.57 32.91 <5 <5 <5 <10 ND <5 - _ <50 <50 <50 <5 TOC Elev. 3/22/2007 30.65 35.73 - - - - 66.38 8/28/2007 30.21 36.17 - - - _ - MW-14(90) 5/l/2002 37.68 28.70 <5 <5 <5 QO ND <5 - - <50 <50 <50 <5 (GW-1,GW-3) 6/12/2002 36.51 29.87 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 TOC Elev. 3/22/2007 30.09 36.29 66.38 MW-15(20) 12/4/2001 34.20 31.11 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - -<50 <50 <50 <5.0 (GW-1,GW-3) 5/1/2002 33.49 31.82 <5 <5 <5 <10 ND <5 - - <So <50 <50 <5 TOC Elev. 3/22/2007 29.66 35.65 - - - _ " 65.31 MW-16(20) 12/4/2001 34.12 31.07 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 (GW-1,GW-3) 5/l/2002 33.36 31.83 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 TOC Elev. 3/22/2007 29.54 35.65 - - _ - 65.19 8/28/2007 30.32 34.87 Page 4 of 17 TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene C5-C8 C9-C12 C9-C30 Naphtha- Methodl Benzene Toluene benzene X lenes BTEX MTBE Lead Dibromid Ali hatics Ali hatics Aromatics lene Standards (P&(L) (u8/L) (18(-) W/L) (NP(-) (I'8(L) (ug/1) _(u&ll) (NP(-) (NP(-) (USR-) (N ) �1N-1 5 11000 700 10,000 N/A 70 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 1,000 5'000 1,000 GW-3 10 000 40,000 5,000 500 N/A 50,000 10 50,000 50,000 20 000 50 000 20,000 Well Data Usability Sample Groundwater Cortec[ed � < � '.`..�..�. a " TOC Elev. Assessment Bias Date Depth(ft) GW Elev.(ft) \ �„ 0 1% MW-16(55) 12/4/2001 34.02 31.08 1,410.0 <50 <50 <100 1,410.0 11,500.0 - - a 1,830.0 <500 555.0 <50 (GW-1,GW-3) 1/3/2002 34.36 30.74 1,490.0 19.8 8.0 24.7 1,542.5 13,600.0 - - 454.0 330.0 560.0 37.3 TOC Elev. 5/1/2002 33.28 31.82 414.0 <5 <5 <10 414.0 4,280.0 - - <50 <50 122.0 <5 65.10 6/12/2002 32.54 32.56 190.0 <10 <70 <20 190.0 2,270.0 - - 137.0 <100 <100 <10 4/30/2003 29.33 35.77 <0.50 <1.0 <1.0 <1.0 ND 154.0 - - - - ' 7/24/2003 29.70 35.40 <2.0 <2.0 <2.0 <4.0 ND 29.1 - - <50 <50 <50 <3.0 10/28/2003 31.19 33.91 <2.0 <2.0 <2.0 4.7 4.7 2.6 - - <50 <50 57.8 8.4 1/12/2004 30.84 34.26 <2 <2 <2 <2 ND 2.1 - - <50 <50 <50 <3 10/19/2005 29.45 35.65 <2.Q <2.0 <70 <40 nin 256.0 �30 <3u 15U <3.0 10/18/2006 29.50 35.60 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 3/22/2007 29.44 35.66 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 6 25/2007 28.71 36.39 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 8/28/2007 30.21 34.89 Q.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 MW-16(90) 6/12/2002 33.95 31.28 Q.0 <1.0 <1.0 <1.0 ND <1.0 (GW-1,GW-3) 7/22/2002 33.60 31.63 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - TOC Ele, 3/22/2007 29.57 35.66 - - - - - - - 65.23 8/28/2007 30.30 34.93 - - - - - - - - - - - MW-17(20) 12/4/2001 35.52 31.29 <5.0 <5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 (GW-1,GW-3) 5/1/2002 34.80 32.01 <5 <5 <5 QO ND <5 - - <50 <50 <50 <5 TOC Elev. 6/12/2002 34.02 32.79 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 66.81 3/22/2007 31.10 35.71 - - - - - - 8/28/2007 31.84 34.97 - - - - - - - - - - MW-18(25) 5/1/2002 35.15 31.66 <5 <5 <5 <10 ND 26.8 - - <50 <50 <50 <5 (GW-1,GW-3) 6/12/2002 34.44 32.37 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 TOC Elev. 1/13/2003 34.66 32.15 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - 66.81 10/28/2003 33.20 33.61 <2.0 12.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 1/12/2004 32.82 33.99 <2 <2 <2 <2 ND <2 - - <50 <50 <50 <3 3/22/2007 31.41 35.40 - - - - - - - - 8/28/2007 32.21 34.60 - - - - - - - - - 5/22/2008 31.42 35.39 - - - - - - - - - MW-18(70) 5/1/2002 34.90 32.02 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 (GW-1,GW-3) 6/12/2002 34.28 32.64 <5 <5 <5 <10 ND <5 - - <50 <50 <50 <5 TOC Elev. 3/22/2007 31.20 35.72 - - - - - 66.92 8/28/2007 32.02 34.90 - - - - - - - - - 5/22/2008 31.20 35.72 - - - - - - - - - - MW-19(20) 6/12/2002 33.31 33.61 <1.0 <1.0 <1.0 <1.0 ND <1.0 (GW-1,GW-3) 7/22/2002 34.06 32.86 <0.50 <1.0 <1.0 <1.0 ND <1.0 TOC Elev. 3/22/2007 30.06 36.86 - - - - - 65.58 8/28/2007 30.86 36.06 - - - - - - - - - - Page 5 of 17 TABLE SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene C5-C8 C9-C12 C9-C10 Naphtha- Method 1 Benzene Toluene benzene X lenes BTEX MTBE Lead Dibromid Ali hatics Ali hatics Aromatics lene Standards (99/L) (991L) (#r/L) (pg/L) (pa/L) (pe/L) (.0) (u8/1) (ps(L) (ps/L) I WIL) (PY ) rW-1 5 1,OM 700 10,000 N/A 70 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 1,000 5,000 1,000 _ GW-3 101000 40,000 51000 500 N/A 50,000 10 50,000 50,000 20,000 50,000 20,000 Well Data Usability Sample Groundwater Corrected i � �\ TOC Elev. Assessment Bias Date Depth(ft) GW Elev.(ft) ..ez.� .�,ir �. MW-19(55) 6/12/2002 33.32 33.60 2.0 <1.0 <1.0 <7.0 2.0 638.0 - - - - - (GW-1,GW-3) 7/22/2002 34.06 32.86 <5.0 <5.0 <5.0 <10.0 NO 1,390.0 - - <50 <50 <50 <5.0 TOC Elev. 1/13/2003 33.30 33.62 249.0 <2.0 <2.0 2.8 251.8 3,040.0 - - <50 <50 <50 7.8 65.60 4/30/2003 30.11 36.81 132.0 <10 <10 <20 132.0 2,430.0 - - <250 <250 <250 <15 7/24/2003 30.43 36.49 27.0 1.1 1.4 8.3 37.8 776.0 - - - - - 10/28/2003 31.84 35.08 26.1 <2.0 <2.0 <2.0 26.1 442.0 - - 1/12/2004 31.43 35.49 50.9 <1 <1 <1 50.9 993.0 - - - - - 7/21/2004 31.74 35.18 <0.50 <1.0 <1.0 <1.0 NO 81.7 - - - - - <5.0 10/4/2004 31.75 35.17 <0.5 <1 <1 <1 NO_ 99.4 - - _ - 7/11/2005 29.05 37.87 <2.0 <2.0 <2.0 <4.0 NO 20.9 - - 150 <50 <50 <3.0 10/19/2005 30.02 36.90 <2.0 <2.0 <2.0 <4.0 NO 14.9 - - <50 <50 <50 <3.0 1/23/2006 29.45 37.47 <1.00 <1.00 <1.00 <3.00 NO <1.00 - - <100 <100 <100 <5.00 4/19/2006 30.02 36.90 <1.00 <3.00 <1.00 <6.00 NO 21.5 - - <100 <100 <100 <5.00 10/24/2006 30.30 36.62 <1.00 <3.00 <1.00 <6.00 ND 7.69 - - <100 <100 <100 <5.00 3/22/2007 30.05 36.87 <1.00 <3.00 <1.00 <6.00 ND 21.30 - - <100 <100 <100 <5.00 6/25/2007 29.20 37.72 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 8/28/2007 30.86 36.06 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 1/3/2008 31.98 34.94 <1.00 <3.00 <1.00 <6.00 ND 1% - - <100 <100 <100 <5.00 3/28/2008 30.84 36.08 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 5/15/2008 30.42 36.5 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 8/18/2008 1 31.50 35.42 <2.0 <2.0 <2.0 <4.0 ND 8.1 - - <50 <30 <50 <3.0 MW-19(90) 6/12/2002 33.45 31.88 <1.0 <1.0 <1.0 <1.0 ND 3.3 - - - - - - (GW-1,GW-3) 8/14/2002 34.78 30.55 <2.0 <2.0 <2.0 <4.0 NO <2.0 - - <50 <50 <50 <3.0 TOC EIe, 7/11/2005 31.60 33.73 <2.0 <2.0 <2.0 <4.0 NO <1.0 - - <30 <50 <50 <3.0 65.33 1/23/2006 32.54 32.79 <1.00 <1.00 <1.00 <3.00 NO <1.00 - - <100 <100 <100 <5.00 4/19/2006 31.14 34.19 <1.00 <3.00 <1.00 <6.00 NO <1.00 - - <100 <100 <100 <5.00 3/22/2007 30.12 35.21 - - - - - - - - - - 8/28/2007 30.16 35.17 - - - - - - - - MW-20(20) 6/12/2002 33.97 32.02 <1.0 11.0 <1.0 <1.0 NO <1.0 - - - - (GW-1,GW-3) 7/22/2002 34.75 31.24 <0.50 <1.0 <7.0 <1.0 NO <1.0 - - - - - TOC Elev. "1/13/2003 33.88 32.11 <0.50 <1.0 <1.0 <1.0 NO <1.0 - - - - - 65.99 3/22/2007 0.65 65.34 - - - - - - - - - - 8/28/2007 31.57 34.42 - - - - - - - - - - MW-20(55) 6/12/2002 33.91 32.02 31.6 <10 <10 <10 31.6 50,300.0 (GW-1,GW-3) 7/22/2002 34.69 31.24 16.3 <5.0 <5.0 <10.0 16.3 59,000.0 - - <50 <50 <50 <5.0 TOC EIev. 1/13/2003 33.82 32.11 18.3 <1.0 <1.0 <].0 18.3 46500.0 - - - - - - 65.93 4/30/2003 30.73 35.20 <25 <50 <50 <50 NO 13,900.0 - - - - - 7/24/2003 31.00 34.93 <20 <20 <20 140 NO 6,860.0 - - <500 <500 <500 <30 10/28/2003 32.45 33.48 <10 <l0 <0 11.5 11.5 5,810.0 - - <250 <250 <250 <15 1/12/2004 32.02 33.91 <2 <2 <2 <2 NO 22.7 - - <50 <50 <50 <3 3/25/2004 32.38 33.55 <2 <2 <2 <4 NO 330.0 - - <50 <50 <50 <3 7/21/2004 32.35 33.58 <2.5 <5.0 <5.0 <5.0 NO 1,440.0 - - - - - <25 10/4/2004 32.35 33.58 0.8 <1 <1 <1 0.8 345.0 - - - - - - 3/2/2005 31-90 34.03 <2.0 <2.0 <2.0 <4.0 NO 15.1 - - <50 <50 <50 <3.0 7/11/2005 29.63 36.30 <2.0 <2.0 <2.0 <4.0 NO 18.4 - - <50 <50 <50 <3.0 10/19/2005 30.63 35.30 <2.0 <2.0 <2.0 <4.0 NO 6.6 - - <50 <50 <50 <3.0 1/23/2006 30.08 35.85 <1.00 <1.00 <1.00 <3.00 NO 1.1 - - <100 <100 <100 <5.00 4/19/2006 30.65 35.28 <1.00 <3.00 <1.00 <6.00 NO 2.8 - - <100 <100 <100 <5.00 10/24/2006 30.90 35.03 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 3/22/2007 30.61 35.32 <1.00 <3.00 <7.00 <6.00 ND <3.00 - - - <100 <100 <100 <5.00 6/25/2007 29.91 36.02 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 8/28/2007 31.51 34.42 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - Q00 <100 <100 <5.00 1/3/2008 32.62 33.31 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 None 5/16/2008 31.08 34.85 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 8/18/2008 1 32.09 33.84 <2.0 <2.0 1 <2.0 1 <4.0 ND 1 <2.0 - - <50 �50 <50 <3.0 Page 6 of 17 TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Farmer Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene C5-C8 C9.C12 C9-C10 Naphtha- Method 1 Benzene Toluene benzene X lenes BTEX MTBE Lead Dibmmid Ali hatics Ali hatics Aromatics lene Standards WA) (µ8/L) (Pg/1.) WIL) OWL) (99/L) (ug/1) (ug(l) (pg/L) ("B/L) I (ue/L) W(L) G4N 1 5 1,000 700 10,000 N/A 70 15 0.02 3UU 4,UW 70U 140 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 1,000 5,000 1,000 GW-3 10,000 40,000 5,000 500 N/A 50,000 10 50,000 50,000 20,000 50,000 20,000 Well Data Usability Sample Groundwater Corrected TOC Elev. Assessment Bias Date Depth(k) GW Elev.(ft) °`;q .� .. �a .,, .� l. 'a � •'^ 's. .. �+�I�... :r.w• �� `�° ti•.�.. MW-20(90) 6/12/2002 35.02 31.05 <1.0 <7.0 <7.0 Q.0 ND 1.5 - - - - - (GW-1,GW-3) 7/22/2002 35.38 30.69 <0.50 <1.0 <1.0 <1.0 ND <1.0 TOC Elev. 3/22/2007 31.25 34.82 - - - - - - 66.07 8/28/2007 32.12 33.95 - - - - - - MW-21(20) 6/12/2002 32.94 32.43 Q.0 <1.0 <1.0 <1.0 ND <1.0 (GW-1,GW3) 7/22/2002 33.78 31.59 <0.50 <1.0 <1.0 <7.0 ND <1.0 - - - - TOCElev. 3/22/2007 29.82 35.55 - - - - 65.37 8/28/2007 30.76 34.61 - - - - - - - - MW-21(55) 6/12/2002 33.01 32.39 -1.0 <1.0 <1.0 <1.0 ND 80.3 (GW-1,GW-3) 7/22/2002 33.80 31.60 <5.0 <5.0 <5.0 <10.0 ND 128.0 - - <50 <50 <50 <5.0 TOC Elev. 1/13/2003 33.03 32.37 <0.50 <1.0 <1.0 <1.0 ND 19.0 - - - - - 65.40 4/30/2003 29.68 35.72 <0.50 <1.0 <1.0 <1.0 ND 5.6 - - - - - 7/24/2003 30.29 35.11 <0.50 4.0 <1.0 <1.0 ND 11.1 - - - - - - 10/28/2003 31.68 33.72 <0.50 <1.0 <1.0 <1.0 ND 1.9 1/12/2004 31.27 34.13 <0.5 <1 <1 <1 ND <1 - - - - - 3/22/2007 30.10 35.30 - - - - 8/28/2007 30.72 34.68 <1.00 <3.00 <1.00 <2.00 ND <3.00 - - <100 <100 <700 <5.00 1/3/2008 31.85 33.55 <1.00 <3.00 <1.00 <2.00 ND <3.00 - - <100 <100 <100 <5.00 3/28/2008 30.50 34.90 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 5/15/2008 30.14 35.26 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 8/18/2008 32.20 33.20 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-21(90) 6/12/2002 34.43 30.88 <1.0 <1.0 <1.0 <1.0 ND <1.0 (GlN-1,GW-3) 7/22/2002 33.95 31.36 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - TOCElev. 3/22/2007 29.80 35.51 - - - - - - - - - 65.31 8/28/2007 30.91 34.40 - - - - - - - - - MW-22(20) 8/14/2002 32.26 29.98 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 9/17/2002 32.57 29.67 <2 <2 <2 <4 ND <2 - - <50 <50 <50 <3 TOC EIe, 1/13/2003 30.92 31.32 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - ' 62.24 3/22/2007 27.71 34.53 - - - - - - - - 8/28/2007 28.47 33.77 - - - - - - - - - 5/22/2008 27.98 34.26 - - - - - - - - - - - MW-22(52) 8/14/2002 32.23 30.01 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 9/17/2002 32.57 29.67 <2 <2 <2 <4 ND <2 - - <50 <50 <50 <3 TOC Elev. 1/13/2003 30.88 31.36 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - - 62.24 3/22/2007 27.70 34.54 - - - - - - - - - 8/28/2007 28.43 33.81 - - - - - - - - - - 5/22/2008 27.98 34.26 - - - - - - - MW-23(20) 8/14/2002 28.27 29.92 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 9/17/2002 28.52 29.67 <2 <2 <2 <4 ND <2 - - <50 <50 <50 <3 TOC EIe, 3/22/2007 23.77 34.42 - - - - - - 58.19 8/28/2007 24.57 33.62 - - - - - - - - - - 5/22/2008 23.94 34.25 - - - - - - Page 7 of 17 w■ w■ ■w w w■ ■w ■w ww w ww w� ■w w■ ww w■ ■w ■■■ � w� TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl• Total Dissolved Ethylene C5-C8 C9-C12 C9-CY0 Naphtha Method 1 Benzene Toluene benzene X lenes BTEX MTBE Lead Dibmmid Ali hatics Ali hatics Aromatics le- Standards (u ) (N..P�-1_ (POL) (ug/Ll p�grt.) {I�en.) (ug/1) (ug/q (u6/L) (Nsft-) (WL) 6-9(L)GW-1 5 1,000 700 10,000 N/A 70 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 1,000 5,000 1,000 GW-3 10,000 40,000 5,000 500 N/A 50,000 10 50,000 50,000 20,000 50,000 200,000 Well Data Usability Sample Groundwater Corrected ` gll' �`� TOC El- Assessment Bias Date Depth(ft) GW Elev.(ft) ale_^ "� �� MW-23(52) 8/14/2002 28.27 29.97 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 ."<3.0 (GW-1,GW-3) 9/17/2002 28.57 29.67 <2 <2 <2 <4 NO <2 - - <50 <50 <50 <3 TOC Ele, 10/28/2003 25.53 32.71 <0.50 <1.0 <1.0 <1.0 NO <1.0 - - - - 58.24 1/12/2004 25.02 33.22 <0.5 <1 <1 <1 NO <1 3/25/2004 25.56 32.68 <0.5 <1 <7 <1 ND <1 - - - - - " 7/21/2004 25.42 32.82 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - <5.0 10/4/2004 25.58 32.66 <0.5 <1 <1 <7 ND <1 3/22/2007 23.81 34.43 - - - _ _ - 8/28/2007 24.61 33.63 - - - - - - - - - - 5/22/2W8 23.96 34.28 _ MW-24(10) 8/14/2002 17.74 29.88 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 9/17/2002 17.94 29.68 <2 <2 <2 <4 ND <2 - - <50 <50 <50 <3 TOC Elev. 1/13/2003 16.27 31.35 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - 47.62 7/21/2004 14.91 32.71 - - - - - _ - - - 1/20/2005 15.01 32.61 <0.50 <1.0 <1.0 <1.0 ND <1.0 3/22/2007 13.25 34.37 _ _ - _ _ _ 8/28/2007 14.10 33.52 - - - - I _ _ - - - - MW24(42) 8/14/2002 17.71 29.90 <2.0 <2.0 <2.0 <4.0 NO <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 9/17/2002 17.94 29.67 <2 <2 <2 <4 ND <2 - - <50 <50 <50 <3 TOC EIe, 1/13/2003 16.26 31.35 <0.50 <1.0 <1.0 <1.0 NO <1.0 - - - - " 47.61 7/24/2003 13.50 34.11 <0.50 <1.0 <1.0 <1.0 ND 56.2 - - - - - 10/28/2003 14.91 32.70 <0.50 <1.0 -1.0 <1.0 NO 14.1 - - - - - 1/12/2004 14.60 33.01 <0.5 <1 <1 <1 NO 6.8 3/25/2004 14.90 32.71 <0.5 <7 <1 <1 NO 3.9 - - - - - 7/21/2004 14.89 32.72 <0.50 <1.0 <1.0 <1.0 NO <1.0 10/4/2004 15.02 32.59 <0.5 <1 <1 <1 NO 1.4 1/20/2005 14.99 32.62 <0.50 <1.0 <1.0 <1.0 NO 10.1 - - - - - 3/2/2005 14.40 33.21 <2.0 <2.0 <2.0 <4.0 NO 4.4 - - <50 <50 <50 <3.0 7/11/2005 12.39 35.22 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 10/19/2005 13.31 34.30 <2.0 <2.0 <2.0 <4.0 ND 1.3 - - <50 <50 <50 <3.0 1/18/2006 12.60 35.01 <1.00 <3.00 <1.00 <6.00 ND 1.4 - <100 <100 <100 <5.00 4/19/2006 13.40 34.21 <1.00 <3.00 <1.00 <6.00 NO 2.0 - - <100 400 <100 <5.00 3/22/2007 13.24 34.37 - - - _ _ - - - - - 8/28/2007 14.11 33.50 <1.00 <3.00 <1.00 <6.00 NO <3.00 - - <100 <100 <100 <5.00 1/3/2008 15.11 32.50 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <700 <100 <5.00 3/28/2008 33.17 14.44 <2.0 <2.0 <2.0 <4.0 NO <2.0 - - <50 <50 <50 <3.0 None 5/15/2008 13.37 34.04 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 8/18/2008 14.57 33.04 <2.0 1 <2.0 1 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 Page 8 of 17 TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene CS-C8 C9-C12 C9-C10 Naphtha- Method1 Benzene Toluene benzene X lenes BTEX MTBE Lead Dibromid Aliphatic Ali hatics Aromatics lene Standards (OWL) (pg/L) (pg/L) (pg/L) (pg/L) (Ag/L) (ug/1) (.gn) (pg/L) (pg/L) (Ag/L) (Ag/L) GW-1 5 1.0no Inn ln,nm M/A 7n 15 0.02 300 4;000 700 140 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 11000 5,000 1,000 GW-3 10,000 40,000 51000 Soo N/A 50,000 10 50,000 50,000 20,OW 50,000 20,000 Well Data Usability Sample Groundwater Corrected ��s �\ ��< �, a' TOC Elev. Assessment Bias Date Depth(fti GW Elev.(ft) x ` �`:. ..`aka,. �.. �.K �=a MW-25(42) 8/14/2002 13.75 29.78 5.3 <2.0 <2.0 <4.0 5.3 599.0 - - 65.9 <50 <50 <3.0 (GW-1,GW-3) 9/17/2002 13.95 29.58 <2 <2 <2 <4 ND 96.5 - - <50 <50 <50 <3 TOC Elev. 1/13/2003 12.30 31.23 <0.50 <1.0 <1.0 <1.0 ND 2.3 - - - - " 43.53 4/30/2003 9.38 34.15 <0.50 <1.0 <1.0 <1.0 ND 3.8 7/24/2003 9.45 34.08 <0.50 <1.0 <1.0 <1.0 ND 1.9 - - - - - 10/28/2003 10.99 32.54 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - 1/12/2004 10.54 32.99 <0.5 <1 <1 <1 ND 4.3 3/25/2004 10.92 32.61 0.8 <1 <1 <l 0.8 75.8 7/21/2004 10.92 32.61 <0.50 <1.0 <1.0 <1.0 N D 24.9 - - - - - <5.0 10/4/2004 11.02 32.51 <0.5 <1 <7 <1 ND 7.1 - - - - - - 1/20/2005 10.98 32.55 <0.50 <7.0 <l.n <1.0 ND 11.0 - - - - 3/2/2005 10.34 33.19 <2.0 <2.0 <2.0 <4.0 ND 3.9 - - <10 <So <50 <3.0 7/11/2005 8.38 35.15 <2.0 <2.0 <2.0 <4.0 ND 583.0 - - <50 <50 <50 <3.0 10/19/2005 9.30 34.23 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 1/18/2006 8.67 34.86 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 4/19/2006 9.27 34.26 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 10/24/2006 9.47 34.06 <1.00 <3.00 <1.00 16.00 ND <1.00 - - <100 <100 <100 <5.00 3/22/2007 9.21 34.32 - - - - - - - - 8/28/2007 10.13 33.40 - - - - - - - - - 5/22/2008 9.41 34.12 - - - - - - - - - MW-25(72) 8/14/2002 13.80 29.75 <2.0 <2.0 <2.0 <4.0 ND 26.4 - - <50 <50 <50 <3.0 6 (GW-1,GW-3) 9/17/2002 13.98 29.57 <2 <2 <2 <4 ND 44. - - <50 <50 <50 <3 TOC Elev. 7/24/2003 9.47 34.08 3.0 <1.0 <I.0 <1.0 3.0 169.0 - - - 43.55 10/28/2003 10.99 32.56 4.0 <1.0 <7.0 <l.0 4.0 177.0 - - - - - - 1/12/2004 10.64 32.91 4.2 <1 <1 <1 4.2 330.0 7/21/2004 10.97 32.58 3.9 <1.0 <1.0 <1.0 3.9 371.0 - - - - - <5.0 10/4/2004 11.06 32.49 4.7 <1 <1 <l 4.7 418.0 - - - - - 1/20/2005 11.05 32.50 6.4 <1.0 <1.0 <1.0 6.4 373.0 - - - - - 3/2/2005 10.43 33.12 4.8 <2.0 <2.0 <4.0 4.8 575.0 - - <50 <50 <50 <3.0 7/11/2005 8.42 35.13 2.0 <2.0 <2.0 <4.0 2.0 412.0 - - <50 <50 <50 <3.0 10/19/2005 9.33 34.22 3.2 <2.0 <2.0 <4.0 3.2 503.0 - - <50 <50 <50 <3.0 1/18/2006 8.60 34.95 4.2 <3.00 <1.00 <6.00 4.2 672.0 - - <100 <100 <100 <5.00 4/19/2006 9.33 34.22 4.8 <3.00 <1.00 <6.00 4.8 671.0 - - <100 <100 <100 <5.00 10/24/2006 9.51 34.04 2.17 <3.00 <1.00 <6.00 2.17 333.0 - - <100 <100 <100 <5.00 3/22/2007 4.25 39.30 <3.00 <1.00 <1.00 <6.00 ND 97.9 - - <700 Q00 <100 <5.00 6/25/2007 8.34 35.21 <3.00 <1.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 8/28/2007 10.18 33.37 <3.00 <7.00 <1.00 <6.00 ND 89.6 - - <100 <100 <100 <5.00 1/3/2008 11.19 32.36 <3.00 <1.00 <1.00 <6.00 ND 38.3 - - <100 <100 < < 0 . 3/28/2008 NM NM <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <5300 <3.<50 None 5/15/2008 9.42 34.13 <2.0 <2.0 <2.0 <4.0 ND 21.1 - - <50 <50 <50 <3.0 None 8/18/2008 1 10.68 32.87 <2.0 <2.0 I <2.0 <4.0 ND 14.3 - - <50 <50 <50 <3.0 Page 9 of 17 TABLE SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene CS-C8 C9-02 C9-CIO Naphtha- MethodI Benzene Toluene benzene X Imes BTEX MTBE Lead Dibcomidt Ali hatics Aliphatic Aromatics lene Standards (99/L) (PS/L) (PQ/L) ("B(L) (PF/L) (PP(L) (-gA) (ug(l) (PS/L) W/L) (PB(L) (P8(L) GW-1 5 11000 700 10,000 N/A 70 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 91000 N/A 50,000 NE 2 3,000 1,000 51000 11000 G W-3 10,000 40 000 5,000 500 N/A 50,000 10 50,000 50,000 20,000 30,000 20,000 Well Data Usability Sample Groundwater Corrected \ , IN TOC Elev. Assessment Bias Date Depth(ft) GW Elev. . MW-25(90) 8/14/2002 13.80 29.80 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 9/17/2002 14.01 29.59 <2 <2 <2 <4 ND <2 - - <50 150 <50 <3 TOC Elev. 1/13/2003 12.35 31.25 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - ' 43.60 1/20/2005 11.05 32.55 <0.50 <1.0 <1.0 <1.0 ND <1.0 8/28/2007 10.14 33.46 - - - - - - - 5/22/2008 9.49 34.11 - - - - - - - MW-26(37) 9/17/2002 14.45 29.57 <2- <2 <2 <4 ND <2 - - <50 <50 <50 <3 (GW-1,GW-3) 1/13/2003 12.71 31.31 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - TOC Elev. 7/24/2003 9.98 34.04 <0.50 -1.0 <1.0 <1.0 ND <1.0 - - - - - - 44,02 10/28/2003 11.47 32.55 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - 1/12/2004 11.03 32.99 <0.5 <1 <1 <1 ND <1 - - - - - 3/25/2004 11.46 32.56 <0.5 <1 <1 <1 ND <1 - - - - - 7/21/2004 11.14 32.88 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - <5.0 10/4/2004 11.66 32.36 <0.5 <1 <1 <1 ND <1 - - - - - 3/22/2007 9.68 34.34 - - - - - - - - - - - 8/28/2007 10.61 33.41 - - - - - - - - 5/22/2008 9.91 34.11 - - - - - - - - - - MW-26(72) 9/17/2002 14.54 29.50 12 <2 <2 <4 ND 31.1 - - <50 <50 <50 <3 (GW-1,GW-3) 7/24/2003 10.02 34.02 0.8 <1.0 <1.0 <1.0 0.8 23.7 - - - - - - TOC Elev. 10/28/2003 11.55 32.49 0.5 <1.0 <1.0 <1.0 0.5 17.5 - - - - 44,04 1/12/2004 11.08 32.96 0.7 <1 <7 <1 0.7 28.4 - - - - - 3/25/2004 11.46 32.58 0.5 <1 <1 <1 0.5 17.0 - - - - - 7/21/2004 11.14 32.90 <0.50 <1.0 <1.0 <1.0 ND 9.3 - - - - - <5.0 10/4/2004 11.60 32.44 <0.5 <1 Q <1 ND 35.8 - - - - - - 3/2/2005 11.52 32.52 <2.0 <2.0 <2.0 <4.0 ND 35.3 - - <50 <50 <50 <3.0 7/11/2005 9.05 34.99 <2.0 <2.0 <2.0 <4.0 ND 2.2.6 - - <50 <50 <50 <3.0 1/18/2006 9.03 35.01 <1.00 <3.00 <1.00 <6.00 ND 18.7 - - <100 <100 <l00 <5.00 4/19/2006 9.80 34.24 <1.00 <3.00 <1.00 <6.00 ND 17.6 - - <100 <100 <100 <5.00 3/22/2007 9.70 34.34 - - - - - - - - - - - 8/28/2007 10.62 33.42 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 1/3/2008 11.32 32.72 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <700 <100 <100 <5.00 3/28/2008 10.44 33.60 <2.0 <2.0 <2.0 <4.0 ND 35.8 - - <50 <50 <50 <3.0 None 5/13/2008 9.89 34.15 <2.0 <2.0 <2.0 <4.0 ND 40.1 - - <50 <50 <50 <3.0 None 8/18/2008 11.48 32.56 <2.0 <2.0 12.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-26(90) 9/17/2002 14.42 29.56 <2 <2 <2 <4 ND <2 - - <50 <50 <50 <3 (GW-1,GW-3) 1/13/2003 12.71 31.27 <0.50 <1.0 <l.0 <1.0 .ND 1.9 - - - - - - TOC Ele, 8/28/2007 14.41 29.57 - - - 43.98 5/22/2008 9.82 34.16 - - - - - - - - - - Page 10 of 17 i� TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene C5-C8 C9-02 C9-00 Naphtha- Method I Benzene I Toluene benzene X lenes BTEX MTBE Lead Dibromid Ali hatics Ali hatics Aromatics lene Standards (p8/L) I (pg/L) W/L) WIL) (fig/L) (A ) (uo) --(u?A) (ug/L) (PE/t.) (rBrt) (Ng/L) UW-1 5 1,000 7W 10,000 N/A 70 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 91000 N/A 50,000 NE 2 3,000 1,000 5,000 1,000 GW-3 10,000 40,000 5,000 500 N/A 50,000 10 50,000 50,000 20,000 501000 20,000 Well Data Usability Sample Groundwater Corrected •� TOC EIev. Assessment Bias Date Depth(B:) GW EIev.(tt) y .. ��i. �k,��. a „? uw ` \• .� •.�-�` *: »� -� • MW-27(47) 9/17/2002 "15.35 29.48 <2 •<2 <2 <4 ND <2 - <50 <50 <50 •<3 (GW-1,GW-3) 1/13/2003 13.63 31.20 <0.50 q"0 <1.0 <1.0 ND <1.0 - - - - - TOC Elev. 7/24/2003 10.89 33.94 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - 44.83 10/28/2003 12.38 32.45 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - 1/12/2004 12.02 32.81 <0.5 <t <1 <1 ND <1 - - - - - - 3/25/2004 12.32 32.51 <0.5 <1 <1 <1 ND <1 - - - - - 7/21/2004 12.38 32.45 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - <5.0 10/4/2004 1,2.43 32.40 <0.5 <1 <t <1 ND <1 - - - - - - 3/2/2005 11.79 33.04 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 7/11/2005 9.75 35.08 <2.0 <2.0 <2.0 <4.0 ND <3.0 - - <50 <50 <50 <3.0 10/19/2005 10.68 34.15 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 4/19/2006 10.68 34.15 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <700 <100 <5.00 3/22/2007 10.60 34.23 - - - - - - 5/16/2008 11.02 33.81 - - - - - - - - - - - - MW-27(9) 9/17/2002 15.37 29.48 <2 <2 <2 <4 ND <2 - - -<50 <50 <50 <3- (GW-1,GW-3) "1/13/2003 13.65 31.20 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - -TOC El- 7/21/2004 12.38 32.47 - - - - - - - - - - - - 44.85 3/22/2007 10.60 34.25 - - - - - - - - - - 5/16/2008 11.02 33.83 - - - - - - - - - - MW-28(29) 9/17/2002 34.03 31.21 <2 <2 <2 <4 ND 37.9 - - <50 <50 <50 <3 (GW-1,GW-3) TOC El-. 65.24 MW-28(55) 9/17/2002 34.10 31.21 <2 <2 <2 <4 ND <2 - - <50 <50 <50 <3 (GW-1,GW-3) TOC Elev. 65.31 MW-28(68) 9/17/2002 34.10 31.22 <2 <2 <2 <4 ND <2 - - <50 <50 <50 <3 (GW-1,GW-3) TOC EIev. 65.32 Page 11 of 17 TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved 1 Ethylene CS-C8 C9-02 C9-00 Naphtha- Method 1 Benzene Toluene benzene X Ienes BTEX MTBE Lead Dibromid Ali hatics Ali hatics Aromatics lene Standards (PP(-) (us(L) (us/L) (Ag/L) (p8R-) (p8(L).... _(uBA) (uBn) (p8(1-) (p8(L) (-Pg/L) (p ) .. GW-1 5 1,000 700 10,00o N/A 70 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 1,000 5,000 1,000 GW-3 10,000 40,000 5,000 500 N/A 50,000 10 50,000 50,000 20,000 50,000 20,000 Well Data Usability Sample Groundwater Corrected TOC Elev. Assessment Bias Date Depth(ft) GW Elev.(h) „11..� �, „v, ;.t, x, ."_ .dr .r. .. :.�.".,„�. ? *.� �.\ a y.o ..�. •:`.j�H�..�. y�..���..5 MW-29(35) 12/16/2002 6.45 29.97 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 1/73/2003 5:53 30.89 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 TOC Elev. 4/30/2003 2.65 33.77 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 36.42 7/24/2003 2.75 33.67 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - - 10/28/2003 4.26 32.16 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - 1/12/2004 3.81 32.61 <0.5 Q <1 <1 NO <1 - - - - - 3/25/2004 4.20 32.22 <0.5 <1 <1 <1 ND <1 - - - - - - 7/21/2004 4.18 32.24 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - <5.0 10/4/2004 4.33 32.09 <0.5 <1 <1 <1 ND <I - - - - - - 3/2/2005 3.63 32.79 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 7/11/2005 1.95 34.47 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 1/18/2006 1.89 34.53 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 4/19/2006 2.54 33.88 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 3/22/2007 2.50 33.92 - - - - - - - - - - - - 8/28/2007 3.41 33.01 - - - - - - - - - - - - 5/22/2008 2.74 33.68 - - - - - - - - - - - - MW-29(4) 12/16/2002 6.72 29.93 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 1/13/2003 5.77 30.88 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 TOC Elev. 4/30/2003 2.92 33.73 <2.0 <2.0 <2.0 2.0 2.0 <2.0 - - <50 <50 <50 <3.0 36.65 7/24/2003 2.99 33.66 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - -3/22/2007 2.75 33.90 - - - - - - - - - - - - 8/28/2007 3.63 33.02 - - - - - - - - - - - - 5/22/2008 2.98 33.67 - - - - - - - - - - - - MW-29(68) 8/18/2005 NM NM 16.3 <2.0 <2.0 <4.0 16.3 2,280.0 - - <50 <50 <50- <3.0 (GW-1,GW-3) 10/19/2005 2.70 NSVD 12.0 <2.0 <2.0 <4.0 12.0 2,210.0 - - <50 <50 <50 <3.0 TOC Elev. 1/18/2006 2.02 NSVD 6.4 <3.00 <1.00 <6.00 6.4 1,050.0 - - <200 Q00 <100 <5.00 NSVD 4/19/2006 2.57 NSVD 16.3 <3.00 <1.00 <6.00 16.3 2,230.0 - - <1000 <700 <700 <5.00 10/18/2006 2.66 NSVD 3.93 <3.00 <1.00 <6.00 3.93 527.0 - - 240.0 <100 <100 <5.00 3/22/2007 2.59 NSVD 6.43 <3.00 <1.00 <6.00 6.43 910.0 - - <500 <100 <100 <5.00 6/25/2007 1.51 NSVD <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 8/28/2007 3.45 NSVD 5.65 <3.00 <1.00 <6.00 ND 721.0 - - 623.0 <700 <100 <5.00 1/3/2008 NM NSVD <I.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 3/28/2008 4.28 NSVD <2.0 <2.0 <2.0 <4.0 ND 138 - - <50 <50 <50 <3.0 5/16/2008 2.85 NSVD 4.0 <2.0 <2.0 <4.0 4.0 512 - - <50 <50 <50 <3.0 None 8/18/2008 3.38 <2.0 <2.0 <2.0 <4.0 ND 90.5 - - 69.0 <50 <50 <3.0 MW-30(35) 12/16/2002 7.50 30.02 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 1/13/2003 6.62 30.90 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 TOC EIev. 4/30/2003 3.73 33.79 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 37.52 7/24/2003 3.85 33.67 <0.50 <1.0 <1.0 <I.0 ND <1.0 - - - - - - 10/28/2003 5.37 32.15 <0.50 <1.0 <1.0 <7.0 ND <1.0 - - - - - - 1/12/2004 4.86 32.66 <0.5 <1 <1 <1 ND 'l - - - - 3/25/2004 5.31 32.21 <0.5 <1 <1 <7 ND <1 - - - - - - 7/21/2004 5.30 32.22 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - <5.0 10/4/2004 5.42 32.10 <0.5 <1 <1 <1 ND <1 - - - - - - 3/2/2005 4.76 32.76 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 7/11/2005 2.80 34.72 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 1/18/2006 2.97 34.55 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 4/19/2006 3.66 33.86 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <700 <100 <5.00 Page 12 of 17 TABLE SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene CS-C8 C9-C12 C9-C10 Naphtha- Method 1 Benzene Toluene benzene X lenes BTEX MTBE Lead Dibromid Ali hatics Ali hatics Aromatics lene Standards (Pg/L) (ug/L) (ARIL) (ug/L) (ug/L) (ug/L) (.g/1) (ng/9 (PE/L) (ug/L) (NPR-) (Ag/L) GW-1 ., 1,000 700 10,000 N/A 70 13 0.02 300 4,000 700 140 GW2 2,000 50,000 20,000 91000 N/A 50,000 NE 2 3,000 11000 5,000 1,000 GW-3 10,000 40,000 5,000 500 N/A 50,000 10 50 000 50 000 20 000 50 000 20 000 NOW Well Data Usability Sample Groundwater Comcted •, TOC Elev. Assessment Bias Date Depth(ft) GW Elev.(ftl ,, ,• a:. "gym ,z.�. .. s ••-� •a��= .a. v ,'al., kar "•i MW-30(4) 12/16/2002 7.85 29.99 12.0 2.0 <2.0 <4.0 NO <2.0 - - <50 <50 <50 <3.0 (GW-1,GW-3) 1/13/2003 6.92 30.92 <2.0 <2.0 <2.0 <4.0 NO <2.0 - - <50 <50 <50 <3.0 TOC Elev. 4/30/2003 4.08 33.76 <2.0 <2.0 <2.0 <4.0 NO <2.0 - - <50 <50 <50 <3.0 37.84 7/24/2003 4.17 33.67 <0,50 <1.0 -1.0 <1.0 NO <1.0 - - - - " MW-31(20) 3/11/2003 33.60 32.61 <2 <2 <2 <4 NO <2 - - 184.0 <50 66.8 <3 (GW-1,GW-3) 3/22/2007 30.92 35.29 - - - - - - - - - - TOCEIev. 8/28/2007 31.71 34.50 - - - - - - 66.21 MW-31(55) 3/11/2003 32.88 33.20 4.8 <2 <2 <4 4.8 2,300.0 - - <50 <50 <50 <3 (GW-1,GW-3) 3/22/2007 60.15 5.93 <1.00 <3.00 <1.00 <6.00 NO 326.0 - - <100 <100 <100 <5.00 TOC Ele, 6/23/2007 29.96 36.12 <1.00 <3.00 <1.00 <6.00 NO <1.00 - - <100 <100 <100 <5.00 66.08 8/28/2007 31.61 34.47 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <l00 <5.00 1/3/2008 37.75 28.33 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 3/28/2008 31.55 34.53 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 150 <3.0 None 5/15/2008 31.17 34.91 -<2.0 <2-0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-32(20) 3/11/2003 32.24 33.22 <2 <2 <2 <4 - ND <2 - - - <50 <50 <50 <3 (GW-1,GW-3) 7/21/2004 31_93 33.53 - - - - - - - - - - - TOC EIe, 3/22/2007 30.15 35.31 - - - - - - 65.46 8/28/2007 30.96 34.50 - - MW-32(55) 3/11/2003 32.19 33.22 <2 <2 <2 <4 ND 16,300.0 - - <50 <50 <50 <3 (GW-1,GW-3) 7/24/2003 30.46 34.95 0.6 <1.0 <1.0 <1.0 0.6 1,920.0 - - - TOC Elev. 10/28/2003 32.93 32.48 <2.5 <5.0 <5.0 <5.0 NO 3,380.0 - - - 65.41 1/12/2004 31.52 33.89 <0.5 <1 <7 <1 NO 332.0 - - - - - - 7/21/2004 31.85 33.56 <0.50 <1.0 <1.0 <1.0 NO 160.0 - - - - - <5.0 10/4/2004 31.82 33.59 <0.5 <1 <1 <1 ND 89.6 - - - 3/2/2005 31.34 34.07 <2.0 <2.0 <2.0 <4.0 NO 5.4 - - <50 <50 <50 <3.0 7/11/2005 29.14 36.27 <2.0 <2.0 <2.0 <4.0 NO 9.6 - - <50 <50 <50 <3.0 10/19/2005 31.10 34.31 <2.0 <2.0 <2.0 <4.0 NO 27.4 - - <50 <50 <50 <3.0 1/23/2006 29.57 35.84 <1.00 <1.00 <1.00 <3.00 ND 50.8 - - <100 <100 -100 <5.00 4/19/2006 20.09 45.32 <1.00 <3.00 <1.00 <6.00 ND 16.0 - - <100 <100 <100 <5.00 10/18/2006 30.24 35.17 <1.00 <3.00 <1.00 <6.00 ND 5.85 - - <100 <100 <100 <5.00 3/22/2007 30.10 35.31 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <700 <100 <5.00 6/25/2007 29.24 36.17 <1.00 <3.00 Q.00 <6.00 NO <3.00 - - <100 <100 <100 <5.00 8/28/2007 31.03 34.38 <1.00 <3.00 <1,00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 1/3/2008 32.10 33.31 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 3/28/2008 31.80 33.61 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <So <3.0 None 3/15/2008 30.48 34.93 <2.0 <2.0 <2.0 <4.0 ND 2.4 - - <50 <50 <50 <3.0 None 8/18/2008 31.48 33.93 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-33(20) 3/11/2003 30.13 35.28 <2 <2 <2 <4 ND <2 - - <So <50 <50 <3 (GW-1,GW-3) 7/21/2004 3"1.90 33.51 - - - - - - - - TOC Elev. 3/22/2007 30.15 35.26 - - - - - - 65.45 8/28/2007 31.05 34.36 - - - - - MW-33(55) 3/11/2003 32.07 33.24 <2 <2 <2 <4 ND 71.4 - - <50 <50 <50 <3. (GW-1,GW.3) 7/24/2003 30.36 34.95 <0.50 <1.0 <1.0 <1.0 NO 37.3 - - - - TOC El- 10/28/2003 31.80 33.51 <0.50 <1.0 <1.0 <1.0 NO 18.8 - - - 65.31 "1/12/2004 31.45 33.86 <0.5 <1 <7 <1 NO 67.9 - - - " 7/21/2004 31.77 33.54 <0.50 <1.0 <1.0 <1.0 NO 17.4 - - - - - <5.0 10/4/2004 31.78 33.53 <0.5 <1 <1 <1 NO 27.7 - - - - 3/2/2005 31.25 34.06 <2.0 <Z0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 . 7/11/2005 29.05 36.26 <2.0 <2.0 <2.0 <4.0 NO 1.4 - - <50 <50 <50 <3.0 10/19/2005 30.02 35.29 <2.0 <2.0 <2.0 <4.0 NO <1.0 - - <50 <50 <50 <3.0 1/23/2006 29.48 35.83 <1.00 <1.00 <1.00 <3.00 NO <1.00 - - <100 <100 <100 <5.00 4/19/2006 30.00 35.31 <1.00 <3.00 <1.00 <6.00 NO <1.00 - - <100 <100 <100 <5.00 3/22/2007 29.98 35.33 - - - - - - - - 8/28/2007 30.94 34.37 - - - - - - Page 13 of 17 TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene C5-C8 C9-02 C9-Clo Naphtha- Method 1 Benzene Toluene benzene X lenes BTEX MTBE Lead Dibromide Ali hatics Ali hatics Aromatics lene Standards (pg/L) (Ng/L) (p8/l.) (ue/L) (ue(L) (ps/L) (u8A) (u6/I) (p8(L) (PP/L) (PS(L) (4B/L) GW-1 5 1,000 700 101000 N/A 70 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 91000 N/A 50,000 NE 2 3,000 1,000 51000 1,000 CW-3 10,000 40,000 5,000 500 N/A 50,000 10 50,000 50,000 20,000 501000 20,000 Well Data Usability Sample Groundwater Corrected TOC Elev. Assessment Bias Date Depth(k) GW Etev.(@) „"gam, , •,� ���, <7.0 ND .<7.0\•. MW-39(17) 6/18/2003 26.57 34.81 �\�<OSOJu� <7.0 <7.0 - - - - ' (GW-1,GW-3) 7/21/2004 28.25 33.13 - - - - - - -TOC Elev. 3/22/2007 26.57 34.87 61.38 8/28/2007 27.42 33.96 5/16/2008 26.92 34.46 - - - - - MW-34(53) 6/18/2003 26.27 34.84 4.4 <1,0 <1.0 <1.0 4.4 5,490.0 - - - - - (GW-1,GW-3) 8/15/2003 26.89 34.22 14.7 <1.0 <1.0 1.0 15.7 46,600.0 - - - - - TOC Elev. 10/28/2003 28.12 32.99 15.3 <1 <1 <1 15.3 64,000.0 - - - - - 61.11 3/25/2004 28.06 33.05 29.3 <7 <1 <1 29.3 49,900.0 - - - - - 7/21/2004 28.02 33.09 53.2 <1 <1 <1 53.2 60,600.0 - - - - - 10/4/2004 28.10 33.01 55.9 <I <1 <1 55.9 43,600.0 - - - - - 3/2/2005 27.60 33.51 <2.0 <2.0 <2.0 <4.0 ND 6,570.0 - - <50 <50 <50 <3.0 7/11/2005 25.45 35.66 <2.0 <2.0 <2.0 <4.0 ND 3.0 - - 150 <50 <50 <3.0 _ 10/19/2005 26.43 34.68 <2.0 <2.0 <2.0 <4.0 ND <1.0 - - <50 <50 <50 <3.0 1/18/2006 25.83 35.28 <1.00 <3.00 <1.00 <6.00 ND 2.0 - - <100 <100 <100 <5.00 4/19/2006 26.40 34.71 <1.00 <3.00 <'1.00 <6.00 ND 218.0 - - <100 <100 <100 <5.00 10/18/2006 28.43 32.68 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 3/22/2007 26.47 34.64 <'1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <700 <5.00 6/25/2004 25.66 35.45 <7.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 8/28/2007 27.22 33.89 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <700 <100 <5.00 1/3/2008 28.28 32.83 <1.00 <3.00 <1.00 <6.00 N D <3.00 - - <100 <100 <100 <5.00 3/28/2008 27.07 34.04 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 3/15/2008 27.49 33.62 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-35(17) 6/18/2003 26.23 34.80 <0.50 <1.0 <7.0 <1.0 ND <7.0 - - - - - (GW-1,GW-3) 7/21/2004 28.01 33.02 - - - - - - - - TOC Elev. 5/16/2008 26.67 34.36 - - - - - - - - - 61.03 MW-35(53) 6/18/2003 26.31 34.80 12.4 <1.0 <1.0 1.2 13.6 1,860.0 - - - - - (GW-1,GW-3) 10/28/2003 28,12 32.99 2.3 <1.0 <1.0 <1.0 2.3 301.0 - - - -TOC Elev. '1/12/2004 27.71 33.40 <0.5 <1 < <1 ND 282.0 - - - - - 61.11 3/25/2004 28.08 33.03 <0.5 <1 <1 <1 ND 279.0 - - - - - - 7/21/2004 28.09 33.02 0.5 <I <1 <1 0.5 181.0 - - - - 10/4/2004 28.14 32.97 <0.5 <1 <1 <1 ND 187.0 - - - - 3/2/2005 27.67 33.44 <2.0 <2.0 <2.0 <4.0 ND 751.0 - - <50 <50 <50 <3.0 7/11/2005 25.35 35.76 <2.0 <2.0 <2.0 <4.0 ND 23.0 - - <50 <50 <50 <3.0 10/19/2005 26.43 34.68 <2.0 <2.0 <2.0 <4.0 ND 63.2 - - <50 <50 <50 <3.0 1/18/2006 25.66 35.45 <1.00 <3.00 <1.00 <6.00 ND 63.8 - - <I00 <100 <100 <5.00 4/19/2006 26.39 34.72 <1.00 <3.00 <1.00 <6.00 ND 455.0 - - <100 <100 <100 <5.00 10/18/2006 26.48 34.63 <1.00 <3.00 <1.00 <6.00 ND 87.8 - - <100 <100 <100 <5.00 3/22/2007 26.37 34.74 <3.00 <1.00 <1.00 <6.00 ND 72.7 - - <100 <100 <100 <5.00 6/25/2007 25.50 35.61 <3.00 <1.00 <1.00 <6.00 ND 11.8 - - <100 <100 <100 <5.00 8/28/2007 27.28 33.83 <3.00 <1.00 <1.00 <6.00 ND 4.73 - - <100 <100 <100 <5.00 1/3/2008 28.27 32.84 <3.00 <1.00 <1.00 <6.00 ND 15.0 - - <100 <100 <100 <5.00 3/28/2008 28.90 32.21 <2.0 <2.0 <2.0 <4.0 ND 32.2 - - <50 <50 <50 <3.0 None 5/15/2008 26.51 34.60 <2.0 <2.0 <2.0 14.0 ND 61.7 - - <50 <50 <50 <3.0 1 None 8/18/2008 27.77 33.34 <2.0 1 <2.0 1 <2.0 <4.0 ND 13.3 - - <50 <50 <50 <3.0 Page 14 of 17 TABLET SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene CS-C8 C9-C12 I C9-00 Naphtha- Method1 Benzene Toluene benzene X lenes BTEX MTBE Lead Dibmmide Ali hatics Ali hatics Aromatics lene Standards (µg/L) _(uvJ(-) (Am/L1 (ug/L) (ug/U (µg/L) (ngA) ("S11) (1-0) (1,0-) (vs/L) (P8(L) GW-1 5 1,000 700 10,000 N/A 70 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 1,000 5,000 1,000 _ GW3 10,000 40,000 5,000 Soo N/A 50,000 10 50,000 50,000 20,000 50,000 20,000 Well Data Usability Sample Groundwater Corrected ;'j �z�_ � � � TOC Elev. Assessment Bias Date Depth R GW Elev. ft 4 �� ° MW-36(15) 6/18/2003 24.02 34.66 <0.50 ¢11.0 <1.0 <1.0 ND <1.0 - - - - - (GW-1,GW-3) 7/21/2004 25.83 32.85 - - - - - - TOC Ele, 8/28/2007 25.00 33.68 58.68 5/16/2008 24.45 34.23 - - - - - - - - - - - MW-36(49.5) 6/18/2003 24.10 34.7-1 <0.5 <1 <1 <1 ND <l - - - - - - (GW.1,GW-3) 10/28/2003 25.91 32.90 <0.5 <1 <1 <7 ND <1 - - - - - TOCElev. 1/12/2004 25.48 33.33 <0.5 <1 <1 <1 ND <1 - - - - - 58.81 7/21/2004 25.89 12.92 <n_5 <1 <1 17 ND <1 - - - 10/4/2004 25.95 32,86 <0.5 <1 <7 <1 ND 1.1 - - - - - 3/22/2007 24.00 34.81 - - - - - - - - - - - 8/28/2007 25.06 33.75 5/16/2008 24.52 34.29 - - - - - - - - - - MW.37(53) 6/3/2004 27.60 33.92 <1.0 <1.0 <1.0 <1.0 ND 7,100.0 - - - - - - (GW-1,GW-3) 7/21/2004 28.44 33.08 15.30 <1.0 Q.0 <1.0 15.3 10,400.0 - - <50 <50 <50 <3.0 TOC Elev. 10/4/2004 28.51 33.01 9.80 <5.0 <5.0 <5.0 9.8 4,390.0 - - - - - - 61.52 3/2/2005 28.03 33.49 6.90 <4.0 <4.0 <8.0 6.9 3,040.0 - - 1100 <100 <l00 <6.0 7/11/2005 25.86 35.66 58.20 <2.0 <2.0 <4.0 58.2 2,860.0 - - <50 <50 <50 <3.0 10/19/2005 26.86 34.66 39.60 <10 <10 <20 39.6 2,890.0 - - <250 <250 <250 <15 1/18/2006 26.03 35.49 41.10 <3.00 <1.00 <6.00 41.1 7,560.0 - - 2,180.0 <100 <100 <5.00 4/19/2006 26.80 34.72 6.58 <3.00 <1.00 <6.00 6.6 983.0 - - <500 <100 <100 <5.00 10/18/2006 26.85 34.67 <1.00 <3.00 <1.00 <6.00 ND 6.26 - - <100 <100 <100 <5.00 3/22/2007 26.80 34.72 <1.00 <3.00 <1.00 <6.00 ND 4.64 - - <100 <100 <100 <5.00 6/25/2007 25.87 35.65 <1.00 <3.00 <1.00 <6.00 ND 14.7 - - <100 <100 <100 <5.00 8/28/2007 27.63 33.89 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 1/3/2008 28.64 32.88 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 3/28/2008 27.46 34.06 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 4/21/2008 27.34 34.18 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <2.0 None 5/15/2008 27.11 34.41 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 8/18/2008 28.13 33.39 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-37(105) 1/18/2006 26.2.2 35.30 <1.00 <3.00 11.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 (GW-1,GW-3) 4/19/2006 27.03 34.49 <1.00 <3.00 <1M <6.00 ND 17.7 - - <00 <100 <100 <5.00 TOC EIe, 10/24/2006 27.30 34.22 Q.00 <3.00 <1.00 <6.00 ND 94.0 - - <100 <100 t100 <5.00 61.52 3/22/2007 27.10 34.42 <1.00 <3.00 <1.00 <6.00 ND 23.0 - - <100 <100 <100 <5.00 6/25/2007 26.16 35.36 <1.00 <3.00 <1.00 <6.00 ND 17.9 - - -100 <700 <100 <5.00 8/28/2007 27.88 33.64 <1.00 <3.00 <1.00 <6.00 ND 4.84 - - <100 <100 <100 <5.00 1/3/2008 28.95 32.57 <1.00 <3.00 <1.00 <6.00 ND 3.38 - - 1100 <100 <100 <5.00 3/28/2008 27.80 33.72 <2.0 <2.0 <2.0 <4.0 ND 10.5 - - <50 <50 <50 <3.0 None 8/18/2008 28.57 32.95 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 Page 15 of 17 TABLE SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Ethylene CS-C8 C9-C12 C9-Cl0 Naphtha- Method 1 Benzene Toluene benzene X Imes BTEX MTBE Lead Dibmmide Ali hatics Ali hatics Aromatics lene Standards (NF/L) I (N8(L) (Y8/L) (N8(L) (v8R-) (18(L) (u8/1) (ultn) WIL) (98/L) (VHA) (MS/L) GW-1 5 1,000 700 10,000 N/A 70 15 0.02 300 4,000- 700 140 GW 2 2AW :A,000 20,000 9,1aa1 N/A 50,000 NE 2 31000 11000 51000 1,000 GW-3 10,000 40,000 51000 500 N/A 50,000 10 50,000 501000 20,000 50,000 20,000 Well Data Usability sample Groundwater Corrected TOC Elev. Assessment Bias Date Depth(it) GW Elev.(ft) MW.37(90) 1/18/2006 26.22 35.30 <7.00 <3.00 <1.00 <6.00 ND <1.00 - - 1100 <100 <100 <5.00 (GW-1,GW-3) 4/19/2006 27.05 34.47 <1.00 <3.00 <1.00 <6.00 ND <3.00 <1.00 <3.00 <1.00 <6.00 <100 <5.00 TOC Elev. 10/24/2006 3351 28.01 <1.00 <3.00 <1.00 <6.00 ND 6.66 <1.00 <3,00 <1.00 <6.00 <100 - 61.52 3/22/2007 26.90 34.62 <1.00 <3.00 <1.00 <6.00 ND 38.8 - - <100 <100 <100 <5.00 6/25/2007 24.89 36.64 <1.00 <3.00 <1.00 <6.00 ND 121 - - <100 <100 <100 <5.00 8/28/2007 27.00 3452 <1.W <3.00 <1.00 <6.W ND 110 - - <100 <100 <100 15.00 1/3/2008 Not sampled-well inaccesible - - - - - - - - - - - - 3/28/2008 Not sampled-well inaccesible - - - - - - - - - - - - None. 8/18/2008 30.30 31.22 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-38(104) 3/3/2006 2555 33.69 <1.00 <1.00 <1.00 <3.00 ND <0.500 - - - - - - (GW-1,GW4) 4/19/2006 26.26 32.98 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 TOC Elev. 10/18/2006 26.38 32.86 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 59.24 3/22/2007 26.22 33.02 - - - - - - - - - - - - 8/28/2007 27.09 32.15 - - - - - - - - - - - 5/16/2008 26.61 32.63 - - - - - - - - - - - - None 8/18/2008 27.64 31.60 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-38(89) 3/3/2006 25.32 33.67 <1.00 <1.00 <1.00 <3.00 ND- <0.500 - - - - - - - - (GW-I,GW-3) -4/19/2006 26.00 32.99 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <100 <100 <5.00 TOC Elev. 10/18/2006 26.12 32.87 <1.00 <3.00 <1.00 <6.00 ND <1.00 - - <100 <700 <100 <5.00 58.99 8/28/2007 26.88 32.11 - - - - - - - - - - - - 5/16/2008 26.38 32.61 - - - - - - - - - - - None 8/18/2008 27.39 31.60 <2.0 <2.0 <D <4.0 ND <2.0 - - <50 <50 <50 <3.0 MW-39(88) 3/3/2006 72.63 33.79 <1.00 <1.00 <1.00 <3.00 ND 9.1 - - _ - - - - (GW-1,GW-3) 4/19/2006 23.39 33.03 <1.00 <3.00 <1.00 <6.00 ND 5.5 - - <1W <100 <100 <5.00 TOC Elev. 10/18/2006 2351 32.91 <1.00 <3.00 <1.00 <6.00 ND <1,00 - - <100 <100 <100 15.W 56.42 3/22/2007 23.37 33.05 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 6/25/2007 22A6 33.96 <1.00 <3.00 <1.00 <6.00 ND <3,00 - - <700 <100 <100 <5.00 8/28/2007 24.27 32.15 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 1/3/2008 25.36 31.06 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 3/28/2008 23.93 32.49 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 5/15/2008 23.70 32.72 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 8/18/2008 24.82 31.60 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <0 <3.0 Page 16 of 17 TABLE 1 SUMMARY OF GROUNDWATER MONITORING DATA-VPH Former Texaco Service Station#100083 1140 Hyannis Road Hyannis,MA Ethyl- Total Dissolved Fthylene CS-C8 C9-C12 C9-00 Naphtha. Method l Benzene Toluene benzene X lenes BTEX NME Lead Dibromide Ali hatics Ali hatics Aromatics lene Standards (pBfL) I 0tg/L) (NBA) (NS/L) ("910 (p8(L) (u8/1) (4,8/1) (p8/L) _ (pBA) (PWL) _ (ug/W GW-1 s 11000 700 10,000 N/A A 15 0.02 300 4,000 700 140 GW-2 2,000 50,000 20,000 9,000 N/A 50,000 NE 2 3,000 11000 5,000 1,000 GW-3 10,000 40,001 1,010 500 N/A 50,000 10 50,000 50,000 20,000 50,000 20,000 Groundwater Corrected y TOC Elev. Assessment Bias Date Depth(ft) GW file Well Data Usability Sample Ground j1 V.(ft) +�. r MW40(85) 3/3/2006 16.09 43.16 <1.00 <7.00 <1.00 <3.00 ND <0.500 - - - - - - (GW-1,GW-3) 4/19/2006 16.75 42.49 <1.00 <3.00 <1.00 <6.00 ND <7.00 - - <100 <100 <100 <5.00 TOC Elev. 10/18/2006 17.02 42.22 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 50.44 3/22/2007 16.82 42.42 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 6/25/2007 15.95 43.29 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <700 <100 <5.00 8/28/2007 17.98 41.26 <1.00 <3.00 <7.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 1/3/2008 18.56 40.68 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 3/28/2008 17.51 41.73 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 5/16/2008 17.21 42.03 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 None 8/18/2008 18.43 32.01 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 <3.0 RW-101 6/3/2004 17.83 33.65 1.0 <7.0 <1.0 <1.0 -1.0 686.0 - - - - - - (GW-1,GW.3) 7/21/2004 18.60 32.88 - - - - ND - - - - - - - TOC Elev. 10/4/2004 18.75 32.73 3.3 <1.0 <7.0 <1.0 3.3 4,860.0 - - - - - - 51.48 1/20/2005 18.25 33.23 <0.50 <1.0 <1.0 <1.0 ND 377.0 - - - - - - 3/2/2005 NM NM 2.4 <2.0 <2.0 <4.0 2.4 1,680.0 - - <50 <50 <50 <3.0 7/11/2005 NM NM 5.6 <2.0 <2.0 <4.0 5.6 1500.0 - - <50 <50 <50 <3.0 10/19/2005 NM NM <2.0 <2.0 <2.0 <4.0 ND 691.0 - - <50 <50 <50 0.0 4/19/2006 NM NM <1.00 <3.00 <1.00 <6.00 ND 528.0 - - 263.0 <1W <100 <5.00 3/22/2007 1920 32.28 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 5/16/2008 16.79 34.69 - - - - - - - - - - - - None 8/18/2008 17.77 33.71 <2.0 <2.0 <2.0 <4.0 ND 22.0 - - <2.0 1,310 506 <3.0 RW-102 6/3/2004 12.13 33.57 <1.0 <1.0 <1.0 <1.0 ND <1.0 - - - - - - (GW-I,GW-3) 7/21/2004 12.95 32.75 - - - - ND - - - - - - - TOC Elev. 10/4/2004 13.08 32.62 <0.50 <1.0 <1.0 <1.0 ND <1.0 - - - - - - 45.70 1/20/2005 12.12 33.58 <0.50 <1.0 <1.0 <1.0 ND 7.4 - - - - - - 10/19/2005 NM NM <2.0 <2.0 <2.0 <4.0 ND 2.8 - - <50 <50 <50 <3.0 1/18/2006 NM NM <1.00 <3.00 <1.00 <6.00 ND 21.6 - - <100 c100 <100 <5.00 4/19/2006 NM NM <1.00 <3.00 <1.00 <6.00 ND 3.4 - - <100 <100 <100 <5.00 3/22/2007 10.39 35.32 <1.00 <3.00 <1.00 <6.00 ND <3.00 - - <100 <100 <100 <5.00 5/16/2008 10.71 34.99 - - - - - - - - - - - - None 8/18/2008 11.76 33.94 <2.0 <2.0 <2.0 <4.0 ND <2.0 - - <50 <50 <50 13.0 TMP-1 8/16/2001 NM NM 65.0 <12 <12 <24 65.0 868.0 - - <120 <120 <120 <12 TMP-2 8/16/2001 NM NM 31.3 <25 <25 <50 31.3 2,040.0 - - <250 <250 <250 <25 TMP-3 8/16/2001 NM NM <5.0 <5.0 G5.0 <10.0 ND 158.0 - - <.50 <50 <50 G5.0 TM1?4 8/16/2001 NM NM <5.0 <5.0 <5.0 <10.0 ND 21.1 - - <50 <50 <50 <5.0 TMP-5 8/16/2001 NM NM <5.0 G5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 TMP-6 8/16/2001 NM NM <5.0 <5.0 <5.0 <10.0 I ND 14.8 - - <10 <50 <50 <5.0 TMP-7 8/16/2001 NM NM <5.0 G5.0 <5.0 <10.0 ND <5.0 - - <50 <50 <50 <5.0 STAFF GAUGE 10/6/2008 0.90 32.90 - - - - - - - - - - 33.8 NOTES: For the Data Usability Assessment,the following qualifiers are utilized: ug/L-micrograms per liter(parts per billion) None-no potential bias exists <5.0-less than the laboratory detection limit of 5.0 ug/L Low-potential low bias exists BTEX-total combined benzene,toluene,ethylbenzene,xylenes High-potential high bias exists MTBE-methyl tertiary-butyl ether NC-data is not-CAM compliant -not sampled ND non-detect NA notapplicable NSVD-not surveyed Bold-concentration above applicable Method 1 Standards MCP Standards for this table are current as of January 2008 Wave III Update Page 17 of 17 ww ww w w w w w ww w w ww ww wi w ■w ■w ww w ww TABLE 2 SUMMARY OF GROUNDWATER MONITORING DATA-EPH Former Texaco Service Station#100083 1140 Iyannough Road Hyannis,MA MCP Method 1 Acenaph Acenaph Benzo(a) Benzo(a) Benzo(b) Benzo(g,h,l) Benzo(k) Dibenz(a,h) Fluoran- Indeno(1,2,3- 2-Methyl- Naphtha- Phenan C9-C18 C19-C36 Cil-C22 GW Standards thene thylene Anthracene anthracene pyrene uoranthen( perylene fluoranthene Chrysene anthracene thene Fluorene cd)pyrene naphthalene lene threne Pyrene Aliphatics Aliphatics Aromatics (ug/L) (ug/L) (ug/L) (pg/L) (ug L) (ugIL) (ug(L) (ug/L) (ug/L) (ug/L) (ug/L) (ug/L) (ug(L) (pg(L) (pg/L) (ug/L) (ug/L) (Ag/L) OWL) (pg(L) GW-1 20 300 2,000 1 0.2 1 300 1 2 0.5 90 300 0.5 10 140 300 80 4,000 14,000 200 GW-3 5,000 3,000 3,000 I,000 500 400 3,000 100 31000 40 200 3,000 100 3,000 20,000 s0 20 20,000 50,000 30,000 Well Sample :.1. r'-.. .` 'y, yry '?# v v ..? - ,y,..x( ` a ;;i4°`° ;f;'a. a llh• '` a`' "' ,',, ,„',, in:": .x •. *j o �.Y."� t.� m,�•- ,"'t �� +.'{ �d.',w+^ ytt.,�* g ,`3;+ ,r, �.+ g'e' '��, „k'r.M if"'` GWCatego Date a� U-. "` rsit"i' s.'.,,: MW-1 6/4/1999 ry <5 .� <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 � <5 8.3 <5 <5 381 1,520 <170 10/12/2000 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 8.9 27.7 <5 <5 1,120 194 <100 4/4/2001 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 8.2 19 <5.0 <5.0 <100 210 127 MW-2 6/4/1999 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <60 <167 <170 MW-4 6/4/1999 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 - <5 <5 <5 <5 96.4 <80 <170 10/12/2000 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <100 <100 <100 MW-5 6/4/1999 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5. <5 <5 <5 - <60 <80 <170 10/12/2000 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 14.4 49 <5 <5 1,010 <100 105 4/4/2001 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 12.3 50.6 <5.0 <5.0 <100 <100 134 MW-9 6/4/1999 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 <5.3 c5.3 <5.3 <5.3 <5.3 <5.3 51.7 156 <5.3 <5.3 1,200 <94 421 10/12/2000 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 98.3 135 <5 <5 3,890 <100 277 MW-10 6/4/1999 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <5.1 <61 <82 <170 10/12/2000 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <100 <100 <100 Notes: EPH is extractable petroleum hydrocarbons and reported in(ug/L)micrograms per liter Bold-type is concentration above applicable Method 1 Standards MCP Standards for this table are current as of April 2006 Wave 11 Update <5.0 is less than the laboratory detection limit of 5.0 ug/L. -not sampled Page 1 of 1 ' TABLE 3 SUMMARY OF GROUNDWATER MONITORING DATA-MNA ' Former Texaco Service Station#100083 1140 Iyannough Rd. Hyannis,MA Dissolved Sample pH Conductivity Temperature Oxygen ORP ' Well Date (N/S/cm) (Deg.C) (mg/L) (mV) AS-1 4/4/2001 5.46 259 14.99 0.39 188.7 8/16/2001 1.14 INJ-1 7/21/2004 5.12 710 11.82 10.97 158.6 MP-1 8/16/2001 - - - 0.9 - MP-2 8/16/2001 - - 0.78 - ' MP-3 8/16/2001 - 0.86 MW-1 4/4/2001 5.85 164 14.93 0.54 68.5 8/16/2001 - - - 0.72 - ' 12/4/2001 5.78 366 14.66 2.71 -21 5/l/2002 5.87 197 14.74 0.22 -57.4 MW-2 4/4/2001 5.21 287 13.87 2.45 228.4 ' 8/16/2001 1.48 MW-2A 4/4/2001 5.46 177 13.81 1.97 232.3 8/16/2001 1.33 12/4/2001 5.35 233 14.96 3.79 202.6 ' 5/1/2002 5.59 195 13.68 0.26 186.9 10/18/2006 4.33 318 19.45 1.41 192.5 MW-3A 4/4/2001 5.99 173 12.04 9.46 248.6 ' 8/16/2001 0.88 12/4/2001 5.31 52 14.29 8.63 211.2 5/1/2002 6.15 54 12.02 6.51 219.1 MW-4 4/4/2001 5.14 522 14.9 3.61 216.2 8/16/2001 - - - 0.81 - MW-5 4/4/2001 5.93 269 13.84 0.27 102.3 8/16/2001 - - - 0.46 12/4/2001 6.22 199 16.45 2.36 -54.4 5/1/2002 6.32 353 14.64 0.61 -81.2 MW-6 4/4/2001 5.69 233 14.6 1.46 203.1 8/16/2001 - - - 0.73 - MW- 5/1/2002 5.94 613 14.73 0.18 -44.9 ' MW-9R 6/25/2007 6.36 467 22.91 12.48 -25.6 8/28/2007 5.42 396 16.80 4.65 249.0 1/3/2008 5.79 342 9.27 5.87 214.0 5/15/2008 5.17 357 16.19 7.28 -74.5 ' Page 1 of 6 ' TABLE 3 SUMMARY OF GROUNDWATER MONITORING DATA-MNA ' Former Texaco Service Station#100083 1140 Iyannough Rd. Hyannis,MA ' Dissolved Sample pH Conductivity Temperature Oxygen ORP Well Date (N/S/cm) (Deg.C) (mg(L) (mV) ' MW-10 4/4/2001 4.6 1133 13.87 0.47 262 8/16/2001 - - - 0.75 - ' MW-11 4/4/2001 5.3 152 14.03 5.55 232.3 8/16/2001 1.22 10/18/2006 4.32 165 18.19 3.03 214.2 3/22/2007 5.09 222 12.42 9.33 163.8 ' 6/25/2007 7.91 381 19.00 11.75 -21.8 MW-12 4/4/2001 5.35 519 13.86 1.91 201.7 8/16/2001 - - - 2.06 - ' MW-13 4/4/2001 5.04 388 13.91 7.61 153.4 8/16/2001 1.4 12/4/2001 5.4 188 15.21 9.53 215.1 5/1/2002 5.35 191 14.09 5.85 279.6 ' MW-14(25) 4/4/2001 5.05 261 13.71 4.16 202.6 8/16/2001 - - - 1.41 - 12/4/2001 4.95 315 15.41 7.59 252.7 ' 5/1/2002 5.16 462 13.78 4.49 84.3 MW-16(55) 10/18/2006 5.24 561 21.05 5.85 145.2 3/22/2007 5.28 561 12.72 4.42 129.7 6/25/2007 6.3 156 18.91 6.59 235.3 8/28/2007 5.67 566 24.16 6.11 300.0 MW-19(55) 10/24/2006 5.66 284 14.59 1.31 107 3/22/2007 6.46 240 11.89 7.18 53.5 6/25/2007 5.41 294 21.18 2.93 276.1 8/28/2007 5.92 269 20.27 4.39 185.0 1/3/2008 5.54 289 11.10 3.83 140.3 ' 3/28/2008 5.71 180 11.42 5.06 -112 5/15/2008 5.89 194 17.68 7.71 -125.9 8/18/2008 5.44 650 23.29 2.71 219.6 MW-20(20) 7/21/2004 - - 14 9.48 - MW-20(55) 7/21/2004 - - 20.6 9.19 - 10/24/2006 5.87 267 12.92 1.14 107.4 ' 3/22/2007 6.98 276 9.68 1.52 192.0 6/25/2007 5.63 206 18.06 5.63 193.3 8/28/2007 5.74 251 15.99 5.06 248.0 1/3/2008 5.59 177 11.27 6.53 189.0 3/28/2008 OBSTRUCTION IN WELL 5/15/2008 7.55 105 11.17 4.91 157.0 8/18/2008 5.80 870 21.63 7.68 201.3 Page 2 of 6 L ' TABLE 3 SUMMARY OF GROUNDWATER MONITORING DATA-MNA Former Texaco Service Station#100083 1140 Iyannough Rd. Hyannis,MA Dissolved Sample pH Conductivity Temperature Oxygen ORP Well Date (N/S/cm) (Deg.C) (mg/L) (mV) MW-21(55) 8/28/2007 5.72 446 15.26 3.36 223 1/3/2008 5.90 413 10.12 7.19 163.0 3/28/2008 5.39 317 11.14 7.25 208 5/15/2008 5.93 395 17.21 7.79 -114.5 8/18/2008 5.53 646 25.19 3.56 243.7 MW-23(20) 7/21/2004 - - 16.7 7.67 - ' MW-23(52) 7/21/2004 - 13.3 5.81 - MW-24(10) 7/21/2004 - 19.3 6.68 ' MW-24(42) 7/21/2004 - 18.7 9.04 8/28/2007 5.93 165 14.06 6.14 241.0 1/3/2008 5.39 348 9.11 3.23 142.0 3/28/2008 5.66 222 11.92 5.01 -96 ' 5/15/2008 5.39 229 13.82 7.54 -106.3 8/18/2008 5.47 337 15.23 2.21 156.0 MW-25(42) 7/21/2004 - - 15.4 4.16 - ' 10/24/2006 7.39 254 12.93 1.15 154.2 3/28/2008 5.85 198 10.95 4.97 -95 MW-25(72) 10/24/2006 5.88 431 12.77 1.08 203.4 ' 3/22/2007 7.45 417 10.78 1.28 179.0 6/25/2007 5.46 400 20.57 10.49 95.0 8/28/2007 6.16 408 14.02 0.32 152.0 1/3/2008 5.66 112 7.88 4.81 109.0 ' 5/15/2008 6.09 360 12.89 1.38 -221.8 8/18/2008 6.10 460 15.36 0.44 97.0 MW-25(90) 7/21/2004 - - 14.9 0.89 - ' MW-26(37) 7/21/2004 - - 16.7 6.47 - 8/28/2007 6.31 197 16.35 0.31 53.0 MW-26(72) 1/3/2008 5.82 486 9.81 3.18 106.0 3/28/2008 6.06 308 11.04 4.65 -65 5/15/2008 6.17 389 14.69 0.89 -214.3 8/18/2008 6.35 510 17.23 0.81 -37.0 ' MW-26(9) 7/21/2004 - - 16.7 8.38 - MW-27(47) 7/21/2004 - 15.3 6.88 MW7(9) 7/21/2004 - 21.9 7.5 Page 3 of 6 _ 1 ' TABLE3 SUMMARY OF GROUNDWATER MONITORING DATA-MNA ' Former Texaco Service Station#100083 1140 lyannough Rd. Hyannis,MA Dissolved Sample pH Conductivity Temperature Oxygen ORP ' Well Date (N/S/cm) (Deg.C) (mg/L) (mV) MW-29(68) 10/18/2006 5.70 380 16.33 1.43 184.7 3/22/2007 5.26 553 13.19 1.48 92.6 6/25/2007 5.29 252 18.28 7.06 135.2 ' 8/28/2007 6.06 427 15.32 0.99 169.0 3/28/2008 5.76 386 11.29 2.35 -71 5/15/2008 7.87 507 13.11 0.90 145.0 8/18/2008 7.36 526 13.59 0.51 -10.0 ' MW-31(55) 3/22/2007 7.16 300 13.79 1.25 182.0 6/25/2007 4.86 429 20.27 5.14 172.0 8/28/2007 5.83 365 21.76 3.08 182.0 ' 1/3/2008 5.70 290 12.77 4.50 129.1 3/28/2008 5.49 283 10.21 5.51 184.0 5/15/2008 5.80 342 13.81 3.44 184.0 MW-32(20) 7/21/2004 5.05 374 13.1 11.53 169.6 MW-32(55) 7/21/2004 5.22 289 13.51 0.55 149.9 10/18/2006 3.6 305 18.82 3.05 259.3 ' 3/22/2007 7.11 255 11.06 1.31 183.0 6/25/2007 4.83 294 20.85 3.00 277.0 8/28/2007 5.36 383 17.40 3.07 118.7 1/3/2008 5.4 263 10.59 6.71 215.8 ' 3/28/2008 5.62 321 10.30 7.08 152 5/15/2008 5.47 291 15.33 4.69 -123.1 8/18/2008 5.36 415 21.82 4.08 254.7 ' MW-33(20) 7/21/2004 5.5 302 12.18 12.46 142.3 MW-33(55) 7/21/2004 5.18 397 12.67 0.97 139.7 MW-34(17) 7/21/2004 5.5 408 13.41 12.19 180.8 MW-34(53) 7/21/2004 5.42 233 13.3 0.4 166.1 10/18/2006 5.16 434 16.5 0.45 183.2 ' 3/22/2007 6.91 324 11.2 1.08 195.0 6/25/2007 5.85 224 20.04 7.44 -7.0 8/28/2007 6.34 271 17.45 3.27 162.0 ' 1/3/2008 5.84 238 10.37 7.72 122.0 3/28/2008 5.71 170 12.51 4.97 -77 5/15/2008 6.08 254 14.41 5.51 158.0 MW-35(17) 7/21/2004 5.39 210 12.91 12.2 165.7 ' MW-35(53) 7/21/2004 5.45 254 12.78 0.44 148 10/18/2006 5.67 436 17.90 2.34 150 ' 3/22/2007 6.75 522 11.43 1.23 207.0 6/25/2007 5.31 447 19.90 3.54 130.1 8/28/2007 5.45 502 15.09 0.51 186.8 1/3/2008 6.37 578 10.65 7.09 -146.9 ' 3/28/2008 5.4 482 11.19 3.60 211 5/15/2008 5.76 437 14.88 0.75 152.0 8/18/2008 5.40 393 18.01 2.93 192.6 ' Page 4 of 6 TABLE3 SUMMARY OF GROUNDWATER MONITORING DATA-MNA ' Former Texaco Service Station#100083 1140 Iyannough Rd. Hyannis,MA Dissolved Sample pH Conductivity Temperature Oxygen ORP ' Well Date (li/S/cm) (Deg.C) (mg/L) (mV) MW-36(15) 7/21/2004 5.35 266 13.7 10.41 161.4 MW-36(49.5) 7/21/2004 5.3 241 13.27 1.41 156 ' MW-37(53) 7/21/2004 5.44 212 13.81 0.35 143.4 10/18/2006 5.89 506 17.02 7.76 128.8 10/24/2006 7.16 0.24 14.93 1.38 11.7 ' 3/22/2007 7.98 368 10.96 3.39 94.8 6/25/2007 5.21 937 21.03 5.63 191.3 8/28/2007 5.59 440 16.26 5.37 221.9 1/3/2008 5.63 334 12.01 6.90 172.2 ' 3/28/2008 5.02 217 11.00 6.30 222 5/15/2008 5.76 358 15.16 2.82 158.0 8/18/2008 5.43 56 21.34 6.63 182.6 MW-37(90) 3/22/2007 7.04 249 10.69 4.99 -75.1 6/25/2007 4.90 281 20.20 4.43 202.7 8/28/2007 7.61 310 20.46 0.36 175.2 ' 3/28/2008 OBSTRUCTION IN WELL 8/18/2008 6.38 15,119 20.83 2.19 20.0 MW-37(105) 10/24/2006 7.16 240 14.93 1.38 11.7 ' 3/22/2007 6.49 215 10.81 4.37 -26.2 6/25/2007 4.96 267 18.32 4.17 197.3 8/28/2007 6.65 262 16.90 0.51 282.0 1/3/2008 6.73 434 10.01 7.64 76.6 3/28/2008 6.94 248 11.39 1.99 -49.0 8/18/2008 6.18 274 20.35 1.91 -17.9 MW-38(104) 10/18/2006 6.31 225 15.11 2.63 122.1 ' 8/18/2008 6.27 377 . 20.79 3.47 101.0 MW-38(89) 10/18/2006 7.55 238 15.08 1.5 65.9 8/18/2008 6.91 413 17.89 1.65 -73.0 MW-39(88) 10/18/2006 6.23 188 15.71 1.78 121.6 3/22/2007 7.63 176 10.54 0.92 149.0 6/25/2007 5.58 492 18.5 2.05 456.7 8/28/2007 6.02 404 14.47 0.38 142.0 1/3/2008 5.83 212 9.17 4.28 142.0 3/28/2008 5.67 178 10.75 3.00 -35 5/15/2008 6.22 197 17.04 5.19 -142.2 8/18/2008 6.16 231 17.57 3.32 105.0 MW-40(85) 10/18/2006 7.65 177 14.79 5.85 73.2 ' 3/22/2007 7.85 164 11.26 1.27 136.0 6/25/2007 7.92 172 16.91 7.38 164.7 8/28/2007 6.52 169 13.95 2.03 101.0 1/3/2008 5.72 241 8.77 3.91 228.0 ' 3/28/2008 5.58 163 11.59 3.46 28 5/15/2008 5.93 197 15.42 3.3 -170.4 8/18/2008 6.57 191 14.55 3.39 71.0 Page 5 of 6 1 TABLE3 SUMMARY OF GROUNDWATER MONITORING DATA-MNA 1 Former Texaco Service Station#100083 1140 Iyannough Rd. Hyannis,MA 1 Dissolved Sample pH Conductivity Temperature Oxygen ORP Well Date (µ/S/cm) (Deg.C) (mg/L) (mV) 1 RW-101 7/21/2004 - - 12.2 1.29 - 3/22/2007 6.53 156 16.43 1.13 170.0 8/18/2008 3.78 433 14.23 2.03 -77.0 ' RW-102 7/21/2004 - - 11.3 6.11 - 3/22/2007 5.52 252 15.91 6.73 54.7 8/18/2008 5.73 198 13.45 3.57 139.0 1 SVE-1 8/16/2001 - - - 0.78 - 1 Notes: -is not sampled mg/L is milligrams per Liter 1 (µg/L)is micrograms per Liter mV is millivolts µS/cm is microSiemens per centimeter i 1 i 1 1 1 1 1 i 1 ' Page 6 of 6 V ' TABLE4 SUMMARY OF GROUNDWATER MONITORING DATA-OXYGENATES Former Texaco Service Station#100083 11401yannough Road Hyannis,MA Method 1 TAME ETBE DIPE TBA Ethanol MTBE Standards (µg/L) (µg/L) (µg/L) (µg/L) (µg/L) (µg/L) GW-1 NE NE NE NE NE 70 GW-3 NE NE NE NE NE 50,000 Data Usability Sample Well Assessment Bias Date ' INJ-1 10/4/2004 <2.0 <2.0 <2.0 <100 ' 10/19/2005 <2.0 <2.0 <2.0 <100 - - 10/19/2005 <2.0 <2.0 <2.0 <100 - - MW-1 7/21/2004 <2.0 <2.0 <2.0 <100 - - ' MW-2A 7/11/2005 <2.0 <2.0 <2.0 <100 - - 10/19/2005 <2.0 <2.0 <2.0 <100 - - ' 1/23/2006 1.08 <1.00 <1.00 - _ = MW-5 7/21/2004 <2.0 <2.0 <2.0 <100 3/2/2005 <2.0 <2.0 <2.0 <100 - - ' 7/11/2005 <2.0 <2.0 <2.0 <100 = MV,7-6 7/21/2004 <2.0 <2.0 <2.0 <100 3/2/2005 <2.0 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 <100 - - MW-9 7/21/2004 <10 <10 <10 <500 - - 3/2/2005 <2.0 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 <100 ' 10/19/2005 <2.0 <2.0 <2.0 <100 - - 4/19/2006 <1.00 <1.00 <1.00 I <10.0 - - M4Y 9R 8/2/2007 <1.00 <1.00 <1.00 <20.0 <100 - 5/15/2008 <2.0 <2.0 <2.0 <20 - <1.0 MW-11 7/11/2005 <2.0 <2.0 <2.0 <100 - - 1/23/2006 <1.00 <1.00 <1.00 - - - 4/19/2006 <1.00 <1.00 <1.00 <10.0 MW-16(55) 10/19/2005 11 <2.0 <2.0 174 - - 8/2/2007 <1.00 <1.00 <1.00 <20.0 <100 - ' ' MW 19(55) 7/21/2004 8.3 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 <100 - - 10/19/2005 <2.0 <2.0 <2.0 <100 - - ' 1/23/2006 <1.00 <1.00 <1.00 - - - 4/19/2006 3.52 <1.00 <1.00 <10.0 8/2/2007 <1.00 <1.00 <1.00 <20.0 <100 - ' None 5/15/2008 <2.0 <2.0 <2.0 <20 - <1.0 MW-19(90) 7/11/2005 <2.0 <2.0 <2.0 <100 1/23/2006 <1.00 <1.00 <1.00 - - - ' 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - ' Page 1 of 5 I ' TABLE 4 SUMMARY OF GROUNDWATER MONITORING DATA-OXYGENATES Former Texaco Service Station#100083 1140 Iyannough Road Hyannis,MA Method 1 TAME ETBE DIPE TBA Ethanol MTBE Standards (µg/L) W/O W/O (µg/L) (µg/L) (µg/L) GW-1 NE NE NE NE NE 70 GW-3 NE NE NE NE NE 50,000 Data Usability Sample Well Assessment Bias Date MW 20(55) 7/21/2004 65.5 <10 <10 <500 - - ' 3/2/2005 <2.0 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 <100 - - ' 10/19/2005 <2.0 <2.0 <2.0 <100 - - 1/23/2006 <1.00 <1.00 <1.00 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - 8/2/2007 <1.00 <1.00 <1.00 <20.0 <100 - None 5/15/2008 <2.0 <2.0 <2.0 <20 - <1.0 MW 21(55) 8/2/2007 <1.00 <1.00 <1.00 <20.0 <100 - None 5/15/2008 <2.0 <2.0 <2.0 <20 - <1.0 ' MW-23(52) 7/21/2004 <2.0 <2.0 <2.0 <100 - MW-24(42) 7/21/2004 <2.0 <2.0 <2.0 <100 - - ' 3/2/2005 <2.0 <2.0 <2.0 <100 - _ 7/11/2005 <2.0 <2.0 <2.0 <100 10/19/2005 <2.0 <2.0 <2.0 <100 - - 1/18/2006 <1.00 <1.00 <1.00 <10.0 - - ' 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - 8/28/2007 <1.00 <1.00 <1.00 <20.0 <100 None 5/15/2008 <2.0 <2.0 <2.0 <20 - <1.0 i ' MW 25(42) 7/21/2004 <2.0 <2.0 <2.0 <100 3/2/2005 <2.0 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 183 - - 10/19/2005 <2.0 <2.0 <2.0 <100 - - 1/18/2006 <1.00 <1.00 <1.00 <10.0 - - 4/19/2006 <1.00 <1.00 <1.00 <10.0 - <1.0 ' MW 25(72) 7/21/2004 <2.0 <2.0 <2.0 <100 3/2/2005 <2.0 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 <100 - - 10/19/2005 <2.0 <2.0 <2.0 <100 - - ' 1/18/2006 1.91 <1.00 <1.00 <10.0 - - 4/19/2006 3.75 <1.00 <1.00 <10.0 8/28/2007 <1.00 <1.00 <1.00 <20.0 <100 - ' None 5/15/2008 <2.0 <2.0 <2.0 <20 - 12 MW 26(37) 7/21/2004 <2.0 <2.0 <2.0 <100 7/21/2004 <2.0 <2.0 <2.0 <100 - - ' 3/2/2005 <2.0 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 <100 1/18/2006 <1.00 <1.00 <1.00 <10.0 - - 4/19/2006 <1.00 <1.00 <1.00 <10.0 - Page 2 of 5 ' TABLE 4 SUMMARY OF GROUNDWATER MONITORING DATA-OXYGENATES Former Texaco Service Station#100083 1140Iyannough Road Hyannis,MA ' Method 1 TAME ETBE DIPE TBA Ethanol MTBE Standards (µg/L) (µg/L) (µg/L) (µg/L) (µg/L) (µg/L) GW-1 NE NE NE NE NE 70 ' GW-3 NE NE NE NE NE 50,000 Data Usability Sample Well Assessment Bias Date �� MW-26(72) 8/28/2007 <1.00 <1.00 <1.00 <20.0 <100 None 5/15/2008 <4.0 <4.0 <4.0 <40 - 50.8 MW 27(47) 7/21/2004 <2.0 <2.0 <2.0 <100 - - ' 3/2/2005 <2.0 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 <100 10/19/2005 <2.0 <2.0 <2.0 <100 - - 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - ' MW-29(35) 7/21/2004 <2.0 <2.0 <2.0 <100 - - 3/2/2005 <2.0 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 <100 - - ' 1/18/2006 <1.00 <1.00 <1.00 <10.0 - _ 4/19/2006 <1.00 <1.00 <1.00 <10.0 MW-29(68) 10/19/2005 16.6 <2.0 <2.0 <100 - - 1/18/2006 5.48 <1.00 <1.00 53 - _ 4/19/2006 21.8 <1.00 2.04 106 8/28/2007 4.53 <1.00 <1.00 29.1 <100 - ' None 5/15/2008 2.9 <2.0 <2.0 28.5 - 475 MW-30(35) 7/21/2004 <2.0 <2.0 <2.0 <100 3/2/2005 <2.0 <2.0 <2.0 <100 - - ' 7/11/2005 <2.0 <2.0 <2.0 <100 - _ 1/18/2006 <1.00 <1.00 <1.00 <10.0 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - < , < , <1.00 < < None 5/15/2008 <2.0 <2.0 <2.0 <20 - <1.0 MW-32(55) 7/21/2004 6.7 <2.0 <2.0 <100 - - 3/2/2005 <2.0 <2.0 <2.0 <100 - - ' 7/11/2005 <2.0 <2.0 <2.0 <100 - - 10/19/2005 <2.0 <2.0 <2.0 <100 1/23/2006 <1.00 <1.00 <1.00 - - - ' 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - 8/28/2007 <1.00 <1.00 <1.00 <20.0 <100 None 5/15/2008 <2.0 <2.0 <2.0 <20 - 2.0 Page 3 of 5 TABLE4 SUMMARY OF GROUNDWATER MONITORING DATA-OXYGENATES Former Texaco Service Station#100083 1140Iyannough Road Hyannis,MA Method 1 TAME ETBE DIPE TBA Ethanol MTBE Standards (pg/L) (pg/L) (40 (pg/L) (per) (µg/L) GW-1 NE NE NE NE NE 70 ' GW-3 NE NE NE NE NE 50,000 Data Usability Sample Well Assessment Bias Date MW 33(55) 7/21/2004 <2.0 <2.0 <2.0 <100 - ' 3/2/2005 <2.0 <2.0 <2.0 <100 - - 7/11/2005 <2.0 <2.0 <2.0 <100 - - 10/19/2005 <2.0 <2.0 <2.0 <100 ' 1/23/2006 <1.00 <1.00 <1.00 - - - 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - ' MW-34(53) 7/21/2004 2680 <2 <2 3470 - _ 3/2/2005 322 <40 <40 <2000 7/11/2005 <2.0 <2.0 <2.0 <100 - - 10/19/2005 <2.0 <2.0 <2.0 <100 - - 1/18/2006 <1.00 <1.00 <1.00 <10.0 - _ 4/19/2006 13.4 <1.00 <1.00 <10.0 8/28/2007 <1.00 <1.00 <1.00 <20.0 <100 - ' None 5/15/2008 <2.0 <2.0 <2.0 <20 - <1.0 MW 35(53) 7/21/2004 9.7 <2 <2 <100 3/2/2005 39.5 <2.0 <2.0 <100 - - ' 7/11/2005 <2.0 <2.0 <2.0 <100 - - 10/19/2005 3.6 <2.0 <2.0 <100 1/18/2006 3.22 <1.00 <1.00 <10.0 - - 4/19/2006 21.8 <1.00 <1.00 <10.0 - - ' 8/28/2007 <1.00 <1.00 <1.00 <20.0 <100 - None 5/15/2008 3.6 <2.0 <2.0 <20 69.7 MW 36(49.5) 7/21/2004 <2 <2 <2 <100 - - MW-37(53) 7/21/2004 720 <2.0 <2.0 262 - - 3/2/2005 240 <2.0 <2.0 <100 - - 7/11/2005 311 <2.0 3.1 504 - - ' 10/19/2005 353 <2.0 <2.0 435 - - 1/18/2006 457 <1.00 2.88 252 4/19/2006 92 <1.00 <1.00 <10.0 - - ' 8/28/2007 <1.00 <1.00 <1.00 <20.0 <100 - None 5/13/2008 <2.0 <2.0 <2.0 <20 <1.0 MW 37(105) 1/18/2006 <1.00 <1.00 <1.00 <10.0 - - 4/19/2006 1.24 <1.00 <1.00 <10.0 8/28/2007 <1.00 <1.00 <1.00 <20.0 <100 - MW 37(90) 1/18/2006 <1.00 <1.00 <1.00 <10.0 - - 4/19/2006 <1.00 <1.00 <1.00 <10.0 ' 8/28/2007 11.0 <1.00 <1.00 <20.0 <100 - Page 4 of 5 ' TABLE 4 SUMMARY OF GROUNDWATER MONITORING DATA-OXYGENATES ' Former Texaco Service Station#100083 1140Iyannough Road Hyannis,MA Method 1 TAME ETBE DIPE TBA Ethanol MTBE Standards (µg/L) (µg/L) (µg/L) (µg/L) W/L) W/L) GW-1 NE NE NE NE NE 70 ' GW-3 NE NE NE NE NE 50,000 Data Usability Sample 1 " Well Assessment Bias Date MW-38(104) 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - ' MW-38(89) 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - MW-39(88) 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - ' 8/28/07 <1.00 <1.00 <1.00 <20.0 <100 - None 5/15/2008 <2.0 <2.0 <2.0 <20 20.1 MW-40(85) 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - ' 8/28/2007 <1.00 <1.00 <1.00 <20.0 <100 - 5/15/2008 <2.0 <2.0 <2.0 <20 <1.0 RW-101 10/4/2004 229 <2.0 <2.0 <100 - - ' 3/2/2005 <10 <10 <10 <500 - _ 7/11/2005 104 <2.0 <2.0 172 10/19/2005 58.6 <2.0 <2.0 204 - - ' 4/19/2006 43.9 <1.00 <1.00 <10.0 - - RW-102 10/4/2004 <2.0 <2.0 <2.0 <100 10/19/2005 <2.0 <2.0 <2.0 <100 - - 1/18/2006 1.14 <1.00 <1.00 <10.0 - - ' 4/19/2006 <1.00 <1.00 <1.00 <10.0 - - Notes: ' All concentration and MCP standards reported in micrograms per liter(ug/L) ETBE-ethyl tert-butyl ether TAME-tert-amyl methyl ether TBA-tert-butyl alcohol ~' DIPE-di-isopropyl ether <10.0-below laoratory detection limit of 10.0 ug/L NE-.not established. ' For the Data Usability Assessment,the following qualifiers are utilized: None-no potential bias exists Low-potential low bias exists ' High-potential high bias exists NC-data is not-CAM compliant III Page 5 of 5 Table 5 Summary of Ground Water Pump and Treatment System ' 11401yannough Road Hyannis,Massachusetts Blower FLOW ' Date Influent Effluent Days of Motor O7eaional FM-101 FM-102 FM-103 FM-201 BTEX MTBE TPH-GRO BTEX MTBE TPH-GRO Operation Hour Meter Pntage (RW-101 INF) (RW-102 INF) (RW-101 &RW-102 INF) (Air Stripper INF) ug/I ug/I ug/I ug/I ug/I ug/I Hours Gallons Total Gallons Gal/Day Gallons Total Gallons Gal/Day Gallons ' Total Gallons Gal/Day Gallons Total Gallons Gal/Day ' 05/03/06 2.50 359 NM 2.50 1.0 NM 0.0 9221.0 NR 4,290,725 4,290,725 0 8,089,115 8,089,115 0 1,688,775 1,688,775 0 1,492,640 1,492,640 0 06/06/06 2.50 274 NM 2.50 1.0 NM 34.0 9981.0 93 5,632,136 5,632,136 39,453 9,012,870 9,012,870 27,169 3,876,460 3,876,460 64,344 3,852,527 3,852,527 69,408 07/13/06 2.50 463 NM 2.50 1.0 NM 37.0 10396.9 47 6,359,216 6,359,216 19,651 9,215,978 9,215,978 5,489 5,067,920 5,067,920 32,202 5,136,206 5,136,206 34,694 08/01/06 2.50 336 NM 2.50 1.0 NM 19.0 10485.9 20 6,510,458 6,510,458 7,960 9,618,387 9,618,387 21,179 5,155,406 5,155,406 4,605 5,393,001 5,393,001 13,516 09/20/06 2,50 244 214 2,50 1.0 50 50.0 10657.7 14 6,809,700 6,809,700 5,985 9,819,130 9,819,130 4,015 5,440,170, 5,440,170 5,695 5,949,100 5,949,100 11,122 10/05/06 2.50 173 100 2.50 1.0 50 15.0 10904.3 68 7,245,410 7,245,410 29,047 10,291,950' 10,291,950 31,521 6,335,550 6,335,550 59,692 6,659,660 6,659,660 47,371 11/16/06 2.50 143 220 2.50 1.0 50 42.0 11274.9 37 7,918,680 7,918,680 16,030 562,480 10,670,650 9,017 6,708,241 6,708,241 8,874 7,817,640 7,817,640 27,571 12/11/06 2.50 272 100 2.50 1.0 50 25.0 11757.8 80 9,434,600, 9,434,600 60,637 997,410 11,105,580 17,397 6,854,460 6,854,460 5,849 9,811,430 9,811,430 79,752 01/03/07 3.74 237 100 2,50 1.0 50 23.0 12142.5 70 10061870'" 10,061,870 27,273 1,342,950 11,451,120 15,023 6,854,460 6,854,460 0 11369970- 11,369,970 67,763 ' 02/06/07 2.50 390 358 2.50 1.0 50 34.0 12687.1 67 618,740 11,184,140 33,008 1,610,780 11,718,950 7,877 6,854,450' 6,854,450 0 3,364,630 13,553,200 64,213 03/08/07 4.86 554 431 2.50 1.0 50 30.0 13265.6 80 2,592,100 13,157,500 65,779 1,610,780 11,718,950 0 8,838,680 8,838,680 66,141 5,214,690 15,403,260 61,669 04/09/07 2.50 488 496 2.50 1.0 50 32.0 13984.9 94 4,985,330 15,550,730 74,788 1,610,780 11,718,950 0 11263020""' 11,263,020 75,761 6,921,350 17,10.9,920 53,333 05/07/07 2.50 423 443 2,50 1.0 50 28.0 14655.6 100 7,196,610 17,762,010 78,974 1,610,780 11,718,950 0 3,501,040 14,764,060 125,037 7,614,620 17,803,190 24,760 ' 06/12/07 2.50 333 283 2.50 1.0 50 36.0 15521.0 100 41,540 20,606,940 79,026 1,610,780 11,718,950 0 6,367,450 17,630,470 79,623 8,357,510 18,546,080 20,636 07/06/07 3.20 739 1,220 2.50 1.0 50 24.0 15626.8 18 384,070 20,949,470 14,272 1,610,780 11,718,950 0 6,711,110 17,974,130 14,319 8,425,190 18,613,760 2,820 08/07/07 2.50 210 161 2.50 1.0 50 32.0 16129.6 65 2,047,930 22,613,330 51,996 1,610,780 11,718,950 0 8,383,910 19,646,930 52,275 159,980 20,348,550 54,212 09/06/07 2.50 255 227 2.50 1.0 100 30.0 16660.0 74 3,811,830 24,377,230 58,797 1,610,780 11,718,950 0 159,030 21,422,050 59,171 2,001,790 22,190,360 61,394 29.0 ' 0/08/07 2.50 241 180 2.50 1.0 100 34.0 17724.3IL 86 7,371,560 27,936,960 69,1411 1,610,780 11,718,950 0 3,740,350 25,003,3 11 70 69,574 5,657,660 25,846,230 70,967 ' Mass Removal: (((Influent Concentration,-Effluent Concentration)+(Influent Concentration2-Effluent Concentration 2))/2)'(Flow2-Flowl)'(3.785 liters/gallon)"(1gram/1,000,000 ug) (0.0022 pounds/gram) BTEX,MTBE,and TPH-GRO concentrations in italics are laboratory detection limits.Compounds not detected above laboratory detection limits "FM-102 rolled over at 10,000,000 on 10/5/06 add 10,108,170 to current reading on entry. ' **FM-101 rolled over at 10,000,000 on 12/5/06 add 10,565,400 to current reading on entry. "'FM-201 rolled over at 10,000,000 on 12/20/06 add 10,188,570 to current reading on entry. "'FM-103 rolled over at 10,000,000 on 4/9/07 add 11,263,020 to current reading on entry. i Table 5 Summary of Ground Water Pump and Treatment System ' 1140 lyannough Road Hyannis, Massachusetts 0 Pressure Mass Removal ' Date FM-301(TOTAL) PI-201 PI-301 PI-302 PI-303 PI-401 PI-402 PI403 LGAC LGAC LGAC FT-301 VGAC VGAC VGAC BTEX MTBE TPH-GRO Total (Air Stripper EFF) Influ. Mid-1 Mid-2 Mid-1 Mid-2 Effl Gallons Total Gallons Gal/Day psi psi psi psi psi psi psi psi psi psi psi psi psi psi pounds pounds pounds pounds 05/03/06 4,836,242 4,836,242 0 15.0 38.0 47.0 25.0 30.0 20.0 18.0 15.0 0.0 0.0 0.0 NM NM NM NM NM NM 0.0 ' 06/06/06 5,759,131 5,759,131 27,144 16.0 28.0 36.0 32.0 18.0 24.0 26.0 15.0 0.0 0.0 27.0 NM NM NM 0.0 2.4 NM 2.4 07/13/06 6,337,097 6,337,097 15,621 NM NM NM NM NM NM NM NM NM NM NM NM NM NM 0.0 1.8 NM 4.2 08/01/06 6,459,980 6,459,980 6,468 18.0 26.0 34.0 34.0 15.0 20.0 34.0 5.0 0.0 0.0 25.0 NM NM NM 0.0 0.4 NM 4.6 09/20/06 6,652,200 6,652,200 3,844 15.0 22.0 30.0 36.0 15.0 19.0 31.0 15.0 0.0 0.0 0.5 NM NM NM 0.0 0.5 NM 5.1 ' 10/05/06 6,846,620 6,846,620 12,961 15.0 49.0 62.0 34.0 44.0 24.0 30.0 20.0 0.0 0.0 0.5 NM NM NM 0.0 0.3 0.2 5.6 11/16/06 7,149,570 7,149,570 7,213 15.0 49.0 62.0 34.0 44.0 24.0 30.0 20.0 0.0 0.0 0.5 NM NM NM 0.0 0.4 0.3 6.2 12/11/06 7,735,120 7,735,120 23,422 30.0 72.0 80.0 32.0 69.0 56.0 32.0 30.0 0.0 0.0 0.6 NM NM NM 0.0. 1.0 0.5 7.8 01/03/07 8,128,650 8,128,650 17,110 33.0 82.0 90.0 34.0 78.0 40.0 38.0 34.0 0.0 0.0 0.7 NM NM NM 0.0 0.8 0.2 8.8 ' 02/06/07 8,519,630 8,519,630 11,499 20.0 52.0 80.0 32.0 50.0 50.0 38.0 40.0 0.0 0.0 0.6 NM NM NM 0.0 1.0 0.6 10.4 03/08/07 8,731,800 8,731,800 7,072 30.0 64.0 80.0 33.0 31.0 31.0 bg 22.0 0.0 0.0 0.6 NM NM NM 0.0 0.8 0.6 11.8 04/09/07 9,086,600 9,086,600 11,088 20.0 80.0 92.0 30.0 70.0 64.0 60.0 60.0 0.0 0.0 0.6 NM NM NM 0.0 1.5 1.2 14.6 05/07/07 9,384,760 9,384,760 10,649 20.0 90.0 >100 30.0 90.0 68.0 64.0 61.0 0.0 0.0 0.6 NM NM NM 0.0 1.1 1.0 16.8 ' 06/12/07 9,848,890 9,848,890 12,893 20.0 98.0 >100 30.0 >100 92.0 86.0 80.0 0.0 0.0 0.6 NM NM NM 0.0 1.5 1.2 19.4 07/06/07 9,917,910 9,917,910 2,876 26.0 82.0 80.0 32.0 51.0 bg bg 45.0 0.0 0.0 0.6 NM NM NM 0.0 0.3 0.4 20.1 08/07/07 10,304,430 10,304,430 12,079 30.0 75.0 >100 30.0 82.0 72.0 72.0 75.0 0.0 0.0 0.6 NM NM NM 0.0 1.5 2.1 23.7 09/06/07 10,733,120 10,733,120 14,290 20.0 80.0 >100 30.0 98.0 94.0 88.0 95.0 0.0 0.0 0.6 NM NM NM 0.0 0.8 0.4 25.0 ' 10/05/07 10,886,740 10,886,740 5,297 20.0 46.0 46.0 30.0 20.0 16.0 20.0 20.0 0.0 0.0 0.5 NM NM NM 0.0 0.4 0.3 25.6 11/08/07 1,202,060 12,202,060 38,686 20.0 50.0 50.0 30.0 34.0 30.0 42.0 36.0 0.0 0.0 0.5 NM NM NM 0.0 -22.9 -16.4 -13.7 9 1 1 0 ' Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts i 1 ' ATTACHMENT A 1 1 e-Hardcopy 2.0 Automated Report ®� New England L L b o ra t o rn 06/12/08 1 Technlcal Report f©r '. Shell Oil SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' EQ 711 Accutest Job Number: M73538 ' g Sam lin Dates: 05/15/08 - 05/16/08 Sampling Report to: Sovereign Consulting Inc. ' 'sherburne@sovcon.com ATTN: Jason Sherburne ' Total number of pages in report: 82 ��C\N ACCpRO4 O� tic ' + , Test results contained within this data package meet the requirements eZa and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. ' Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) ' k . S. NY(11791) NJ(MA926) PA(68-01121).NC(653) IL(200018) NAVY USACE �. �. This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. • Test results relate only to samples analyzed. New England • 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • http://www.accutest.com An 1 of 82 GACC TEST. M73536 =a Sections: Table of Contents -I- Section1: Sample Summary ................................................................................................... 3 Section2: Case Narrative!Conformance Summary .............................................................. 5 Section3: Semple llesults ........................................................................................................ 7 3.1: M73538-1: MW-9R ...................................................................................................... 8 3.2: M73538-2: MW-21 (55) ............................................................................................... 10 3.3: M73538-3: MW-19 (5 5) ............................................................................................... 12 3.4: M73538-4: MW-32 (55) ............................................................................................... 14 3.5: M73538-5: MW-26 (72) ............................................................................................... 16 3.6: M73538-6: MW-25 (72) ............................................................................................... 18 3.7: M73538-7: MW-24 (42) ............................................................................................... 20 3.8: M73538-8: MW-39 (88) ............................................................................................... 22 3.9: M73538-9: MW-40 (85) ......................... .. .... 24 ' .................................. IN: M73538-10: MW-31 (55) ........................................................................................... 26 3.11.: M73538-11: MW-35 (53) ........................................................................................... 28 3.1.2: M73538-12: MW-34 (53) ........................................................................................... 30 �. 3.13: M73538-13: MW-37 (53) ........................................................................................... 32 3.14: M73538-14: MW-29 (68) ........................................................................................... 34 3.15: M73538-15: MW-20 (55) .......................................................................................... 36 1 Section4: Misc. Forms ............................................................................................................ 38 4.1: Chain of Custody ........................................................................................................... 39 �. 4.2: MCP Form ..................................................................................................................... 41 4.3: VPH Form ...................................................................................................................... 42 4.4: Sample Tracking Chronicle ........................................................................................... 57 ' Section 5: GC/MS Volatiles - QC Data Summaries .............................................................. 60 5.1: Method Blank Summary ................................................................................................ 61 5.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 66 1 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 71 5.4: Surrogate Recovery Summaries ..................................................................................... 75 Section. 6: GC Volatiles - QC Data Summaries .................... ' 6.1: Method Blank Summary ................................................................................................ 78 6.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 80 6.3: Surrogate Recovery Summaries ..................................................................................... 82 Q 2 of 82 j3ACCI.R'EST. M73538 ._,..:... ....c: Accutest Laboratories 1 Sample Summary ' Shell Oil Job No: M73538 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Collected° Matrix Client Number Date Time By Received Code Type Sample ID M�73538 1 05/15/08 09:00 RD 05/19/08 AQ Ground Water MW 9R ' M73538 2 05/15/08 09:30 RD 05/19/08 AQ Ground Water ' M73538-3 05/15/08 10:10 RD 05/19/08 AQ Ground Water MW ' 1VI735384 05/15/08 10:40 RD 05/19/08 AQ Ground Water M1V 32 (55) ' M73538 5 05/15/08 11:10 RD 05/19/08 AQ Ground Water MW 26 (72) M73538 6 05/15/08 11:45 RD 05/19/08 AQ Ground Water MW 25 (72) M735,38 7 05/15/08 12:10 RD 05/19/08 AQ Ground Water MW 2.4 (42) M73538 8 05/15/08 13:00 RD 05/19/08 AQ Ground Water MW 39 (88) ' M73538 9 05/15/08 13:50 RD 05/19/08 AQ Ground Water W,40 (85) M73538 10 05/15/08 14:05 RD 05/19/08 AQ Ground Water MW-31 (55) ' M7.3538 11 O5/15/08 13:35 RD 05/19/08 AQ Ground Water MW 35 (53) M73538 12 05/15/08 13:00 RD 05/19/08 AQ Ground Water °MW-34 (5-3 M73538 13 05/15/08 12:25 RD 05/19/08 AQ Ground Water MW 37 (53)r ® 3 of 82 M73538 .-a- -t-.. Accutest Laboratories Sample Summary Shell Oil (continued) ' SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Job No: M73538 Project No: EQ 711 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID M73538 14 05/16/08 11:15 RD 05/19/08 AQ Ground Water MW 29 (68) M73538 15 05/16/08 08:45 RD 05/19/08 AQ Ground Water MW 20 (55) 1 ® 4 of 82 GA ..CS7 ' M73538 f ' L aboratori .es SAMPLE DELIVERY GROUP CASE NARRATIVE Client: Shell Oil Job No M73538 Site: SCMAW:97346878(REIMBMA)1140Iyannough Road Hyannis MA Report Date 6/12/2008 12:05:15 PM 15 Sample(s)were collected on between 05/15/2008 and 05/16/2008 and were received at Accutest on 05/19/2008 properly preserved, at 2.5 Deg.C and intact. These Samples received an Accutest job number of M73538.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. ' Except as noted below,all method specified calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. Volatiles by GCMS By Method SW846 8260B ' Matrix AQ Batch ID: MSG3306 ` All method blanks for this batch meet method specific criteria. ' ` Sample(s) M73491-21MS,M73491-21MSD were used as the QC samples indicated. M73538-5:Elevated RL due to dilution required for matrix interference. Only MTBE,DIPE,TAME,ETBE and TBA requested. Matrix AQ Batch ID: MSG3307 ` All samples were analyzed within the recorruuended method holding time. ` Sample(s) M73577-2MS,M73577-2MSD were used as the QC samples indicated. ' ` All method blanks for this batch meet method specific criteria. ` Only MTBE,DIPE,TAME,ETBE and TBA requested. Matrix AQ Batch ID: MSG3308 ` All method blanks for this batch meet method specific criteria. ® Sarr_ple(s) M73586-6MS,M73586-6MSD were used as the QC samples indicated. ' Matrix AQ Batch ID: MSP952 ` All method blanks for this batch meet method speck criteria. o Sar_ple(s) M73513-5MS,M73513-5MSD were used as the QC samples indicated. ® Only MTBE,DIPE,TAME,ETBE and TBA requested. Matrix AQ Batch ID: MSR188 ® All method blanks for this batch meet method specific criteria. a Only MTBE,DIPE,TAME,ETBE and TBA requested. ' Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GAB2377 a All<amples were analyzed within the recommended method holding time. ' = All method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GWX1970 ' All samples were analyzed within the recommended method holding time. 4 All method blanks for this batch meet method specific criteria. Thursday,June 12,2008 Page 1 of 2 Ell 5 of 82 ' 13ACG4JTE.ST. M73538 The Accutest Laboratories of New England certifies that all analysis were performed within method specification. It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M73538). t 1 t I i Thursday,June 12,2008 Page 2 of 2 ' Qll 6 of 82 ACCUTEST� M73538 _,_..... % a� New England ,. AC U�'EST. C Section Nr Sample Results Report of Analysis II ' Q 7 of 82 CIAGCUTEST. M73538 . '.' '---° r ^s Accutest Laboratories ' Report of Analysis Page 1 of 1 ' Client Sample ID: MW-9R Lab Sample ID: M73538-1 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 R4922.D 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates ' CAS No. Compound Result RL Units Q ' 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/I ' 75-65-0 Tert Butyl Alcohol 'ND!:. 20 ug/I 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I CAS No. Surrogate Recoveries Run# I Run#2 Limits ' 1868-53-7 Dibromofluoromethane 94% 79-130% 2037 26-5 Toluene D8 101% 80 120% ' 460-00-4 4-Bromofluorobenzene 101% 80120% I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME2 8 of 82' 12ACCLJTE3T M73536 " ^'= ' Accutest Laboratories ' Report of Analysis Page 1 of 1 Client Sample ID: MW-9R Lab Sample ID: M73538-1 Date Sampled: 05/15/08 ' Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB42661.1) 1 05/28/08 AP n/a n/a GAB2377 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND, 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene NO 2.0 ug/I ' 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND ; 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9 C10 Aromatics (Unad3 ) ND 50 ug/I C5 C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I tCAS No. Surrogate Recoveries Run# I Run#2 Limits __............_. ... . ... 615-59-8 2,5-Dibromotoluene 76% 70-130% 615-59-8 2,5-Dibromotoluene 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®E 9 of 82 13AC CAJTEW.. M73536 Accutest Laboratories ' Report of Analysis Page 1 of I Client Sample ID: MW-21 (55) ' Lab Sample ID: M73538-2 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 ' Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 R4923.1) 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates ' CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 ' 75-65-0 Tert Butyl Alcohol ND 20 ug/l 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits ' 1868-53-7 Dibromofluoromethane 88% . 79 130% 2037-26-5 Toluene-D8 103% 80-120% ' 460 00 4 4 Bromofluorobenzene 1•02% 80 120% e ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Mffl 10 of 82 M AIC 6rTE5T.' ......................._..............._... M73538 ' °`' -., ' Accutest Laboratories Report of Analysis Page 1 of 1 ' Client Sample ID: MW-21 (55) Lab Sample ID: M73538-2 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB42662.1) 1 05/28/08 AP n/a n/a GAB2377 Run#2 Purge Volume Run#1 5.0 ml Run#2 1 MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634 04 4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 ' 95 47 6 o Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 76% 70-130% 615-59-8 2,5-Dibromotoluene 869/o. 70130% ND = Not detected J = Indicates an estimated value RL Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound fll 11 of 82 13ACCiJ'iEErr. M73538 Accutest Laboratories , Report of Analysis Page 1 of 1 w Client Sample ID: MW-19 (55) Lab Sample ID: M73538-3 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 R4924.1) 1 05/29/08 AA n/a n/a. MSR188 Run#2 Purge Volume , Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q ' 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 , 75-65-0 Tert Butyl Alcohol N 1 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits ' 1868-53-7 Dibromofluoromethane 88% 79-130% 2037 26 5 Toluene D8 101% 80-120% 460-00-4 4-Bromofluorobenzene 101% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound "a( 12 of 82 13ACCl.ITEEr.r M73536 a_ ........e.s ' Accutest Laboratories Report of Analysis Page 1 of 1 w Client Sample ID: MW-19 (55) Lab Sample ID: M73538-3 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch IRun#1 AB42663.1) 1 05/28/08 AP n/a n/a GAB2377 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene END 20 ug/1 1634 04 4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-213-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 ' 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj ) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/1 C9- C10 Aromatics (Unad3 ) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9 C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-39-8 2,5-Dibromotoluene 77% 70-130% 615-39-8 2,5-Dibromotoluene 87% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q11 13 of 82 ' 13ACCUTEST. M73536 Accutest Laboratories ' Report of Analysis Page 1 of 1 Client Sample ID: MW-32 (55)1 ' Lab Sample ID: M73538-4 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch , Run#1 R4925.1) 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q ' 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 2 0 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 , 75-65-0 Tert Butyl Alcohol ND, 20 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits ' 1868-53-7 Dibromofluoromethane 91% 79-130% 2037-26-5 Toluene-D8 404% 80-120% ' 460-00-4 4-Bromofluorobenzene 101% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Mn 14of82 13ACAJTEST., M73538 - - Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-32 (55) Lab Sample ID: M73538-4 Date Sampled: 05/15/08 ' Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 AB42664.1) 1 05/28/08 AP n/a n/a GAB2377 Run#2 Purge Volume Run#1 5.0 ml Run#2 ' MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634 04 4 Methyl Tert Butyl Ether 2 4 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene NO 2.0 ug/1 ' 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) N.D.: 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5 C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND: 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 79% 70130% 615-59-8 2,5-Dibromotoluene 88% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MIN 15 of 82 ' ®ACCI.17MBT M73536 Accutest Laboratories , Report of Analysis Page 1 of 1 Client Sample ID: MW-26 (72) Lab Sample ID: M73538-5 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 a G81910.1) 2 05/29/08 EL n/a n/a. MSG3306 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates ' CAS No. Compound Result RL Units Q ' 108-20-3 Di-Isopropyl ether ND 4.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 50.8 2.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 4.0 ug/1 ' 75-65-0 Tert Butyl Alcohol ND 40 ug/1 637-92-3 tert-Butyl Ethyl Ether ND 4.0 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits ' 1868-53-7 Dibromofluoromethane iO3% 79-130% 2037-26-5 Toluene-D8 95% 80-120% ' 460-00-4 4-Bromofluorobenzene 101% 80-120% (a) Elevated RL due to dilution required for matrix interference. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 16 of 82 ACC ,M73538 ''.: Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-26 (72) Lab Sample ID: M73538-5 Date Sampled: 05/15/08 ' Matrix: AQ -Ground Water Date Received: 05/19/08 Metod: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41554.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71 93 2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 40 1 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 ' 95 9:7 6 o Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 ' C9- C10 Aromatics (Unadj ) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# l Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81%, 70-130% 615-59-8 2,5-Dibromotoluene 86% 70-130% S ND = Not detected j = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ©11 17 of 82 ' ®ACCIJI'EW. M73538 Accutest Laboratories ' Report of Analysis Page 1 of 1 Client Sample ID: MW-25 (72) Lab Sample ID: M73538-6 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 ' Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 P28623.1) 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume , Run#1 5.0 ml Run#2 Oxygenates ' CAS No. Compound Result RL Units Q ' 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 1 2 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/I 75-65-0 Tert Butyl Alcohol ND 20 ug/I , 637-92-3 tert-Butyl Ethyl Ether NDI 2.0 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 1868-53-7 Dibromofluoromethane 0Y% 79 130% 2037-26-5 Toluene-D8 1'03% 80-120% 460-00 4 4-Bromofluorobenzene 01% 80-120% ' r I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME] 18 of 82 ®ACCUTEST' M73538 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-25 (72) Lab Sample ID: M73538-6 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Protect: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41555.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 tMA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND':::, ,- 2.0 ug/I ' 1634 04-4 Methyl Tert Butyl Ether 21 1 2.0 ug/l 91-20-3 Naphthalene :NDI. 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/l ' 95-47-6 o-Xylene tNDl 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/1 ' C9 C10 Aromatics (Unad3 ) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/l ' CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 83% 70130% I ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ElB 19 of 82 13ACCl.ITEErr M73538 Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-24 (42) Lab Sample ID: M73538-7 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 I.REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch , Run#1 P28624.D 1 105/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume , Run#1 5.0 ml Run#2 Oxygenates , CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether 'ND 1.0 ug/1 994 05 8 tert-Amyl Methyl Ether :ND.. 2.0 ug/I ' 75-65-0 Tert Butyl Alcohol ND 20 ug/I 637-92-3 tert-Butyl Ethyl Ether NO:, 2.0 ug/1 CAS No. Surrogate Recoveries Run# l Run# 2 Limits ' 1868-53-7 Dibromofluoromethane 105% 79-130% 2037-26 5 Toluene D8 100% 80-120% ' 460-00-4 4-Bromofluorobenzene 102% 80-120% r � ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 20 of 82. �ACrGUTEST M73538 ' Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-24 (42) Lab Sample ID: M73538-7 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41556.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 tMA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634 04 4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/I ' C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 ' CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 70130% i ND = Not detected j = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound EMffi 21 of 82 MA►CCUTEST. M73538 i_a;,or•,+,-•;es 1 Accutest Laboratories ' Report of Analysis Page 1 of 1 b Client Sample ID: MW-39 (88) Lab Sample ID: M73538-8 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch , Run#1 P28625.1) 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates t CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND . 2.0 ug/1 , 1634-04-4 Methyl Tert Butyl Ether 20 1 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 u /1 I _ g 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits ' 1868-53-7 Dibromofluoromethane i105% .- 79-130% 2037 26-5 Toluene D8 99% 80-120% , 460-00-4 4-Bromofluorobenzene 102% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Jill 22 of 82 ®ACCIJTEBT' M73538 Accutest Laboratories Report of Analysis Page 1 of 1 00 Client Sample ID: MW-39 (88) Lab Sample ID: M73538-8 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Met-iod: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41557.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 ' MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634 04 4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND :` 2.0 ug/I m,p-Xylene NI 2.0 ug/1 1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 ' C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# I Run#2 Limits 615-59-8 2,5-Dibromotoluene 790/6 70-130% 615-59-8 2,5-Dibromotoluene 82% 70130% S ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 23 of 82 ' ®ACCUTEST. M73538 Accutest Laboratories 1 Report of Analysis Page 1 of 1 Client Sample ID: MW-40 (85) Lab Sample ID: M73538-9 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 P28626.1) 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates ' CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether `ND ; 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol .ND . ;; 20 ug/I ' 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits ' 1868-53-7 Dibromofluoromethane 1t05:% 79-130% 2037-26 5 Toluene D8 101% 80-120% 460-00-4 4-Bromofluorobenzene 100% 80-120% 1 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 1 M11 24 of 82 12 M73538 '-' ' Accutest Laboratories Report of Analysis Page I of 1 Client Sample ID: MW-40 (85) Lab Sample ID: M73538-9 Date Sampled: 05/15/08 ' Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41558.13 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene N=D <: 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47 6 o Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9-C12 Aliphatics (Unadj.) ND 50 ug/I C9- CIO Aromatics (Unadj ) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics NI), 50 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits 615-59-8 2,5-Dibromotoluene 789/8 70-130% 615 59 8 2,5 Dibromotoluene 80% 70-130% i 1 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MB 25 of 82 GA4C.Ct.iTEST. ..........__...--.. .......--...... M73538 Accutest Laboratories ' w Report of Analysis Page 1 of 1 Client Sample ID: MW-31 (55) Lab Sample ID: M73538-10 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 P28627.1) 1 05/29/08 AMY n/a n/a MSP952 Run#2 Purge Volume Run#1 5.0 ml Run#2 Oxygenates t CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND;, 1.0 ug/1 994-05-8 tent-Amyl Methyl Ether ND . 2.0 ug/1 ' 75-65-0 Tert Butyl Alcohol ND 20 ug/l 637-92-3 tert-Butyl Ethyl Ether 1VD 2.0 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 1868-53-7 Dibromofluoromethane 102% 79-130% 2037-26-5 Toluene-D8 100% 80-120% 460-00-4 4-Bromofluorobenzene 98% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q�B 26 of 82 M73538 ' Accutest Laboratories tClient Sample ID: MW-31 (55) Report of Analysis Page 1 of 1 0 Lab Sample ID: M73538-10 Date Sampled: 05/15/08 Mat-ix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41559.D 1 05/28/08 AF n/a n/a GWX1970 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 ' MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene ND - 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I 163�-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND, 2.0 ug/1 m,p-Xylene ND ; 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 ' C5 C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 79% 70130% 615-59-8 2,5-Dibromotoluene $3% 70-130% 1 ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M® 27 of 82 ®AC:CUTEST. M73538 Accutest Laboratories ' ca Report of Analysis Page I of I Client Sample ID: MW-35 (53) Lab Sample ID: M73538-11 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 R4911.1) 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates ' CAS No. Compound Result RL Units Q , 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 69.7 1.0 ug/I 994-05-8 tert-Amyl Methyl Ether 3 6 2.0 ug/1 , 75-65-0 Tert Butyl Alcohol ND 20 ug/I 637-92-3 ter(-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# l Run# 2 Limits ' 1868-53-7 Dibromofluoromethane 96%.. 79-130% 2037-26-5 Toluene-138 i00% 80-120% ' 460-00-4 4-Bromofluorobenzene YOI% 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound EME1 28 of 82' 13ACCUTEST_. M73538 I ' II ' Accutest Laboratories w ' Report of Analysis Page 1 of 1 Client Sample ID: MW-35 (53) Lab Sample ID: M73538-11 Date Sampled: 05/15/08 ' Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA t File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41560.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene ,ND.. 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 ' 163c-04 4 Methyl Tert Butyl Ether 61 7 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 ' 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) 53 1 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) NiD 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits ..... ....... .... ...... ........... ....._.... 615-59-8 2,5-Dibromotoluene 74% 70-130% 615-59 8 2,5 Dibromotoluene 776/0 70-130% ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Mo 29 of 82 M73538 Accutest Laboratories , Report of Analysis Page 1 of 1 , Client Sample ID: MW-34 (53) Lab Sample ID: M73538-12 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 ' Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 R4912.1) 1 05/29/08 AA n/a n/a MSR188 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates ' CAS No. Compound Result RL Units Q ' 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/1 ' 637-92-3 tert-Butyl Ethyl Ether NO 2.0 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits ' 1868-53-7 Dibromofluoromethane 98% 79-130% 2037-26-5 Toluene-D8 103% 80-120% ' 460-00-4 4-Bromofluorobenzene '102% 80-120% I' ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ffin 30 of 8 CIACCUTEBTR M73538 ' ' Accutest Laboratories Report of Analysis Page 1 of 1 Client Sample ID: MW-34 (53) Lab Sample ID: M73538-12 Date Sampled: 05/15/08 ' Matrix: AQ- Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project:..... SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41561.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 ' MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/t 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND . 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 ' 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I ' C9- C10 Aromatics (Unadj.) AND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND F50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run## 2 Limits 615-59-8 2,5-Dibromotoluene 730/. 70-130% 615-59-8 2,5-Dibromotoluene 76% 70130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ' ;r® 31 of 82 JjACggTEST. M73538 Accutest Laboratories t Report of Analysis Page 1 of 1 , Client Sample ID: MW-37 (53 ) Lab Sample ID: M73538-13 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 R4914.1) 1 05/29/ '08 AA n/a n/a MSR188 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates ' CAS No. Compound Result RL Units Q , 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/1 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/t 75-65-0 Tert Butyl Alcohol ND 20 ug/1 ' 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits ' 1868-53-7 Dibromofluoromethane 9:7%0 79-130% 2037-26-5 Toluene-D8 05% 80-120% 460-00-4 4-Bromofluorobenzene `102% 80-120% , ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound fll 32 of 82' 13ACCLr .E.ST. M73538 11 ' Accutest Laboratories ' Client Sample ID: MW-37 (53) Report of Analysis Page 1 of 1 G, Lab Sample ID: M73538-13 Date Sampled: 05/15/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41562.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 ' MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether N.D. 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/t 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 ' 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) I ID 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND :: 50 ug/I ' CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 75% 70-130% 615-59-8 2,5-Dibromotoluene 78% 70-130% ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Q19 33 of 82 ' 12A►CC JTEST M73538 ..- Accutest Laboratories ' ca Report of Analysis Page 1 of 1 Client Sample ID: MW-29 (68) Lab Sample ID: M73538-14 Date Sampled: 05/16/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 G81927.1) 1 05/29/08 EL n/a n/a MSG3307 Run#2 G81956.1) 2 05/30/08 EL n/a n/a MSG3308 Purge Volume ' Run#1 5.0 ml Run#2 5.0 ml Oxygenates ' CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 475 a 2.0 ug/1 994-05-8 tert-Amyl Methyl Ether 2 9 2.0 ug/I ' 75-65-0 Tert Butyl Alcohol .28,51. 20 ug/1 637-92-3 tert-Butyl Ethyl Ether �ND 2.0 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 96% 96% 79-130% 2037-26-5 Toluene-D8 97% 98% 80-120% ' 460-00-4 4-Bromofluorobenzene 96% 96% 80-120% (a) Result is from Run# 2 t ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 11 34 of 82, A ' Accutest Laboratories 51, Report of Analysis Page 1 of 1 Client Sample ID: MW-29 (68) Lab Sample ID: M73538-A Date Sampled: 05/16/08 ' Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW.97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41563.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q ' 71-43-2 Benzene 4 0 2.0 ug/1 100-41-4 Ethylbenzene N.D 2.0 ug/1 1634 04 4 Methyl Tert Butyl Ether 512 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj ) 385 50 ug/1 C9- C12 Aliphatics (Unadj ) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics NU:, 50 ug/1 C9- C12 Aliphatics N.R. 50 ug/1 ' CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene 81% 70-130% ND = Not detected j = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M11 35 of 82 ' 12ACPVt'EST M73538 '- - Accutest Laboratories , Report of Analysis Page 1 of 1 ; Client Sample ID: MW-20 (55) Lab Sample ID: M73538-15 Date Sampled: 05/16/08 Matrix: AQ - Ground Water Date Received: 05/19/08 Method: SW846 8260B Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 G81928.13 1 05/29/08 EL n/a n/a MSG3307 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 Oxygenates CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 , 75-65-0 Tert Butyl Alcohol ND 20 ug/I 637-92-3 tert-Butyl Ethyl Ether ND: 2.0 ug/I CAS No. Surrogate Recoveries Run# I Run#2 Limits 1868-53-7 Dibromofluoromethane 96% 79-130% 2037-26-5 Toluene-D8 956/0 80-120% 460-00-4 4-Bromofluorobenzene 97%' 80-120% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank , E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound © 36 of 8 M73538 ..,. .r�.1 r.r I e 0 Accutest Laboratories w Report of Analysis Page 1 of 1 ' Client Sample ID: MW-20 (55) Lab Sample ID: M73538-15 Date Sampled: 05/16/08 ' Matrix: AQ - Ground Water Date Received: 05/19/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 WX41564.1) 1 05/28/08 AF n/a n/a GWX1970 Run#2 Purge Volume Run#1 5.0 ml Run#2 ' MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND. 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadi.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 ' C9- C10 Aromatics (Unadj ) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics 50 ug/1 CAS No. Surrogate Recoveries Run# I Run#2 Limits 615'59-8 2,5-Dibromotoluene 75% 70-130% ' 615'S9 8 2,5 Dibromotoluene 79% 70-130% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®ffl 37 of 82 CIAClJTEST. M73536 1 M19 New England , 14CCU I EB I L b°'a i Section 4 ys 3Y A€€ rat Y€a€ v.tdtM€5:Y{tY M><sc Forms Custody Documents and Other Forms Includes the fallowing where applicable: ' • Chain of Custody ' • MCP Form • VPH Form • Sample Tracking Chronicle ®� 38 of 82 11ACCI.R'EST.' M73538 LAB(LOCATION) 4 Shell Oil Products Chain Of Custody Record m 3 S?>6 --�<P�lease:Cfieik�Appropl'iateBoz- --Print13J17a0oaladName _ .INCIDENTk1ENV:SEFtVIGES} pCNr«eNDINaDexr,AeruEs O AtturesY ❑M.SERVICES p NDTIYA 0.ETAIL ❑SHELL RETAIL pave Weeks 9 7 31 41 6 817181 DATE: S l« d 8 ------ ❑rrornc soe,a+ p'CDNSLCTANi ❑weEs ::pp y SAP�t 11 Z ' ❑OTHER 1 1 p �PIPS p D^'ER PAGE:1 0 0 0 8 3 alT EU laa.w.cln.aaawwl: Sovereign Consulting Inc 1140 lyannough Road,Hyannis,MA 935B South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Repon to):Jason Sherbum CONSULTANT PROJECT NO.:E073T ' :e<ProaE Mansfield.MA 02048 K uevsEowLr 508.339.3200 508.339.3248 Isherburneansovcon.com rc Gtih ��GK�✓ , �a' �g11�Sr P� TURNAROUND TIME(CALENDAR DAY5): REQUESTED ANALYSIS p'STANDARD ANDARD(1�DAY) 115 DAYS ❑3 GAYS ❑1 DAYS p H HOURS DELIVERABLES: Cl CONNA ❑CO mu O MCP ❑0.ff ❑o""ER (SPECIFY)' TEMPERATUREONRECEIPTC° —1.111 :Coale/] 1Cao1a R3 SPECIAL INSTRUCTIONS OR NOTES: 77 « SAMPLING PRESERVATNE C Field Sample lden6fication AT..DATE TIME C-01—PIDR...i,,p O a Laoorslory NotK ?IICV' F /�It✓-4Q 5 If 07ao 6W 11 IM `tl X X FRW-2.1(5' P9?0 �3; Mw-14(651 Toro { MW-3 2(ss) low Mw-26C�y) IIrO ' ' rGw- 2 S(7z) trys 14W-ZN(LIZ) 1210 $ Kw- 39(u 13ao ' 9 ptw-40 (S5) 11:10 31 (5S) 14ds ' as n<E'l /Z+ aY,•vti Ren<iPn OL. �c 31-5- 3-14 a.5 ' M73.538: Chain of Custody Page 1 of 2 Q� 39 of 82 ®ACCUTESTR M73538 - LAB(LOCATION) Shell Oil Products Chain Of Custody Record late Print Bill Tp:Contact:Nim[6; :ANCIDENTWIEWSERVICIES 9­1E11 RUA �: C. V NO INcioDn t MPUES ACC�W Dave Weeks' 91 71 31 41 61 81 7 1 8 GATE: �� .. ............ 0 OT PAGE. j [0oT­___. 1 1 1 1 1 1 1 1 1 1 1701 01 01 R I Sovereign Consulting Inc 1140 Innnough Road,Hyannis,MA 905E South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Report to)Jason She Mansfield,MA 02048 n�CONSULTANT PROJECTNO.:EQ711 sae ..... .. .... .. ..... ...... isherburne(@.sovcon.com �yu ) G /�� Wkl�eeS M (! �T :; , 0 3DAYS 0 2 DAYS Cl 24 HOURS REQUESTED ANALYSIS DELIVEPAsLes: 0 Co ma 111 MCP 0 RCP 0 OTH (SPEC-) TEMPERATURE ON Cooler 1 ;Cook AT c_l­3 SPECIAL INSTRUCTIONS OR NOTES ... SAMPLING Field Sample Identification DATE TIME CeN1. C.M.M.,PlD iteading. T­ > 0 «Lab«alOry Notes M W-3 5-(5 3 VIA* 1335r C,w K u 14 X X 14w-31t 01) ) /300 1 1 Mw- 37.(s3> 12zg msv-7 1(6S 5 16 41 1,ir (r5 7) R&O Ti— aszao««leo. oZt,j�, , M73538: Chain of Custody Page 2 of 2 40 of 82 12.ACCLMEST ............ M73538 Massachusetts Department BWSC-CAM Exhibit VII A-1 of Environmental Protection 21 May 2004 Revision No. 3.2 Bureau of Waste Site Cleanup Final Page 10 of 32 A N Title: MADEP MCP Response Action Analytical Report Certification Form s Laboratory Name: Accutest Laboratories of New England Project#: M73538 ' Project Location: SCMAW:97346878(REIMBMA)1140 lyannough Road MADEP RTN None Hyannis MA This form provodes certifications for the following data set: M73538-1,M73538-10,M73538-11,M73538-12,M73538-13,M73538-14,M73538-15,M73538-2 M 73538-3,M 73538-4,M 73538-5,M73538-6,M 73538-7,M73538-8,M 73538-9 Sample Matrices Groundwater X Soil/Sediment () Drinking Water () Other: () () � F MCP SW$ 6 8260E X 8151A 8330_U 6010E 7470A/1A y iflelho'Sr seEt 8270C O 8081A ( VPH X) 6020 9014M z ssptfieduhA�P� 8082 ) 8021B ( EPH O 7000 S 3 O 7196A Compendiurt�of� 1Ls"Rele�s ;,Braclnn N mbsr`a(aRTf J )f�{(rlvwn k ` An�aly�tI Methsa 2 MSW8463��g014 or�MAf�FPPhys a ogically va�lableCyan+deq{PACE)Method C�@�C�C aid"that� )� (�3��?'�SW-846t���a 0©Senes Lt�`ttrrdividua`mettiod An affirmative response to questions A, B, C, and D is required for"Presumptive Certainty status A Were all samples received by the laboratory in a condition consistent with 2 Yes ❑ No ' ' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and 2 Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty",as described in Section 2.0(a),(b), (c)and 21 Yes ❑No ' (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only:Was the VPH or EPH method run without E Yes ❑No significant modifications,as specified in Section 11.3? A response to questions E and Fbelow is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the Yes ❑ No specified methods achieved? Refer to Narrative F Were results for all analyte-list compounds/elements for the specified ❑ Yes LI No ' method(s)reported? Refer to Narrative All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this ' analytical report is, to the best of my knowledge and belief, accurate and complete. Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 06/12/2008 Uri 41 of 82 ' 0AMUTE.BT. M73538 i MADEP VPH FORM msim EM Aqueous Fy-1 Soil F-I Sediment n Other Curt.arners w Satisf act or ✓ Broken f Leaking f 1 A u outs Preservatives N/A H <=2 ✓, H >2 �eGhitr� � Received on !Ice r-1 Received at 4 De . C Other ✓ Read at z.5 deg c Wifffib"NONEWOM NIA A. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-9R Lab ID: M73538-1 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: ' N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q ' C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 ' Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 ' Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 9547-6 C9-C12 ug/1 ND 2 ' m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges ' C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 ' Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 76 70-130% PID:2,5-Dibromotoluene % 85 70-130% Footnotes i A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-CS Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude ' conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A U qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes No-Details Attatched ' Were all performance/acceptance standards for required QA/QC procedures achieved? CiYes l__' No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? JNo i._.' Yes-Details Attatched I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for ' obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director ' Printed Name Reza Tand Date 6/12/2008 QLJ 42 of 820 ®A M73538 ..„t...... ... ' MADEP VPH FORM Matrtx .g N :sA Aqueous Soil Sediment F1 Other I Curt>talEners ,.. .,�, d Satisfactory I41 Broken - Leaking ' 1 A�"u_eous Preservatives N/A pH <=2 IW PH >2 Fj Tom eatUie� � Received on Ice 0 Received at 4 Deg. C El Other �' Redd at 2.5 deg C AJ1ethatol , y N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-21 (55) Lab ID: M73538-2 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 ' Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/I ND 2 ' Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 76 70-130% PID:2,5-Dit,romotoluene % 86 70-130% ' Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range a Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(,)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Y qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? I-..!Yes _ No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No Yes-Details Attatched ' I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and j complete. ' Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 Q11 43 of 82 MACCITTEST. M73538 : 1-1 MADEP VPH FORM ' Ma#nx A ueous Pe Soil Sediment I Other I Conttar-iers „5� Satisfactor Broken 71 Leakin Ar` u'eous�Prese�iattves; N/A F , PH <=2 E%* H >2 ' TAerpa#urea; Received on Ice Received at 4 Deg. C Other .I Rec'd at 2.5 deg C r tetrha �o1 A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-19(55) Lab ID: M73538-3 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: - N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics (Unadj.) N/A u /1 ND 9 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analvtes Ethy(benzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 , Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m, -X lene P Y C9 C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND e 50 ' C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range ' FID:2,5-Dibromotoluene % 77 70-130% PID:2,5-Dibromotoluene % 87 70-130% Footnotes ' A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analyles eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude ' conc of Target Analyles eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes No-Details Attatched ' Were all performance/acceptance standards for required QA/QC procedures achieved? ✓_Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? Imo'No L.] Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for ' obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director ' Printed Name Reza Tand Date 6/12/2008 Q(J 44 of 82 �AC�JIEST.� M73538 - MADEP VPH FORM A ueous w, Soil i' Sediment i i Other C.antalEners.mxh ,.,, :, Satisfactor i Broken Leaking MbMszPrese gat ues'- N/A Ej pH <=2 Fej PH >2 T e attrre Received on Ice F1 Received at 4 Deg. C r- Other Fy-j Rec'd at 2.5 deg C MetC}anol� N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-32(55) Lab ID: M73538-4 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 5/28/2008 N/A ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-Cl 2 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/1 2.4 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID.2,5 Dibromotoluene % 79 70-130% PID:2,5-Dibromotoluene % 88 70-130% ' Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? !✓Yes F ii No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? LV]Yes !__I No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? EVI No r j Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 ' Q® 45 of 82 OACCUTFST. M73538 -a- -- - i MADEP VPH FORM Matrix' �� Aw Aqueous ✓ Soil Sediment 1 Other Containers` p .' Satisfactory n Broken Leaking ueota�reservatiues: N/A H <--2 Fri PH >2 Trem Received on Ice rn Received at 4 Deg. C Other ✓' Rec'd at 2.5 deg C Met alai �., N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-26(72) Lab ID: M73538-5 Ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: i N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q ' C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND A 50 C9-C12 Aliphatics('Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-Cl 2 ugh ND 2 ' Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 40.1 2 i Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-Cl 2 ug/I ND 2 i m,p-Xylene C9-Cl 2 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 ---- - - ... -- - ---- --... Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'Yqualifier indicates an estimated value 1 Were all QA/QC procedures REQUIRED by the VPH Method followed? I '1Yes L_i No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? L No '. Yes-Details Attatched I attest under the pains and penalties of perjury that, based upon my inquiry of those individuals immediately responsible for i obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director i Printed Name Reza Tand Date 6/12/2008 Q11 46 of 82i ®ACCIJ MST. ........................................... M73538 i tMADEP VPH FORM Matrtx..:. cx� A ueous we Soil Sediment _ Other Satisfactory F*_*1 Broken Leaking F ' ueots Preservatlue`s N/A Ll PH <=2 Wi H >2 1 Tern eratur Received on Ice Received at 4 De . C Other �I Rec'd at 2.5 deg C N1eihanoi r �T "'n ' N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-25(72) Lab ID: M73538-6 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A ' FID: 25-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/1 ND A 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analvtes ' Ethylbenze-te 100-41-4 C9-Cl 2 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/1 ND 2 Methyl Tert Butyl Ether 1634-04A C5-C8 ug/I 21.1 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalere 91-20-3 N/A ugh ND 3 o-Xylene 95-47-6 C9-Cl 2 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 A-diusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 1 _ ..._.-- -- -- - ----- Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon;Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon range data exclude concentrations of any surrogate(,)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier i idicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ' :Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? :Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? Vi No _... Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 f® 47 of 82 ' GAC CUTEST: M73538 MADEP VPH FORM ' A ueous I�i Soil Sediment Other F Satisfactory W Broken I Leakin ark`.wei A ueou�s Rr eservatlwes, N/A H <=2 I� H >2 Tent ei Received on Ice L Received at 4 Deg. C Other J Rec'd at 2.5 deg C 01614%ol N/A �a Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-24(42) Lab ID: M73538-7 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/t ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 ' Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/1 ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 , m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 ' C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 84 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AU qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? I�Yes !._. No-Details Attatched ' Were all performance/acceptance standards for required QA/QC procedures achieved? Yes -.- No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? No '_ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for , obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director ' Printed Name Reza Tand Date 6/12/2008 Q� 48 of 8 13A M73538 ''' I MADEP VPH FORM MatrizX' ' A ueous ✓ Soil . Sediment i 1 Other 1 ConYalners3 ; Satisfactory✓ Broken 1 Leaking 1 1 A ueausPreservatlues N/A H <=2 PH > 2 171 Tem, 'eratu�e _ Received on Ice Received at 4 Deg. C Other ✓! Rec'd at 2.5 deg C McYhano N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-39(88) Lab ID: M73538-8 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 ' C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes ' Ethylbenzene 100-41-4 C9-C12 ug/1 ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-X.ylene. C9-C12 ug/I ND 2 ' Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9_C12 Aliphatics N/A ug/I ND` 50 1 Surrogate Reccveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Ditromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of a-ty surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude gong of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. z A V qualifier irdicates an estimated value Were all QA/QC procedures REQUIRED b tYe VPH Method followed?P Y Yes 1 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? LYes L No-Details Attatched Were any significant modifications made to'.he VPH method,as specified in Sect. 11-3? J No 1 Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director 6/12/2te Printed Name Reza Tand Da 008 QB 49 of 82 13 ACCUTE_BT M73538 - e_ L 1 MADEP VPH FORM Aqueous w Soil Sediment F_' Other rl Conf lnelrs � Satlsfactor Broken , Leakin ' ueQus ?r ser nataves N/A D PH <=2 ✓' PH >2 n Tern Received on Ice r_1 Received at 4 Deg. C Other ✓ Rec'd at 2.5 deg C MR N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-40(85) Lab ID: M73538-9 is Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ` PID: 2,5-Dibromowluene N/A 5/28/2008 N/A FID: 2,5-Dibromo* luene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 ' Target Analytes Ethylbenzene 100-41-4 C9-Cl 2 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 r Naphthalene� 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 ' C9-C12 Aliphatics N/A ug/I ND` 50 -—---- -.. - -- - - - ---------- Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 78 70-130% PID:2,5-Dibromotoluene % 80 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. - C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A 7 qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? IIYes -! No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? keIYes _ No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? �'No Lr Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 [NB 50 of 8 A ....................._....._...... M73538 - ` ''' 11 MADEP VPH FORM Ma#rtx A ueous Wei Soil Fi Sediment F- Other Contahners , F ,, E Sati sfactory W, Broken —i Leakin A ueous Pr se ervkat`Tves N/A p H <=2 L.,j pH >2 f Tern eraturE Received on Ice Received at 4 Deg. C Other Reed at 2.5 deg C iVlethaiolwy N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-31 (55) Lab ID: M73538-10 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Anmatics(Unadj.) N/A ug/I ND A 50 ' C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-Cl 2 ug/1 ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tart Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 ' Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-Cl 2 ug/1 ND 2 m,p-Xylene C9-Cl 2 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% PID:2,5-Ditromotoluene % 83 70-130% Footnotes A Hydrocarbon F:ange data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon P.ange data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. i Z A'Yqualifier irdicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 4Yes 1-.._., No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? FWl Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? Lv!No !__; Yes-Details Attatched ' I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and Icomplete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 QB 51 of 82 ®ACC XrEST. M73538 i a MADEP VPH FORM Matdrtx A� Aqueous W,, Soil � '-1 Sediment � I Other _ Leaking Con3talners.. kx Satisfactor ✓I Broken ueous Preservatives N/A PH —2 Ey', PH >2 T€$11 e #tteE Received on ice i Received at 4 Deg. C Other ./ Rec'd at 2.5 deg C Methanol N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-35(53) Lab ID: M73538-11 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I 53.1" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 ' Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 61.7 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-Cl 2 ug/I ND 2 m,p-Xylene C9-Cl 2 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 74 70-130 PID:2,5-Dibromotoluene % 77 70-130% Footnotes ' A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ✓_Yes I No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes L No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? '_✓_.!No _ Yes-Details Attatched , I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 QEJ 52 of 82 t3 AC+CUT1BT� M73538 MADEP VPH FORM Aqueous Soil r-, Sediment 7 Other Coh#alit s � Satisfactory[y Broken 1 Leaking ueotas Pr+servatly s N/A D P H <=2 Lv] H >2 Tim eraW&64 r: Received on Ice Received at 4 De . C Other `✓ Reed at 2.5 deg C Methanol '"< '' N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-34(53) Lab ID: M73538-12 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 C5-C8 Alip-iatics(Unadj.) N/A ug/I ND' 50 C9-C12 Ali:)hatics(Unadj.) N/A ug/I ND" 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ug/I NO 2 ' Naphthalen= 91-20-3 N/A ug/I NO 3 Benzene 7143-2 C5-C8 ug/1 NO 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I NO 2 m,p-Xylene C9-Cl 2 ug/l ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I NO 2 Adjusted Ranges C5-C8 Alip-iatics N/A ug/I ND e 50 C9-C12 Aliohatics N/A ug/I ND' 50 —_- --------_.----- Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 76 70-130% FID:2,5-Dibromotoluene % 73 70-130% Footnotes A Hydrocarbon Fange data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Fange data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration cf Target Analytes eluting in that range. C Hydrocarbon Fange data exclude concentrations of aiy surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. z A V qualifier indicates an estimated value tWere all QA/QC procedures REQUIRED by the VPH Method followed? [-*]yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? L Yes E-i No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? Fle�No [_I Yes-Details Attatched ' I attest under tre pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the irformation,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 ®B 53 of 82 MACCUTEST, M73538 i a 1 � MADEP VPH FORM , Aqueous dl Soil 71 Sediment 71 Other F-1 Sat isfactor 'y Broken 1 Leaking 'eruvattV68� N/A E pH <=2 pH >2 1 TeR7 �ttc Received on Ice Received at 4 Deg. C Other .I Reed at 2.5 deg C = N/A ,p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(53) Lab ID: M73538-13 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/15/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units. Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND A 50 1. C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 ' Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/1 ND 2 1 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Toluene 108-88 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-Cl 2 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges 1 C5-C8 Aliphatics N/A ug/I ND' 50 C9-C12 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 78 70-130% FID:2,5-Dibromotoluene % 75 70-130% Footnotes 1 A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude 1 conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value 1 Were all QA/QC procedures REQUIRED by the VPH Method followed? W_Yes No-Details Attatched 1 Were all performance/acceptance standards for required QA/QC procedures achieved? ISlIYes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? i No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 M12 B 54 of 8 A ..........._................................ M73538 MADEP VPH FORM A ueous ICI Soil Sediment —I Other Can.tainers 3 Sat is factory h! Broken F 1 Leaking ueous�Pr�eseruatlwves� N/A _ I PH <=2 �� H >2 T= Received on Ice Received at 4 Deg. C Other L Rec'd at 2.5 deg C Mthano N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-29(68) Lab ID: M73538-14 to Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/16/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I 385 A 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I 4 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 512 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 C9_C12Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 81 70-130% FID:2,5-Dibromotoluene % 77 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target.Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes i._i No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? (]Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W No i Yes-Details Attatched ' I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and I complete. ' Signature Postition Laboratory Director Printed Name Reza Tand Date 6/12/2008 ®B 55 of 82 QACCIL E C M73538 :.a- . MADEP VPH FORM Aqueous W1 Soil i Sediment 1 - Other Satisf act or Broken n Leaking ueousPeservaflues N/A I: H <=2 Wi PH >2 Tema er f re ,,: Received on Ice L! Received at 4 Deg. C Other ✓ Redd at 2.5 deg C (Netao( N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-20(55) Lab ID: M73538-15 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 5/16/2008 Date Received: 5/19/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 5/28/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 rn,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges ' C9-C12 Aliphatics N/A ug/I ND c 50 C5-C8 Aliphatics N/A ug/I ND' 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 79 70-130% FID:2,5-Dibromotoluene % 75 70-130% Footnotes E ' A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ✓Yes I-1 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W Yes !-_I No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W1 No 0 Yes-Details Attatched ' I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete. Signature Postition Laboratory Director ' Printed Name Reza Tan Date 6/12/2008 MEJ 56 of 82 QA Accutest Laboratories Internal Sample Tracking Chronicle fShell Oil Job No: M73538 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes �13��8�I�Coll cued 1��5�MAY�08�(1��0f1 By RI�3 �Recervecl�MAY 08 By " � � M73538-1 MADEP VPH REV 1.128-MAY-08 05:29 AP VMAVPH M73538-1 SW846 8260B 29-MAY-08 20:37 AA V82600XY5 117�3538 2� ollecicYIS MAY ?$0 "� Il+ RD� �RcQv�ed9MAY 08By " M73538-2 MADEP VPH REV 1.128-MAY-08 06:12 AP VMAVPH M73538-2 SW846 8260B 29-MAY-08 21:04 AA V82600XY5 M�73538 3 Collectec1 �M� Y010QBy RDA Receed �9,MAY . .H . . _ ems' , M73538-3 MADEP VPH REV 1.128-MAY-08 06:54 AP VMAVPH M73538 3 SW846 8260B 29 MAY 08 21 31 AA V82600XY5 )147353 4 ollected1*1 MANY 0$ K MW 3 Z 55 15 10 40Y1)s " Receve� 19VItY 0$ ByeH , { rs. M73538-4 MADEP VPH REV 1.128-MAY-08 07:37 AP VMAVPH M73538-4 SW846 8260B 29-MAY-08 21:58 AA V82600XY5 M3�538 S �Colletec 151VAYBO B IZecived 19 MAY �By` M73538-5 MADEP VPH REV 1.128-MAY-08 08:19 AF VMAVPH M73538-5 SW846 8260B 29-MAY-08 15:04 EL V82600XY5 M7 538 6 Collected�15 N1A ' 08 11 45 3 RD )�ecetve- - D MAY i18 By 5 M73538-6 MADEP VPH REV 1.128-MAY-08 09:03 AF VMAVPH M73538 6 SW846 8260B 29 MAY 08 19:11 AMY V82600XY5 M73538 7 �Collected 15 MAY 08 12 �O.�B,y �RD ,;� Received„^19-MAY�8 By �� � M73538-7 MADEP VPH REV 1.128-MAY-08 09:47 AF VMAVPH Page 1 of 3 57 of 82 CIACGLT M73538 1 Accutest Laboratories Internal Sample Tracking Chronicle � Shell Oil SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Job No: M73538 Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M73538-7 SW846 8260B 29-MAY-08 19:39 AMY V82600XY5 MP58 8 Coll 06b4, 15 MY �B I3�0U By RD Rcceiv�d9aMAY08 By s i M 39 (88) aw x h M73538-8 MADEP VPH REV 1.128-MAY-08 10:31 AF VMAVPH ' M73538-8 SW846 8260B 29-MAY-08 20:07 AMY V82600XY5 73 3$ Collected 15 MAY 18 13 50 By � R e vw 19 MAY p8 By e M73538-9 MADEP VPH REV 1.128-MAY-08 11:16 AF VMAVPH M73538-9 SW846 8260B 29-MAY-08 20:35 AMY V82600XY5 M7358 10 Collected: 1N 5 eceved ' 9MAX }8 By .5 R ' . , e ,., v,... M73538-10 MADEP VPH REV 1.128-MAY-08 12:00 AF VMAVPH ' M73538-10 SW846 8260B 29-MAY-08 21:03 AMY V82600XY5 Ms38 1 I olleted 15�AYF0813 35Y� RDA leceXved`� 11AY 08By ' M73538-11 MADEP VPH REV 1.128-MAY-08 12:44 AF VMAVPH M73538-11 SW846 8260B 29-MAY-08 14:05 AA V82600XY5 �U173538 lf� Collected 15 MAY 08 13 OQ By� R ceived 19 v1Y'08 -�y `� k M73538-12 MADEP VPH REV 1.128-MAY-08 13:29 AF VMAVPH M73538-12 SW846 8260B 29-MAY-08 14:32 AA V82600XY5 M7358 �3Collectedl5 MAY118 12 25 By Rt Rgceived 19�MY�Y.08 $y lNO W7 }• m -- M73538-13 MADEP VPH REV 1.128-MAY-08 14:13 AF VMAVPH M73538-13 SW846 8260B 29-MAY-08 16:53 AA V82600XY5 Page 2 of 3 58 of 8 12 A __ _............' M73538 ' Accutest Laboratories Internal Sample Tracking Chronicle Shell Oil Job No: M73538 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' Project No: EQ 711 Sample ' Number Method Analyzed By Prepped By Test Codes M73538-14 MADEP VPH REV 1.128-MAY-08 14:50 AF VMAVPH ' M73538-14 SW846 8260B 29-MAY-08 22:57 EL V8260OXY5 M73538-14 SW846 8260B 30-MAY-08 13:59 EL V8260OXY5 M7��538 15 Collected 16 NI��Y08�08�45 By�RD`�7` �Receiver1�19 �AY�O$��By�'� '��'F` y� � `� r .. M73538-15 MADEP VPH REV 1.128-MAY-08 15:34 AF VMAVPH M73538-15 SW846 8260B 29-MAY-08 23:25 EL V8260OXY5 ' Page 3 of 3 59 of 82 ' ®ACCUTEST M73538 New England A=u-rssr '0 t...r Section 5 GCWS Volatiles QC Data Summaries 1 � Includes the following where applicable: ' • Method Blank Summaries • Blank Spike Summaries 1 • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries 1 1 1 i 1 i 60 of 8 12A ................................................_ M73538 Method Blank Summary Page 1 of 1 Job 'Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' MSG3306-MB G81900.1) 1 05/29/08 EL n/a n/a MSG3306 w 3 The QC reported here applies to the following samples: Method: SW846 8260B ' M73538-5 ' CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/I ' 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 75-65-0 Tert Butyl Alcohol ND 20 ug/l 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/l CAS No. Surrogate Recoveries Limits ' 1868-53-7 Dibromofluoromethane 97% 79-130% 2037-26-5 Toluene-D8 98% 80-120% 460-00-4 4-Bromofluorobenzene 100% 80-120% 1 I, Q� 61 of 82 ' 13ACCtITEST M73538 Method Blank Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSP952-MB P28608.1) 1 05/29/08 AMY n/a n/a MSP952 ' w i The QC reported here applies to the following samples: Method: SW846 8260B M73538-6, M73538-7, M73538-8, M73538-9, M73538-10 ' CAS No. Compound Result RL Units Q ' 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 994-05-8 tert-Amyl Methyl Ether ND 2.0 ug/1 ' 75-65-0 Tert Butyl Alcohol ND 20 ug/l 637-92-3 'tert-Butyl Ethyl Ether Np 2.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 102% 79-130% ' 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene 164% 80-120% ® 62 of 82 ®AC lJ7ES..T. .............................................. M73538 - ' Method Blank Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR188-MB R4910.1) 1 05/29/08 AA n/a n/a MSR188 ' The QC reported here applies to the following samples: Method: SW846 8260B ' M73538-1, M73538-2, M73538-3, M73538-4, M73538-11, M73538-12, M73538-13 ' CAS No. Compound Result RL Units Q 108-20-3 Di-Isopropyl ether ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 994 05 8 tert Amyl Methyl Ether ND 2.0 ug/l 75-65-0 Tert Butyl Alcohol ND 20 ug/l 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Limits ' 1868-53-7 Dibromofluoromethane 97% 79-130% 2037-26-5 Toluene-D8 103%:... . 80-120% 460-00-4 4-Bromofluorobenzene 101% 80-120% Q� 63 of 82 ' 12ACCI (TEST M73538 a_ Method Blank Summary Page 1 of 1 ' Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3307-NIB G81926.1) 1 05/29/08 EL n/a n/a MSG3307 , o, The QC reported here applies to the following samples: Method: SW846 8260B M73538-14, M73538-15 ' CAS No. Compound Result RL Units Q ' 108-20-3 Di-Isopropyl ether ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l 994 05 8 tert Amyl Methyl Ether ND 2.0 ug/l , 75-65-0 Tert Butyl Alcohol NEY. 20 ug/I 637-92-3 tert-Butyl Ethyl Ether ND 2.0 ug/1 CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 960/. 79-130% ' 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene 97% 80-120% ® j 64 of 82 �AGCUTEST.' M73538 ' Method Blank Summary Page I of I Job Number: M73538 ' Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' MSG3308-MB G81952.1) 1 05/30/08 EL n/a n/a MSG3308 w The QC reported here applies to the following samples: Method: SW846 8260B M73538-14 ' CAS No. Compound Result RL Units Q 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/l ' CAS No. Surrogate Recoveries Limits ' 1868-53-7 Dibromofluoromethane 93% 79-130% 2037-26-5 Toluene-D8 99% 80-120% 460-00-4 4-Bromofluorobenzene 97% 80-120% I 65 of 82 13ACCUTEST. M73536 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 , Job Number: M 73538 Account: SHELLWIC She'll Oil ' Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3306-BS G81898.1) 1 05/29/08 EL n/a n/a MSG3306 ' MSG3306-BSD G81899.1) 1 05/29/08 EL n/a n/a MSG3306 N The QC reported here applies to the following samples: Method: SW846 8260B t M73538-5 ' Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/I % ug/I % RPD Rec/RPD ' 108-20-3 Di-Isopropyl ether 50 50.0 100 49.1 98 2 56 145/25 1634-04-4 Methyl Tert Butyl Ether 50 49.3 99 49.1 98 .0 70 130/25 994-05-8 tert-Amyl Methyl Ether 50 50.7 101 50.4 101 1 51-138/25 ' 75-65-0 Tert Butyl Alcohol 500 490 98 499 100: 2 60-146/25 637-92-3 tert-Butyl Ethyl Ether 50 52.0 1.04'; 51.6 103 1 ` 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits I 1868-53-7 Dibromofluoromethane 99% 100% 79-130% ' 2037-26-5 Toluene-D8 80-120% 460-00-4 4-Bromofluorobenzene 9.3% 93% 80-120% v g® 66 of 82 �ACCIJTE WT. ' M73536 ' Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 ' Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID -DF Analyzed By Prep Date Prep Batch Analytical Batch MSP952-BS P28605.1) 1 05/29/08 AMY n/a n/a MSP952 MSP952-BSD P28606.D 1 05/29/08 AMY n/a n/a MSP952 w iv The QC reported here applies to the following samples: Method: SW846 8260B ' M73538-6, M73538-7, M73538-8, M73538-9, M73538-10 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/I % ug/l % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 51.0 102 51.2 102 0 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 50.0 100 49.9 1;00 0 70 130/25 994 05 8 tert-Amyl Methyl Ether 50 42.7 85 44.7 89 5 51 138/25 75-E•5-0 Tert Butyl Alcohol 500 531 P06 517 103' 3 60 146/25 637-92-3 tert-Butyl Ethyl Ether 50 44.5 89 45.3 91 2 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits ' 1868-53-7 Dibromofluoromethane 100% 1Q2% . 79-130% 2037-26-5 Toluene-D8 100% _ _ ..1.00% 80-120% .................._... ....... .. ......_...._.. 460-00-4 4-Bromofluorober.zene 96% 96% 80-120% li I 67 of 82 ' ®ACCLITEST. M73538 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 ' Job Number: M73538 Account: SHELLWIC Shell Oil , Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSR188-BS R4908.D 1 05/29/08 AA n/a n/a MSR188 ' MSR188-BSD R4909.1) 1 05/29/08 AA n/a n/a MSR188 iv The QC reported here applies to the following samples: Method: SW846 8260B M73538-1, M73538-2, M73538-3, M73538-4, M73538-11, M73538-12, M73538-13 , Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/I % ug/I % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 35.0 70 33.6 67 i 4 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 56.5 113" 53.6 1'07 5 70-130/25 994-05-8 tert-Amyl Methyl Ether 50 60.9 122 57.0 114 7 51-138/25 I 75-65-0 Tert Butyl Alcohol 500 367 13 389 78 :: 6 60-146/25 637-92-3 tert-Butyl Ethyl Ether 50 47.8 96. 45.6 91 5 46-147/25 CAS No. Surrogate Recoveries BSP BSD Limits 1868-53-7 Dibromofluoromethane 100% 98%0 79-130% ' 2037-26-5 Toluene-D8 T03% 104% 80-120% 460-00-4 4-Bromofluorobenzene 1.,01916 102% 80-120% 68 of 82 12A[ UTEE. M73538 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' MSG3307-BS G81924.D 1 05/29/08 EL n/a n/a MSG3307 MSG3307-BSD G81925.1) 1 05/29/08 EL n/a n/a MSG3307 iv The C reported here applies to the following samples: Method: SW846 8260B Q P PP g P M73538-14, M73538-15 Spike BSP BSP BSD BSD Limits ' CAS No. Compound ug/I ug/l % ug/I % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 50 48.7 97 47.1 94 3. 56-145/25 1634-04-4 Methyl Tert Butyl Ether 50 49.0 1&1., 47.5 95 3 ' 70-130/25 ' 994-05-8 tert-Amyl Methyl Ether 50 51.3 103 50.8 102 1 51 138/25 75-65-0 Tert Butyl Alcohol 500 504 101 486 97 4 60-146/25 637-92-3 tert-Butyl Ethyl Ether 50 51.5 103 50.0 100' 3 46-147/25 S CAS No. Surrogate Recoveries BSP BSD Limits ' 1868-53-7 Dibromofluoromethane 98% 98%0 79-130% 2037-26-5 Toluene-D8 98% 996/o 80-120% 460-00-4 4-Bromofluorobenzene 9:3% 929/ 80-120% 1 I 1 I Q� 69 of 82 ' t3ACCUTEST. M73538 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 ' Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch MSG3308-BS G81949.1) 1 05/30/08 EL n/a n/a MSG3308 ' MSG3308-BSD G81950.1) 1 05/30/08 EL n/a n/a MSG3308 The QC reported here applies to the following samples: Method: SW846 8260B M73538-14 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/l ug/I % ug/I % RPD Rec/RPD , 1634-04-4 Methyl Tert Butyl Ether 50 47.4 -95 46.3 93, 2 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits ' 1868-53-7 Dibromofluoromethane 96% 96% 79-130% 2037-26-5 Toluene-D8 100%° 99% 80-120% 460-00-4 4-Bromofluorobenzene 92% 92% 80-120% i F 1 I Q� 70 of 82 AMIJT6S'r,' M73538 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73491-21MS G81921.D 1 05/29/08 EL n/a n/a MSG3306 M73491-21MSDG81922.D 1 05/29/08 EL n/a n/a MSG3306 w M73491-21 G81919.D 1 05/29/08 EL n/a n/a MSG3306 LI) The QC reported here applies to the following samples: Method: SW846 8260B IN M73538-5 M73491-21 Spike MS MS MSD MSD Limits ' CAS No. Compound ug/I Q ug/1 ug/I % ug/I % RPD Rec/RPD 108-20-3 Di-Isopropyl ether ND 50 52.7 1,05 50.3 101 5 54-155/30 1634 04 4 Methyl Tert Butyl Ether ND 50 48.9 98 48.7 97 0 54 144/30 994<05-8 tert-Amyl Methyl Ether ND 50 49.4 99 50.1 1+00 1 47-142/30 75-65-0 Tert Butyl Alcohol ND 500 486 97 494 99 2 60-148/30 637-92-3 tert-Butyl Ethyl Ether ND 50 52.5 I05 51.4 1013 2 46-151/30 CAS No. Surrogate Recoveries MS MSD M73491-21 Limits ' 1868-53-7 Dibromolluoromethane 1.04% 101% 104% 79-130% 2037-26-5 Toluene-D8 98% 98% 99% 80-120% 460-00-4 4-Bromofluorobenzene 9A% 93% 101% 80-120% III I Q� 71 of 82 j3ACCt.!'(I T. M73538 ' ' - Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73513-5MS P28628.1) 5 05/29/08 AMY n/a n/a MSP952 ' M73513-5MSD P28629.1) , 5 05/29/08 AMY n/a n/a MSP952 M73513-5 P28615.1) 1 05/29/08 AMY n/a n/a MSP952 is The QC reported here applies to the following samples: Method: SW846 8260B PP g M73538-6, M73538-7, M73538-8, M73538-9, M73538-10 ' M73513-5 Spike MS MS MSD MSD Limits CAS No. Compound ug/I Q ug/l ug/I % ug/l % RPD Rec/RPD 108-20-3 Di-Isopropyl ether ND 250 295 148 289 116° 2 54-155/30 1634-04-4 Methyl Tert Butyl Ether 1.1 250 245 98 246 98" 01. 54 144/30 994 05-8 tert Amyl Methyl Ether ND 250 164 66 167 67 2 47-142/30 ' 75-65-0 Tert Butyl Alcohol ND 2500 2820 113", 2870 115 '" 2 60-148/30 637-92-3 tert-Butyl Ethyl Ether ND 250 212 85 209 84 1 46-151/30 CAS No. Surrogate Recoveries MS MSD M73513-5 Limits 1868-53-7 Dibromofluoromethane 105% 103% 100% 79-130% ' 2037-26-5 Toluene-D8 102% 103% 1001% 80-120% 460-00-4 4-Bromofluorobenzene 910/0 93% 95% 80-120% 72 of 82 ACCUTEST' M73538 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: M73538 ' Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch ' M73577-2MS G81945.1) 5 05/30/08 EL n/a n/a MSG3307 M73577-2MSD G81946.1) 5 05/30/08 EL n/a n/a MSG3307 M73577-2 G81939.1) 1 05/30/08 EL n/a n/a MSG3307 w The QC reported here applies to the following samples: Method: SW846 8260B ' M73538-14, M73538-15 M73577-2 Spike MS MS MSD MSD Limits CAS No. Compound ug/I Q ug/I ug/I % ug/l % RPD Rec/RPD 108-20-3 Di-Isopropyl ether 0.48 250 237 95 227 91 4 54-155/30 1634-04-4 Methyl Tert Butyl Ether 531 E 250 827 118 805 110 3 54-144/30 ' 994-05-8 tert-Amyl Methyl Ether 1.2 250 254 101 247 98 3 47-142/30 75-65-0 Tert Butyl Alcohol 2490 2500 4860 95 4750 90 2 60-148/30 637 92 3 tert Butyl Ethyl Ether 1.4 250 253 1'O1 246 98 3 46-151/30 CAS No. Surrogate Recoveries MS MSD M73577-2 Limits 1868-53-7 Dibromofluoromethane 97% 96%>> 95% 79-130% 2037-26-5 Toluene-D8 100% 99% 98% 80-120% 460-00-4 4-Bromofluorobenzene 91% 93%° 98% 80-120% Q 73 of 82 ' 9IACrAJTEE T M73538 Matrix S ike/Matrix Spike Duplicate Summary p p p y Page 1 of 1 Job Number: M73538 Account: SHELLWIC She'll Oil ' Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch M73586-6MS G81965.D 5 05/30/08 EL n/a n/a MSG3308 , M73586-6MSD G81966.1) 5 05/30/08 EL n/a n/a MSG3308 M73586-6 G81964.1) 1 05/30/08 EL n/a n/a MSG3308 The QC retorted here applies to the following samples: Method: SW846 8260B M73538-14 ' M73586-6 Spike MS MS MSD MSD Limits CAS No. Compound ug/I Q ug/I ug/l % ug/l % RPD Rec/RPD 1634-04-4 Methyl Tert Butyl Ether 5.3 250 246 96 241 94 2 54-144/30 CAS No. Surrogate Recoveries MS MSD M73586-6 Limits 1868 53-7 i Dibromofluoromethane99% 99% 79-130% ' 2037-26-5 Toluene-D8 100% 99%0 971 80-120% 460-00-4 4-Bromofluorobenzene 949/ 93% 101% 80120% Q� 74 of 82 MAC' M73538 i Volatile Surrogate Recovery Summary Page 1 of 2 .lob Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: SW846 8260B Matrix: AQ ' Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 S2 S3 M73538-1 R4922.D 940` 101.0 M73538-2 R4923.D 88 0 103.0 lOZ.O M73538 3 R4924.D 88.0 ~ . 101.0 101 0 M73538-4 R4925.1) 91.0 104.0 1OV. M73538-5 G81910.1) 103 0 95.0 101 0 M73538 6 P28623.1) i01 0 103.0 101 0 M73538-7 P28624.D 105 0 100.0 10Z.0 M73538-8 P28625.D 105 0 99.0 102.0, M73538-9 P28626.1) 10 ,0 ';' 101.0 100.0_ M73538 10 P28627.1) 142 0 100.0 M73538-11 R4911.1) 96.0 100.0 1.01.0 :. M73538-12 R4912.1) 98:0 103.0 10Z-:0 ' M73538 13 R4914.D 0 97 105.0 lOZ 0 M73538-14 G81956.1) 96 a.Q. 98.0 96:0 M73538-14 G81927.1) 96 0 97.0 960 M73538-15 G81928.1) 96.0 95.0 97 0 ' M73491-21MS G81921.D 104 0 98.0 94:0 M73491-21MSD G81922.1) aOLO 98.0 930 M73513-5MS P28628.D 105.0:: 102.0 910 .. _. ' M73513-5MSD P28629.1) 103.0 103.0 93.0 M73577-2MS G81945.1) 97.0` 100.0 910 M73577-2MSD G81946.1) 96.0 .: 99.0 91'0 M73586-6MS G81965.1) 101.0 :.. 100.0 940 M73586-6MSD G81966.1) 994 99.0 930 MSG3306-BS G81898.1) 99 A.L. 98.0 930 MSG3306-BSD G81899.1) 100 0';` 99.0 93 0 MSG3306-MB G81900.D 97 0 98.0 1000. MSG3307 BS G81924.1) 98 0 " 98.0 930 MSG3307-BSD G81925.D 98.0 99.0 920 MSG3307-MB G81926.D 96.0 99.0 97'0 MSG3308-BS G81949.1) 96 0 100.0 92:0 MSG3308-BSD G81950.1) R 0 99.0 92 0 MSG3308-MB G81952.D 93.0 99.0 97110 MSP952-BS P28605.D 100:0; 100.0 96?0 ' MSP952-BSD P28606.1) 1624 :; 100.0 96 0 MSP952-MB P28608.D 102 0 99.0 104 0; MSR188-BS R4908.1) 100.0' 103.0 10 .0 MSR188-BSD R4909.1) 98 0 104.0 1.OZ.0 MSR188-MB R4910.1) 9T.0Y 103.0 101.0' as 75 of 82 ' ®ACCIJTEST M73538 :. Volatile Surrogate Recovery Summary Page 2 of 2 ' Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' Method: SW846 8260B Matrix: AQ Samples and QC shown here apply to the above method � I Surrogate Recovery Compounds Limits Surrogate Recovery ' Compounds Limits S 1 = Dibromofluoromethane 79 130% ................._............._... S2 = Toluene D8 80 1209 S3 = 4-Bromofluorobenzene 80 120% I 76 of 8 UA .......:............................._........ M73538 New England ACCUTEST } T i b o r i I'r)r e..�.t�. x S on b r€t€ CxE,A€S'.YAv GC Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries ' Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries �B 77 of 82 ' IZACCAJnssT. M73538 Method Blank Summary Page 1 of 1 , Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' Sample File ID DF Analyzed BY Prep Date Prep Batch Analytical Batch GAB2377-MB AB42642.1) 1 05/27/08 AP n/a n/a GAB2377 ' a, 'The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M73538-1, M73538-2, M73538-3, M73538-4 CAS No. Compound Result RL Units Q ' 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene N=D 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene N'D 3.0 ug/1 108-88-3 Toluene Nv 2.0 ug/1 m,p-Xylene N 2.0 ug/1 ' 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (UnadJ ) ND 50 ug/1 C9- C12 Aliphatics (UnadJ ) ND 50 ug/1 C9- C10 Aromatics (UnadJ ) ND 50 ug/I , C5- C8 Aliphatics N;D 50 ug/1 C9- C12 Aliphatics NO 50 ug/1 CAS No. Surrogate Recoveries Limits I 615-59-8 2,5-Dibromotoluene 77% 70-130% 615-59-8 2,5-Dibromotoluene 850/ 70130% I Q� 78 of 8 QA ....:.:............................_......:. M73538 -' . :.t- S Method Blank Summary Page 1 of 1 Job :Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' GWX1970-MB WX41550.D 1 05/28/08 AF n/a n/a GWX1970 m The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M73538-5, M73538-6, M73538-7, M73538-8, M73538-9, M73538-10, M73538-11, M73538-12, M73538-13, M73538- 14, M73538-15 CAS No. Compound Result RL Units Q 71 43 2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene N17 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene N'D 3.0 ug/l 108-88-3 Toluene NDI 2.0 ug/1 ' m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj ) ND 50 ug/l C9- C12 Aliphatics (UnadJ ) Nib. 50 ug/l ' C9 C10 Aromatics (Unadj ) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND . 50 ug/l CAS No. Surrogate Recoveries Limits ' 615-59-8 2,5-Dibromotoluene 79% 70-130% 615-59-8 2,5-Dibromotoluene 85% 70-130% Q� 79 of 82 ' ®ACCI,ITEST M73538 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GAB2377-BSP A1342643.1) 1 05/27/08 AP n/a n/a GAB2377 ' GAB2377-BSD A1342644.1) 1 05/27/08 AP n/a n/a GAB2377 rn The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M73538-1, M73538-2, M73538-3, M73538-4 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/1 % ug/1 % RPD Rec/RPD , 71-43-2 Benzene 50 55.2 110 53.0 106 : 4 70-130/25 100-41-4 Ethylbenzene 50 56.8 114 54.3 109 ' S 70-130/25 1634 04-4 Methyl Tert Butyl Ether 50 53.2 106 51.9 1>04 2 70 130/25 ' 91-20-3 Naphthalene 50 50.5 101 47.9 96 5 70-130/25 108-88-3 Toluene 50 53.8 108 51.5 103 4 70-130/25 m,p Xylene 100 110 110 106 106 4 70 130/25 ' 95-47-6 o-Xylene 50 53.9 108 51.5 103 5 70 130/25 C5- C8 Aliphatics (Unadj.) 150 123 82 119 79 3 70 130/25 C9- C12 Aliphatics (Unadj.) 150 118 79, 127 .85 :. 7 70-130/25 C9- C10 Aromatics (Unadj.) 50 56.8 114 54.2 108: 5 70-130/25 ' CAS No. Surrogate Recoveries BSP BSD Limits t 615-59-8 2,5-Dibromotoluene 8600. 81% 70-130% 615-59-8 2,5-Dibromotoluene 97% 91% 70-130% Q® 80 of 82 13ACCUTEST.' M73538 .,_.._,-...e Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' GWX1970-BSP WX41551.1) 1 05/28/08 AF n/a n/a GWX1970 GWX1970-BSD WX41552.1) 1 05/28/08 AF n/a n/a GWX1970 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 iv M73538-5, M73538-6, M73538-7, M73538-8, M73538-9, M73538-10, M73538-11, M73538-12, M73538-13, M73538- ' 14, M73538-15 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/I % ug/I % RPD Rec/RPD 71-43-2 Benzene 50 52.1 104 52.6 105-; 1 70-130/25 100-41-4 Ethylbenzene 50 49.6 .991 149.9 100 1 70-130/25 ' 1634-04-4 Methyl Tert Butyl Ether 50 49.8 100 50.2 100 1 70-130/25 91-20-3 Naphthalene 50 53.5 107 53.6 107 > 0 70-130/25 108-88-3 Toluene 50 51.5 103 51.9 104 1,.. 70-130/25 m,p-Xylene 100 101 101 101 101 0 70-130/25 95-47-6 o-Xylene 50 47.6 95 47.8 96 0 70-130/25 C5- C8 Aliphatics (Unadj.) 150 149 99 152 101 2 70-130/25 C9- C12 Aliphatics (Unadj.) 150 139 93. 141 94 I 70-130/25 C9- C10 Aromatics (Unadj.) 50 45 90 45 91` 1 ' 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 81% 81:°/0 _ 70-130% 615-59-8 2,5-Dibromotoluene 88% 88% 70-130% �B 81 of 82 ' 13A[ 'EST M73538 = - Volatile Surrogate Recovery Summary Page 1 of 1 , .lob Number: M73538 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method Lab Lab Sample ID File ID S1 a Sl b w M73538-1 AB42661.1) 76 0 . `', 85.0 M73538-2 AB42662.1) 76.0...-.. 'i 86.0 e M73538-3 AB42663.1) 77 0 87.0 M73538-4 AB42664.D 88.0' M73538-5 WX41554.1) 81>0 86.0 M73538-6 WX41555.D 80 0 83.0 ' M73538-7 WX41556.1) 80 0 84.0 M73538-8 WX41557.1) 79 0 82.0 M73538-9 WX41558.1) 78:0 ::.:-: : 80.0 M73538 10 WX41559.1) 79 0 83.0 ' M73538-11 WX41560.1) 74:0 77.0 M73538-12 WX41561.1) 73 0 76.0 M73538-13 WX41562.1) 75.9 78.0 ' M73538-14 WX41563.1) 77 0 81.0 M73538-15 WX41564.1) 75 79.0 GAB2377-BSD AB42644.1) 810. 91.0 GAB2377-BSP AB42643.D 86 0 97.0 GAB2377-MB A1342642.1) 7T.0= 85.0 GWX1970-BSD WX41552.1) 810 88.0 GWX1970-BSP WX41551.D 810 88.0 GWX1970IV1B WX41550.1) 79-0 85.0 ' Surrogate Recovery Compounds Limits . ...... ........... SI = 2,5-Dibromotoluene 70 130% ..... . ................ (a) Recovery from GC signal#1 ' (b) Recovery from GC signal#2 I Qffi 82 of 82 CIACCAJTEST. M73538 e-Hardcopy 2.0 Automated Report ®n New England UACCUTEST. ��L.aborator .. Y�" ":, yk Y7' A L Lt3 P it 1: t_k i 6 TAN 09/02/08 Tea�h�ni�al��Rep�l�t for. Shell Oil SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA EQ 711 Accutest Job Number: M76363 g Sam lin Date: 08/18/08 Sampling Report to: Sovereign Consulting Inc. ' 'sherburne@sovcon.com ATTN: Jason Sherburne Total number of pages in report: 55 4�9 ACCgRO.p- V 'l 1 a 4.. t * i,: • IN Test results contained within this data package meet the requirements X, and of the National Environmental Laboratory Accreditation Conference Lab Director and/or state specific certification programs as applicable. ' Client Service contact: Kristen Blanchard 508-481-6200 Certifications:MA(M-MA136) CT(PH-0109) NH(2502) RI(00071) ME(MA0136) FL(E87579) ' Y E A R $111 NY(11791) NJ(MA926) PA(68-01121) NC(653) IL(200018) NAVY USACE This report shall not be reproduced,except in its entirety,without the written approval of Accutest Laboratories. ` Test results relate only to samples analyzed. I New England 495 Tech Center West • Building 1 • Marlborough,MA 01752 • tel:508-481-6200 • fax:508-481-7753 • bttp://www.accutes(.com 1 of 55 �ACCUTEST M76363 =a�oretaries Table of Contents Sections: -1- Section 1: Sample Summary ................................................................................................... 3 Section2: Case Narrative/Conformance Summary .............................................................. 5 Section3: Sample Results ........................................................................................................ 6 3.1.: M76363-1: MW-21 (55) ............................................................................................... 7 3.2: M76363-2: MW-24 (42) 3.3: M76363-3: MW-26 (72) ............................................................................................... 9 3.4: M76363-4: MW-19 (55) ............................................................................................... 10 3.5: M76363-5: MW-20 (55) 3.6: M7636376: MW-29 (68) ............................................................................................... 12 3.7: M76363-7: MW-32 (55) 3.8: M76363-8: MW-35 (53) ............................................................................................... 14 3.9: M76363-9: MW-37 (53) ............................................................................................... 15 ' 3.10: M76363-10: MW-37 (90) 3.11.: M76363-11: MW-37 (105) ......................................................................................... ' 17 3.12: M76363-12: MW-39 (88) ........................................................................................... 18 3.13: M76363-13: MW-40 (85) ........................................................................................... 19 3.14: M76363-14: MW-38 (104) ......................................................................................... 20 3.15: M76363-15: MW-38 (89) ........................................................................................... 21 3.16: M76363-16: RW-101 .................................................................................................. 22 3.1.7: M76363-17: RW-102 .................................................................. ............. 23 ' 3.18: M76363-18: MW-25 (72) Section4: Misc. Forms ............................................................................................................ 25 4.1: Chain of Custody ........................................................................................................... 26 t 4.2: MCP Form ..................................................................................................................... 28 4.3: VPH Form ...................................................................................................................... 29 ' 4.4: Sample Tracking Chronicle ........................................................................................... 47 Section 5: GC Volatiles - QC Data Summaries ......................:.............................................. 50 5.1: Method Blank Summary ................................................................................................ 51 ' 5.2: Blank Spike/Blank Spike Duplicate Summary 5.3: Surrogate Recovery Summaries .......&......................... 55 .................................................... � I �Q 2 of 551 13ACC47EPT. M76363 I ^' 'i p l Accutest Laboratories Sample Summary ' Shell Oil ' SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Job No: M76363 Project No: EQ 711 Sample Coflected Matrix Client ' Number Date Time By Received Code Type Sample ID M76363-11.1. 08/18/08 10:30 AW 08/20/08 AQ Ground Water MW=21 (5'5 M76563.2 08/18/08 10:55 AW 08/20/08 AQ Ground Water MW-24 (42j>> 08/18/08 10:10 AW 08/20/08 AQ Ground Water MW 26 ' M7636'3 4 08/18/08 09:30 AW 08/20/08 AQ Ground Water MW49 (55)'.. M76363=5 08/18/08 13:35 AW 08/20/08 AQ Ground Water MW720 (55) M76363=:6 08/18/08 14:00 AW 08/20/08 AQ Ground Water MW-29 (68). M70363-7 08/18/08 13:15 AW 08/20/08 AQ Ground Water MW-32 (55) ' M763fi3 8: 08/18/08 12:45 AW 08/20/08 AQ Ground Water MW=35 (53) ' MO.- 0.:_ 08/18/08 11:00 AW 08/20/08 AQ Ground Water MW-37.(55). ' T'fi363-:1.11 .08/18/08 11:50 AW 08/20/08 AQ Ground Water MW-37(90) ' M76363 1.<1 08/18/08 12:15 AW 08/20/08 AQ Ground Water MW-37 (105) M783G3 12 08/18/08 12:20 AW 08/20/08 AQ Ground Water MW-39'(88) M76363 13 08/18/08 11:55 AW 08/20/08 AQ Ground Water NIW-40(85) 3 of 55 UACCLMEST M76363 " Accutest Laboratories Sample Summary ' Shell Oil (continued) SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Job No: M76363 ' Project No: EQ 711 Sample Collected. . Matrix Client Number Date Time By Received Code Type Sample ID , M76363 + 08/18/08 12:55 AW 08/20/08 AQ Ground Water MW 38 (Iq4): M76363 15: 08/18/08 13:30 AW O8/20/08 AQ Ground Water IYIW=3$ (89):: M76363 I6 08/18/08 09:40 AW 08/20/08 AQ Ground Water RW 1:01. ' M76363- 7 08/18/08 11:20 AW 08/20/08 AQ Ground Water RW 142 M76363-18 08/18/08 10:30 AW 08/20/08 AQ Ground Water MW-25 (72)' ' ® 4 of 55 L. a. boratories ' SAMPLE DELIVERY GROU P CASE NARRATIVE ' Client: Shell Oil Job No M76363 Site: SCMAW:97346878(REIMBMA)1140 Iyannough Road Hyannis MA Report Date 9/l/2008 1:46:16 PM ' 18 Sample(s)were collected on 08/18/2008 and were received at Accutest on 08/20/2008 properly preserved,at 2 Deg.C and intact. These Samples received an Accutest job number of M76363.A listing of the Laboratory Sample ID,Client Sample ID and dates of collection are presented in the Results Summary Section of this report. ' Excep as noted below,all method specked calibrations and quality control performance criteria were met for this job.For more information,please refer to QC summary pages. ' Volatiles by GC By Method MADEP VPH REV 1.1 Matrix AQ Batch ID: GBD990 ■ A]samples were analyzed within the recommended method holding time. ' ® A7 method blanks for this batch meet method specific criteria. Matrix AQ Batch ID: GBD991 All samples were analyzed within the recommended method holding time. ' All method blanks for this batch meet method specific criteria. ' The Accutest Laboratories of New England certifies that all analysis were performed within method specification.It is further recommended that this report to be used in its entirety.The Accutest Laboratories of NE,Laboratory Director or assignee as verified by the signature on the cover page has authorized the release of this report(M76363). III Monday,September 01,2008 Page 1 of 1 Mill 5 of 55 ' 12ACCUTEEST M76363 ^. . ®11 New England t MACCUTEST I..aborator:e, Section 3 Sample Results ' Report of Analysis 1 ®B 6 of 55' raACCUTEST. M76363 .. ... ....... .> ' Accutest Laboratories Report of Analysis Page 1 of 1 ' Client Sample ID: MW-21 (55 Lab Sample ID: M76363-1 ) Date Sampled: 08/18/08 ' Matrix: AQ- Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20859.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND` 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I ' 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND- 2.0 ug/1 m,p-Xylene ND 2.0 ug/I ' 95-47-6 o-Xylene ND' 2.0 ug/1 C5-C8 Aliphatics (Unadj.) ND: 50 ug/I C9-C12 Aliphatics (Unadj.) ND 50 ug/1 C9-CIO Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9-C12 Aliphatics ND 50 ug/I ' CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 7.0% 70-130% ' 615-59-8 2,5-Dibromotoluene 86% 70-130% I i I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ' ®ln 7 of 55 ®ACC TF_3T Accutest Laboratories ' Report of Analysis Page I of I Client Sample ID: MW-24 (42) Lab Sample ID: M76363-2 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 ' Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 BD20860.D 1 08/27/08 AF n/a n/a GBD990 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 , MA-VPH List CAS No. Compound Result RL Units Q ' 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l ' 91-20-3 Naphthalene ND 3.0 ug/I 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 u /I J g C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/1 , C5- C8 Aliphatics NO 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits ' 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 87%0 70-130% ' ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 8 of 55' 12AC UTEST. M76363 Accutest Laboratories Report of Analysis Page 1 of 1 ' Client Sample ID: MW-2 p 6 (72) Lab Sample ID: M76363-3 Date Sampled: 08/18/08 ' Ma.rix: AQ -Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Rur,#1 BD20861.D 1 08/27/08 AF n/a n/a GBD990 Rur.#2 ' Purge Volume Run#1 5.0 ml Run#2 MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene NO 2.0 ug/1 100-41-4 Ethylbenzene NLl 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether NA. 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND, 2.0 ug/l m,p-Xylene ND> 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND. 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I ' C9-C10 Aromatics (Unadj.) ND 50 ug/I C5-C8 Aliphatics NT3 50 ug/1 C9-C12 Aliphatics NI) 50 ug/1 ' CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene 72% 70-130% 615-59-8 2,5-Dibromotoluene 80°!a 70-130% ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 55 12/ACC.L r1'ESi; Accutest Laboratories Report of Analysis Page 1 of 1 ' Client Sample ID: MW-19 (55) Lab Sample ID: M76363-4 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 BD20862.D l 08/27/08 AF n/a n/a GBD990 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q , 71-43-2 Benzene ND,. 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/l ' 1634-04-4 Methyl Tert Butyl Ether 8.1 2.0 ug/I 91-20-3 Naphthalene NI) 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/1 ' 95-47-6 o-Xylene ND 2.0 ug/I C5-C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) NO 50 ug/I ' C9-C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene $0% 70-130% ' 615-59-8 2,5-Dibromotoluene 87% 70-130% ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 10 of 55' 12ACCLffEST. M76363 Accutest Laboratories ' Report of Analysis Page 1 of 1 Ln Client Sample ID: MW-20 (55) Lab Sample ID: M76363-.5 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Prcject: SCMAW:97346878(REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20863.D 1 08/27/08 AF n/a n/a GBD990 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/l ' 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/l ' m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene N'D 2.0 ug/t C5-C8 Aliphatics (Unadj.) ND 50 ug/I C9-C12 Aliphatics (Unadj.) ND 50 ug/1 ' C9-C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND 50 ug/l C9-C12 Aliphatics ND 50 ug/I ' CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 78% 70-130% 615-59-8 2,5-Dibromotoluene 86% 70-130% ND = Not detected ' J = Indicates an estimated value II RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ' ®p 11 of 55 13AICCIlTEST M76363 �' °'-'^' Accutest Laboratories Report of Analysis Page I of I ' Client Sample ID: MW-29 (68) Lab Sample ID: M76363-6 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878�(REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch , Run#1 BD20864.D 1 08/27/08 AF n/a n/a. GBD990 Run#2 Purge Volume Run#1 5.0 ml Run#2 ' MA-VPH List CAS No. Compound Result RL Units Q ' 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether 90.5 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/1 ' C5- C8 Aliphatics (Unadj.) 69.0 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I ' C9-C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 80% 70-130% 615-59-8 2,5-Dibromotoluene 89% 70-130% ' ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®B 12 of 5 M76363 !a b ........ .. Accutest Laboratories ' Report of Analysis Page I of I Client Sample ID: MW-32 (55) ' Lab Sample ID: M76363-7 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20865.D 1 08/27/08 AF n/a n/a GBD990 Run#2 ' Purge Volume Run#1 5.0 ml ' Run#2 MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene V, 2.0 ug/1 100 41 4 Ethylbenzene ND 2.0 u9/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND, 3.0 ug/1 108-88-3 Toluene N-D': 2.0 ug/1 ' m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene ND. 2.0 ug/1 C5- C8 Aliphatics (Unadj.) NI) 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I ' C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics NO 50 u0/1 C9- C12 Aliphatics NO 50 ug/1 ' CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81°'0 70-130% ' 615-59-8 2,5-Dibromotoluene 88%.. 70-130% 1 ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound EJ 13 of 55 M .. ACCIREST Accutest Laboratories Report of Analysis Page 1 of 1 a ' Client Sample ID: MW-35 (53) Lab Sample ID: M76363-9 Date Sampled: 08/18/08 ' Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ! ' Run#1 BD20866.D 1 08/27/08 AF n/a n/a. GBD990 Run#2. Purge Volume Run#1 5.0 ml Run#2 ' MA-VPH List CAS No. Compound Result RL Units Q ' 71-43-2 Benzene NID 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/I 1634-04-4 Methyl Tert Butyl Ether 13.3 2.0 ug/1 91-20-3 Naphthalene NO 3.0 ug/1 108-88-3 Toluene 'N'D 2.0 ug/1 m,p-Xylene Nll 2.0 ug/1 ' 95-47-6 o-Xylene NO 2.0 ug/I C5- C8 Aliphatics (Unadj.) NI) 50 ug/I C9- C12 Aliphatics (Unadj.) NI) 50 ug/1 ' C9- C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics NI) 50 ug/1 C9- C12 Aliphatics N1) 50 ug/l CAS No. Surrogate Recoveries Run# 1 Run#2 Limits ' 615-59-8 2,5-Dibromotoluene :82% 70-130% 615-59-8 2,5-Dibromotoluene 80% 70-130% ' I ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®B 14 of J M76363 .. . ..... ... Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-37 (53) Lab Sample ID: M76363-9 Date Sampled: 08/18/08 Matrix: AQ- Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20867.D 1 08/27/08 AF n/a n/a GBD990 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 MA-VPH List ' CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/I ' 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/l 91-20-3 Naphthalene ND 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/l ' m,p-Xylene MD 2.0 ug/1 95-47-6 o-Xylene ND 2.0 ug/I C5- C8 Aliphatics (Unadj.) NI) 50 ug/1 C9-C12 Aliphatics (Unadj.) NI) 50 ug/1 ' C9- C10 Aromatics (Unadj.) N:I? 50 ug/1 C5-C8 Aliphatics "ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I ' CAS No. Surrogate Recoveries Run# l Run# 2 Limits 615-59-8 2,5-Dibromotoluene 81% 70-130% ' 615-59-8 2,5-Dibromotoluene 8.8% 70-130% S N ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ' ®n 15 of 55 ®ACCUTEST M76363 ' f Accutest Laboratories J Report of Analysis Page 1 of 1 0 Client Sample ID: MW-37 (90) Lab Sample ID: M76363-10 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20868.D 1 08/27/08 AF n/a n/a GBD990 Run#2 ' Purge Volume Run #1 5.0 ml Run#2 ' MA-VPH List CAS No. Compound Result RL Units Q ' 71-43-2 Benzene RD 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether NO 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l m,p-Xylene ND 2.0 ug/l ' 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) NO 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 t C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 87% 70-130% 615-59-8 2,5-Dibromotoluene 94% 70-130% ' ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®� 16 of 5 M76363 ' Accutest Laboratories Report of Analysis Page 1 of I Client Sample ID: MW-37 (105) ' Lab Sample ID: M7636341 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' Fite ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20869.D 1 08/27/08 AF n/a n/a GBD990 Run #2 ' Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene N=D 2.0 ug/l ' 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene N,D 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/l ' m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene NI 2.0 ug/1 C5- C8 Aliphatics (Unadj.) NOD 50 ug/1 C9-C12 Aliphatics (Unadj.) ND 50 ug/l C9- C10 Aromatics (Unadj.) NI) 50 ug/1 C5-C8 Aliphatics b 50 ug/1 C9-C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Run# 1 Run#2 Limits 615-59-8 2,5-Dibromotoluene :83% 70-130% ' 615-59-8 2,5-Dibromotoluene 92%q 70-130% ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ' 17 of 55 M76363 inboret cri.s Accutest Laboratories Report of Analysis Page 1 of 1 ' Client Sample ID: MW-39 (88) Lab Sample ID: M76363-12 Date Sampled: 08/18/08 Matrix: AQ -Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 BD20870.D 1 08/27/08 AF n/a n/a GBD990 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 ' MA-VPH List CAS No. Compound Result RL Units Q ' 71-43-2 Benzene ND! 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND. .. 2.0 ug/l m,p Xylene No 2.0 ug/I , 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) ND 50 ug/I C5- C8 Aliphatics ND 50 ug/I C9- C12 Aliphatics Nj) 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run#2 Limits t 615-59-8 2,5-Dibromotoluene 82% 70-130% ' 615-59-8 2,5-Dibromotoluene 91%a 70-130% ND = Not detected j = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 18 of 5 W6363 - . ..._ ... ' Acc:utest Laboratories Report of Analysis Page 1 of 1 4, Client Sample ID: MW-40 (85) Lab Sample ID-: M76363-13 Date Sampled: 08/18/08 ' Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20871.D 1 08/27/08 AF n/a n/a GBD990 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 ' MA.-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene `ND 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/1 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene NI), 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 ' 95-47-6 o-Xylene ND 2.0 ug/1 C5-C8 Aliphati:s (Unadj ) ND 50 ug/1 C9-C12 Aliphatics (Unadj.) ND, 50 ug/1 C9 C10 Aromatics (Unadj.) ND 50 ug/1 C5- C8 Aliphatics ND.. 50 ug/1 C9-C12 Aliphatics NU 50 ug/1 ' CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene $ °�o. 70-130% ' 615-59-8 2,5 Dibromotoluene 9300 > 70-130% ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ' ®B 19 of 55 MAC.CUTEST Accutest Laboratories , w Report of Analysis Page 1 of 1 Client Sample 1D: MW-38 (104) Lab Sample ID: M76363-14 Date Sampled: 08/18/08 Matrix: AQ -Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878(REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 BD2088O.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume , Run#1 5.0 ml Run#2 MA-VPH List ' CAS No. Compound Result RL Units Q ' 71-43-2 Benzene ND 2.0 ug/t 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether ND 2.0 u10/1 , 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND- 2.0 ug/1 m,p-Xylene N-D 2.0 ug/1 ' 95-47-6 o-Xylene ND` 2.0 ug/1 C5-C8 Aliphatics (Unadj.) ND: 50 ug/1 C9-C12 Aliphatics (Unadj.) NO 50 ug/1 C9- C10 Aromatics (Unadj.) NI). 50 ug/1 ' C5-C8 Aliphatics ND' 50 ug/l C9- C12 Aliphatics ND 50 ug/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits , 615-59-8 2,5-Dibromotoluene 81'% 70-130% 615-59-8 2,5-Dibromotoluene J0°10 70-130% ' ND = Not detected j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®® 20 0f 5 IV6363 r Accutest Laboratories ' Client Sam Report of Analysis Page 1 of 1 �,le I -p D. MW 38 (89) Lab Sample ID: M76363-15 Date Sampled: 08/18/08 ' Matrix: AQ - Grcund Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20881.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume Run#1 5.0 ml - Run#2 ' MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene N) 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether ND. 2.0 ug/I 91-20-3 Naphthalene N`D 3.0 ug/1 108-88-3 Toluene ND. 2.0 ug/l ' m,p-Xylene ND 2.0 ug/t 95-47-6 o-Xylene ND 2.0 ug/l C5-C8 Aliphatics (Unadj.) ND 50 ug/I C9-C12 Aliphatics (Unadj.) NO 50 ug/I ' C9- C10 Aromatics (Unadj.) NO 50 ug/1 C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/l ' CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotol-lene 81`Yo 70-130% ' 615-59-8 2,5-Dibromotolliene 90% 70-130% I ND = Not detected J = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®B 21 of 55 QA=CMEEM M76363 Accutest Laboratories ' w Report of Analysis Page 1 of 1 Client Sample 1D: RW-101 Lab Sample ID: M76363-16 Date Sampled: 08/18/08 Matrix: AQ- Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run #1 BD20882.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume ' Run#1 5.0 ml Run#2 ' MA-VPH List CAS No. Compound Result RL Units Q ' 71-43-2 Benzene N.D; 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 22.0` 2.0 ug/1 ' 91-20-3 Naphthalene NO 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/I 95-47-6 o-Xylene N1) 2.0 ug/1 , C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9-C12 Aliphatics (Unadj.) 1810: 50 ug/l • C9- C10 Aromatics (Unadj.) 506 50 ug/1 ' C5- C8 Aliphatics ND 50 ug/1 'C9- C12 Aliphatics 131:0 50 ug/I CAS No. Surrogate Recoveries Run# I Run# 2 Limits , 615-59-8 2,5-Dibromotoluene 87% 70-130% 615-59-8 2,5-Dibromotoluene 96% 70-130% ' ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank ' E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound E1 22 of 5 MAC....__..------._._.._. M76363 i ' Accutest Laboratories w Report of Analysis Page 1 of 1 ' Client Sample ID: RW-102 Lab Sample ID: M76363-17 Date Sampled: 08/18/08 ' Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA ' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run#1 BD20883.D 1 08/27/08 AF n/a n/a GBD991 Run#2 ' Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/1 100-41-4 Ethylbenzene ND 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether NO 2.0 ug/1 91-20-3 Naphthalene ND 3.0 u9/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/1 95-47-6 o-Xylene NI) 2.0 ug/I C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) 67.4 50 ug/l ' C9- C10 Aromatics (Unadj.) NJ) 50 ug/I C5- C8 Aliphatics NO 50 ug/1 C9- C12 Aliphatics ND 50 ug/I ' CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 615-59-8 2,5-Dibromotoluene 92% 70-130% 615-59-8 2,5-Dibromotoluene 9:1% 70-130% i ND = Not detected j = Indicates an estimated value ' RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ' r 23 of 55 12ACCUTEBT. M76363 : a b�... ....-.s Accutest Laboratories ' J Report of Analysis Page 1 of 1 m Client Sample ID: MW-25 (72) Lab Sample ID: M76363-18 Date Sampled: 08/18/08 Matrix: AQ - Ground Water Date Received: 08/20/08 Method: MADEP VPH REV 1.1 Percent Solids: n/a Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' Run#1 BD20884.D 1 08/27/08 AF n/a n/a GBD991 Run#2 Purge Volume Run#1 5.0 ml Run#2 MA-VPH List CAS No. Compound Result RL Units Q ' 71-43-2 Benzene D 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 1634-04-4 Methyl Tert Butyl Ether 14.3 2.0 ug/1 ' 91-20-3 Naphthalene ND: 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/I m,p-Xylene ND 2.0 ug/1 , 95-47-6 o-Xylene ND 2.0 ug/1 C5- C8 Aliphatics (Unadj.) ND 50 ug/I C9- C12 Aliphatics (Unadj.) ND 50 ug/1 C9- C10 Aromatics (Unadj.) -NO 50 ug/1 ' C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics N-D 50 ug/1 CAS No. Surrogate Recoveries Run# I Run# 2 Limits , 615-59-8 2,5-Dibromotoluene $1% 70-130% 615-59-8 2,5-Dibromotoluene J2%o 70-130% ' 1 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank t E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ®rl 24 of 55' 12ACCUTEST M76363 a ®� New England �t0rato __ Section 4 Msc. Forms Custody Documents and Other Forms ' Includes the following where applicable: ' • Chain of Custody • MCP Form • VPH Form • Sample Tracking Chronicle ®B 25 of 55 MAMEB T M76363 a '' 's LAB(LOCATION) Q Shell Oil Products Chain Of Custody Record , Please Check:Ap ro Nate Boil :P nl1101 oCextarl NatTlCt:,` _ INC T.S'IENV:6ERVICE51.:❑IaEa le la APPLIES ❑EIrv.3FAVi�i ❑IAINA RtTAA ❑4:EU FETI�4. . O.aaREST Dave Weeks 9 6 9 2 5 012 8 DATE: ❑IonYA SDea. OmvslarArR ❑war ❑OTHER 1 ❑LIfl1.IvftMF ❑01N91 PAGE: ( a P art.00na.a P..w ew.+«w: v Sovereign Consulting Inc 1140 I annou h RoadHyannis,MA 905E South Main Street,Unit 202 CONSULTANT PROJECT CONTACT(Report to):Jasan Sherbwne CONSULTANT PROJECT NO.:EOT11 an: Mansfield.MA 02048 568.339.3200 508.339:3248 I e TURNAnouIwT.E1ctLL>,oAROArsn jsherbume(a)sovconcom. l ti�+'i Mj Q �r,v �V MSTAMDARD(T.DAY) ❑SMrs ❑tDAYS ❑I DAYS 024Rdp5 REQUESTED ANALYSIS , oEUJERAeLEs: ❑owm ❑omwe ❑wp ❑R@ ❑OREq(SPEQFY) ?FAPERAlV11[ON REGlPTC HC m iCmler rJ ' SPECIAL INSTRUCTIONS OR NOTES: SAMPLING .NaTINA— ' swd. Field Sample Id..0floatlon Iu,Tnx Ia.a DATE TIRE �°�^ = C..-I-.MRUEi-, LaW."Notes a> /h U- 1030 G .. u . a I�ri i aE 7� > vlr ' u -a, Am S� U 1 G 4tlt U" r ( s GJ -3 ' AV, �y S t1Do S F3 F l (Ox 0 o y i a) `sa / Z.c J N.Iapa. awwMb(Syn.V.I V �' mil. /�Q � , a.. M76363: Chain of Custody ' Page 1 of 2 ' I ®B 26 of 5 M76363 ^: LAB(LOCATION) Shell Oil Products Chain Of Custody Record f.(ENy1KRV(CES)::[]�F.DnTMRIAPPM ❑ ro—_,WTAk . ... OACOfrM Dave Weeks 91 61 91 21 51 0 2 8 DATE: j000au— ❑Fb�0 7 7:77.7.0.4.. ....... PAGE a a9- 11. 01.01 01 .1 Sovereign Consulting Inc 1140 Iyannough Road,Hyannis,MA qnrR South Ua1.Street.Unit 202 CONSULTANT PROJECT CONTACT(ROW to):Jawn Sherburne CONSULTANT PROJECT NO.:EO711 Mansfi.ld,MA 02048 ..................... . —'�8.339.3200 509.339.3248 ishef burne(ahovcon.com C V—w—) 05MYS 03mys cj2ws 0 N,"MVS REQUESTED ANALYSIS oft-, LEs: owmw Dowe ONU 0 Rcp 0 OTM mcffy) TEY{e/:TGeEMREMVTC- c.W.11 7 SPECIAL INSTF UCTIONS OR NOTES: S—umG ' 'r.,y Field Sample Identification x tnulnemoReadinp Lb—ty Notes 4. a.4 f[A lub- I)= I Rw - )0( 014-, 1 �.v...ral �.• w,mwmn�.n L�(� O z A-) 5-0 U9L WL M76363: Chain of Custody Page 2 of 2 27 of 55 13ACCaaTEST M76363 Massachusetts Department BWSC-CAM Exhibit VII A-1 LI of Environmental Protection 21 May 2004 Revision No. 3.2 ' Bureau of Waste Site Cleanup Final Page 10 of 32 P, N Title: MADEP MCP Response Action Analytical Report Certification Form Ste. ,Laboratory Name: Accutest Laboratories of New England Project#: M76363 Project Location: SCMAW:97346878(REIMBMA) 1140 lyannough Road ' MADEP RTN None Hyannis MA This form provides certifications for the following data set: M76363-1,M76363-1 0,M76363-1 1,M76363-12,M76363-13,M76363-14,M76363-15,M76363-16 M76363-17,M76363-18,M76363-2,M76363-3,M76363-4,M76363-5,M76363-6,M76363-7 M76363-8,M76363-9 Sample Matrices: Groundwater X Soil/Sediment O Drinking Water O Other: 8260B 8151A 8330 6010B 7470A/1A 8270C ) 8081A ) VPH X 6020 9014M 2 K, '. 8082 8021 B EPH 7000 S s *7196A An affirmative response to questions A, B, C,and D is required for"Presumptive Certainty status A I Were all samples received � ,b th p y e laboratory m a condition consistent with Yes ❑ No that described on the Chain-of-Custody documentation for the data set? ' Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed,including the requirement to note and I] Yes ❑ No ' discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? ' Does the data included in this report meet all the analytical requirements C for"Presumptive Certainty",as described in Section 2.0(a),(b),(c)and 0 Yes ❑No ' (d)of the MADEP document CAM VII A,"Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? ' D VPH and EPH methods only:Was the VPH or EPH method run without 0 Yes ❑No significant modifications,as specified in Section 11.3? A response to questions E and Fbe/ow is required for"Presumptive Certainty"status 1 E Were all QC performance standards and recommendations for the Yes El No ' specified methods achieved? Refer to Narrative ' F Were results for all analyte-list compounds/elements for the specified El Yes No ' method(s)reported? Refer to Narrative , All Negative responses must be addressed in an attached Environmental Laboratory case narrative. 1 the undersigned, attest under the pains and penalties of perjury that,based upon my personal '- inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my/knowledge and belief,accurate and complete. T~� �- Signature: Position: Laboratory Director Printed Name: Reza Tand Date: 09/01/2008 ®� 28 of 5 ' M76363 ' MADEP VPH FORM N1a "°Y Aqueous Wl Soil Sediment 1^ Other Co DR-OP s i Satisfactor vi Broken Leaking ouFeserauat :; N/A D _ H <=2 H >2 titratu>e . � � Received on Ice I I Received at 4 Deg. C Other i✓' Rec'd at 2.0 Deg.C KNO HE N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-21 (55) Lab ID: M76363-1 ' Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: ®' First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges. CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj) N/A ug/I ND" 50 ' C9-C12 Aliphatics(Unadj.) N/A ug/I NDA 50 Target Analytes ' Ethylbenzene 10041-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 ' o-Xylene 9547-6 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/I ND 2 ' Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND' 50 ' C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 79 70-130% ' PID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? : `Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 'Yes No-Details Attatched ' Were any significant modifications made to the VPH method,as specified in Sect.11.3? VNo Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete ' Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 ®rl 29 of 55 ' 12ACCUTF . M76363 .._,k _`_ _s MADEP VPH FORM W!, ueous 1�; Soil -- Sediment _ Other .__sfactor ✓ Broken ;-i LeakinA F-; H —2 ice. H >2 Received at 4 De . C Other Rec'dat2.0De Ceived on Ice g. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-24(42) Lab ID: M76363-2 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A , FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q ' C5-C8 Aliphatics(Unadj.) N/A ugh ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/1 ND" 50 , C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 ' Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 ' Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 ' o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges ' C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 , Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 87 70-130% ' .Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were - e eall QA/QC procedures REQUIRED by the VPH Method followed? IJYes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? WlYeS .....: No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? r�No ! Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director , Date 9/1/2008 30 of 5� Printed Name Reza Tand Eg� ACCUT M76363 ' MADEP VPH FORM wmmvamiia—�Ov' ueous '�, Soil Sediment I Other isfactor '✓ Broken Leakin/A H <=2 `� H >2 Received on Ice -I Received at 4 Deg. C Other i�l Rec'd at 2.0 Deg.C Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-26(72) Lab ID: M76363-3 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A ' Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes ' Ethylbenzene 10041-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04A C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 ' o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 ' Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 72 70-130% ' PID:2,5-Dibromotoluene % 80 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value ' Were all QA/QC; rocedures REQUIRED —i 1 P by tte VPH Method followed? I�iYes �, No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? IJYes (... No-Details Attatched ' Were any significant modifications made to'fie VPH method,as specified in Sect. 11.3? No L': Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 ® 31 of 58 1 OAS M76363 a"' MADEP VPH FORM ' Itti iXt n� A ueous �� Soil � Sediment '�':. Other rr t5 Satisfactor W Broken I._.i Leakin i eFr�zeuutlu N/A H <=2 2 PH >2 ' z era u e a. Received on Ice 1 Received at 4 Deg. C F-s Other 1✓j Rec'd at 2.0 Deg.C flltshto� N/A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-19(55) Lab ID: M76363-4 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q ' C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 ' C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 ' Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 8.1 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND" 50 C9-C12 Aliphatics N/A ugll ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 87 70-130% ' Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 'Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 4Yes No-Details Attatched ' Were any significant modifications made to the VPH method,as specified in Sect.11.3? Y No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 ®® 32 of 551 12ACCUTEST M76363 ' P r MADEP VPH FORM Aqueous ` , Soil Sediment Other � ;- -- f � Satisfactor W Broken Leaking �; � sera true N/A PH <=2 WF PH >2 �rafulr Received on Ice Received at 4 Deg. C 1 7, Other �l Rec'd at 2.0 Deg.C N/A Pl Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-20(55) Lab ID: M76363-5 W ' Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: ®' PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A ' Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 ' C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes ' Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 ' Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/I ND 2 ' Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 ' Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND B 50 ' C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 78 70-130% ' PID:2,5-Dibromotoluene % 86 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the ' concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AT qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? itYes No-Details Attatched ' Were all performance/acceptance standards for required QA/QC procedures achieved? : 'Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? W�No Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete ' Signature Postition Laboratory Director Printed Name Reza Tan Date 9/1/2008 ®® 33 of 55 OACCMEST. atrtz, �� e r: MADEP VP H FORM- Aqueous W1, Soil Sediment Other .., s i- Satisfactory✓, Broken Leaking f t o t -watiu i N/A EL PH <=2 W PH >2 Received R e on Ice ec�d at 2.0 Deg.C an &--- N/A Received at 4 Deg . C Other ice' s Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-29(68) Lab ID: M76363-6 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units g Result RDL Q ' C5-C8 Aliphatics(Unadj.) N/A ug/I 69," 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 t C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 Tar An alytes nalvtes ' Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 90.5 2 ' Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 u /I ND 9 2 m,p-Xylene C9-C12 ug/l ND 2 Adjusted Ranges ' C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 ' Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 80 70-130% PID:2,5-Dibromotoluene % 89 70-130% ' Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the ' concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? L'Yes '_.1 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? LiYes r No-Details Attatched �: Were any significant modifications made to the VPH method,as specified in Sect.11.3? No Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 ®E1 34 of 5 M76363 ' MADEP VPH FORM Ma y A ueous ✓ Soil Sediment Other Co itte�� Satisfactor w1 Broken Leaking ' out Pceseru t ar s= N/A _, PH <=2 W! PH ,2 -, Received on Ice 7' Received at 4 Deg. C Other ✓i Rec'd at 2.0 Deg.C Nhanol :ter N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-32(55) Lab ID: M76363-7 w ' Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A ' Unadjusted Ranges CAS# Elution Range Units Result C5-C8 Aliphatics(Unadj.) N/A ug/I ND" RDL Q 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 ' C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes ' Ethylbenzere 100-41-4 C9-C12 ug/1 ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 ' Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 71-43-2 C5-C8 ug/1 ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 ' o-Xylene 95-47-6 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/I ND 2 ' Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 ' C9-C12 Aliphatics N/A ugll ND' 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target.Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z AV qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? WYes j No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? W!Yes i_, No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? WNo Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Postition Labo ratory Director Signature � Printed Name Reza Tand Date 9/1/2008 ®® 35 of 55 ' 12ACCLITEST. M76363 MADEP VPH FORM ' ttaffi � A ueous ivi Soil Sediment F7 Other Satisfactor Broken Leaking teou�Pe�serv�tla�e N/A PH <=2 y PH >2 ' " fli er =u Received on Ice f Received at 4 De . C Other Rec'd at 2.0 Deg.C Method for Ranges: MADE VPH REV 1.1 Client ID: MW-35(53) Lab ID: M76363-8 ca ' Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: WA 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q ' C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 ' C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 ' Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 13.3 2 ' Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 ' o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges , C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 ' Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 82 70-130% PID:2,5-Dibromotoluene % 89 70-130% , Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogates)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range ANDtoncentration of C9-_10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 'Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? 4.Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? :!t.No Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Postition Laboratory ' Signature � Director Printed Name Reza Tan Date 9/1/2008 ®® 36 of 55 ' ®ACCUTEST. M76363 €. .. .. ....... .. ' MADEP VPH FORM M4010'� � �",, N A ueous :i Soil 7. Sediment i Other ti e s A Satisfactor Fvi Broken 7 Leaking ' ous resery t=ues:; N/A F-1 PH <=2 W. pH ,2 Received on Ice i Received at 4 Deg.C Other ICI Rec'd at 2.0 Deg.C ' Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(53) Lab ID: M76363-9 W Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/1812008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 NIA Unadiusted Ranges. CAS# Elution Range Units Result RDL Q ' C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ugh ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 ' Methyl Teri.Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 Benzene 7143-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 ' o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND c 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 70-130% PID:2,5-Dibromotoluene % 88 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of'.any surrogate(s)and/or internal standards eluting in that range - B Hydrocarbon Range data exclude concentrations of.any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of.any surrogate($)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? ✓.Yes No-Details Attatched ' Were all performance/acceptance standards for required QA/QC procedures achieved? 'Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? 'No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete III ' Signature Postition Laboratory Director 9/1/2008te Printed Name Reza Tan Da ®® -37 of 55 OAC CUTEST W6363 MADEP VPH FORM ' Aqueous ✓ Soil ;- Sediment 1 Other f, Satisfactor k Broken Leaking e�i p else pie :. N/A H <=2 Fvl� PH >2 ^� ' Received on Ice Received at 4 Deg. C Other Fj, Rec'd at 2.0 Deg.C t .. N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(90) Lab ID: M76363-10 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 8/27/2008 N/A ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q: , C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 ' C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 , Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 , Benzene 71-43-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 ' o-Xylene 9547-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges ' C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 ' Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 87 70-130% PID:2,5-Dibromotoluene % 94 70-130% ' Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range e Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? iviYes L.-1 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? �Yes '._._�L No-Details Attatched ' Were any significant modifications made to the VPH method,as specified in Sect. 11.3? Ev],No �._•: Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature _ Postition Laboratory Director ' 9/1/2008te Printed Name Reza Tand Da ®el 38 of 55 ' OACCUTEST. M76363 MADEP VPH FORM ueous �I Soil 1 Sediment Other o tatr 8, Satisfactorvivi Broken Leaking t��u��Pr�eser�v�`tives N/A IF, H <=2 Wi H>2 Received on Ice Received at 4 Deg. C F7 Other Fdi Rec'd at 2.0 Deg.C N/A P. Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-37(105) Lab ID: M76363-11 w ' Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run, PID: 2,5-Dibromotoluene N/A 8/27/2008 NIA ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A ' Unadjusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/1 ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 ' C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-044 C5-C8 ug/I ND 2 Benzene 71A3-2 C5-C8 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 o-Xylene 95-47-6 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges C5-C8 Aliphatics N/A ugll ND a 50 ' C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 83 70-130% PID:2,5-Dibromotoluene % 92 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range.C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 6Yes L-1 No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ;kYes I__' No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? IV i_ Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete ' Signature _ Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 Mo 39 of 55 ' JOACCUTEST. M76363 MADEP VPH FORM Aqueous kv Soil Sediment Other Satisfactory i!i Broken - Leaking �' 1afreseifv� > N/A p H <=2 PH >2 Received on Ice Received at 4 Deg. C ' Other F j,! Rec'd at 2.0 Deg.C Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-39(88) Lab ID: M76363-12 Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 ' VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: ' N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result. RDL Q , C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND A 50 C5-C8 Aliphatics(Unadj.) N/A ug/t ND" 50 Target Analytes Toluene 108-88-3 C5-C8 ug/I ND 2 ' m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 9547-6 C9-C12 ug/t ND 2 ' Naphthalene 91-20-3 N/A ug/I ND 3 Benzene 7143-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 ' Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 Adjusted Ranges , C9-C12 Aliphatics N/A ug/I ND c 50 C5-C8 Aliphatics N/A ug/I ND' 50 ' Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 91 70-130% FID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude cone of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ' iYes No-Details Attatched , Were any significant modifications made to the VPH method,as specified in Sect.11.3? VNo Yes-Details Attatched attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director ' Printed Name Reza Tan Date 9/1/2008 MB 40 of 55' M76363 - ' MADEP VPH FORM Aqueous :f' Soil (- Sediment Other ` rs - satisfactory Broken F Leakin tsP=eSftl #tvs N/A - H <=2 H>2 s Received on Ice Received at 4 Deg. C Other 14 Rec'd at 2.0 Deg.C ttt �iae� N/A p Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-40(85) Lab ID: M76363-13 ' Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) NIA ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 ' C5-C8 Aliphatics(Unadj.) N/A ugly ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ugh ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ugh ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 95-47-6 C9-C12 ugh ND 2 ' Naphthalene 91-20-3 N/A ugh ND 3 Benzene 71-43-2 C5-C8 ugh ND 2 Adiusted Ranges C9-C12 Aliphatics N/A ugh ND` 50 ' C5-C8 Aliphatics N/A ugh ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 93 70-130% ' FID:2,5-Dibromotoluene % 83 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration o`Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? V'No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director Printed Name Reza Tan Date 9/1/2008 ®B 41 of 55 ' 13ACCUTEWE M76363 =:. MADEP VPH FORM ' ft �t � A ueous 1W Soil Sediment FJ Other Satisfactorviiii Broken Leaking ��iix�Pre�setta#tue N/A PH <=2 PH >2 ' er ur Received on Ice ,r1 Received at 4 Deg. C 1 i Other ;4j Rec'd at 2.0 Deg.C ' Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-38(104) Lab ID: M76363-14 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008- N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: ' N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q ' C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 ' C5-C8 Aliphatics(Unadj.) N/A ugll ND" 50 Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I ND 2 ' Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 ' o-Xylene 95-47-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 ' Benzene 7143-2 C5-C8 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adjusted Ranges C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND a 50 ' Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 90 70-130% FID:2,5-Dibromotoluene % 81 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A'J qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Ji6Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? ! ;Yes ' No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect.11.3? WNo Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Postition Laboratory ' Signature v Director Printed Name Reza Tand Date 9/1/2008 ME1 42 of 550 MAGC JT'EST M76363 MADEP VPH FORM Mar m' A ueous vi Soil Sediment Other F_i Satisfactori Broken Leakin C ou P ese a yes N/A 15 PH <-2 ✓ H >2 �: m.3,�ratt��e'� � �` Received on Ice r Received at 4 De . C � i Other i�l Rec'd at2.o Deg.C lleo N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-38(89) Lab ID: M76363-15 W ' Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5-Dibromotoluene N/A 8/27/2008 NIA ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A ' Unadjusted Ranges CAS# Elution Range Units Result RDL Q C9-C12 Aliphatics(Unadj.) N/A ug/I ND' 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND' 50 ' C5-C8 Aliphatics(Unadj.) N/A ug/I ND' 50 Target Analvtes ' Naphthalene 91-20-3 N/A ug/I NO 3 Benzene 7143-2 C5-C8 ug/I NO 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I NO 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I NO 2 ' m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 9547-6 C9-C12 ug/I NO 2 Adjusted Ranges C9-C12 Aliphatics N/A ugh NO' 50 ' C5-C8 Aliphatics N/A ug/I ND a 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 90 70-130% ' FID:2,5-Dibromotoluene % 81 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)andfor internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. CS-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analvtes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analyles eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? IL'Yes ..... No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? I!06Yes -.. No-Details Attatched ' Were any significant modifications made to the VPH method,as specified.in Sect.11.3? L']N0 Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete ' Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 Sri 43 of 55 ' MACCUTEBT. M76363 `" = MADEP VPH FORM ' (1�artx � Aqueous ✓ Soil - Sediment - Other i- �; _ W, Satisfactor 4; Broken Leaking u�o� r�esQrya�t� es N/A pH <=2 PH ,2 -- F Received on Ice Received at 4 Deg. C Other (Ji Rec'd at 2.0 Deg.C N/A A Method for Ranges: MADEP VPH REV 1.1 Client ID: RW-101 Lab ID: M76363-16 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run ` PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: ' N/A 1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q_ t C9-C12 Aliphatics(Unadj.) N/A ug/1 1810A 50 C9-C10 Aromatics(Unadj.) N/A ug/I 506' 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 Target Analytes o-Xylene 95-47-6 C9-C12 ug/I ND 2 ' Naphthalene 91-20-3 N/A ug/1 ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 ' Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l 22 2 Toluene 108-88-3 C5-C8 ug/l ND 2 ' Ethylbenzene 10041-4 C9-C12 ug/1 ND 2 m,p-Xylene C9-C12 ug/I ND 2 Adiusted Ranges , C9-C12 Aliphatics N/A ug/I 1310` 50 C5-C8 Aliphatics N/A ug/I ND a 50 ' Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 96 70-130% FID:2,5-Dibromotoluene % 87 70-130% , Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9•C10 Aromatic Hydrocarbons. Z A'J'qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? :Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? !!Yes : . No-Details Attatched ' Were any significant modifications made to the VPH method,as specified in Sect.11.3? I No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director ' Date 9/1/2008 Printed Name Reza Tan Da ®ri 44 of 55, ®ACCUTEBT. M76363 -^ ' MADEP VPH FORM tltak� � Aqueous ov, Soil Sediment I Other =tahe s r Satisfactor � Broken Leaking u�eaf�PMs1 a es N/A H <=2 14I H >2 F_ Received on Ice Received at 4 Deg. C I._ Other Recd at 2.0 Deg.C Ittia ate - NIA A Method for Ranges: MADEP VPH REV 1A Client ID: RW-102 Lab ID: M76363-17 ca Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: PID: 2,5 Dibromotoluene N/A 8/27/2008 N/A ' FID: 2,5-Dibromotoluene %Solids: Low Dilution: High Dilution: N/A 1 N/A Unadiusted Ranges CAS# Elution Range Units Result RDL Q C5-C8 Aliphatics(Unadj.) N/A ug/l ND" 50 C9-C12 Aliphatics(Unadj.) N/A ug/I 67.4A 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 Target Analytes ' o-Xylene 95417-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/l ND 3 Benzene 71-43-2 C5-C8 ug/I ND 2 Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/l ND 2 m,p-Xylene C9-C12 ug/I ND 2 Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 ' Adjusted Ranges C5-C8 Aliphatics N/A ug/I ND a 50 C9-C12 Aliphatics N/A ug/I ND` 50 Surrogate Recoveries Acceptance Range PID:2,5-Dibromotoluene % 91 70-130% ' FID:2,5-Dibromotoluene % 82 70-130% Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range B Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Analytes eluting in that range. C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-C10 Aromatic Hydrocarbons. Z A V qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? Yes No-Details Attatched ' Were any significant modifications made to the VPH method,as specified in Sect. 11.3? ;No Yes-Details Attatched I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete ' Signature Postition Laboratory Director Printed Name Reza Tand Date 9/1/2008 ®® 45 of 55 ' ®AC,'CUTEST. M76363 MADEP VPH FORM tlatrc .3� F A ueous Soil — -- Sediment Other t ' g Satisfactor 4: Broken Leakin : eattvs<`: N/A i - H <=2 .i; H ,2 t?h1 a£yire Received on Ice Received at 4 Deg. C ' - Other ice; Reed at 2.0 Deg.C ' Methane ,F `. N/A _ A Method for Ranges: MADEP VPH REV 1.1 Client ID: MW-25(72) Lab ID: M76363-18 w Method for Target Analytes: MADEP VPH REV 1.1 Date Collected: 8/18/2008 Date Received: 8/20/2008 VPH Surrogate Standards Date Extracted: First Date Run: Last Date Run: , PID: 2,5-Dibromotoluene N/A 8/27/2008 N/A FID: 2,5-Dibromotoluene %Solids: t High Dilution: N/A Low Dilution:1 N/A Unadjusted Ranges CAS# Elution Range Units Result RDL Q ' C9-C12 Aliphatics(Unadj.) N/A ug/I ND" 50 C9-C10 Aromatics(Unadj.) N/A ug/I ND" 50 C5-C8 Aliphatics(Unadj.) N/A ug/I ND" 50 ' Target Analytes Methyl Tert Butyl Ether 1634-04-4 C5-C8 ug/I 14.3 2 , Toluene 108-88-3 C5-C8 ug/I ND 2 Ethylbenzene 100-41-4 C9-C12 ug/I ND 2 m,p-Xylene C9-C12 ug/I ND 2 o-Xylene 9547-6 C9-C12 ug/I ND 2 Naphthalene 91-20-3 N/A ug/I ND 3 ' Benzene 71-43-2 C5-C8 ug/I ND 2 Adjusted Ranges ' C9-C12 Aliphatics N/A ug/I ND` 50 C5-C8 Aliphatics N/A ug/I ND a 50 ' Surrogate Recoveries Acceptance Range FID:2,5-Dibromotoluene % 81 Lance PID:2,5-Dibromotoluene % 92 70-130% ' Footnotes A Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range 8 Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C5-C8 Aliphatic Hydrocarbons exclude the concentration of Target Ahalytes eluting in that range. ' C Hydrocarbon Range data exclude concentrations of any surrogate(s)and/or internal standards eluting in that range. C9-C12 aliphatic Hydrocarbons exclude conc of Target Analytes eluting in that range AND concentration of C9-CIO Aromatic Hydrocarbons. Z A W qualifier indicates an estimated value Were all QA/QC procedures REQUIRED by the VPH Method followed? 1141Yes No-Details Attatched Were all performance/acceptance standards for required QA/QC procedures achieved? kz_!Yes No-Details Attatched Were any significant modifications made to the VPH method,as specified in Sect. 11.3? WNo '..I Yes-Details Attatched ' I attest under the pains and penalties of perjury that,based upon my inquiry of those individuals immediately responsible for obtaining the information,the material contained in this report is,to the best of my knowledge and belief,accurate and complete Signature Postition Laboratory Director ' Printed Name Reza Tand Date 9/1/2008 ®E] 46 of 55 ' ACCUTEST M76363 ' Accutest Laboratories Internal Sample Tracking Chronicle ' Shell Oil Job No: M76363 i SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes M76363-1 MADEP VPH REV 1.127-AUG-08 01:19 AF VMAVPH M76363-2 MADEP VPH REV 1.127-AUG-08 02:00 AF VMAVPH ' M76363-3 MADEP VPH REV 1.127-AUG-08 02:42 AF VMAVPH M76363-4 MADEP VPH REV 1.127-AUG-08 03:23 AF VMAVPH� M76363-5 MADEP VPH REV 1.127-AUG-08 04:04 AF VMAVPH ?����.,���a� �✓ ... �',v o...�. ,. ' '°s,,r .ss.. . .. ,.r,. _�,s,',,.s:�"i: , ''?B�.�;���, .�.«bs„��z��'�T. _ .? ' M76363-6 MADEP VPH REV 1.127-AUG-08 04:45 AF VMAVPH ��- �_ - M76363-7 MADEP VPH REV 1.127-AUG-08 05:25 AF VMAVPH M76363-8 MADEP VPH REV 1.127-AUG-08 06:06 AF VMAVPH ' Page 1 of 3 ®� 47 of 55 1 UACGtJTEST. M76363 Accutest Laboratories ' Internal Sample Tracking Chronicle Ph Shell Oil SCMAW:97346878 (REIMBMA) 1140 lyannough Road Hyannis MA Job No: M76363 Project No: EQ 711 ' .Sample Number Method Analyzed By Prepped By Test Codes ' ^r M76363-9 MADEP VPH REV 1.127-AUG-08 06:47 AF VMAVPH e. c M76363 10 MADEP VPH REV 1.127-AUG-08 07:28 AF VMAVPH ' m 7', 1g1ollected8I1�G081 � $ t51J aRece�ve 20t?.11Sy' M76363-11 MADEP VPH REV 1.127-AUG-08 08:10 AF VMAVPH M76363-12 MADEP VPH REV 1.127-AUG-08 08:51 AF VMAVPH M76363-13 MADEP VPH REV 1.127-AUG-08 09:32 AF VMAVPH , M76363-14 MADEP VPH REV 1.127-AUG-08 15:44 AF VMAVPH M76363-15 MADEP VPH REV 1.127-AUG-08 16:26 AF VMAVPH ' M76363-16 MADEP VPH REV 1.127-AUG-08 17:07 AF VMAVPH ' Page 2 of 3 ' ®® 48 of 55 91ACS M76363 i.::'r n r r.r i••s Accutest Laboratories Internal Sample Tracking Chronicle A Shell Oil Job No: M76363 SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Project No: EQ 711 Sample Number Method Analyzed By Prepped By Test Codes R�jL-t3 M76363-17 MADEP VPH REV 1.127-AUG-08 17:49 AF VMAVPH - �-�.t..v xn�.. �,�.a _ .:�n.,,n.��'�-...r,..,.�.R ...,... F......,�xaa ,.�< .,_. .,-��`�;�s � w�'?°�'�`_,I�,"a3 � ,?:�.,..:� .,,�' �,�s....�.��-�irtr ..,.c� •. ,t, M76363-18 MADEP VPH REV 1.127-AUG-08 18:30 AF VMAVPH Page 3 of 3 ®B 49 of 55 ' 12ACCI.ITEST. M76363 a.^.- .... . .®E2 New England ACCUTEST. ,* . .. .. ... . _..... Section 5 L�"•5 Aft 2H Ymt;c ti.E:M S7#Y GC Volat-ales QC Data Summaries Includes the following PP where applicable: • Method Blank Summaries ' • Blank Spike Summaries • Matrix Spike and Duplicate Summaries • Surrogate Recovery Summaries t ®B 50 of 55' 12ACCI.TTEEM M76363 ="b f Method Blank Summary Page 1 of 1 Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID . DF Analyzed By Prep Date Prep Batch Analytical Batch ' GBD990-MB BD20849.1) 1 08/26/08 AF n/a n/a GBD990 j ' The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 ' M76363-1, M76363-2, M76363-3, M76363-4, M76363-5, M76363-6, M76363-7, M76363-8, M76363-9, M76363-10, M76363-11, M76363-12, M76363-13 ' CAS No. Compound Result RL Units Q 71-43-2 Benzene ND 2.0 ug/l 100-41-4 Ethylbenzene ND 2.0 ug/l 1634-04-4 Methyl Tert Butyl Ether NO 2.0 ug/l 91-20-3 Naphthalene NO 3.0 ug/l 108-88-3 Toluene ND 2.0 ug/l m,p Xylene ND 2.0 ug/l 95-47-6 o-Xylene ND 2.0 ug/l C5- C8 Aliphatics (Unadj.) ND 50 ug/l C9- C12 Aliphatics (Unadj.) ND 50 ug/l C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/l C9- C12 Aliphatics ND 50 ug/l CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 8z%: 70-130% 615-59-8 2,5-Dibromotoluene 88% 70-130% f 51 of 55 12AlCCUTEST M76363 ^' ^; Method Blank Summary Page I of I Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA 1 Sample File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch GBD991-MB BD20873.D 1 08/27/08 AF n/a n/a GBD991 ' The C reported h ,Q p ere applies to the foliowin samples: Method. M t � A)Er VrH REV 1.1 M76363-14, M76363-15, M76363-16, M76363-17, M76363-18 ' CAS No. Compound Result RL Units Q ' 71-43-2 Benzene ND 2.0 ug/I 100-41-4 Ethylbenzene ND 2.0 ug/1 ' 1634-04-4 Methyl Tert Butyl Ether ND 2.0 ug/I 91-20-3 Naphthalene ND 3.0 ug/1 108-88-3 Toluene ND 2.0 ug/1 m,p-Xylene ND 2.0 ug/l 95-47-6 o-Xylene NO 2.0 u 1 ' C5- C8 Aliphatics (Unadj.) ND 50 ug/1 C9- C12 Aliphatics (Unadj.) ND 50 ug/I C9- C10 Aromatics (Unadj.) ND 50 ug/l C5- C8 Aliphatics ND 50 ug/1 C9- C12 Aliphatics ND 50 ug/I CAS No. Surrogate Recoveries Limits 615-59-8 2,5-Dibromotoluene 82% 70-130% 615-59-8 2,5-Dibromotoluene 910/a 70-130% ®® 52 of 55 �ACCIJTE�T ' M76363 ' Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: M76363 ' Account: SHELLWIC Shell Oil Projezt: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch ' GBD990-BSP BD20850.1) 1 08/26/09 AF n/a n/a GBD990 GBD990-BSD BD20851.1) 1 08/26/08 AF n/a n/a GBD990 v, iv ' The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 M76363-1, M76363-2, M76363-3, M76363-4, M76363-5, M76363-6, M76363-7, M76363-8, M76363-9, M76363-10, M76363-11, M76363-12, M76363-13 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/I ug/I % ug/I % RPD Rec/RPD 71-43-2 Benzene 50 51.7 103 51.7 1`03 0 70-130/25 ' 100-41-4 Ethylbenzene 50 52.6 105 52.7 105. 0. 70-130/25 1634-04-4 Methyl Tert Butyl Ether 50 51.6 103: 51.7 103 0 70-130/25 91-20-3 Naphthalene 50 48.4 97 49.9 100 3 70130/25 108-88-3 Toluene 50 52.3 1`05 52.4 105 0 70-130/25 ' m,p-Xylene 100 105 105 105 105 0 70-130/25 95-47-6 o-Xylene 50 49.4 99 49.5 99 0 70-130/25 C5- C8 Aliphatics (Unadj.) 150 142 95 144 96 1 70-130/25 C9- C12 Aliphatics (Unadj.) 150 141 94 141 94 0 70-130/25 ' C9- C10 Aromatics (Unadj.) 50 50.1 100 50.3 101 0 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 615-59-8 2,5-Dibromotoluene 81% 83% 70-130% 615-59-8 2,5-Dibromotoluene 80% 91% 70-130% ®® 53 of 55 ' 12ACCUTEBT. M76363 "s Blank Spike/Blank Spike Duplicate Summary Page 1 of I Job Number: M76363 Account: SHELLWIC Shell Oil , Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GBD991-BSP BD20874.D 1 08/27/08 AF n/a n/a GBD991 ' GBD991-BSD BD20875.D 1 08/27/08 AF n/a n/a GBD991 w N The QC reported here applies to the following samples: Method: MADEP VPH REV 'r 1.1 M76363-14, M76363-15, M76363-16, M76363-17, M76363-18 ' Spike BSP BSP BSD BSD Limits ' CAS No. Compound ug/l ug/I % ug/I % RPD Rec/RPD 71-43-2 Benzene 50 53.6 1=07 52.2 1Q.4 3 70-130/25 100-41-4 Ethylbenzene 50 54.2 108: 52.7 105 3 70-130/25 , 1634-04-4 Methyl Tert Butyl Ether 50 54.1 108:: 51.2 102>;. 6 70-130/25 91-20-3 Naphthalene 50 53.1 1'06 50.9 102 ::. 4 70-130/25 108-88-3 Toluene 50 53.7 107 52.3 1055 3 70-130/25 m,p-Xylene 100 108 108 105 105` 3 70-130/25 ' 95-47-6 o-Xylene 50 50.9 1.02 49.3 99. 3 70 130/25 C5- C8 Aliphatics (Unadj.) 150 150 100. 141 94 6 70-130/25 C9- C12 Aliphatics (Unadj.) 150 143 9`5 138 92. 4 70-130/25 C9- C10 Aromatics (Unadj.) 50 52.2 104 50.0 100 4 70-130/25 ' CAS No. Surrogate Recoveries BSP BSD Limits ' 615-59-8 2,5-Dibromotoluene 84% 85% 70-130% 615-59-8 2,5-Dibromotoluene 93% 93% 70-130% I ®B 54 of 55 ACC.UTEST. ' Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: M76363 Account: SHELLWIC Shell Oil Project: SCMAW:97346878 (REIMBMA) 1140 Iyannough Road Hyannis MA Method: MADEP VPH REV 1.1 Matrix: AQ Samples and QC shown here apply to the above method v, w LaE Lab Sample ID File ID S1 a S1 b M76363-1 BD20859.D 79.0 : 86.0 M76363-2 BD20860.D 80 0>:._ 87.0 M76363-3 BD20861.D 72 0. 80.0 M76363-4 BD20862.D 80 0 ':., 87.0 M76363-5 BD20863.D 78 0:' 86.0 M76363-6 BD20864.D 89.0 ' M76363-7 BD20865.D 810 88.0 M76363-8 BD20866.D 82 0 >'. 89.0 81 M76363-9 BD20867.D 0 88.0 ' M76363-10 BD20868.D 8.7,D,. 94.0 M76363-11 BD20869.D 83{)': 92.0 M76363-12 BD20870.D 824 91.0 M76363-13 BD20871.D 914 93.0 ' M76363-14 BD20880.D 810. 90.0 M76363-15 BD20881.D 81.0 90.0 M76363-16 BD20882.D 87.0 96.0 M76363-17 BD20883.D 82.0 91.0 M76363-18 BD20884.D 81.0 92.0 GBD990-BSD BD20851.D 830 91.0 ' GBD990-BSP BD20850.D 81.0 89.0 GBD990-MB BD20849.D 82.0 88.0 GBD991-BSD BD20875.D SIT 93.0 GBD991-BSP BD20874.D 840 93.0 GB:D991-MB BD20873.D 82{) 91.0 Surrogate Recovery Compounds Limits S1 = 2,5-Dibromotoluene 70-;13U% ' (a) Recovery from GC signal#1 (b) Recovery from GC signal#2 ®( 55 of 55 MACCUMB-T M76363 ^} Inspection and Monitoring Report for Phase V ROS-RTN 4-11301 October 17,2008 Former Texaco-Branded Service Station,1140 Iyannough Road,Hyannis,Massachusetts ATTACHMENT B SOVEP, EIGN CONSULTING INC . ' July 1,2008 DHL#27987250852 ' Town of Hyannis Town Engineer 367 Main Street ' Hyannis,Massachusetts 02601 Re: Groundwater Sampling Results,May 2008 ' In the Vicinity of: Former Texaco Service Station 1140 Iyannough Road ' RTN 4-11301 To Whom it May Concern; Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater g p gr ater samples from monitoring wells installed at the above referenced property. The samples were ' submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH) and gasoline oxygenates. A copy of the laboratory analytical is attached. ' As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVE CONSULTING,INC. ' JasoA Sherburne Project Manager ' cc: Mr.David Weeks,Motiva MassDEP-SERO Sovereign File-EQ711 ' 905B S. Main Street, Unit 202 •Mansfield,MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan BWSC 123 ' I This Notice is Related to Release Tracking Number 0 11301 I ' A. The address of th e disposal site related to this Notice and Release Tracking Number(provided above): ' 1. Street Address: 1140 tyannough Road City/Town: Hyannis Zip Code: 02601. ' B. This notice is being provided to the following party: 1. Name: Town of Hyannis,Town Engineer ' 2. Street Address: 367 Main Street City/Town: Hyannis Zip Code: 02601 ' C. This notice is being given to inform its recipient(the party listed in Section B): 2111.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ' ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from ' the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: ' 1. Street Address: 1140 tyannough Road City/Town: Hyannis Zip Code: 02601 ' 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ' ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase Ii Comprehensive Site Assessment ❑ Other ' 3. Description of property where sampling will be/has been conducted: (specify) ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other ' (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. ' Groundwater from monitoring wells E.Contact information related to the party providing this notice: ' Contact Name: Jason Sherburne Street Address: 905E South Main Street,Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: Sherburne@sovcon.com i ' NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE ' This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or ' hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts ' Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner ' subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving ' this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling ' will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. ' FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency 'Plan and related public involvement opportunities may be found at http://www.mass.qov/dei)/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule htm if you would like. to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. SOVEREIGN • July 1,2008 DHL#27987774850 ' The Wilder Companies Attn:Mary Ellen Cunha 800 Boylston Street ' Suite 1300 Boston,MA 02199 ' Re: Groundwater Sampling Results,May 2008 In the Vicinity of: Former Texaco Service Station 1140 lyannough Road RTN 4-11301 To Whom it May Concern; Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater ' samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH) and gasoline oxygenates. A copy of the laboratory analytical is attached. ' As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the ' undersigned at 508-339-3200. Sincerely, ' S OVE CONSU LTING,,INC. ' Jason Sherburne Project Manager ' cc: Mr.David Weeks,Motiva MassDEP-SERO ' Sovereign File-EQ711 ' 905B S. Main Street, Unit 202 •Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan LL I BWSC 123 I This Notice is Related to Release Tracking Number 4� 11301 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): ) 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 ' B. This notice is being provided to the following party: 1. Name: The Wilder Companies, Mary Ellen Cunha ' 2. Street Address: 800 Boylston Street,Suite 1300 City/Town: Boston Zip Code: 02199 ' C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ' ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (if item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ' ❑Utility-related Abatement Measure ❑ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase 11 Comprehensive Site Assessment ❑ Other ' 3. Description of property where sampling will be/has been conducted: (specify) ❑residential ✓❑commerical ❑industrial ❑school/playground ❑Other ' (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E.Contact Information related to the party providing this notice: ' Contact Name: Jason Sherburne Street Address: 905E South Main Street, Suite 202 CitylTown: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: isherbume@sovcon.com NOTICE OF ENVIRONMENTAL SAMPLING ' As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE ' This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the"disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts ' Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following ' the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling ' will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the ' Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal ' site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/reaion/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper ' right hand corner on the reverse side of this form when making file review appointments. I , i ' SOVEREIGN CONSULTING INC . July 1, 2008 DHL#27987809452 Festival of Hyannis, LLC 3333 NY Hyde Park New Hyde Park,NY 11042 ' Re: Groundwater Sampling Results,May 2008 In the Vicinity of: ' Former Texaco Service Station 1140 Iyannough Road RTN 4-11301 To Whom it May Concern; ' Pursuant to your authorization Sovereign Consulting Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH) and gasoline oxygenates. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation ' efforts. if you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. ' Sincerely, SOVE EI N CONSULTING,INC. Ja on Sherburne ' Project Manager cc: Mr.David Weeks,Motiva ' MassDEP-SERO Sovereign Pile-EQ711 905B S. Main Street, Unit 202 •Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 I� NOTICE OF ENVIRONMENTAL SAMPLING Is _� j As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan i BWSC 123 ' t i This Notice is Related to Release Tracking Number 11301 A. The address of the disposal site related to this o p Notice and Release Tracking Number(provided above): ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Festival of Hyannis LLC 2. Street Address: 3333 NY Hyde Park City/Town: New Hyde Park Zip Code: 11042 ' C. This notice is being given to inform its recipient(the party listed in Section B): n✓ 1.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ' ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. Z✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked,the analytical results from the environmental samplin2 must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ✓❑ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring Phase II Comprehensive Site Assessment ❑Other ' 3. Description of property where sampling will be/has been conducted: (specify) ❑residential E commerical ❑industrial ❑school/playground []Other ' (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E.Contact information related to the party providing this notice: Contact Name: Jason Sherburne Street Address: 905E South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: Sherburne@sovcon.com I ' NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or ' hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE ' This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts ' Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner ' subsequent'.y receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving ' this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis. of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, -' groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling ' will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. ' FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the ' Massachusetts Contingency Plan and related public involvement opportunities may be found at hftp://www.mass.gov/dep/­cleanuD/oview.htm. For more information regarding this notice, you may contact the: party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. SOVEREIGN CONSULTING INC . July 1,2008 DHL,#27987869350 ' Prime 132 LLC 1140 Iyannough Road Hyannis,MA 02601 Re: Groundwater Sampling Results,May 2008 In the Vicinity of: ' Former Texaco Service Station 1140 lyannough Road RTN 4-11301 ' To Whom it May Concern; ' Pursuant to your authorization Sovereign Consulting, lnc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPF} and gasoline oxygenates. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation ' efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. ' Sincerely, SOVE CONSULTING,INC. Ja on Sherburne ' Project Manager cc: Mr.David Weeks,Motiva 1 MassDEP-SERO Sovereign File—EQ711 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING LL7t ] As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan BWSC 123 This Notice is Related to Release Tracking Number 0' 11301 ' A. The address of the disposal p sal site related to this Notice and Release Tracking Number(provided above): ' 1. Street Address: 1140 lyannough Road. Cityrrown: Hyannis Zip Code: 02601 ' B. This notice is being provided to the following party: 1. Name: Prime 132 LLC 2. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 ' C. This notice is being given to inform its recipient(the parry listed in Section B): ❑✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. Z 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from ' the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 ^' 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response,Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ' ❑Utility-related Abatement Measure ✓❑ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑Other 3. Description of property where sampling will be/has been conducted: (specify) ❑residential E]commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater) to the extent known at the time of this notice. tGroundwater from monitoring wells E.Contact information related to the party providing this notice: Contact Name: Jason Sherburne Street Address: 905E South Main St.,Suite 202 City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: Jherburne@sovcon.com ' NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSONS PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts ' Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving ' this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, ' groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at hftp://www.mass.gov/deD/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form_ Information about the disposal ' site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedUte.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. SOVEREIGN y t July 1,2008 DHL#27987909751 ' Mr.Hans Keijser Town of Barnstable Water Supply Division ' 47 Old Yarmouth Road Hyannis,MA 02601 ' Re: Groundwater Sampling Results,May 2008 In the Vicinity of: Former Texaco Service Station ' 1140 Iyannough Road RTN 4-11301 ' Dear Mr.Keijser; Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater ' samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH) and gasoline oxygenates. A copy of the laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the ' undersigned at 508-339-3200. Sincerely, ' SOVE N CONSULTING,INC. J n Sherburne Project Manager ' cc: Mr.David Weeks,Motiva MassDEP-SERO ' Sovereign File-EQ711 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 I NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan LL� BWSC 123 This Notice is Related to Release Tracking Number 11301 ' A. The address of the disposal site related to this Notice P t ce and Release Tracking Number(provided above): ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Hans Keijser ' 2. Street Address: 47 Old Yarmouth Road City/Town: Hyannis Zip Code: 02601 ' C. This notice is being given to inform its reciplent(the party listed in Section B): ❑✓ 1.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ' Z 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked,the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ' ❑Utility-related Abatement Measure 0✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other 3. Description of property where sampling will be/has been conducted: (specify) ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other ' (specify) 4. Description of the sampling locations and types(e.g., soil,groundwater)to the extent known at the time of this notice. ' Groundwater from monitoring wells E. Contact information related to the party-providing this notice: ' Contact Name: Jason Sherburne Street Address: 905E South Main St.,, Suite 202 ' City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: jherburne@sovcon.com 1 NOTICE OF ENVIRONMENTAL SAMPLING ' As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan ' MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or ' hazardous material) to the environment. THE PERSONS PROVIDING THIS NOTICE ' This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner ' subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, ' groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling ' will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will betwere collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the ' Massachusetts Contingency Plan and related public involvement opportunities may be found at hfti)://www.mass.gov/dep/cleanUD/OView.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal ' site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See hftp://mass.gov/dep/about/region/Schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper ' right hand corner on the reverse side of this form when making file review appointments. SOVEPLEIGN CONSULTING INC . ' July 1,2008 DHL#27987959053 ' Ms. Donna Z. Miorandi Town of Barnstable Public Health Division ' 200 Main Street Hyannis,MA 02601 ' Re: Groundwater Sampling Results,May 2008 In the Vicinity of: Former Texaco Service Station ' 1140 Iyannough Road RTN 4-11301 Dear Ms. Miorandi; Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH) and gasoline oxygenates. A copy of the laboratory analytical is attached. ' As always, we thank you for our continued consideration and cooperation operatzon in our remediahon efforts. If you have any questions regarding this submittal, please feel free to contact the ' undersigned at 508-339-3200. Sincerely," SOVE I CONSULTING,INC. ' Jason Sherburne Project Manager cc: Mr.David Weeks,Motiva MassDEP-SERO ' Sovereign File—EQ711 ' 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 I 11 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan i LL BWSC 123 I This Notice is Related to Release Tracking Number [4 11301 ' A. The address of the disposal p sal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 ' B. This notice is being provided to the following party: 1. Name: Town of Barnstable,Donna Miorandi ' 2. Street Address: 200 Main Street City/Town: Hyannis Zip Code: 02601 ' C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. R2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. 0 3. Check to indicate if the analytical results are attached. (If item 2.above is checked,the analytical results from ' the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 ' 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ' ❑Utility-related Abatement Measure ✓❑ Phase WRemedy Operation Status ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑Other ' 3. Description of property where sampling will be/has been conducted: (specify) ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other ' (specify) 4. Description of the sampling locations and types(e.g.,soil,groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells E.Contact information related to the party providing this notice: ' Contact Name: Jason Sherburne Street Address: 905B South Main St.,Suite 202 ' City/Town: Mansfield Zip Code: 02048 Telephone: (508)339-3200 Email: jherburne@sovcon.com 1 ' NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan ' MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or ' hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE ' This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) ' PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts ' Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner ' subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, ' groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling twill be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. ' FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the ' Massachusetts Contingency Plan and related public involvement opportunities may be found at hftp://www.mass.gov/dep/cleanur)/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.-gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. CONSULTINGSOVEREIGN September 25,2008 DHL#29116771655 Town of Hyannis Town Engineer 367 Main Street Hyannis,Massachusetts 02601 ' Re: Groundwater Sampling Results,August 2008 In the Vicinity of: Former Texaco Service Station ' 1140Iyannough Road RTN 4-11301 To Whom it May Concern; Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater ' samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons(VPH). ' As always,we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SO WI CONSULTING,INC. ' Jrburne Project Manager ' cc: Mr.David Weeks,Motiva MassDEP-SERO Sovereign File-EQ711 905B S. Main Street, Unit 202 •Mansfield,MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 — NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan LBWSC 123 I This Notice is Related to ' Release Tracking Number KJ 11301 ' A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 ' B. This notice is being provided to the following party: 1. Name: Town of Hyannis,Town Engineer ' 2. Street Address: 367 Main Street City/Town: Hyannis Zip Code: 02601 ' C. This notice is being given to inform its recipient(the party listed in Section B): n1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ' Q 2. Of the results of environmental sampling conducted at property owned b the recipient of this notice.Y p t ce. ✓n 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from ' the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 ' 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑Phase ill Feasibility Evaluation ' ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring Phase 11 Comprehensive Site Assessment ❑ Other ' 3. Description of property where sampling will be/has been conducted: (specify) [l residential ❑✓ commerical ❑industrial ❑school/playground ❑Other 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. tGroundwater from monitoringwells s ' E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne ' Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 ' Telephone: (508) 339-3200 __ Email: Jsherburne@sovcon.com NOTICE OF ENVIRONMENTAL SAMPLING ' As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE ' This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or ' hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE ' This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner ' subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving ' this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, ' groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. ' Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during ' which the samples will be/were collected. FOR MORE INFORMATION ' Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at hftp://www.mass.gov/dep/cleanuPloview.htm. For more information regarding this notice, you may ' contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See hftp://mass._qovldep/about/reqion/schedule.htm' if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. SOVEREIGN CONSULTING INC . September 25,2008 DHL#29116728152 The Wilder Companies Attn: Mary Ellen Cunha ' 800 Boylston Street Suite 1300 ' Boston,MA 02199 Re: Groundwater Sampling Results,August 2008 ' In the Vicinity of: Former Texaco Service Station 1140 Iyannough Road R N 4-11301 To Whom it May Concern; ' Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were ' submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH). A copy of the laboratory analytical is attached. ' As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. ' Sincerely, SOVE CONSULTING,INC. Jas Sherburne Pr ject Manager ' cc: Mr.David Weeks,Motiva MassDEP-SERO Sovereign File-EQ711 5'05B S. Main Street Unit 2 _ -' 02 Mansfield,MA 02048 Tel: 508-339-3200 Fax: 508 339 3248 ' NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan ' I BWSC 123 L This Notice is Related to ' i Release Tracking Number ,44 11301 ' A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 11401yannough Road ' City/Town: Hyannis Zip Code: 02601, ' B. This notice is being provided to the following party: 1. Name: The wilder Companies, Mary Ellen Cunha ' 2. Street Address: 800 Boylston Street, Suite 1300 City/Town: Boston Zip Code: 02199 ' C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ' F/I 2. Of the results of environmental sampling conducted at property p g p perty owned by the recipient of this nonce. ' 0✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 ' 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ' ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ✓❑ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation [j Post-Class C Operation, Maintenance and Monitoring ' ❑Phase II Comprehensive Site Assessment ❑ Other (specify) 3. Description of property where sampling will be/has been conducted: ' ❑residential Ocommerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells ' E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne ' Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 Tclonhnnw (508) 339-3200 r-r„�ii- isherburne(cD..sovcon.com NOTICE OF ENVIRONMENTAL SAMPLING ' As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) ' PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner ' subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving ' this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, ' groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. ' Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during ' which the samples will be/were collected. FOR MORE INFORMATION ' Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at ' http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental ' Protection. See http://mass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. SOVEP, EIGN CONSULTING INC . September 25,2008 DHL#29116843556 Festival of Hyannis,LLC 3333 NY Hyde Park New Hyde Park,NY 11042 ' Re: Groundwater Sampling Results,August 2008 In the Vicinity of: Former Texaco Service Station 1140 Iyannough Road RTN 4-11301 ' To Whom it May Concern; Pursuant to your authorization Sovereign Consulting Inc. personnel collected groundwater ' samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH). A copy of the laboratory analytical is attached. ' As always, we thank you for your continued consideration and cooperation in our remediation efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, ' SOVE CONSULTING,INC. Jas Sherburne P ject Manager ' cc: Mr.David Weeks,Motiva MassDEP-SERO Sovereign File-EQ711 ' 905B S. Main Street. Unit 202 • Mansfield. MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 ' NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan L7/ i BWSC 123 ! This Notice is Related to Release Tracking Number 11301 ' A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road ' City/Town: Hyannis Zip Code: 02601 ' B. This notice is being provided to the following party: 1. Name: Festival of Hyannis LLC ' 2. Street Address: 3333 NY Hyde Park CitylTown: New Hyde Park Zip Code: 11042 ' C. This notice is being given to inform its recipient(the party listed in Section B)c Q 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ' ❑✓ 2. Of the results of environmental sa mpling conducted at property owned by the recipient of this notice. ❑✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will belhas been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ' ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase 1 Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring ' ❑Phase II Comprehensive Site Assessment ❑ Other 3. Description of property where sampling will be/has been conducted: (specify) ' ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types (e.g., soil, groundwater) to the extent known at the time of this notice. Groundwater from monitoring wells ' E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne Street Address: 905B South Main Street, Suite 202 City/Town: Mansfield Zip Code: 02048 ' -roio.,ti,,.,o• (508)339-3200 c.,...,a• iSharhiirnanN czrwrnn rnm 1 .NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE ' This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or ' hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE ' This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) ' PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts ' Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner ' subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving ' this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, t groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. ' Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during ' which the samples will be/were collected. ' FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at hftp://www.mass.qov/dep/cleanur)/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental ' Protection. See hftp://mass.-CLO-Vldep/about/region/scheduIe.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. 1 September 25,2008 DHL#t29116695952 Mr. Hans Keijser Town of Barnstable ' Water Supply Division 47 Old Yarmouth Road Hyannis,MA 02601 Re: Groundwater Sampling Results,August 2008 In the Vicinity of: ' Former Texaco Service Station 1140 Iyannough Road .RTN 4-11301 Dear Mr.Keijser; ' Pursuant to your authorization Sovereign Consulting, Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH). A copy of the ' laboratory analytical is attached. As always, we thank you for your continued consideration and cooperation in our remediation ' efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. ' Sincerely SOVE G CONSULTING,INC. Jaso Sherburne Pro ect Manager cc: Mr.David Weeks,Motiva ' MassDEP-SERO Sovereign File-EQ711 905B S. Main Street, Unit 202 • Mansfield,MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan ' BWSC 123 This Notice is Related to ' Release Tracking Number 11301 ' A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road ' City/Town: Hyannis Zip Code: 02601 B. This notice is being provided to the following party: ' 1. Name: Town of Barnstable, Hans Keijser ' 2. Street Address: 47 Old Yarmouth Road City/Town: Hyannis Zip Code: 02601 ' C. This notice is being given to inform its recipient(the party listed in Section B): Q✓ 1. That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ' �✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. Q✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑Immediate Response Action ❑ Phase III Feasibility Evaluation ' ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation, Maintenance and Monitoring R Phase II Comprehensive Site Assessment ❑ Other 3. Description of property where sampling will be/has been conducted: (specify) ❑residential []✓ commerical ❑industrial ❑school/playground ❑Other ' tion of the sampling (specify) 4. Description mpling locations and types (e.g., soil, groundwater) to the extent known at the time of this notice. ' Groundwater from monitoring wells ' E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne ' Street Address: 905B South Main St., Suite 202 City/Town: Mansfield Zip Code: 02048 ' Telephone: (508)339-3200 Finail- jsherburnePsovcon.com NOTICE OF ENVIRONMENTAL SAMPLING ' As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE ' This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE ' This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts ' Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner ' subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving ' this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. ' Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during ' which the samples will be/were collected. FOR MORE INFORMATION ' Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at hftp://Www.mass.qov/dep/cleanuD/oview.htm. For more information regarding this notice, you may ' contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.gov/dep/about/region/schedule htm if you would like to make an ' appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. SOVEItEIGN CONSULTING INC . September 25,2008 DHL##29116656656 Ms. Donna Z.Miorandi Town of Barnstable ' Public Health Division 200 Main Street Hyannis,MA 02601 ' Re: Groundwater Sampling Results,August 2008 In the Vicinity of: ' Former Texaco Service Station 1140 Iyannough Road RTN 4-11301 ' Dear Ms.Miorandi; ' Pursua_rit to your authorization Sovereign Consulting, Inc. personnel collected groundwater samples from monitoring wells installed at the above referenced property. The samples were submitted for laboratory analysis of volatile petroleum hydrocarbons (VPH). A copy of the ' laboratory analytical is attached. As always,we thank you for your continued consideration and cooperation in our remediation ' efforts. If you have any questions regarding this submittal, please feel free to contact the undersigned at 508-339-3200. Sincerely, SOVE7 CONSULTING,INC. jaso herburne ' Pr ' ct Manager cc: Mr.David Weeks,Motiva ' MassDEP-SERO Sovereign File-EQ711 ' 905B S. Main Street, Unit 202 • Mansfield, MA 02048 •Tel: 508-339-3200 • Fax: 508-339-3248 J NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan L BWSC 123 This Notice is Related to Release Tracking Number 4 1 11301 ' A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address: 1140 lyannough Road ' City/Town: Hyannis Zip Code: 02601 ' B. This notice is being provided to the following party: 1. Name: Town of Barnstable, Donna Miorandi ' 2. Street Address.. 200 Main Street City/Town: Hyannis Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): ❑✓ 1_ That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ' z 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. ✓❑3. Check to indicate if the analytical results are attached. (If item 2. above is checked, the analytical results from ' the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: ' 1. Street Address: 1140 lyannough Road City/Town: Hyannis Zip Code: 02601 2. MCP phase of work during which the sampling will be/has been conducted: ❑immediate Response Action ❑ Phase III Feasibility Evaluation ' ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑✓ Phase V/Remedy Operation Status ❑Phase I Initial Site Investigation ❑ Post-Class C Operation,Maintenance and Monitoring ❑Phase Il Comprehensive Site Assessment ❑ Other ' 3. Description of property where sampling will be/has been conducted: (specify) ' ❑residential ❑✓ commerical ❑industrial ❑school/playground ❑Other (specify) 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the time of this notice. Groundwater from monitoring wells ' E. Contact information related to the party providing this notice: Contact Name: Jason Sherburne ' Street Address: 905B South Main St., Suite 202 City/Town: Mansfield Zip Code: 02048 ' TAIPnhnnP• (508)339-3200 r-mn;i- iherbume ansovcon.com NOTICE OF ENVIRONMENTAL SAMPLING ' As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE ' This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSONS PROVIDING THIS NOTICE ' This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts ' Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner ' subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during ' which the samples will be/were collected. FOR MORE INFORMATION ' Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass.gov/dep/cleanup/oview.htm. For more information regarding this notice, you may ' contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See http://mass.qov/dep/about/region/schedule.htm if you would like to make an ' appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. 1