Loading...
HomeMy WebLinkAbout0009 SCUDDER'S LANE - Health (2) c�e�s ��C; cc - s NOTICE OF ENVIRONM TAL SAM LI i As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan r' I BWSC 123 J' ( This Notice is Related to Release Tracking Number 4� 21167 A. The address of the disposal site related to this Notice and Release Tracking Number(provided above): 1. Street Address:�ealves.,l?asture_Lane_anScudder's-Lane City/Town We`st`Barnstable: Zip Code°_02630.000.0 B. This notice is being provided to the following party: 1. Name: Thomas A. McKean, Health Division 2. Street Address: 200 Main Street City/Town: Hyannis, MA Zip Code: 02601 C. This notice is being given to inform its recipient(the party listed in Section B): z1.That environmental sampling will be/has been conducted at property owned by the recipient of this notice. ❑✓ 2. Of the results of environmental sampling conducted at property owned by the recipient of this notice. Q✓ 3. Check to indicate if the analytical results are attached. (If item 2. above is checked,the analytical results from the environmental sampling must be attached to this notice. D. Location of the property where the environmental sampling will be/has been conducted: 1. Street Address: Calves Pasture Lane,Scudder's-Lane-and-shoulder-of RtAA-fromScudder's Lane to center of Hifckley-Pond-(500'+) City/Town: West Barnstable Zip Code: 02630-0000 2. MCP phase of work during which the sampling will be/has been conducted: �[ .I mm ediate Response Action ❑Phase III Feasibility Evaluation ❑Release Abatement Measure ❑ Phase IV Remedy Implementation Plan ❑Utility-related Abatement Measure ❑ Phase V/Remedy Operation Status k ❑Phase I Initial Site Investigation ❑Post-Class C Operation, Maintenance and Monitoring ❑Phase II Comprehensive Site Assessment ❑ Other C: (specify) ' 3. Description of property where sampling will be/has been conducted: El residential ❑commerical El industrial ❑school/playground ❑✓ Other Put Lroad (specify) " 4. Description of the sampling locations and types(e.g., soil, groundwater)to the extent known at the dime of ttiis notice. On April 17, 2008 soil, surface water and sediment samples where collected in the area of the above.:' referenced public roadways. The associated laboratory data is attached. Further sampling and assessment a s proposed for Thursday,May 8, 2008. The laboratory results will follow. E. Contact information related to the party providing this notice: Contact Name: Susan A. Jason, LSP Street Address: PO Box 1088 City/Town: Lakeville Zip Code: 02347 Telephone: (508)947-0050 Email: sjason@primeengineering.org i NOTICE OF ENVIRONMENTAL SAMPLING As required by 310 CMR 40.1403(10) of the Massachusetts Contingency Plan MASSACHUSETTS REGULATIONS THAT REQUIRE THIS NOTICE This notice is being provided pursuant to the Massachusetts Contingency Plan and the notification requirement at 310 CMR 40.1403(10). The Massachusetts Contingency Plan is a state regulation that specifies requirements for parties who are taking actions to address releases of chemicals (oil or hazardous material) to the environment. THE PERSON(S) PROVIDING THIS NOTICE This notice has been sent to you by the party who is addressing a release of oil or hazardous material to the environment at the location listed in Section A on the reverse side of this form. (The regulations refer to the area where the oil or hazardous material is present as the "disposal site".) PURPOSE OF THIS NOTICE When environmental samples are taken as part of an investigation under the Massachusetts Contingency Plan at a property on behalf of someone other than the owner of the property, the regulations require that the property owner (listed in Section B on the reverse side of this form) be given notice of the environmental sampling. The regulations also require that the property owner subsequently receive the analytical results following the analysis of the environmental samples. Section C on the reverse side of this form indicates the circumstance under which you are receiving this notice at this time. If you are receiving this notice to inform you of the analytical results following the analysis of the environmental samples, you should also have received, as an attachment, a copy of analytical results. These results should indicate the number and type(s) of samples (e.g., soil, groundwater) analyzed, any chemicals identified, and the measured concentrations of those chemicals. Section D on the reverse side of this form identifies the property where the environmental sampling will be/has been conducted, provides a description of the sampling locations within the property, and indicates the phase of work under the Massachusetts Contingency Plan regulatory process during which the samples will be/were collected. FOR MORE INFORMATION Information about the general process for addressing releases of oil or hazardous material under the Massachusetts Contingency Plan and related public involvement opportunities may be found at http://www.mass. oq v/dep/cleanup/oview.htm. For more information regarding this notice, you may contact the party listed in Section E on the reverse side of this form. Information about the disposal site identified in Section A is also available in files at the Massachusetts Department of Environmental Protection. See httg:Hmass.gov/dep/about/region/schedule.htm if you would like to make an appointment to see these files. Please reference the Release Tracking Number listed in the upper right hand corner on the reverse side of this form when making file review appointments. TABLE 2 SUMMARY OF ANALYTICAL RESULTS FOR GROUNDWATER SAMPLES COLLECTED ON APRIL 17 AND 18,2008 WITHIN SHEPHARDS WAY,CALVES PASTURE LANE AND SCUDDER LANE WEST BARNSTABLE,MA METHOD 1 MCP' STANDARDS SAMPLE IDENTIFACTION ANALYTES UNITS GW-1 GW-2 GW-3 SW-1 SW BACK SW BARN STANDARD STANDARD STANDARD HINCK HARBOR EXTRACTABLE PETROLEUM HYDROCARBONS(EPH Method) C9-C18 Aliphatics ug/L 700 5,000 50,000 <100 Z <101 <102 C19-C36 Aliphatics ug/L 14,000 NA 3 50,000 <100 <101 <102 C11-C22 Aromatics ug/L 200 50,000 5,000 <100 <101 <102 POLYAROMATIC HYDROCARBONS(EPH Method) Acenaphthene ug/L 20 NA 6,000 <0.400 <0.404 <0.408 Acenaphthylene ug/L 30 10,000 40 <0.400 <0.404 <0.408 Anthracene ug/L 60 NA 30 <0.400 <0.404 <0.408 Benz(a)Anthracene ug/L 1 NA 1,000 <0.400 0.417 <0.408 Benzo(a)Pvrene ug/L 0.2 NA 500 <0.200 6.405 4 <0.202 Benzo(b)Fluoranthene ug/L 1 NA 400 <0.400 0.522 <0.408 Benzo(g,h,i)Perylene ug/L 50 NA 20 <0.400 <0.404 <0.408 Benzo(k)Fluoranthene ug/L 1 NA 100 <0.400 <0.404 <0.408 Chrysene ug/L 2 NA 70 <0.400 0.564 <0.408 Dibenzo(a,h)Anthracene ug/L 0.5 NA 40 <0.400 <0.404 <0.408 Fluoranthene ug/L 90 NA 200 <0.400 1.18 <0.408 Fluorene ug/L 30 NA 40 <0.400 <0.404 <0.408 Indeno(1,2,3-cd)Pyrene ug/L 0.5 NA 100 <0.400 <0.404. <0.408 Methylnaphthalene,2- ug/L 10 2,000 20,000 <0.400 <0.404 <0.408 Naphthalene ug/L 140 1,000 20,000 <0.400 <0.404 <0.408 Phenanthrene ug/L 40 NA 10,000 <0.400 0.488 <0.408 Pyrene ug/L $0 NA 20 <0.400 0.838 <0.408 OTE: 1 MCP -Supplemental MCP Amendments"Clean"Version of Amendments to the Massachusetts Contingency Plan,310 CMR 40.0000;effective February 14,2008 2 <100=Parameter was not found above the detection limit of 100. 3 NA - Not Applicable. 4 Bold and underlined values exceed most strineent MCP Standards. 5 NS - No Standard. Generated Table by VH 5/2/08 QA'd DATA by ESW 5/6/08 PRIME ENGINEERING, INC. QA STANDARDS CEE 5/7/08 -- .a 04280820:22 HA T 1 C A L - ANALYTICAL REPORT Lab Number: L0805612 Client: Prime Engineering 350 Bedford Street PO Box 1088 Lakeville, MA 02347 ATTN: Scott Kraihanzel Project Name: CAVES PASTURE/SCUDDERS LN. Project Number:. 14190101 Report Date: 04/28/08 Certifications&Approvals: MA(M-MA086),NY NELAC(11148),CT(PH-0574),NH(2003),NJ(MA935),RI(LA000065),ME(MA0086), PA(Registration#68-03671),USDA(Permit#S-72578),US Army Corps of Engineers,Naval FESC. Eight Walkup Drive, Westborough, MA 01581-1019 508-898-9220 (Fax)508-898-9193 800-624-9220-www.alphalab.com Page 1 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 Alpha Sample ID Client ID Sample Location L0805612-01 COMP1 WEST BARNSTABLE, MA L0805612-02 COMP2 WEST BARNSTABLE, MA L0805612-03 COMP3 WEST BARNSTABLE, MA L0805612-04 COMP4 WEST BARNSTABLE, MA L0805612-05 INFILTRATOR CLEAN OUT WEST BARNSTABLE, MA L0805612-06 BG-1 CP WEST BARNSTABLE, MA L0805612-07 BG-2SHEP WEST BARNSTABLE, MA L0805612-08 MH-1 WEST BARNSTABLE, MA L0805612-09 SW-1 WEST BARNSTABLE, MA L0805612-10 SED/WL-1 WEST BARNSTABLE, MA L0805612-11 WL-2 WEST BARNSTABLE, MA L0805612-12 WL-3 WEST BARNSTABLE, MA L0805612-13 WL/ROAD SHOULDER 4 WEST BARNSTABLE, MA L0805612-14 WL-5 WEST BARNSTABLE, MA L0805612-15 B-23 WEST BARNSTABLE, MA L0805612-16 B-24 WEST BARNSTABLE, MA L0805612-17 SW BACK HINCK WEST BARNSTABLE, MA L0805612-18 SED BACK HINCK WEST BARNSTABLE, MA L0805612-19 SW BARN HARBOR WEST BARNSTABLE, MA L0805612-20 SED BARN HARBOR WEST BARNSTABLE, MA L0805612-21 B-32 2656 RTE 6A WEST BARNSTABLE, MA L0805612-22 BG 6A CB 2631 WEST BARNSTABLE, MA L0805612-23 BG WL 2615 WEST BARNSTABLE, MA L0805612-24 RAW PRODUCT WEST BARNSTABLE, MA Page 2 of 117 f 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 MADEP MCP Response Action Analytical Report Certification This form provides certifications for all samples performed by MCP methods. Please refer to the Sample Results and Container Information sections of this report for specification of MCP methods used for each analysis.The following questions pertain only to MCP Analytical Methods. An affirmative response to questions A, B, C& D is required for"Presumptive Certainty"status A Were all samples received by the laboratory in a condition consistent with those described on YES their Chain-of-Custody documentation for the data set? B Were all QA/QC procedures required for the specified analytical methods(s)included in this YES report followed, including the requirement to note and discuss in a narrative QC data that did not meet appropriate erformance standards orguidelines? C Does the analytical data included in this report meet all the requirements for"Presumptive YES Certainty", as described in section 2.0 of the MADEP document CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? D VPH and EPH methods only: Was the VPH or EPH method run without significant modifications, YES as specified in Section 11.3? A response to questions E and F is required for"Presumptive Certainty"status E Were all QC performance standards and recommendations for the specified method(s) NO achieved? F Were results for all analyte-list compounds/elements for the specified method(s)reported? YES For any questions answered "No", please refer to the case narrative section on the following page(s). Please note that sample matrix information is located in the Sample Results section of this report. Page 3 of 117 04280820:22 r Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted.Sample Receipt,Container Information,and the Chain of Custody are located at the back of the report. The data presented in this report is organized by parameter(i.e.VOC,SVOC,etc.).Sample specific Quality Control data(i.e. Surrogate Spike Recovery)is reported at the end of the target analyte list for each individual sample,followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported,the Laboratory ID of the re-analysis or re- extraction is designated with an"R"or"RE", respectively.When multiple Batch Quality Control elements are reported(e.g. more than one LCS),the associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch,Sample Specific%recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. Non-MCP Related Narratives Report Submission The analysis of TPH-PHI is being performed at our Mansfield facility,and the results will be issued under separate cover. TOC The analysis of TOC was performed at our Mansfield facility.The results are provided within this report and a copy of the laboratory report is included as an addendum. MCP Related Narratives Sample Receipt Sample containers were not received for the sample identified as"WIL-Y. Page 4 of 117 �'� C 04280820:22 i Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 Case Narrative (continued) EPH L0805612-01,-04 and-15 have elevated detection limits due to the dilutions required by the matrix interferences encountered during the concentration of the samples and by additional analytical dilutions required by the matrix of the samples. L0805612-02,-16,-21 and-23 have elevated detection limits due to the dilutions required by matrix interferences encountered during the concentration of the samples. L0805612-24, as well the associated QC, have elevated detection limits due to the limited sample volume utilized during extraction, as required by the sample matrix. L0805612-24 also required a dilution due to matrix interferences encountered during the concentration of the sample. In reference to question E: i The surrogate recovery for L0805612-01 is below the acceptance criteria for o-Terphenyl-MS due to the dilutions required to quantitate the sample. Re-extraction is not required;therefore,the results of the original analysis are reported. The surrogate recoveries for L0805612-04 are below the acceptance criteria for Chloro-Octadecane,o- Terphenyl and o-Terphenyl-MS due to the dilutions required to quantitate the sample. Re-extraction is not required; therefore,the results of the original analysis are reported. The surrogate recoveries for L0805612-10 were below the acceptance criteria for Chloro-Octadecane, o- Terphenyl and o-Terphenyl-MS; however, re-extraction achieved similar results.The results of both extractions are reported; however, all associated compounds are considered to have a potentially low bias. The WG319714-2/3 LCS/LCSD RPD, associated with L0805612-14 and-23, is above the acceptance criteria for Nonane; however, the individual LCS/LCSD recoveries are within method limits.The results of the associated samples are reported. The WG319733-2/3 LCS/LCSD RPD, associated with L0805612-24, is above the acceptance criteria for Benzo(b)fluoranthene; however,the individual LCS/LCSD recoveries are within method limits.The results of the associated sample are reported. I, the undersigned, attest under the pains and penalties of perjury that,to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: `� �N ►`�``v"`�Y"0 Title: Technical Director/Representative Date: 04/28/08 Page 5 of 117 NxE . 04280820:22 d ORGANICS Page 6 of 117 04280820:22 PETROLEUM HYDROCARBONS i Page 7 of 117 04280820:22 r Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-01 Date Collected: 04/17/08 11:00 Client ID: COMP1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/23/08 17:37 Analyst: AJ Percent Solids: 97% :: QualityContratlnformatton� x.,.,=... Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor EPH wtth MS Targets j C9-C18 Aliphatics ND mg/kg 68.7 10 __... _......... . ........... C19-C36 Aliphatics 3300 mg/kg 68.7 10 _...._ _ __.. .. ........._.. ...... C11-C22 Aromatics 541 mg/kg 68.7 10 C11-C22 Aromatics,Adjusted 528 mg/kg 68.7 10 Naphthalene ND mg/kg 1.37 50 ......... _.. _... ___ _ _.__.... 2-Methyl naphthalene ND mg/kg 1.37 50 Acenaphthylene ND mg/kg 1.37 50 _._......_.. ... _...._.__ ...__....... ......... Acenaphthene ND mg/kg 1.37 50 Fluorene ND mg/kg 1.37 50 _.._. ......._ _........... ............_ _._ .... Phenanthrene 1.42 mg/kg 1.37 50 ......... _....__.... . .... _.__..... ......._. Anthracene ND mg/kg 1.37 50 Fluoranthene 3.64 mg/kg 1.37 50 ........... ........ ..._.I ............._..__. ......... _...__... ... ............................... Pyrene 2.92 mg/kg 1.37 50 Benzo(a)anthracene 1.93 mg/kg 1.37 50 _......... ..... .__.....__. _ ._......... .......... .,........ Chrysene 1.71 mg/kg 1.37 50 Benzo(b)fluoranthene 1.70 mg/kg 1.37 50 ......_....__ .... ......... ..... ..._. Benzo(k)fluoranthene ND mg/kg 1.37 50 .......... _......_.... ..._...... ._._.... ..... _.. _.. ... Benzo(a)pyrene 1.54 mg/kg 1.37 50 ........ _.. Indeno(1,2,3-cd)Pyrene ND mg/kg 1.37 50 ............ ... .... ........ ........ __.... Dibenzo(a,h)anthracene ND mg/kg 1.37 50 Benzo(ghi)perylene ND mg/kg 1.37 50 _.. ................ ... __..... .... _................ � HA Page 8 of 117 it i 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-01 Date Collected: 04/17/08 11:00 Client ID: COMP1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep, Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPHfwlth M"�STargets '' 07'w- '— Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 81 40-140 o-Terphenyl 101 40-140 2-Fluorobiphenyl 91 40-140 2-Bromonaphthalene 93 40-140 O-Terphenyl-MS ND 40-140 HA 1 Page 9 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 � r Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-02 Date Collected: 04/17/08 11:30 Client ID: COMP2 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/25/08 16:59 Analyst: AJ Percent Solids: 95% Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor C9-Cl8 Aliphatics ND mg/kg 70.2 10 C19-C36 Aliphatics 747 nI 70.2 10 C11-C22 Aromatics 251 mg/kg 70.2 10 C11-C22 Aromatics,Adjusted 240 mg/kg 70.2 10 Naphthalene ND mg/kg 0.281 10 2-Methylnaphthalene ND nI 0.281 10 Acenaphthylene !ND mg/kg_ - 0.281 10 ...... _ ...... .. ._ _...... _ _.......... ...... ..._._....... ... ....... ............. Acenaphthene ND mg/kg 0.281 10 Fluorene ND mg/kg 0.281 10 Phenanthrene 0.566 mg/kg 0.281 10 .........._ ........... ......._. _.._. Anthracene ND mg/kg 0.281 10 _ ....... ......... _.._....._. __......._ ...__ .... ......... _...._ Fluoranthene 2.10 mg/kg 0.281 10 ._....... ... ..._..._..__ ............ __.....__. .... ......_ ... _ ......__...... ............._....._ ....._ ......._.....__ ........... Pyrene 1.52 mg/kg0.281 10 Benzo(a)anthracene 1.16 mg/kg 0.281 10 _. .....- ......... __...... ........ ......... Chrysene 0.944 nI 0.281 10 Benzo(b)fluoranthene 0.702 mg/kg 0.281 10 ..... __.. Benzo(k)fluoranthene 1.02 mg/kg 0.281 10. __ .......... ........__ _. ..... _ _ . ..... Benzo(a)pyrene 0.943 nI 0.281 10 .......... _..._..._. _ ......_... _. _.._...._.. Indeno(1,2,3-cd)Pyrene 0.575 mg/kg 0.281 10 -_... ................__.........................._ .......... ..._ ..... .. ........... ......... Dibenzo(a,h)anthracene ND mg/kg 0.281 10 Benzo(ghi)perylene 0.653 mg/kg 0.281 10.._... _..... ......_....._ .._..__._ _.......... ..._._, . _ . _........ Page 10 of 117 I i 04280820:22 Y Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-02 Date Collected: 04/17/08 11:30 Client ID: COMP2 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH with MS Tar�ets � �� � ,., Im � Ow Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 83 40-140 o-Terphenyl 92 40-140 2-Fluorobiphenyl 84 40-140 2-Bromonaphthalene 84 40-140 O-Terphenyl-MS 94 40-140 HA Page 11 of 117 04280820:22 r r Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-03 Date Collected: 04/17/08 12:00 Client ID: COMP3 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 18:23 Analyst: AJ Percent Solids: 87% h � , Qualit�r` Cont�ol Infor a Ion �a' r Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method 7777 Parameter Result Qualifier Units RDL Dilution Factor I EPH wlth MS Tar ets st° z, :.• C9-Cl8 Aliphatics 18.0 mg/kg 7.66 1 C19-C36 Aliphatics 1270 mg/kg 7.66 1 __..... .... ....._.... ....... _..._.._, C11-C22 Aromatics 86.8 mg/kg 7.66 1 _.... _.....__. .. ..__......... __.. .._...... C11-C22 Aromatics,Adjusted 86.7 mg/kg 7.66 1 Naphthalene ND mg/kg 0.031 1 2-Methylnaphthalene ND mg/kg 0.031 1 Acenaphthylene ND mg/kg 0.031 1 _ ._....... ......... ........... .......__..._._....... Acenaphthene ND mg/kg 0.031 1 Fluorene ND mg/kg 0.031 1 __ _.._.... ... Phenanthrene ND mg/kg 0.031 1 ........... _...... _ __ . ....._.... Anthracene ND mg/kg 0.031 1 _... _.. .... _............. ....... _.__ .... _._ ........ ....... _._ .._....... Fluoranthene 0.048 mg/kg 0.031 . 1 ....... ...... _.......... __.. ...._..... . .... ......_-_.. .. ..........._ _...__ ..._.._.. .....--_.... _....... Pyrene 0.041 mg/kg 0.031 1 Benzo(a)anthracene ND mg/kg 0.031 1 _.... _. . ._._..... ......... _.........._............. ......... Chrysene ND mg/kg 0.031 1 Benzo(b)fluoranthene ND mg/kg 0.031 1 Benzo(k)fluoranthene ND mg/kg 0.031 _ 1 ....... ... .. _ ......_.... ............. Benzo(a)pyrene ND mg/kg 0.031 1 ....... _. _ .... . ......__.... Indeno(1,2,3-cd)Pyrene ND mg/kg 0.031 1 ......... ....._.... ......... ............ Dibenzo(a,h)anthracene ND mg/kg 0.031 1 Benzo(ghi)perylene ND mg/kg 0.031 1 ........._ ......... - ........ .. ........................__ ..... , 14A Page 12 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-03 Date Collected: 04/17/08 12:00 Client ID: COMP3 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH WIth,MS,TargetstM �� ,.,� _ � � Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 76 40-140 o-Terphenyl 80 40-140 2-Fluorobiphenyl 76 40-140 2-Bromonaphthalene 78 40-140 O-Terphenyl-MS 97 40-140. All Y�Firl Page 13 of 117 04280820:22 ►Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 r Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-04 Date Collected: 04/17/08 12:30 Client ID: COMP4 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/25/08 11:19 Analyst: AJ Percent Solids: 94% QualltyCon#rot Infvrmatlon Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method � x Parameter Result Qualifier Units RDL Dilution Factor EP th MS Targets .��� '° "�'� �°�� 3� '•� 7, � � �F: q C9-C18 Aliphatics ND mg/kg 177 25 C19-C36 Aliphatics 454 mg/kg 177 25 C11-C22 Aromatics 371 mg/kg 177 25 C11-C22 Aromatics,Adjusted 369 mg/kg 177 25 .. ........ Naphthalene IND mg/kg 2.84 100 2-Methylnaphthalene ND mg/kg 2.84 100 Acenaphthylene ND mg/kg 2.84 100 ......... _... Acenaphthene ND mg/kg 2.84 100 Fluorene ND mg/kg 2.84 100 ....... ...._........ __......... _ _ Phenanthrene ND mg/kg 2.84 100 ......_. ......__.... ___ _. - ..... Anthracene ND mg/kg 2.84 100 __..... _._ _ ........_........ _..... __... ....... _.... _ Fluoranthene 5.03 mg/kg 2.84 100 ......... .. - ..... _. ......... .......... Pyrene 4.10 mg/kg 2.84 100 Benzo(a)anthracene ND mg/kg 2.84 100 ._. .... _....._ ._......... Chrysene ND mg/kg 2.84 100 Benzo(b)fluoranthene ND mg/kg 2.84 100 .. _....__ __...... Benzo(k)fluoranthene ND mg/kg2.84 100 . ........ ........ ..__._.. Benzo(a)pyrene ND mg/kg 2.84 100 _....... ..... _ _.. .. Indeno(1,2,3-cd)Pyrene ND mg/kg 2.84 100 .............. ... _._ ..._......... ........._ ... ......... ......... Dibenzo(a,h)anthracene ND mg/kg 2.84 100 Benzo(ghi)perylene ND mg/kg 2.84 100 ..... ...._._____.. . ........- .. ........... .. . ......... . .......... .....__...._.. Page 14 of 117 i 04280820:22 v Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-04 Date Collected: 04/17/08 12:30 Client ID: COMP4 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor rj"9u EPI -..... a�rinei ,Gb w 'S i with �� ., _ . Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane ND 40-140 o-Terphenyl ND 40-140 i 2-Fluorobiphenyl 77 40-140 2-Bromonaphthalene 77 40-140 O-Terphenyl-MS ND 40-140 ?HA Asp, Page 15 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-05 Date Collected: 04/17/08 09:00 Client ID: INFILTRATOR CLEAN OUT Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/25/08 13:28 Analyst: AJ Percent Solids: 74% '� � 'N � �Quality Control In ormatron � � � x Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor EPH with C9-C18 Aliphatics ND mg/kg 9.01 1 C19-C36 Aliphatics 33.9 mg/kg 9.01 1 C11-C22 Aromatics 15.5 mg/kg 9.01 1 C11-C22 Aromatics,Adjusted 15.3 mg/kg 9.01 1 Naphthalene ND mg/kg 0.036 1 2-Methylnaphthalene ND mg/kg 0.036 1 Acenaphthylene ND mg/kg 0.036 1 _....._.. ......._. _... Acenaphthene ND mg/kg 0.036 1 Fluorene ND mg/kg 0.036 1 __... ..._.......... _... .......... _.._... _...... Phenanthrene ND mg/kg 0.036 1 Anthracene ND mg/kg 0.036 1 _......... ............ _.... . Fluoranthene 0.060 mg/kg 0.036 1 .....____ ........... _...._ ......__....__ ....._._ _ .._.......... _. ........ ................_ _ ..I....... .__ ....... ............... Pyrene 0.049 mg/kg0.036 1 Benzo(a)anthracene ND mg/kg 0.036 1 .................. Chrysene ND mg/kg 0.036 1 Benzo(b)fluoranthene 0.037 mg/kg 0.036 1 _........ . ......... ... ...___ __. _...._ ....... _....._ _ Benzo(k)fluoranthene ND mg/kg 0.036 1 - - _.. _.._.._ .. _._.......... __..__... ..........__... .._... .. _ Benzo(a)pyrene ND mg/kg 0.036 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.036 1 ........ ......... _ _ ..........._ .....__....... _, _....__ ................ .. .............. -.....-_ ......... ......... Dibenzo(a,h)anthracene ND mg/kg 0.036 1 Benzo(ghi)perylene ND mg/kg 0.036 1 ................ L�t iA Page 16 of 117 ti 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-05 Date Collected: 04/17/08 09:00 Client ID: INFILTRATOR CLEAN OUT Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH wlthMS Tar9 etsF � y w � IM Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 89 40-140 o-Terphenyl 77 40-140 2-Fluorobiphenyl 79 40-140 2-Bromonaphthalene 81 40-140 O-Terphenyl-MS 82 40-140 l Page 17 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 � t Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-06 Date Collected: 04/17/08 09:30 Client ID: BG-1CP Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 14:02 Analyst: AJ Percent Solids: 96% Quallty�Controiolnformatton * " ., .,.u..,,. .. . ... M ...._ .....u. Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method -"o Parameter Result Qualifier Units RDL Dilution Factor pq wh MS Targets ,„A M ; ,, .... _ .,w C9-C18 Aliphatics ND mg/kg 6.94 1 __ _.. ._ ._ ........ .... C19-C36 Aliphatics 12.3 mg/kg 6.94 1 C11-C22 Aromatics ND mg/kg 6.94 1 C11-C22 Aromatics,Adjusted ND mg/kg 6.94 1 _ .. ... .. .......... _....... _ _ __.. Naphthalene ND mg/kg 0.028 1 2-Methylnaphthalene ND mg/kg 0.028 1 Acenaphthylene ND mg/kg 0.028 1 Acenaphthene ND mg/kg 0.028 1 Fluorene ND mg/kg 0.028 1 Phenanthrene ND mg/kg 0.028 1 Anthracene ND mg/kg 0.028 1 ..... __......_... __. . .._...... . Fluoranthene 0.055 mg/kg 0.028 1 -_I...__ ......_... .._... .__...... .. ....... ..__...__..._ .. _...._...._................ .._ .._. ....._. Pyrene 0.042 mg/kg 0.028 1 Benzo(a)anthracene ND mg/kg 0.028 1 _..._ ................. _.. . ........_... ..._. .. ........._. _ _ ........._.. ........ ...................... _ ....._.. Chrysene ND mg/kg 0.028 1 Benzo(b)fluoranthene ND mg/kg 0.028 1 Benzo(k)fluoranthene ND mg/kg 0.028 1 _..__..__.. _. ......_..... _.._. Benzo(a)pyrene ND mg/kg 0.028 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.028 1 ..............................._...._.... .........-. ......... _ . Dibenzo(a,h)anthracene ND mg/kg 0.028 1 Benzo(ghi)perylene ND mg/kg 0.028 1......_. _._. ............... .... ..... . ... ........... _...._...... ......... L -PHA Page 18 of 117 04280820:22 i ' Project Name: CAVES PASTURE/SCUDDERS LN: Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-06 Date Collected: 04/17/08 09:30 Client ID: BG-1CP Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA' Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH wlthMS Targets � �" . ....w..,.........�. ........-_........:......«.«.mil/.r.,,.,,..,,...«...it,.9. .R� �e r...,u.., ........rv.... Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 73 40-140 o-Terphenyl 88 40-140 2-Fluorobiphenyl 91 40-140 2-Bromonaphthalene 88 40-140 O-Terphenyl-MS 87 40-140 AI 'YI i"A Page 19 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 ` Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-07 Date Collected: 04/17/08 14:00 Client ID: BG-2SHEP Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 14:00 Analyst: AJ Percent Solids: 87% ', Q " Quality C a ontrol.1 fn ormtron Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method "Tr Parameter Result Qualifier Units RDL Dilution Factor EPA wtthMS targets .a�. . ..... , ,_ ., C9-Cl8 Aliphatics ND mg/kg 7.66 1 C19-C36 Aliphatics ND mg/kg 7.66 1 .. ... _ ..... C11-C22 Aromatics ND mg/kg 7.66 1 ._.. ..... _ .......__.. C11-C22 Aromatics,Adjusted ND mg/kg 7.66 1 Naphthalene ND mg/kg 0.031 1 2-Methylnaphthalene ND mg/kg 0.031 1 Acenaphthylene ND mg/kg 0.031 1 _ _...._. Acenaphthene ND mg/kg 0.031 1 Fluorene ND mg/kg 0.031 1 Phenanthrene ND mg/kg 0.031 1 _.... ._.. __..... ......._.... .........._. Anthracene ND mg/kg 0.031 1 ......... .... Fluoranthene ND mg/kg 0.031 1 __...... ........... ......-- ....__...... .._ ...._...... .............. ......... Pyrene ND mg/kg 0.031 1 Benzo(a)anthracene ND mg/kg 0.031 1 ........ .....___.. __..... ......... ........ ................... ,, ......_... .............. __..... Chrysene ND mg/kg 0.031 1 Benzo(b)fluoranthene ND mg/kg 0.031 1 ..... _ _.... _......... _.. Benzo(k)fluoranthene ND mg/kg 0.031 1 Benzo(a)pyrene ND mg/kg 0.031 1 ......_ .. __ ._........ Indeno(1,2,3cd)Pyrene ND mg/kg 0.031 1 .......... ---....I........... _ ........ ........ ... .__. ........ ..._ ......... .__ .............. _ .. ...................._ ...._.... Dibenzo(a,h)anthracene ND mg/kg 0.031 1 Benzo(ghi)perylene ND mg/kg 0.031 1 ........ ...._ __.. .. ........- Page 20 of 117 i 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: LO8O5612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: LO8O5612-07 Date Collected: 04/17/08 14:00 Client ID: BG-2SHEP Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH wlth�MS Ta gets _ K "a" Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 58 40-140 o-Terphenyl 72 40-140 2-Fluorobiphenyl 77 40-140 2-Bromonaphthalene 73 s 40-140 O-Terphenyl-MS 83 40-140 Page 21 of 117 04280820:22 r Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 ' Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-08 Date Collected: 04/17/08 15:00 Client ID: MH-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 13:30 Analyst: AJ Percent Solids: 88% z �C t5 : emu- �. Quaitty ontroi lnformatton M. .... .`` ..., . .F a .. Wk ,...,... Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method - Parameter Result Qualifier Units RDL Dilution Factor C9-C18Aliphatics ND mg/kg 7.58 1 ..... ...._.__.._ _._ . . _..... . ....... C19-C36 Aliphatics ND mg/kg 7.58 1 C11-C22 Aromatics ND mg/kg 7.58 1 C11-C22 Aromatics,Adjusted ND mg/kg 7.58 1 Naphthalene ND mg/kg 0.030 1 2-Methylnaphthalene ND mg/kg 0.030 1 Acenaphthylene ND mg/kg 0.030 1 _ ......_.._-- ......1.... Acenaphthene ND mg/kg 0.030 1 Fluorene ND mg/kg 0.030 1 _.._ ........... _ Phenanthrene ND mg/kg 0.030 1 Anthracene ND mg/kg 0.030 1 ......................_-.. Fluoranthene ND mg/kg 0.030 1 ...... ....... ..__... ._..... - ....... ....__...... ...... .. _ .........__.. ..... Pyrene ND mg/kg 0.030 1 Benzo(a)anthracene ND mg/kg 0.030 1 ......... _ _.......... ... .... ..._...... __ ............ __........ ......._..._ .... ............. _.._. Chrysene ND mg/kg 0.030 1 Benzo(b)fluoranthene ND mg/kg 0.030 1 _. . Benzo(k)fluoranthene ND mg/kg 0.030 1 ..... .............. _ _..... __..... _...._.._.. Benzo(a)pyrene ND mg/kg 0.030 1 _....__.. .......... _........ ........... Indeno(1,2,3-cd)Pyrene ND mg/kg 0- ........... __......... Dibenzo(a,h)anthracene ND mg/kg 0.030 1 Benzo(ghi)perylene ND mg/kg 0.030 1 _.._._. ...._-_... _..... ......__ _....._.._. _...__ _.... Page 22 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-08 Date Collected: 04/17/08 15:00 Client ID: MH-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane B6 40-140 o-Terphenyl 75 40-140 2-Fluorobiphenyl 86 40-140 2-Bromonaphthalene 83 40-140 O-Terphenyl-MS 79 40-140 Eirl Page 23 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 r ' Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-09 Date Collected: 04/17/08 14:05 Client ID: SW-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Water Extraction Method: EPA 3510C Analytical Method: 61,EPH-04-1 Extraction Date: 04/22/08 08:30 Analytical Date: 04/23/08 20:48 Analyst: AJ �� QiaalltyControl Information _ . � . Condition of sample received: Satisfactory Aqueous Preservative: Laboratory Provided Preserved Container Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method OR Parameter Result Qualifier Units RDL Dilution Factor EPHwith INS gets T�im�Yx C9-Cl8 Aliphatics ND ug/I 100 1. ... C19-C36 Aliphatics ND ug/I 100 1 _ _ _......._ _ ......... .._. _ C11-C22 Aromatics ND ug/I 100 1 ............ ... ....... ._......_... __..__.... ......... C11-C22 Aromatics,Adjusted ND ug/I 100 1 Naphthalene ND ug/I 0.400 1 .._. .........I..._ _- .......... ..._ ........ _......... _........ _.. _.....__.. _............ ....._.._._......... 2-Methylnaphthalene ND ug/I 0.400 1 Acenaphthylene ND ug/I 0.400 1 _._ ........_.... _..._._ _. .......... Acenaphthene ND ug/I 0.400 1 _._.. - .._. .......... _._._. Fluorene !ND ug/I 0.400 1 1 ..-.-__ _ _.... _... ........ ........... Phenanthrene ND ug/I 0.400 1 _. .._- ..._ .__ ..._....... ._.. ........... __...... .. _................. Anthracene ND ug/I 0.400 1 Fluoranthene ND ug/I 0.400 1 .- _ ......... _............. ........._._ _......__.. _. _... Pyrene ND ug/I 0.400 1 Benzo(a)anthracene ND ug/I 0.400 1 _.... .. ....... .. ... ......... _. .... ............... ....................._.._...................._...__. . ......... _.. ......... .......... Chrysene ND ug/I 0.400 1 _. ... Benzo(b)fluoranthene ND ug/I 0.400 1 .._.. ..... ...... _.. _ Benzo(k)fluoranthene ND ug/I 0.400 1 Benzo(a)pyrene ND ug/I 0.200 1 Indeno(1,2,3-cd)Pyrene ND ug/I 0.400 1 _. ....... _. _........ _ ........... Dibenzo(a,h)anthracene ND ug/I 0.400 1 Benzo(ghi)perylene ND ug/I 0.400 1 ..................._....._....... .__. ........... __.. _........_ ...__....._ )V ESA Page 24 of 117 04280820:22 ` Project Name: CAVES PASTURE/SCUDDERS LN. tab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-09 Date Collected: 04/17/08 14:05 Client ID: SW-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH with'MS Targets _ ,r__ „" Acceptance Surrogate %,Recovery Qualifier Criteria Chloro-Octadecane 65 40-140 o-Terphenyl 79 40-140 2-Fluorobiphenyl 88 40-140 2-Bromonaphthalene 85 40-140 O-Terphenyl-MS 87 40-140 };A Page 25 of 117 04280820:22 ' r Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 ` Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-10 Date Collected: 04/17/08 14:30 Client ID: SED/WL-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 14:36 Analyst: AJ Percent Solids: 37% F� Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Rill Parameter Result Qualifier Units RDL Dilution Factor EPH�with C9-C18 Aliphatics ND mg/kg 18.0 1 C19-C36 Aliphatics ND mg/kg mg/kg 18.0 1 C11-C22 Aromatics ND mg/kg 18.0 1 C11-C22 Aromatics,Adjusted ND mg/kg 18.0 1 Naphthalene ND mg/kg 0.072 1 _.... _..... __ _ ...._...... 2-Methylnaphthalene ND mg/kg 0.072 1 Acenaphthylene ND mg/kg 0.072 1 _. ... ......... Acenaphthene ND mg/kg 0.072 1 Fluorene ND mg/kg 0.072 1 ......... ... ............ Phenanthrene ND mg/kg 0.072 1 ......... __ _ . .......... Anthracene ND mg/kg 0.072 1 _. _ Fluoranthene ND mg/kg 0.072 1 ........11 1--_._.... ..._ ...... __..... ...... _-............... __....................... __. ......... Pyrene ND mg/kg 0.072 1 Benzo(a)anthracene ND mg/kg 0.072 1 _._ .. . ........ _ _. .._...._.. _...__. __. .,....... Chrysene ND mg/kg 0.072 1 Benzo(b)fluoranthene ND mg/kg 0.072 1 ... _... ............. Benzo(k)fluoranthene ND mg/kg 0.072 1 ....................... _........................_........_ ........_.... _.. Benzo(a)pyrene ND mg/kg 0. _. Indeno(1,2,3-cd)Pyrene ND mg/kg 0.072 1__..... ..........__...._. . __....... ._... . ............. Dibenzo(a,h)anthracene ND mg/kg 0.072 1 Benzo(ghi)perylene ND mg/kg 0.072 1 ........... _.._. ........ .__..........._ ._ .......- _..... . .. ......... _....... _....__........ Acz HA Page 26 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-10 Date Collected: 04/17/08 14:30 Client ID: SED/WL-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor IEP"with MS Targets x 3„ .,. Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 23 40-140 o-Terphenyl 32 40-140 2-Fluorobiphenyl 76 40-140 2-Bromonaphthalene 73 40-140 O-Terphenyl-MS gg 40-140 - I 2A HA Page 27 of 117 a 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-10 RE Date Collected: 04/17/08 14:30 Client ID: SED/WL-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: Extraction Date: 04/25/08 11:30 � 61 EPH-04-1 Analytical Date: 04/28/08 12:17 Analyst: AJ Percent Solids: 37% Mw mx � 477777-11 �. . .,., .,.. Quality Controlnfarmattonfi Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method v.o Parameter Result Qualifier Units RDL Dilution Factor MAN -7 EP�H tFi.MS Targets C9-Cl8 Aliphatics ND mg/kg 18.0 1 _,...... _.._ ....--__ C19-C36 Aliphatics ND mg/kg 18.0 1 C11-C22 Aromatics 23.0 mg/kg 18.0 1 _. ........ __ _ .......... . C11-C22 Aromatics,Adjusted 23.0 nI 18.0 1 Naphthalene ND mg/kg 0.072 1 _._ _ __.......... _....__.. _. __.. ......__ 2-Methylnaphthalene ND mg/kg 0.072 1 Acenaphthylene ND nI 0.072 1 __- ._........... ...... .__....... _.. ..... _. ...... Acenaphthene ND nI 0.072 1 Fluorene ND mg/kg 0.072 1 ......_ _.__.._. ......... _..... ........__ _... ..........._ Phenanthrene ND mg/kg 0.072 1 .. ._..._ _... Anthracene ND nI 0.072 1 Fluoranthene ND mg/kg 0.072 1 ........ ........ ..._......_. _ ._ ...._..... ....__...._... ............._ ..... _..................... _...,...... Pyrene ND mg/kg 0.072 1 Benzo(a)anthracene ND nI 0.072 1......... _...... ......-I......__I ........ Chrysene ND mg/kg 0.072 1 Benzo(b)fluoranthene IND mg/kg 0.072 1 ............. .. .......... _ Benzo(k)fluoranthene ND nI 0.072 1 ......... .._ _. Benzo(a)pyrene ND mg/kg -0.072 __...._ _....__.... _....... _ ....__..... _.......... . Indeno(1,2,3-cd)Pyrene ND mg/kg 0.072 1 .__....._ ....._..- .._. .......... .__.................. .......... ........... ... ............. _...__..... ...................... Dibenzo(a,h)anthracene ND mg/kg 0.072 1 Benzo(ghi)perylene ND mg/kg 0.072 1 . .......... _........ ........ ..._ Page 28 of 117 ` 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: LO8O5612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-10 RE Date Collected: 04/17/08 14:30 Client ID: SED/WL-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPIi with MS Targ .. ,.. .., .. Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 30 40-140 o-Terphenyl 39 40-140 2-Fluorobiphenyl 92 40-140 2-Bromonaphthalene 91 40-140 O-Terphenyl-MS 47 40-140 Q F� �irt Page 29 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 ` Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-11 Date Collected: 04/17/08 14:10 Client ID: WL-2 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 12:58 Analyst: AJ Percent Solids: 77% Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method VM i ., Parameter Result Qualifier Units RDL Dilution Factor C9-Cl8 Aliphatics 25.6 mg/kg 8.66 1 C19-C36 Aliphatics 19.3 mg/kg 8.66 1 .......... __._ .... .....-..... _ ..._.... C11-C22 Aromatics 37.9 mg/kg 8.66 1 C11-C22 Aromatics,Adjusted 37.9 mg/kg 8.66 1 Naphthalene ND mg/kg 0.035 1 2-Methylnaphthalene ND mg/kg 0.035 1 Acenaphthylene ND mg/kg 0.035 _�.._... Acenaphthene ND mg/kg 0.035 1 Fluorene ND mg/kg 0.035 1 ........ _._.... _ _.. Phenanthrene ND mg/kg 0.035 1 Anthracene ND mg/kg 0.035 1 ....... _...__._ _...... _.....:...... __..._ Fluoranthene ND mg/kg 0.035 .. 1 _...... .. ........... __. ...._....._.. ....._..__.. ...._.. ...__ .. .........._ .........__...._....... Pyrene ND mg/kg 0.035 1 Benzo(a)anthracene ND mg/kg 0.035 1 ...._. __ . ......._.. .. . ............ _.._ ....._..... Chrysene ND mg/kg 0.035 1 Benzo(b)fluoranthene ND mg/kg 0.035 1 Benzo(k)fluoranthene ND mg/kg 0.035 1 .... ._ ... _..... _.. ...... Benzo(a)pyrene ND mg/kg 0.035 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.035 1 ....... . _..-........ ................. ........... .........._ ...._..... ................ ... ..........._..._. ......__...- ................_.. ............ Dibenzo(a,h)anthracene ND mg/kg 0.035 1 Benzo(ghi)perylene ND mg/kg 0.0315 1 .. ... ......... . - ........ __ .......... Page 30 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-11 Date Collected: 04/17/08 14:10 Client ID: WL-2 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH withMS Ta"getsx ; Acceptance Surrogate %Recovery Qualifier criteria Chloro-Octadecane 45 40-140 o-Terphenyl 58 40-140 2-Fluorobiphenyl 77 40-140 2-Bromonaphthalene 107 40-140 O-Terphenyl-MS 58 40-140 Lll PHA Page 31 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-13 Date Collected: 04/17/08 14:50 Cl ient ID: WL/ROAD SHOULDER 4 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/25/08 16:26 Analyst: AJ Percent Solids: 71% 4u tyGontronform�atton a y .,., � Satisfactory Condition of sample received: Received on Ice Sample Temperature upon receipt: Extracted Per the Method Sample Extraction method: Parameter Result Qualifier Units RDL Dilution Factor EPH wtth,MS Targets F . ..�? Z- C9-C18 Aliphatics ND mg/kg._ 9.39 C19-C36 Alip hat ics 31.5 mg/kg 9.39 1 ..... C11-C22 Aromatics 17.7 mg/kg 9.39 C11-C22 Aromatics,Adjusted 17.4 mg/kg 9.39 Naphthalene ND mg/kg 0.038 1 2-Methyln 1.aph 1.1halene ND mg/kg 0.038 1 Acenaphthylene ND mg/kg 0.038 1 __..... Acenaphthene ND mg/kg 0.038 Fluorene ND mg/kg. ... 0.038 1 Ph1 1.enanthrene 0.057 mg/kg 0.038 1 Anthracene ND mg/kg 0.038 ...... Fluoranthene 0.110 mg/kg 0.03 Pyrene 0.077 mg/kg 0.0 38 Benzo(a)anthracene 0.044 mg/kg 0.038 1 __.. Chrysene 0.047 mg/kg 0.038 Benzo(b)fluoranthene 0.045 mg/kg 0.038 1 .... Benzo(k)fluoranthene ND mg/kg 0.03 .. _. Benzo(a)pyrene ND mg/kg „ 0.038 1 In deno(1,2,3-cd)Pyrene ND mg/kg 0.038 Dibenzo(a,h)anthracene ND mg/kg 0.038 Benzo(ghi)perylene ND mg/kg 0.038 11.11.11 __.... ......._.. z WAL Page 32 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-13 Date Collected: 04/17/08 14:50 Client ID: WL/ROAD SHOULDER 4 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 64 40-140 o-Terphenyl 65 40-140 2-Fluorobiphenyl 79 40-140 2-Bromonaphthalene 78 40-140 O-Terphenyl-MS 68 40-140 p3�Eie'l Page 33 of 117 04280820:22 V Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-14 Date Collected: 04/17/08 15:10 Client ID: WL-5 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/25/08 11:30 Analytical Date: 04/28/08 12:49 Analyst: RT Percent Solids: 77% Info attvn—17 M Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor EPH with MS Targets A H C9-Cl8 Aliphatics ND mg/kg 8.6 11 6 1 C19-C36 Aliphatics ND mg/kg 8.66 1 _...._.._ ......... C11-C22 Aromatics ND mg/k9 8.66 1 C11-C22 Aromatics,Adjusted ND mg/kg 8.66 1 Naphthale I.ne ND mg/kg 0.035 1 ..... _.. 2-Methyinaphthalene ND mg/kg 0.035 1 Acenaphthylene ND mg/kg 0.035 1 Acenaphthene ND mg/kg 0.035 1 Fluorene ND mg/kg 0.0 1.35 1 _.......... 1. Phenanthrene ND mg/kg 0.035 Anthracene ND mg/kg 0.035 1 __.... ........ ..............._.............._ ........._ _...._..........._. m ND mg/kg 0.035 1 Fluoranthene 9 Pyrene ND mg/kg 0.035 1 Benzo(a)anthracene ND mg/kg 0.035 1 _.... _. ........... .. .....__..._ __. .... ..... ..........__........__ Chrysene ND mg/kg 0.035 Benzo(b)Fluoranthene ND mg 1./kg 0.035 1 Benzo(k)Fluo rant hene ND mg/kg 0.035 Benzo(a 1.)pyrene ND mg/kg 0.035 1 .... Indeno(1,2,3-cd)Pyrene ND mg/kg 0.035 Dibenzo(a,h)anthracene ND mg/kg 0.035 Benzo(ghi)perylene ND mg/kg 0.0 1.35 1 _._.. _..... .......... 1 ?Eir1 Page 34 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-14 Date Collected: 04/17/08 15:10 Client ID: WL-5 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH with MS aT getsf� ..; Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 42 40-140 o-Terphenyl 40 40-140 2-Fluorobiphenyl 82 40-140 2-Bromonaphthalene 79 40-140 O-Terphenyl-MS 54 40-140 Page 35 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-15 Date Collected: 04/17/08 14:45 Client ID: B-23 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 , Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/25/08 11:51 Analyst: AJ Percent Solids: 94% ... , _ .f w...Qualtty�C.ontrol Information .._... _. E , y., ..... .a... . Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor EPith MS Targets' t 3 C9-Cl8 Aliphatics ND mg/kg 35.5 5 ......... C19-C36 Aliphatics 116 mg/kg 35.5 5 _ .......... .......... _......_. C11-C22 Aromatics 83.3 mg/kg 35.5 5 C11-C22 Aromatics,Adjusted 83.3 mg/kg 35.5 5 _... _. ...... Naphthalene ND mg/kg 0.284 10 ........... ... ..... ...... 2-Methylnaphthalene ND mg/kg 0.284 10 Acenaphthylene ND mg/kg 0.284 10 Acenaphthene ND mg/kg 0.284 10 Fluorene ND mg/kg 0.284 10 __....... __.. ...... _. Phenanthrene ND mg/kg 0.284 10 _.............. .... ...... .. ....__..... __...__.... Anthracene ND mg/kg 0.284 10 Fluoranthene ND mg/kg 0.284 10 . . ..__............... ........ ...... . ............ .......... ..........._ .............__. ................................ Pyrene ND mg/kg 0.284 10 Benzo(a)anthracene ND mg/kg 0.284 10 __... ..... ... .... . ........ .........._ Chrysene ND mg/kg 0.284 10 Benzo(b)fluoranthene ND mg/kg 0.2841. 10 . _I......... ....... ............ Benzo(k)fluoranthene ND mg/kg 0.284 10 ......... .... _..._. Benzo(a)pyrene ND mg/kg 0.284 10 ._. I 1 11-............ .................... _... Indeno(1,2,3-cd)Pyrene ND mg/kg 0.284 10 ........ ........ _................ ........ Dibenzo(a,h)anthracene ND mg/kg 0.284 10 Benzo(ghi)perylene ND mglkg 10 __... ......... ....._... .........._ _.__..._ ......... ..0.284.. _. ._.__.._ _............_ .... _. E•;A Page 36 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-15 Date Collected: 04/17/08 14:45 Client ID: B-23 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Mr EPH with MSTargets Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 82 40-140 o-Terphenyl 91 40-140 2-Fluorobiphenyl 77 40-140 2-Bromonaphthalene 80 40-140 O-Terphenyl-MS 117 40-140 L�HA Page 37 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-16 Date Collected: 04/17/08 14:55 Client ID: B-24 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/25/08 12:56 Analyst: AJ Percent Solids: 90% e_ � Quaitt Control Information ., Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor EPH withMS' Targets C9-Cl8 Aliphatics ND mg/kg 37.0 5 C19-C36 Aliphatics 145 mg/kg 37.0 5 C11 C22 Aromatics 40.0 mg/kg 37.0 5 C11-C22 Aromatics,Adjusted 40.0 mg/kg 37.0 5 Naphthalene ND mg/kg 0..148 5 2-Methylnaphthalene ND mg/kg 0.148 5 Acenaphthylene ND mg/kg 0.148 5 Acenaphthene ND mg/kg 0.148 5 Fluorene ND mg/kg 0.148 5 _. __...._ . _ Phenanthrene ND mg/kg 0.148 5 Anthracene ND mg/kg 0.148 1.5 __...._ Fluoranthene ND mg/kg 0.148 5 _... ......__... . ._............ ...... ............. ............................... Pyrene ND mg/kg 0.148 5 Benzo(a)anthracene ND mg/kg 0.148 5 ........... Chrysene ND mg/kg 0.148 Benzo(b)fluoranthene ND mg/kg 0.148 5 Benzo(k)fluoranthene ND mg/kg 0.148 5 .......... ........ _..... _._ _.._..._._ Benzo(a)pyrene ND mg/kg 0.148 Indeno(1,2,3-cd)Pyrene ND mg/kg0.148 .....__ .....__ Dibenzo(a,h)anthracene ND mg/kg 0.148 5 Benzo(ghi)perylene ND mg/kg 0.148 5 _.... ..... ............._. �14 HA Page 38 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: LO8O5612 .Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: LO8O5612-16 Date Collected: 04/17/08 14:55 Client ID: B-24 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH'With'MS Targets ,z, y �� �3 g Acceptance Surrogate %Recovery. Qualifier Criteria Chloro-Octadecane 89 40-140 o-Terphenyl 103 40-140 2-Fluorobiphenyl 91 40-140 2-Bromonaphthalene 89 40-140 O-Terphenyl-MS 98 40-140 LZt 2HA Page 39 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-17 Date Collected: 04/18/08 08:50 Client ID: SW BACK HINCK Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Water Extraction Method: EPA 3510C Analytical Method: 61,EPH-04-1 Extraction Date: 04/22/08 08:30 Analytical Date: 04/23/08 17:04 Analyst: AJ �„ Qualtty�Control Information� „ � >- � �� Condition of sample receroed: Satisfactory Aqueous Preservative: Laboratory Provided Preserved Container Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor EP wlth MST iJ6O'ts C9-Cl8 Aliphatics ND ug/I 101 1 C19-C36 Aliphatics ND ug/I 11 101 1 __._........ C11-C22 Aromatics ND ug/I 101 1 ......... _................. _ ........ _... ..... ................... C11-C22 Aromatics,Adjusted ND ug/1 101 1 Naphthalene ND ug/I 0.404 1 2-Methylnaphthalene ND ug/I 0.404 1 Acenaphthylene ND ug/I 0.404 1 Acenaphthene ND ug/I 0.404 1 Fluorene ND ug/I 0.404 1 Phenanthrene 0.488 ug/I 0.404 1 ... ... . ......... __ _.......... Anthracene ND ug/I 0.404 1 Fluoranthene 1.18 ug/I 0.404 1 ... . ..... _.. Pyrene 0.838 ug/I 0.404 1 Senzo(a)anthracene 0.417 11111 ugll 0.4 1.04 1 Chrysene 0.564 ug/I 0.404 1 _.. Be nzo(b)fluoranthene 0.522 ug/I 0.404 ......... __......... Benzo(k)fluoranthene ND ug/I 0.404 1 Benzo(a)pyrene 0.405 ug/I 0.200 1 Indeno(1,2,3-cd)Pyrene ND ug/I 0.404 1 Dibenzo(a,h)anthracene ND ug/I 0.404 1 Benzo(ghi)perylene ND ug/I 0.404 1 ? Page 40 of 117 f 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-17 Date Collected: 04/18/08 08:50 Client ID: SW BACK HINCK Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH tf MS Targets FMOW Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 74 40-140 o-Terphenyl 96 40-140 2-Fluorobiphenyl 92 40-140 2-Bromonaphthalene 91 40-140 O-Terphenyl-MS 93 40-140 WA Page 41 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-18 Date Collected: 04/18/08 08:50 Client ID: SED BACK HINCK Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 15:07 Analyst: AJ Percent Solids: 54% a Condition of sample received: �.... - .M.� °ry Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor EP,H wth AAS Targets �A.._. _ ... .... C9-C18 Aliphatics ND mg/kg 12.3 1 C19-C36 Aliphatics 21.7 mg/kg 12.3 C11-C22 Aromatics 43.3 mglkg 12.3 1. C11-C22 Aromatics,Adjuste11 d 32.2 mg/kg 12.3 1 .......... Naphthalene 0.063 mg/kg 0.049 1 2-Methylna 1.phth ale ne ND mg/kg 0.049 1 Acenaphthylene 0.056 mg/kg 0.049 1 .. _.,. Acenaphthene 0.050 mg/kg 0.049 Fluorene 0.125 mg/kg 0.049 1 Phenanthrene 1.83 mg/kg 0.049 Anthracene 0.192 mg/kg 0.049 Fluoranthene 2.67 mg/kg 0.049 1 Pyrene 1.71 mg/kg 0.049 Benzo(a)anthracene 0.864 mg/kg 0.049 1 .. ..._ .... _ ....... .................. Chrysene 0.823 mg/kg 0.049 1 Benzo(b)fluoranthene 0.562 mg/kg 0.11 049 1 Benzo(1.k)fluoranthene 0.695 mg/kg 0.049 ... Benzo(a)pyrene 0.610 mg/kg 0.049 1 Indeno(1,2,3-cd)Pyrene 0.360 mg/kg 0.049 1 .......... Dibenzo(a,h)anthracene 0.103 mg/kg 0.049 Benzo(ghi)perylene 0.368 mg/kg 0.049 1 Eirl Page 42 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-18 Date Collected: 04/18/08 08:50 Client ID: SED BACK HINCK Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EP.H wtth',MSyTargets ' Acceptance,,,.::..., Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 60 40-140 ! o-Terphenyl 74 40-140 2-Fluorobiphenyl 80 40-140 2-Bromonaphthalene 79 40-140 O-Terphenyl-MS 73 40-140 L.l�?iie� z Page 43 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 ' Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-19 Date Collected: 04/18/08 09:15 Client ID: SW BARN HARBOR Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Water Extraction Method: EPA 3510C Analytical Method: 61,EPH-04-1 Extraction Date: 04/22/08 08:30 Analytical Date: 04/23/08 16:31 Analyst: AJ w Quality Con�troll form ton m` „ Condition of sample received: Satisfactory Aqueous Preservative: Laboratory Provided Preserved Container Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method �c71 Parameter Result Qualifier Units RDL Dilution Factor EPH with) Targets C9-C18 Aliphatics ND ug/I 102 1 _ ._. ....._... _ __.... ......... C19-C36 Aliphatics ND ug/I 102 1 ........ _ _. _ _ ..... ............... _ C11-C22 Aromatics ND ug/I 102 1 _.... ... ........... _ ......... _ .. .__.... _..... .. ............. ......... __ ............ C11-C22 Aromatics,Adjusted ND ug/I 102 1 Naphthalene ND ug/I 0.408 1 _.... _....__ ..._.....__........... ....... 2-Methylnaphthalene ND ug/I 0.408 1 Acenaphthylene ND ug/I 0.408 1 Acenaphthene ND ug/I 0.408 1 _........ __..... ........ Fluorene ND ug/I 0.408 1 Phenanthrene ND ug/I 0.408 1 ._ .......... ......... ....... _............ __. _...... _ _............. Anthracene ND ug/I 0.408 1 Fluoranthene ND ug/I 0.408 1 ......__... ._......... .... _ .............. Pyrene ND ug/I 0.408 1 Benzo(a)anthracene ND ug/I 0.408 1 .......... Chrysene ND ug/I 0.4 11 08 1 Benzo(b)fluoranthene ND ug/I 0.408 1 Benzo(k)fluoranthene ND ug/I 0.408 1 __.... ..... Benzo(a)pyrene ND ug/1 0.202 1 Indeno(1 2,3-cd)Pyrene ND ug/I 0.408 1 ............ ..... _...._.. Dibenzo(a,h)anthracene ND ug/I 0.408 1 Benzo(ghi)perylene ND u9/�.........._.. 0.408 . .............. Page 44 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-19 Date Collected: 04/18/08 09:15 Client ID: SW BARN HARBOR Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH with MSj,a-gets `, fq ,x � � �� Acceptance Surrogate %Recovery Qualifier Criteria i Chloro-Octadecane 72 40-140 o-Terphenyl 88 40-140 2-Fluorobiphenyl 98 40-140 2-Bromonaphthalene 97 40-140 O-Terphenyl-MS 81 40-140 l Page 45 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 ' SAMPLE RESULTS Lab ID: L0805612-20 Date Collected: 04/18/08 09:15 Client ID: SED BARN HARBOR Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: . Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 15:12 Analyst: AJ Percent Solids: 81% Quality Control Information Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method .....w Paramet er Result Qualifier Units RDL Dilution Factor EPH withMS Targets` " NMI- _, .. C9-C18 Aliphatics ND mg/kg 8.23 1 C19-C36 Aliphatics ND mg/kg 8.23 1 C11-C22 Aromatics ND mg/kg 8.23 1 C11-C22 Aromatics,Adjusted ND mg/kg 8.23 1 Naphthalene ND mg/kg 0.0 1.3 11 3 1 2-Methylnaphthalene ND mg/kg 0.033 1 Acenaphthylene ND mg/kg 0.033 1 Acenaphthene ND mg/kg 0.033 1 Fluorene ND mg/kg 0.033 1 ....... _.... _..__..... ....._ Phenanthrene ND mg/kg 0.033 1 _.._.. Anthracene ND mg/kg 0.033 1 .........- _._ .........-_. _ ........ Fluoranthene ND mg/kg 0.033 1 ......._. .... ... ............ .. .......... _ .........._ -_... Pyrene ND mg/kg 0.033 1 Benzo(a)anthracene ND mg/kg 0.033 1 Chrysene ND mg/kg 0.033 1 Benzo(b)fluoranthene ND mg/kg 0.033 1 Benzo(k)fluoranthene ND mg/kg 0.033 1 _. Benzo(a)pyrene ND mg/kg 0.033 1 Indeno(1,2,3-cd)Pyrene ND mg/kg 0.033 . .......... Dibenzo(a,h)anthracene ND mg/kg 0.033 1 Benzo(ghi)perylene ND mg/kg 0.033 1 .......... . .... ........._......... HiA Page 46 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-20 Date Collected: 04/18/08 09:15 Client ID: SED BARN HARBOR Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor _,•% Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 53 40-140 o-Terphenyl 86 40-140 2-Fluorobiphenyl 82 40-140 2-Bromonaphthalene 78 40-140 O-Terphenyl-MS 76 40-140 Page 47 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-21 Date Collected: 04/18/08 08:20 Client ID: B-32 2656 RTE 6A Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 17:50 Analyst: AJ Percent Solids: 77% QualityControllnform'atfon 4 Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method �.�. .,...... �„,,,,,,,..�tt „c,,�„,:.. %. �,��;,� .. .»K ».�+�.,�e��....,w..,_�, ;..�.-....... .tea _�.suu�,'�.. ,�Za._..,�:�➢a w�.a.. ,.,,..�� ,,,,,,,,,,,, ,, Parameter Result Qualifier Units RDL Dilution Factor EI?H With MS Targets :'' �� 77 t. a s... .... :.. ` :' . _. ,. C9-Cl8 Aliphatics ND mg/kg 43.3 5 C19-C36 Aliphatics 65.5 mg/kg 43.3 5 _.. _._ C11-C22 Aromatics 54.0 mg/kg 43.3 5 _...__.._ ._... __._. . C11-C22 Aromatics,Adjusted 51.2 mg/kg 43.3 5 Naphthalene ND mg/kg 0.173 5 2-Methylnaphthalene ND mg/kg 0.173 5 Acenaphthylene ND mg/kg 0.173 5 _. .- ....... _......._. ........--_.. _.._. Acenaphthene ND mg/kg 0.173 5 Fluorene ND mg/kg 0.173 5 _ ... _. ._. Phenanthrene 0.221 mg/kg 0.173 5 Anthracene ND mg/kg 0.173 5 ........ Fluoranthene 0.592 mg/kg 0.173 5 _..._........ .........__ .. ......... ...... .............. ................. ........ Pyrene 0.446 mg/kg 0.173 5 Benzo(a)anthracene 0.268 mg/kg 0.173 5 ....... _... Chrysene 0.304 mg/kg 0.173 5 Benzo(b)fluoranthene 0.321 mg/kg 0..173 5 ........ _.._. ......__.... _ __........ Benzo(k)fluoranthene 0.207 mg/kg 0.173 5 Benzo(a)pyrene 0.255 mg/kg 0.173 5 ......... _.. Indeno(1,2,3-cd)Pyrene ND mg/kg 0..173 5 ........__..... ........ .._......__ ........... Dibenzo(a,h)anthracene ND mg/kg 0.173 5 Benzo(ghi)perylene 0.196 mg/kg 0.173 5 .....__.. ............. I iA Page 48 of 117 ` 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-21 Date Collected: 04/18/08 08:20 Client ID: B-32 2656 RTE 6A Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor wh §Tar gets , . 00, EPH tt MS Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 84 40-140 o-Terphenyl 79 40-140 2-Fluorobiphenyl 78 40-140 2-Bromonaphthalene 76 40-140 O-Terphenyl-MS 82 40-140 I iA Page 49 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-22 Date Collected: 04/18/08 08:35 Client ID: BG 6A CB 2631 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/23/08 03:30 Analytical Date: 04/24/08 14:34 Analyst: AJ Percent Solids: 50% \ " �Qual�ty Contr'd14h ormatlo�n . . ..- _ ... , ...., µ.. ...v ,, Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method Parameter Result Qualifier Units RDL Dilution Factor �PFI with IBIS Targets - . . ...... ,.,.,.. ,w .._. _ - C9-Cl8 Aliphatics ND mg/kg 13.3 1 __.... .......... _._..... _ . ..... C19-C36 Aliphatics 59.6 mg/kg 13.3 1 C11-C22 Aromatics 34.5 mg/kg 13.3 1 C11-C22 Aromatics,Adjusted 34.4 mg/kg 13.3 1 Naphthalene ND mg/kg 0.053 1 2-Methylnaphthalene ND mg/kg 0.053 1 Acenaphthylene ND mg/kg 0.0 1.53 1 Acenaphthene ND mg/kg 0.053 1 Fluorene ND mg/kg 0.053 1 Phenanthrene ND mg/kg 0.053 1 ........ _ __ ..... Anthracene ND mg/kg 0.053 1 Fluoranthene 0.084 mg/kg 0.053 1 ......... .............._....._ ........ _. ._........................_- ........... .... Pyrene 0.073 mg/kg 0.053 1 Benzo(a)anthracene ND mg/kg 0.053 1 ...... .. Chrysene ND mg/kg 0.053 1 Benzo(b)fluoranthene ND mg/kg 0.0513 1 Benzo(k)fluoranthene ND mg/kg 0.053 1 ......... _. ..... Benzo(a)pyrene ND mg/kg 0.053 1 Indeno(1,2,3-cd)Pyrene ND _ mg/kg 0.053 .........-1".. ........... _.......... .. __ ............ ._. .............__ . ........_...__ .......-- Dibenzo(a,h)anthracene ND mg/kg 0.053 1 Benzo(ghi)perylene ND mg/kg 0.053 1 ........ _ _ ....... _ _..._......... ........... _...... Page 50 of 117 F. 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-22 Date Collected: 04/18/08 08:35 Client ID: BG 6A CB 2631 Date Received: .04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPH wtthMS Targets Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 56 40-140 o-Terphenyl 63 40-140 2-Fluorobiphenyl 79 40-140 2-Bromonaphthalene 77 40-140 O-Terphenyl-MS 72 40-140 Page 51 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-23 Date Collected: 04/18/08 08:40 Client ID: BG WL 2615 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Soil Extraction Method: EPA 3546 Analytical Method: 61,EPH-04-1 Extraction Date: 04/25/08 11:30 Analytical Date: 04/28/08 13:22 Analyst: RT Percent Solids: 73% Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method IQ Mw Parameter Result Qualifier Units RDL Dilution Factor C9-Cl8 Aliphatics ND mg/kg 45.7 5 C19-C36 Aliphatics 211 mg/kg 45.7 5 C11-C22 Aromatics 173 mg/kg 45.7 5 C11-C22 Aromatics,Adjusted 153 mg/kg 45.7 5 Naphthalene ND mg/kg 0.183 5 ......... _......_ ....... _.._.... __.._ _. 2-Methylnaphthalene ND mg/kg 0.183 5 Acenaphthylene ND mg/kg 0.183 5 _ ........ ......... __..__..._. . ..._..._..... ..__ _......... ..... ._..... _...__. _ ...... Acenaphthene ND mg/kg 0.183 5 Fluorene ND mg/kg 0.183 5 Phenanthrene 1.94 mg/kg 0.183 5 Anthracene 0.389 mg/kg 0.183 5 _ _......_ .....__.......... ....... .......... _ ............. . .......... Fluoranthene 3.49 mg/kg 0.183 5 Pyrene 2.56 mg/kg 0.183 5 Benzo(a)anthracene 1.44 mg/kg 0.183 5 ....._...... _..__....... _..._.......... Chrysene 1.90 mg/kg 0.183 5 Benzo(b)fluoranthene 1.78 mg/kg 0.183 5 ..._............. Benzo(k)fluoranthene 2.12 mg/kg 0.183 5 Benzo(a)pyrene 1.98 mg/kg 0.183 5 ....._..._ ._.._...... .........._. ......... _ __._.._... _ . ......... Indeno(1,2,3-cd)Pyrene 1.06 mg/kg 0.183 5 ........ ...... .._.._........ ............... ....__...__. ._.. _.,_ Dibenzo(a,h)anthracene 0.231 mg/kg 0.183 5 Benzo(ghi)perylene 1.32 mg/kg 0.183 5 .. .............. .... ..... _... ........_. _ _............ FOAL Page 52 of 117 I f 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: LO805612 Project Number: 14190101 Report Date: ' 04/28/08 SAMPLE RESULTS Lab ID: LO8O5612-23 Date Collected: 04/18/08 08:40 Client ID: BG WL 2615 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor EPHwith:MS Targets ' � d Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 74 40-140 o-Terphenyl 109 40-140 2-Fluorobiphenyl 104 40-140 2-Bromonaphthalene 100 40-140 O-Terphenyl-MS 56 40-140 III FOAL Page 53 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-24 Date Collected: 04/18/08 10:35 Client ID: RAW PRODUCT Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Matrix: Oil Extraction Method: EPA 3580A Analytical Method: 61,EPH-04-1 Extraction Date: 04/28/08 14:30 Analytical Date: 04/28/08 16:25 Analyst: RT Condition of sample received: Satisfactory Sample Temperature upon receipt: Received on Ice Sample Extraction method: Extracted Per the Method - �" Parameter Result Qualifier Units RDL Dilution Factor MS 'Targets EP:H with R .. _ � k C9-C18 Aliphatics 4390 mg/kg 1000 10 ...... ._..... __ ............ C19-C36 Aliphatics 716000 mg/kg 1000 10 C11-C22 Aromatics 52300 mg/kg 1000 10 C11-C22 Aromatics,Adjusted 51400 mg/kg 1000 10 ............ Naphthalene ND mg/kg 4.00 10 2-Methylnaphthalene ND mg/kg 4.00 10 Acenaphthylene ND mg/kg 4.00 10 ................ _ _._ ......... _...... ..... _.-_.. . Acenaphthene ND mg/kg 4.00 10 Fluorene ND mg/kg 4.00 10 Phenanthrene ND mg/kg 4.00 10 ......... _........... _......._. _._....... _ _ _...... _...__. Anthracene ND mg/kg 4.00 10 __ _ -_....... ..... - Fluoranthene ND mg/kg 4.00 10 _._.._ ...... _..._ ......... _.__...._ ..- Pyrene ND mg/kg 4.00 10 Benzo(a)anthracene ND mg/kg 4.010 10 .......... ........... ... __..._.. Chrysene ND mg/kg 4.00 10 Benzo(b)fluoranthene ND mg/kg 4.00 10 Benzo(k)fluoranthene ND mg/kg 4.00 10 __.....-.... ......... __. .... ...... Benzo(a)pyrene ND mg/kg 4.00 10 Indeno(1,2 ......................_ ......... .....__..__. ... ..... ... Dibenzo(a,h)anthracene ND mg/kg 4.00 10 Benzo(ghi)perylene ND mg/kg 4.00 10 ........-_. _ ...... _ _ _ - ........... ........ ..-......... KA Page 54 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-24 Date Collected: 04/18/08 10:35 Client ID: RAW PRODUCT Date Received: 04/21/08 Sample Location: WEST BARNSTABLE, MA Field Prep: Not Specified Parameter Result Qualifier Units RDL Dilution Factor Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 87 40-140 o-Terphenyl 104 40-140 2-Fluorobiphenyl 94 40-140 2-Bromonaphthalene 97 40-140 O-Terphenyl-MS 54 40-140 P• L1 ?HA Page 55 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 Method Blank Analysis Batch Quality Control Analytical Method: 61,EPH-04-1 Extraction Method: EPA 3510C Analytical Date: 04/23/08 12:39 Extraction Date: 04/22/08 08:30 Analyst: AJ Parameter Result Qualifier Units RDL P w..th �f. : tMS Targets, om e 31895O 1 .. . . . p C9-C18 Aliphatics ND ug/I 100 C19-C36 Aliphatics ND ug/I 100 ...... ... ......... ...... _......-... .._ C11-C22 Aromatics ND ug/I 100 C11-C22 Aromatics,Adjusted ND ug/I 100 Naphthalene ND ug/I 0.400 _ _ _...... .... _...... .,........ 2-Methylnaphthalene ND ug/l 0.400 1.111 Acenaphthylene ND ug/l 0400 ...__... .._ ......... Acenaphthene ND ug/I 0 400 Fluorene ND ug/I 0.400 Phenanthrene ND ug/l 0.400 ..__I . ......... _ ......... __. ........ ....._.._. __.... Anthracene ND ug/I 0.400 _.. _..._....... ....._.__.. ....... ...... Fluoranthene ND ug/I 0.400 _ ._......_.. _........_.... _.. _........ Pyrene ND ug/I 0.400 _......... ......... Benzo(a)anthracene ND ug/I 0 400 Chrysene ND ug/l 0.400 ..._....- ..... Benzo(k)fluoranthene ND111 ug/I 0.4.00 Benzo(a)pyrene ND .ug/1 . ._- 0.200 ... ... _ . ....._.... _....._ _. Indeno(1,2,3-cd)Pyrene ND ...... ....__.. .............._ Dibenzo(a,h)anthracene ND ug/l 0.400 Benzo(ghi)perylene ND ug/I 0.400 Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 71 40-140 o-Terphenyl 82 40-140 2-Fluorobiphenyl 88 40-140 2-Bromonaphthalene 85 40-140 O-Terphenyl-MS 84 40-140 'L, HA F � Page 56 of 117 f 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 Method Blank Analysis Batch Quality Control Analytical Method: 61,EPH-04-1 Extraction Method: EPA 3546 Analytical Date: 04/23/08 15:59 Extraction Date: 04/23/08 03:30 Analyst: AJ Parameter Result Qualifier Units RDL EPH with MSTargetsyforsample�s) 01-0810-11t13;15 16;182Q-22�Batch U1/G319119 1N ' =k. � ,.. . . � .. ..��= .:1 C9-C18 Aliphatics ND m................... ......._._.._ ..._..... C19-C36 Aliphatics ND mg/kg 6.67 .._... .. _...._...._ ......... C11-C22 Aromatics ND mg/kg 6.67 .... ._ _............ . _._.. .....__... .__...._.._...... _..._.... C11-C22 Aromatics,Adjusted ND mg/kg 6.67 _.. ... ..... _ ...._. _., ... .......... ...... -, .........__. .__..__. Naphthalene ND mg/kg 0.027 _ _ ....................._... _..... _ ... ..._._..... ..__..._....... _ .. ._ _ _...... ...._ _........... ._ - 2 Methylnaphthalene ND mg/kg 0.027 _..._...... .... __._..__ . ..... . ........ ..._..... ._.. _ .......... Acenaphthylene ND mg/kg 0.027 ..... Acenaphthene _ ND mg/kg 0.027 _ __ . ... ...... ......... ... _...... . .........__...__.._.... Fluorene ND mg/kg 0.027 ............ ............... ................ _........ Phenanthrene „_ ._....._ ___.. .. .. ND_..__. .. ._.._...._ mg/kg .....__. .0...0.2.7.......... ........ --_ .._..... _... Anthracene ND mg/kg 0.027 __.... . ...._...._., ............, Fluoranthene ND mg/kg 0.027 ....... .. .............. - .._..... _....... ........... _....._... .... ......_..... ..._....... Pyrene ND mg/kg 0.027 ...._.... _. .. .... ....... .._ .._ .... ....... _....._.... . ....... ..... Benzo(a)anthracene ND mg/kg 0.027 _...- _.._.._ _ _.......... ......... Chrysene_.__..... ..... ......... D mg/kg 0.02_7....... ..... ...... _.._.. . .. . __ . Benzo(b)fluoranthene ND mg/kg 0.027 _._ .. .......... .. Benzo(k)fluoranthene IN mg/kg 0.027 _. ......_.. - -._.. ...... . _.___......... Benzo(a)pyrene ND mg/kg 0.027 _... _._ ......... _ ..............__. _.. ..... ............ Indeno(1 2 3-cd)Pyrene ND mg/kg ....... 0.027 _._ ...._-. _..... .......... ..:.......... . _.._.._...__ ........ Dibenzo(a,h)anthracene ND m .. ....... ..... .._....._ Benzo(ghi)perylene ND mg/kg 0.027 Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 63 40-140 o-Terphenyl 82 40-140 2-Fluorobiphenyl 92 40-140 2-Bromonaphthalene 90 40-140 O-Terphenyl-MS 83 40-140 L1t�F+A Page 57 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: LO805612 Project Number: 14190101 Report Date: 04/28/08 Method Blank Analysis Batch Quality Control Analytical Method: 61,EPH-04-1 Extraction Method: EPA 3546 Analytical Date: 04/28/08 11:46 Extraction Date: 04/25/08 11:30 Analyst: RT Parameter Result Qualifier Units RDL EPHwtth MS�Targetsforsample(s} 14,23 Batch W3197141 -* _rt4? M.m r�,d.,., �_ C9-C18 Aliphatics ND mg/kg 6.67 C19-C36 Aliphatics ND mg/kg 6.67 C11-C22 Aromatics ND mg/kg 6.67 C11-C22 Aromatics,Adjusted ND mg/kg 6.67 Naphthalene ND mg/kg 0.027 2-Methylnaphthalene ND mg/kg 0.027 Acenaphthylene ND m .0.027 .._. Acenaphthene ND mg/kg 0 027 Fluorene ND mg/kg 0.027 ....__..... Phenanthrene ND mg/kg 0.027 Anthracene ND mg/kg 0.027 Fluoranthene ND mg/kg 0.027 ...... Pyrene ND mg/kg 0 027 ...... __.._. Benzo(a)ant.........._ _ ....._.. Chrysene ND mg/kg...............__ 0.1027.. Benzo(b)fluoranthene ND mg/kg 0.027 .......... Benzo(k)fluoranthene ND mg/kg 0.027 .. ..... ........Benzo(a)pyrene ND mg/kg 01.0.2.7 Indeno(1,2,3-cd)Pyrene ND mg/kg 0 027 Dibenzo(a,h)anthracene ND mg/kg 0.027 Benzo(ghi)perylene ND mg/kg 0.027 Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 68 40-140 o-Terphenyl 76 40-140 2-Fluorobiphenyl 89 40-140 2-Bromonaphthalene 86 40-140 O-Terphenyl-MS 77 40-140 Page 58 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 Method Blank Analysis Batch Quality Control Analytical Method: 61,EPH-04-1 Extraction Method: EPA 3580A Analytical Date: 04/28/08 16:42 Extraction Date: 04/28/08 14:30 Analyst: RT Parameter Result Qualifier Units RDL EPH uv�th�MS't'a�gets or�s�amle s,•. 24 'Batch WG3�19733-1 '� l � � � ��' C9-C18 Aliphatics ND mg/kg 1000 ___. . _.._....... .._......... ..._.. ........ _. _..._... . .. C19-C36 Aliphatics ND mg/kg 1000 __.... __.. .......... ._ _.._... _._.. ._..__... C11-C22 Aromatics ND mg/kg 1000 ........ _...:...._.. _.. _.._... C11-C22 Aromatics,Adjusted ND mg/kg 1000 Naphthalene ND mg/kg 4.00 ......... _... ............. 2-Methylnaphthalene ND mg/kg 4.00 ._ -........ ....._.._.. .-. . ..._. ...... _..... .._................. .. ._...._........... Ac enaphthylene ND mg/kg_ 4.00 _.... -.... .......... . .................... . ........................ .Acenaphthene ND mg/kg 4.00 ......... .. . ........... ._........ ......_.. . _..._.....- _.._..._._ ...._... Fluorene ND mg/kg 4.00 ....._ . ...-. ........................ Phenath .mg/kg 4.00 . 9 ...._ _. . nrene ND __.. _. .. ..._.- A_n..t._h..r_a.cene ND m....g_../_kg 4.00 _ .... Fluor....................__ ......... ..._._... ........._. .._..._....... Pyr_e...n...e _ - -,... ND mg/kg 4 00......... _... ..... 1. .............. Benzo(a)anthracene ND . . _.............. mg/kg 4.00 ....... ........ _........... _. ................................ Chrysene ND mg/kg ... . Benzo(b)fluoranthene ND mg/kg 4.00 _._- ... .....__..._. ..__..._ Benzo(k)fluoranthene ND mg/kg 4.00 _.._.._._ _..._ ....._...... ............_. .... ._.. _....... ,._....-__.... .. ......... Benzo(a)pyrene ND mg/kg 4.00 ............_. _..._.._......................._......... _ .... ................................................. Indeno(1 2,3-cd)Pyrene ND mg/kg 4.00 _ __.... _....__.. ._...... Dibenzo(a,h)anthracene ND mg/kg 4.00 .. ...__.._. ................... . ............_ .. .._...... ... _..... ........... . ...... Benzo(ghi)perylene ND mg/kg 4.00 Acceptance Surrogate %Recovery Qualifier Criteria Chloro-Octadecane 91 40-140 o-Terphenyl 95 40-140 2-Fluorobiphenyl 89 40-140 2-Bromonaphthalene 86 40-140 O-Terphenyl-MS 65 40-140 Ilk �,��✓ r3 'A Page 59 of 117 04280820:22 Lab Control Sample Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits 7. " -" . . 0-2 :1IUG31E8950-.3 ,.. , w ssoclated sam le s..,;09,17;19Satch WG31895 _µ EPHs Oth MS Targets A // .. ._. .a, C9-C18 Aliphatics £ y 53` 40-140 8. .......... 25......_._ ___._.... _..... 49 �... ....... ...... C19-C36 Aliphatics a 75 68 ...„ 40 140 1Q 25 ........ _.__ _....... . _... C11-C22 Aromatics Ff fig 8, f 74� �' 40-140 5 25 Naphthalene ;. ._ .� 40140 25 5 _.._....... __.... ............ _.__........ _,. 2-Methyl naphthalene 67 _ .�, 40 140 _ �'..::-. .µ9 w" , 25 _ ..__ _... . _... 40-140 Acenaphthylene 11 25 . 0 72 �, f 66 40-140 �. w. _....... 25..... Acenaphthene x �� .......... Fluorene 40-140 11 *f .. 25 Phenanthrene ;72 ,r . El f ,7 ... , ..,`. 40-140 5 25 Anthracene _. _.... 40-140._ _........ fi .a. .. . _... 25...._. _..._... __._...__.90 83 z. Fluoranthene 90 83: 40-140 8 25.._._ _Pyrene € 40-140 6 25 8�g,- 84 ., .. Benzo(a)anthracene 116� 102; 40-140 13 ... .._. _..._. . ...25 __..__... .. ...... .......... . Chrysene _ $�. .. 74 40-140 0.. .... 25.._.. .. ._..__. ....... _. _...... __.._ .. ............ Benzo b fluoranthene 40-140 7° 25 �! Benzo(k)fluoranthene85 r 73 40-140 15"_> 25 . .- . .. Benzo(a)PYrene 90 __._ .. 77 ..._ 40-140 25 __... Indeno(1,2,3-cd)Pyrene 40-140 13 _e 25 92 Dibenzo(a,h)anthracene 95 g84 � 40-140 12 25 ���' _. Benzo(ghi)perylene u` 88 i : 78;" ... 40 140 .. ......_ 2mm^ 25 .......... _.. _. _ Nonane(C9) _ ,. .,40.:.. 30-140 �10 u..,,. 25 ` Page 60 of 117 �;a _ 04280820:22 Lab Control Sample Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits ,,, P _ , . P w th T 'r,ets.4 Assocl t m: I 7...1. a W 3 50=3 MSS,a a edsa e s : .09,,1, , ,5 Batch. 1tVG318950,2 G• 189. Decane(C10) 52 W 47 40-140 t10 < 25 Dodecane(C12) 60 F 55 40-140 9 25 Tetradecane(C14) .63 .._. :`„ ,„SST; .�,,,, ............. 40-140 10 � __ 25 ... ... ...... ......... �,. Hexadecane(C16) �67 ,T 40-140 11 25 Octadecane(C18) 69 62 40 140 . 1 .r 25...._.,. NonadecaneC19 T1 L , '" 12 ( � J 40 140 25 ._ .� .. .. :....... . .....__. - ......_..... ......................................................_........ .. ...... _. Eicosane(C20) 73 65' 40-140 1F2 25 Docosane(C22) 7567 40-140 11 25 .... . , ,.. ,.r.. .......... .... u, „ 72 40140 1`2 25 Tetracosane(C24) 81 ,. .... _. . ...4 , Hexacosane(C26) 40-140 12 ,' 25 Octacosane(C28) 80� T1 40-140 12 25 .......... ..... ....._. __.... ..> i ..._. ..._..... ..... ._ Y ..`.,a ... a... .... ...... Triacontane(C30) 72; 40-14011 _. 26 _..... Hexatriacontane(C36) �BU�� `;' 80 40-140 0 25 F...._ .. ... ....� ,. %Naphthalene Breakthrough 0 . .,� 0 - �- .. ........ .............. PNam . .. %2 Methylnaphthalene Breakthrough % 0; ,� ., .r . ..... ..... ......_....... �.. ._.. :..., _..... . . ..,... VNI Page 61 of 117 WA 04280820:22 Lab Control Sample Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits .,, ,. t. ;.,.ATM, „�-; : , ' Associated sarrr>le s .09�17 19 ::Batch. WG318950 2; ,WG318950 3, ... EPHwith,MS Targzets � ) �,.t M _ a . a,..�..,.._. �. . . . ...., -�: � :. LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Chloro-Octadecane 71 66 40-140 o-Terphenyl 90 90 40-140 2-Fluorobiphenyl 81 82 40-140 2-Bromonaphthalene 79 79 40-140 O-Terphenyl-MS 96 89 40-140 •Naphthalene Breakthrough 0 0 •2-Methylnaphthalene Breakthrough 0 0 ratedsam le s . 0.:1: 08,130 1 113,15:1:,6,1.8,20 22 :,, Batch ,,WG319.1,19-2 W.G-,,3191 t9-3 m N . . EPH ,withMSTargts A °C ._m pt.� _.': � _. #:. , r .H_ :; .. ,. � _„ _. _ _,T. . . C9-C18 Aliphatics 6970 f q 40-140 1 25 .z.�...0 .......__._.._...... •.. .. __. .._. _.... C19 C36 Aliphatics .. _......... _..., .. � _ `' ._ 7S _e '......_ _. 40-140 _.._._. 5 _ _. . ._...._... 25....... C11-C22 Aromatics 88 �94 40-140 7 25 Naphthalene __ _ ... .65...... 68 �..._ 40140 25 2-M ethyl naphthalene 66 70 40-140 6 25 _..._ .. �.. _.. ......... .......__... _..__. _..._. Acenaphthylene 40-140 9 25 40-140 Acenaphthene �. 69 73 6 _ e _.. . 25__. . _.. r .� 77° 40-140 _...._....... 5 25 Fluorene3 _. .. _ .� _. __ ......... Phenanthrene ,72 77, ._ _ .. 40-140 �? � . 25 Page 62 of 117 ;� �;� 04280820:22 Lab Control Sample Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits Anthracene SXMIVK1 � 97 40-140 6 25 Fluoranthene 91 100 40 140 9 25 �,. .. ... .._..... ... #. . ........... Pyrene 90 98 :; ... 40.140 .. __.... ... ._._ ... .. ..._. 25 Benzo(a)anthracene $5 '' 92 40-140 8 25 A. Chrysene 40 1407 25......_.. .. _ ......_ .....,_: ,. _ ._ ... .. ......................_. Benzo(b)fluoranthene 83 92 40-140 10 25 40-140 25 Benzo(k)fluoranthene 7$ $8 .... ....,...m,. Benzo(a)pyrene 81 �$4 40-140 4 .......... . _....._.... .._...__...._.. .. w..�. .,' .......... _......_ . P..,.. .�_ ...... _..... 25 Indeno(1,2,3 cd)Pyrene 76 86 40-140 12 25 ............... .,.. . . _;..,__...___. .. ._... ... . ..__._. . _.... .. ... ......._ .. Dibenzo(a,h)anthracene 80 91 40-140 13 25 Benzo(ghi)perylene 7�� ...... .. 86 40 140 4 .._...... 25 ...... ...... ....... Nonane(C9) kiiU61 30-140 y 2 25 _ _... _..... _.:.. ... ......,... ... . _ Decane C10 70' 70" 40-140 0 25 Dodecane(C12) 76 n.. ...: 40-140 1 � . ... .25 Tetradecane(C14) 7376 40 140 4 25 _,, s... ... €..._ ._, .. __....- .... ......... .. ..... Hexadecane(C16) 73, 76 + 40-140 4 2 5 ..,u. .... a.. _, t Octadecane(C18) 73 75 ff ' 40-140 3l 25 ., Nonadecane(C19) �a 76 ' 40-140 �4N 25 Eicosane C20 75' 40-140 25 Docosane(C22) I �80 40-140 t�5 25 " . s_ m" -Tetracosane(C24) $0 8�A " 40-140 5 25 ..x. .... .. .,.. Page 63 of 117 HA 042808 20:22 Lab Control Sample Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits W_... 11: 1315-1,6 18 20 22. Batch:.. �xWG - 9,11.9.2 ,WG31911°9-3� �. EPH,with MS Tar ets Assochated ,, kLA _,_ Hexacosane(C26) 76 80 40-140 .._..._ .. '� 25 Octacosane(C28) 75 .F.�80 ....�� ._ 40-140_ 25 Triacontane(C30) 7479 40-140 7 25 Hexatriacontane C36 72 ( 79. 40-140 9 25 %Naphthalene Breakthrough 0�' NC ....... . �. %2-Methyl naphthalene BreakthroughQ 0 , LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Chloro-Octadecane 61 73 40-140 o-Terphenyl 102 105 40-140 2-Fluorobiphenyl 91 91 40-140 2-Bromonaphthalene 91 92 40-140 O-Terphenyl-MS 87 99 40-140 •Naphthalene Breakthrough 0 0 •2-Methyl naphthalene Breakthrough 0 0 Page 64 of 117 t1tia 04280820:22 Lab Control Sample Analysis - Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits r. :- " EPH,wlth Tar ts,A F . • MS r e ssoclated"sam s Le s 14 23 Batch.,...WG319Z.14, 2 W.G319Z14 3,, ., . .,� �. �., .�.� C9-C18 Aliphatics 73 62 40-140 u, s 25 C19 C36 Ahphatics �82 „ _ _. 40-14t0 . ............ .....'�8 „�.',, . ... 25 C11 C22 Aromatics 6,,,.�..-�__ 7=9�;:.,, .. 40 140 8 25 _.. ,.. ............... ......... ., Naphthalene M 63 x 40-14024 25 2-Methylnaphthalene 8 , .. :M _. :...... . ............40 140 ... _ ...... �.' 20 _ 25.__...... . .. .... a _ ....... Acenaphthylene 8 71 40-140 18 25 ...... ......__........__. ... ..... _ .. ,:. a.._ ....... ,. .x�.. .. .,: ._,_.. ... . . ...... Acenaphthene 82 �69 n 40-140 �� 7 25 AX Fluorene ,. 85 ... 72 40-14017 ,. 25.._._... _. ...... < .......... ...... .. ...__._...... '. '�.. .._... Phenanthrene 95 87 40-1409 25 ....,.... .. . . .;.. .,. .., ,......_ Anthracene 113 104 40-140 8 „ 25 Fluoranthene ' �, a..., .. .... . .. .... ......... _. ._ ....... �127�...... 118 40 140 7 25 Pyrene 40 140 ., 25 ........ i Benzo(a)anthracene ° 1F36 123 '': 40-140 .. v 25 Chrysene.___ a98' ...._ .. 92 ^` 40-140 .. .. ...... _: 6 ......... 25 Benzo(b)fluoranthene 127 117� ' 40 140 8 26 .......... s..:: ._ ., .. ........ . r.... .'._ ... Benzo(k)fluoranthene 82 :-�80 40-140 '2 25 "•. �. .» .,. .. ,, M Benzo(a)pyrene 40-140 8 25 Indeno(1,2,3 cd)Pyrene 101 ' 96 40-140 5 25 ....._ .. ............ _...........,__....._............... Dibenzo(a,h)anthracene 105 100 40-140 5 25 Benzo(ghi)perylene 9994 40-140 W17K., 5 11,11"'1525 Nonane(C9) ��> ...._. 45 : ) ......_ 30-140 29 25 Page 65 of 117 AARtip,. 04280820:22 Lab Control Sample Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L08O5612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits : . STar'ets Associated sam ie s, .;, 14,23 ;,..Batch,„ ,, , ,• .r, �, , � _� � _ �.,� .,.�.,.. ..m u .' Decane(C10) ... ..7'',.. .... ,, _ _..... 40-140 __... a, 22 25 67 40 140mr Dodecane(C12) __. Tetradecane(C14) 77 68 40-140 12 25 _. ..�,.. 3 77 69y 40-140 11 25 Hexadecane(C16) ....... 40140 9r h 25 Octadecane(C18) 7 t _... ..__ ` .... 40-140 9 25 Nonadecane E cosane C20C19) � 7 a ( ) 40-140 _..__.._ _......_.._ .. ... ..... 9 25 80; 40 140 7,aY ......_ 25 ocosane(C22) � _.D _.. ... _ ..._.... 40-140 7 25 __... Tetracosane(C24) Q� , i36� 40-140 ? ..�' _........ 25 Hexacosane(C26) - _ _.... 40 140 25 ( Octacosane C28 �86 _ .,' ......_ ._.. ..._._...... ......... _ 78 40-140 �� 25 Triacontane(C30) _. ... .. ,, ;. 25 Hexatriacontane(C36) $3 78 .... 40 140 6, _ .. _ ...... ... a %Naphthalene Breakthrough .. ...... .._... __............ ......__....... .......__.. _.... ._. _ ......... ......... ,.� _ _.... ...... %2-Meth Ina hthalene Breakthrough NC Page 66 of 117 HA 04280820:22 s Lab Control Sample Analysis - Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits 1, ;6 EP,H wlth.MS Tar. .etsAssoc�atetl sam- e s 14 23 Batch. 1�UG319714,=2 WG31:9714 3 9. P. ( ) LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Chloro-Octadecane 74 71 40-140 o-Terphenyl 94 90 40-140 2-Fluorobiphenyl 79 80 40-140 2-Bromonaphthalene 79 79 40-140 O-Terphenyl-MS 123 120 40-140 •Naphthalene Breakthrough 0 0 •2-Methylnaphthalene Breakthrough 0 0 V. EPH with MS Tarr ets Associated sate ,le sWJ , 24. Batch. WG319733 2� WG319733=3 ,. F C9-C18 Aliphatics 40-140 0 25 C19 C36 Aliphatics 7882 40-140 5 25 ............ , "Iff C11-C22 Aromatics 89, _ 11 8'75 40-140 ;,, s. 25 Naphthalene NAM 77 F 1t 40-140 }, 2 25 2-Methylnaphthalene" 40 140 �' 14 " 25 Acenaphthylene 60 ..... t ... �.7�h_ ,,,,_,. 40-140 25 _ . Acenaphthene �� 64� 73 ';� 40-140 13 , 25 Fluorene 61 69 40-140 12 25 r .......... _................ ._.._........ __...... .............. 411 m.....:'. ..�.. ._............... ...,,,. ,.. ....' _ ........ ...... . -ra...... .. .. ......._... .. ... ........_ ..............._ _._......................_.. Phenanthrene 40 140 ,. ...... r �, ... 25 _... w... .: __...__ .......................... Page 67 of 117 tia 04280820:22 Lab Control Sample Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits is Associated sacra ens24 Batch , UVG31g733,2, VUG31,9733;3 ., y ... EPH with MS Targe p,. (:.)� _ .. .,• � . u -.. _. , - _. z - _ w. .. Anthracene 74� 84 ' ....... .. m 40-140 13 25 ., i .: _ ......_. om-.. __..... . Fluoranthene 76 92u 40-140 19 ;"� 25 ....._- .... € Pyrene 71 _. � 3 40-140 �1.6 25 Benzo(a)anthracene 82 96 40-140 �6 25 _....ry .. ........__.. .... ........__.... _ .. .. Ch sene >77f $T � 40-140 12 25 ..........-_-. ........... .._....... .. 5 ... .... . . . n a Benzo(b)fluoranthene T7 € 100 40-140 26 25 �, ..�, Benzo(k)fluoranthene 62 72 = 40-140 15 .__. .. 25...... .... .. .W.. ;.... ...,,,. __. __....... 78 40-140 15 25 Benzo(a)pyrene 67 __..._ Indeno(1,2,3-cd)Pyrene67 79, . _.... 40-140 16 - 25 a,h anthracene 69 82 40-140 1a7 fl 25 Dibenzo _ _(...._ )._ ........._ _. . f .... .... ... ....... Benzo(ghi)perylene 66 _ 40 140 ; 18 25 __. __ ..... 0 Nonane(C9) € 3.. .. � 30-140 25 Decane(C10) .. 79 7g 40-140 4 25_.. ... ..... 79 40-140 5 25 Dodecane(C12) 83 ....... 4 . ... ................_. .. ._.......__...........__.- Tetradecane C14 ;79 ' 76 40-140 25 Hexadecane(C16) -M 8 ^.77', 40140 ••-1 TH 25 77 40-140 1 25 Octadecane(C18) �::..._ ... -_ ..... __ .. _...__n .___.... 8 _. .. ... ......... ......... Nonadecane(C19) J 40-140 0 25 Eicosane(C20) 40-140 m 25 � 40-14 Docosane C22 gp 81 w ) 0 1 25 _..._ ......... Tetracosane(C24) 87 90w 40-1403 _ 25 . Page 68 of 117 04280820:22 Lab Control Sample Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits EPH with°MS;Tar be Assocl t ,m :: . a ed,sa lets . 24. Batch.. WG31-9733.2: WG3;19733 Hexacosane(C26) - 8 40-140 „ ; 25 Octacosane(C28) 17 2 89....:: <. . 40 140 '6� .. ....... . .......... 25 ....... .. 40 140 25 Triacontane(C30) 81 89 9 ......... Hexatriacontane(C36) BI 84 ,3 40-140 4 25 %Naphthalene Breakthrough - 0 0•, NC %2 Methylnaphthalene Breakthrough 0 0 NC Z ... ............ ...... ... ' 'x.,.. LCS LCSD Acceptance Surrogate %Recovery Qualifier %Recovery Qualifier Criteria Chloro-Octadecane 80 72 40-140 o-Terphenyl 98 94 40-140 2-Fluorobiphenyl 90 80 40-140 2-Bromonaphthalene 88 75 40-140 O-Terphenyl-MS 85 104 40-140 %Naphthalene Breakthrough 0 0 %2-Methylnaphthalene Breakthrough 0 0 Page 69 of 117 HA A 04280820:22 a Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L08O5612 Project Number: 14190101 Report Date: 04/28/08 Fractionation Check Standard Quality Control „ , Fractlonation check stanch"rd forFISHO61149 mr 11 Parameter %Recovery QC Criteria C9-C18 Aliphatics 60 40-140 C19-C36 Aliphatics 72 40-140 C11-C22 Aromatics 83 40-140 Naphthalene 77 40-140 2-Methylnaphthalene 72 40-140 .......... Acenaphthylene 72 40-140 ........ ...... _._.._. Acenaphthene 74 40-140 Fluorene 74 40-140 Phenanthrene 77 40-140 Anthracene 72 40-140 ... Fluoranthene 82 40-140 Pyrene 82 40-140 Benzo(a)anthracene 82 40-140 __..._ ...__......_. _._ ........... ......... ... Chrysene 82 40-140 Benzo(b)fluoranthene 81 40-140 Benzo(k)fluoranthene 84 40-140 Benzo(a)pyrene 76 40-140 Indeno(1,2,3-cd)Pyrene 76 40-140 ....__......_ ......._..... .................. .... _............ Dibenzo(a,h)anthracene 80 40-140 Benzo(g,h,i)perylene 80 40-140 ............ _.. Nonane ... 54 30-140 .... __. ....._.... ......_ _. ....._..... ............... ...... ----..... Decane 58 40-140 Dodecane 62 40-140 _ .... _.............._..__................ .. .........._... _ .. ..__..._ . .. .......... Tetradecane 62 40-140 ........... ........... _ .__ ... Hexadecane 63 40-140 ............. .......... .......... .............--.. .............. _...... Octadecane 64 40-140 Nonadecane 64 40-140 Eicosane 66 40-140 _....._ ......... _......__ Docosane 70 40-140 _ ......--.. ...__......._ Tetracosane 73 40-140 Hexacosane 76 40-140 ........ ......... ......... ........... .... ......... ._ ......... ......... ....................--_........... Octacosane 77 40-140 Triacontane 78 40-140 Hexatriacontane 82 40-140 L1 'HA Page 70 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 Fractionation Check Standard Quality Control , . ., Fractionation_ _ . check standard for FISHO61149 Surrogate % Recovery QC Criteria Chloro-Octadecane 52 40-140 o-Terphenyl 77 40-140 2-Fluorobiphenyl 76 40-140 2-Bromonaphthalene 76 40-140 f „7 Page 71 of 117 04280820:22 INORGANICS MISCELLANEOUS Page 72 of 117 f 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-01 Date Collected: 04/17/08 11:00 Client ID: coMP1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Solids,Total 97 % 0.10 1 04/22/08 21:25 30,2540G NM Ogg` .,,A Page 73 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-02 Date Collected: 04/17/08 11:30 Client ID: COMP2 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst General 3Che'mistry. � - ��._ Mom. ... _ . _. � a_ '� _ .. .v Solids,Total 95 % 0.10 1 ... -- _ A Page 74 of 117 I < 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-03 Date Collected: 04/17/08 12:00 Client ID: COMP3 Date Received: 04/21/08 Sample Location: WEST BARNSTABI_E,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Ana lytical ytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst N Solids,Total 87 % 0.10 1 04/22/08 21:25 30,2540G NM ti Page 75 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-04 Date Collected: 04/17/08 12:30 Client ID: COMP4 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst ' 'A General Cliemist « Solids,Total 94 % 0.10 1 04/22/08 21:25 30,2540G NM `'.�L Page 76 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-05 Date Collected: 04/17/08 09:00 Client ID: INFILTRATOR CLEAN OUT Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Solids,Total 74 % 0.10 1 04/22/08 21:25 30,250G NM ....... ..... .._.. . . . _. ........... ..... ............ I A Page 77 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-06 Date Collected: 04/17/08 09:30 Client ID: BG-1CP Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Solids,Total 96 % 0.10 1 04/22/08 21:25 30,2540G NM Page 78 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-07 Date Collected: 04/17/08 14:00 Client ID: BG-2SHEP Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst ; Solids,Total 87 % 0.10 1 04/22/08 21:25 30 2540G NM _ . . ....... . __..._ _........._ _. Page 79 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-08 Date Collected: 04/17/08 15:00 Client ID: MH-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst air __..... w Solids,Total 88 % 0.10 1 04/22/08 21:25 30,2540G NM Page 80 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-10 Date Collected: 04/17/08 14:30 Client ID: SED/WL-1 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Total Organic Carbon(Rep1) 2.3 % 0.01 1 04/25/08 14:00 1,9060 ES _ . __.. _ _..._. . -__..._.. Total Organic Carbon(Rep2) 2.5 % 0.01 1 04/25/08 14:00 1,9060 ES General istry s f FIV Solids,Total 37 % 0.10 1 04/22/08 21:25 30,2540G NM Page 81 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L08O5612 I Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-11 Date Collected: 04/17/08 14:10 Client ID: WL-2 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst SUbcontractedAnalysls .. _ .. __,_ ..._... v..:::.. _.., ... 3 Total Organic Carbon(Rep1) 1.1 % 0.01 1 04/25/08 14:00 1,9060 ES ...._ _._._ _...... __. Total Organic Carbon(Rep2) 1.2 % 0.01 1 04/25/08 14:00 1,9060 ES ..._ _. .......... General Cheinlstrjr .. a... N,.... _. 32-1 __ __ _. __' ...H. . wFF_. .... a........... Solids,Total 77 % 0.10 1 04/22/08 21:25 30,2540G NM Page 82 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-13 Date Collected: 04/17/08 14:50 Client ID: WL/ROAD SHOULDER 4 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Gene"ral Chemistry . Solids,Total 71 % 0.10 1 04/22/08 21:25 30,2540G NM Page 83 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 , Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-14 Date Collected: 04/17/08 15:10 Client ID: WL-5 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Subcontracted Analys�lsa. .. .,,, . _.,. �. u ... Total Organic Carbon(Rep1) 0.75 % 0.01 1 04/25/08 14:00 1,9060 . ES Total Organic Carbon(Rep2) 0.71 % 0.01 1 04/25/08 14:00 1 9060 ES t .. . ... ..... ry��. .M ... ,�.. .. .. .„ ... .. z.�. . �. gym.......... �, ,...�..._. Solids,Total 77 % 0.10 1 04/22/08 21:25 30,2540G NM Page 84 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-15 Date Collected: 04/17/08 14:45 Client ID: B-23 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Solids,Total 94 % 0.10 1 04/22/08 21:25 30,2540G NM hA Page 85 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 , Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-16 Date Collected: 04/17/08 14:55 Client ID: B-24 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst General Chemistrywww � ,. _..... . ,:�,,.. ... ._:mow �..,.,,. ,. ... ..:�... z` .. .� vi� Solids,Total 90 0.10 1 0_4../_2..2/08 21:25 30,2540G NI VI. ...... ........ ......_. _ ✓G� HA Page 86 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: LO805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-18 Date Collected: 04/18/08 08:50 Client ID: SED BACK HINCK Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Sufic_ontractedAnalysls .., Total Organic Carbon(Repl) 1.8 % 0.01 1 04/25/08 14:00 1,9060 ES _..... ........ ......-.1 .._. ......_ - _ .......__ Total Organic Carbon(Rep2) 2.1 % 0.01 1 04/25/08 14:00 1,9060 ES ........... ._....._ _...._...... .. ......_.. _._ ....... ......... ....... .... ........ .... ....... ........_. .........,_,...... . General Chemist y ,p �� xx Solids,Total 54 % 0.10 1 04/22/08 21:25 30,2540G NM Page 87 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-20 Date Collected: 04/18/08 09:15 Client ID: SED BARN HARBOR Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Subcontrac#ed�Anal sts " .+ ... .. ,. Total Organic Carbon(Rep1) 0.07 % 0.01 1 04/25/08 14:00 1,9060 ES Total Organic Carbon(Rep2) 0.07 % 0.01 1 04/25/08 14:00 1,9060 ES ......_. . __._... .,,,,.,.u.. .......... S ..i.a'.1nw,, a......a•.a�e.lw9',,, gib.;. .w'>a, ,+>,.. i.,.�..•.-. .- ..xAnh.:.' z ._rr., ,+,� ... em3., .N,aA...,�` Solids,Total 81 % 0.10 1 04/22/08 21:25 30,2540G NM kl, l-i�i Page 88 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-21 Date Collected: 04/18/08 08:20 Client ID: B-32 2656 RTE 6A Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst General Chemist b y Solids,Total 77 % 0.10 1 - 04/22/08 21:25 30,2540.. Page 89 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-22 Date Collected: 04/18/08 08:35 Client ID: BG 6A CB 2631 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst s � v General Chemrst .... �,, ..,.. . .. . Solids,Total 50 % 0.10 1 04/24/08 10:13 30,2540G JL . _ Page 90 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number:1 e 14190101 Report Date: 04/28/08 SAMPLE RESULTS Lab ID: L0805612-23 Date Collected: 04/18/08 08:40 Client ID: BG WL 2615 Date Received: 04/21/08 Sample Location: WEST BARNSTABLE,MA Field Prep: Not Specified Matrix: Soil Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Total Organic Carbon(Rep1) 2.5 % 0.01 1 04/25/08 14:00 1 ....__....... 9 ( P ) 0.01 1 - 04/25/0814:00 1,9060 ES Total Organic Carbon Re 2 2 2 Me Solids,Total 73 % 0.10 1 04/24/08 10:13 30,2540G JL Page 91 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L08O5612 Project Number: 14190101 Report Date: 04/28/08 Method Blank Analysis Batch Quality Control Dilution Date Date Analytical Parameter Result Qualifier Units RDL Factor Prepared Analyzed Method Analyst Subcontracted�Analysls for.sample(s} 1�0=11,14,18 20,23= Batch WG319568 1� ,� � :, � � ;, Total Organic Carbon(Rep1) ND % 0.01 1 04/25/0814:00 19060 ES Total Organic Carbon(Rep2) ND % 0.01 1 - 04/25/08 14:00 1,9060 E Page 92 of 117 04280820:22 4 Lab Control Sample Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 LCS LCSD %Recovery Parameter %Recovery %Recovery Limits RPD RPD Limits " " 3, rMn Subcontr cted'Ana'I: sls:,-:Associated saris,to s.. 10 11,14 18 20 23 Batch: WG319568 2 a Y P ), 1. M Total Organic Carbon(Rep1) 3• 90 75-125 Total Organic Carbon(Rep2) 90 75-125 - Page 93 of 117 L1 t;A 04280820:22 Lab Duplicate Analysis Project Name: CAVES PASTURE/SCUDDERS LN. Batch Quality Control Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 Parameter Native Sample Duplicate Sample Units RPD RPD Limits :.. _ _ ..,_ >. 74-01�Cllent I®.,DUP.Sam le 0.1:-08�90 1>1 13.16.18 20 21:. Q,C-Batch ID._WG3'l9091, 1,.,,QC Sample. L08055 , p ,Associated sample(. ? r:- : . .. - . �- :f T. . . .-�. , : : : _ :: �_._.,tea ;�,. . .. ... . m._,. Solids,Total 89 91 % - 2 20 ;s. ssocatedsarnple(s.). .., , , 393 ...y .,. ,. ..805 2 QCB ID G 606-A _. Solids,Total 81 81 % 0 - 20 Page 94 of 117 LITtil� ' 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 Sample Receipt and Container Information Were project specific reporting limits specified? YES Cooler Information Cooler Custody Seal A Absent B Absent Container Information Container ID Container Type Cooler pH Temp Pres Seal Analysis L0805612-01A Amber 250ml unpreserved A N/A 2C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-02A Amber 250ml unpreserved A N/A 2C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-03A Amber 250ml unpreserved A N/A 2C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-04A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-05A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-06A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-07A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-08A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-09A Amber 1000ml HCI preserved B <2 2.6C Y Absent EPHD-GC-04,EPH-MS L0805612-09B Amber 1000ml HCI preserved B <2 2.6C Y Absent EPHD-GC-04,EPH-MS L0805612-10A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-10D Amber 100ml unpreserved B N/A 2.6C Y Absent SUB-MAN-TOC9060 L0805612-11A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-11D Amber 100ml unpreserved B N/A 2.6C Y Absent SUB-MAN-TOC9060 L0805612-13A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS L0805612-13B Amber 250ml unpreserved B N/A 2.6C Y Absent TS L0805612-14A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-14D Amber 100ml unpreserved B N/A 2.6C Y Absent SUB-MAN-TOC9060 L0805612-15A Amber 250ml unpreserved A N/A 2C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-16A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-17A Amber 1000ml HCI preserved A <2 2C Y Absent EPHD-GC-04,EPH-MS L0805612-17B Amber 1000ml HCI preserved A <2 2C Y Absent EPHD-GC-04,EPH-MS L0805612-17C Amber 1000ml unpreserved A 7 2C Y Absent EPH-MS L0805612-18A Amber 250ml unpreserved A N/A 2C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-18D Amber 100ml unpreserved A N/A 2C Y Absent SUB-MAN-TOC9060 L0805612-19A Amber 1000ml HCI preserved A <2 .2C Y Absent EPHD-GC-04,EPH-MS L0805612-19B Amber 1000ml HCI preserved A <2 2C Y Absent EPHD-GC-04,EPH-MS L0805612-19C Amber 1000ml unpreserved A 7 2C Y Absent EPH-MS L0805612-20A Amber 250ml unpreserved B N/A 2.6C Y Absent EPHD-GC-04,EPH-MS,TS ^ L1Y�iiA Page 95 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 ' Project Number: 14190101 Report Date: 04/28/08 Container Information Container ID Container Type Cooler pH Temp Pres Seal Analysis L0805612-20D Amber 100ml unpreserved B N/A 2.6C Y Absent SUB-MAN-TOC9060 L0805612-21A Amber 250ml unpreserved A N/A 2C Y Absent EPHD-GC-04,EPH-MS L0805612-21B Amber 250ml unpreserved A N/A 2C Y Absent TS L0805612-22A Amber 250ml unpreserved A N/A 2C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-23A Amber 250ml unpreserved A N/A 2C Y Absent EPHD-GC-04,EPH-MS,TS L0805612-23D Amber 100ml unpreserved A N/A 2C Y Absent SUB-MAN-TOC9060 L0805612-24A Amber 100ml unpreserved A N/A 2C Y Absent EPHD-GC-04,EPH-MS Container Comments L0805612-01A IR Gun L0805612-02A IR Gun L0805612-03A IR Gun L0805612-15A IR Gun L0805612-17A IR Gun L0805612-17B IR Gun L0805612-17C IR Gun L0805612-18A IR Gun L0805612-18D IR Gun L0805612-19A IR Gun L0805612-19B IR Gun L0805612-19C IR Gun L0805612-21A IR Gun L0805612-21B IR Gun L0805612-22A IR Gun L0805612-23A IR Gun L0805612-23D IR Gun L0805612-24A IR Gun Page 96 of 117 04280820:22 Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 GLOSSARY Acronyms EPA - Environmental Protection Agency. LCS - Laboratory Control Sample:A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. LCSD- Laboratory Control Sample Duplicate: Refer to LCS. MS - Matrix Spike Sample:A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. MSD - Matrix Spike Sample Duplicate: Refer to MS. NA - Not Applicable. NI - Not Ignitable. NC - Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. ND - Not detected at the reported detection limit for the sample. RDL - Reported Detection Limit: The value at which an instrument can accurately measure an analyte at a specific concentration.The RDL includes any adjustments from dilutions, concentrations or moisture content,where applicable. RPD - Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. I Terms Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260E is shown as 1,8260B.)The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers The following data qualifiers have been identified for use under the CT DEP Reasonable Confidence Protocols. A-Spectra identified as"Aldol Condensation Product". B-The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte. E-Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. J-Estimated value. The analyte was tentatively identified; the quantitation is an estimation. (Tentatively identified compounds only.) Standard Qualifiers H-The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. Report Format: Data Usability Report Page 97 of 117 04280820:22 ' Project Name: CAVES PASTURE/SCUDDERS LN. Lab Number: L0805612 Project Number: 14190101 Report Date: 04/28/08 REFERENCES 1 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I -IIIA, 1997. 30 Standard Methods for the Examination of Water and Wastewater.APHA-AWWA- WPCF. 18th Edition. 1992. 61 Method for the Determination of Extractable Petroleum Hydrocarbons(EPH). Massachusetts Department of Environmental Protection, DEA/ORS/BWSC. May 2004, Revision 1.1. LIMITATION OF LIABILITIES Alpha Woods Hole Labs performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error,the sole and exclusive responsibility of Alpha Woods Hole Labs shall be to re-perform the work at it's own expense. In no event shall Alpha Woods Hole Labs be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Woods Hole Labs. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. Page 98 of 117 CHAIN OF CUSTODY 4 '� �&.-, PA.—i—OF .a gp `�. A f.�b N •t 1t1.tYl' I',, e?" t,. Swr ` ,�t e=IC��� �l� t kt�i �slt�4 Project Information Report Informatior-Data Deliverables Billing Information w � cty i "t O WESTEORO.MA MANSFIELD,MA 04 TEL: 508•a95.9220 TEL 508S22-9300 00 Protect Name: sad�r� O FAX O EMAIL O Sarne as Ghent info ...............99- PO�: FAX: sose9i9s FAX: 508-622.1288 C aL ej A - — —'---Vn n _ DO O ADEx ❑Add'I Deliverables —......------..—....__._ ..__..__.._.._.._.._._ -..... _..__. N Client InformationProject Location_ r! nd444a__.. •.._. Regulatory 0 Client: _.._..._..... . En Project 0p1 ._ _ State/Fed Program Criteria Address: PO (30 01 j! Project Manager S Z`� ------- --- --------...____.._..__....—..._.___.....__....__._------.._._._.....____.__ ALPHA Quote f: VIA MCP •_ESUMPTIVE CERTAINTY---CT REASONABLE CONFIDENCE •-• • Phone: & 00$'Q • O Yes ❑No Are MCP Analytical Methods Required? Fax: S Or y � f O Yes O No Are CT RCP(Reasonable Confidence Protocols)Required? Jid Standard O RUSH(my•.nm.d•p•.oa_.d) Email: �/ c % / (e c!.►+ �s to Duo: Db Time: E a ' ❑ These samples have been prevtously analyzed by Alpha 12 O GJi O SAMPLE HANDLING Other project S Specific Requirements/Comments/Detection Limits: 13Done O Not needed O Lab to ido o � Preservation ' O Lab to do Lp i z. Colleclil Sample Sampler's / % (P1a•WD HYWow) Sample ID Date Time Matrix Initials�� Sample Speafic Comments e� Cc, I 4 /t�vk 4:ao s,'/ SE X B/C X I . Gur►�o �, n..3v ,, _ r ' a Corr+ 4 SEK X A S61 —.. — --- - -- -"- — -- h C PLEASE ANSWER QUESTIONS ABOVEI Container Ty _H7 Preservative G y'C # c•''1►S , IS YOUR PROJECT �� r» r� ""gyp Relinquished By: DateMme Received By: DateMme �IS18r rrrt Apy $tra{84f s "' MA MCP or CT RCP? �' - -'- - ORM NO:01-01(rev.14.00T-07) _. .. .._--___—_—.___ . _ _/yi 01 0) M CHAIN OF CUSTODYIN PA°E of 3 C) WESTBORO,6AA MANSFlEID,MA Project Information Report Informitiou -Data Deliverables Bilhiig Information N TEL 506 898 9220 TEL s°e-4¢as2, Project Name: ��__ /�/ �� //" ❑FAX 0 EMAIL O Same as Client info PO : 00 FAX: 506898.9793 FAX: 508-022J2ee lQi<t �CS{[xyc-A"4&�. .— — -----. Project L°cation:— O ADEx O Add9 Deihrerables aoInformaol, Regtilatory e(It0remerits/Report Limits � Client: Project P: • --__ ,i�nt E1�$;n���t -- l y19 010! State iFed Program Gtterta ddress: P x B 3d Project Manager: S c.► C� —'-- —-- — i i ---- ALPHA Quote#: VIA MCP PRESUMPTIVE CERTAINTY--CT REASONABLE • s ••• • Phone: G775 a ' O Yes O No Are MCP Analytical Methods Required? Fax: , � O Yes 0 No Are CT RCP(Reasonable Confidence Protocols)Required? ❑Standard D RUSH I14*w4 .a.y..ppowal Email: ' SKra;�M Zd�C r,'ntiCn nee , "ate Du•: Time: O These samples have been prexiously analyzed byAlPhe �v SAMPLE HANDLING Other Project Specific Requirements/Comments/Detection Limits: 0 13 Done o Done O Not needed O Lab to do Z Preservation ' ❑Lab to do Collection Sample Sampler's rPMi'°' °"0M1 Sample ID Date Time Matrix Initials Sample Specific omments ' Gv�,��Q.rt. Shor,lotrr- -1:sty SD. _ d< X 4� i PLEASE ANSWER QUESTIONS ABOVEI Container Type Preservative IS YOUR PROJECT Relinquished By: DateMme Received By: DateRme r A MCP or CT RCP? M i rr y p i I .Co I CHAIN OF CUSTODY 3 3 Nl MAProject Information Report Information-Data Defiverables Billing Information WESTBORO.MA MANSFIELD, i � TEL 500-BW9220 TEL 508-022-9309 Project Name: O FAX O EMAIL O Same as Client info PO*: 0 FAX:50&e9a•9199 FAX 50a-022J28a C.JaiF�4. 1�—.G, /A,_._ _..__.....—._____..-_._.._.._—,... Project Locafion. O ADEx O Add1 Deliverables v -— __ j -/17�__ Pegulatory Requirements/R(!port Limits o Client: p Project*: l q190/D/ State iFed Prognvrr Criteria Ad dress: PC.�or /OiSS Qtii Project Manager: 1 -- ----___ [.c A tI• l6 /l7iC� — ALPHA Quote*: •- REASONABLE • a •-• • Phone: S* 947 mno Ttirn-AtotindO Yea 0 No Are MCP Analytical Methods Required? Fax: O Yea O No Are CT RCP(Reasonable Confidence Protocols)Required? 5G� 9k 7 Standard O RUSH t.a ae+••�•,•,ov�•s, Email: SI<re,%•n ss( dr �+ter>S;,eI'r n .o Dato Dug• Tirrr•: SAMPLE HANDLING O These samples have been previously analyzed by Alpha l Fittretion Other Project Specific Requirements/Comments/Detection Limits: n " / Cl Done ❑Not needed O Lab to do Preservation / O Lab to do Collection Sample Samplers Sample ID Date nTe Matrix Initials Sample Specific Comments � fti Kio s6/c X e.K —— Z 6A G X&31 —_-------- cu[._ ft PLEASE ANSWERER QUESTIONS ABOVE! Contalner Type � Preservative 'L f` IS YOUR PROJECT DateMme Relinquished BY: Oate/Tlme Received By: MA MCP or CT RCP? Mow ORM NO:01-01(m.. -07I 14-OCT -- -'-- -----------_--'— ----- a O a) rn co a 04280820:22 ANALYTICAL REPORT Prepared for: Alpha Analytical -Westborough 8 Walkup Drive Westborough, MA 01581 Project: L0805612 - PRIME ETR: 0804112 Report Date: April 25, 2008 Certifications and Accreditations Massachusetts M-MA030 Connecticut PH-0141 New Hampshire 2206 Rhode Island LA000289 New Jersey MA015 Maine MA0030 New York 11627 Louisiana 03090 Florida E87814 Pennsylvania 68-02089 Army Corps of Engineers Department of the Navy This report shall not be reproduced except in full,without written approval from the laboratory. 320 Forbes Blvd Mansfield MA 02048, (508)822-9300,Fax(508)822-3288 1/16 Page 102 of 117 � a 04280820:22 Sample ID Cross Reference Client: Alpha Analytical-Westborough Lab Code: MA00030 Project: L0805612-PRIME ETR: 0804112 _ HA = ry'A'„JVc Ail :L_T J C A i ' I Lab Sample ID Client Sample ID 0804112-01 SED/WL-1 . 0804112-02 WL-2 0804112-03 WL 5 0804112-04 SED BACK HINCK 0804112-05 SED BARN HARBOR 0804112-06 BG WL 2615 320 Forbes Blvd,Mansfield MA 02048, (508)822-9300, Fax(508)822-3288 2/16 Page 103 of 117 04280820:22 s CASE NARRATIVE Alpha Analytical ETR: 0804112 Project: L0805612—PRIME All analyses were performed according to Alpha Analytical quality assurance program and documented Standard Operating Procedures(SOPS).The analytical results contained in this report were performed within holding time,and with appropriate quality control measures,except where noted.A summary of all state and federal accreditation is provided within this report. Blank correction of results is not performed in the laboratory for any parameter.Alpha Analytical certifies that the test results within meet all of the requirements of NELAC,for all NELAC accredited parameters. The enclosed results of analyses are representative of the samples as received by the laboratory. Alpha Analytical makes no representations or certifications as to the method of sample collection, sample identification, or transporting/handling procedures used prior to the receipt of samples by Alpha Analytical.To the best of my knowledge,the information contained in this report is accurate and complete. For any questions regarding this report, please contact the signatory below at 508- 822-9300. /1 Approved b : I Title:, Project Manager Date: 4/25/08 PP y — Peter Henriksen f 0:1 ReporrWARRTEMP I Z0081 Alpha 10804112.doc Alpha Analytical,320 Forbes Blvd.,Mansfield,MA 02048,508-822-9300 3/16 Page 104 of 117 I 04280820:22 0 Total Organic Carbon 4/16 Page 105 of 117 04280820:22 Form I Inorganics ��-¢_ Client: Alpha Analytical-Westborough Lab Code: NIA00030 Project: L0805612 -PRIME ETR: 0804112 °ia==f. Case: N/A SDG: N/A Lab ID: 0804112-01 Client ID: SED/WL-1 Date Collected: 04/17/08 Matrix: Sediment Date Received: 04/22/08 Percent Solid:N/A Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst -.-. Total Organic Carbon(Run 1) � 2.3 0.01 1 04/25/08 % 9060 ES Total Organic Carbon(Run 2) 2.5 0.01 1 04/25/08-...._ % 9060 ES i i N/A-Not Applicable 04/25/OS IQIS 320 Forbes Blvd,Mansfield, MA 02048, (508) 822-9300, Fax(508) 822-3288 Page 106 of 117 04280820:22 Form I Inorganics ` = Client: Alpha Analytical-Westborough Lab Code: MA00030 Project: L0805612-PRIME E 1 R: 0804112 HA Case: N/A SDG: N/A _ c Lab 1D: 0804112-02 Client 1D: WI 2 Date Collected: 04/17/08 Matrix: Soil Percent Solid:N/A Date Received: 04/22/08 Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst Y(b@ Organic Carbon(Run 1) 1.1 0.01 1 04/25/08 % 9060 E'S Total Organic Carbon(Run 2) 1.2 0.01 1 04125/ 88 % 9060 ES N/A-Not Applicable .BIOS 16:16 320 Forbes Blvd Mansfield, AM 02048, (508)822-9300, Fax(508)822-3288 Page 107 of 117 04280820:22 • Form I Inorganics Client: Alpha Analytical-Westborough Lab Code: MA00030 T q Project: L0805612-PRIME ETR: 0804112 HA " = Case: N/A SDG: N/A -,- Lab ID: 0804112-03 Client ID: WL 5 Date Collected: 04/17/08 Matrix: Soil Date Received: 04/22/08 Percent Solid:N/A Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst Total Organic Carboni(Run 0 0.75 0.01 1 04/25/08 % 9060 ES Total Organic Carbon(Run 2) 0.71 0.01 1 04/25/08 /o 9060 ES N/A-Not Applicable 0025109 ne:is - 320 Forbes Blvd, Mansfield,MA 02048, (508)822-9300,Fax(508)822-3288 Page 108 of 117 3. ' 04280820:22 10 Form I Inorganics w: Client: Alpha Analytical-Westborough Lab Code: MA00030 4c. Project. L0805612 - PRIME ETR: 0804112 HA Case: N/A SDG: N/A re4=tT. 1sx 7 1 C R. L Lab ID: 0804112-04 Client ID: SED BACK HINCK Date Collected: 04/17/08 Matrix: Soil Date Received: 04/22/08 Percent Solid:N/A Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst Tot11 Organic Carbon(Run 1) 1.8 0.01 1 04/25/08 % 9060 ES 'Total Organic Carbon(Run 2) 2.1 _-._._.. 0.01 l 04/25/08 ° _...._..-.....__9060 - ES I N/A-Not Applicable . 5J08 IG:18 320 Forbes Blvd,Mansfield MA 02048, (508)822-9300, Fax(508)822-3288 Page 109 of 117 04280820:22 ' Form I Inorganics Client: Alpha Analytical-Westborough Lab Code: MA00030 y,-- o Project: L0805612-PRIME ETR: 0804112 'w Case: N/A Lab 1D: 0804112-05 SDG: N/A r c A, L Client ID: SED BARN HARBOR Date Collected: 04/17/08 Matrix: Soil Date Received: 04/22/08 Percent Solid:NIA Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst Total Urgallic Carbon(Run 1) 0.07 0.01 1 04/25/08 % 9060 ES Total Organic Carbon(Run 2) 0.07 0.01 I 04/25/08 % _ 9060 ES N/A-Not Applicable 04/25/08 16:18 9/1i 6 -- 320 Forbes Blvd, Mansfield, AM 02048, (508)822-9300, Fox(508)822-3288 Page 110 of 117 04280820:22 r,. Form I Inorganics ° Client: Alpha Analytical-Westborough Lab Code: MA00030 '- Eq. Project: L0805612-PRIME ETR: 0804112 `MHA rt;A I e A Case: N/A SDG: N/A Lab ID: 0804112-06 - Client ID: BG WL 2615 Date Collected: 04/17/08 Matrix: Soil Percent Solid:N/A Date Received: 04/22/08 Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst Total Organic Carbon(Run 1) 2.5 0.01 1 04/25/08 R % 9060 ES Total Organic Carbon(Run 2) 2.2 0.01 1 04/25/08 % 9060 ES I i ; i i � I i I i N/A-Not Applicable 04n5/06 MIS 320 Forbes Blvd, Mansfield,MA 02048, (508)822-9300, Fax(508)822-3288 Page 111 of 117 04280820:22 ` Form III Inorganics r-� Client: Alpha Analytical-Westborough Lab code: MA00030 Project: L0805612-PRIME ) TR: 0804112 Case: N/A S DG: N/A 4 C „ i Lab ID. WSO42508B14 Client ID: Blank Date Collected: N/A Matrix: Sediment Date Received: N/A Percent Solid:100 Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst Total Organic Carbon(Rim l) 0.01 U 0.01 1 04/25/08 % 9060 ES Total Organic Carbon(Run 2) 0.01 U 0.01 1 04/25/08 % 9060 ES N/A-Not Applicable U-The analy-te was analyzed for but not detected at the sample specific level reported. 04/25/08 16:18 ---- 320 Forbes Blvd Mans veld, MA Off 64 , 508 822-9300,Fax(508)822,3288 Page 112 of 117 e Form III 04280820:22 Inorganics Client: Alpha Analytical-Westborough Lab Code: MA00030 Project: L0805612 -PRIME ETR: 0804112 F a n' is �r I C aCase: N/A SDC,: N/A Lab ID: WSO42508BI4 Client ID: Blank Date Collected: N/A Matrix: Soil Date Received: N/A Percent Solid:100 Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst Total Organic Carbon I) 0.01 U 0.01 1 04/25/08 % 9060 ES Total Organic Carbon(Run 2) 0.01 U 0.01 1 04/25/08 % 9060 ES N/A-Not Applicable U-The analytc was analyzed for but not detected at the sample specific level reported. 04/25/08 16:18 6 320 Forbes Blvd, Mansfield MA 02048, (508)822-9300, Fax(508)822-3288 Page 113 of 117 04280820:22 Form I Laboratory Control Sample Inorganics k Client: Alpha Analytical-Westborough Lab Code: NMA00030 ='- Project: L0805612-PRIME ETR: 0804112 Case: N/A SDG: N/A J e A � Lab ID: WSO42508L03 Client ID: Laboratory Control Sample Date Collected: N/A Matrix: Sediment Date Received: N/A Percent Solid:100 Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst ES 'Total Organic Carbon(Run 1) 27 6.01 1 04/25/08 % 9060 Total Organic Carbon(Run 2) 27 0.01 1 04/25)08 % 9060 ES N/A-Not Applicable 04/25/08 16:18 320 Forbes Blvd,Mansfield,MA 02098, (508)b22-9300,Fax(508) 822-3288 Page 114 of 117 04280820:22 Form I Laboratory Control Sample Inorganics Client: Alpha Analytical-Westborough Lab Code: MA00030 Project: L0805612 -PRIME ETR: 0804112 t ..---— _- Case: NIA SDG: N/A -,i'"z i C A L Lab ID: WSO42508L03 Client ID: Laboratory Control Sample Date Collected: N/A Matrix: Soil Percent Solid:100 Date Received: NIA Reporting Date Analytical Parameter Result Qualifier Limit Dilution Analyzed Unit Method Analyst Total Organic Carbon(Run 1).... 27 0.01 1 04/25/08 % 9060 ES l`�tal Organic Carbon(Run 2) 27 0.01 1 04/25/08 % 9060 ES N/A-Not Applicable i 04n5ro8 i6a8 - 320 Forbes Blvd, Mansfield MA 02048, (508)822-9300,Fax(508)822-3288 - 6 Page 115 of 117 04280820:22 Form VII Laboratory Control Sample Inorganics T. Client: Alpha Analytical-Westborough Lab Code: MA00030 r Y ti Project: L0805612 -PRIME ETR: 0804112 HA Case: N/A SDG: N/A Lab ID: WSO42508L03 -" Client ID: Laboratory Control Sample Date Collected: N/A Matrix: Sediment Date Received: N/A Percent Solid:100 %Recovery Parameter Conc. %Recovery Limits n..._._........r .-�,..r 27 90,,,,,,,,,,,;,,...., 75-125 Total Organic Carbon(Run 1) _....... " Total Organic Carbon(Run 2) 27 90 75-125 N/A-Not Applicable I Concentrations reported as calculated values,which includes rounding for significant figures. Percent recoveries and RPD values are calculated from the unrounded results. onrzvos leas .... - - .. _-- 320 Fo�•bes Blvd, Mansfield,M.4 02048, (508)8229300, Fax(508)822-3288 Page 116 of 117 • 04280820:22 Certificate/Approval Program Summary Method numbers assume the most recent EPA revisions.For a complete listing of analytes for w the referenced methods please contact your Alpha Woods Hole Lab Project Manager or the � HA Quality Assurance Manager. ti=! N A=ICY.7 1 C A L Connecticut Department of Public Health Certificate/Lab ID :PH-0141 - Wastewater(General Chemistry:EPA 120.1, 150.1, 160.1, 160.2, 180.1,300.0,310.1,335.2;Metals: 200.8,245.1;Organics: 608-PCB,ETPH) Solid Waste/Soil(General Chemistry: 1010,9010/9014,9045,9060;Metals: 6020,7470,7471;Organics: 8081, 8082, 8260,8270,ETPH). Florida Department of Health Certificate/Lab ID:E87814-Primary NELAP Accreditation Authority for Air& Emissions.Secondary NELAP Accreditation for Wastwater and Solid&Hazardous Waste. Wastewater (General Chemistry:EPA 120.1/SM2510B, 150.1, 160.1/SM2540C, 160.2/SM2540D, 180.1,300.0,335.2, SM2320B, SM2340B, SM2540G,SM4500NH3;Metals:245.1;Organics:608-PCB).Solid and Hazardous Waste (General Chemistry:9010/9014,9045,9050,9056,9065,Reactivity 7.3; Metals:6020, 7470,7471;Organics: 8081,8082, 8260,8270). Air&Emissions (Organics:EPA TO-15). Louisiana Department of Environmental Quality Certificate/Lab ID :03090-Primary NELAP Accrediting Authority for Wastewater,Solid&Hazardous Waste. Wastewater(General Chemistry:EPA 120.1/SM2510B, 150.1, 160.1/SM2540C, 160.2/SM2540D, 180.1,300.0,310.1/SM232013,335.2,376.2,9010/9014,9056,SM2540G;Metals:200.8,245.1, 6020;Organics: 608-PCB,8015-DRO,8081,8082,8260, 8270). Solid and Hazardous Waste(General Chemistry: 1010, 1311,9010/9014,9040,9045,9056,9060,Reactivity 7.3;Metals: 6020,7196,7470, 7471;Organics: 8015-DRO, 8081, 8082,8260, 8270). Maine Department of Human Services Certificate/Lab ID:MA0030-Wastewater (General Chemistry:EPA 120.11 SM2510B, 160.1/SM2540C, 160.2/SM2540D,300.0,310.1/SM232013,335.2;Metals:EPA 245.1;Organics: 608-PCB). Massachusetts Department of Environmental Protection Certificate/Lab ID:M-MA030- Wastewater (General Chemistry: EPA 120.1/SM2510B, 150.1, 160.1/SM2540C, 160.2/SM2540D,300.0,310.1/SM2320B,335.2;Metals: EPA 245.1;Organics: EPA 608-PCB). New Hampshire Department of Environmental Services Certificate/Lab ID:2206-Secondary NELAP Accreditation. Wastewater (General Chemistry:EPA 120.1/SM25IOB, 150.1, 160.1/SM2540C, 160.2/SM2540D, 180.1,300.0, 310.1/SM2320B,335.2,376.2,SM2540G;Metals: 200.8,245.4;Organics:608-PCB). New Jersey Department of Environmental Protection Certificate/Lab ID: MAO 15- Secondary NELAP Accreditation. Wastewater(General Chemistry:EPA 120.1/SM2510B, 150.1, 160.1/SM2540C, 160.2/SM2540D, 180.1,300.0, 310.1/SM2320B,335.2,376.2,9010/9014,9056,SM2540G;Metals:200.8,245.1 6020;Organics:608-PCB, 8081, 8082, 8260, 8270).Solid&Hazardous Waste(General Chemistry: EPA 1010, 1311,9010/9014,9040,9045, 9056,9060;Metals: 6020,7196,7470,7471;Organics: 8015-DRO, 8081,8082,8260, 8270). Air&Emissions (Organics: EPA TO-15). New York Department of Health Certificate/Lab ID : 11627-Secondary NELAP Accreditation. Wastewater (General Chemistry: EPA 120.1/SM2510B, 150.1, 160.1/SM2540C, 160.2/SM2540D,300.0,310.1/SM2320B,376.2; Metals: 200.8,245.1;Organics:608-PCB). Solid and Hazardous Waste(General Chemistry:EPA 1010, 1311; : 200.8;B®S41,;7041;Organics: 8081,8082,8260,8270). Air&Emissions (Organics:EPA TO-15). Rhode Island Department of Health Certificate/Lab ID : LA000289-Chemistry: Organic and Inorganic in Non- Poratable Water, Wastewater/Sewage and Soil (Refer to LADEQ and MADEP certificates for method numbers.) Pennsylvania Department of Environmental Protection Certificate/Lab ID: 68-02089-Registered laboratory U.S.Army Corps of Engineers Department of the Navy 320 Forbes Blvd,Mansfield MA 02048, (508)822-9300,Fax(508)822-3288 16/16 Page 117 of 117 HA ANM-07r2 I C A L ANALYTICAL REPORT Prepared for: Alpha Analytical - Westborough 8 Walkup Drive Westborough, MA 01581 Project: L0805617 - PRIME ETR: 0804111 Report Date: May 02, 2008 Certifications and Accreditations Massachusetts M-MA030 Connecticut PH-0141 New Hampshire 2206 Rhode Island LA000289 New Jersey MA015 Maine MA0030 New York 11627 Louisiana 03090 Florida E87814 1 Pennsylvania 68-02089 Army Corps of Engineers Department of the Navy ,491K ACC09C This report shall not be reproduced except in full,without written approval from the laboratory. 320 Forbes Blvd Mansfield MA 02048, (508)822-9300, Fax(508)822-3288 1 of 45 r Sample ID Cross Reference Client: Alpha Analytical-Westborough Lab Code: MA00030 Project: L0805617-PRIME ETR: 0804111 HA A c a,L Lab Sample ID Client Sample ID 0804111-01 Infiltrator Clean Out 0804111-02 BG-1 cp 0804 1 1 1-03 BG-2 shep 0804111-04 MH-1 0804111-05 BG 6A CB 2631 0804 1 1 1-06 Stockpile j 0804111-07 Raw Product i 320 Forbes Blvd,Mansfield, MA 02048, (508)822-9300,.Fax(508)822-3288 2 of 45 CASE NARRATIVE Alpha Analytical ETR: 0804111 Project: L0805617-PRIME All analyses were performed.according to the Alpha-Analytical quality assurance program and documented Standard Operating Procedures (SOPS). The analytical results contained in this report were performed within holding time, and with appropriate quality control measures,except where noted. All soil/sediment results are reported on a dry weight basis unless otherwise noted. A summary of all state and federal accreditations is provided within this report. Blank correction of results is not performed in the laboratory for any parameter. Alpha Analytical certifies that the test results within meet all of the requirements of NELAC,for all NELAC accredited.parameters. Total Petroleum Hydrocarbons(TPH)by GC/FID 1. All data quality objectives were met. Total Petroleum Hydrocarbon Identification The following samples have GC/FID characteristics which is similar to a combination of heavy molecular weight components in the lubricating oil range and mid molecular weight components that chromatograph as an irregular pattern of peaks on top of an unresolved complex mixture. Client ID Lab ID Infiltrator Clean Out 0804111-01 BG 6A CB 2631 0804111-05 The following samples have GC/FID characteristics which is similar to a combination of heavy molecular weight components in the lubricating oil range, mid molecular weight components that chromatograph as an irregular pattern of peaks on top of an.unresolved complex mixture,and low molecular weight resolved peaks in the C7-C10 range. Client ID Lab 1D BG-I cp 0804 1 1 1-02 BG-2 shep 0804 1 1 1-03 MH=1 0804111-04 The following samples have GC/FID characteristics which*is similar to heavy molecular weight components in the _ lubricating oil range. Client ID Lab ID Stockpile 0804111-06 Raw Product 0804111-07 The enclosed results of analyses are representative of the samples as received by the laboratory. Alpha Analytical makes no representations or certifications as to the method of sample collection, sample identification, or transporting/handling procedures used prior to the receipt of samples by Alpha Analytical.To the best of my knowledge,the information contained i 0;IReporlWARRTEMP420081Wpha10804111.doc Alpha Analytical, 320 Forbes Blvd.,Mansfield,MA 02048,508-822-9300 3 of 45 y in this report is accurate and complete. For any questions regarding this report, please contact the signatory below at 508- 822-9300. Approved by: OUI-16-7• Title: TU!�fMt— l Date: ! F4izabeth Porta Forensic Manager U O:IReporlWARRTEbfPI2008UIpha108041I Ldoc Alpha Analytical, 320 Forbes Blvd.,Mansfield,MA 02048,508-822-9300 4 of 45 Total Petroleum Hydrocarbons By 'GC/FID 5ous �i e• Form I Total Saturated Hydrocarbons by GC/FID Client: Alpha Analytical-Westborough Lab Code: MA00030 >t° Project: L0805617-PRIME ETR: 0804111 P''�® Client 1D: Infiltrator Clean Out LAID: 0804111-01 A N•nv r i c A t_Case: N/A SDG: N/A Associated Blank: TSO42508B06 Matrix: Sediment Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution Collected Received Extracted Analyzed Percent Solid Amount(g) Volume(ml) Factor Analyst 04/17/08 04/22/08 04/25/08 04/30/08 76.1 30.56 28.57 l NLJr Parameter Result Total Petroleum Hydrocarbons(C9-C44) 569 N/A-Not Applicable Acceptance Surrogate %Recovery Range(%) ortho-Terphenyl 73 50-130 00-Tetracosane 62 50-130 6 of 4 oiw 16:48 320 Forbes Blvd, Mansfield, Mil 02048, (508)822-9300, Fax(508)822-3288 i File :0:\Forensics\Data\FID6\APR08\APR28.SEC\A63392.D Operator NI.Jr Acquired 30 Apr 2008 10:03 pm using AcgMethod FID6A.M Instrument FID6 Sample Name: 0804111-01 Misc Info : 1X Vial Number: 88 ..........................---- ....._. --- ...--............. - ......_ ..,.. ...-._. . _.__..--............................. ---.. ..... ................................. _.......-.......................................--._............. .. ........_.. _ _. ..... ..... .... .... Response_ .. Signal:A63392.D\FID2B.CH i 450000 400000 350000 I I 300000 I i 250000 200000 i 150000 100000 50000 Cyl t--j L,,�- U-0 a-rrrl-r-rrrT'-^Tr�T'-1-r'-rT' Time _____ _ _5_00_—___10.00__ _15:00 20.00 .-.. 25.00 30:00 35.00 40.00 45.00 50.00 55.00 _60A0 _ 65.00 70.00 __ 75_00 _ 80 00 r Form I Total Saturated Hydrocarbons by GOOD Client: Alpha Analytical- Westborough Lab Code: MA00030 Project: L0805617-PRIME ETR: 0804111 Client ID: BG-1 cp Lab ID: 0804111-02 n.ry 5 r c A LCase: N/A SDG: N/A Associated Blank: TSO42508B06 Matrix: Soil Concentration Units: mg/Kg Date Date I Date Date Sample Final Dilution Collected Received Extracted Analyzed �PercentSolidlAmount(g) Volume(ml) Factor Analyst 04/17/08 04/22/08 04/25/08 04/30/08 95.4 30.10 1.03 1 NLJr Parameter Result Total Petroleum Hydrocarbons(C9-C44)_ 30.1 N/A-Not Applicable Acceptance Surrogate %Recovery Range(%) ortho-Terphenyl 85 50-130 d50-Tetracosane 84 50-130 8 of 4050110816:57 320 Forbes Blvd, Mansfield,MA 02048, (508)822-9300, Fax(508)822-3288 File :0:\Forensics\Data\FID6\APROB\APR28.SEC\A63394 .D Operator NLJr Instrument FID6 Sample Name: 0804111-02 Misc Info Ix Vial Number: 89 Signal:A63394.DXFID2B.CH 2400000 2200000 2000000 1800000 1600000 1400000 1200000 1000000 800000 600000 � 400000—_ C Form I Total Saturated Hydrocarbons by GC/FID Client: Alpha Analytical-Westborough Lab Code: MA00030 Project: L0805617-PRIME H ETR: 0804111 - Client ID: BC-2 steep Lab ID: 0804111-03 A'lVbA ,L;,Yj r i c ACase: N/A SDG: N/A Associated Blank: TSO42508BO6 Matrix: Soil Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution Collected Received Extracted Analyzed Percent Solid Amount(g) Volume(ml) Factor Analyst 04/17/08 04/22/08 04/25/08 05YO1/08 89.6 30.42 1.03 1 NLJr Parameter Result Total Petroleum Hydrocarbons(C9-C44) 26.6 N/A-Not Applicable Acceptance Surrogate %Recovery Range(°a} ortho-Terphenyl 86 50-130 d50-Tetracosane 85 50-130 10 of 4 501/08 16:58 320 Forbes Blvd,Mansfield, MA 02048, (508)822-9300, Fair(508)822-3288 I Y File :0:\Forensics\Data\FIDE\APR08\APR28.SEC\A63396.D Operator NLJr Acquired 01 May 2008 1:21 am using AcgMethod FID6A.M Instrument FID6 Sample Name: 0804111-03 Misc Info : 1X Vial Number: 90 Response_ Signal.A63396.D1FID2B.CH.. 1500000 1400000 1300000 i 1200000 1100000 I 1000006 900000 i 800000 700000 600000 500000 400000 ' I 30000.0 i 200000 100000 CP Time 5.00 10.00 15.00 20.00 25.00 30.00 35.00 40.00 45.00 50.00 _ _5_5.00 _ 60_00 _65:00 70_00 75.00 B0.00 85.00 f Form I Total Saturated Hydrocarbon's by GUND Client: Alpha Analytical-Westborough Lab Code: MA00030 805617-PRIME L Project: 0 ETR: 0804111 ■ �p � A Client ID: MH-1 Lab ID: 0804111-04 a�tiA z `ter + c A LCase: NIA SDG: N/A Associated Blank: TSO425081306 Matrix: Soil Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution Collected I Received Extracted Analyzed Percent Solid Amount(g) Volume(ml) Factor Analyst 04/17/08 I 04/22/08 04/25/68 1 05/01/08 i 88.8 I 30.12 1.74 1 NLJr Parameter Result Total Petroleum Hydrocarbons(C9-C44) 60.4 N/A-Not Applicable Acceptance Surrogate %Recovery Range(%) ortho-Terphenyl 88 50-130 d50-Tetracosane 85 50-130 12 of 45o1/o816:59 320 Forbes Blvd, Mansfield, kL4 02048, (508)822-9300, Fax(508)822-3288 i File :0: \Forensics\Data\FIDE\APR08\APR28.SFC\A63398.D Operator NLJr Acquired 01 May 2008 2:59 am using AcgMethod FID6A.M Instrument FID6 Sample Name: 0804111-04 Misc Info : 1X Vial Number: 91 ........ ..-----.._.... . .....-.._.._._...... --... ..-.--... _.-___._............................... .- -----. -....-..................... _ .......,......_........_.--..................................._..._......_...--...... _ . ...........Respo�se_ Signal:A63398D1FID2BCH ..,...... ! 2000000 i 1800000 1600000 i f j 1400000 ! 1200000 1000000 4 800000 600000 400000 W 200000 � � I j T- . ime 5.00__ __ _ 10.00 ..............00„_ _ 20.00 25.00 30.00 35.00 40.00 45.00 50.00 55.00 60.00 65.00 70.00 75.00 80.00 85.00 Form I Total Saturated Hydrocarbons by GC/FID Client: Alpha Analytical -Westborough Lab Code: MA00030 Project: L0805617-PRIME ETR: 0804.111 HA Client ID: BG 6A CB 2631 Lab ID: 0804111-05 s►;N n.... i c -4 Case: NIA SDG: NIA -- Associated Blank: TSO425081306 Matrix: Soil Concentration Units: mg/Kg Date Date I Date Date Sample Final Dilution Collected Received I Extracted Analyzed I Percent Solid Amount(g) Volume(ml) Factor Analyst 04/18/08 04/22/08 ' 04/25/08 05/01/08 41.4 36.60 37.04 1 NLJr Parameter Result Total Petroleum Hydrocarbons C9-C44 4460 NIA-Not Applicable Acceptance Surrogate %Recovery Range(%) ortho-Terphenvl 76 50-130 d50-Tetracosane 56 50-130 14 of 4501/0B 17:00 320 Forbes Blvd, Mansfield A14 02048, (508)822-9300, Fwc(508)822-3288 File :0: \Forensics\Data\FIDE\APR08\APR28.SEC\A63400.D Operator NLJr Acquired 01 May 2008 4:37 am using AcgMethod FID6A.M Instrument FID6 Sample Name: 0804111-05 Misc Info : 1X Vial Number: 92 --------............ .....-----._._.._..__-....._..-, Re Signal:A63400.DW102B.CH 2400000 2200000 2000000 ' 1800000 ' 1600000 i 1400000 1200000 • i 1000000 800000 600000 EE 1 400000 ' 0 200000 � J �� 1 'Vd nti t -LiAAJJ Time 5.00 10.00 16.00 20.00 25.00 30.00 35.00 40.00 45.00 50.00 56.00 60.00 65.00 70.00 75.00 80.00 85.00 i Form I Total Saturated Hydrocarbons by GC/FID Client: Alpha Analytical-Westborough Lab Code: MA00030 Project: L0805617-PRIME ETR: 0804111 Client ID: Stockpile Lab 1D: 0804111-06 Case: N/A SDG: N/A Associated Blank: TSO42508B06 Matrix: Soil Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution Collected Received Extracted Analyzed Percent Solid Amount(g) I Volume(ml)I Factor Analyst 04/18/08 04/22/08 04/25/08 05/01/08 95.8 30.04 1 200 1 NLJr Parameter Result Total Petroleum Hydrocarbons(C9-C44) 22300 i N/A-Not Applicable Acceptance Surrogate %Recovery Range(%) ortho-Terphenyl 118 50-130 d50-Tetracosane 102 50-130 16 of 4C601/0817:04 320 Forbes Blvd, Mansfield, MA 02048, (508)822-9300, Fax(508)822-3288 File :0:\Forensics\Data\FIDE\APROB\APR28.SEC\A63402.D Operator NLJr Acquired 01 May 2008 6: 15 am using AcgMethod FID6A.M Instrument FID6 Sample Name: 0604111-06 Misc Info : 1X Vial Number: 93 Response_ ..............._........._....._,....._..........................._................... ....._...._...............-.......Signal:�Afi3402.D\FID2....... .......,.,__.,...__...__._......_..__-.---..._._.-..________.-_...._.__._._..._....__........_.............___..._......._,......._....................,__--_ .._....___...__: B.CH 1300000 I 1200000 t 1100000 1000000 ' � I 900000 800000 700000 600000 500000 i 400000 300000 �Ili"Yfr'� { a�zoa000 �1r 0 100000 rim-r-r rr-�-•*--�f�-�-r-r-r-�rrrr- Time 5.00 10.00 15.00 20.00 25.00 30.06 35.00 40.00 45:00,,. 50.00 55.00 60.00 65.00 70-00 75.00 80.00 85.00 i Form I Total Saturated Hydrocarbons by GOFID Client: Alpha Analytical-Westborough Lab Code: MA00030 Project: L0805617-PRIME ETR: 0804111 HA Client ID: Raw Product Lab ID: 0804.111-07 A�1J fC r r + c A Case: NIA SDG: N/A Associated Blank: TO0429081308 Matrix: Product Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution Collected Received Extracted Analyzed Percent Solid Amount(g) Volume(ml) Factor Analyst 04/18/08 04/22/08 04/29/08 04/30/08 100 0.1088 20 1 NLJr Parameter Result Total Petroleum Hydrocarbons C( 9-C44) 1000000 I i N/A-Not Applicable Acceptance Surrogate %Recover,,, Range(%) ortho-Terphenyl 92 50-130 d50-Tetracosane 99 50-13 0 18 of 4601108 16:47 320 Forbes Blvd, Mansfield, MA 02048, (508)822-9300, Fax(508)822-3288 File :0: \FORENSICS\DATA\FIDE\APR08\APR28.SEC\A63370.D i Operator NLJr Acquired . 30 Apr 2008 3:55 am using AcgMethod FID6A.M Instrument FID6 Sample Name: 0804111-07 Misc Info : 1X Vial Number: 77 ................ .... _ ... .... ...........__.._.....-.............-.. .._. ., Response_.............. ..... . ._.. ...._-_ ..... ... .......... .. Signal:A63370.D1FID28.CH i i 2800000 I 2600000 2400000 2200000 2000000 i 1800000 i i .1600000 1400000 1200000 1000000 I 800000 II7rA'��d 600000I�f'Yr'",�i��; 400000 C � 200000 ,fit Time 5.00 10.00 15.00 20.00 25.00 30.00 35.00 40.00 45.00 50.00 55.00 60.00 65.00 70.00 75.00 80.00 85.00 Form I Total Saturated Hydrocarbons by GGFID Client: Alpha Analytical-Westborough Lab Code: MA00030 HAProject: L0805617- PRIME ETR: 0804111 Client ID: Blank Lab ID: TSO42508B06 !►.N;n,L Yf T f CA L Case: NIA SDG: N/A Associated:Blank: NIA Matrix: Soil Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution Collected Received Extracted Analyzed Percent Solid Amount(g) Volume(ml) Factor Analyst N/A N/A 04/25/08 04/30/08 100 30.00 1 1 I NLJr Parameter Result Total Petroleum Hydrocarbons(C9-C44) 1.10 U N/A-Not Applicable Acceptance U-The anal}4e was analyzed for but not detected at the sample specific Surrogate %Recovery Range /o 'level reported. ortho-Terphenyl r85 50-130 d50-Tetracosane 83 50-130 20 of 4@01f0816:47 320 Forbes Blvd, Mansfield, MA 02048, (508)822-9300, Fax(508)822-3288 File :0:\Forensics\Data\FIDE\APR08\APR28.SEC\A63386.D r Operator NLJr Acquired 30 Apr 2008 5:08 pm using AcgMethod FID6A.M Instrument FID6 Sample Name: TSO42508B06 Misc Info : 1X ETR 0804111, 122, 129 & 130 Vial Number: 85 Response_ _.. __............. ....... _ ._.. -._----- .... ... Signal:A63386.D1FID2B.CH I 2600000 Internal Standard Surrogate . I 2400000 2200000 I 2000000 1800000 i i 1600000 I 1400000 Surrogate 1200000 i 1000000 800000 � I 600000 i 400000 I 200009 un Time 5.00 10.00 15.00 20.00 25.00 30.00 35.00 40.00 45.00 50.QQ 55.00 60.00 65.00 70.00 75.00 80.00 85.00 I r Form I Total Saturated Hydrocarbons by GUND Client: Alpha Analytical-Westborough Lab Code: MA00030 HA Project: L0805617 -PRIME ETR: 0804111 Client ID: Blank Lab ID: T0042908BOS Case: N/A SDG: NIA Associated Blank: N/A Matrix: 'Product Concentration Units: mg/Kg Date Date Date Date Sample Final I Dilution Collected Received , Extracted Analyzed iPercentSolid� Amount(g) Volume(mi)l Factor Analyst N/A N/A 04/29/08 04/29/08 100 0.10 1 1 NLJr Parameter Result Total Petroleum Hydrocarbons(C9-C44) 330 U N/A-Not Applicable Acceptance U-The analyte was analyzed for but not detected at the sample specific Surrogate %Recovery Range(% level reported. ortho-Terphenyl 91 50-130 d50-Tetracosane 91 50-130 22 of 46oUos 16:47 320 Forbes Blvd, Mansfield, MR 02048, (508)822-9300, Fax(508)822-3288 i File. II :0.:\Forensics\Data\FIDE\APR08\APR28.SEC\A63364.D Operator NLJr Acquired 29 Apr 2008 10:58, pm using AcgMethod FID6A.M Instrument FID6 - Sample Name: T0042908808 Misc Irifo : 1X ETR 0804111, 114, 136 & 149 Vial Number: 74 __._........ ............ .........................__._......... .......__ Rsp _.................. . ......- _..._............._._..... . . .eonse_ Signal:A63364.DiFID2B.Cli � 2600000 Surrogate i Internal Standard 2400000 . I 2200000 i 2000000 1800000 i 1600000 i 1400000 Surrogate 1200000 1000000 800000 I 600000 i N 400000 W I i O 200000 cn Time, 5..00-.__.- _ 10.00 15,00 20.00 25.00 30.00 35.00 40.00 45.00 50.00 55.00 60.00 65.D0 T0,00 75.D0 80.00 85.00 __.............._....................-.......... .. .........__.__................_._.--...........----_-...__...-..._......_......__..._ -..... .-----..,...--.--.........._...-.__.-._.._._...._....-................._...__._........ _...__............__......___......._..__......._..__._......__..._.._.-_-.------ _ ...- - --...-._.........._._..._....._...-.___......._..._._.........._...._._.._...... Form III Spike Recovery Summary Total Saturated Hydrocarbons by GC/FID Client: Alpha Analytical-Westborough Lab Code: MA00030 Project: L0805617-PRIME ETR: 0804111 HA Client ID: Laboratory Control Sample Lab ID: See Below n-nr n r.T + c A LCase: N/A SDG: N/A Associated.Blank: TSO42508B06 Matrix: Soil Concentration Units: mg/Kg Date Collected Date Received Date Extracted Percent Solid Analyst N/A N/A 04/25/08 100 l NLJr Lab ID: TSO42508B06 TSO42508LCSOI TSO42508LCSDOI Blank LCS LCSD RPD % Recovery Parameter Conc. Conc. %Recovery Conc. %Recove % RPD Limit Limits n-Nonane(9) 0.0333 U 1.22 73 1.32 79 8 30 50-130 n-Decane C10 0.0333 U 1.32 79 1.38 83 4 30 50-130 n-Dodecane(C 12) 0.0333 U 1.46 88 1.43 86 2 30 50-130 n-Tetradecane C14 0.0333 U 1.49 89 1.43 86 4 30 50-130 n-Hexadecane C16 0.0333 U 1.50 90 1.52 91 1 30 50-130 n-Octadecane(C18) 0.0333 U 1.54 93 1.56 94 1 30 50-130 n-Nonadecane(C19) 0.0333 U 1.52 91 1.54 92 1 30 50-130 n-Eicosane(C20) 0.0333 U 1.54 93 1.60 96 3 30 50-130 n-Docosane C22 0.0333 U 1.61 96 1.63 98 1 30 50-130 n-Tetracosane C24 0.0333 U 1.55 93 1.58 95 2 30 50-130 n-Hexacosane(C26) 0.0333 U 1.55 93 1.57 94 1 30 50-130 n-Octacosane C28 0.0333 U I 1.48 89 1.49 89 1 30 50-130 n-Triacontane C30 0.0333 U 1.46 88 1.47 88 0 30 50-130 n-Hexatriacontane(C36) 0.0333 U 1.50 90 1.46 88 2 30 -50-136 N/A-Not Applicable Acceptance U-The analyse was analyzed for but not detected at the sample specific Surrogate %Recovery Range( level reported. ortho-Terphenyl 89 89 50-130 d50-Tetracosane 86 88 50-130 Concentrations reported as calculated values,which includes rounding for significant figures. Percent recoveries and RPD values are calculated from the unrounded result. 24 Of 4(&01108 16:51 320 Forbes Blvd, Mansfield MA 02048, (508)822-9300, Fax(508)822-3288 e Form I Total Saturated Hydrocarbons by GOOD Client: Alpha Analytical-Westborough Lab Code: MA00030 HAProject: L0805617-PRIME ETR: 0804111 Client 1D: Laboratory Control Sample Lab ID: TSO42508LCSOI Case: NIA SDG: N/A Associated Blank: TSO425081306 Matrix: Soil Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution ! k Collected Received Extracted Analyzed Percent Solid Amount(g) Volume(ml) Factor Analyst N/A N/A 04/25/08 04/30/08 100 30.00 [ I 1 N l Parameter Result Total Petroleum Hydrocarbons(C9-C44) 22.3 N/A-Not Applicable Acceptance Surrogate %Recovery Range(%) ortho-Terphenyl 89 50-130 d50-Tetracosane 86 50-130 25 of 46olm 16:48 320 Forbes Blvd, Mansfield, MA 02048, (508) 822-9300, Fax(508)822-3288 I File :0: \Forensics\Data\FIDE\APR08\APR28.SEC\A63388.D Operator NLJr Acquired 30 Apr 2008 6:47 pm using AcgMethod FID6A.M Instrument : FID6 Sample Name: TSO42508LCS01 Misc Info : 1X ETR 0804111, 122, 129 & 130 Vial Number: 86 ......::.:.:.....-- ...................._..-..__.. --------..._.._........... ....__.._...... --_......._... - - .._....................._._...---- .--.-.... -............._....__..._.................--- - __...__._._... _....... _. ..._.....__ ._. ....__........_ . . Response_ Signah A63388.D\FID2B.CH 5500000 5000000 4500000 - I 4000000 I 3500000 3000000 2500000 i 2000000 1500000 I i 1000000 1 N q 500000 4. CT Time 5 00 10.00 15.00 20.00� 25.00�_ 30A0 35.00 40 00 - 45_00__ 50_00_ 55.00 60.00 65.00 70.00-" �75 00- 80.00 85.00 Form I Total Saturated Hydrocarbons by GOOD Client: AIpha Analytical-Westborough Lab Code: MA00030 " Project: L0805617-PRIME ETR: 080411t HA Client 1D: Laboratory Control Sample Dup Lab ID: TSO42508LCSD01 A3r.......T r C A LCase: NIA SDG: N/A Associated Blank: TSO425081306 Matrix: Soil Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution Collected Received Extracted Analyzed Percent Solid Amount(g) I Volume(ml) Factor Analyst N/A N/A I 04/25/08 04/30/08 100 30.00 1 1 NLJr Parameter Res u It Total Petroleum Hydrocarbons(CO-C44 22,6 i N/A-Not Applicable Acceptance Surrogate %Recovery Range(%) ortho-Terphenyl 89 50-130 d50-Tetracosane 88 50-130 j 27 of 4)5D 1/08 16:48 320 Forbes Blvd,Mansfield,MA 02048, (508)822-9300, Fax(508)822-3288 I File :0: \Forensics\Data\FIDE\APROB\APR28.SEC\A63390.D Operator NLJr Acquired 30 Apr 2008 8:25 pm using AcgMethod FID6A.M Instrument , FID6 Sample Name: TSO42508LCSDO1 Misc Info : 1X ETR 0804111, 122, 129 & 130 Vial Number: 87 -.:_.,_......_._................................_...__......................_.._._..._..............._.__._. Response_ Signal:A63390.D1FID2B.CH I 5500000 i 5000000 i I 4500000 i I i 4000000 3500000 3000000 i 2500060 i 2000000 1 1 1500000 I 1000000 0 I 0 500000 Cn i Time .................. , 5.00 MOO 15.00 20.00 25.00 30.00 35.00 40.00 45.00 50.00 55.00 60.00 65.00 70.00 75.00 80.00 85.00 r i Form III Spike Recovery Summary Total Saturated Hydrocarbons by GC/FID y; Client: Alpha Analytical- Westborough Lab Code: MA00030 rA H-AProject: L0805617-PRIME ETR: 0804111 Client ID: Laboratory Control Sample Lab ID: See Below I1 lY.A r c A 'Case: N/A SDG: N/A Associated Blank: T0042908B08 Matrix: Product Concentration Units: mg/Kg Date Collected Date Received Date Extracted Percent Solid Analyst N/A N/A 04/29/08 100 NLJr Lab ID: T0042908B08 T0042908LCS07 T0042908LCSD06 Blank LCS LCSD RP D %Recovery Parameter Conc. Conc. %Recovery Conc. %Recove %RPD Limit Limits n-Nonane C9 10.0 U 487 97 1 486 97 1 0 30 50-130 n-Decane(C 10) 10.0 U 1 465 93 1 463 93 1 0 1 30 50-130 n-Dodecane(C1 10.0 U 1 478 96 1 476 95 ( 0 1 30 50-130 n-Tetradecane(C14) 10.0 U 1 478 96 1 480 96 1 30 50-130 n-Hexadecane(C 16) 10.0 U 1 496 99 1 483 97 3 30 50-130 n-Octadecane(C18) I0.0 U 490 98 1 494 99 1 30 50-130 n-Nonadecane C19 10.0 U 481 96 486 97 1 30 50-130 n-Eicosane C20 10.0 U 499 100 504 101 1 30 50-130 n-Docosane(C22) 10.0 U 505 101 509 102 1 30 50-130 n-Tetracosane C24 10.0 U f 492 98 497 99 1 30 50-130 n-Hexacosane C26 10.0 U 490 98 496 99 1 30 50-130 n-Octacosane C28 10.0 U 467 93 472 95 1 30 50-130 n-Triacontane(C30) 10.0 U 461 92 466 93 1 30 50-130 n-Hexatriacontane C36 10.0 U 467 93 468 94 0 30 50-130 I N/A-Not Applicable Acceptance U-The analyte was analyzed for but not detected at the sample specific Surrogate %Recovery Range(N). level reported. ortho-Terphenyl 93 93 50-130 d50-Tetracosane 92 92 50-130 Concentrations reported as calculated values,which includes rounding for significant figures. Percent recoveries and RPD values are calculated from the unrounded result. 29 Of 46ou08 16:50 320 Forbes Blvd,Mansfield, MA 02048, (508)822-9300,Fax(508)822-3288 f Form I Total Saturated Hydrocarbons by GC/FID :x Client: Alpha Analytical-Westborough Lab Code: MA00030 A Project: L0805617- PRIME ETR: 0804111 �x Client ID: Laboratory Control Sample Lab ID: T0042908LCS07 a nr n;L Y,r i c A `Case: N/A SDG: NIA Associated Blank: T004290819108 Matrix: Product Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution Collected Received Extracted Analyzed Percent Solid Amount(g) Volume(ml) Factor Analyst N/A N/A 04/29/08 04/30/08 100 0.10 1 l NLJr Parameter Result Total Petroleum Hydrocarbons(C9-C44) 7090 N/A-Not Applicable Acceptance Surrogate %Recovery Range(%) ortho-Terphenyl 93 50-130 d50-Tetracosane 92 50-130 30 of 4`&01/0816:47 320 Forbes Blvd, Mansfield,MA 02048, (508)822-9300, Fax(308)822-3288 File :0:\Forensics\Data\FIDE\APR08\APR28.SEC\A63366.D Operator NLJr Acquired 30 Apr 2008 12:37 am using AcgMethod FID6A.M Instrument FID6 Sample Name: T0042908LCS07 Misc Info : 1X ETR 0804111, 114, 136 & 149 Vial Number: 75 _ .._... _ ........................ ._ . ... ....... .... ... _ .._........._.............__ ..._. .... ._.......... --- _. . Response_ Signal.A63366.0T102B.CH -- i j 5500000 5000000 j 4500000 i 4000000 ' i 3500000 I 3000000 ` i i 1 . 2500000 i 2000000 i • I 1500600 j 1000000 O ~` 500000 I A V1 I - I Yime _ _ +_ 5_00_.____10_00 _15.00 __20.00�_ 25.00_____ 30.00 _35_00_ 40A0 _ 45400_____50.00____ _55.00 ;_60.000_._._._65.00 70.00 75.00 ___80.00 85.00 _j Form I Total Saturated Hydrocarbons by GOFID Client: : Alpha Analytical-Westborough Lab code: MA00030 HAProject: L0805617-PRIME ETR: 08041I t Client ID: Laboratory Control Sample Dup Lab ID: T0042908LCSD06 ANA f c A lCase: N/A SDG: N/A . Associated Blank: T0042908B08 Matrix: Product Concentration Units: mg/Kg Date Date Date Date Sample Final Dilution Collected Received Extracted Analyzed Percent Solid Amount(g) Volume(ml)I Factor Analyst N/A N/A 04/29/08 04/30/08 100 0.10 1 1 _ NLJr Parameter Result Total Petroleum Hydrocarbons(C9-C44) 7150 N/A-Not Applicable Acceptance Surrogate %Recovery Range(%) ortho-Terphenyl 93 50-130 d50-Tetracosane 92 50-130 32 of 4(60110316A7 320 Forbes Blvd, Mansfield.MA 02048, (508)822-9300, Fax(508)822=3288 t, • Fils :0:\Forensics\Data\FIDE\APR08\APR28.SEC\A63368.D Operator NLJr . Acquired 30 Apr 2008 2:16 am using AcgMethod FID6A.M Instrument FID6 Sample Name: T0042908LCSD0.6 Miss Info : 1X ETR 0804111, 114, 136 & 149 Vial Number: 76 ............... .... ....... ................ .. _..... . .---.._...._.-..._.......-.----...-.._..._...-...... ..-......- . .. ..Response Res onse .__.6 _68_...FI ......... _ P Signal:A63368.D1FID28.CH .-_•....-____.......-....---.__...-.--- . ...._._.............................. ...... I 5500000 i i 5000000 j i 4500000 I l 4000000 i 3500000 I 300000D 2500000 2000000 i 1500000 j j 1000000 w w' 0 �j 500000 i cri 'time 5.00 10.00 15.00 20.00 25.00 30.00 35.00 40.00 45.00 50.00 55.00 60.00 65.00 70.00 75.00 80.00 85.00 • I I Petroleum Reference Standards 34 of 45 Quantitation Report (QT Reviewed) Data Path 0:\Forensics\Data\FIDE\APR08\APR28.SEC\ Data File A63404.D Signal(s) FID2B.CH Acq On 01 May 2008 7:54 am Operator NLJr Sample C6042803R Misc CC ALS Vial 94 Sample Multiplier: 1 Integration File: SHCINT2.E Quant Time: May 01 14:40:26.2008 Quant Method 0:\FORENSICS\METHODS\FID6\HC61221R.M Quant Title FID Forensics QLast Update Thu May 01 14:29:30 2008 Response via Initial Calibration Integrator•: ChemStation 6890 Scale Mode: Large solvent peaks clipped Volume Inj . 1.0 Signal Phase Rtx-5MS Signal Info 0.25mm Compound R.T. Response Conc Units Internal Standards 1) I 5-alpha-androstane 30.55 57675325 50.000 ug/mLm System Monitoring Compounds 19) s ortho-terphenyl 28.57 60459876 48.930 ug/mLm Spiked Amount 50.000 Range 50 - 130 Recovery ' = 97.86% 24) s d50-Tetracosane 35.25 51861173 48.258 ug/mL Spiked Amount 50.000 Range 50 - 130 Recovery = 96.52% Target Compounds 2) t n-Octane (C8) 5.21 48155852 49.979 ug/mLm 31 t n-Nonane (C9) 7.34 50397321 49.541 ug/mL 4) t n-Decane (C10) 9.78 50683907 48.623 ug/mL 5) t n-Undecane (Cll) 12.27 51996687 50.443 ug/mL 6) t n-Dodecane (C12) 14.68 53341224 50.690 ug/mL 7) t n-Tridecane (C13) 16.97 53734885 50.553 ug/mL 9) t n-Tetradecane (C14) 19.14 54233923 50.514 ug/mi, 11) t n-Pentadecate (C15) 21.20 54473590 50.385 ug/mL 12) t n-Hexadecane (C16) 23.15 53942689 49.925 ug/mL 14) t n-Heptadecane (C17) 25.00 51972843 47.613 ug/mLm 15) t Pristane 25.11 57248728 50.864 ug/mL 16) t n-Octadecane (C18) 26.76 55320838 50.543 ug/mL 17) t Phytane 26.92 56529529 51.230 ug/mL 18) t n-Nonadecane (C19) 28.44 55873331 51.412 ug/mL 20) t n-Eicosane (C20) 30.03 56308859 51.596 ug/mLm 21) t n-Heneicosane (C21) 31.56 56538259 50.610 ug/mL 22) t n-Docosane (C22) 33.03 56569068 52.776 ug/mL 23) t n-Tricosane (C23) 34.44 56983820 51.347 ,ug/mL 25) t n-Tetracosane (C24) 35.79 57378489 51.630 ug/mL 26) t n-Pentacosane (C25) 37.08 56963733 50.868 ug/mL 27) t, n-Hexacosane (C26) 38.34 57180664 50.812 ug/mL 28) t n-Heptacosane (C27) 39.54 56304754 50.946 ug/mL 29) t n-Octacosane (C28) 40.71 56843173 49,890 ug/mL 30) t n-Nonacosane (C29) 41.83 56916866 49.763 ug/mL 31) t n-Triacontane (C30) 42.92 58301629 51.975 ug/mL 32) t n-Hentriacontane (C31) 43.98 57021179 50.986 ug/mL 33) t n-Dotriacontane (C32) 45.00 55380523 50.802 ug/mLm 34) t n-Tritriacontane (C33) 45.99 55418626 50.000 ug/mLm 35) t n-tettatriacontane (C34) 46.95 55791510 49.922 ug/mLm 36) t n-Pentatriacontane (C35) 47.97 53963511 50.505 ug/mL 37) t n-Hexatriacontane (C36) 49.13 56811969 50.361 ug/mL 38) t n-Hentatriacontane (C37) 50.46 54492973 48.344 ug/mL 39) t n-Octatriacontane (C38) 52.01 55519461 50.648 ug/mL 41) t n-Tetracontane (C40) 55.95 55600548 50.405 ug/mLm 35 of 45 HC61221R.M Thu May 01 14:32:31 2008 Page: 1 File . :0: \Forensics\Data\FIDE\APR08\APR28.SEC\A63404.D Operator NLJr Acquired 01 May 2008 7:54 am using AcgMethod FID6A.M Instrument FID6 Sample Name: C6042803R Misc Info : CC Vial. Number: 94 _.._Re -.--- __-- sponse_ . _.._.._ -Signal:A63404.D1FID2B.CH �� 1 5500000 i 5000000 i 4500000 4000000 I 3500000 3000000 2500000 i i i 2000000 1500000 1000000 G•> Gn � h 500000 4r i :Time 5.00 10.00 15.00 20.00 25.00 30.00 35.00 40.00 45.00 50.00 55.00 60.00 65.00 70.00 75.00 80.00 85.00 r, Iw I File :0:\Forensics\Data\PAH1\January06\JAN23.SEC\Pl7717.D Operator AC Acquired 24 Jari 2006 9:00 am using AcgMethod FRNCID.M Instrument PAH-1 Sample Name: R1012310-AFID Misc' Info : 50W Motor Oil ID: WHAC35 Vial Number: 64 esponse Signal:P17717.D1FID2B.CH 3400000 3200000 3000000 2800000 2600000 2400000 2200000 2000000 1800000 1600000 1400000 1200000 1000000 800000 6C0000 4C0000 O 2C0000 rime __. 5.00 10.00 15.00 20.00 25.00 30.00 35.00 40.00 45.00 50.00 55.00 60.00 65.00 70.00 75.00 i Chain of Custody Records 38 of 45 ,v Rip ��F• `� rr F���`6";°t��r�CHAlN OF CUSTODY �� �.: .r �PAGEOF ,`�fr n aLat} 1� :ALPH*A"" ••ob�ep # f 1ii� ' ,1NKrnc,u r�.i.i{Ia r'' •At$:~'H;_�, � ROM ...-.FAS'��R -... WESTBORO,MA MANSFIELD,MA Project Information •• • • Data Deliverables Billing Information TEL:508-896-9220 TEL:508.822-9300 " FAX:508.898-9193 FAX:Sos•sz2-32ee Project Name: ❑FAX ❑EMAIL ❑Same as.Client into PO#: • Project Location:. ❑ADEx ❑Add'I Deliverables Client: { Project#: Requirement s/Report Limits L State/Fed Program Criteria Address: Project Manager: G ALPHA Quote MA MCP PRESUMPTIVE CERTAINTY--CT REASONABLE CONFIDENCE -• • • Phone: i es ❑No Are,MCP Analyticat.Methods Required? Fax: ❑Yes ❑No Are CT,RCP(Reasonable Confidence Protocols)Required? tandard ❑RUSH(onryconllmedllproamrovoml Email: 'Date Due: fUC/ Time: *y� SAMPLEPLEHANOLING ❑ These samples have been previously.analyzed by Alpha I Qb Yr:�c� FJJtr Other Project Specific.Requirements/Comments/Detection Limits:. ❑Done ❑Not needed ❑Lab to do bra' Preservation ❑Lab to do (Pleaso epeclty below) )ALPHA Lab;la� t Collection" Sample Sampler's ,x(LabUse Only)'r r' Sample ID Matrix Initials / Sample S .,,v,.,.,,..,,,,•� .,,._ . -•- Date Time. pacific Comments qIn Iff. fed M� iti1'r-f;! F y57iyt� 4 :�-f�i, •+ice. �t _ War, b .�.}gib ,����:��. �•�� rr M SGA•R"b'yS rlwe X'k}a ri YT Vf'LTtSI-��N'' fit PLEASE ANSWER QUESTIONS ABOVEI GontainerTypePleaseprintclearlyleglbly,and{? + F.dY,•J > rJf} ( •F Y i (71 cdmpletelySampies2can not bea,�' IS YOUR PROJECT Preservative ry.r , .0 IOggedlln andturftazound time do", Relinquished By: DateTme a ived 8y: DateTme ,�W116r �tafr3�t;Lu"�flllany_InambIguities are; MA MCP or CT RCP? G}, re"sblved��'All samples sutsmrtted�arex 41F4. !� '�subtect'to Alpha s�P�ymeritif�rms�k` FOfiA4N0:01-01 rev.30JUL-07 .EB feVefS�SIdB�li Ys� 1.aa�{{ {. CHAIN OF CUSTODY PAGE_ -OF .,a , , 4 'fHii•'. ���� �'�i�..S'. ___{{{t 1. o . VUESTaORO,MA MANSRELD•MA - • • • `.• • • • - TEL 508-890.9220 TEL 50"22.9300 FAX 50"ga-9193 FAX soe.822,3=ee I Project Name: �� � ^ ❑FAX ❑EMAIL D Same as Client Info J PO a: f O ADEx O Add9 Deliverables — -----' Project Location:L[Jer f_ nS�n Client: �p Project*: 1�-1194j0� RegulatoryRequirements/Report Address: ^� State/Fer! Program Criteria P.O. a ,1,+ ,Q Project Managers e- ,�+er+ � ALPHA Quote Phone: 00'rP O Yes CI No Are MCPAnalytical Methods Required? Fax: S�� 9 y � ,f O Yes O No Are CT RCP(Reasonable CoMidence Protocols)Required? Email: )d Standard CI RUSH »enp.e •op - 5 z�151em=CiQ 005ate Duo: Time: ❑ These samples have been previously analyzed by Alpha k)K �Q, / SAMPLE HANDLING Other Project Specific Requirements/Comments/Oetection Limits: �`1f ,�'�\.•� FirMarton O Done O Not needed O Lab to do Preservation rAl{'Wf1 L6 IQ / O Lab to do Sample ID Collection Sample Sampler's a ! / lrnene.wdry W*,) Date Time Matrix ample SpeGRc Comments set x 3--- /L:eo -Ave. x .Q x n-4�14 C IftA C W :QO Seo� 5 Et[ X • r ZOO 1 .1 -lzU SE C v .J a, -. ........_:_._..................- __........._.............,.........._-.....-..._._.__.....__...................._ ,_.._...........— -- .,._.._ ___.._._....._..,.�`- ...._ _ .. - - _..........-.._....._........ .._.._....---..... PLEASE ANSWER QUESTIONS ABOVEt Container Ty e oP, ae)p�Tr1t1, eaH Ce 1 co ... Preservative •G y L p ea`ca rio{'h�t o9�� IS YOUR PROJECTcri �dt n o d e oYJiTr� Relinquished By: Datemme y " 9 s MA MCP or CT RCP? Reoeivede : oatemme a rJh1 tJe a I a ea a e�s s ainitted a s td R 's er. a bond tl'cS� . ORM NO:01-01(rev.14-OCT-07) Ltx t t Il CHAIN �Av� OF CUSTODY PAGE OF F n to A VVESTBORO,MA MANSFIELD,MA • • •• • • •_ TEL 50"93-9220 TEL: $08422.9300 FATc'50ae98-e193 F,vc: 508422-3288 Project Name:ca'-_s p �t /� � O FAX Q EMAIL O Same as Client info PO#: . Project Location:wg{ c� 6� �A ❑ADEx ❑Add1 Deliverables Client: � • •.aa Project Pro #: I rr?t _n BC t'ar�� j 14/ 9 o j o r Slate/Fed Program Criteria ; Address:Pp lDox O b SiD 0,a s/ Project Manager: ALPHA Quote#: -14 Phone: r� r CaSa ❑Yes O No Are MCP Analytical Methods Required? Fax: ❑Yes O No Are CT RCP(Reasonable Confidence Protocols)Required? ❑Standard O RUSH" Emall: 5Kf a;hoan Y$I Cprr'n,e�.+ nee�� -O "ate Due: • . ElThese samples have been previously analyzed by Alpha 515)6�, Time: f / SAMPLE HANDLING / Other Project Specific Requirements/Comments/Detection Limits: IF11fretion__ 0� � ❑Done V O Not needed �-► / 0 Lab todo Preservation AINab I O Lab to do fL. , s Collection Sample Samplers / i�••••+o•a"vo•I�n ( a e�7nly� Sample ID Date Time Matrix Initials Sample Specific Comments 49 z, s s I st/(- k •x T'r :.�ix�la w yr PLEASE ANSWER QUESTIONS ABOVEI Container Type I ' P A 01"I 001Preservative MI pl srgIS YOUR PROJECTd4lll': Relinquished By: DateMme Received By: Date�me to MA MCP or CT RCP? +'q`II pee ue, iEt (asiij ato ORM N 01.01(rev,14:pCT_07) --•— —f — __ �7 y. _ � NO,. e arse sfd , CHAIN OF CUSTODY PAGE OF • .s6• eY^eMy r WESTBORO.MA MANSFIELD•MA Froject,infor,maiion •o • �. • }•• TEL: 60&890.9220 TEL $08422-9300 - FAX: 50&SWID193 FAX.50"2s-32e9 Project Name: 0 FAX p EMAIL O Same as Client Into PO#:___.._-___.-._._ _.P : _ - -- __ -- _._..__—-•------------....._.--- ---------- ' Project Location: O ADEx Q Add'I Deliverables _ _- /7zA_.__ Clent: jQ Project#: Regulatory ' _-_.� r►�`_'�•k l:3 in�C6r.�-'----•----- l�l i 9ClO J Stare/Fed Program Address: Cr/terfa ' (?Q.� /oat qV �,t(,dV Project Manager. 4a ke L,t 10. IWA ALPHA Quote#: Phone: UC:?�U • w Q Yes 101 Q No Are MCP Analytical Methods Required? Fax. SCE Q Yes O No Are CT RCP(Reasonable Confidence Protocols)Required? Standard .O RUSH Email: ra�romen,a"p..ppr.wa) SIG ro i��.n se� � .'ra•+EC�inC,gr^.'n ,0 8(� Date pue:5�s,O Time: w y Q These samples have been previously analyzed by Alpha SAMPLE HANDLINGV Other Project Specific Requirements/Comments/Detection Limits: n R' Filtration }� Q Done O Not needed Lab to do Preservation AL,}4A4fab I• ,,� 0 Lab to do ( e{ I Sample ID Collection Sample Sampler's, - (PUS .P.OYW—� Date Time Matrix Initials / Sample Specific Comments g' S_ A60 56it K z I� N1U 5 / --- - - __-.---- --------- -- --._`t r..__. ri o S•,I �c, r z Ih ° V4. {3G 6A C_a ?.63! _A /r �lh3t So,j 56r� X 8, 7------ ....... 14 PLEASE ANSWER QUESTIONS ABOVEI Container Type o a Preservative 'r— y a IS YOUR PROJECT Relinquished By: DateMme Received By: DateRme MA MCP or CT RCP? 3'•i8 av iiu�,. :.,/ �—__ y P�Q �• j r :m�� � ro0 9 - FORM NO:W-01(rev.14.00T-07) - — ------ 2'I�'_, _ • iG�e, Sample Delivery Group FOPM LaboratoryJob No: 8'bs�l� . Wrw-- Client. L'1'itCYZa�(t'TA Receipt DatelTime: r7 I ICP� I [oiJ SDG Reviewer: 1 `T Samples Delivered B : J�Vlpha Courier [ J Client ( ] UPS ( ] FedEx [ ]Other Bill of Laden:[]Yes[J Unavailable Tracking M Chain of Custodresent [ ]Absent: Custody Seals: absent ( j Presentlintact [. J Present/Broken j Cooler/Sample Temperature: I e/Bl a Ice present? �4Yes []No ( j N/A Temp taken from: Temp Blank.-(a) Lev (b) a'�`L(c) (d) (e) IR Gun: (a) Z°4(— (b) (c) (d) (e) Was Temp: Celsius ] <2 Celsius ...were samples frozen upon receipt? []Yes []No [ ] >6 Celsius ...were samples delivered direct from site? [J Yes [ ]No Containers Received: �L,94ntact [ ]Broken/Leaking Sample IDs: Sam le IDs: , I All Containers Accounted For? Extra Samples Received"o [ ]Yes: i Do Sample Labels and COC agree?-��Yes [ ]No: Are Samples in Appropriate Containers?,H>Yes [ ]No: Are samples rec'd within holding time?$1Yes [ J No. `Please note:the analysis of pH will always be performed beyond the regulatory-required holding time of 15 min.from the time of co4ection. FChlondne ples upon receipt: [ ]N/ [ J>12 and/or�[�] - 4m r r c npr . s properly preserved? [ ]Yes [ ]No If No then initial preserved In-House with[]HCL []HxSO 4 [J HNO3 (]NAOH<<Final pH= >> Bay'� , j sSW,V)W-keck. /A Present f j Absent S LO Q�o r n } A((Z rd cl rn be r rec 0 rn trn vole v u -- 4QDrJpry erV - VOAlVP H vials: [ ]Yes,L4VD CEO e KfrA VD I to l U . Aqueous:vials contain h a� d space?[ ]No [ ]Yes: Soils: McOH covering soil?[ ]Yes f ]No: Reagent H2O Preserved vials Frozen @ date/time: Frozen by Client?[ ]No[ J Yes @ date/time: Was Client notified.of any discrepancies fisted above? [ ]Yes [ ]No ( J NIA If Yes: Call Tracker# Form No.:01-02 4?0/Of5/2 07 Sample Receipt Checklist Page +r of Client: �-P(4` Receipt Date: Oy Project: pri M Q Log-in Date: ETR#: $v Lf I Inspection by: Login by:ir— ALL SECTIONS BELOW MUST BE COMPLETED Comments/Notes Were samples shipped? Yes,_FedEx_L_._.I.1.PS/ Other: o, Alpha Analytical Courier pick-u _/ and delivered Sample storage refrigerator#: tr 2 Is bill of lading retained? Yes, Tracking#: Sample storage freezer#: No,Unavailable / Number of coolers received for this project delivery: Indicate cooler temperature upon opening(if multiple coolers,record all temps): Cooler 2: Cooler 3: Note: If all coolers are 2-6°C,use one checklist,if NOT,use separate checklists and note all samples received above 60C Cooler 4: Cooler 5: Cooler 1: 0 Cooler 6: Cooler 7: Temperature(s)taken from: `7 IR Gun,(Circle one)SN(60647143 r 94031 —Temp.Blank, / NA More: Were min les received on ice? Yes / No Chain-of-Custody present? Yes / No Complete? es / No Custody seals present on Cooler? Yes /OD on Bottles? Yes /k hIc( Intact? Yes / No Note:AITLx custody seals to back o this a Were sample containers intact? / No If No, list samples: i Did VOA/VPH waters contain headspace(>5mm)?Yes/ No, N)f Yes, list samples:4 Were 5035 VOA soils,or VPH soils,covered with McOH? Yes / No / N If No,list sam � Was a su cient amount of sample received for each test indicated on the COC? j es / No If No,list samples: 4 If chemical preservation is appropriate- Chemical preservation OK for ALL Were samples field preserved? Yes / No / NA samples? ❑C=HC1 . ❑ M=MeOH ❑S=H2SO4 Yes / No / /A ❑H=NaOH ❑ N=HNO3 ❑ Other: ❑ U=Unknown If No,list samples below: Preservation(pH)verified at lab for EVERYbottle?(Not-VOA/VPH/Sulfide) YES: <2 or >12(CN) or NO 1A If No,why?: �--� Were samples received within hold time. Yes / No If No,.list samples: a Discrepancy between samples rec'd&COC? Yes / o. If Yes,lists les: 4 Was the Project Manager notified of any other problems? Yes / No/ A' Project Manager Acknowledgement: Date: 41251 Please use back for any additional notes! Form No.: 101-04 Alpha Analytical,Inc. 0411712008 Mansfield,Massachusetts 44 Of 45 i A. f Certificate/Approval Program Summary Method numbers assume the most recent EPA revisions.For a complete listing of analytes for the referenced methods please contact your Alpha Woods Hole Lab Project Manager or the HAQuality Assurance Manager. Connecticut Department of Public Health Certificate/Lab ID : PH-0141 - Wastewater(General Chemistry: EPA 120.1, 150.1, 160.1, 160.2, 180.1,300.0,310.1,335.2;Metals:200.8,245.1;Organics: 608-PCB, ETPH) Solid Waste/Soil(General Chemistry: 1010,9010/9014,9045,9060;Metals: 6020,7470,7471;Organics:_ 8081, 8082,8260, 8270,ETPH). Florida Department of Health Certificate/Lab ID: E87814-Primary NELAP Accreditation Authority for Air& Emissions.Secondary NELAP Accreditation for Wastwater and Solid&Hazardous Waste. Wastewater (General Chemistry: EPA 120.1/S:M2510B, 150.1, 160.1/SM2540C, 160.2/SM2540D, 180.1,300.0,335.2, SM2320B, SM234013,SM2540G,SM4500NH3;Metals: 245.1.;Organics: 608-PCB).Solid and Hazardous Waste(General Chemistry: 9010/9014,9045,9050,9056,9065,Reactivity 7.3; Metals: 6020,7470,7471;Organics: 8081,8082, 8260,8270). Air&Emissions (Organics:EPA TO-15). Louisiana Department of Environmental Quality Certificate/Lab ID :03090-Primary NELAP Accrediting Authority for Wastewater,Solid&Hazardous Waste.Wastewater(General Chemistry: EPA 120.1/SM2510B, 150.1, 160.1/SM2540C, 160.2/SM2540D, 180.1,300.0,310.1/SM2320B,335.2,376.2,9010/9014,9056, SM2540G;Metals:200.8,245.1, 6020;Organics: 608-PCB, 8015-DRO, 8081, 8082,8260,8270). Solid and Hazardous Waste(General Chemistry: 1010, 1311,9010/9014,9040,9045,9056,9066,Reactivity 73;Metals:6020, 7196,7470,7471;Organics: 8015-DRO, 8081, 8082, 8260, 8270). Maine Department of Human Services Certificate/Lab ID : MA0030- Wastewater (General Chemistry:EPA 120.1/ SM251013, 160.1/SM2540C, 160.2/SM2540D,300.0,310.]/SM2320B,335.2; Metals:EPA 245.1;Organics: 608-PCB). Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA030- Wastewater (General Chemistry:EPA 120.1/SM2510B, 150.1, 160.1/SM2540C, 160.2/SM2540D,300.0,310.1/SM2320B,335.2;Metals: EPA 245.];Organics: EPA 608-PCB). New Hampshire Department of Environmental Services Certificate/Lab ID:2206-Secondary NELAP Accreditation. Wastewater (General Chemistry: EPA 120.1/SM2510B, 150.1, 160.1/SM2540C, 160.2/SM2540D, 180.1,300.0, 310.1/SM2320B,335.2,376.2,SM2540G; Metals: 200.8,245.4;Organics: 608-PCB). New Jersey Department of Environmental Protection Certificate/Lab ID: MAO 15- Secondary NELAP Accreditation. Wastewater(General Chemistry: EPA 120.1/SM25IOB, 150.1, 160.1/SM2540C, 160.2/SM2540D, 180.1,300.0, 310.1/SM232013, 335.2,376.2,9010/9014,9056, SM2540G;Metals: 200.8,245.1 6020;Organics: 608-PCB,8081, 8082, 8260, 8270).Solid&Hazardous Waste(General Chemistry: EPA 1010, 1311,9010/9014,9040,9045, 9056,9060;Metals: 6020,7196,7470, 7471;Organics: 8015-DRO, 8081, 8082, 8260,8270). Air&Emissions (Organics: EPA TO-15). New York Department of Health Certificate/Lab ID : .11627-Secondary NELAP Accreditation. Wastewater (General Chemistry: EPA 120.1/SM251013, 150.1, 160.1/SM2540C, 160.2/SM2540D,300.0,310.1/SM2320B,376.2; Metals: 200.8,245.1;Organics: 608-PCB). Solid and Hazardous Waste(General Chemistry: EPA 1010, 1311; : 200.8,0930L, 041;Organics: 8081, 8082, 8260, 8270). Air&Emissions (Organics: EPA TO-15).. Rhode Island Department of Health Certificate/Lab ID : LA000289-Chemistry: Organic and Inorganic in Non- Poratable Water, Wastewater/Sewage and Soil (Refer to LADEQ and MADEP certificates for method numbers.) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-02089-Registered laboratory U.S.Army Corps of Engineers Department of the Navy 320 Forbes Blvd Mansfield, MA 02048, (508)822-9300, Far(508)822-3288 45 of 45 TABLE 1 SUMMARY OF SOIL ANALYTICAL RESULTS FOR SOIL SAMPLES COLLECTED ON APRIL 17,2008 WITHIN SHEPHERDS WAY,SCUDDER LANE AND CALVES PASTURE LANE,WEST BARNSTABLE,MA .. METHOD 1 MCP STANDARDSF 7 Soil Sample Identification ANALYSIS UNITS S-1/GW-4` S-1/GW-2 S-1/GW-3 INFILTRATOR -' COMP.1 COMP 2 COMP 3 COMP 4 BG-1CP BG-2SHEP MH-1 SED/INL-1 WL-2 WL ROAD/ ' STANDARD STANDARD STANDARD � CLEAN OUT x. SHOULDER 4 TOTAL PETROLEUM HYDROCARBON 8100M - TPH m /k -- PPm , 1,000 1,000 1,000- ---- ---- 569' 30.1 26.6 6 ---- EXTRACTABLE PETROLEUM HYDROCARBONS EPH . F " C9-C18Ali hatics •m /k m 1,000 1,000 1;000 <68:73 <70.2" - <9.01 <6.94 <7.66 <7.'18.0 <177 ' - 58 " <18.0 25.6 <9.39 ' C19-C36 Ali hatics m /k m .3,000 3;000 3,000 3 300 747 1,270 454.. 33.9 12.3. <7.66 <7.58 <18.0 19.3 31.5 C11-C22 Aromatics m /k m 1,000 1,000 1,000 528 240 86.7 369, 15.3 <6.94 <7.66 <7.58 23* 37.9 17.4. POLY CYCLIC AROMATIC HYDROCARBONS EPH Acena hthene m /k m - 4 1,000 1,000 -<1.37 <0.281 <0.031' <2.84' <0.036 <0.028 <0.031 <0.030 <0.072 <0.035' <0.038 Acena hth lene -fi /k m 1 600 10 <1.37 <0.281. <0.031 <2.84 <0.036 <0.028 <0.031 <0.030 <0.072 <0.035 <0.038 Anthracene m /k m 1,000 1,000 1,000 <1:37 <0.281 <0.031 <2.84 <0.036 . <0.028 <0.031. <0:030 <0.072 <0.035 <0.038 Benz a Anthracene nn /k rn 7. 7 7 1.93 1.16 - <0.031., <2.84 <0.036 <0.028 <0.031 <.0.030 <0.072 <0.035 0.044 Benzo a P rene m /k ppm 2 2 2 J Z4 0.943 <0.031 <2.84 -<0.036 '` <0.028 <0.031 <0.030 <0.072 <0.035 <0.038 Benzo b Fluoranthene m /k m 7 7 7 -1.70° `-0.702 <0.031 <2.84 0.037 <0.028 <0.031 <0.030 <0.072 <0.035 0.045 Benzo(g,h,l)Perylene nn 7k m' 1,000 1,000 _ 1,000 <1*37 0.653 <0.031 <2.84 <0.036 <0.028 <0.031 <0.030 <0.072 <0.035 <0.038 Benzo k Fluoranthene m /k m ` 70 70 Y 70 <1.37 1'.02 <0.031 <2.84 <0.036 <0.028 <0.031 <0�.030 <0.072 <0.035 <0.038 Chrysene m /k m 70 70 70 1.71. 0.944 <0.031 " <2.84 <0.036 <0.028 <0.031 50.030 <0.072 <0.035` 0.047 Dibenzo a h Anthracene _ m /k ppm 0_7 0_7 0_7 <1.37 <0.281 <0.031 <2.84, <0.036 <0.028. <0.031 . - <0.030 <0.072 <0.035 " <0.038 . Fluorant mg/kq(ppnn) 1,000 1,000 1,000 Fluorenehene m /kgj m `1000 1,000 1 000 <1637 <0.281 <0.031 <2.84 0060 036 _ <0.028 <0.031.031 c0.030 <0.072 <0.035 0.110 - • 5.03 055 030 <0.072 <0.035 <0.038 Indeno 1,2,3-cd P rene m /k m 7 7 7_ _. <1:37 0.575 <0.031 <2.84 <0.036 <0.028 <0.031 <0`030 <0.072 <0.035 <0.038 Naphthalene m /k m 4 40 500 <1.37 <0.281 <0.031 <2.84 <0.036 <0.028 <0.031 <0:030 <0.072 <0.035 <0.038 Phenanthrene m /k m 10 500 500 1.42 0.566 <0.031 <2.84 . <0.036 <0.028 <0.031 <0.030 <0.072 <0.035 0.057 Pyrene m /k m, 1,000 1,000 1,000 2.92 1.52 0.041 4.10 0.049 0.042 <0.031 :<0:030 <0.072 <0.035 0.077 2-Methyl na hthalene m /k m 0_7 80 300 <1.37 <0.281 <0.031 <2.84 <0.036 <0.028 _ <0.031 <0.030 <0.072 <0.035 <0.038 GENERAL CHEMISTRY - Total Solids % ,NSS NS NS 97 95 87 94 -74 -'_ 96 87 88 37 77 71 NS "---- ---- -=- 2.5, 1.2 ---- - TOTAL ORGANIC CARBON* % NS :: NS ---- - .____ ____ ____ ____ NOTES: E 1 MCP-Massachusetts Contigency Plan Supplemental"Clean"Version,Effective February 14,2008 . 2--Not Analyzed. 3<68.7-.Parameter was not found above the detection limit of 68.7. 4 Bold and underlined values exceed MCP Standards. 5 No Standard *Analysis run in duplicate,higher value reported here. Generated by VH 5/2/08 Pagel of 2 PRIME ENGINEERING,INC. QA'd Data and Standards by ESW 516/08 y `; 3 TABLE 1 SUMMARY OF SOIL ANALYTICAL RESULTS FOR SOIL SAMPLES COLLECTED ON APRIL 17,2008 WITHIN SHEPHERDS WAY,SCUDDER LANE AND CALVES PASTURE LANE,WEST BARNSTABLE,MA 1. METHOD 1'MCP STANDARDS Soil Sample Identification ANALYSIS UNITS S-1/GW-1 S-1/GW-2 S-1/GW-3 ::B:-23� SB-24 ED BACK SED BARN B-32 BG 6A BG RAWSTANDARD STANDARD STANDARD WL-5HINCK HARBOR 2656 RTE 6A CB 2631 WL 2615 STOCKPILE PRODUCT TOTAL PETROLEUM HYDROCARBON(8100M) TPH m /k m 1,000 1,000 1,000 ---- ---•* ---- ---- ---- ---- 4.460 ---- 22.300 1.0 00.000 EXTRACTABLE PETROLEUM HYDROCARBONS EPH C9-C18 Ali hatics m /k m 1,000 1,000 1,000 <8.66 <35.5 <37.0 <12.3 <8.23 <43.3 <13.3 <45.7 ---- 4,390 C19-C36 Ali hatics m /k m 3,000 3,000 3,000 <8.66 116 145 21.7 <8.23 65.5 59.6 211.0 716,000 C11-C22 Aromatics m /kg(ppm) 1,000 1,000 1,000 <8.66 83.3 40.0 32.2 <8.23 51.2 34.4 153.0 - 51,400 POLY CYCLIC AROMATIC HYDROCARBONS(EPH) s Acena hthene mg/kg_(ppm 4 1,000 1,000 <0.035 <0.284 <0.148 0.050 <0.033 <0.173 <0.053 <0.183 ---- <4.00 Acena hth lene m /k m 1 600 10 <0.035 <0.284 <0.148 0.056 <0.033 <0.173 <0.053 <0.183 <4.00 Anthracene mg/kg( m) 1,000 1,000 1,000 <0.035 <0.284 <0.148 0.192 <0.033 <0.173 <0.053 0.389 <4.00 Benz(a)Anthracene mg/kg(Ppm) 7 7 7 <0.035 <0.284 <0.148 0.864 <0.033 0.268 <0.053 1.44 --- <4.00 Benzo a P rene m /k m 2 2 2 <0.035 <0.284 <0.148 0.610 <0.033 0.255 <0.053 1.98 ---- 0.00 Benzo b Fluoranthene m /kg(ppm 7 7 7 <0.035 <0.284 <0.148 0.562 <0.033 0.321 <0.053 1.78 - <4.00 Benzo ,h,l Pe lene m /kg_( m) 1,000 1,000 1,000 <0.035 <0.284 <0.148 0.368 <0.033 0.196 <0.053 1.32 -- <4.00 Benzo k Fluoranthene mg/kg(ppm) 70 70 70 <0.035 <0.284 <0.148 0.695 <0.033 0.207 <0.053 2.12 - <4.00 Chrysene m /k m 70 70 70 <0.035 <0.284 <0.148 0.823 <0.033 0.304 <0.053 1.90 ---- <4.00 Dibenzo a h Anthracene m /kg(ppmL 0.7 0.7 0.7 <0.035 <0.284 <0.148 0.103 <0.033 <0.173 <0.053 0.231 --- 0.00 Fluoranthene m /kg(ppm) 1,000 1,000 1,000 <0.035 <0.284 <0.148 2.67 <0.033 0.592 0.084 3.49 ---- <4.00 Fluorene mg/kg_(ppnn) 1000 1,000 1,000 <0.035 <0.284 <0.148 0.125 <0.033 <0.173 <0.053 <0.183 ---- <4.00 Indeno 1,2,3-cd P rene m /k -M_ 7 7 7 <0.035 <0.284 <0.148 0.360 <0.033 <0.173 <0.053 1.06 ---- <4.00 Naphthalene m /kg_(ppm) 4 40 500 <0.035 <0.284 <0.148 0.063 <0.033 <0.173 <0.053 <0.183 <4.00 Phenanthrene mg/kg(ppm 10 500 500 <0.035 <0.284 <0.148 1.83 <0.033 0.221 <0.053 1.94 ---- <4.00 rene mg/kg_(ppm) 1,000 1,000 1,000 <0.035 <0.284 <0.148 1.71 <0.033 0.446 0.073 2.56 ---- <4.00 2-Meth Ina hthalene mg/kg (ppm) 0_7 80 300 <0.035 <0.284 <0.148 <0.049 <0.033 <0.173 <0.053 <0.183 ---- 0.00 GENERAL CHEMISTRY Total Solids % NSS NS NS 77 94 90 54 81 77 50 73 ---- ---- TOTAL ORGANIC CARBON* % NS NS NS 0.75 --- --- 2.1 0.07 ---- --- 2.5 ---- ---- NOTES: 1 MCP-Massachusetts Contigency Plan Supplemental"Clean"Version,Effective February 14,2008 2--Not Analyzed. 3 <68.7-Parameter was not found above the detection limit of 68.7. 4 Bold and underlined values exceed MCP Standards. 5 No Standard "Analysis run in duplicate,higher value reported here. Generated by VH 5/2/08 QA'd Data and Standards by ESW 5/6/08 Page 2 of 2 PRIME ENGINEERING,INC. ,